NCS000568_Dudley NPDES Permit Application_20130731

SwSGStormwater Services Group, LLC
NPDES Individual
Stormwater Discharge
Permit Application
Prepared for
National Salvage & Service Corp.
Dudley, NC
May 15, 2013

GStormwater Services Group, LLC
8916 Oregon Inlet Court
Raleigh, North Carolina 27603
Phone: [phone]
Fax: [phone]
May 15, 2013
Mr. Bradley Bennett, PE
Stormwater Permitting Unit
NCDENR/ DWQ
1617 Mail Service Center
Raleigh NC 27699-16I7
RE: National Salvage & Service Corp
Wayne County NC
NPDES Individual Permit Application
Mr. Bennett:
Please find enclosed the application package for an NPDES Individual Stormwater Discharge
Permit for the subject facility.
If you have any questions, do not hesitate to call Mr. Clayton Walters at 919.739.5639 or the
signatory below.
Sincerely,
ST7esD.
M 8ERVICE3 GROUP, LLC
.;,Frei
Senior Project Manager
cc: C. Walters, NSSC
File

Please print or We in the unshaded areas only
Form Approved. OMB No, 2040-0086.
FORM U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA I.D. NUMBER
1-iEPA GENERAL INFORMATION
A
TF_
Consolidated Permits Program
D
GENERAL (Read the "General Instructions" before starting.)
2 131 14 1 15
GENERAL INSTRUCTIONS
If a preprinted label has been provided, affix it in the
LABEL ITEMS
designated space Review the information carefully; if any of it
I. EPA I.D. NUMBER
is incorrect, cross through it and enter the correct data in the
appropriate fill-in area below, Also, if any of the preprinted data
is absent (the area to the left of the label space lists the
III. FACILITY NAME PLEASE PLACE LABEL IN THIS SPACE
information that should appear), please provide it in the proper
fill-in areais) below, If the label is complete and correct, you
V FACILITY MAILING
need not complete Items I, III, V, and VI (except VI-B which
ADDRESS
must be completed regardless) Complete all items if no label
has been provided, Refer to the Instructions for detailed item
descriptions and for the legal authorizations under which this
VI. FACILITY LOCATION
data is collected.
11. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must
submit this form and the supplemental form listed in the parenthesis following the question. Mark "X" in the box In the third column if the supplemental form is attached. If
you answer "no" to each question, you need not submit any of these forms You may answer "no" if your activity Is excluded from permit requirements; see Section C of the
instructions. See also, Section 0 of the instructions for definitions of bold-faced terms.
mark'X'
Me1k"X' _
SPECIFIC QUESTIONS YES No FORM
ATTACHED
SPECIFIC QUESTIONS YES No FORM
ATTACHED
A. Is this facility a publicly owned treatment works whfch
B. Does or will this facility (either existing or proposed)
results in a discharge to waters of the U.S.? (FORM 2A) X
include a concentrated animal feeding operation or X
aquatic animal production facility which results in a
,s W ,s
discharge to waters of the U.S.? (FORM 2B) 19 20 21
C, Is this a facility which currently results in discharges to �/
X
D. Is this a proposed facility (other than those described in A "
waters of the U,S. other than those described in A or B
or B above) which will result in a discharge to waters of n
above? (FORM 2C) a 24
23
the U.S.? (FORM 2D)
E. Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this facility industrial or
hazardous wastes? (FORM 3) X
municipal effluent below the lowermost stratum X
containing, within one quarter mile of the well bore,
28 28 30
underground sources of drinking water? (FORM 4) 31 32 33
G. Do you or will you inject at this facility any produced water
H. Do you or will you inject at this facility Fluids for special
or other fluids which are brought to the surface in
processes such as mining of sulfur by the Frasch process,
connection with conventional oil or natural gas production, X
solution mining of minerals, in situ combustion of fossil X
Inject fluids used for enhanced recovery of oil or natural
