Loading...
HomeMy WebLinkAboutNCS000303_MONITORING INFO_20180926--"---STORIVIVHATER-DIVISfON-CODING"SHEET -------- PERMIT NO. Ncs a)b�6D� DOC TYPE El FINAL PERMIT MONITORING INFO APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ Zz(PJ Oq Z (p YYYYMMDD F/ l % Craig Fulcher deAfteAAM Environmental, Health & Safety Manager eFzzm SPX Transformer Solutions, Inc. Aem 07 craig.fulcher@spx.com 7d 0 T 919 288 8378 S P X WAUKESHNX September 26, 2018 Division of Water Quality RECEIVED Attn: Central Files OCT 0 8 2018 1617 Mail service Center Raleigh, North Carolina 27699-1617 CENTRAL FILESDWR SECTION RE: Discharge Monitoring Report for SDO-001 for August 2018 To Whom it May Concern: Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) August 2018. Due to the lack of flow for the month of August this was a "No Flow" event and the DMR is filled out accordingly. This fulfils the requirement of the Stormwater Permit NCS000303, Tier lI monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Craig Fuicher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27530 www.spxtransformerwiLitions.com Permit Number NCS000303 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from s; the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAMPLE(S) Kristen Lowder/AECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific MonitoringRe uirements Outfall No.. Date Sample Collected pH Total Rainfall molddl r S.U. Inches SDO 001 NO FLOW ND = Non Detect Outfall No. Date Sample Collected TSS Oil & Grease moldd/ r m m SDO 001 NO FLOW ND = Non Detect Outfall No. Date Sample Collected PCBs Total Nitrate mo/ddl r mg1L m SDO 001 NO FLOW ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note. No Flow was available in August 2018. Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) rart is: v entcte maintenance AC vity ivionnoring Ke utrements Outfall Date ; 50050 , ` . =00556: ': " -00530 00400 No. _ Sample Total Flow Total=. - - Oil:&_Giese N :No =-. :Total pH New"Motor Collected 6 ;(iLapplicable)= Rauifall (tf'appl:} :' O&GLYPH " 'Suspended = Oil' -Usage (Method,1664= Solids �SGT''HEM), ifs qpp :. mo/dd/Yr : MG:: ;inches meLl ..: _ M24: unit :: 2allmo STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Watcr Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 September 26, 2018 Division of Water Quality Attn: Central Files 1617 Mail service Center Raleigh, North Carolina 27699-1617 RE: Discharge Monitoring Report for SDO-001 for July 2018 To Whom it May Concern: f'I WAUKESHNA RECEIVED OCT 08 2018 CENTRAL FILES DWR SECTION Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) July 2018. No parameters were recorded over the benchmarks. The facility is still under monthly monitoring due to the Tier II status of previous months. This fulfils the requirement of the Stormwater Permit NCS000303, Tier II monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27530 www.spxtransformersolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAMPLE(S) Steven PiresIAECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific MonitoringRe uirements Outfail No. Date Sample Collected pH Total Rainfall mo/dd/ r S.U. Inches SDO 001 07/30/2018 7.43 0.00* ND = Non Detect Outrall No. Date Sample Collected TSS Oil & Grease mo/dd/ r m m SDO 001 07/30/2018 6.9 <4.8 ND = Non Detect Outfall No. Date Sample Collected PCBs Total Nitrate moldd/ r m m SDO 001 07/30/2018 <0.0005 1.1 ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note: Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Momtortne Reauirements OutfaD No. Date' Sample 50050 ''0DSS6::: 00530. 00400 Total Flow _Total _ _ Oil'&'Grease- Non -polar Total pIi` . New Mofor Collected (if applicable) Rainfall . (if appl.). O&G/TPH ' :Suspended Oil_Usage (Method 1664 ', Solid s: . SGT-HEM), if:; mo/dd/yr MG inches '' -`' mvJl mall` unit 'gallmo STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date: 07/30/2018 Attn: Central Files Total Event Precipitation (inches): 0.00* 1617 Mail Service Center Event Duration (hours): (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 d (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) *Rain gauge onsite had not been emptied during the previous week. Therefore, historic rainfall data obtained from a local NOAA climate station was reviewed. The Iocal station reported no rain; however, the storm event on 7/30118 was isolated and resulted in discharge from the outfall after a hard, short 10 — 20 minute rain event. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of 2 - (=,-/1F (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 AM NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit; hh tp //portal.ncdenr.ori! jweb,a/npdes-stormwater/ Permit No.: or Certificate of Coverage No.: Facility Name: /ec { t_ f few County: iJJr--1 h e_ Phone No. "'V I -- 1 6 7-7 Inspector: Date of Inspection: Time of Inspection: Za } k. a •ter �l � i� Wc. S `�` Total Event Precipitation (inches): v d Qf'e,,,rr� '�'(� ��5t �k S0 LvtS�>PiG Q O OA C.iGi awl I,& Was this a "Representative Storm Event" or "Measureable Storm Event" as defined y he permit? (See information below.) ,tjelC, , . � fi p� \.Jus ks s L.6a t S�G fio4 Yes ❑ No vio ra-\o-, weu '.N _ r+- Please verify whether Qualitative Monitoring must he performed during a "representative stor-rrT- it /o — 29 �� rm event" or "measureable storm event" (requirements vary, depending on the permit). PJl1 Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this sign,aI ire, I certify at t Kreport is accurate � to the best of my knowledge: (Signature Page 1 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: D p r Outfall No. a-"0 { Structure ( ipe, ditch, etc.] Receiving Stream: nJt "s9t, Lve.r Describe the industrial activities th t o cur within the outfall drainage area: TrS�. 2. Color: Describe the color of the dis (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4 arm 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 �3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 C.% 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 � 3 4 5 7. Is there any foam in the stormwater discharge? Yes Pam' B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Nr t Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 aceAnalytical e »vrwpewlebs.com August 09, 2018 Craig Fulcher SPX Transformer Solutions, Inc. 2701 Highway 117 South Goldsboro, NC 27530 RE: Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 Dear Craig Fulcher: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NEIAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc; Jennifer Wheat, AECOM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 Pace Analytical Services, LLC aceAnalyticale 9800 KinceyAve. Suite 100 Huntersville, NC 28078 w»wpeaelabacom (704)875-9092 CERTIFICATIONS Project: Slormwater (SPX Goldsboro) Pace Project No.: 92393866 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical www,p&cwobs.com SAMPLE ANALYTE COUNT Project: Stormwater (SPX Goldsboro) Pace Project No.; 92393866 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92393866001 SDO-001 SM 2540D-2011 SOB 1 PASI-E EPA 1664B JMS 1 PASI-C EPA 608.3 PKS 9 PASI-C TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 BRJ 1 PASI-A EPA 353.2 Rev 2.0 1993 CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical www.pamlebxcnm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 Sample: SDO-001 Lab ID: 92393866001 Collected: 07/30/18 14:20 Received: 07/31/18 08:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 6.9 mg/L 2.5 1 08/01/18 15:21 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 4.8 1 08/09/18 05:19 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 12674-11-2 PC13-1221 (Aroclor 1221) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 11104-28-2 PCBA232 (Aroclor 1232) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 11141-16-5 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 53469-21-9 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 12672-29-6 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 11097-69-1 PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 08/02/18 07:52 08/03/18 13:38 11096-82-5 Surrogates Tetrachloro-m-xylene (S) 31 % 60-140 1 08/02/18 07:52 08/03/18 13:38 877-09-8 S5 Decachlorobiphenyl (S) 43 % 60-140 1 08/02/18 07:52 08/03/18 13:38 2051-24-3 S5 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.1 mg/L 0.52 1 08/07/18 17:37 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 361.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 0.69 mg/L 0.50 1 08/02/18 16:51 08/03/18 03:13 7727-37-9 353.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.01993 Nitrogen, NO2 plus NO3 0.44 mg/L 0.020 1 08/07/18 12:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 ,�aceAnalyticalo www.pecekbaoorn QUALITY CONTROL DATA Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 QC Batch: 422384 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92393866001 METHOD BLANK: 2338196 Matrix: Water Associated Lab Samples: 92393866001 Blank Parameter Units Result Total Suspended Solids mg/L ND LABORATORY CONTROL SAMPLE: 2338197 Spike Parameter Units Conc. Total Suspended Solids mg/L 250 Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Reporting Limit Analyzed Qualifiers 2.5 08/01/1815:14 LCS LCS % Rec Result % Rec Limits Qualifiers 232 93 90-110 SAMPLE DUPLICATE: 2338198 92393748003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 13.4 18.6 32 D6 SAMPLE DUPLICATE: 2338199 92393748004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6.0 14.4 82 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical e www.P xc= QUALITY CONTROL DATA Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 QC Batch: 423879 Analysis Method: EPA 1664B QC Batch Method: EPA 16648 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92393866001 METHOD BLANK: 2345115 Matrix: Water Associated Lab Samples: 92393866001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 4.8 08/09/18 05:17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2345116 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 38.5 37.7 98 78-114 MATRIX SPIKE SAMPLE: 2345117 35407941002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 21.1 38.5 58.2 96 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnalytical" www.pat�efa6acom QUALITY CONTROL DATA Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 QC Batch: 422567 Analysis Method: EPA 608.3 QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol Associated Lab Samples: 92393866001 METHOD BLANK: 2338858 Matrix: Water Associated Lab Samples: 92393866001 Parameter Units PCB-1016 (Aroclor 1016) ug/L PCB-1221 (Aroclor 1221) ug/L PCB-1232 (Aroclor 1232) ug/L PCB-1242 (Aroclor 1242) ug1L PCB-1248 (Aroclor 1248) ug/L PCB-1254 (Aroclor 1254) ug/L PCB-1260 (Aroclor 1260) ug/L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % LABORATORY CONTROL SAMPLE: 2338859 Blank Result Reporting Limit Analyzed Qualifiers ND 0.50 08/03/1814:29 ND 0.50 08/03/1814:29 ND 0,50 08/03/1814:29 ND 0.50 08103/1814:29 ND 0.50 08/0311814:29 ND 0.50 08103/1814:29 ND 0.50 0810311814:29 45 60-140 08103/1814:29 SO 47 60-140 08/03/1814:29 SO Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Decachlorobiphenyl (S) % 82 60-140 Tetrachloro-m-xylene (S) % 49 60-140 SO MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2338860 2338861 MS MSD 92393578001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Decachlorobiphenyl (S) % Telrachloro-m-xylene (S) % 43 70 60-140 SO 29 34 60-140 SO Results presented on this page are In the unite indicated by the "Units" column except where an aRemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical e wwtwpecakb&com QUALITY CONTROL DATA Project: Stormwater {SPX Goldsboro} Pace Project No.: 92393866 QC Batch: 422741 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92393866001 METHOD BLANK: 2339571 Associated Lab Samples: 92393866001 Parameter Units Nitrogen, Kjeldahl, Total mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 08/03/18 03:49 Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)B75-9092 LABORATORY CONTROL SAMPLE: 2339572 Spike LCS LIDS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg1L 10 9.5 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2339573 2339574 MS MSD 92394071001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.5 10.6 105 105 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2339575 2339576 MS MSD 92393889002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 6.6 10 10 17.D 16.1 105 96 90-110 6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate un@ Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalytical " wirmpnoela tcom QUALITY CONTROL DATA Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 OC Batch: 423394 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2:0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92393866001 METHOD BLANK: 2342282 Associated Lab Samples: 92393866001 Parameter Units Nitrogen, NO2 plus NO3 mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 08/07/1811:26 Pace Analytical Services, LLC 9800 Kincey Ave. Sulte 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2342283 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg1L 2.5 2.6 . 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2342284 2342285 MS MSD 92394405001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL ND 2.5 2.5 1.4 1.4 57 57 75-125 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2342286 2342287 MS MSD 92393999004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL ND 2.5 2.5 2.4 2.2 97 89 75-125 9 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 Pace Analytical Services, LLC 9800 acemalxical Hu'ntersvlle, NC1280778 www.pscelabs cam (704)875-9092 QUALIFIERS Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. 5o Surrogate recovery outside laboratory control limits, S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Dale: 08/09/2018 01:44 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 14 aCaAnalytical� xnrxcpenie &c= QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704 )875-9092 Project: Stormwater (SPX Goldsboro) Pace Project No.: 92393866 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92393866001 SDO-001 SM 254OD-2011 422384 92393866001 SDO-001 EPA 1664E 423879 92393866001 SDO-001 EPA608.3 422567 92393866001 SDO-001 TKN+NO3+NO2 423551 Calculation 92393866001 SDO-001 EPA 351.2 Rev 2.0 1993 422741 92393866001 SDO-0D1 EPA 353.2 Rev 2.0 1993 423394 Date: 08/09/2018 01:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. EPA 608.3 422636 EPA 351.2 Rev 2.0 1993 422833 Page 11 of 14 Document Name: Document Revised: February 7, 2018 Sample [ondition Upon Rece! t SCUA Page 1 of 2 Document No.: Issuing Authority: f ace.4na1 real F-CAR-0-033-Rev.06 Pace Carolinas Quality Off Ice Laboratory receiving samples: Asheville ❑ Eden Greenwood Huntersville2 Raleigh[] MechaniesvilleC] Client Name: Upon RoctiptY • Project p: Courier: _ ❑FedFx __❑UPS_ _ _❑USPS_ _ _._ _ Client _.❑Commercial n0ace . - — []Other; WO#:92393866 -�-1I I��I�II:I.I_Iai l�l4aalall�._ -�.. I Custody Seal Present? [:Dyes [2Wo Seals Intact? ❑Yes ffNa Date/Initials Person EMamining Contents: J Packing Material: ❑Bubble Wrap Bubble Bags []None ❑ Other Biological Tissue Fraten? Thermometer: ❑Yes to ❑N/A 7R Gun ID: 92TO40 Type of Ice: (aWet ❑Blue []None Cooler Temp ('C): CCorrection Factor: Add/Subtract rC) +0.4 Temp should be above freezing to VC Cooler temp Corrected(�CI:' r []Samples out of temp criteria. Samples on Ice, cooling process hasbegun USDA Regulated Sall ([E -N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source iinternatlonally, [:]Yes []No including Hawaii and Puerto Rico)? ❑Yes ❑Na Comments/Discrepancy: Chain of Custod Present? oVeS No N/A 1. Samples Arrived within Hold Time? Yes []NO N/A 2. Short Hold Time Analysis -72 hr.)? rlVeS 40NO UNIA 3. Rush Tum Around Time Requested? Yes Erho N/A 4. Sufflclent Volume? es ONG N/A S. Correct Containers Used? -Pace Containers Used? (Yes Del []NO JJN0 ❑N/A ❑N/A 6. Containers Intact? Cbs QNo N/A 7. Dissolved analysis: Sam les Field Filtered? MYes []No -Un/A S. Sample labels Match COC? -Includes Date/Time/io/Anal sis Matrix: Oyes []No []N/A 9. Headspace In VOA Vials (:�5.6mm)7 Yes QN0 A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes On Caft ❑N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review:_ Field Date Required? Oyes ❑ho Date: 07--3 1 ? QQ Date: --4- �J \ U Page 12 of 14 Document name: Document Revised: February 7, 2018 a ceAnalWical /. Sample Condition Upon Recel t SCUR Page 1 of 2 Document No.: issuing Authority: — F.0 -0-033•Rev.A6 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DDC, LLHg **Bottom half of box is to list number of bottle Project a WO# : 92393866 PM: NMG Due Date: 08/09/18 CLIENT: 92—SPX Golds a a z 7! G E e��y eY `J ` 2Ee+ L y n a E N = z a o E VI V 9 u .-1 1IR u V a g a E ., i, v a v E d ry z'Itj Z a 39 a a E A n z y E /V�� �y 7 ° 12 C E a`r r� y t� rl a c E n V n E < .i v v i d E o N z �Cj `� :J d a E $ TO /y N O �' aE 'd p o tE a f ? D EJa pa 1 « 9i �' �'n M $ ... °' (LM M .i x " R ,I /�V ry = z � E Jp� IV Z z z .0 a E ... Q q Tb J{ F p N v Y C q 1 2 3 4 \\NN. I N�s\ I 6 7 N\\ N N\��\ N NN 10 11 12 pH Adjustment Log for Preserved Samples Semple ID Type of Preservative pH upon recelpt date preservation adjusted Time preservation adjusted Amount of Preservattve added Lot # Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will Ue sent to the North Carolina DEHNR Certification Orfice (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers. Page 13 of 14 v 1 CHAIN -OF -CUSTODY 1 Analytical Request Document -" The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Completed accurately. Section A Section a Section C Required Ctient Information: I Required Project Intonation: Invoice Intonation: Page : 1 Of 1 Company, SPX Goldsboro I = Report Tm Craig Fulr w Atlentwr iA vl L cie �r Address: 2701 H' 117 South I . Copy To: TQ A IfewtiC' [n1 Company Name. C 60-1 , Goldsboro. NC 27530 I i,r r. G P.0 -� (.�N'i Address: W atfn*1SC Rmic Gt.✓lV`Z. - --A- _ __ - - Email: I 1 Purchase Drder #- Paco Ouole: Phone: Fax I ProjedName: Stortnrater rp)}- Pace ProjectManager rtiab. Iabs.eorri r-_state!1.6=0oa_-. - Requested Due Date: I Project 4; Pace Profile Or 8430.1 NC _ _.-. = 31 t uq,x ccos ,,,T f S 0 COLLECTED z Preservatives } - - Z ! Or" "Wore Gw v S V I W" WT WaOe Wee WW '3 m V N Z SAMPLE ID Pm P a N° a > (tt7, t? START END p m Fy: } One Character per box. W W T WO 4 zAN t cc jA z o a r. I AR oaw dT 0 LL w z M S 2sarwic ids must be unique Taxes SS K W n O g : W', y p .� m _ W m `2 w DATE TIME DATE TIME _= x z z D r O a >r C -oo T�3� lyZa I X L 2- 1=:4 X 7 ` ! apt' I� 11 ADC nDKAL, C.=Mim B `I f F•-• - 1€ l '.� � = SYIAFFUJA1TDN . �N:E• - - T[YE: - - AC�T®BYIAFFi1.lA,110N _ DAiE i]ME ShAtPI.E CONDISWNS I' SAMPLER NAME AND SIGNATURE . I a m PRINT Name of SAMPLER.\ m W g= m m z SIGNATURE of SAMPLER: DATE Signed:-� 0 v m m a aw`a Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fuicher@spx.com T 919 288 8378 July 31, 2018 Division of Water Quality Attn: Central Files 1617 Mail service Center' Raleigh, North Carolina 27699-1617 RE: Discharge Monitoring Report for SDO-001 for June 2018 To Whom it May Concern: 4 WAUKESHA A RECEIVED AUG 0 7 2018 CENTRAL FILES DWR SECTION Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) June 2018. Due to the lack of flow for the month of May this was a "No Flow" event and the DMR is filled out accordingly. This fulfils the requirement of the Stormwater Permit NCS000303, Tier lI monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 1117 South, Goldsboro, NC 27530 www,spxlransforrnersolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAMPLE(S) Nick Shore/AECOM PHONE NO.919-581-1577 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected PH' Total Rainfall moldd/ r S.U. inches SDO 001 NO FLOW ND = Non Detect Outfall No. Date Sample Collected TSS Oil & Grease moldd/ r mg1L m SDO 001 NO FLOW ND = Non Detect Outfall ''No. Date Sample Collected PCBs Total Nitrate moldd/ r m mgjL SDO 001 NO FLOW ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note: No Flow was available in June 2018. Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form S WU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no (if yes, complete Part B) Part B: vehicle Maintenance Activitv Monitortna Reauirements OutfaU - _a No. Date-.' Sample 50050 �` - -00556 0053-0.' - -00400_ - `Total Flow Total Oil & Grease Non -polar Total pA :New. Motor. Collected (if applicable) Rainf all f; &GlTP_ S::!dd_ en ' Oil Usage- ;(Method 1664�' Solids -�- x,;.'� iapp1 �mol inclie n Ui llM STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) W MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAMPLE(S) Nick Shore/AECOM PHONE NO. 919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. ##12, 5342, 37706 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Part A: SDecinc Monitoriniz Reauirements Outfall No., Date Sample : .Collected• pH Total: Rainfall " mo)dd/ r S.U. inches SDO 001 NO FLOW ND = Non Detect Outfall No. Date Sample Collected TSS Oil''& Grease mo/dd/*r mPjL mgJL - SDO 001 NO FLOW ND = Non Detect Odtfall.; Date No Sample PCBs . Total Nitrate ,Collected,: mo/dd/ r , m m SDO 001 NO FLOW ND = Non Detect RECERIPP JUN 2 r RECEIVED JUN 2 5 2018 CENTRAL FILES DWR SECTION Note: No Flow was available in May 2018. Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form SWU-247, last revised 1/1/1012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activitv Monitoring Keauirements Outfall., Date - 50050.: 00556 00530 0040EI" No. Sample Total Flow . ;;` _Total Oil & Grease " Non -polar Total pH ;` New'Motor Collected. (if applicable). Rainfall '(if.appl.) O&G/TPH Suspended Oir"age (Method 1664 Solids 'SGT-HEM), if - - a 1. mo/dd/vr A MG linches min mall;.. ' unit - ✓ . eaUmo STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm Permit Number NCS000303 Z-15-17- (Date) Form SN •Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 May 22, 2018 Division of Water Quality Attn: Central Files 1617 Mail service Center Raleigh, North Carolina 27699-1617 WAUKESHA 71 RECEIVED MAY 2 4 2018 CENTRAL FILES DWR SECTION RE: Discharge Monitoring Report and Qualitative Monitoring Report for SDO-001 To Whom it May Concern: Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report and Qualitative Monitoring Report for the sampling that occurred on April 24, 2018. This fulfils the requirement of the Stormwater Permit NCS000303, First Period, Year 6. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, % I a�� Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27530 www.spxtransformersolutions.com Permit Number NCS000303 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wad PERSON COLLECTING SAMPLE(S) Nick Shore/AECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Part A: S ecific MonitoringRequirements Outfall Date.- Na. ' Sample pH. Total - Collected Rainfall mold inches- SDO 001 04/24/2018 5.96 0.09 ND = Non Detect Outfall Date No. Sample TSS Oil & .Grease Collected. mo/dd/ r m mgtL SDO 001 04/24/2018 217 <5.0 D ND = Non Detect Outfall Date No: ' Sample PCBs Total Nitrate Collected: moldd/ r m m SDO 001 4/24/2018 <0.00050 mg1L 2.1 ND ND = Non Detect Note: SDO-001 was in exceedance for the benchmark for TSS and is now in a Tier II condition. SDO-001 was in exceedance for the benchmark of pH and is now in a Tier I condition for pH. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no (if yes, complete Part B) Vart W. Vehicle Maintenance Activity Monitoring xeouirements Out -fill`: Date 50050' 00556 00530 00400.:; No. Sample...," ample Total E16w, ;: Total ; Oil & Grease— Non -polar..:• -Total pH New'Motor Collected .: (if applicable) Rainfall (if_appl) ' O&G/TPH '. Suspended Oil Usage (Method 1664. Solids `SGTHEM): if appl. = mo/dd/vr ` -MG inches m�J[ ,mafl unit eal/mo STORM EVENT CHARACTERISTICS: Date 04/23/2019 Total Event Precipitation (inches): 0.09 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ft (Signature E z L / S' (Date) Permit Number NCS000303 Form SW-U-247, last revised 21212012 Page 2 of 2 A�A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: htt/portal.ncdenr.org/web/ir/npdes-stormwater/ Permit No.: N/C/S / 0 / / e // o/ 3/ or Certificate of Coverage No.: Facility Name: SfX ca s `ems County: Phone No. -e' Inspector: Date of Inspection: i a3 Ao Time of Inspection: Y9 � A A4 Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ryes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours a prior, The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee 11obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: Cn 0 igriature of Permittee or Designee) Pagel of Z sWU-242, Last modified 7/31/2013 1. Outfall Description: Outfali No. S Dc-o01 Structure (pipe, ditch, etc.) Receiving Stream: Un 'j OF wAwj,-w✓ Describe the industrial activities that occur within the outfall drainage area: /4 f "fX 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: tdr.,, 1qr,..,,,4 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): o—t- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 O 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: @1 2 )!§, 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. B. 9. 1 2 V Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes No Is there evidence of erosion or deposition at the outfall? Yes NN 10. Other Obvious Indicators of Stormwater Pollution: List and describe Na - J-jr- ,- Aoff -4 -'Me� o�-' sra.,� Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 aceAnalyticale eww.pocabb mm May 03, 2018 Craig Fulcher SPX Transformer Solutions, Inc. 2701 Highway 117 South Goldsboro, NC 27530 RE: Project: Stormwater Pace Project No.: 92382508 Dear Craig Fulcher: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NEL AC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Wheat, AECOM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services. LLC, Page 1 of 14 c'eAnalytical wwwpecobamrn Project: Stormwater Pace Project No.: 92382508 Pace Analytical Services, LLC 9800 KinoeyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #:12 Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exr;ept in full, without the written consent of Pam Analytical Services, LLC. Page 2 of 14 I eAnalytical www:pacefabscom SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92382508 Analytes Lab 1D Sample ID Method Analysts Reported Laboratory 92382608001 SDO-001 EPA 1664B JMS 1 PASI-C EPA608.3 PKS 9 PASI-C SM 2540D MVC 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA351.2 CJH1 1 PASi-A EPA353.2 DMN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aCf'eAnalytical' wwwpambbmm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)87&9092 Project: Stormwater Pace Project No.: 92382508 Sample: SDO-001 Lab ID: 92382608001 Collected: 04/24/18 0&56 Received: 04/26/18 08:36 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quaff HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 5.0 1 05/03/18 05:38 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 04/27/18 20:59 05101/18 15:11 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 04/27/18 20:59 06/01/18 15:11 11104-28-2 PCB-1232 (Aroclor 1232) NO ug1L 0.50 1 04/27/18 20:59 05/01/18 15:11 11141-16-5 PCB-1242 (Aroclor 1242) NO ug1L 0.50 1 04/27/18 20:59 05/01/18 15:11 53469-21-9 PCB-1248 (Aroclor 1248) NO ug1L 0.50 1 04/27/18 20:69 05/01/18 15:11 12672-29-6 PCB-1254 (Arodor 1254) NO ug1L 0.50 1 04/27/18 20:59 05/01/18 15:11 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 04/27/18 20:59 05/01/18 15:11 11096-82-5 Surrogates Tetrachloro-m-xylene (8) 49 % 60-140 1 04/27/18 20:59 05/01/18 15:11 877-09-8 S5 Decachiorobiphenyl (S) 60 % 60-140 1 04/27/18 20:59 05/01/18 15:11 2051-24-3 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 217 mg/L 25.0 1 05/01/18 20:50 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.1 mg/L 0.52 1 06/03/18 11:12 361.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1.5 mg/L 0.50 1 05/02/18 04:07 7727-37-9 353.2 Nitrogen, NO2IN03 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.67 mg/L 0.020 1 05/01/18 14:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 10, Analytical www.pscewmcom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92382508 QC Batch: 409045 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92382508001 METHOD BLANK: 2269372 Matrix: Water Associated Lab Samples: 92382508001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 05/03/18 05:26 Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (744)875-9092 LABORATORY CONTROL SAMPLE: 2269373 Spike LCS LCS % Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 38.5 38.1 99 78-114 MATRIX SPIKE SAMPLE: 2269374 35388937002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 1 A U 38.5 37.9 98 78-114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 a�eAnalytical www.pawsbs.aom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92382508 QC Batch: 408348 Analysis Method: EPA 608.3 QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol Associated Lab Samples: 92382508001 METHOD BLANK: 2265929 Matrix: Water Associated Lab Samples: 92382508001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 05/01/18 12:00 PCB-1221 (Aroclor 1221) ug/L ND 0.50 05/01/18 12:00 PCB-1232 (Aroclor 1232) ug/L ND 0.50 05/01/18 12:00 PCB-1242 (Aroclor 1242) ug/L ND 0.50 05/01/18 12:00 PCB-1248 (Aroclor 1248) ug/L ND 0.50 05/01/18 12:00 PCB-1254 (Aroclor 1254) ug1L ND 0.50 05/01/18 12:00 PCB-1260 (Aroclor 1260) ug/L ND 0.50 05/01/18 12:00 Decachlorobiphenyl (S) % 83 60-140 05/01/18 12:00 Tetrachloro-m-xylene (S) % 52 60-140 05/01/18 12:00 SO Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 VO4)875-9092 LABORATORY CONTROL SAMPLE 8 LCSD: 2265930 2265931 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Cone, Result Result % Rec % Rec Limits RPD RPD Qualifiers Decachlorobiphenyl (S) % 78 83 60-140 Tetrachloro-m-xylene (S) % 57 54 60-140 SO Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, LLC. 0 Page 6 of 14 adeAnalytical e wwwpaaefaWom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92382508 QC Batch: 408609 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382508001 METHOD BLANK: 2267183 Matrix: Water Associated Lab Samples: 92382508001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/01/18 20:50 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2267184 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 256 102 90-110 SAMPLE DUPLICATE: 2267185 30250799001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 327 376 1406 SAMPLE DUPLICATE: 2267186 92382746001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1860 1960 5 Results presented on this page are In the units indicated by the `Units" column except where an alternate unit Is presented to the right of the resutL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aLeAnalytical� 19rrw0800w a.cxm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92382508 QC Batch: 408557 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92382508001 METHOD BLANK: 2266927 Matrix: Water Associated Lab Samples: 92382508001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 05/02/18 03:41 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2266928 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Neldahl, Total mg/L 10 9.9 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2266929 2266930 MS MSD 92382471001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Neldahl, Total mg/L 2.3 10 10 12.4 12.4 102 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2266931 2266932 MS MSD 92382501004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 28.7 10 10 47.0 47.2 184 186 90-110 0 M6 Results presented on this page are In the units Indicated by the "Units" column except where an aRernate unit is presented to the right or the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 I.A.Analyiical' 0 pacaowacom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92382508 QC Batch: 408531 Analysis Method: EPA 353.2 OC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92382508001 METHOD BLANK: 2266810 Matrix: Water Associated Lab Samples: 92382508001 Btank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.020 05/01/18 14:08 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntetsville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2266811 Spike LCS LCS % Rec Parameter Units Cane. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2266812 2266813 MS MSD 92382587004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.013.1 2.5 2.5 2.1 2.1 83 83 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2266814 2266815 MS MSD 30250921003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.1 2.5 2.5 3.2 3.1 81 80 75-125 1 Result presented on this page are In the unite Indicated by the'Unit' column except where an a@emate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 05/03/2018 03:22 PM without the written consent of Passe Analytical Services, LLC. Page 9 of 14 PaceAnalyticai Services, LLC ac"eAnalytical a 9800 Kincey Ave. Suite 100 Hunteraville, NC 28078 xarw.peoelabs.WM (704)875-9092 QUALIFIERS Project: Stormwater Pace Project No.: 92382508 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG -Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. SO Surrogate recovery outside laboratory control limits. 