NCS000537_COMPLETE FILE - HISTORICAL_20100514

NORTH CAROLINA
Department of Environmental Qual

STORMWATER DIVISION CODING SHEET
RESCISSIONS
PERMIT NO. /Jcsc) D053q
DOC TYPE
DATE OF
RESCISSION
COMPLETE FILE - HISTORICAL
� o2,n l 0 OS/'f
YYYYMMDD

Patterson, Robert
From: Patterson, Robert
Sent: Friday, May 14, 2010 10:09 AM
To: '[e-mail]'
Cc: Nisely, Myrl
Subject: Stormwater Permit - Snipes Brothers Oil Company, Inc. - Person County
Steve,
Here is the information 1 spoke to you about on the phone today. Once I hear back about refunding the application fee
you submitted with the individual application, I'll let you know. When you submit your NOI for coverage under NCG08,
please include a note stating you want to withdraw your individual permit application and instead apply for NCG08.
The NO], permit text, and other relevant information regarding NCG080000 can be found here:
http://portal.ncdenr.org/web/wq/ws/su/npdessw#General_Permits_NPDES
Let me or Myrl know if you have any questions.
Thanks.
Robert D. Patterson, PE
Environmental Engineer
NCDENR I DWQ I Stormwater Permitting
1617 Mail Service Center, Raleigh, NC 27699-1617 lmnjii
512 N. Salisbury St, Raleigh, NC 27604 1 9th Floor il.ockirio, & 1,.arcelsi
[phone] I'll! my 1 [phone] V. i:<
I. mo i 1. robert. patterson(u�ncdenngov
%V(•l),dii•: http//portal.ncdenr.org/web/wq/ws/su
ABefore printing this email, please consider your budget and the environment.
'I you must print, please print only what you need and save ink with the free Eco-Font.
Email correspondence to and from this address maybe subject to the North Carolina Public Records Law and maybe disclosed to third parties.

Qualitative Monitoring Summary
Date
Location
Rainfall
Color
Odor
Clarity
Floating Solids
Settled Solids
Suspended Solids
Foam
Oil Sheen
Other
9/5/2008
Storm 1
2
light Brown
NIA
Clear
NIA
Satisfactory
Satisfactory
NIA
N/A
9/5/2008
Storm 2
2
light Brown
NIA
CLEAR
NIA
Satisfactory
Satisfactory
NIA
NIA

Staff Report May 13, 2010
To: Robert Patterson
From: Myrl Nisely Q
7
Through: Danny S i py to Barry Herzberg
Subject: Snipes B thers Oil Co., Roxboro
Stormw ter Permit Staff Report
Person County
A site visit was made May 6, 2010 by Autumn Romanski and Myrl Nisely. Mr. Steve Barnwell, Vice
President of Snipes Bros. was also present. Autumn and I believe that NCG08 is the apj2rgLnate
Permitting mechanism for this facility. The following points were observed:
The site visit identified several devices and practices posing potential sources of stormwater
contamination that can readily be changed. Mr. Barnwell agreed they will be modified or removed.
These are:
• disable the "hold open" device on the gasoline fueling pump on the north side of the site
• remove two inactive fueling hoses/nozzles at the loading platform in the center of the drive-in
area. This will reduce the activities at this platform to bulk loading via overhead lines.
• move a used -oil collection tank under roof, and start an inventory record along with archival of
shipping manifests when this oil is picked up by a recycler.
• fully decommission an idle fuel pump serving an abandoned mineral spirits tank. This tank has
not been used in a long time but may have some water in it. The tank will be certified to be
empty, and will not be put to any use in the future. We find it acceptable to just leave it in
place.
• about ten old residential fuel oil tanks stationed along the east fence will be taken from the site
• discard a stack of old wooden pallets
Operating Practices
• Tank inventories are made daily
• New oils of various kinds are stored in 55 gallon drums under a lean-to shed. These are
emptied gradually in the process of filling customer orders, and then are sent to Burlington for
drum recycle
• Stormwater collected in an earthen containment dike serving 6 — 15,000 gallon tanks will be
carefully released to the new retention pond (planned to be located immediately next to the
dike). That pond will have a valve by which the contents can be again be carefully released.
• The stormwater retention pond is to be engineered by a North Carolina certified PE. Drawings
will be submitted to the Stormwater Permitting Unit for review to obtain an A to C letter.
Per a telephone conversation between Myrl and Robert, the SPU will contact Mr. Barnwell with
instructions to apply for the general permit. There is no existing permit to be rescinded.

Tabte 3
Subbasin (WBD-8 Nustber) 03020201
DWQ Subbasin
03-04-01
Assessment Unit Number Name
I !se
Use
Description
O.erall
Fntential Stressors Support
Support Reason for
ppa
Parameter IR
Collection Listfn�
Classification DWQ Subhasin Miles Acres
L atcgE'
Potential Sources Cattgon
Rating Rating
Interest Year
Year Calegon
Watershed
(WBD-10
Number) 0302020101
Flat River
Subwatershed (WBD-12 Number) 030202010101
North
Flat River
27-3-2 North Flat River
2
Aquatic Life
Supporting No Criteria Exceeded
Ecological/biological Integrity
2005 1
Fishcom
From source to Flat River
WS-Ill;NSW 03-04-01 16.4 FW Miles
Subwatershed (WBD-12 Number) 030202010102
South Flat River
27-3-3a South Flat River
3a
Aquatic Life
Not Rated Data Inconclusive
Ecological biological Integrity
2004 3a
Renthos
From source to SR 1009
WS-I11;NSW 03-04-01 3.0 FW Miles
27-3-3b South Flat River
'2
Aquatic Life
Supporting No Criteria Exceeded
I:cological/biological integrity
2005 1
FishCom
From SR 1009 to Flat River
WS-I II;NS W 03-04-01 14.2 FW Miles
Aquatic Life
Supporting No Criteria Exceeded
Ecological biological Integrity
2004 1
Renthos
Subwatersbed (WBD-12 Number) 030202010103
Deep Creek
27-34 Deep Creek
2
Aquatic Life
Supporting No Criteria Exceeded
Ecologicabbiological Integrity
2005 1
FishCom
From source to Flat River
WS-111;NSW 03-04-01 16.3 FW Miles
Aquatic Life
Supporting No Criteria Exceeded
Ecologicalfbiological Integrity
2005 1
Benthos
Subwatershed (WBD-12 Number) 030202010104
Lake Michie-Flat River
27-(1) NEUSE RIVER (Falls Lake below
5
Chlorophyll a Aquatic Life
Impaired Standard Violation
Turbidity
2006 2008 5
normal pool elevation)
Aquatic Life
Impaired Standard Violation
Chlorophyll a
2006 2008 5
From source (confluence of Eno River Arm of Falls Lake and
Nutrient Impacts
Water Supply
Supporting No Criteria Exceeded
Water Quality Standards Water
2006 I
Flat River Arm of Falls Lake) to 1-85 bridge
General Agricultwe/Pasture
Supply
WS-IV;NSW,CA 03-04-01 2,703.6 FW Acres
Land Clearing
MS4 NPDES
W WTP NPDES
Turbidity
General Agriculture/Pasture
Land Clearing
MS4 NPDES
WWTP NPDES

