NCS000338_MONITORING INFO_20101103

-----__STORMWATER-DIVISION--CODING SHEET''
PERMIT NO.
DOC TYPE
❑ FINAL PERMIT
[-MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 1 l-91 n I I u�
YYYYM M DD

•
November-3, 2010
Crop
Production
Services
PS
1160 Brake Road, Rocky Mount, NC 27801
252-977-0308 Phone
252-973-0761 Fax
Mitch Hayes, Environmental Specialist
North Carolina Division of Water Quality
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re.: NPDES Permit NCS 000338
Crop Production Services, Inc., Wilson Facility
September 17, 2010 Compliance Evaluation Inspection
Dear Mr. Hayes:
RECEIVED
NOV - 5 2010
NC OENR
Raleigh Regional Office
This is in response to your letter and report subsequent to your compliance inspection of
our Wilson Terminal on September 17, 2010.
Storm Water Pollution Prevention Plan
We have updated the Storm Water Pollution Prevention Plan to incorporate the
deficiencies you noted in the September 17, 2010 report, including current personnel
contact and training information. We have also added Goggle generated maps for the
terminal and surrounding area. An Annual Review has been documented.
Qualitative Monitoring
Forms were printed from the NC DENR website so that Qualitative Monitoring could be
documented. Terry Dellinger had completed a Sample Observation Form at the time of
pulling the samples.
Analytical Monitoring
DMR was submitted via e-mail to you and to Brian Lowther today for Year 1, Period 1 of
Permit NCS000338, followed with hard copy to the Mail Service Center in Raleigh as
instructed in the permit. No parameters checked outside of the benchmark values stated
in the Permit.

•
0
Mr. Mitch Hayes, NC DENR
Page 2
November 3, 2010
Permit and Outfalls
A copy 'of the Permit is included as Tab 7 within the SWP3 Plan.
Once the current DMR was submitted to Brian Lowther today, he responded that the
permit had been rescinded and that the letter was mailed last week. Upon receipt of the
rescission letter, current contact information for Billy Pirkle was forwarded to Mr. Lowther
for State DENR, Division of Water Quality records. A copy of the letter is filed with the
SWP3 and Permit Copy.
We do appreciate all of your input and assistance with this matter.
Please contact me at the number above or Terry Dellinger at the Wilson Terminal at 252-
237-5431 if you need any further information.
Sincerely,
0
Nancy Vincek
Manager, Operations Compliance
C: Kirk Williams
Dana Reineke
Bill Coleman
Terry Dellinger

Wed 11/3/2010 1:17 PM 0
Brian:
Thanks for the update. Please update your contact information for future reference.
Billy Pirkle
Crop Production Services, Inc.
P. 0. Box 22
3005 Rocky Mountain Ave.
Loveland, CO 80538
970-685-3300
We appreciate your consideration in this matter.
Nancy Vincek
Manager, Operations Compliance
Crop Production Services, Inc.
1160 Brake Road
Rocky Mount, NC 27801
252-977-0308 - Office
252-973-0761 - Fax
618-407-5616 - Mobile
nancy.vincek(a),cpsagu.com
From: Lowther, Brianfmailto:brian.lowtherOncdenr.gov1
Sent: Wednesday, November 03, 2010 9:31 AM
To: Nancy Vincek; Hayes, Mitch
Cc: Bill Coleman; Kirk Williams; Reineke, Dana; Terry Dellinger
Subject: RE: Year 1, Period 1 DMR - Wilson CPS Terminal
Nancy,
Thanks for the sampling results. we did decide to rescind this permit based on the site not having any
blending/manufacturing on the site. i sent the attached rescission letter out last week. It was sent to the owner that we
have in our system for the facility. I apologize for not copying you on it. Please let me know if you have any questions.
Brian
Brian C. Lowther
Environmental Engineer
NCDENR � DWQ I Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Email: brian,low_t_hercr,ncdenr..gov-
Website: http://Portal.nedenr.org/web/wq/ws/su
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law
and may be disclosed to third parties.
From: Nancy Vincekfmailto:[e-mail]
Sent: Wednesday, November 03, 2010 10:05 AM
To: Hayes, Mitch; Lowther, Brian

Cc: Bill Coleman; Kirk Williams; Reineke, a; Terry Dellinger (�
Subject: Year 1, Period 1 DMR - Wilson CoTerminal
Mitch and Brian:
Attached is the report which is being mailed certified mail today to Division of Water Quality, Central Files in Raleigh (two
copies). Due to recent correspondence with both of you, I wanted you to have an advance copy. Please let me know if
you need further information.
Dana: Please place this on the server under Wilson Terminal Loc. # 146. I will be forwarding updates to the SWP3 Plan
shortly.
Thanks, and have a safe day,
Nancy Vincek
Manager, Operations Compliance
Crop Production Services, Inc.
1160 Brake Road
Rocky Mount, NC 27801
252-977-0308 (office)
618-407-5616 (mobile)
252-973-0761 (fax)
IMPORTANT NOTICE ! This E-Mail transmission and any accompanying attachments may contain confidential information intended only for the
use of the individual or entity named above. Any dissemination, distribution, copying or action taken in reliance on the contents of this E-Mail by
anyone other than the intended recipient is strictly prohibited and is not intended to, in anyway, waive privilege or confidentiality. If you have
received this E-Mail in error please immediately delete it and notify sender at the above E-Mail address. Agrium uses state of the art anti -virus
technology on all incoming and outgoing E-Mail. We encourage and promote the use of safe E-Mail management practices and recommend you
check this, and all other E-Mail and attachments you receive for the presence of viruses. The sender and Agrium accept no liability for any
damage caused by a virus or otherwise by the transmittal of this E-Mail.

NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Billy Pirkle
Agrium US Inc
3105 Glenn Ave
Winston Salem, NC 27105
Dear Permittee:
Division of Water Quality
Coleen H. Sullins
Director
October 25, 2010
Dee Freeman
Secretaryr
IRI OCT 2 820, , J
pEiiRALrlCll ;it�ui?1'';�L OFFICE
Subject: Rescission of NPDES Stormwater Permit
Certificate of Coverage Number NCS000338
Agrium US Inc
Wilson County
On 2/23/2010, the Division of Water Quality received your request to rescind your coverage under
Certificate of Coverage Number NCS000338. In accordance with your request, Certificate of Coverage
Number NCS000338 is rescinded effective immediately.
Operating a treatment facility, discharging wastewater or discharging specific types of stormwater to
waters of the State without valid coverage under an NPDES permit will subject the responsible party to a
civil penalty of up to $25,000 per day. It is the intention of DWQ that enforcement proceedings will
occur for persons that have voluntarily relinquished permit coverage when, in fact, continuing permit
coverage was necessary. If, in retrospect, you feel the site still requires permit coverage, you should
notify this office immediately. Furthermore, if in the future you wish to again discharge to the StatCs
surface waters, you must first apply for and receive a new NPDES permit.
If the facility 15 In the pr0%c55 of being sold, you vG'ii p r p ifyou
h e erfornnin r a public service ii `"ou woult-1 inform
the new or prospective owners of their potential need for NPDES permit coverage.
If you have questions about this matter, please contact Brian Lowther at [phone], or the Water
Quality staff in our Raleigh Regional Office at NPDES SW.
Sincerely,
for Coleen H. Sullins, Director
cc: Raleigh Regional Office
Stormwater Permitting Unit
DWQ Central Files
Fran McPherson, DWQ Budget Office
Wetlands and Stormwater Branch One
1617 Mail Service Center, Ralegh, North Carolina 27599.1617 North Carob na
1512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: 91M07.63001 FAK 919-807.64941 Customer Service: 1-877-623-6748 �%tjfl'�!!1/
Internet: www.rimaterquality.org ;/
An Equal Opportunity 1 Affirmative Action Employer

Crop
Production
Services
1160 Brake Road, Rocky Mount, NC 27801
252-977-0308 Phone
252-973-0761 Fax
November 3, 2010
Division of Water Quality
Attn. Central Files
1617 Mail Service Center
Raleigh, NC .27699-1617
Re.: Permit Number NCS 000338
Crop Production Services, Inc., Wilson Terminal
Wilson County
Enclosed is the DMR for the required sampling per the above permit for the period April
1, 2010 through September 30, 2010. The sample was pulled on September 27, 2010.
Results were received on October 4, 2010.
Please note that the lab did not perform BOD and COD on the samples, even though
these tests were included in the instructions supplied to the Lab.
Please contact me at the number above or Terry Dellinger at the Wilson Terminal at 252-
237-5431 if you need any further information.
Sincerely,
0
Nancy Vincek
Manager, Operations Compliance
Enc.
C: Kirk Williams
Dana Reineke
Bill Coleman

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 0 0 4 3 3 8
r i
FACILITY NAME C-"P PRa D{[C i i O I►f S �RVi CE�i
PERSON COLLECTING SAMPLE(S) -rE1efX 7WLLIM669 _
CERTIFIED LABORATORY(S) A+L GaFar ES Lab i#
Lab ##
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 7i0/Q
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY �+►� I Sp/1/
PHONE NO. (2SZ]
(SIGNAT'UJ OF PERMITTEE OR DESIGNEE)
By this sigriature, I certify that this report is accurate
complete to the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes �no
(if yes, complete fart $)
Part B: Vehicle Maintenance A ivity Monitoring ReqWremcnts
•
+e
i8 CNA'Wwy
�'as Di�soived Sw1-�,.k��
Outfall
No.
Date
Sample"
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non polar
O&GtrPH
(Method 1664
SGT-HEM), If
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
malddl r
MG
inches
nwfl
unit
Umo
Form SWU-247-062310
Page 1 of#3

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS O o 9
FACILITY NAME 0 rf iVl 66
PERSON COLLECTING SAMPLE(S) E 2444iM'4F
CERTIFIED LABORATORY(S) ♦ r Lab #
Lab #
Part A: Specific Monitoring Requirements) CcV,+ `a
SAMPLES COLLECTED DURING CALENDAR YEAR: 20 I,o
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY W 1' ) $O AV _
PHONE NO. 2{ S2 ) 2 3
(SIGNATURE WPERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oit per month? ^ yes 1Lno
(if yes, complete Part 13)
Part L• Vphirip Maintenance Actlyity Monitorinx Requirements
e
�CnAAm4rg
sF ns bi5KeJVe41'lmncb+6(m,POkn0
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
([f applicable)
Total
Rainfall
Oil & Grease
(if appi.)
Non -polar
O&GI TPH
(Method 1664
SGT-HEM), if
apol.
Total
Suspended
Solids
pH
I New Motor
Oil Usage
molddl r
MG
[riches
MizR
Me
unit
at/mo
Form SWU-247-062310
Page[ of,S
2 3

STORM EVENT CHARACTERISTICS:
Date _42 `r - Z 010
2
Total Event Precipitation (inches):
Event Duration (hour's): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours); (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
. !� /-f-a0/Z?
(Signature of Pe ttee) (Date)
Form SWU-247-062310
Page f *
3
0

I
rn
m i Report Nun*e,
l 10-272-0214 Page: 2 of 2
CL
E Aecount Nur►rber
46605
Seri! To. CROP PRODUCT1011 SERVICES
P08 2149
WILSON , NC 27894
Project, Ot1TFALL 1 AND 2MIATER SAMPLES
f
U
z
zz Lab Number: 78733
J 3amP1e fd : OUTFALL 2
H
Tn Analysis
A&L Eastem Laboralon"es, Inc.
tu+r�r■tee �r,�n�grotsarr pagrna� r�{a�gtn�e
rams.
REPORT OF ANALYSIS
Quantitation
U Result
Toga! Njefdahl Nitrogen,
Llm1t .
mg1L
TDfal P 4 _
hosphorers , rrlgl�
1
Ammonia Nitrogen. mg/L 0.5 -
0.1
Nlrafe+Nitrite-N . mg Kg <1
1
roraf Su <1
tended Soups, �
1
78
Dissolved Magms;ura , Ipm
1
1
Dissolved Sulfate , Ppm
1
+n od R 10
tr "lethReference:
1
m Methods }br theDetermination of Metals In Errvironn)ental Samples, EPA160014-9i-010,
CA v rd Methods �e A��s of Water
June 1991
Test n and Wastewater, 20th Ed. 19M
Test *j?tjjd fnr the analyses of Imidazolinone herbicides in solids and water.
N Corrgr,erna:
m
CP
m
m
m
B
.4
SubWttad By: TERRY DELLOC-ER
Purchase Order:
Report Date : I0104/2D10
Data Received. 0912912010
Date Sampled : 09127/2010
Hate and Time
Method
Test Started
Analyst
SM-4500-NH3C-TKN
101D112010 0819
JM
EPA-200.7
D913012010 08:45
i M
SM-4500441-13C
0913012010 09:15
JM
SM-450ONO3F
09130/2010 09.00
JM
SM-2540D
0913012010 14-15
MW
IRRIGATION WATER
09/30/2010 09-20
MW
IRRIGATION WATER
0913012010 09:20
MW
Pauric McGroary '
•
0