85 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/03/2018 03:22 PM without the written consent of Pace Analytical Services, I.I.C. Page 10 of 14 adeAnalyficale wwwpeo0Aft0)M k QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92382508 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92382508001 SDO-001 EPA 1664E 92382508001 SDO-001 EPA 608.3 92382608001 SDO-001 SM 2540D 92382508001 SDO-001 TKN+NO3+NO2 Calculation 92382608001 SDO-001 EPA 351.2 92382508001 SDO-001 EPA 353.2 Date: 05/03/2018 03:22 PM 409045 408348 EPA 608.3 408609i 409125 408557 408531 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 408637 Page 11 of 14 ' - • Document Name: Document Revised: February7, 2018 Sample Condition Upon Rece1 t(SCUR) Page 1 of 2 Document No-4 Issuing Authority: aceAnoticaiN F-CAN-CS-033•Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[:) Greenwood ❑ Client Name: —upon Rr(elpt P4 Project Courier. Fed Ex UPS USPS Client ❑ Commercial (ace ' ❑¢ther: Raleigh[] Mechanicsville❑ `9238°2�508� �N� i. Custody Seal Present? Des � Seals tntltttT ❑Yes %�� Date/InitialsPersonExamining "Lqbwt�� Packing Material: ❑Bubble Wrap 1,01bble Bags []None ❑ Other Blologl 1 Tissue Frozen? Yo N A Thermom tGun ID: 991936 Type of Ica: et ❑ffiue ©Nona ❑ 111������ ❑ I Cooler Temp rrection Factor: Add Subtract ' e p (C} / { 1 +4.1 T *phould be above freezing to 6'C Gaoler temp Corrected ples out of temp criterla. Samples on ice, cooling process lign USDA Regulated SoII\iN/A, water sample) Old samples originate in'a quarantine zone within the Untied States: CA, NY, or SC (check maps)? old rgmpies ariginate from a foreign source (interpganally, 1—iYes n, r-Q indudlna Rawall and Puerto Ricnli f1Yes UMd Comments 01scre a Chain of Custody Present? Y s ONO N A 1. Samples Arrived within Hold Time? es ONO N A 2. Short Hold Time Analysis 472 hr.)? b Yes o N A 3. Rush Turn Around Time Requested? Yq N ONJA 4. Sufficient Volume? Y NO N A S. Correct Containers Used? -Pace Containers Used? s (:]No No ❑N/A ONJA 6. Containers Intact? CEJQ ONa ' N A 7. Dissolved analysis. Samples Field Flitered? ❑Yet ONo AZW S. Sample Labels Match COC? -Includes Datefnme/1D/Anal is Matrix: 17T"' 9yp (:IN. NIA 9. `� r �_VA__ ` Heads ace in V0A Vials >S-6mm ? Oyes 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Oves UNo NIA 'ID? A. 11. COMMSNTS/SAMPLE DISCREPANCY Field Date Required? ❑Yes ❑Na off- r �t ,rot Q Person contacted: �' ° Date/Tlme: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Page 12 of 14 Document Name: Document Reprised: February 7, 2018 sampleCondition U Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: L'BAflBiytlL"dr< F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is Project #' �� verified and within the acceptance range for preservation W0# j49238250`5. samples. PM :` NMG Ous Date .,'05/07/.113�. Eeceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, UHg CL 1ENT 92 SPx.. Ga l ds'Y r **Bottom half of box Is to list number of bottle u� pH Adjustment log for Preserved Samples Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot Al Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. out of hold, incorrect preservative, out of temp, Incorrect containers. Page 13 of 14 / CHAIN -OF -CUSTODY ! Analytical Request Documen The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be complet d a rcurately. Section A section 8 section C Regldred Client bdormation: Requh'ed Project 1140HI &ML briolce bdarmstkw Page Of 1 Garnproy: SP%Goidsboro Report To: Fjdf4 & 2701 Howisy 117South Copy To: — i w�„l- Qrr�.-.u,.-. ConWarryNa7ro: Goldsboro, NC 27530 � l+n: . 7 � nr,.� --. r.c.•- ". zr. 1 - Email: Purchase Order e: Pace Qr.ote: Phom Fmc Propo Name: Startrnaaty Pace Project Manager. nimle. tabz.Corrr. - °-:.>7,, Requested Due Date: Project t Pace Prarlle 0: 0430-1 NG IrnTRM Cane .$ COLLECTED x Preservatives Yt: Onnkkry was Ow v U 2 _ Z \Nov NfT m $ m O w - O SAMPLE ID Pr°m'e p n" a i START EHD O U 5 One Character Par box. VA"wP .. W < a Z @ W r to Z, 0-9 / r) Smltple Ida rnrrti tfar Akr aO&W a Sraw 76 o W F 9 M g o z y.� ~ NN � i O z i DATE TIME DATE TIME .s o_ F O A r y x ,� x cry t .2 24 c.r Y• )tt.iY B' 40 12 - t� -�, '�`-.' .AOdTtONItE:m�ls�YrB_x: -- �• ,R9]AIGEAWED6YIAfFaIATtON QA7F>' -- 77ItE it ACr�P1iS�$Yf_ a ;TOtE,�;, • 8lIItPLf s- _ � F _ �.._,OA1E� S �. ���.P -z�ju U'd3r� , 2f1� SAMPLER NAME AIiEO SIGNATURE , - PRINT Name of SAMPLER SIGNATURE of SAMPLER DATE Signed _ $ s m a t Craig fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 WAUKESHA A May 10, 2017 Division of Water Quality Attn: Central Files 1617 Mail service Center Raleigh, North Carolina 27699-1617 RE: Discharge Monitoring Report and Qualitative Monitoring Report for SDO-001 To Whom it May Concern: Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report and Qualitative Monitoring Report for the sampling that occurred on April 17, 2017. This fulfils the requirement of the Stormwater Permit NCS000303, Second Period, Year 5. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, . ' 441 4�4 e7 Craig Fulcher Environmental, Health & Safety Manager REC MAY 15 2017 CENTRk Fr LSS DWR SECTION SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27630 www.spxtransfortnersolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAMPLE(S) Jenna Bacic/AECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected pH Total Rainfall mold r S.U. inches SDO 001 04/17/2017 6.6 0.06 ND = Non Detect Outfall No. - Date Sample Collected TSS Oil & Grease mo/d r m m SDO 001 04/17/2017 233 v.0 ND = Non Detect Outfall No. 'Date Sample Collected PCBs Total Nitrate mold m mgtL SDO 001 4/17/2017 1 ®.00050 mg/L 14.5 ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note: SDO-001 was in exceedance for the benchmark for TSS and is now in a Tier I condition. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activ!q Monitoring Requirements Outfall Date 50054 -- SV= -- QQ556.' `� :y t1Q530 µ• t00400 ,. Sample Tata1 Flow Total, _ Od & Grease h Non polar :Total pHzs" New Motor Collected _ (tf applicable) Rainfall x 'y� (if a�pl) }9&G/TPH `Snspeuded � _ OdUsage >' (Method 1664 . "Solids . A? ' x : 4 5 f SGT REM), «" tno/d MG` 'line hes al{mo' Y' ; m nnif: STORM EVENT CHARACTERISTICS: Date 04/17/2017 Total Event Precipitation (inches): 0.06 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C (Signature of Permit Number NCS000303 S-/0 -12 (Date) Form SWU-247, last revised 21212012 Page 2 of 2 RIMA WEDAFLA Stormwater Discharge Outfali (SDO) Qualitative Monitoring Report Forguidance on filling out thisforrk please vlslt: http;/mortal.ncdenr.orgtmb/lrinpdgs--stormwateE/ Permit No.: J/CIELI-0/Q1�?1_01Af or Certificate of Coverage No.: Facility Name: K County: Phone Inspector: Omda ULCAC, Date of Inspection: Time of Inspection: Total Event Precipitation (Inches): 0.06" I 10-t6A.W �.Q1�Z�. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) �/Yes 0 No Please verify whether Qualitative Monitoring must be performed during a "representative storm event"or "measureablestorm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event° is a storm event that measures greater than 0.1 Inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter Interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By thi tgnature, I certifyL$!�t this report is accurate and complete to the best of my knowledge: of Permittee Pagel of 2 SWU-242, Last modified 7/31/2013 i. Outfail Description: Outfall No!�M- I Structure (pipe, ditch, etc.) 1/ t Receiving Stream: Describe the Industrial activities that occur within the outfall drainai M Z. Color: Describe the color of the discharge using bas' olors (red, bKown, blue, ) and tint (H ed um, dAr.,as igscriptors:LoA�r ����'��� 3. Odor: Describe any distinonet", odorse discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): 4.' Clarity: Choose the number which best describes the cl of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating s lids: (�-V ��"��r)t1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 11s no solids a d 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 0. Is there an oil sheen in the stormwater discharge? Yes 9. is there evidence of erosion or deposition at the outfall? es No 10. other Obvious Indicators of Stormwater Pollution: VAO Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 n �J aceAnalytical • WmPecaft com April 27, 2017 Craig Fulcher SPX Transformer Solutions, Inc. 2701 Highway 117 South Goldsboro, NC 27530 RE: Project: Stormwater Pace Project No.: 92337411 Dear Craig Fulcher: Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9082 Enclosed are the analytical results for sample(s) received by the laboratory on April 18, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Wheat, AECOM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 (�Ia'cmnalyficale www.pecsirl5mm CERTIFICATIONS Project: Stormwater Pace Project No.: 92337411 i Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification We 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida)NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Vlrginla/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow (toad Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginlafVELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 a aceAnalytical e www.pecakebs.com SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92337411 Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92337411001 SDO-001 SM 2540D CTB 1 PASI-E EPA 1664B JMS 1 PASI-C EPA 608 RES 9 PASI-C TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA 353.2 DMN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 ceAnaly 019 rrww.pacelebe.carrr ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92337411 Pace Analytical Services, LLC 9800 Kincey Ave. suite 100 Huntersvltle, NC 28078 (704)875.9092 Sample: SDO-001 Lab ID: 92337411001 Collected: 04/17/17 10:00 Received! 04/18/17 08:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 233 mg/L 6.1 1 04/19/17 13:52 HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 04/25/17 06:49 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016) ND uglL 0.50 1 04/21/17 13:25 04/24/17 14:51 12674-11-2 PCB-1221 (Aroclor 1221) ND ug1L 0.50 1 04/21/17 13:25 04/24/17 14:51 11104-28-2 PCB-1232 (Aroclor 1232) ND ug1L 0.50 1 04/21/17 13:25 04/24/17 14:51 11141-16-5 PCB-1242 (Aroclor 1242) ND ug1L 0.50 1 04/21/17 13:25 04/24/17 14:51 53469-21-9 PCB-1248 (Aroclor 1248) ND ug1L 0.50 1 04/21/17 13:25 04/24/17 14:51 12672-29-6 PCB-1254 (Aroclor 1254) ND uglL 0.50 1 04/21/17 13:25 04/24/17 14:51 11097-69-1 PCB-1260 (Aroclor 1260) ND uglL 0.50 1 04/21/17 13:25 04/24/17 14:51 11096-82-5 Surrogates Tetrachloro-m-xylene (S) 65 % 20-110 1 04/21/17 13:25 04/24/17 14:51 877-09-8 Decachlorobiphenyl (S) 46 % 20-136 1 04/21/17 13:25 04/24/17 14:51 2051-24-3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 4.5 mg/L 0.12 1 04/26/17 17:54 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 3.6 mg1L 0.50 1 04/26/17 00:25 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.97 mglL 0.020 1 04/26/17 10:32 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 ceAnalyfical www.paoviabs.oum QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92337411 QC Batch: 357208 Analysis Method: SM 2540D QC Batch Method: SM 2640D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92337411001 METHOD BLANK: 1981499 Matrix: Water Associated Lab Samples: 92337411001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/19/17 12:54 Pace Analytical Services, LLC 9800 KlnoeyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE! 1981500 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 260 104 90-110 SAMPLE DUPLICATE: 1981627 92337468001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 