fuel, or recovery of geothermal energy? (FORM 4)
gas, or inject fluids for storage of liquid hydrocarbons?
(FORM 4) 34 35 36
1. Is this facility a proposed stationary source which is one
J, Is this facility a proposed stationary source which is
of the 28 industrial categories listed in the instructions and
�/
X
NOT one of the 28 industrial categories listed in the
X
which will potentially emit 100 tons per year of any air
instructions and which will potentially emit 250 tons per
pollutant regulated under the Clean Air Act and may affect
year of any air pollutant regulated under the Clean Air Act
40
41
42
^^
or be located in an attainment area? (FORM 5)
and may affect or be located in an attainment area?
(FORM 5)
III. NAME OF FACILITY
c slctP NATIONAL ISALVI .I
1 AGE & SERVICE CORPORATION
efi 1e - 29 I 39
I I I I I I I I I I I t l
IV. FACILITY CONTACT
A. NAME & TITLE (lavi.nrsf, & title)
B.``PHONE (area code & no.)
ll
2
W 'E S, CLA TON, G N L G R
(919) 7 9-563
15
1fi
ds 48 40 49 51 52- 55
V.FACILTY MAILING ADDRESS
A. STREET OR P.O. BOX
c
g 4OF 0 D MO T OLIV W
s
45
B. CITY OR TOWN
r
C. STATE D. ZIP CODE
�C
2 3 3
4
D D EY—(—(—�—I�—
i.
is
49 41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
5 4 0 O D MO T OLIV W
15 is
45
B. COUNTY NA IE
WAYN
C. CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE (fknuwn)
6
-L
D&LE4 1� 1I I
C
2 3 3
u 54
EPA Form 3510-1 (8-90) CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES 4-di N in order of nbri
A. FIRST
B. SECOND
,,rr
{1-11101
7 2429
E0 RAILROAD TIE CHIPPING/ GRINDING
%
y
C. THIRD
D- FOURTH
(,t- 0)
Mile��fktif��
1tl LISIM
Vill.. OPERATOR INFORMATION
A. NAME 8.Is the name listed In Item
I I I VIII-A also the owner?
g NA'tTONAL SALVAGE & SERVICE CORPORATION m YES ❑ NO
Is l so
C. STATUS OF OPERATOR (Enter the appropriate letter into the answer box: If "Other, " s ecify.)
D. PHONE (area code & no.)
F = FEDERAL M = PUBLIC (other than federal orslate)
S= STATE
P
(SP-11y)
=
,q
II I I
(B 12) 3 3 9— 9 0 0 0
0= OTHER (specify)
P = PRIVATE
x
+ e jig n 26
E. STREET OR P.O. BOX
P OX 300
F. CITY OR TOWN IG,$TATE
H. ZIP CODE IX- INDIAN IANO
—I
I I I I I I I I I I I I I I
1 Is th9 fatality located on Indian lands?
B
CLEAR CREEK
IN 47426 ❑ YES m NO
X. EXISTING ENVIRONMENTAL PERMITS
A. NPOES Dircha s to sarf= Ilrarsr
D. PSD qhlYimlxs[ruts P Sburrrs
c r
9 P
a fa
9
N
ks
it
lqu
B. UIC 1nde roundln'ection o Fluids
E. OTHER s eci
c,
I I
t
I
(s�cifa)
9
U
9
C. RCRA Hazardous• Nasles
E. OTHER eci
se r r-j- — (sped)
a
r
9
R
1a >o
9
Se 1S 1i is
is
10
'7
xl, MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the
location of each of Its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it
injects fluids underground. Include all springs, rivers, and other surface water bodies In the map area. See instructions for precise requirements.
xll. NATURE OF BUSINESS (provide a brief description)
'Phis facility receives old railroad ties. It sorts them. Those in excellent condition are re -sold as RR ties,
those in good condition are sold as landscape timbers, and those in poor condition are placed into a chipper
,and ground into small pieces which is sold for boiler fuel to local electric power co -generation plants.
metal pieces recovered while grinding are sold to a local scrap metal yard.
Old railroad ties are received on -site via trains.
Chipped product is transported off -site via trucks.
XIII. CERTIFICATION (See irlSlrt of orls)
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and ail attachments and that, based on my
inquiry of those persons immediately responsible for obtaining the information contained in the application, I believe that the information is true, accurate, and complete. I
am aware Mat Mere are significant penalties for submitting false Information, including the possibility of fine and imprfsonment.
A. NAME & OFFICIAL TITLE (type orprint) B. SIGNATURE C. DATE SIGNED
COMMENTS FOR OFFICIAL USE ONLY
c
s rn
EPA Form 3510-1 (8-91))