Report Number.
f D-272-0214
Page: T of 2
Account Number
46805
Send To: CROP PRODUCTION Sl=-WC rS
POB 2t49
WILSON , IVC 2-1894
Project: OUTFAU- 1 AND 21WATER SAMPLES
Lab Number: 78732
Sdrnple ld : OUTFALL 1
Analysis
A&L Eastern Laboratories Inc
rift tite�i em aa.ne4 vpp.q aitr I�gleiier to poq znwu
wwsi.Yr.r�oamn
REPORT OF ANALYSIS
Quantttation
Result.
Tclal Kjeldahl-N&ogen , mg1L
Limit
Pt�
Total ovhoras , nglt
1
Arnrnon;a Nitrogen. �� 1 A
0-1
c1
Nilra`l +N*jte-N , mg11C9
1
c1
Tofaf Suspended Solids, mg/L
1
D'15s ed Ma 38
Magnesium, ppm
1
3
Dissolved StrffaN , ppm
1
v Method Reference3
:
1
Methodsfor the Determinati
v Standard Methods on of Metals in Environmental Samples, EPAWD14-91-010,
for fhe Analysis of Water
Test
June 1991
N and Wastewater, 20th Ed. 1996
Ln
method for the N Cammerets: analg Of Irnfdazaftnone herbicides irr Soliand water.
awater.
Suhrnit ;1 By: TERRY DELLINGER
Purchase Order:
Raport Date : 1010412010
Data Received: 09/29/2010
Date Sampled : 09V2712010
Date and Time
Method Test Started
SM-45OMH3C-TKN
EPA 200.7
SM-4500-NH3C
SM-450(IN03F
StW-2540D
IRRIGATION WATER
IRRIGATION WATER
Tom& PC r
Pauric McGroary
1010112010 08:19
0913012010 08:45
0913012010 09:15
09*012010 09:00
09130/2010 14:15
0913012010 09:20
09130/201 D 0920
Analyst
JM
JM
JM
.1M
MW
MW
MW
•
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Chain oFCustody Record "UP5
' A & L Great Lakes Laboratories, Inc.
3505 Conestoga Drive • Fort Wayne, IN 46808-4414 - Phone [phone] - Fax [phone]
www.algreatlakes.com. - tab c@i atgreatlakes.com
I PARAMETERS
Account
Number: 77516
Submitted by: Crop Production Services
Contact: 841-1494ex-
e OeUmSrr
a.
'
Matrix
TYIX
Phone=. x3rJ'j+31
Fax
Address: PO Box 2149 Wilson, NC 27894
PON:
Project No.
Project Name/Locaiion: W' .a NG NG
Sample
Identification
Container
Number
Date
Sampled
Time
Sampled
Container
Type
Sample
Type
Sample Preservation
crn
Plank
Grob
Cam
cc'
Fes.
'vr+�Qa`
n�'
a
",,a
own
L
-lo
1
RIL
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t _
SPECIAL INSTRUCTIONS: (Please indicate any special detection limits, method numbers. QA/QC requirements. or highly hazardous sample.)
TURN -AROUND TIME: (circle one Standar Rush
ANALYZE SAMPLE: (circle one) As is Dry Weight Biosolid (Wet & Dry)
Matrix Types: Soil Wat Wastewater Sludge Plant Tissue Form ulationliank Mix Other (Please specify)
Sampled by:
(sits'—!
Date
Comments/Additional Instructions
(Prim Namc)
Time
Shipping Condition:
Relinquished by.
tsit t
Date
ShipperlWnybitttk
(wwe Name)
Time
� e S -
Received by:
isir„ LWO
Date
P ns e1 W- a 4 4- _t c.
tlkim Hann)
Tim!
4G1Cs
1
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_ •a
Permit No. NCS000338
S. Specific Storniwater Monitoring Requirements
The specific stormwater monitoring requirements includes both analytical and visual monitoring of
stormwater samples. Spccific monitoring requirements are defined below.
(1) Analytical Monitoring
9to6water Discharge
Charaqgdgja
Uad
Mmurement
affiu=11=2
Sample
Sample
a ' 3
Biochemical Oxygen Demand
m —.annually
grab
SDO
Cherrdcal OxZgen Demand
MW
annually
SDO
Total Suspended Solids
]DO
anntially
grab
SDO
Total Phosphorus
rr
minuafly
imb
SDO
Ammonium Sulfate
W
Altoannaallgrab
SDO
Total Kieldahl Nitre en
mol
annually
ab
SDO
Nitrate -Nitrite Nitrogen
171110
annually
grab
SDO
Ma nesium Sulfate
ETAarnuallgrab
$DO
Total Rainfs114
inches
-annually_
71at k4u'lred
minutes
annually
4 malec/
MG
annual!
—
Measurement Frequency: Once per calendar yeah. The facility must perform
analytical satrtpling during the first and last year of'thc permit term regardless of cut-
off concentration conditions.
2 Sample Type: Defined in Pan 11, Standard Conditions, Section A.
3 Sample Location: Samples to be taken at each stormwater discharge ou[Wl (SDO)
unless representative outfall status has been granted.
4 For each sampled representative storm event the total precipitation, storm duration,
and total flow must be monitored. Total flow shall be either, (a) measured
continuously, (b) calculated based on the amount of ama draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c)
estimated by the measurtment of flaw at 20 minute intervals during the rainfall
event.
Page 8 - .