164 165 1 SAMPLE DUPLICATE: 1981744 92337468002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 11.8 10.2 14 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical. www.pacalalmoom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92337411 QC Batch: 357838 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 ITEM, Oil and Grease Associated Lab Samples: 92337411001 METHOD BLANK: 1984972 Associated Lab Samples: 92337411001 Parameter Units Oil and Grease mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/25/17 06:40 Pace Analytical Services, LLC 9800 Kincey Ave. Sufte 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1984973 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 38.2 96 78-114 MATRIX SPIKE SAMPLE: 1984974 92336894004 Spike MS MS % Rea Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 37.3 93 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC, Page 6 of 14 ceAnalytical www.pecghbs.rxlm QUALITY CONTROL DATA Project: Stormwaler Pace Project No.: 92337411 QC Batch: 357593 Analysis Method: EPA608 QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB Associated Lab Samples: 92337411001 METHOD BLANK: 1983519 Associated Lab Samples: 92337411001 Parameter PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Decachlorobiphenyl (S) Tetrachloro-m-xytene (S) Matrix: Water Units Blank Result Reporting Limit Analyzed Qualifiers ug1L ND 0.50 04/24/1711:52 uglL ND 0.50 04124/1711:52 ug1L ND 0.50 04/2411711:52 uglL ND 0.50 04/2411711:52 ug1L NO 0.50 0412411711:52 uglL ND 0.50 04/2411711:52 ug/L ND 0.50 04/24/1711:52 % 75 20-138 04/24/1711:52 % 76 20-110 04/24/1711:52 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)876-9092 LABORATORY CONTROL SAMPLE & LCSD: 1983520 1983521 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Decachlorobiphenyl (S) % 86 76 20-138 Tetrachloro-m-xylene (S) % 87 82 20-110 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resutt REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www.peceleba.mm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92337411 QC Batch: 357736 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92337411001 METHOD BLANK: 1984303 Matrix: Water Associated lab Samples: 92337411001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg1L ND 0.50 04/26/17 00:15 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersvllle, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1984304 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mglL 10 10.0 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984305 1984306 MS MSD 92337394001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone, Result Result % Rec % Rec Limits RPD Qual Nitrogen, Neldahl, Total mglL 6.7 10 10 16.6 16.6 98 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984307 1984308 MS MSD 92337867003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 1.2 10 10 11.1 11.7 100 105 90-110 5 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalyticale www.peoNebs.com QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92337411 QC Batch: 357829 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92337411001 METHOD BLANK: 1984929 Associated Lab Samples: 92337411001 Parameter Nitrogen, NO2 plus NO3 Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg1L ND 0.020 04126/1710:24 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1984930 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mglL 2.5 2.5 99 90.110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984931 1984932 MS MSD 92337763001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec . Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 1.6 2.5 2.5 4.1 4.1 103 102 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984933 1984934 MS 'MSD 92337355002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.37 2.5 2.5 2.7 2.7 93 92 75-125 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 ace I Analytical wnrW.Pm tbmam QUALIFIERS Project: Stormwater Pace Project No.: 92337411 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 KlnceyAve. Sulte 100 Huntersviile, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable, SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Dale: 04/27/2017 08:49 AM without the written consent of Pace Analytical Services, I.I.C. Page 10 of 14 11 ceAnaljftal e www.p�cw QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92337411 Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 26078 (704)875.9092 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92337411001 SDO-001 SM 2540D 357208 92337411001 SDO-001 EPA 1664E 357838 92337411001 SDO.001 EPA 3510 357593 EPA 608 357758 92337411001 SDO-001 TKN+NO3+NO2 358169 Calculation 92337411001 SDO-001 EPA 351.2 357736 92337411001 SDO-001 EPA 353.2 357829 Date: 04/27/2017 08:49 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Uccument Name: E51 Tech 5poe Uocument Revised; Sept. 21, 2016 i le Condition Upon Recel SOUR Page 1 of 2 Document No.: Issuing Authority: FCAR-GA- W3-Rov.02 Pace Ouallty Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh® IV1ec:6njtsvlile[] Client Name: WO ,:92337411. ' djPX `, ICourier. UFed Protect �,' ❑ Commercial ❑Pa e� ups [:]Other LJUSPS Rent r: 01,2111 73a u Custody Seal Present? Dyes ARO Seals Intact? Dyes gNo T Datellnitlals Person Examining Contants Packing Maternrial: ❑Bubble Wrap ubble Bags [:]None.e. []Other:r: / ��� Thermaeter. ®I R Gun ID: — IS-3492 _ Type of ba: t []Blue ©None DSamplas on ice, cooling process has begun CorrectioonFactorcAwa-o Cooler Temp Corrected ('Cj: Biological Tissue Frozen? ❑Yes []No �14/A ting to 6'C Temp should be abovekaarantlne y.�yy USDA Regulated Soil (/A, water sample) Did same! s r[ginate In []Yes IWO zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (in ' tlonally, Including Hawaii and Puerto Rico)? Dyes o Cantmant Dls on , Chain of Custody Present? 3, Samples Arrived within Hold Time? 2. short Hold TimaAna s 02 hr.? 3. Rush Turn Around Time ested? 0 13 4. Sufficient Volume? S. Correct Containers Used1 -Pace Containers Used? Iff � 0 � 6. Containers Intact? Samples Field Filtered? B: Note IF sediment is visible In the dissolved container Sample Labels Match COO -includes 0ate/Time/ID/Anal05 ri/H! 9. Head ace In VOA Vials >6-6mm ? Yes No N 10. Trip Blank Present? TripBlank CustodySeals Present? Yes o Yes No ❑ No H N 1L CLIENT NQTIF"'rI0WRESOLUTION Person Contacted; Date/rlme: Comments/Sample Discrepancy; Project Manager SCURF p� Review: NVA — -- Date: Field Data Required? UYes U,iNo Project Monejer SRIF Review: 64^ Date: .--4�la Note: Whenever there Is a discrepancy alleCt" North CaTollna Compliance samples, a copy of this form will be sent to the North Caroline DEHNR Certification Office (I.e. Out of hold, Incorrect preservative, out of temp, incorrect contalners) Page 12 of 14 uocument Name: mw tech Spec uocument xev►sea: Sept. Eli i.ulb Sample Condition Upon Rocef SCUR page 2 of 2 Document No.: Issuing Authority:. F-W-QA•003.Rev.02 Pace Quall office "Check mark top half of box if pH and/or dechlorination Protect N - is verified and with in the acceptance range for �O ' 9.233741.1 preservation samples. - PM: NMG Due Date: '04/27t 17 *'"Bottom half of box is to list number of bottles CLIENT: '92 SPR Golds �. ..mod. pH Adjustment log for Preserved Samples sample 10 7ype Of pmervative pH upon reMpt pate pmervation adjusted Time Preservation adjusted Amount of freea metive added Lot # .� Page 13 of 14 I r CeAnalXicaC- CHAIN-OF-CUSTODY 1 Analytical Request Document The Chain-of-Cumody is a LEGAL DOCUMENT. AII retevant fields must be completed a="*. Q Section A Section B Section C 1 !Z FP, ' of Required CherO Irdprin31i0n: Required Project IMetrttasian: Invoice Irdaitniary al elf- SPX Goldsboro Report To- Craig Fulrher Aftenbom 2701 Highway 117 South Copy TO: Jennifer Wheat (jenni%r.wheat®aecom.com) company name: REGULATORY AGENCY Goldsboro; NC 27530 Addrew. F NPDES r— GROUNDWATER F DRINKING WATER r UST F RCRA r OTHER Emm1 To: P rctmm Order No.: pm= Chao daren[s: Phone' Far Awn Name: Stormwater —l"oled nko1e.gasiorowski@pacelabs.00M She t..ocatioe srAr,F: NC Requested Duo DwIxITAT: RIj d Number Pam PrerY C 8430-1 Requested Ana"Is Filtered (Y40 Section D Vaud Matrbi Codes fz Rtrt{Tdntl Ckntt4ien M sRx yob - M COLLECTED Preservatives > N .N N N ORae41G WATER CN U Z WATER WT b e Q WASTEWATER MW 8 Q CCrFOSTE CDNPOWTE f PROULXT P 04 START Epon3 Ae 2 A OL ron OL SAMPLE ID W i = K 0E; U1 F W m „AR (A-Z, 0-9 1;) 07"M Or to ui as to mM m Sample IDS MUST BE UNIQUE thSrt TS O a a eo S! m o U V O o 0 — s a a U m <7 x Q to c d v Ito 9a33�`I 1( a `o o z�mm mm a� m m DATE TIME DATE TIME w st x x x z z p Ix Pace Project Not Lab J.D. 1 SDO - oat Wr s x x x x x x a 3 4 i 6 7 a g 10 Y1 12 .11, LL ADDEnONAL COMMENTS Quis BY 1 Ai=Fli.IATIOri DATE TIME BY IAFFMKMON DATE TDIE SAMPLE CONDITIONS SAtIPLER NAME AND SIGNATURELO u c O -• c PRINT Name o1 SAMPLER, p G _ d SIGNATURE of SAMPLER. u 3 _ g E IYTE mpomarm Noe: ey s+la um em Iam yW am accoWtoV Pacds NET 30 / i to -I day ptrymerq tnrtncaM apreeirq m fate charge of t.5x px nwNh for IIIWlICe3 not pW witltYa 30 «aye. F-Ali-Q-020tev.09, 12-0Ct-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 FACILITY NAME SPX PERSON COLLECTING SAMPLE(S) Craig Fulcher/SPX CERTIFIED LABORATORY(S) Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall mo/dd/ r MG inches SDO 001 NA NA NA Unable to sample this quarter due to no flow or unsafe conditions SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Wayne PHONE NO.919-581-1677 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. RECEIVE DEC 01 2016 CENTRAL FILES DWR SECTION No Samples were collected for these outfalls during the first sampling period of 2016 through October 30 Form SWU-247, last revised 21212012 Page 1 of 2 Permit Number NCS000303 Doe this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no (if yes, complete Part B) rart is: vemcee maintenance AC vity iviLonitoring mequirements Oiitfall Date 50050 . 00556 _ _ :60530.. .. '; 00400 ". "Total;Flow Total .. -Oil-& Grease- Non -polar- _ Totak pH New, Motor No: " Sample Collected (if applicable). ` `Rainfall S (if apply-..O&G/TPH -Suspended' `.Oi1:Usage t : 'SGT=HEM), if 'app;,- - molddtvr MG ^ • _ . inches: mgJl .: - mg/l unit: sallmo STORM EVENT CHARACTERISTICS: Date 10/30/2016 Total Event Precipitation (inches): _NA Event Duration (hours): NA (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature o ermittee) (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidanceonfilling out this form, please visit: hht n:/th2o.enraa.nc.uslsu/Fonna 17oa peat t ml Permit No.: IY19111J VI 01J9_3f or Certificate of Coverage No.: Facility Name: + a County: WakIrIc Phone No. q l4 — 5g 1- i V 7 7 Inspector: Qx Date of Inspection: Time of Inspection: Total Even t' Precipitation (inches); o 10 Was this a Representative Storm Event? (See information below) [Yes ❑ No ED MAY, 2 3 2w CENTRAL FILES DWR SECTION Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A 'Representative Storm Event" Is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, r certify that this roport is Ocurate and complete to the best of my knowledge: (Signature 1. Outfall Description: Oatfall No. 00.1 Structure (pipe, ditch, etc.) C kl: Receiving Stream: 1 Describe the industrial activities that occur within the outfall drainage area: rn ' �. 