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r 9 T 1 I M L• ��~. � I
l ' amp• n ti'a
' l:� �1 '•, - �-•' , • 1 fey • \ I '•'�AM 74
4 s RI
• , rr �0�
Trailer . s• • .r J`r ' ,
1 0 \
ark
�$r-_ � ' -_.} McArthur•\ _
Sratfe •••` _ Lake
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r Lore Ks ! ••'� � �TraiEee _ , % . •� � . - - -
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IC
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7%,;,�ti,, �_,a. is I � , r a l��` • i ti ' �•l ,
� }� �• �� as i tir , .I ;� ]
`' = �'.I !u railer
1j a ig^''", , . Park
>Cero �• ��
IV
SOUTHWEST GOLDSBORO, NC (1988) (QUADRANGLE
7.5 MINUTE SERIES,1:24000
FIGURE 1 - SITE LOCATION MAP
National Salvage & Service Corp - Dudley NC Stormwater Pollution Prevention Plan
NPDES Permit No. TBD Page 5

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
Please print or type In the unshaded areas only _ Approval expires 5-31-92
U.S. Environmental Protection Agency
Washington, DC 20460
FORM ticif
2F Application for Permit to Discharge Storm Water
NPDES Discharges Associated with Industrial Activity
Paperwork Reduction Act Notice
Public reporting burden for this application Is estimated to average 28.8 hours per application, Including time for reviewing instructions, searching existing data sources,
gathering and maintaining the data needed, and completing and reviewing the collection of Information. Send comments regarding the burden estimate, any other aspect
of this collection of information, or suggestions for improving this form, including suggestions which may increase or reduce this burden to: Chief, Information Policy
Branch, PM-223, U.S. Environmental Protection Agency, 1200 Pennsylvania Avenue, NW, Washington, DC 20460, or Director, Office of Information and Regulatory
Affairs, Office of Management and Budget, Washington, DC 20503.
I. Outfall Location
For each outfall, fist the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water _
A. Outfall Number
(lisp
B. Latitude
C. Longitude
0. Receiving Water
(name)
001
35.00
19,00
56.00
78.00
1,00
32.00
Unnamed tributary to Neuae I
Il.Improvements
A. Are you now required by any Federal, State, or local authority to meet any Implementation schedule for the construction, upgrading or operation of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described In this application? This includes, but is not limited
to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
2- Affected Outfalls 4. Final
1- Identification of Conditions, Compliance Date
Agreements, Etc. number source of discharce 3. Brief Description of Project a. req. b, proj.
None
B: You may attach additional sheets describing any additional water pollution (or other environmental projects which may affect your discharges) you now have under
way or which you plan. Indicate whether each program is now under way or planned, and indicate your actual or planned schedules for construction.
IIII. Site Drainage Map
Attach a site map showing topography (or indicating the outline of drainage areas served by the outfalls(s) covered in the application if a topographic map Is unavailable)
depicting the facility including: each of its intake and discharge structures; the drainage area of each storm water outfall; paved areas and buildings within the drainage
area of each storm water outfall, each known past or present areas used for outdoor storage of disposal of significant materials, each existing structural control measure
to reduce pollutants in storm water runoff, materials loading and access areas, areas where pesticides, herbicides, soil conditioners and fertilizers are applied; each of
Its hazardous waste treatment, storage or disposal units (including each area not required to have a RCRA permit which is used for accumulating hazardous waste
under 40 CFR 262.34); each well where fluids from the facility are injected underground; springs, and other surface water bodies which received storm water discharges
from the facility.
EPA Form 3510-2F (1-92) Page 1 of 3 Continue on Page 2

Continued from the Front
W. Narrative Description of Pollutant Sources
A. For each outfall, provide an estimate of the area (Include units) of Imperious surfaces (Including paved areas and building roofs) drained to the butfall, and an estimate of the total surface area
drained by the oulfall.
Outfall
Area of Impervious Surface
Total Area Drained
Outrall
Area of Impervious Surface
Total Area Drained
Number
(provide units)
(provide units)
Number
(provide units)
(provide units)
001 5.73 ac 9.54 ac
B. Provide a narrative description of significant materials that are currently or In the past three years have been treated, stored or disposed in a manner to allow exposure
to storm water; method of treatment, storage, or disposal; past and present materials management practices employed to minimize contact by these materials with
storm water runoff; materials loading and access areas, and the location, manner, and frequency in which pesticides, herbicides, loll conditioners, and fertilizers are
applied.
See Attchment No, 2
C. For each outfall, provide the location and a description or existing structural and nonstructural control measures to reduce pollutants in storm water runoff; and a
description of the treatment the storm water receives, including the schedule and type of maintenance for control and treatment measures and the ultimate disposal
of any solid or fluid wastes other than by discharge_
Outfall List Codes from
Number Treatment Table 2F-1
001 See Attachment No. 2 4-A
V. Nonstorinwater Discharges
A. I certify under penalty of law hat the outfoll(s) covered by this application have been tested or evaluated for the presence of nonstormwater discharges, and that all
nonstormwater discharged from these outfall(s) are identified in either an accompanying Form 2C or From 2E application for the outfell.
Name and Official Title (type or print)
Signature Date Signed
B. Provide a description of the method used, the date of any testing, and the onsite drainage points that were directly observed during a test.
Visual observation of site and drainage area. April 15, 2013, SDO-001.
The east side of the facility has no point source discharges. Runoff is sheet flow across an overgrown field,
VI. Significant Leaks or Spills
Provide existing Information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility In the last three years, Including the
approximate date and location of the spill or leak, and the type and amount of material released.
No significant spills or leaks have occurred in the previous three years,
EPA Form 3510-2F (1-92) Page 2 of 3 Continue on Page 3