Soil Map—Edgecombe County, North Carolina
35' 53' 25•
35" 5T 20"
K%p Scuts: 11857 r ptirksd ooA aize (8.5' x 11') *hest,
N ttilelers
^, 0 S 10 20 30
Feel
0 25 50 100 150
35' 53' 20•
ifUSDA Natural Res,,m Web Soil Survey 12/14/2009
= Conservation Servil, National Cooperative Soil Survey Page 1 of 3

HUFFMAN OIL COMPANY, INC.
January 21, 2010
Certified Mail 7003 31100005 6949 1984
Return Receipt Requested
Mr. Cory Larsen
Stormwater Permitting Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Notice of Violation/ Notice of Intent to Enforce
NOV-2009-OC-0008
Snipes Bros. Oil Co. — Roxboro
Diesel Fuel Discharge
Person County
Dear Mr. Larsen:
F7;store
Please find enclosed as application for a stormwater permit EPA forms 1 & 2F, lab
results, two (2) maps, and a check for $860.00. 1 apologize for the delay in resubmitting
the forms; we did not receive the lab results until January 19, 2010.
Please contact me with any questions.
Sincerely,
1)11r�Oj'
Steve Barnwell
Operations Manager
Phone [phone] • Fax [phone] • P O. Box 730 • Burlington, NC 27216-0730

HUFFMAN OIL CO., INC.
12/22/09 122209
HUFFMAN OIL CO., INC.
A.O. BOX 730
BURLINGTON, N.C. 27216-0730
336-227-8881
12/22/2009 138795
Eight Hundred Sixty and 00/100 Dollars
NCDENR
DIV. WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
860.00
No. 138795
00 860.00
No. 138795
BssT � 1,2
Burlington, NC 531

✓F I

Piease print or type in the unshaded areas only,
IYC�•p�038�I �. r�rf�i-1� ��1
Form Approved. OMB No. 2040-0086.
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA I.O. NUMBER
1
"EPA GENERAL INFORMATION
J
F
I Consolidated Permits Program
D
GENERAL
(Read flee "General 1n irr ceour" heyiwe, furling)
r
, Is
LABEL ITEMS
GENERAL INSTRUCTIONS
tf a prepnnted label has been provided, affix it In the
designated space Review the mlormaaon Carefully, rl any of it
1. EPA I.D. NUMBER
Is incorrect, Cross through it and enler the correct data in the
appropriate Mkn area I)elow. Alen. d any of the prepnnied data
is absent (rho area is the left of the rabel space fcsrs the
III, FACILITY NAME PLEASE PLACE LABEL IN THIS SPACE information that should eppearl, please provide ft in the proper
fill-in ares(s) beiowp the label is complete and Correll. you
V. FACILITY MAILING
need not complete Items I. Ili, V. pad Vt (except VI-B which
ADDRESS
musf be completed regardless) Complete all items it no label
has been provided. Refer to the instructions for detailed item
Vt. FACILITY LOCATION
descriptions and for The legal aulhanzallons under which this
data is collected.
11. POLLUTANT CHARACTERISTICS
INSTRUCTIONS; Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must
submit this form and the supplemental form listed in the parenthesis following the question. Mark -X" in the box in the third column it the supplemental form Is attached. If
you answer "no" to each question. you need not submit any of these forms. You may answer "no" if your activity Is excluded from permit requirements; see Section G of the
instructions. See also, Section O of the instructions for definitions of bold-faced terms.
Mart
'K
Mar, ,)-
YES
Nn
rnaRr
AItACHEd
YEsL
rORte
AIFORU b
SPECIFIC QUESTIONS
SPECIFIC QUESTIONS
A. Is this facility a publicly owned treatment works which
results in a discharge to waters of the U.S.? (FORM 2A)
X
B. Does or wit[ this facility (either existing or proposed)
include a concentrated animal feeding operation or
aquatic animal production facility which results in a
discharge to waters of the U.S ? (FORM 28)
C. is this a facility which currently results in discharges to
�/
X
D. Is this a proposed facility (other than those described in A
waters of the U.S. other than those described in A or B
or 8 above) which will result in a discharge to waters of
above? (FORM 2C)
a
a
N
the U.S-? (FORM 2D)
A
E, Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this facility industrial or
hazardous wastes? (FORM 3)
X
municipal effluent below the lowermost stratum
X
containing, within one quarter mile of the well bore,
,t
a
x
underground sources of drinking water? {FORM 4)
G. Do you or will you inject at this facility any produced water
H, Do you or will you inject at this facility fluids for special
or other fluids which are brought to the surface in
processes such as mining of sulfur by the Frasch process,
connection wHh conventional oil or natural gas production,
X
solution mining of minerals, In situ combustion of fossil
X
Infect fluids used for enhanced recovery of oil or natural
fuel, or recovery of geothermal energy? (FORM 4)
gas, or Inject fluids for storage of liquid hydrocarbons?
(FORM 4)
w
15
t
1. Is this facility a proposed stationary source which is one
J. Is this facility a proposed stationary source which is
of the 28 Industrial categories listed in the instructions and
�(
X
NOT one of the 28 industrial categories listed in the
�/
X
which will potentially emit 100 tons per year of any air
instructions and which will potentially emit 250 tons per
pollutant regulated under the Clean Air Act and may affect
year of arty air pollutant regulated under the Clean Air Act
'1'
+'
or be located in an attainment area? (FORM 5)
and may affect or be located in an aftainment area?
(FORM 5)
III. NAME OF FACILITY
C
1 SKIP Snipes Brothers Oil Company
1NL,
IV. FACILITY CONTACT
A. NAME & TITLE (larf, first & title)
B. PHONE (urru , ride A ow)
J2c
S L eve Barnwell, ice Presi ent
(SA) I 2 7-8 B
Ifi1.
V. FACILTY MAILING ADDRESS
A. STREET OR P.O. BOX
3 P.O. Box 730
B. CITY OR TOWN
G STATE
D ZIP CODE
2 T216
al 5,
4
Bur ington
C
R
1,
Vt. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
e
5 6 6 Sou h Morgan Street
B- COUNTY NAME
Person
C- CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE (rJAn-,or)
]6'
R x o o
1 fC 1 12403
3
EPA Form 3510.1 (8.90) CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES 4-di it, in order of rior'
A. FIRST B.SECOND
1,-v,r,.a >,-s:.teu. gas deals r
(lk•ryr)
7
5989
,e +9
re r9
C. THIRD D_ FOURTH
7
,e If
,n ly
Vill, OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
g
Snipes Brothers Oil Company / Huffman Oil Company 0 YESso the owner?
❑ NO
C. STATUS OF OPERATOR (Enter the appr rf' beret wi,, rhr ,,rr..orrr hm , f '0&,,. ".+prrill }
O, PHONE (,ara „kte d
F =FEDERAL
M = PUBLIC (other rhau federal rx arWeJ
S=STATE
P
('T"'r ilv)
11111111
A (336) 227-8t381
P = PRIVATE O =OTHER (tfarrifV)
x
,e a ,a ,n a, In
E. STREET OR P.O. BOX
P.O.
ox 730
Ja 5r
F. CITY OR TOWN
G, STATE H. ZIP CODE
JIX. INDIAN LAND
Is the fscility located on Indian lands?
B
Burlington
NC
27216
❑ YES 0 NO
v
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDE5 t?ir�'hu ec ru Wa Su urrter
0. PSD Ate F,miuials cram Pea wscd Soarers
r
9 P
,e n +e >a
r.
9
r
N
se
u
n
u fio
B. UIC L•'nFluids
E. OTHER .t •rr p
r
I
(rtk'l'ifl')
su
9
,a
w
C. RCRA lfa:urr6rur liovrm
E. OTHER .r acri ''
L'
f
(Stk•llfl'J
9
R
9
30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the
location of each of its existing and proposed intake and discharge structures. each of its hazardous waste treatment, storage. or disposal facilities, and each well where it
injects fluids underground. Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements.
XII, NATURE OF BUSINESS(provide a brrei descri ion
Snipes Brothers Oil cMpany operates a liquified petroleum gas distribution business and bulk oil t,rtail
business on the property. The LPG business revenue Far exceeds bulk oil sales.
XIII. CERTIFICATION (see instructions)
I certify under penalty of few that I have personalty examined and am famifiar with the information submitted in this sppfication and all attachments and that, based on my
Inquiry of those persons immediately responsible for obtaining the information confairwd in the appficalion. I believe that the information is true. accurate, and comptate_ I
am aware that there are significant penalties for submitting false information, including the possibddy of fine and impffsonment,
A. NAME 3 OFFICIAL TITLE (flpear print)
B. SIGNATURE
C. DATE SIGNED
Steve Barnwell, Vice President
�[,�J1,
��•• ��
COMMENTS FOR OFFICIAL USE ONLY
I I
C
,e
1fi
EPA Form 3510-1 (8.90)