6) A 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: IluIL_ 3. Odor; Describe any distinct odors that the discharge may have.{i,e., smells strongly of oil, weals chlorine odor,'etc-):-1,���se Page 1 of 2 SWU-242-112608 d 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: Ci 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: Cj 2 3 4 5 66 Suspended Solids: Choose the number which best describes the amount of suspended solids in the storinwater discharge, where 1 is no solids and 5 is "ftmely muddy: 2 3 4 5 G 7. Is there any foam In the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes Eo) 9. is there evidence of erasion or deposition at the outfall? Yes No y 10. Other Obvious Indicators of Stormwater Pollutlon; List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further Investigation, swtl-242-112MB Page 2 of 2 STORMWATER DISCHARU OUTFALL (SDO) MONITORING RTPORT Permit Number NCS FACILITY NAME Irtern tw PERSON COLLECTING SAMPLE(S) rS CERTIFIED LABORATORY(S) _ V c, c_-t. Lab #t tE 0 Lab # Part A: Spectffc Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR , (This monitoring report shall be reoclved by the Division no later than 30 days from the date the facility rectives the sampling resul#s from the laboratory.) COUNTY i6 ja (! ne PHONE NO. R l • SIGNATURE OF PERMIPTRE OR DESIGNEE REOMRED ON PAG E 2, KIM Does this facility perform Vehicle Mabsenaace Actfviiirs using more than 55 p1lons of new motor oil per month? _ yes �no (if3es. cwnPiete Pmt B) Part S: Vehicle Maintenance Activity Monitorlm Reauirements ` N W14V. Sampletor Collected `' -r•. .. o7V1C�•CC• ,` t 'rjti: V4RW00530-.VaL7LL i . a iicalilalolfsll s L )- " p t�ZPH; (Method l664 Sided SoifWs. ' l Wiw Md Uil iT m01 '*: ",, holies, 4:.' iu [tact O Form S WU-247, last revised 2WO12 Page 1 of 2 STORM EVEW CHARACTERISTICS: Date Total Event Predpltadon (Inches): Event Duration (hoots): (only if applicable — see permit.) (if more than one atom event was sampled) Date Total Event Precipitation (inches): Eventbumbon(houra):(only if applicable —see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center lialelg% North Carolina 27699-1617 "I certify, under penalty or law, that this document and all attachments were prepared Under my direction or supervision in aoeordanee whb a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted is, to the beat of my knowledge and beliefs true, accurate, and complete. I am aware that there are signiffeant penalties for sabmitttag false Informatiou, including the possi bil ity of tmzss and imp n t for knowing violations." .S'- ZO -16 (Signature of Permittee) (Date) Form SWU-247, last nwL9edZW012 Page 2 of 2 ceftlyb`cal e xrrrxpeoadabs.+:ers April 22, 2016 r Mr. Johnny Baines Eastern Environmental Management PO Box 4030 518 S. Pearl Street Rocky Mount, NC 27803 RE: Project: SPX Pace Project No.: 92293583 Dear Mr. Baines: Pace Analytical BeMces, Ina. 98001(hceyAve. Suite 100 Huntersvllle. NC 28078 (704)878-4092 Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report Analyses were performed at the Pace Analytical Services location Indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures or: Ms. Cathy Baines, Eastern Environmental Management REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, wuhout the wrlden consent of Pace Analytical Services. Inc.. Page 1 of 13 Paco Analytlnal Srrrvlon, Ine- aceAnalytical a VaOD 1QnceyAve. Suite i00 HunlmAlle, NC 28078 W#WPM*d& om (704)878.9092 CERTIFICATIONS Protect: SPX Pace Project No.: 92293383 Charlotte Certification IDs Him iGncey Ave. Ste 100, HmAersvlfle, NC 28078 South Carolina Certification t 99M6001 North Carolina Ddnldng Water Certification 0: 37708 Florida/NELAP Certification 0: E87627 North Carolina Field 5endees Certffication 0: 6342 Kentucky UST Certification t 84 North Carolina Wastewater Certification M 12 %ArginieNELAP Certification #; 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater CerfMcallon C 40 Florfda/NEIAP Certification 0: E87648 South CaroAne Certification A 99030001 Massachusetts Certification it M-NC030 %ArglnislVELAP Certification it: 480222 North Carolina Drinking Water Certification A 37712 REPORT OF LABORATORY ANALYSIS Thle report shall not he reproduced, except In fu11, wiftut the written eonsent of Paoe Analytical Services, lne.. Page 2 of 13 acMnafyi+r'cal' rrww,oudebl. m SAMPLE ANALYTE COUNT Pace Ans"cal Services, ine. 98DO MnoeyAvc, Suite 100 Hunterevsue, NC 28078 (704)875-8D92 Project: SPX Pace Project No.: 92293583 Angtes Lab ID Sample ID Method Analysts Reported Laboratory 92293583001 S004 EPA 1664E JMS 1 PASI-C EPA 8082 SWB 5 , PAST-C SM 25400 MJP 1 PASI-A EPA 351.2 SER 1 PASI-A EPA353.2 DMN 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except to full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 Ana"cal Project. SPX Pace Project No.: 92293583 Sample: 8 DO-1 i Pace Analytical Services, Inc. 9800 Ioncey Ave. Suite 100 F unterevine, NC 28078 V041875.9092 ANALYTICAL RESULTS Lab ID: 92293583001 Colleclsd: 04/12/1616:30 Received: 04113/iB 09:25 Matrix: Mter Parameters Results Unlis Report Limit DF Prepared Analyzed CAS No, qua] HEM, Oil and Grease Analytical Method: EPA 1664E 01 and Grease ND mg/L 6.0 1 04/22/18 09:36 8082 GC$ PCB Analytical: Method: EPA 8082 Preparation Method., EPA 3510 , PCB-1010 (Aroctior 1016) ND u9/L 0,80 1 04/14/16 09:46 04M4116 18:17 12674-11-2 PCB-1221 (Arodor 1221) ND Wt. 0.60 1 04/14116 09:48 04114116 18.17 11104-28-2 PCB-1232 (Aroclor 1232) ND ugA 0.50 1 D4/14/16 09:46 04114M616:17 11141-16-6 PCB-1242 (Arodor 1242) ND ug1L 0.50 1 04114M6 09:48 04/14/16 16:17 8309-21-9 PCB4248 (Arodor 1248) NO ug1L 0.60 1 04/14116 09.48 04/14/16 16,17 12672 29-6 PCB-1254 (Arodor 1254) ND Wt. 0.60 1 04/14116 09,46 04/14116 16:17 11097-Wi PCB-1280 (Arodor 1280) ND ug/L 0.60 1 04/14/16 00:46 04/14/16 16:17 11098-82-5 suffogatles Decachlorobiphenyl(S) 25 % 10-132 1 04114/1609:46 04114116 16; 17 2051-24-3 2540D Total Suspondad Solids Analytical Method: SM 25400 Total Suspended Solids 28.7 mg/L 4.6 1 04/14A6 12:25 361.2 Total Jgeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjefdahl, Total ND mg/L 0,50 1 D4121M6 D4:14 7727.37-9 363.2 Nitrogen, N021ND3 unpres Analytical Method. EPA 353.2 Nitragen, Nitrate 0.27 m91L 0.020 1 04/14/16 09:49 Nitrogen, Nitrite ND mg/L 0.020 1 04/14/16 00:49 Nhmgen, NO2 plus NO3 0.27 mg/L 0,020 1 04114/16 09:49 Date: 04/2212016 D4:48 PM REPORT OF LA 130RATORY ANALYSIS This report ahail not be reprodurnd, except In Bell, without the written consent of Pace Analytical Sarvloas, inc.. Page 4 of 13 Poem Ana""] 8erAces, Inc. ^n p„ f� 9800 1QnceyAve. Suite 100 cam ( 1 Huntersv0s, NC 28070 wmepscsArDs oom {704}978-9092 QUALITY CONTROL DATA Project: SPX Pace Project No.: 92283583 QC Batch: GCSW24756 Analysis Method: EPA 16648 QC Batch Method: EPA 1604B Analysis Deseriptfon: 1604 HEM, OR and Grease Associated Lab Samples: 92293583001 METHOD BLANK: 1717087 Matrix: Water Associated Lab Samples: 922936830DI Blank Reporting Parameter Unite Result Limit Analyzed Ouallfiers Oil and Grease mg1L ND 5.0 D4122/16 09:24 LABORATORY CONTROL SAMPLE: 1717088 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers OB and Grease mgfL 40 37.2 93 78-114 MATRIX SPIKE SAMPLE 1717089 35239549001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits QualNfers 00 and Grease mglL 6.6 40 41.7 88 78-114 Results presented an thts page are In the unhs Indlcated by the "units" celuma except where an ultimate unll is prsseMed to the rtgM or trw result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date:04I29J2016 0448 PM vdthout the written consent of Pace Analytical Services, Inc.. Page 5 of 13 aceAnaly[rcal "Osallulcom QUALITY CONTROL DATA Project SPX Pace Project No.: 8229M3 Pace Analytical Services, Inc, 0800 ICetcey Ave. Suite 100 Hurderayllle. NC 28078 (704)876.9092 OC Batch: OEXT/41945 Analysis Method: EPA BD82 QC Batch Method: EPA3610 Ans"Is Description: 8082 GCS PCB Associated Lab Samples: 922OUS3001 METHOD BLANK: 1709769 — Matrix: Water Associated Lab Samples: 02203583001 Parameter Units PCB-1016 (Aroclor 1016) uglL PCB-1221 (Arodor 1221) uglL PCB-1232 (Arador 1232) UG1L PCB-1242 (Arodor 1242) u911- PCB-1248 (Arodor 1248) UgIL PCW1254 (Arodor 1254) ugrL PCB-1260 (Arodor 1280) ugA- Decachlorobiphenyl (8) % Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 04/14/16 21:00 ND 0.50 04/14/16 21:06 ND 0.80 04/14/16 21:05 ND 0.50 0411411821:06 ND 0.50 0411,06 21:06 ND 0.50 D4/14/16 21:08 ND 0,50 "14116 21:06 80 10-132 04/14/16 21;08 LABORATORY CONTROL SAMPLE 8 LCSD: 1709770 1709771 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Core. Result Result % Rec % Rec Limits RPO RPD Qualifiers PCB-1016 (Aroclor 1016) ug1L 6 3.9 4.1 78 82 50-150 5 3o PCB-1260 (AroClor 1200) uglL 5 4.1 4.3 82 87 60-150 6 30 Decachtorobipharyt (S) % 74 51 ID-132 Remo presented an this page are In Ihs un8e Indlcaled bythe 'UnBe" column except when an sttcrrrety untt Is presanted to the right of the resutL REPORT OF LABORATORY ANALYSIS This report shall not he reproducod, enept in hAl, Date: 0412?120161308 PM without the written consent of Pace Analytical Services, Ina. Page 6 of 13 ac"Analytical" ewxpecalags,rom QUALITY CONTROL DATA Project: SPX Pace Project No.: =93583 Pace Analytical Services, Inc. 9a00lOnceyAve. Suits 100 Huntetevlpe, NC 28e78 (704)075.9M QC Batch: WET/44234 Analysis Method: SM 2540D QC Batch Method: SM 2640D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92293683001 METHOD BLANK: 1709599 Matrix: Water Associated Lab Samples: 92293583001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 04/14/16 12:10 LABORATORY CONTROL SAMPLE: 1709600 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids moll. 260 250 100 90-110 SAMPLE DUPLICATE 1709601 92293525003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids nmg/L ND ND SAMPLE DUPLJCATE: 1709602 92293531001 Dup Parameter Units Result Result RPD Quallflars Total Suspended Solids mg1L ND ND Resulte presented on this page am in the unae Indicated by the "Units" column except "are an anerrlate unit to presented to the right of the recuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except In full. Date: 041M1316 04:46 PM without tho written consent of Pace Anelyliml Services. Inc.. Page 7 of 13 cCAMMiCal rraryoaaf�IJSa.com f QUALITY CONTROL DATA Protect: SPX Pace Project No.: 92203583 QC Batch: WETA127267 Analysis Method: EPA351.2 QC Batch Method: EPA 3512 Analysis Description: 381.2 TKN Associated Lab Samples: 92293583001 METHOD BLANK: 1714784 Matrix: Water Associated Lab Samples: M936MMI Stank Reporting Parameter Units Result Limit Analyzed Qualmera Nitrogen, IQetdald, Total mg/L ND 0.50 04/21/16 04:02 Pace Analytical Servl cos, lm 9800 Klncey Ave. Suite 100 Hunters0e, NC 28078 (704)878.9092 LABORATORY CONTROL SAMPLE: 1714785 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.8 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1714786 1714787 MS MSD 92203710001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Resull % Rec % Rec Limits RPD Qua] Nitrogen, Klddshl, Total mg/L 0•68 10 10 10.0 11.4 94 107 90-110 12 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: -1714788 