Continued from Page 2 1
EPA ID Number (copy from Item 1 of Form 1)
'VII. Discharge Information
A, B, C, & D: See instructions before proceeding. Complete one set of tables for each outfall Annotate the outfall number in the space provided.
Table VII-A, VII-B, VII-C are included on separate sheets numbers VII-i and VII-2.
E. Potential discharges not covered by analysis — Is any toxic pollutant listed in table 2F-2, 2F-3, or 217-4, a substance or a component of a substance which you
currently use or manufacture as an Intermediate or final product or byproduct?
Z Yes (list all such pollutants below) ❑ No (go to Section lX)
Tables 2F-2, 2F-3, and 2F-4 are attached. Toxic pollutants that may be expected to be in this facility's stormwater
discharges are underlined.
Note that this Operator does not use any toxic pollutants in any manufacturing process and does not manufacture a product.
Some toxic pollutants underlined may be expected to be in the preservative used to treat railroad ties.
This Operator does not treat railroad ties.
Vill. Biological Toxicity Testing Data
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
❑ Yes (list all such pollutants below) Q No (go to Section )X)
IX. Contract Analysis Information
Were any of the analyses reported In Item VII performed by a contract laboratory or consulting firm?
© Yes (list the name, address, and telephone number of, and pollutants
❑ No (go to Section )Q
analyzed by, each such bore toey or firm below)_
A. Name
B. Address
C. Area Code & Phone No.
D. Pollutants Analyzed
Pace Analytical Services, Inc.
6701 conference Drive
[phone]
All indicated on the
Raleigh NC 27607
attached laboratory report
X. Certification
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure
that qualified personnel property gather and evaluate the Information submitted. Based on my Inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false Information, including the possibility of fine and Imprisonment for knowing violations.
A. Name & Official Tille (Type Or Print) B. Area Code and Phone No.
C Signature
D. Date Signed
EPA Form 3510-2F (1-92) Page 3 of 3

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
l Approval oxpires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A— You must provide the results of at least one analysis for every pollutant in this table Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(rf avalla6/e)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
flow -Weighted
Composite
Oil and Grease
< 5.0 mg/L
N/A
1.00
Trucks and loaders
Biological Oxygen
Demand (BOOS)
10.7 mg/L
1.00
Micro-organisms in the discharge
Chemical Oxygen
Demand (COD)
106 mg/L
1.00
Organic matter in discharge
Total Suspended
Solids (TSS)
26.1 mg/L
1.00
Dust/ dirt from site
Total Nitrogen
1.9 mg/L
1.00
Atmospheric deposits
Total Phosphorus 0.066 mg/L 1.00 Unknown
pH Minimum 9.66 Maximum Minimum Maximum 1.00 ^�
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfail. See the instructions for additional details and
requirements.
Maximum Values Average Values
(Include units) (include units) Number
Pollutant Grab Sample Grab Sample I of
and Taken During Taken During Storm
CAS Number First 20 Flow -Weighted First 20 Flow -Weighted Events
(if available) Minutes Composite Minutes Composite Sampled Sources of Pollutants
EPA Forth 3510-2F (1-92) Page VII-1 Continue on Reverse

Continued from the Front
Part C - List each pollutant shown in Table 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfall.
Pollutant
and
CAS Number
(ifavailable)
Maximum Values
(include units)
Average Values
rinclude units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Phenol
0.084 mg/L
1.00
RR tie preservatives
Arsenic
< 10.0 ug/L
1.00
Cadmium
< 1.0 ug/L
1.00
Chromium
< 5.0 ug/L
1.00
Copper
18,2 ug/L
1.00
Past operations/ RR tie preservative
Lead
< 5.0 mg/L
1.00
Nickel
< 5.0 mg/L
1.00
zinc
10.7 ug/L
1.00
Galvanized roofs
Part D — Provide data for the stone event(s) which resulted in the maximum values for the flow weighted composite sample.
1.
Date of
Storm
Event
2.
Duration
of Storm Event
(in minutes)
3.
Total rainfall
during storm event
(in inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum flow rate during
rain event
(gallonalminufe or
specify units)
6.
Total flow from
rain event
(gallons or specify units)
04/26/13
1250
1.13
186
unknown
172,698 gallons
7. Provide a description of the method of flow measurement or estimate.
Total Flow was calculated using Schueler's Simple Method as described in Controlling Urban Runoff, July 1987.
EPA Form 3510-2F (1-92) Page VII-2