4k
..���► NCDENR 17
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H, Sullins
Governor Director
September 22, 2010
Ms. Nancy Vincek, Operation Compliance Manager
Crop Production Services, Inc.
1160 Brake Road
Rocky — Mount, North Carolina 27801
SUBJECT: Compliance Evaluation Inspection
Crop Production Services Inc., Wilson Facility
NPDES Permit NCS000338
Wilson County
Dear Ms, Vincek;
Dee Freeman
Secretary
On September 17, 2010, Mitch Hayes of the Raleigh Regional Office conducted a compliance
evaluation inspection of the subject facility. The time and assistance of Terry Dellinger, Terminal
Manager, with this inspection was greatly appreciated. Below is a list of findings and recommendations
developed from the inspection:
1. The subject permit was issued March 26, 2010 and became effective April 1, 2010 and will
expire March 31, 2015.
2. The facility is a distribution site for dry and liquid fertilizers. There is one pesticide product
that is stored and sold in bulk. The pesticide is stored in an Aboveground Storage Tank
(AST) under roof, on a concrete pad. Liquid fertilizers are pumped directly from AST's
through a manifold system into tanker trucks. Potassium magnesium sulfate (K-Mag) is a dry
product and stored in a building. Bagged fertilizers are also stored in buildings on site.
3. Some items noted during the site review: The north side of the facility sits on a ridge and
slopes gently toward the southern end of the property. Outfall #1 is located in front of
property in a road ditch. Potential source of runoff exists from trucks carrying fertilizers when
entering and leaving the property. A gravel covered swell directs stormwater from the liquid
fertilizer manifold loading area to a storm drain. The storm drain is piped to a small catch
basin, Outfall #2, located behind the emptied anhydrous ammonia tanks. When the catch
basin is full, stormwater flows in a ditch parallel to a railroad spur on the property and into
another small catch basin. Stormwater from this catch basin flows via buried PVC pipe into a
very large catch basin which is connected to another very large catch basin by buried PVC
pipe. There was no stormwater in any of the outfalls or catch basins.
4. A copy of the permit was not on site. This makes it very difficult for the terminal manager to
follow monitoring schedules and be aware of permit conditions and requirements. Please
ensure that a copy of the permit is available at the facility. All elements of the Stormwater
Pollution Prevention Plan (SPPP) are not being updated. Qualitative and analytical
monitoring for Period 1 did not occur. Monitoring was last completed 06/16/2009. Please note
that failure to abide by the conditions and limitations contained in the permit may subject the
Permittee to a civil penalty up to $25,000 per day per violation.
North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone [phone] Customer Service
Internet: www,ncwaterquality.org 1628 Mail Service Center Raleigh, NC 27699-1628 FAX [phone]
An Equal Opportunity/Affirmative Action Employer — 50% Recycled110% Post Consumer Paper NOne
o hCarolina
Ammra!!il

Crop Production Services CEI
F
Page 2
5. A request,to. rescind the permit was made by you to the Stormwater Permitting Unit February
23, 2010. You based your request on the fact that the facility does not manufacture or blend
fertilizers on site. Currently this request is being reviewed. The Raleigh Regional Office will
provide the Central Office and the Stormwater Permitting Unit a recommendation regarding
your request. Please continue to operate under the stormwater permit until the Stormwater
Permitting Unit informs you of the decision to rescind the permit.
I would like to thank Terry Dellinger again for his time and assistance with this inspection. If you
have any questions about the inspection or this letter, please contact me at 919.791.4261 or by email
[e-mail]
Sincerely,
MQ��
f�W+
Mitch Hayes
Environmental Specialist
Cc: Permit Files
Central Files, Brian Lowther, Stormwater Permitting Unit
Terry Dellinger, Terminal Manager
P.O. Box 2149
Wilson, NC 27893

Compliance Inspection Report
Permit: NCS000338 Effective: 04/01/10 Expiration: 03/31/15 Owner: Agrium U S Inc
SOC: Effective: Expiration: Facility: Crop Production Services, Inc.
County: Wilson 2404 Wilco Blvd
Region: Raleigh
Wilson NC 27893
Contact Person: J Billy Pirkle Title: Phone: [phone]
Directions to Facility:
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
24 hour contact name Nancy Vincek Phone: [phone]
On -site representative Terry Dellinger Phone: [phone]
Related Permits:
Inspection Date: 09/17/2010 Entry Time: 10:15 AM Exit Time: 11:30 AM
Primary Inspector: Mitchell SHayes /j%j�� �� Phone: [phone]
Secondary Inspector(s): l
Reason for Inspection: Routine Inspection Type: Stormwater
Permit Inspection Type: Stormwater Discharge, Individual
Facility Status: ❑ Compliant IN Not Compliant
Question Areas:
Storm Water
(See attachment summary)
Page: 1

Permit: NCS000338 Owner - Facility: Agrium U S Inc
Inspection Date: 09/17/2010 Inspection Type: Stormwater Reason for Visit: Routine
Inspection Summary:
The facility is a distribution site for dry and liquid fertilizers. One pesticide product that is stored and sold in bulk. The
pesticide is stored in an Aboveground Storage Tank (AST) under roof, on a concrete pad. Liquid fertilizers are pumped
directly from AST's through a manifold system into the tanker truck. Potassium magnesium sulfate (K-Mag) is a dry
product and stored in a building. Bagged fertilizers are also stored in buildings on site.
The north side of the facility sits on top a ridge and slopes gently toward the southern end of the property. Outfall #1 is
located at in front of property in the road ditch. Potential source of runoff exists from trucks carrying fertilizers when
entering and leaving the property. A gravel covered swell directs stormwater from the liquid fertilizer manifold loading area
to a storm drain.'The storm drain is piped to a small catch basin, Outfall #2, located behind the emptied anhydrous
ammonia tanks. When the catch basin is full, stormwater flows in a ditch parallel to a railroad spur on the property and into
another small catch basin. Stormwater from this catch basin flows via buried PVC pipe into a very large catch basin which
is connected to another very large catch basin by buried PVC pipe. There was no stormwater in any of the outfalls or
catch basins.
A copy of the permit was not on site. All elements of the Stormwater Pollution Prevention Plan (SPPP) are not being
updated. Qualitative and analytical monitoring for Period 1 did not occur. Monitoring was last completed 06116/2009.
A request to rescind the permit was made to the stormwater permitting unit February 23, 2010. The rescision is based on
the fact that the facility does not manufacture or blend fertilizers on site. The Raleigh Regional Office recommends that
the permit be rescinded as long as fertilizers are not manufactured or blended on site.
Page: 2

Permit: NGS000338 Owner - Facility: Agrium U S Inc
Inspection Date: 09/17/2010 Inspection Type: Stormwater
Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes
No
NA
NE
Does the site have a Stormwater Pollution Prevention Plan?
■
❑
❑
❑
# Does the Plan include a General Location (USGS) map?
■
❑
❑
❑
# Does the Plan include a "Narrative Description of Practices"?
■
❑
❑
❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
❑
■
❑
❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
❑
■
❑
❑
# Has the facility evaluated feasible alternatives to current practices?
❑
■
❑
❑
# Does the facility provide all necessary secondary containment?
■
❑
❑
❑
# Does the Plan include a BMP summary?
■
❑
❑
❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
■
❑
❑
❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
❑
❑
❑
# Does the facility provide and document Employee Training?
❑
■
❑
❑
# Does the Plan include a list of Responsible Party(s)?
❑
■
❑
❑
# Is the Plan reviewed and updated annually?
❑
■
❑
❑
# Does the Plan include"a Stormwater Facility Inspection Program?
■
❑
❑
❑
Has the Stormwater Pollution Prevention Plan been implemented?
■
❑
❑
❑
Comment: The stormwater Pollution Prevention Plan has not been updated since
2008. According to a 1998 site plan, Outfall #2 is different from the sampling point for
Outfall #2 now being used.
Qualitative Monitoring
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
❑
■
❑
❑
Comment: Last monitoring was completed 06.16.2010.
Anglytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
❑
■
❑
❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
❑
❑
■
❑
Comment: Last monitoring was completed 06.16.2010.
Permit and Outfalls
Yes
No
NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
❑
■
❑
❑
# Were all outfalls observed during the inspection?
■
❑
❑
❑
# If the facility has representative outfall status, is it properly documented by the Division?
❑
❑
■
❑
# Has the facility evaluated all illicit (non stormwater) discharges?
❑
■
❑
❑
Page: 3