EPA ID Number (copy from Item 1 of Fomi 1) Form Approved OMB No 2040-0086
Please print or type in the unshaded areas only. I I Approval expires 5-31-92
U.S. Environmental Protection Agency
FORM Washington, DC 20460
ZFSOEPAApplication for Permit to Discharge Storm Water
NPDES Discharges Associated with industrial Activity
Paperwork Reduction Act Notice
Public reporting burden for this application is estimated to average 28.6 hours per application, including time for reviewing instructions. searching existing data sources,
gathering and maintaining the data needed, and completing and reviewing the collection of information. Send comments regarding the burden estimate. any other aspect
of this collection of Information, or suggestions for improving this form, Including suggestions which may increase or reduce this burden lo: Chief, Information Policy
Branch, PM•223, U.S. Environmental Protection Agency, 1200 Pennsylvania Avenue, NW, Washington. DC 20460, or Director, Office of Information and Regulatory
Affairs, Office of Management and Budget, Washington, DC 20503.
I. Outfall Location
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. Outfall Number
(list)
B. Latitude
C. Longitude
D_ Receiving Water
(name)
1 Ti'
30,00
L .00
59.00
94.0o
North Flat River
II. Improvements
A. Are you now required by any Federal. State, or local authority to meet any implementation schedule for the construction. upgrading or operation of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described In this application? This includes, but is not limited
to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
1. Identification of Conditions,
Agreements, Etc.
2. Affected Qutfalls
3 Brief Description of Project
4. Final
Compliance Dale
number
source of discharge
a. r
b. pro;.
B. You may attach additional sheets describing any additional water pollution (or other environmental projects which may affecl your discharges) you now have under
way or which you plan. Indicate whether each program is now under way or planned, and indicate your actual or planned schedules for construction
III. Site Drainage Map
Attach a site map showing topography (or indicating the oudine of drainage areas served by the outfallsis) covered in the application it a topographic map is unavailable)
depicting the facility including: each of its intake and discharge structures: the drainage area of each storm water outfall; paved areas and buildings within the drainage
area of each storm water outfall, each known past or present areas used for outdoor storage of disposal of significant materials. each existing structural control measure
to reduce pollutants in storm water runoff, materials loading and access areas, areas where pesticides, herbicides, soil conditioners and fertilizers are applied, each of
its hazardous waste treatment, storage or disposal units (including each area not required to have a RCRA permit which is used for accumulating hazardous waste
under 40 CFR 262.34): each well where fluids from the facility are injected underground; springs, and other surface water bodies which rsceived storm water discharges
from the facility.
EPA Form 3510.21' (1-92) Page 1 of 3 Continue on Page 2