National Salvage & Service Corporation
NPDES Individual Stormwater Permit Application
Form 2F — Attachment No. 2
IV. Narrative Description of Pollutant Sources
B. This facility was the former GAF Materials Corp dimensional asphalt roofing shingles
which closed January 31, 2008.
NSSC, the current operator, has no knowledge of significant materials treated, stored,
or disposed in a manner to allow exposure to stormwater in the past three years.
Present materials exposed are used wooden railroad ties and metal pieces used to
attach the rails to the ties.
Railroad ties are brought to this facility by train, off-loaded and stacked on the ground
and concrete slabs. The ties are then sorted: to be re -sold as RR ties, to be sold as
landscape timbers, or to be chipped into boiler fuel.
The stacked RR ties are exposed to precipitation.
The tie chipper discharges directly into trailers which are used to haul the chipped ties
to local electric power co -generation plants.
This operator has not applied pesticides, herbicides, soil conditioners, and fertilizers
since commencing operations. If these items were to be applied, the applicator will
follow the directions specified on the product container.
C. Treatment BMPs implemented for SDO-001 include:
Structural
Discharge flows through a grass -lined ditch.
Vegetated buffer along site perimeter.
Non -Structural:
Good Housekeeping.
Spill Prevention & Response.
Preventative Maintenance of Industrial Equipment, Ditch, and Buffers.
Storage of POLs and other hazardous materials is indoors.
Used POL, scrap debris, and trash is hauled off -site for proper disposal.

VII. Discharge Information
PartB. This facility is not subject to any effluent guidelines.
Part G. Refer to the attached Pace Analytical laboratory report. None of the expected
semi -volatile organics or volatile organics were reported to be in the discharge.

Table 2F-2
Conventional and. N onconventlonal Pollutants
Bromide
01 odne, Total Rasidual
Color
Focal Coliform
Fluoride
Nitrate-Nitrfie
N11rogen, Total Drganlc
Oil and Grease
Phosphoms, Total
Radloertivny
Sulfate
Suiirte
Surfactants
ants
AhxninUM ToW
Barium, Too
Boron, Total
Cobaait Total
[Toro, TOW
Magnesium, Total
Molybdenum, Total
Manganese, Total
Tin, Total
Titanium, Total
EPA Farm 3610-2F (Rev. 1-92) 1-9

Table 2F-3
Toxic Pollutants
Toxic Pollutants: and Total Phenol
Antimony, Total
['npperf Total
Silver, Total
Arsenic, Total
Lead, Total
Thallium, Total
Beryllium, Total
Mercury, Total
Zinc, Total
Cadmium, Total
Nickel, Total
Cyanide, T5157
Chromium, Total
Selenium, Total
Phenols, Total
GCIMS Fraction Volatiles Compounds
Acrolein
Dichlorobromomethane
1,1,2,2,-Tetrachioroethane
Acrylonihile
1,1-Dichloroelhane
Tetrachloroethylene
Benzene
1,2-Dichloroethane
Toluene
Bromoform
1,1-Dichloroethylene
1,2-Trans-Dichloroethylene
Carbon Tetrachloride
1,2-Dichloropropane
1,1,1-Tdchloroethane
Chlorobenzene
1.3-Dichloropropylene
1,1,2-Trichloroethane
Chlorodibromomethane
Ethylbenzene
Trichloroethylene
Chloroethane
Methyl Bromide
Vinyl Chloride
2-Chloroethylvinyl Ether
Md"thyl Chloride
Chloroform
Methylene Chloride
Acid Compounds
2-Chlorophenol
2,4-Dinifrophenol
Pentachlorophenoi
2,4-Dichlorophenol
2-Nitrophenol
Phenol
2,4-Dimethylphenol
4-Nitrophenol
2,4,6-Tdchiorophenol
4,6-Dinitro-O-Cresol
p-Chioro-M-Cresol
2-methyl-4,6 dinitrophenol
Base/Neutral
Acenaphthene
2-Chloronaphthalene
Fluroranthene
Acenaphthylene
4-Chlorophenyl Phenyl Ether
Fluorene
Anthracene_
Chrysene
Hexachlorobenzene
,
Benzidine
Dibenzo(a,h)anthracene
Hexachlorobutadiene
Benzo(a)anthrecene
1,2-Dichlorobenzene
Hexachloroethane
Benzo(a)pyrene
1,3-Dichlorobenzene
Indeno(1,2,3-cd)pyrene
3,4-Benzofluoranthene
1,4-Dlchlorobenzene
Isophorone
Benzo(ghi)perylene
3,3'-Dichlorobenzidine
Napthalene
Senzo(k)fiuoranthene
Diethyl Phthalate
i robenzene
Bis(2-chloroethoxy)methene
Dimethyl Phthalate
N-Nitrosodimethylamine
Bis(2-chloroethyl)ether
Di-N-Butyl Phthalate
N-Ndrosodi-N-Propylamine
Bis(2-chlorolsopropyl)ether
2,4-01nitrotoluene
N-Nitrosodiphenylamine
Bis(2-ethylyhexyl)phthalate
2,6-Dindrotoluene
Phenanthrene
4-Bromophenyl Phenyl Ether
DI-N-Octyphthalate
Pyrene
Butylbenzyl Phthalate
1,2-Diphenyihydrazine (as Azobenzene)
1,2,4-Trichlorobenzene
Pesticides
Aldrin
Dieldrin
PCB-1254
Alpha-BHC
Alpha-Endosulfan
PCB-1221
Beta BHC
Beta-Endosulfan
PCB-1232
Gamma-BHC
Endosulfan Sulfate
PCB-1246
Delta-BHC
Endrin
PGB-1260
Chlordane
Endrin Aldehyde
PCB-1016
4,4'-DDT
Heptachlor
Toxaphene
4,4'-DDE
Heptachlor Epoxide
4,4'-DDD
PCB-1242
EPA Form 3510-2F (Rev. 1-92) 1- 10