Permit: NCS000338
Inspection Date: 09/17/2010
Owner - Facility: Agrium U S Inc
Inspection Type: Stormwater
Comment: Facility has not evaluated non stormwater discharges for 2010. Last
evaluation was in 2008.
Reason for Visit: Routine
Page: 4

-44,
ti _ REPORT NO.
F099 73-8004
!N `A & L GREAT LAKES LABORATORIES,
75
.� + 3505 Conestoga Dr. Fort Wayne, IN 46808 • 260-483-4759 • FAX [phone]
www.algreallakes.corn - lab(Oalgreatlakes.com
QUALITY ANALYSES FOR INFORMED DECISIONS.
:.• . I��I�II���II��I�I�I���I��I��IJ���II�I��ILL„I��II
To: -CROP PRODUCTION SERVICES FOR: WILSON NC TERMINAL
PO BOX 2149 WILSON, NC
WILSON, NC 27894-2149
ATTN: BILL BAILEY
LAB NUMBER: 50573 REPORT OF ANALYSIS
• SAMPLE ID: OUTFALL 1
INC.
DATE SAMPLED. 6/16/2009 7:30
DATE RECEIVED: 6/22/2009 9:30
DATE REPORTED: 7/1 /2009 PAGE: 1 of 2
EAR L N M� Y57 A�E,�c� OD . FERf�ICE S•
R
Solids, Total Suspended 135 mg/L 1.0 LD 6/29/2009 SM-2540D
Nitrogen, Ammonia (as N) 0.39 mg1L 0.10 SH 6/29/2009 EPA-350.2
Nitrogen, Nitrate+Nitrite (as N) 0.58 mg1L 0.05 SH 6/23/2009 EPA-353.2
Nitrogen, Total Kjeldahl 19 mg/L 1 GVP 6/24/2009 SM4500 N(org)B and NH3C
Phosphorus, Total 0.53 mg/L 0.10 SH 6/24/2009 EPA-365.3
Magnesium 1.34 mg/L 0.23 MTG 6/29/2009 EPA-200.7
Sulfur (as Sulfate) 2 mg/L 0.5 MTG 6/29/2009 EPA-200.7
BOD, 5-Day 7 mg/L 1 SH 6/24/2009 SM-5210B
COD 69 mg/L 5 SH 6/29/2009 EPA 410.4
Add.

N REPORTNO.
F09173-8004
,�77516o -A & L GREAT LAKES LABORATORIES, INC.
r: 3505 Conestoga Dr. - Fort Wayne, IN 46808 - 260-483-4759 - FAX [phone]
www.algreatiakes.com - [e-mail]
QUALITY ANALYSES FOR INFORMED DECISIONS
�• .. I„I,II,,,II,�I,ICI,�.I„I„I,I„,Il,f„II,I,,,I,.II
TO: CROP PRODUCTION SERVICES FOR: WILSON NC TERMINAL
PO BOX 2149 WILSON, NC
WILSON, NC 27894-2149
ATTN: BILL BAILEY
LAB NUMBER: 50574
• SAMPLE ID: OUTFALL 2
REPORT OF ANALYSIS
DATE SAMPLED: 6/16/2009 7:30
DATE RECEIVED: 6/22/2009 9:30
DATE REPORTED: 7/1 /2009 PAGE: 2 of 2
L
t*
gig g.
IBM
0-1 INC
Solids, Total Suspended
8
mg/L
1.0
LD
6/29/2009
SM-2540D
Nitrogen, Ammonia (as N)
1.44
mg/L
0.10
SH
6/29/2009
EPA-350.2
Nitrogen, NIII Nitrite (as N)
1.71
mg1L
0-05
SH
6/23/2009
EPA-353.2
Nitrogen, Total Kjeldahl
15
mg/L
1
GVP
6/24/2009
SM-4500 N(org)B and NH3C
Phosphorus, Total
1.53
mg/L
0.10
SH
6/24/2009
EPA-365.3
Magnesium
1.85
mg/L
0.23
MTG
6/29/2009
EPA-200.7
Sulfur (as Sulfate)
4
mg/L
0.5
MTG
6/29/2009
EPA-200.7
BOD, 5-Day
5
mg/L
1
SH
6/24/2009
SM-521OB
COD
14
mg/L
5
SH
6/29/2009
EPA 410A
AAL

r}-
Sample Receipt Summary for Crop Production Services
COC Complete? Y Sufficient sample volume for analysis requested? Y Was sufficient ice used? N
Samples,intad 1 Good condition? Y Sample submitted within required Bolding time? N Temperature: 27.6 degrees C
Proper containers for analysis requested? Y Sample preserved correctly for analysis requested? N Packing material: Onfln Ice
Other Noted Compliance Issues: SAMPLES WARM ON ARRIVAL, SHIPPED OVER WEEK -END MAKING BOD OUT Receipt pH: NIA
OF HOLDING TIME. -
Shipper. UPS Ground
Tracking #_ 1Z2790E40350552512
Custody seals intact (if applicable): NIA
COC Complete? Y Sufficient sample volume for analysis requested? Y Was sufficient ice used? N Shipper. UPS Ground
•Samples intact I Good condition? Y Sample submitted within required holding time? N Temperature: 27.6 degrees C Tracking #: 1Z279OE40350552512
Proper containers for analysis requested? Y Sample preserved correctly for analysis requested? N Packing material: Onfin Ice Custody seals intact (if applicable): WA
Other Noted Compliance Issues: SAMPLES WARM ON ARRIVAL, SHIPPED OVER WEEK -END MAKING BOD OUT Receipt pH: NIA
OF HOLDING TIME.
i
.
•