Continued from the Front
IV. Narrative Description of Pollutant Sources
A, For each oudatl, provide an estimate of the area (mClude units) of Imperious surfaces tmdudin8 paved areas and buitding roofs) drained to the Curtail, and an estimate of the total surface area
drained by the outlay
Oudaa
Area of Impervious Surface
Toter Area Drained
Outran
Area of Impetuous Sudece
Total Area Oramed
Number
(provrda units)
(provide finds)
Number
(provide unds)
trwMIde unds)
Pl
�7,fj0` ft2
227.000 !`.2
B Provide a narrative description of significant materials that are currently or in the past three years have been treated, stored or disposed in a manner to allow exposure
to storm water; method of treatment, storage, or disposal; past and present materials management practices employed to minimize contact by these materials with
storm water runoff; materials loading and access areas, and the location, manner, and frequency in which pesticides, herbicides, soil conditioners, and fertilizers are
applied.
The outfall area includes bulk oil storage and miscellaneous storage items for bulk fuel sales. Storage areas within the
iiralnage area include: a diked above ground storage tank ato:a, fuel loading and unloadtng areas, and nr{uipment st'ot'arte,
C. For each outfall, provide the location and a description of existing structural and nonstructural control measures to reduce pollutants in storm water runoff; and a
description of the treatment the storm water receives, Including the schedule and type of maintenance for control and treatment measures and the ullimale disposal
of any solid or fluid wastes other than by discharge,
Outfall
List Codes from
Number
Treatment
Table 2F-1
01 Snipes Brothers Oil Company is in the process of constructing a retention basis on site to treat
atormwat.er.
V. Nonstormwater Discharges
A. I certify under penalty of law hat the outfall(s) covered by this application have been tested or evaluated for the presence of nonslormwater discharges, and that all
nonstormwalef discharged from these outfall(s) are identified in either an accompanying Form 2C or From 2E application for the outtall.
Name and Official Title (type or prrnf)
Signature
Date Signed
Steve tlatnwell. Vice Presidvnl
8, Provide a description of the method used, the date of any testing, and the onsile drainage points that were directly observed during a lest.
visual ❑baerVar:on8 during September 2009,
VI. Significant Leaks or Spills
Provide existing information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility in the last three years. Including the
approximate date and location of the spill or leak, and the type and amount of material released.
fuel spill ncrurred due ro a failure of a pipe nipple between an above ground storage tank located inside the r-nnrainmenr dike
And a water drain valve at the botrom of the tank. The pipe nipple failed afrer an empty 1000 gallon propane tank fell against
he water drain valve. The propane tank was sitting on top of the dike and slid into the dike sometime during the night July 11,
009 or early morning August 1, 2009. The dike drain valve was open and subsequently the product was abbe to drain from the
iiku.
ased on daily inventory records, approximately 2.67? gallons of diesel was released. Approximately 1,800 gallons reached the
rainage ditch and creek.
Wipes Brothers Oil Company personnel and an environmental contractor responded to -he release on Auguac Z, 2009. The stream
.as been restored.
EPA Form 3510-2F (1-92) Page 2 of 3 Continue on Page 3

Continued from Page 2 1
EPA 10 Number (copy from tram f of Form f )
VII. Discharge Information
A, B, C. & D: Bee Instructions before proceeding. Complete one set of tables for each outfall. Annotate the curtail number in the space provided.
Table VII-A, VII-B, VII-C are included on separate sheets numbers VII-i and VII.2.
E. Potential discharges not covered by analysis - is any toxic pollutant listed in table 2F-2, 2F-3, or 2F4, a substance or a component of a substance which you
currently use or manufacture as an intermediate or final product or byproduct?
❑ Yes (Fist alf such pollutants below) ❑ No (go to Section IX)
III. Biological Toxicity Testing Uata
Do you have any knowledge or reason to believe that any biological lest for acute or chronic toxicity has been made on any of your discharges or on a recelvinp water in
relation to your discharge within the last 3 years?
❑ Yes (list all such pollutants below) ❑ No (go to Section IX)
IX. Contract Analysis Information
Were any of the analyses reported in Item VI performed by a contract laboratory or consulting firm?
❑ Yes (lisf the name, address, and telephone number of. and pollutants
❑ No (go to Section X)
analyzed by, each such laboratory or firm below)
A. Name
B- Address
C. Area Code & Phone No
D. Pollutants Analyzed
Snipes Brothers W 1 company will
use a contract laboratory to
analyze stormwater samples.
SAME, Inc. is working with
Snipes nrcthcrs nil Company gn a
sampling sched,:lr.
X. Certification
l certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submdled Based on my Inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is. to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information. including the possibility of line and imprisonment for knowing violations.
A. Name & Official Tole ( type or print)
B. Area Code and Phone No,
Steve Barnwell, Vice President
(3361 227-8881
C. signature
D. Date ign
]]S
/ 01 � r?
EPA Fonn 3510-2F (1-92) Page 3 013

EPA ID Number (copy from Item 1 0l Form 1) Form Approved. OMB No. 2040-0086
Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A - You must provide the results of at least one analysis for every pollutant in this table Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composas
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
NIA
Demand(BOD5
Demaical d(BO 5)
lab analyses
to be completed
Chemical Oxygen
Demand (COD)
Total Suspended
Solids (TSS)
Total Nitrogen
Total Phosphorus
pH
Minimum
Maximum
Minimum
Maximum
Part B - List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit- Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Row -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
lab analyses
to be completed
for vat:e
EPA Form 3510-2F (1-92) Page VII.1 Continue on Reverse

Continued from the Front
Pan C - List each pollutant shown in Table 2F-2. 2F-3. and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfall.
Pollutant
and
CAS Number
(if available)
Maximum Valves
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
lab analyses
to be completed
Pan D - Provide data for the storm event(s) which resulted In the maximum values for the flow weighted composite sample,
1.
Date of
Storm
Fvenl
2-
Duration
of Storm Event
(in nrinufes)
3
Total rainfall
during storm event
(tn inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum now rate during
rain event
(gallonshninute or
specify units)
6.
Total flow from
rain event
(gallons or specify units)
to be completed
7. Provide a description of the method of flow measurement or estimate.
EPA Form 3510-2F (1-92) Page VII.2

1 1 i
N
r �
ti•
72A
r
r -
` ko #p, Drainage Ditches �
Dike
UST I'I
CanopyO l
Approximately 27,000 Sq. Ft I I O ET
Drainage Area u
78 59' 58" O 1}
36 23' 30" ASTs
' F
U
I�
Storrnwater Basin to
be Constructed I ;'
9 � 4
Outfall 01
Underground Stromwater Pipe
I h
` 50
N= Feet
Source' USGS topography provided y NCDOT GIS Department website
SCALE: As Shown
DATE. 11-1LSE S&ME
DRAWN BY: SE
PROJECT NO, A(WWV.
1584-09-041
k -1
Legend
Drainage Ar a
Topographic ntours
Surface Flow
FIGURE
SITE DRAINAGE MAP NO
SNIPES OIL 2F
616 S. MORGAN STREET
ROXBORO, NORTH CAROLINA