Table 2F4
Hazardous Substances
Toxic Pollutant
Asbestos
Hazardous Substances
Acetaldehyde
Dinitrobenzene
Napthenic acid
Allyl alcohol
Diquat
Nitrotoluene
Allyl chloride
Disulfoton
Parathion
Amyl acetate
Diuron
Phenolsulfonate
Aniline.
Epichlorohydrin
Phosgene
Benzonitrile
Ethion
Propargite
Benzyl chloride
Ethylene diamine
Propylene oxide
Butyl acetate
Ethylene dibromide
Pyrethrins
Butylamine
Formaldehyde
Quinoline
Carbaryl
Furfural
Resorcinol
Carbcfuran
Guthion
Stronthium
Carbon disulfide
Isoprene
Strychnine
Chlorpyrifos
Isopropanolamine
Styrene
Coumaphos
Kelthane
2,4,5-T (2,4,5-Trichlorophenoxyacetic
acid)
Cresol
Kepone
TDE (Tetrachlorodiphenyl ethane)
Crotonaldehyde
Malathion
2,4,5-TP (2-(2,4,5-Tdchlorophenoxy)
propanoic acid]
Cyclohexane
Mercaptodimethur
Trichlorofan
2,4-D (2,4-Dichlorophenoxyacetic
Methoxychlor
Triethylamine
acid)
Diazinon
Methyl mercaptan
Trimethylamine
Dicamba
Methyl methacrylate
Uranium
Dichlobenil
Methyl parathion
Vanadium
Dichlone
Mevinphos
Vinyl acetate
2,2-Diphloropropionic acid
Mexacarbate
Xylene
Dichlorvos
Monoethyl amine
Xylenol
Diethyl amine
Monomethyl amine
Zirconium
Dimethyl amine
Naled
EPA Form 351 Q-2F (Rev. 1-92) 1 - 11

PaceAnaoical
www.pa6e/eb&0w
Jim Frei
Stormwater Services Group
8916 OREGON INLET CT.
Raleigh, NC 27603
Project: NATIONAL SALVAGE
Pace Project No.: 92156106
Sample: NS-001
Parameters
Oil and Grease
Arsenic
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo (b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphtha late
4-Chloro-3-methylphenol
bis(2-C h loroethoxy)metha ne
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3-Dlchlo robenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphtha late
Di-n-butylphthalate
4,6•Dinitro-2-methylphenol
2,4-DInitro phenol
2,4-Dlnlirotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phtha late
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachla rocyclope ntadien e
Laboratory Report
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 3
Report Date: 05/09/2013
Date Received: 04/29/2013
Lab ID: 92156106001 Collected: 04128/13 19:50 Matrix: Water
Results Units Report Limit Analyzed Qualifiers
NO mg/L
5.0
05101/1310:29
NO ug/L
10.0
05/02/13 20:17
NO ug/L
1.0
05/02/13 20:17
NO ug/L
5.0
05/02/13 20:17
18.2 ug/L
5.0
05/02/13 20:17
NO ug/L
5.0
05/02/13 20:17
NO ug/L
5.0
05/02/13 20:17
10.7 ug/L
10.0
05/02/13 20:17
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05102/13 20:04
NO ug/L
5.0
05102/13 20:04
NO ug/L
5.0
05/02/13 20:04
ND ug/L
5.0
05/02/13 20:04
NO ug/L
50
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
10.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
25.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
10.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
20.0
05/02/13 20:04
NO ug/L
50.0
05/02/13 20:04
NO ug/L
5.0
05102J13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
NO ug/L
5.0
05/02/13 20:04
ND ug/L
5.0
05/02/13 20:04
ND uglL
10.0
05/02/13 20:04
Page 1 of 5