FUV173-0004 Lakes Laboratories, Inc.
3505 Conestc IM®mIM111®Doff ® 68084414 - Phone [phone] - Fax [phone]
,.-,. ,..,..�............com - [e-mail]
/ PARAMETERS
Account 77516
Number:-
submitted by:
n] ser s C
Contact: Bill Bailey
Matrix
Type
Phone A5-2 33q 51+3 i .
Fax
Address: PO Box 2149 Wilson, NC 27894
PO#1:
Project Na -
Project NameA ocation:C , f„ fU
Sample
[dentificati Ems-
050573
l
ainer
nber
Date
Sampled
Time
Sampled
Container
'Type
Sample
Type
Sample Preservation
cry,
a
p}otic
cab
C�
r41c'
Fm
p-04 F<l
v 2
p
l
7: 30
✓✓
�
l a tt
rl 30
✓
FMrrr�y
050574
r'
SPECIAL INSTRUCTIONS: (Please indicate any special detection limits, method numbers, QA/QC requirements, or highly hazardous sample.)
lie?
L nify
URN -AROUND TIME: (circle one) tandar Rush
ALYZE SAMPLE: (circle one)(As [s Dry Weight Biosolid (Wet & Dry)
Matrix Types: Soil Cater Waste ater Sludge Plant Tissue Formulation/Tank Mix Other (Please specify)
Sampled by:
(Sip--)
Date
_ � $ �
Comments/Additional Instructions
l L (Print Name)
Time
a . DD A'/n
Shipping Condition:
Relinquished by:
(sigaftnv)
Date
Shipper/Waybili#:
(Print Name)
Time
S aV S
Received by:
- (Sig--)
Date
;� 2 -O `�sr-
N c4. � t^_ e,
/L� v T/V (print Naim)
Time
c
1 so

397 A & L GREAT LAKES LAL0JRATORIES, INC.
3505 Cones"a Drive - Fort Wayne, Indiana 46808-4414 - Phone [phone] FAX [phone]
www.algreadakes_com • [e-mail]
INVOICE
Royster-Clark, Inc.
Bill Bailey -
PO Box 2149
Wilson, NC 27894-2149
12/14/05 F05341-8013 556747
12/14/05 F05341-8013 556747
12/14/05 F05341-8013 556747
12/14/05 F05341-8013 556747
.12/14/05 F05341-8013 556747
�12/14/05- 1�05341-8013 556747
12/14105: F05341-8013 556747
12/14/d5 F05341-8013 556747
12/14/05 F05341-8013 556747
Federal ID No. 3S-1381134
77516
556747
Net 30 Days
12/31 /2005
1/31/2006
AFL .
WILSON NC TERMINAL: 1 / 2-
2
BOD, 5-Day
25.00
25.00
50.00
50:00
WILSON NC TERMINAL: 1 / 2
2
COD
20.00
20.00
40.00
40.00
WILSON NC TERMINAL: 1 / 2
2
Solids, Total Suspended
10.00
10.00
20-00
20.00
WILSON NC TERMINAL 1 / 2
2
Phosphorus, Total
15.00
15.00
30.00
30.00
WILSON NC TERMINAL: 1 12
2
Nitrogen, Ammonia (as N)
10.00
10.00
20-00
20-00
WILSON NC TERMINAL: 1 / 2
2
Sulfur (as Sulfate)
12-00
12.00
24.00
24.00
WILSON NC TERMINAL: 1 / 2
2
Nitrogen, Total Neldahl
20.00
20.00
40.00
40.00
WILSON NC TERMINAL: 1 / 2
2
Nitrogen, Nitrate+Nitrite(as N)
15.00
15.00
30-00
30.00
WILSON NC TERMINAL: 1 / 2
2
Magnesium
12-00
12.00
24.00
24.00
$278.00
Page 1

i REPORT NO.
F07037-8014
ACCOUNT NUMBIEm
77516
A & L GREAT LAKES LAdORATORtES, INC.
3505 Conestoga Drive • Fort Wayne, Indiana 46808-4414 • Phone 26d-483-4759 - FAX [phone]
www.algreatlakes.com • [e-mail]
`• II I I I Ito I I IIII I III I I I I Ito I I I I I I I IJ I I III I Is I I I I I I I II
TO: CROP PRODUCTION SERVICES
PO BOX 2149
WILSON, NC 27894-2149
ATTN: BILL BAILEY
LAB NUMBER: 14251
• SAMPLE ID: OUTFALL 1
FOR: STORMWATER
REPORT OF ANALYSIS
0
DATE SAMPLED: 2/2/2007 8:00 AM
DATE RECEIVED: 2/6/2007 12:1 O PM
DATE REPORTED: 2/12/2007 PAGE: 1
I ME:n N
-
UL
ilN
REPO t+iG
L4Mn-
INDL'Y5
ANAL St5�A�
ETHOD} . CEO- -
Solids, Total Suspended
38
mg/L
1-0
DT
2/12/2007
EPA-160.2
Nitrogen, Ammonia (as N)
0.18
mg/L
0.10
DT
217/2007
EPA-350.2
Nitrogen, Nitrate+Nitrite (as N)
4.02
mg/L
0.05
0.01 DT
2/8/2007
EPA-353.2
Nitrogen, Total Kjeldahl
2
mg/L
1
MG
2/7/2007
EPA-351.3
Phosphorus, Total
0.61
mg/L
0.10
DT
2/12/2007
EPA-365.3
Magnesium
1.14
mg/L
0.23
0.05 DT
2/9/2007
EPA-200.7
Sulfur (as Sulfate)
2
mg1L
0.5
0.1 DT
2/9/2007
EPA-200.7
BOD, 5-Day
3
mg/L
1
DT
2/7/2007
EPA-405.1
COD
BDL'
mg/L
5
DT
2/12/2007
EPA-410.1
A&L.�
" BDL - Below detection level of method utilized.