NOTE: NO �PUBLIC;WATERTAKE� LOCATED-WITHIN/,1y•,� L � •
MILE D©WNSTREAMPOF,1 DISCHARGE =
! Ifi�i.� - ;�- i�-,; r' (i • r�% f r lti�� r-s� ,` i �•' ��r +r -
y, ,r ,� /Jhel;�}(��`,'!% a�rf 1T 1 �;r•c'� G`-�a`'�a' ` `,; 1;1Z .,{; JZ
NO:HAZARDOUSWASTED:MANAG EMENT/FACIL'ITIES`
�I•;� \ -i + .�1•��,���" � � 1 � r . � �r � �� r try .�{
NOSKNOWN?DRlNKlNG WATER.WELL`S�WITHING'• MMILE.�
.:i� !f , • r L'-'�.y � �`f''i i t - y, ,. . �•-' »I� r � '.,��y . ,. �i 4, � �r ' ''rJ� if
��i ti s a• � i �C�' ``;` � S �4�i, ♦' .ff rf,�,� , r-..,��� ,�i• • __ � � 4 r J''' fr
~ �� r-y l � t �� I! � lf/ r1� \ - � . � fI �f .' �� , 1' f��i,, f _ � i •- �� Y` it /f !
��� � if �`� ` �� - � •} \'',��•
t r { �` =I�,;^ +r ••'�� �) Proposed Stormwater Basin
rR
1,
Nearest Surface Water Body
Outfall 01 r1
Discharge Point
V { t+Q, �1"7'r� ,I` `w.� ^i �, ~ r �` •^� r ►•fit};� r�``�``i r�
all
r � •' f� I �y`� � �l1 r
,,'r 4 r/f 1'�� .. .`-'�b• }�t � (.' ��- -•V •'' 1 k-✓�..J `n.5 r �ji 1 `1+ t _ �, �// � l .
'-. fi�tt,, r t���1 `�-' / ,..� � f � �`�, ♦'- � a I. �•
,_ �`��1, � � ,, �Y+' r.'I' �:T'.3���- .M_r' { �.�',.lt�'It� r � lllr. ,��* • t'�}�•'��•1".
__ �..=• r 9 �.1'r� va +�]~ r L- - � acv�/ f L l�� Y \` t { 1 �'r
�1! • y� - I '%r• l II _ 4 - r'�- ,ram 1 ! " ` �% ��jq�� �-'
r ~Surface Water. Flaw Direction
`� I � n ,� ( �;L " j f i 1�. i'_" 1 `--... r.,� --- •i � - RltliD'�� S 1 ';;•. /�i � I _ ��i � :,+ �\.1
Souroe: USGS topography provided by NCDOT GIS Department website
SCALE: I" = 2 000' RGURE
DATE: 9-8-09 USGS TOPOGRAPHIC MAP NO
DRAWN BY: JBP S&M E
SNIPES OIL
PROJECT NO, WWW.SMEINC.COM
1584-09-041 RDXBDRD NORTH CARDLINA

ace Analytical
wwwpacalabs.cam
January 19, 2010
Mr. Wayne Watterson
S&ME, Inc.
3718 Old Battleground Road
Greensboro, NC 27410
RE: Project: SNIPES 158409041
Pace Project No.: 9260247
Dear Mr, Watterson:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PacoAnalytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersviile, NC 2807E
Enclosed are the analytical results for sample(s) received by the laboratory on December 23, 2009,
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
cc: Wayne Watterson, 5&ME, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
A neh&
(704)B75.9092
Page 1 of 23

aceAnalytical
wwwpocotabs.com
Project: SNIPES 158409041
Pace Project No.: 9260247
Charlotte Certification IDs
9800 Kincey Ave. - Ste 100 Huntersville, NC 28078
West Virginia Certification #: 357
Connecticut Certification #: PH-0104
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
North Carolina Drinking Water Certification #: 37706
Paco Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #; 990060001
South Carolina Drinking Water Cert. #: 990060003
Tennessee Certification #: 04010
Virginia Certification #: 00213
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification IDS
2225 Riverside Dr. Asheville, NC 288D4
Pennsylvania Certification #: 68.03578
Connecticut Certification #: PH-0106
South Carolina Bioassay Certification #: 99030002
Louisiana/LEI-AP Certification #: 03095
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Tennessee Certification #; 2980
New Jersey Certification #; NC011
Virginia Certification #: 00072
North Carolina Bioassay Certification #: 9
West Virginia Certification M 356
North Carolina Drinking Water Certification #: 37712
Florida/NEL AP Certification #: E87648
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wniten consent of Pace Analytical Services, Inc..
Page 2 of 23
Sri"elac�

aceAnalytrcal`
wwwpecsfe6,t.cam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SNIPES 158409041
Pace Project No.: 9260247
Sample: STORMWATER Lab ID: 9260247001 Collected: 12/22/09 11:28 Received: 12/23/09 15:50 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Quai
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
ND mg/L
5.0
1
12/30/09 08:58
8270 MSSV Semivolatile Organic
Analytical Method: EPA
8270 Preparation Method: EPA 3510
Acenaphthene
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
63.32-9
Acenaphlhylene
NO ug/L
10.4
1
01/13/10 09:00
01115110 11:29
208-96-8
Aniline
NO ug/1-
10A
1
01/13/10 09:00
01/15/10 11:29
62.53-3
Anlhracene
NO ug/L
10A
1
01113110 09:00
01/15/10 11:29
120-12-7
Benzo(a)anthracene
NO ug/L
10A
1
01/13110 09.00
01/15110 11:29
56-55-3
Benzo(a)pyrene
NO ug/L
10-4
1
01113/10 09:00
01115/10 11-29
W32-8
Benzo(b)fluoranthene
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
205.99-2
Benzo(g,hJ)perylene
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
191-24-2
Benzo(k)fluoranthene
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
207-08-9
Benzoic Acid
NO ug/L
52.1
1
01113110 09:00
01115110 11:29
65-85-0
Benzyl alcohol
ND ug/L
20.8
1
01/13/10 09:00
01/15/10 11:29
100-51-6
4-Bromophenylphenyl ether
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
101-55-3
Butylbenzylphthalate
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
85-68-7
4-Chloro-3-methylphenol
NO ug/L
20.8
1
01/13/10 09:00
01/15/10 11:29
59-50-7
4-Chloroaniline
NO ug/L
52.1
1
01113/10 09:00
01/15/101129
106-47-8
bis(2-Chloroethoxy)methane
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
111-91-1
bis(2-Chloroethyt) ether
NO ug1L
10.4
1
01/13110 09:00
01/15/10 11:29
111-44-4
bis(2-Chloroisopropyl) ether
NO uglL
10.4
1
01/13110 09:00
01/15110 11:29
108-60-1
2-Chloronaphthelene
ND ug/L
10.4
1
01/13/10 09:00
01115110 11:29
91-58.7
2-Chlorophenol
NO ug/L
10.4
1
01/13/10 09:00
01115/10 11:29
95.57-8
4-Chlorophenylphenyl ether
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
7005-72-3
Chrysene
NO ug/L
10.4
1
Dill W10 09:00
01/15/10 1119
218-01-9
Oibenz(a,h)anlhracene
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
53-70-3
Dibenzofuran
NO ug/L
10.4
1
01113/10 09:00
01/15/10 11:29
132-64-9
1,2-Dichlorobenzene
N❑ ug1L
10.4
1
01/13/10 09:00
01/15/10 11;29
95-50-1
1,3-Dichlorobenzene
NO ug/L
10.4
1
0111311009:00
01115110 11:29
541-73-1
1,4-Dichlorobenzene
NO ug/L
10.4
1
0111311009:00
0111511011:29
106-46.7
3,3'-Dichlorobenzidine
ND ug/L
52.1
1
0111311009700
01115110li:29
91-94-1
2,4-Dichlorophenol
NO ug/L
10.4
1
01113/10 09:00
01/15/10 11:29
120-83.2
Diethylphtha late
ND ug/L
10.4
1
01/13/10 09:00
01115110 11:29
84-66-2
2,4-Dimethylphenol
NO ug/L
10A
1
01/13/10 09:00
01/15/10 11:29
105-67.9
Dimethylphthalate
ND ug/L
10.4
1
01/13/10 09:00
01/15110 11:29
131-11-3
Di-n-butylphthalate
NO ug/L
10.4
1
01/13/10 09:00
01/15/10 11:29
84-74-2
4,6-Dinitro-2-methylphenol
NO ug/L
20.8
1
01/13/10 09:00
01/15/10 11:29
534-52-1
2,4-Dinitrophenol
NO ug11-
52.1
1
01/13/10 09:00
01/15/10 11:29
51-28-5
2,4-Dinitrotoluene
NO ug/L
10.4
1
01/1311009:00
01/15/10 11:29
121-14.2
2,6-Dinitrotoluene
ND ug/L
10.4
1
01/1311009:00
01/15/10 11:29
606-20-2
Di-n-oclylphlhalate
ND ug/L
10-4
1
01/13/10 09:00
01115110 11:29
117-84-0
bis(2-Ethylhexyl)phihalate
ND ugiL
6.3
1
01/1311009:00
01115/1011:29
117-81-7
Fluoranthene
NO ug/L
10A
1
01113110 09:00
01/15/10 11:29
206-44-0
Fluorene
NO ug/L
10A
1
01113/10 09:00
01/15/10 11:29
86.73-7
Hexachloro-1.3-buladiene
ND ug/L
10.4
1
01/1311009:00
01/1611011:29
87-68-3
Hexachlorobenzene
NO ug1L
10.4
1
01/13/10 09:00
(11115/10 11:29
118-74.1
Hexachlorocyclopentadiene
ND ug/1-
10A
1
01/13/10 09:00
01/15/10 11:29
77-47-4
Date: 01/19/2010 05:01 PM
REPORT
OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..
- neb
Page 3 of 23

o
aceAnalyfical
»wwpecelsbs.com
Project: SNIPES 158409041
Pace Project No.: 9260247
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: STORMWATER Lab ID: 9260247001 Collected: 12122/09 11:28 Received: 12/23/09 15:50 Matrix: Water
Parameters Results units Report Limit OF Prepared Analyzed CAS No, Qual
8270 MSSV Samivolatile Organic
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenoi(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nilroaniline
4-Nitroanillne
Nitrobenzene
2-Nitraphenol
4-Nitrophenol
N-Mtrosadimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodtphenylamine
Pentachlorophenol
Phenanlhrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4 , 5-Trichlorophenol
2,4 ,6-Trichtorophenol
'Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 IVISV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bro mod! chloro methane
Bromoform
Bromomeihane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlarotoluene
Date: 01/1912010 05:01 PM
Analytical Method: EPA 8270 Preparation Method: EPA 3510
NO ug1L
10.4
1
01/13/10 09:00 01/15/10 11:29
67-72-1
NO ug1L
10.4
1
01/13/10 09:00 01115110 11:29
193-39-5
NO ug1L
10.4
1
01/13/10 09:00 01/15110 1129
7B-59-1
NO ug/L
10.4
1
01/13/10 09:00 01/15110 1129
90-12.0
NO ug1L
10,4
1
01113/10 09:00 01/15110 1129
91-57.6
NO ugIL
10.4
1
01/13/10 09:00 01/15/10 1129
95-48-7
NO ug/L
10.4
1
01/13/10 09:00 01115/10 11:29
ND uglL
10.4
1
01113/10 09:00 01/15/10 1119
91-20-3
ND ug1L
52.1
1
01/13110 09:00 01/15/10 11:29
88-74-4
ND ug1L
52.1
1
01113110 09:00 01/15/10 11:29
99-09-2
ND ug1L
52.1
1
01/13110 09:00 01/15/10 11729
100-01-6
ND ug1L
10.4
1
01/13/10 09:00 01115110 11:29
98-95-3
ND ug1L
10.4
1
01/13/10 09:00 01/15/10 11:29
88-75-5
ND ug1L
52.1
1
01/13/10 09:00 01/15110 11:29
100-02-7
ND ug1L
10.4
1
01/13/10 09:00 01115MO 11:29
62-75-9
NO ug/L
10.4
1
01/13/10 09:00 01/15/10 11:29
621-64-7
ND ug1L
10.4
1
01/13/10 09:00 01/15/10 11:29
86-30.6
ND ug/L
52.1
1
01/13/10 09:00 01/15/10 11:29
87-86-5
ND ug/L
10.4
1
01/13/10 09:00 0111511011:29
85.01-8
NO ug/L
10A
1
01/13/10 09:00 01/15110 11:29
108.95-2
ND ug/L
1OA
1
01/13/10 09:00 01/15110 11:29
129-00-0
NO ug/L
10.4
1
01/13/10 09:00 01115/1011:29
120-82-1
ND ug1L
IOA
1
01/13/10 09:00 01/15/10 11.29
95-95-4
ND ug1L
10.4
1
01/13110 09.00 01/15/10 11:29
86-06-2
44 %
30-150
1
01/13/10 09:00 01/15/10 11:29
4165-60-0
51 %
30-150
1
01113/10 09:00 01/15110 11:29
321-60-8
86 %
30-150
1
01113110 09:00 01115/10 11:29
1718-51-0
22 %
25-150
1
01113/10 09:00 01115/10 11:29
13127-88-3 SO
26 %
25-150
1
01/13/10 09:00 01/15/10 11:29
367-12-4
68 %
25-150
1
01/13/10 09:00 01/15/10 11:29
118-79-6
Analytical Method: EPA 8260
ND ug/L
25.0
1
01/04/10 18:38
67-64-1
ND ug/L
1.0
1
0110411018:38
71.43-2
NO ug/L
1.0
1
01104/1018:38
108-86-1
NO ug1L
1.0
1
01/04/1018:38
74-97-5
NO ug/L
1.0
1
0110411018:38
75-27-4
NO uglL
1.0
1
01 /04110 19:38
75-25-2
ND uglL
5.0
1
01104/1018:38
74-83-9
ND ug1L
5.0
1
01104/1018:38
78-93-3
NO ug/L
1.0
1
01104/10 18:38
56-23-5
NO ug1L
1.0
1
01/04/10 18:38
108-90-7
NO ug/L
1.0
1
0110411018:38
75-00-3
NO ug/L
1.0
1
01/0411018:38
67-66-3
NO ug/L
1.0
1
01/04110 18:38
74-87.3
NO ug/L
1.0
1
01/0411018:38
95-49-8
NO ug/L
1.0
1
0110411018:38
106-43-4
REPORT
OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.cce�
i neh .
Page 4 of 23