m
;alceAnalylical
1 www.pecefabs.com
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 2 of 3
Sample: NS-001
Lab ID: 92156106001 Collected; 04128/1319:50
Matrix: Water
Parameters
Results Units
Report Limit
Analyzed
Qualifiers
Hexachloroethane
NO ug/L
5.0
05/02/13 20:04
Indeno(1,2,3-cd)pyrene
NO ug/L
5.0
05/020320:04
Isophorone
NO ug/L
10.0
05/02/13 20:04
Naphthalene
NO ug/L
5.0
05/02/13 20:04
Nitrobenzene
NO ug/L
5.0
05/02/13 20:04
2-Nitrophenol
NO ug/L
5.0
05/02/13 20:04
4-Nftrophenal
NO ug/L
50.0
05/02/13 20:04
N-Nltrosodimethylamine
NO ug/L
5.0
05/02/13 20:04
N-Nitroso-di-n-propylemine
NO ug/L
5.0
05/02/13 20:04
N-Nitrosodiphenylamine
NO ug/L
10.0
05/02/13 20:04
Pentachlorophenol
NO ug/L
25.0
05/02/13 20:04
Phenanthrene
NO ug/L
5.0
05/02/13 20:04
Phenol
NO ug/L
5.0
05/02/13 20:04
Pyrene
NO ug/L
5.0
05/02/13 20:04
1,2,4-Trichlorobenzene
NO ug/L
5.0
05/02/13 20:04
2,4,6-Trichlorophenol
NO uglL
10.0
05/02/13 20:04
Nitrobenzene-d5 (S)
63 %
10-120
05/02/13 20:04
2-Fluoroblphenyl (S)
66 %
15-120
05/02/13 20:04
Terphenyl-dl4 (S)
56 %
11-131
05/02/13 20:04
Phenol -dB (S)
26 %
10-120
05/02/13 20:04
2-Fluorophenol (S)
37 %
10-120
05/02/13 20:04
2,4,6-Tribromophenol (S)
82 %
10-137
05/02/13 20:04
Benzene
NO ug/L
5.0
05/0311314:51
Bromodichloromethane
NO ug/L
5.0
05/03/13 14:51
Bromoform
NO ug/L
5.0
05/03/13 14:51
Bromomethane
NO ug/L
10.0
05103/1314:51
Carbon tetrachloride
NO ug/L
5.0
05/03113 14:51
Chlorobenzene
NO ug/L
5.0
05/03/13 14:51
Chloroethane
NO ug/L
10.0
05/03/13 14:51
Chloroform
NO ug/L
5.0
05/03/13 14:51
Chloromethane
NO ug/L
5.0
05103/1314:51
Dibromochloro methane
NO ug/L
5.0
05/03/1314:51
1,2-Dichlorobenzene
NO ug/L
5.0
05/03/13 14:51
1,3-Dichlorobe nzene
NO ug/L
5.0
05/03/13 14:51
1,4-Dichlorobenzene
NO ug/L
5.0
05/03/1314:51
1,1-Dichloroethane
NO ug/L
5.0
05/0311314:51
1,2-Dichloroethane
NO ug/L
5.0
05/0311314:51
1,1-Dichloroethene
NO ug/L
5.0
05/0311314:51
cis-1,2-Dichloroethene
NO ug/L
5.0
05/03/13 14:51
trans-1,2-Dichloroethene
NO ug/L
5.0
05/03/13 14:51
1,2-Dichloropropans
NO ug/L
5.0
05103/1314:51
ci5-1,3-Dichl0r0propene
NO uglL
5.0
05/03/13 14:51
trans-1,3-Dichloropropene
NO ug/L
5.0
0510311314:51
Ethylbenzene
ND ug/L
5.0
05/0311314:51
Methylene Chloride
NO ug/L
5.0
05/03/13 14:51
1,1,2,2-Telrachloroethane
NO ug/L
5.0
0510311314:51
Tetrachloroethene
NO ug/L
5.0
05103/1314:51
Toluene
NO ug/L
5.0
05103/1314:51
1,1,1-Trichloroethane
NO ug/L
5.0
05/03/13 14:51
1,1,2-Trichloroethane
NO ug/L
5.0
0510311314:51
Trlchloroethene
NO ug/L
5.0
05/0311314:51
Trichlorofluoromethane
NO ug/L
10.0
05/03/13 14:51
Vinyl chloride
NO ug/L
5.0
05/03/13 14:51
Dibromofluoromethane (S)
97 %
70-130
05/03/13 14:51
4-Bromofluorobenzene (S)
105 %
70-130
05/03/13 14:51
Toluene -dB (S)
97 %
70-130
05/03/13 14:51
1,2-Dichloroethane-d4 (S)
98 %
70-130
05/03/13 14:51
BOD, 5 day
10.7 mg/L
2.0
05/04/13 00:00
B3
Total Suspended Solids
26.1 mg/L
2.5
05/01/13 08:32
Total Nitrogen
1.8 mg/L
0.12
05/06/13 16:12
Page 2 of 5
Nitrogen, Kjeldahl, Total
1.8 mg/L
0.50
05/03/13 14:41