REPORT NO.
F07037-8014
ACCOUNT NUMBVK
77516
A & L GREAT LAKES LAIdDRATORIES, INC.
3505 Conestoga Drive • Fort Wayne. Indiana 4680&4414 . Phone [phone] • FAX 26U-483-5274
www.algreatlakes.com • [e-mail]
�.• .. • I��I�II���II��l�l�l���l.�I��I�I���II�l.�ll�l���l��ll
To: CROP PRODUCTION SERVICES
PO BOX 2149
WILSON, NC 27894-2149
ATTN: BILL BAILEY
LAB NUMBER: 14252
• SAMPLE ID: OUTFALL 2
FOR: STORMWATER
REPORT OF ANALYSIS
DATE SAMPLED: 2/2/2007 8:00 AM
DATE RECEIVED: 2/6/2007 12:10 PM
DATE REPORTED: 2/12/2007 PAGE: 2
-
ARA�IlETER
REStiL
gN .
� RT1NG
Mrf
lIADL
1'ST
ANALI!SIS�A
— -,:
METHOB, . CE
Solids, Total Suspended
14
mg/L
1.0
DT
2/12/2007
EPA-160.2
Nitrogen, Ammonia (as N)
BDL*
mg/L
0.10
DT
2/7/2007
EPA-350.2
Nitrogen, Nitrate+Nitrite (as N)
BDL*
mg/L
0.05
0.01
DT
2/8/2007
EPA-353.2
Nitrogen, Total Kjeldahl
2
mg/L
1
MIS
2/7/2007
EPA-351.3
Phosphorus, Total
0.96
mg/L
0.10
DT
2/12/2007
EPA-365.3
Magnesium
0.94
mg/L
0.23
0.05
DT
2/9/2007
EPA-200.7
Sulfur (as Sulfate)
2
mg/L
0.5
0.1
DT
2/9/2007
EPA-200.7
BOD, 5-Day
7
mg/L
1
DT
2/7/2007
EPA-405.1
COD
BDL*
mg/L
5
DT
2/12/2007
EPA410.1
ALL-1yIpL
` BDL - Below detection level of method utilized.

+keport: F0b133-b001
AccouW.: 7751 F'
' A & L GREAT LAKES LABORATORIES,
3505 Conestoga Dr. - Fort Wayne, IN 46808 - 260-483-4759 - FAX [phone]
www.algreatiakes.com - lab@algreatiakes-corn
QUALITY ANALYSES FOR INFORMED DECISIONS
TO: CROP PRODUCTION SERVICES FOR: STORMWATER
PO BOX 2149 WiLSON, NC TERMINAL
WILSON, NC 27894-2149
Arm_ BILL BAILEY
INC.
REPORT O F ANALYSIS DATE SAMPLED: 5/9/2098 7:15 AM
LAB NUMBER: 31418 DATE RECEIVED: 5/12/2008 9:40 AM
• SAt4PLE ID: 1 DATE REPORTED: 5121 /2008 PAGE: 1
KIM=
Solids, Total Suspended
36
mg/L
1
RH
5/19/2008
SM-2540D
Nitrogen, Ammonia (as N)
0.54
mg/L
0.10
AB
5/19/2008
EPA-350.2
Nitrogen, Nitrate1Nitrite (as N)
1.41
mg/L
0.05
RH
5/13/2008
EPA-353.2 `
Nitrogen, Total Kjeldahl
13
mg/L
1
MG
5/15/2008
SM-4500 N(org)B and
Phosphorus, Total
0.35
mg/L
0.10
AB
5/14/2008
.NH3C
EPA-365.3
Magnesium
0.93
mg/L
0.05
CRT
5/13/2008
EPA-200.7
Sulfur (as Sulfate)
6
mg/L
1
. CRT
5/13/2008
EPA-200.7
BOD, 5-Day
5
mg/L
1
RH
5/14/2008
SM-5210B
COD
38
mg/L
5
RH
5/19/2008
EPA 410.4
ALL

! Heport: r ub i J3-buu 1
Account 7751E
A & L .GREAT LAKES LABORATORIES, INC.
3505 Conestoga Dr. • Fort Wayne, IN 46808 • 260-483-4759 • FAX [phone]
' www.a[greatlakes.com • [e-mail]
QUALITY ANALYSES FOR INFORMED DECISIONS
To: CROP PRODUCTION SERVICES FOR: STORMWATER
PO BOX 2149 WILSON, NC TERMINAL
WILSON, NC 27894-2149
arrN: BILL BAILEY
REPORT O F ANALYSIS
DATE SAMPLED: 5/9/2008 T 25 AM
.
Las NUMBER: 31419 DATE RECEIVED: 5/12/2008 9:40 AM
SAMPLE ID: 2 DATE REPORTED: 5/21/2008 PAGE: 2
Solids, Total Suspended -
20
mg/L
1
RH
5/19/2008
SM-2540D
Nitrogen, Ammonia (as N)
0.53
mg/L
0.10
AB
5/19/2008
EPA-350.2 ,
Nitrogen, N itrate+ Nitrite (as N)
1.16
mg/L
0.05
RH
5/13/2008
EPA-353.2 _
Nitrogen, Total Kjeldahl
140
mg/L
1
MG
5/15/2008
SM-4500 N(org)B and-NH3C
Phosphorus, Total
0.71
mg/L
0.10
AB
5/14/2008
EPA-365.3
Magnesium
0-90
mg/L
0.05
CRT
5/13/2008
EPA-200.7
Sulfur (as Sulfate)
5
mg/L
1
- CRT
5/13/2008
EPA-200.7
BOD, 5-Day
4
mg/L
1
RH
5/14/2008
SM-5210B
COD
221
mg/L
5
RH
5/19/2008
EPA 410.4

REPORT NO.
F04245 -8001'. .
ACCOUNT NUMBER
775.16
A & L GREAT LAKES LABORATORIES, INC.
3505 Conestoga Drive • Fort Wayne. Indiana 46808 4414 • Phone [phone] • FAX [phone]
www.atgreadakes.com • lab9algreadakes.com
To: ROYSTER-CLARK, INC.
PO BOX 2149
WILSON. NC 27894-2149
ATTN: BILL BAILEY
•LAB NUMBER: 81694
SAMPLE ID: #1 -
t-oR: GRAB SAMPLES
OUTFALL 1 8 2
REPORT OF ANALYSIS
copy: ROYSTER CLARK
BEV TEVEBAUGH
6 EXECUTIVE DR
COLLINSViLLE IL 62234
DATE SAMPLED: 8/31/04 8:30AM
DATE RECEIVED: 9/1104 9:OOAM
DATE REPORTED: 918104 PAGE: 1
rn.#
�}° `tRFSLIL' _
RPARAWgQ
21'a
.ter`
=12 "`f�.;i�,.�ANAI�i�i'
DATE•
t
• Y
Solids, Total Suspended
112
mg/L
1 DT
9/7/04
EPA-160.2
Nitrogen, Ammorria (as N)
BDL"
mg/L
0.10 DT
9/8/04
EPA-350-2
Nitrogen, Nittrate+Nitrite (as N)
0.75
mg/L
0-20 DT
9/2/04
EPA-353.2
Nitrogen, Total Kjeldahl
7.0
mg/L
1.0 MG
9/7104
EPA-351
Phosphorus, Total
1.12
mg/L
0.10 DT
9/7/04
EPA-365.2
Magnesium
1.8
mg/L
1-0 DT
9/2/04
EPA-200.7
Sulfur (as Sulfate)
8
mg/L
1 DT
9/2/04
EPA-200.7
BOD, 5-Day
13
mg/L
1 DT
9/1/04
EPA-405.1
COD
40.0
mg/L
5.0 DT
917/04
EPA-410.1
BDL - Below detection level of method utilized.