a
gnalytrca j
www.pacwabs.com
r
Project: SNIPES 158409041
Pace Project No.: 9260247
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Hunlersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Sample: STORMWATER
Lab ID: 9260247001 Collected: 12122l09 11:28 Received:
12123/09 15:50 Matrix:
Water
Parameters
Results
Units Report Limit
OF Prepared
Analyzed
CAS No, Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane
NO ug1L
3.0
1
01/0411018:38
96-12-8
Dibromochloromethane
NO ug1L
1.0
1
01/0411018:38
124-48-1
1,2-Dibromoethane (EDB)
ND ug1L
1.0
1
01/04/10 18:38
106-93-4
Dibromomethane
NO ug/L
1.0
1
0110411018:38
74-95-3
1,2-Dichlorobenzene
NO ug/L
1.0
1
0110411018:38
95-50-1
1,3-Dichlorobenzene
ND ug1L
1.0
1
01/04/10 18:38
541-73-1
1,4-Dichlorobenzene
ND ugIL
1.0
1
01/04/10 18:38
106-46.7
Dichlorodifluoromethane
ND ug/L
1.0
1
01/04/10 18:38
75-71-8
1,1-Dichloroethane
ND ug1L
1.0
t
01104/1018:38
75.34-3
1,2-Dichloroethane
ND ug/L
1.0
1
01/04/10 18:38
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
01/0411018:38
75-35-4
cis -1,2-Dichloroethene
ND ug1L
1.0
f
01/0411018:38
156-59-2
trans-1.2-Dichloroethene
ND ug/L
1.0
1
01/04/10 18:38
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
01104/1018:38
78.87-5
1,3-Dichloropropane
ND ug1L
1.0
1
01/04/10 18:38
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
01/0411018:38
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
01104/1018:38
563.58.6
cis- 1,3-Dichloropropene
ND ug1L
1.0
1
01/04/10 18:38
10061-C1-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
01/04/10 18:38
10061-C2-6
Diisopropyl ether
ND ug/L
1.0
1
01/04/10 18:38
108-20-3
Ethylbenzene
ND ug/L
1.0
1
01/04/10 18:38
100.41.4
Hexachioro-1,3-butadiene
ND ug/L
1.0
1
01/04/10 18:38
87-68-3
2-Hexanone
ND ug/L
5.0
1
0110411018:38
591.78.6
p-Isopropyltoluene
NO ug/L
1.0
1
01/04/10 18:38
99-87-6
Methylene Chloride
ND ug/L
2.0
1
01/04/10 18:38
75.09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
01/04/10 18:38
108-10-1
,Methyl-tert-butyl ether
3.0 ug/L
1.0
1
01/04/10 18:38
1634-04-4
Naphthalene
ND ug/L
1.0
1
01/04/10 18:38
91-20-3
Styrene
ND ug/L
1.0
1
0110411018:38
100.42-5
1,1,1,2-Tetrachloroethane
NO ug/L
1.0
1
011D4110 18:38
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
0110411018:38
79.34-5
Tetrachloroethene
1.7 ug/L
1.0
1
01/04/10 18:38
127-18-4
Toluene
NO ug/L
1.0
1
01/04/10 18:38
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
0110411018:38
87.61-6
1,2,4-Trichlorobenzene
NO ug/L
1.0
1
01/04/10 18:38
120-82-1
1,1,1-Trichloroethane
NO ug/L
1.0
1
01/0411018:38
71-55-6
1,1,2-Trichloroethane
NO ug/L
1.0
1
01/04/1018:38
79-00-5
Trichloroethene
NO ug/L
1.0
1
0 1 /04110 113:38
79-01-6
Trich lorofluo romethane
NO ug/L
1.0
1
01/04/10 18:38
75-69-4
1,2,3-Trichloropropane
NO uglL
1.0
1
01/04/10 18:38
96-18-4
Vinyl acetate
NO ug/L
2.0
1
01/04/10 18:38
108.05-4
Vinyl chloride
NO ug/L
1.0
1
01/04/10 18:38
75-01-4
m&p-Xylene
NO ug/L
2.0
1
01/04/1018:38
1330-20-7
o-Xylene
ND ug/L
1.0
1
01/04/10 18:38
95-47-6
4-Bromofluorobe nzene (S)
95 %
87-109
1.
01/04/10 18:38
460-00-4
Dibromofluoromethane (S)
104 %
85-115
1
01/04/10 18:38
1868.53-7
1,2-Dichloroethane-d4 (S)
100 %
79-120
1
01/04/10 18:38
17060-07-0
Date: 01119/2010 05:01 PM
REPORT OF LABORATORY
ANALYSIS
Page 5 of 23
This
report shall not be reproduced,
except in full,
without the
written consent of Pace Analytical Services, Inc..
�rielac�

acmnalytical®
wwwpocsfabs.crom
Project: SNIPES 158409041
Pace Project No.: 9260247
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Kuntersvl1ie, NC 2807E
[phone]
Sample: STORMWATER
Lab ID: 9260247001 Collected:
12/22/09 11:28
Received: 12/23/09 15:50 Matrix: Water
Parameters
Results Units Report Limit
OF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Toluene-d8 (S)
99 %
70-120
1
01/04/10 18:38
2037.26.5
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
14.0 mg/L
8.3
1
12/29/09 11:07
5210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
2.3 mg1L
2.0
1
12/24109 10:45 12/29/09 10:15
82.84
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units
0.10
1
12130109 18:15
H6
Total Nitrogen Calculation
Analytical Method: 40CFR PART 503
Nitrogen
NO mg1L
0.60
1
01/0511018:25
7727-37.9
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
NO m911-
0.50
1
01/04/10 11:35
7727-37.9
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.16 mg1L
0.10
1
12/31/09 12:32
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
NO mg/L
0.10
1
12/31109 20:13
7723-14-0
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L
25.0
1
01/02/10 13:00
Date: 01119/2010 05:01 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc..
nehc.
Page 6 of 23