PaceAnapicat4
*"..Pae6WS.="
Sample: NS-001
Lab ID: 92156106001 Collected: 04/28/13 19:50 Matrix: Water
Parameters
Results Units
Report Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3
ND mg/L
0.020
05/01/13 18:02
Phosphorus
0.066 mg/L
0.050
05/07/1311:01
Phenol
0.084 mg/L
0.050
05/03/13 13:57
Chemical Oxygen Demand
106 mg/L
25.0
05/08/13 15:00
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
Reviewed by:�'
Nikitia Jones -Jackson
[e-mail]
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florlda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiafVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh. NC 27607
(919)6344964
Page 3 of 3
Page 3 of 5

aceArralyieal
_ urww.parnlaNs.eutt7
6701 Conference Drive, Raleigh, NC 27607
ph: [phone], law [phone]
NC1MN CerM7, NCDW CerW37731
Chain of Custody
Report Results To: Bill To:
Company:sTdRfLwPT,-p, !;Ve-s_C;Pp_
Address: _ T
Attn: -
-
Phone:lfvCoJ-
Fax:
Sampled by (signature): s�
Project Reference;
t mowAL
Project Number:
Purchase Order #:
& SSndard Report Delivery
❑ Bush Report Delivery (wfsurchafge)
"Bush pralecra are subJeat to prlor approval ny
the laboratory
Requestad Due Date: _
fi .i {Yr14i�'
`/ rr d
r �
Y�
f�
Y
it
■
RvUr naiu
ellnqulshed by (signatu
Rek qulshed by (eignatu
L- -
ey R i►reri nature)
e) Received by Ignature)
e) Received by (signature)
U 1
17me l
Time
Date
Date
Tlme
I#ecelpt Condl0ons (Lab Use Only)
❑ 4t2°C ❑ Temp:_,°C
Res. Chlorine:
❑ Absent ❑ Present ❑ rda
Acid preserv. <27
❑ Yee ❑ No ❑ n/a
Base presery. >12?
❑ Yes ❑ NPab; Of 5
I

Document Name: Sample Condition Upon Document Revised: March 13, 2013
Recei t SCUR Pagel of 2
Document No.:
Issuing Authorities:
Pace Asheville Quality C
Client- Name:;S.16 r
Where Received: © Huntersvllie [] Asheville Aden �aleigh
Courier (Circle): Fed Ex PIPS U.SPS Cllen Commercial Pace Other
Custody Seal on Cooler/Box Present: Q yes no Seals Intact [] yes no
Packing Material: Ej Bubble Wrap ❑ Bubble Bags one [] Other
Circle Thermometer Used: IR Gun SN:122066387Type of Ice: V�G6Blue None Samples on Ice, cooling process has begun
IR Gun Back Up SN:122065371
Temp Correction Factor: Add I Subtract C
p..
Corrected Cooler Tem � C
Temp should be above frea;Jng to 6°c
Biological Tissue Is Frozen: Yes No p
�
Comments:
Date an InttlaI of era exa 1n
cvni3onta���� ~ ��'" f .3
Chant of Custody Present:
es ❑Na ©wA
1.
2.
Chain of Custody Filled Out: OY08 ONO ❑wA
Chain of Custody Relinquished-.
er: QNo ❑NIA
3.
Sampler Nerno & Si nuluro on COC:
as ON. ❑wA
4.
T
Sam lee Arrived within Hold lime:
" ea ONo ❑wA
5,
_
Short Hold Time Analysis C<72hr-
Yee ON, ONfA
6,
_
Rush Turn.Around Time Re uested:
Byes J26 ❑wA
-7.
Su#licieM Volume:
96 ONO I_ WA
S.
Correct Container's Used:
-Pace Containers Used:
Yes ONO ❑NIA
es ON. ❑NIA
9.
.
Containers lntact:
es ON, I-) WA
10.
Filtered volume received for Dissolved tests
Oyes ONo IA
11.
Sample Labels match COC;
-includes dateftlmellwAnal is Matfl:c
cs ONo ❑NIA
12.
All conlolnare needing preservallon have been checked,
All containers needing preservation are found to be In
00rytipliance with EPA recornolandkalicn.
exce Ilona: VOA, oallfonn,7 oat WR0 eteg
r . ❑No ONIA
fir" ONo ONIA
/�'r
os ONo
13.
—6
Initial when com leted
Samples checked for dechlodnation:
es ON, OwA
14,
Heads ace In VOA Vials y8mm :2f.
ONo_ ❑wA
15.
Trip Blank- Present:
Trip Slank Custody Seals Present -�
Pace Trip Blank Lot # if 6rnhased :
Gres ONO RQA
C3Yes �[qw
JO.
Client Notifleationt Resolution: Field Data Required? Y f N
Person Contacted:
Comments/ Resolution:
SCURF Review:
SRF Review:
Datefrime:
Note: Whenever there Is a discrepancy at[+}dtir4 North Carolina compliance
samples," a copy of this form will be sent to the North Carolina Dr=HNR
Certifleatlon Office ( Le out of hold, Incorrect preservatIve, out of temp.
Incorrect containers)
WO#•92156105
111i1�uwumim
Page 5 of 5