1714789 MS MSD 92293BB8001 Spike Splice MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result 9ti Rec % Rec omits RPD Qual Nitrogen, Kjeldahl, Total mg1L 25.6 100 1DD 137 138 112 111 Milo 1 MB Rmu&s presented on this pegs are In the units Indicated by the `Units" column asccpt where an aaeMRte unit to pnaerdW to the right of ale ream,, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu8, Date: 04/2212016 04,48 PM without the written ecnaeni of Pace Analytcel Services, Ina. Page 8 of 13 �:� xt s a of 1 I eftOcal waw.pscslitte.txml QUALITY CONTROL DATA Project SPX Pace Project No.: 92ZM583 QC Batch: WETA127199 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Anslysls Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92293563001 METHOD BLANK 1709687 Matrix: Water Associated Lab Samples: 92293583001 Pace Analytical Services, Inc. e890 Klncey Ave. Suite 100 Hunterwille, NC 28M (704)M-9092 Parameter Unite Blank Result Reporting Llmlt Analyzed Quallfiers Nitrogen, Nitrate mglL ND 0.020 04/14/16 09:46 Nitrogen, Nitrite mg1L ND 0.020 04/14115 09:46 Nitrogen, NO2 plus NO3 mg/L ND 0.020 04/14/16 09:46 LABORATORY CONTROL SAMPLE: 1709688 ` Spike LCS LCS % Rec Parameter Units Conc. Resull % Rec Llmlls Quallflere Nitrogen, Nitrate mg/L 2.5 2.4 97 9t1-110 Nitrogen, Nitrite mg& 1 0.98 96 90-110 Nitrogen. NO2 plus NO3 mg1L 2.5 2.4 97 90-i10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1709889 1709090 MS MSD 92293583001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cane. Conc. Result Result % Rec % Rec Limits RPD Qua[ Nitrogen, Nltrale mg/L 0.27 2.6 2.5 2.6 2.6 94 94 00-110 1 Nitrogen, Nili to mg/L ND 1 1 1.0 1.0 101 98 90-110 2 Nitrogen, NO2 plus NO3 mg/L 0.27 2.5 2.5 2.6 2.6 94 94 90-110 1 Results presented on this page are rn the unite Indleatod by the "Untie" column except where an allemate unit is presented to the right or the resulR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Dale: 0412712016 04:48 PM wboul the written consent of Pace AnalytioW ServIon. Ina. Pago 9 of 13 Cek?al cal• axw.peor�bsaorn QUALIFIERS Project: SPX Pace Project No.. 92293683 DEFINITIONS DF - Dilution Fedor, if reported, represents Me factor applied to the reported data due to dilution of the sample allquaL ND - Not Detected at or above adjusted reporting llmlt. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantltallon Limit RL- Reporting Limit. Pace Analytical Serviose, Inc. MO Klncey Ave. Sure 100 Hunteraville, NC 2807a 1704)876.9092 S - Su"ale 1,2-Diph anythydrazina decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anslyte Is a combined concentration. Consistent with EPA guldellnes, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appreprfale for 2 Chloroethylvinyl ether, Styrene. and Vinyl chloride. A separate vial preserved to a pH of 4-5 Is recommended In SW846 Chapter 4 for the analysis ofAcrolein and AcrytonHrRe by EPA Method 8250. N-Nitrosodipharrylamine decomposes and cannot be separated from Olphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace AnWytcal Is TNI acoredhed. Contact your Pace PM for the current list of aceredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pain Analytical Services -Asheville PASI-C Pace Analyticcal Services - Charlotte ANAI-YTE QUALIFIERS M8 Matrix spike and Matrix spike dupileate recovery not evaluated against control limits due to sample dliuRon. R1 RPD value was outside control limits, REPORT OF LABORATORY ANALYSIS This reparl &hall not bo reproduced, except In full, Date: 0412212f116 04:48 PM without the mftm consent of Pace Anayural Services, Inc.. Page 10 of 13 AnalX cal" IceC, " wrrrpecdabtcom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SPX Pace Project No.; 92283583 Pace Analytical Services, Inc. 9900 WnceyAve. Butte 100 Hunterevills, NC 26078 (704)875-NO2 Analytical Lab 1D Sample 10 QC Batch Method QC Batch Analytical Method Batch 92293583001 S00-1 EPA 1664E GCSV/24756 92293583001 300.1 EPA 3510 DEXT141945 EPA 8082 GCBV/24688 92293683001 SDO.1 SM 25400 WETl44234 92293583001 SDO.1 EPA351.2 WETA127287 92293583001 SDO-1 EPA353.2 WETA127109 REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 04/22/200 04,48 PM without the written consent of PaceAnalylieal Services, Inc.. Page 11 of 13 Document Name:,.. Document Revised: ISFE02016 undltlon Upon Recel t SCUR Page t of 2 Document No.: I lssuingAgthodty: Mehl; Name: WO� ' 9.2L�IV583 Project If: Courier: Fed Est LJUPS�O LISPS ❑ Commercial ❑Pace Other: Z83l3�3 Cur<tady Seal Present? ❑Yes Wit`o Seals Intact? OYes Quo 1 F Date/tnitiaG Parma E►ramlhing Cantents:(1}. �,..) Packing Material: OBub wrap ❑Bubble Bags ❑Siang ❑Others Thermrnneter: iV1505 Type of icar et ❑alue ❑Narie 63h5vason Ice, ctloling process hadhegun Corractlon Factor: OA'C Cooler Tamp Corrected ('C)s 8.pr Biological Tissue Frozen? ❑Yes []No QN>`!C• Temp should be above freezing to,OT USDA Rogulated Soil ( ©.Ikwater sample) Did samples orW a Ina quarantine zohe wlthln the United States: CAW, orSC (check map;)? ' old samples originate from a farolgp_source Ontemattanaft C Indudiner Hawaa and Puerto RIcdW ❑Yes MNW-- Chain of Custody Present? Na [INIA 1. Chah1 of CrustodV Fgled Out? dF UNo L N A 2. Chain ofCOM .Rel! mad? No QWA 3. Sam er Name aKnrVicnature on COC? No N A Al. Samples Arrived wlihlh Hold TWO 9 es No N A S. 5 ort Hold?Time Anal <n hrr ? f $ J3iqo N A 6. Rush Turn Around Time Requested? Oyes JOIC LlyLA 7. Suifident Volume? IQNO K N A S. . CorrectCnntalnersUsed? -Pace Containers Used? ®rft— MVdCDN. GNo (]N/A QNJA 9. Containers intact? MXIr QNO QYLA SD. Filtered Volume Recakd for Dlssolvetl Tests? Oyes Na RNA 11. Note Viediment is Asible In the dissolved container Sample Labels Match COC? _Fn�hrHne na trh alinla—twir uW &i4w G 1 1— ❑Yes 01o ❑NJA 12. a 00 Wti•}- l,u(pi-e 1 All containers needing acldlbase preservation have been checked? Allcontalners needing preservation -are found to be In cornpBance with EPA recommendation? (HNO], H,90,, HCH2; NaOH 4 Sulfldk NaOH>12 Cyanide) Earueptions: VOA, Coliform, TOC, 0II and Grease, TYtp Blank custody Seals Present? CUEHT N(MFICATfON/R0OWr10N Person Contacted: Cansmems/ReWIL100a: Oar- (3Na ❑WA 113. I]Yei ❑Na pNJA []Yes ❑No is, DatOme: Fleld Data Requlmd? ❑Yes ❑Na Project Manager SWRF Revtews Dates A"I Project Manager SRF Review: Date: �( ,Note: Whenever there i4 a discrepancy affecting North Ctirallna camp lance samples, a copyof this form will be sent to the North Carolina DEHNR Certlllcation Office (I.e. .Out of hold, Incorrect preservathm, out of temp, Incorrect contalners) 4- Page 12 of 13 r'.Pafce,4nafytfcal. L152m., CHAIN -OF -CUSTODY / Analytical Request Document Thi Cif-c��stadY is a LEGhL �OCl7MEN7. Ail telelra�sttfelds must be cam0l�d aeuratiely. r.,.MA"II r' I���.i�l_ a l►. .14754.87 - • - c ENCY Dej*�Mgwww ow PI p SIL SAM .° ., - e c AIIIr-A MWINNUMEFUR■F1 FAME ■■■■■ r■■■■■■■■■■■■ ,, m ■■■�■■■■■■■■■■■■ IN 0 0 0 0 0 IN IN IN 0 IN 0 0 a =410- R. It M� _ �o •_ - ■moo !! 'momw4 Nam 4 illil the fm" 7w etc mcaprg PI NET= do➢ o&lrrAM mmsad,peW of i.la ehayo, CI('?-%W Mang GN Al0 edMm[ P.d weom 3o Ma®s FALL' .07, i54tv"7 Semi-annual Stormwater Discharge-MonitoringDischarge-Monitoring Report h or North Carolina Division of Water Quality General Permit No. NCG030000 I V ` 1 Date submitted I', - zl%A -14 CERTIFICATE OF COVERAGE NO. NCG03 O a " FACILITY NAME `.J P X COUNTY JAI' . t 1ynr0_ PERSON COLLECTING SAMPLES LABORATORY_ P�rj C.7-- iab Cert. tI �d CoMmerns on sample coRection or analysis: Part A: Stormwater Benchmarks and Monitoring Resufts SAMPLE COLLECTION YEAR dQ{S SAMPLE PERIOD ❑ Jan -June F'Juiy-Dec DISCHARGI NG TO CLASS ❑ORW ❑HQW - ❑Trrout th❑PNA ❑Zero -flow ❑Water Supply []SA r3 - jc 3 [Other U.1 nitzjAc K1,L6 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this periods pr j .� .... • .... ..� , .. .... • di�'ali:Nb . . .. ., . ;.: .� .,.. .... .. �( .i� I .i i; i :• ��-'., .,J• �Ilectec�.... °ii1. �. .��:��' rrSO �t{� .......... ..c ......... j ••� b w T'�1. Mt. i01 •� . airriif'0 �'::,.... rjTlC�ieS;:' to -.�;, .. ..:r.-.� is. . J:1.: 1.:: 'i"i': :r�.. V t :..:•.,::. 1 oia� d- SIir�S': �'�F ..1 , �:: :.,r• .+:•. :•I�-. '7: •r' .�,- .r.-�' a:.,:a .::, :: i •lid•' ,r•,� a'tid�rtl=ur�li�': 9i'. i.i: _ ..-i. .1 �i..' �;: „L.:,..r.a.. vFii:c::. ;=; a :.:. ��u;Y::.• �°a•�i'' •,;� ' :ZIt1c= :.la•' =ldail� Polar'=p .'. f a#..1�. . •T .91. OCdrbO11.�ic:: - ..i". '.Ber}�hrelm�rs--.->::.._...: _ •_•�.....::::.... .•..:.;:.'.......,.., .:,_.,. r ;i418i1'5 ",'6/... �- -':��.'-•'fr.•�9s��.�•�� 't. : .r.. r.0:'iri,',/�� S/.�::r.:i�.lTl�.i,•�:i�.�i`a��6/.ti:: :�MLI1. .:1•i�"'GL.�::... io- -tom rAr) i Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. gThe total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433_11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the defnitlon as hound in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2022 Page 1 of 3 Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (Tro), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since fl11ng the last discharge monitoring report. I further certify that this facility is Implementing the all the provisions of the solvent management plan Included in the Stormwate�r Pollution Prevention Plan."" &4 �/ r Name (Print na e) Title (Print title) /— (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Nan -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "SM me/O where XX is the numerical value of the detection limit, reporting limit, etc. -in mg/L. Note: if you report a sarnple value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new all per month. ❑ No discharge this perlod?2 :..... :..:. :• `Q�tetl:-.::•:'`... mn df ar>s�urt>y.•::::;;:` tsrdiessiy' ,•>:;II <i S: ;�Nrolar;d&G�j.TPHby,,'; i:��t!`b'6?4 sperirledl pH JSA6 :0 5U: Footnotes from Part A also apply to this Part B " See General Permit text, Table 5, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-gas, last revised 10/25/2012 Page 2 of 3 4 J A STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year eta tS Individual NPDES Permit No. NCSI Certificate of Coverage (COC) No. NCG or This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March a of the following year. Facility Name: gip, County: Phone Number. (^) 'ra7:S S ' `� Total no.' of SDOs monitored Outfall No.. 1s this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No 21 If this outfall was in -Ter 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No �w .I :1 : a: {{., •.Its:•: - ;r,. �... .{i�M ta: � x}:ry �c[-. y_' R - :I_ i�t:': -•rP' . i. .:...IL a ;eM•. f �i'' F "'eE : �i in: Pir r s_iT'•'?'ii y �:"t ; s :,'', ..t:.. r•,.$ 1 .]!'!'>'F'^ :•�'1:^.r �I Y.^::fY r5i_ 'ry :�; f: {1.• ;FY. , !?[?.... - 7 ?'Si%' ;s ..i•: r :.i's:•. ,, .s... - r •l „i:r.Fc^:.I� �.Y"«._. - ,�,vtA'r•:; _.`�.�� .:�;y:r Mi"::x:.-�'. 'ifs. {!-:•�•:m'�.`'. :!. :-.._ it .yfr _.. .__.�...._�:f �.. •.r.ki ».+'�-a ...�.t.:'i•'aF .k;t�in. .in ..I �a x .M.,e:•� f -:2%?.,: .•a.-. :,_1!�'� ..r, n• .., _..r.y _ :. -' p.., i.i:• :.7.. ,�1�i ;' .-r[•a �1+� 'i-'. �i'�:' Yost a ;., 3'c.: Q. r.:..l S' -Ii:• "U I i i�11 ...<-4,_:: ,:.:. .. A-f :.:Y+ 9 .:r`t• Y.'� ..w5! ."sa•�' :�,L`��.T"-�', �i'Li. �`4'E'i.' :wS"'� R-t L.' .a. k.-. . K' ' .I6] :fY' f. '•�ii%PM:i� � t�• T:'- ALn.. �:i=7...,, �:' ,I • l•yY. YY :��. •� � i-iw.x y.. � $ "'a!