REPORT NO
F02304-8007
ACCOUNT NUMBER
87039
A & L GREAT LAKES LABORATORIES, INC.
3505 Conestoga Drive • Fort Wayne. Indiana 46808-4413 • Phone [phone] • FAX [2601483-5274
www.algreatlakes.00m • lab@akjr+eadakes.com
I011ie nl�Inl�I�.II„i��L��lll,l.�l��l��ll��111411
TO: ROYSTER-CLARK, INC.
6 EXECUTIVE DRIVE•
P O BOX 1986
COLLINSVILLE, IL 62234-1986
ATTN. BEV TEVEBAUGH
•LAB NUMBER: 62852
SAMPLE ID: 2
FOR: GRAB SAMPLES FOR
OUTFALL #1, #2
REPORT OF ANALYSIS
IfIDtL
copy: ROYSTER CLARK
PO BOX 2149
WILSON, NC 27894
DATE SAMPLED: 10/30/02 9:15 AM
DATE RECEIVED: 10/31 /02
DATE REPORTED: 11/8/02 PAGE: 2
PARiWETER
RESULT:
UNIT
DETECTION
L]MR
ANALYST
ANALYSIS DATE
ME MOD REFERENCE
Solids, Total Suspended
15
mg/L
1
TS
11/4102
EPA-160.2
Nitrogen, Ammonia (as N)
0.71
mg/L
0.10
TS
11/6/02
EPA-350.2
Nitrogen, Nitrate+Nitrite (as N)
2.09
mg/L
0.20
TS
11/5/02
EPA-353.1
Nitrogen, Total Kjeldahl
7.0
mg/L
1.0
MG
11/5/02
EPA-351
Phosphorus, Total
1.31
mg/L
0.10
TS
11/4/02
EPA-365.2
Magnesium
16.0
mg/L
1.0
TS
11/7102
EPA-200.7
Sulfur (as Sulfate)
22
mg/L
1
TS
11/7/02
EPA-200.7
BOD, 5-Day
3
mg/L
1
LKP
10/31/02
EPA-405.1
COD
23.0
mg/L
5.0
TS
11/4/02
EPA-410.1
ARt

. a
REPORT NO.
*. F02304-8007�'
ACCOUNT NUMBER
87039
r
A & L GREAT LAKES LABORATORIES, INC.
3505 Conestoga Drive • Fort Wayne. Indiana 46808-4413 • Phone (260]483-4759 • FAX [phone]
www.algreaUakes"com • [e-mail]
To: ROYSTER-CLARK, INC.
6 EXECUTIVE DRIVE
P0BOX 1986
COLLINSVILLE, IL 62234-1986
ATTN: BEV TEVEBAUGH
&B NUMBER: 628551
SAMPLE ID: 1
FOR: GRAB SAMPLES FOR
OUTFALL #1, #2
REPORT OF ANALYSIS
copy: ROYSTER CLARK
PO BOX 2149
WILSON, NC 27894
DATE SAMPLED: 10/30/02 9:00 AM
DATE RECEIVED: 10/31/02
DATE REPORTED: 1 118/02 PAGE: 1
PARAMETER
=' RESULT=
UNIT''" '
DETECTION' "
LIMIT:
ANALYST
-
ANALYSIS DATE
METHOD REFERENCE
Solids, Total Suspended
107
mg/L
1
TS
11/4102
EPA-160.2
Nitrogen, Ammonia (as N)
0.15
mg/L
0.10
TS
11/6102
EPA-350.2
Nitrogen, N6ate+Nitrite (as N)
5.82
mg/L
0.20
TS
11/5102
EPA-353.1
Nitrogen, Total Kjeldahl
2.0
mg/L
1.0
MG
11/5/02
EPA-351
Phosphorus, Total
0.22
mg/L
0.10
TS
11/4102
EPA-365"2
Magnesium
2.0
mg/L
1.0
TS
11/7/02
EPA-200.7
Sulfur (as Sulfate)
10
mg/L
1
TS
1117102
EPA-200.7
BOD, 5-Day
1
mg/L
1
LKP
10/31/02
EPA-405.1
COD
35.0
mg/L
5.0
TS
11/4/02
EPA-410.1
A&I

REPORT NO.
F04245-8001
ACCOUNT NUMBER
77516
u
A & L GREAT LAKES LABORATORIES, INC.
3505 Conestoga Drive • FOrC Wayne, Indiana 46808-4414 • Phone 26G483-4759 • FAX 260-4B3-5274
www alureatlakes.com • [e-mail]
`�• - ' I..III..JI..I.#.i..,1.J.JJ...II.L.I1.L.,1..11
TO:' ROYSTER-CLARK, INC.
PO BOX 2149
WiLSON, NC 27894-2149
ATTN. BILL BAILEY
11
•LAB NUMBER: 81695
SAMPLE ID: #2
FOR: GRAB SAMPLES
OUTFALL 1 & 2
REPORT OF ANALYSIS
copy: ROYSTER CLARK -
BEV TEVEBAUGH
6 EXECUTIVE DR
COLLINSVILLE IL 62234
DATE SAMPLED: 8/31 /04 8:35AM
DATE RECEIVED: 9/1/04 9:00AM
DATE REPORTED: 9/8104 PAGE: 2
am. Z-Allt
Z�5; p5AZ mr—ffl�
9-1- 1 � � -!-19
Solids, Total Suspended
42
mg1L
1
DT
917/04
EPA-160.2
Nitrogen, Ammonia (as N)
16.52
mg/L
0-10
DT
9/8104
EPA-350.2
Nitrogen, Nitrate+Nitrite (as N)
76.56
mg/L
0-20
DT
9/2104
EPA-353.2
Nitrogen, Total Kjeldahl
19.0
mg/L
1-0
MG
9/7/04
EPA-351
Phosphorus, Total'
3.49
mg/L
0.10
DT
9/7104
EPA-365.2
Magnesium
32.0
mg[L
1-0
DT
912/04
EPA-200.7
Sulfur (as Sulfate)
28
mg./L
1
DT
9/2104
EPA-200.7
BOD, 5-Day
9
mg/L
1
DT
9/1/04
EPA-405.1
COD
30.0
mg/L
5.0
DT
9/7/04
EPA-410.1
AJL.