/ ! ~ Al'iA
•
�rrsri� �0
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
August 10, 2009
CERTIFIED MAIL 7009 0080 0000 9785 7613
RI"ITURN RECEIPT REQUESTED
Mr. Steve Barnwell, Manager
Huffman Oil Co.
1021 Queen Anne St.
Burlington, NC 27215
Subject: Notice of Violation/ Notice of Intent to Enforce
NOV-2009-OC-0008
Snipes Brothers Oil Co. - Roxboro
Diesel Fuel Oil Discharge
Person County
Dear Mr. Barnwell:
Dee Freeman
Secretary
This letter concerns a spill of Diesel File] Oil that was reported on August 1, 2009. The spill amount reported
was 2000 gallons and it was reported to have discharged to the stormwater system which discharges to Flat
River via an unnamed tributary through Roxboro neighborhoods.
Free product was observed in the creek. Oil absorbent booms and pads were placed at several locations along
the creek.
Cleanup was performed by Snipes personnel, and A and D Environmental spill response consultants were called
in to -help control and cleanup the spill, including the installation of two underflow dams. An EPA spill,
response representative was on -site to help direct these activities.
Accordingly, the fuel oil discharge is a violation of the following General Statutes:
Article 21A. Oil Pollution and Hazardous Substance Control
NCGS 143-215.83 states that "It shall be unlawful, for any person to discharge, or cause to be discharged, oil or
other hazardous substances into or upon any waters, tidal flats, beaches or lands within this State, or into any
sewer, surface water drain or other waters that drain into waters of this State, regardless of the fault of the
person having control of the oil or other hazardous substances, or regardless of whether the discharge was the
result of intentional or negligent conduct, accident or other cause."
NCGS 143-215.84 states that "Any person having control over oil or other hazardous substances discharged in
violation of this Article shall immediately undertake to collect and remove the discharge and to restore bJje area
as nearly as may be to the condition existing prior to the discharge." No-thC.aralina
1*111rrrr!!Y
North Carolina Division of Waler Quality Raleigh Regional Office
Surface Water Protection
Phone [phone]
Customer Service
Internet: www.ncwaterquality.org 1628 Mail ServlCC Center
Raleigh, NC 27699-1628
FAX [phone]
1-877-623-6149
An Equal OpportunifylAffirmalive Action Employer-50% Recycled110% Post
Consumer Paper

Snipes Brothers Oil Co. 8/10/2009
Page 2 of 3 r
NCGS 143-215.88A states that "Any person who intentionally or negligently discharges oil or other hazardous
substances, or knowingly causes or permits the discharge of oil in violation of this Part or fails to report a
discharge as required by GS 143-215.85 or who fails to comply with the requirements of G.S. 143-215.84 (a) or
orders issued by the Commission a result of violations thereof, shall incur, in addition to any other penalty
provided by law, a penalty in an amount not to exceed five thousand dollars ($5,000) for every such
violation..."
Article 21. Water and Air Resources
"NCGS 143-215.1 (a) Activities for Which Permits Required. — No person shall do any of the following things
or carry out any of the followi-ing activities unless that person has received a permit from the Commission and
has complied with all conditions set forth in the permit:
(1) Make any outlets into the waters of the State.
The violation above under Article 21 A is potentially subject to $5,000 and up to $25,000 dollars per day for
each violation. You are requested to respond to this Notice in writing within 30 days of receipt. Your response
should specifically address the following items:
1) Explain how the Fuel Oil Discharge occurred.
2) Please provide an account of the size of the vertical tank, the size of the containment basin, the
lock out procedures, alarm systems, and how the volume of the spill was determined. If you
have a revised calculation of the volume, please include that data.
3) Explain how the discharge was discovered and reported (include a timeline of these -events).
4) Please note: NCGS 143-215.84 states that "Any person having control over oil or other
hazardous substances discharged in violation of this Article shall immediately undertake to
collect and remove the discharge and to restore the area as nearly as may be to the condition
existing prior to the discharge."
Accordingly, please detail your cleanup response efforts and those future/ongoing efforts for the
following locations:
a) The containment structure.
b) The unnamed tributary (UT) through Iocal neighborhoods
Include copies of invoices for cleanup of these affected areas.
5) Please explain how control of the containment area release valve will be addressed to eliminate
the possibilities of future spills of Fuel Oil or other product to the collection system or
stormwater drains.
Based upon this spill event; the volume of petroleum product handled routinely at this facility and observations
by this office of the presence of potential stormwater pollutants, I am recommending by copy of this letter to
DWQ's Stormwater Permitting Unit that this facility obtain a NPDES stormwater permit. There is no general
permit to fit this situation, so an individual permit is to be established.

+i / . 1
Snipes Brothers Oil Co. 8/10/2009
Page 3 of 3
Accordingly, Acrobat pdf files of the appropriate stormwater permit application forms (EPA forms 1 and 2F)
will be emailed to you by the time YOU receive this letter, to be completed and mailed to:
Attn: Cory Larsen, Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
along with and an application fee of $860. If you have questions about the fee or how to answer any of the
questions, you may contact Mr. Ken Pickle at 919-807-6376, or Cory Larsen at 919-807-6365, in the
stormwater permitting unit for guidance.
If you have comments or questions about this letter or want to further review aciy details with our office, please
contact Myrl Nisely or myself at 919-791-4200. _
Sincerely,
Danny Smith
Surface Water Protection Supervisor
Raleigh Regional Office
Enclosures
cc: SWPIRRO Files
Central Files
Mr. Harold Kelly, Person County Flealth Department
Shelton Sullivan, NI S Assistance and Compliance Oversight Unit
Ms. .1ack .lacq jsic .lacq Jack,
USEPA Region IV, 61 Forsyth St., SW, Mail Code 9T25, Atlanta, GA 30303-8960

HUFFMAN OIL CO., INC.
12/22/09 122209
i
ORIGINAL CHECK IS ON CHEMICAL REACTI��
HUFFMAN OIL CO:, INC.
P.O. BOX 730
BURLINGTON, N.C. 27216-0730
336-227-8881
12/22/2009 138195
Eight Hundred Sixty and 00/100 Dollars
NCDENR
DIV. WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
860.00
BBff 6s +tz
Sur%ngton, NC Sat
No. 13879
.00 860.00
No. 138795
111&3#3'795i1' J:U5310L121j:511485607111'