_:. ai tf.'b :'i: `�L� "-'1 _ + {. _ iJ`__" - � . <_.- ,7'c i '� .,�. • .-.C.^1,:... �i. '4` ' P-[ .i.. - .hl - +. . P: .S"..Y - '• i.li ° :,. T•.:,:,__ ,"s;; .......•...'_.�. �l-, ;S• Lt . I ., u - n . a .ate .�' 3 : r _+.. .e� s ,';r. �._� a gat:: Inf . s. :r ,�. .ta•'•. r :J� .? ,^ •� c if �'S'" �,.�._ ._~." ..� - 'a..... u a ia�, - i . ♦. `3�...:,,.:. �!.� •'t"' ��''-� .aiL:cy.-�ri:'::._-.! :'r•:"�ti.. '.x':.`:`. Y�arl.c `''�::�^1•':; ..r ... _ _ _. .. �� Y: .. :i�. f .4•'�illi'. .%..a. , ....:.. �._ .... .. .1[t.... .. _.a•'•':.• .�...Y.. �:+.r.l' iT--4 .N.� -'7Cc. _+�`�•�`�•�.,s'.Y:�..�•.'y'-%=Y r>, :'3T _ - ..�y�''aP.« i2_ SL. ._ .._..,. •...-.. .._ _. _... -.. .. .--.. s .._...„...,la: f!••�. a- ^-: •!rlr.:,�;;,.;-.,,. ;.,�rM� ;^.Tirk '.�a�l:,. t.r :!' .i"..:4i '..hs s+. ..=M:< -:ir' .'$•`� Yv:: ;. Benchmark- JWA 100 .[ 7 15' 7 (41, 4el1 � v3 O 16V/! R 5 ,� r 3 - IC- r• SWU 264-Generio-25May2010 t't Note: if you report a sample value in excess of the benchmark you must Implement Tier I, ?Ter Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DMR Induding all "No D1schaEge" reports, within 19 daig g f recelot of the lab results for at end of monitoring period In the case of "No Discharge" reports} to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION IFOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 /— Z6 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 41� , • ..;' Additi6nal Ouffall Attachment Outfall No. Is this outfall currently In Tier 2 (monitored monthly)? Yes C:1 No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes [:3 No E:j If this outfall was In Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency F Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑ I. . M ......... ....... A. & 4�7 77. SWU-264-Geneft,25MaY201 0 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date /- Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: .�now 225 Green Street 610 East Center Avenue/Suite 301 2090 US !-lighway 70 Swarmanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 2964500 Fayetteville, NC 28301-5043 (704) 663-1699 (910 433-3300 r ..._.... C r tl 943 Washington Square Mall 127 Cardinal Drive Extension 3800 Barrett Drive Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 ` (910) 796-7215 - 1617 Mail Service Center 585 Waughtown Street f Winston-Salem, NC 27107 (336) 77I-5000 Raleigh, NC 27699-16I 7amd 919 807-6300 _;___ SWU-264-Generic-25May2010 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCGO30000 SAMPLES COLLECTED DURING CALENDAR YEAR. CERTIFICATE OF COVERAGE NO. NCG03 Q90 0 3 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACELXrY NAME P COUNTY V-%C- PERSON COLLECTING SAMPLES nA�l Fcdihag PHONE NO. (93CQ -1 <ftt — 11 _& CERTIFIED LABORATORY Lab# L145 —Lab # PLEASE SIGN ON THE REVERSE 4 Part A: Specific Monitoring Requirements Lr-C,A FJ iiia MR. US . . . . . . . . . . I r- — - - - - - - - - SD0 I I I ILI I Iq -_X x Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2-;Rl See General Permit text. ;ram %UEIVED Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes &no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring ReankVnients JAN 3, 0 2014 CEN TRAL FILES DWQ180G A MWIM.S. i M50. 1. K -4- P ZIP .—N. Pj _4 Md LIPz?far-414 GI''01, mo ZLQ,'j-'ffi diskiltuff 'R ''' N-, -t"M2NNY " Ly1NNi L3d O Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you mast implement Tim I or Tier 2 responses. See General Permit text STORM EVENT CHARACTEFJMCS- Date _ILIt'j(first event sampled) Total Event Precipitation (inches): • 19 Date — (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Atim DWQ Central Files 1617 Mail Service Center Raleigh, Nardi Carolina 27699-1617 SWU-245-031308 Page 1 of 2 n�. Total Toxic Organics sampling is applicable only for those.facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention PIan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the foIlowing certification statement: Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief; no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan_" Name (Paint namo Title (Print title) (Site) (Date) "I certify, under penalty of law, that this document and all attachments were prepared under nay direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 1 (Date) SWU 245-031308 Page 2 of 2 Stormwater Discharge Out€all. (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.statc.nc.us/pu/Forms Documents.htm#rniscf6xms Permit No.: N& S/ O d1293/U/ 3/ or Certificate of Coverage No.: NjgGG 1 I 1 1 I I Facility Name: "K County: WA.64 nz Phone No. 02 ` -7 Inspector. t Date of Inspection: _ k t t 4 t� Time of Inspection: { a- •• + v` Total Event Precipitation (inches): % ( q Was this a Representative Storm Event? (See information below) ayes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred, A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfali Description: Outfall No. _� Structure ( ipe, ditch, etc,) _ _d i4f-k Receiving Stream: Z- A=r Describe the industrial activities that occur within the outfall drainage area: 1"5 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: I < <ik} M 'tf- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): r -& c�l N. tc` Page 1 of 2 5 WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy- 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes S. Is there an oil sheen in the stormwater discharge? Yes Nio 9. Is there evidence of erosion or deposition at the outfalI? Yes (10 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 Weather History for Goldsboro, NC I Weather Underground Pagel of S Weather History for Goldsboro, NC Tuesday, January 14, 2014 Tuesday, January 14, 2014 . Previous day January n 14 2014 Next Day r Dolly Weekly Monthly Cuslom� Actual Average Rarrord Temperature Mean Temporelura 48 T - Max Temperature so IF 60 IF 113 IF (2a13) Min Temperalure 38 IF 32 T 21 T (1997) Degree Days Healing Degree Days to Mersture Dew Paint 49 IF Average Humidity 91 Maximum Humidily 100 Mtnim4m Humldily 85 Precipitation Precipitation 0.19 In - Sea Level Pressure Sea Laval Pressure 20A8In tNlnd Wind Speed 4 mph (SSW) Max Nod Speed 21 mph Max Oust Speed 26 mph VWbllily 0 rnites Events Rein Averages and records for this station are not official NW$ values. `r w Trace o1 Predplle0an. MM a AAisft Value Source: NWS Daily Summary http://www.wunderground.comlhistorylairportlKGSBI201411114IDai]yHistory.html?req_ci... 1 /28/2014 aceAnalytical www.pacelabs.com October 22, 2013 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Mr. Billy Rawls Eastern Environmental Management PO Box 4030 518 S. Pearl Street Rocky Mount, NC 27803 RE: Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Rawls: Enclosed are the analytical results for sample(s) received by the laboratory on October 09, 2013. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, a,". Angela Baioni angela.baioni@pacelabs.com Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 (.��A'neAnabftal www.pacelabs.com Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Ashevifle, NC 28804 (828)254-7176 CERTIFICATIONS Charlotte Certification Me 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification M 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification A 357 North Carolina Wastewater Certification #: 12 Mrginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 acmnalytical ..pacelahs.coin Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92175150001 SPX-1 EPA 1664B CLW 1 PASI-C EPA 8082 EJK 8 PASI-C SM 2540D DAS 1 PASI-A 40CFR PART 432.2 EWS 1 PASI-A EPA 351.2 JDA 1 PASI-A EPA 353.2 DMN 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc- Page 3 of 13 RA.L1L�JwG�i'.. �:, aceAnalX cal www.pacwabs.com Project: SDX-3rd Quarter Pace Project No.: 92176160 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-6921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SPX-1 Lab ID: 92175150001 Collected: 10/08/13 15:30 Received: 10/09/13 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease NO mg1L 5.0 1 10/10/13 12:34 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Arodor 1016) NO uglL 0,50 1 10/10/13 11:07 10/11113 23:32 12674-11-2 PCB-1221 (Aroclor 1221) NO uglL 0.50 1 10/10/13 11:07 10/1111323:32 11104-28-2 PCB-1232 (Aroclor 1232) NO uglL 0.50 1 10/10/13 11:07 10/11/13 23:32 11141-16-5 PCB-1242 (Arodor 1242) NO ug1L 0,50 1 10/10/13 11:07 10/11/13 23:32 53469-21-9 PCB-1248 (Aroclor 1248) ND ug1L 0.50 1 10/10/13 11:07 10/11/13 23:32 12672-29-6 PC8-1254 (Arodor 1254) NO uglL 0.50 1 10/10/13 11:07 10/11/13 23:32 11097-69-1 PCB-1260 (Arodor 1260) NO uglL 0.50 1 10/10/13 11:07 10/11/13 23:32 11096-82-5 Surrogates Decachlorobiphenyl (S) 32 % 10-132 1 10/10113 11:07 10/11/13 23:32 2051-24-3 25400 Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.0 mg1L 5.0 1 10/11/13 17:19 Total Nitrogen Calculation Analytical Method: 40CFR PART 432.2 Total Nitrogen 1.1 mg1L 0.12 1 10/14/13 14:12 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 0.92 mg1L 0.50 1 1012211311:23 7727-37-9 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 0.14 mg/L 0.020 1 10/09/13 23:16 Nitrogen, Nitrite NO mg1L 0.020 1 10/09/13 23:16 Nitrogen, NO2 plus NO3 0.14 mg1L 0,020 1 10/09/13 23:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1012212013 06:05 PM without the written consent of Pace Analytical Services, Inc . Qual Page 4 of 13 aceAnalytical� www.pecelabs.com Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 20804 (828)254-7176 QUALITY CONTROL DATA QC Batch: GCSV116717 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92175150001 METHOD BLANK: 1063355 Associated Lab Samples: 92175150001 Parameter Units Oil and Grease mglL LABORATORY CONTROL SAMPLE: 1063356 Parameter Units Oil and Grease mg1L MATRIX SPIKE SAMPLE: 1063357 Parameter Units Oil and Grease mglL Date: 10/22/2013 06:05 PM Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/10/1312:28 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 40 32.6 82 78-114 92175199004 Spike MS Result Cone. Result ND 40 34.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. MS % Rec % Rec Limits Qualifiers 84 78-114 Page 5 of 13 aceAnalytical *".pacelabs com Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27208 (336)623-8921 Pace Analytical services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: OEXT124192 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Associated Lab Samples: 92175150001 METHOD BLANK: 1063320 Matrix: Water Associated Lab Samples: 92175150001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug1L ND 0.50 10/11/13 19:55 PCB-1221 (Aroclor 1221) ug1L NO 0.50 1011111319:55 PCB-1232 (Aroclor 1232) ug/L NO 0.50 1011111319:55 PCB-1242 (Aroclor 1242) ug1L ND 0.50 10111IM3 19:55 PCB-1248 (Aroclor 1248) ug/L NO 0.50 10/11/13 19:55 PCB-1254 (Aroclor 1254) ug/L ND 0.50 10/11/13 19:55 PCB-1260 (Aroclor 1260) ug/L NO 0.50 10/11/13 19:55 Decachlorobiphenyl (S) % 88 10-132 10/11/13 19:55 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1063321 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 3.2 63 50-150 PCBA260 (Aroclor 1260) ug1L 5 3.6 71 50-150 Decachlorobiphenyl (S) % 79 10-132 MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 1063322 1063323 MS MSD 92174953007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 10 10 6.1 7.7 61 77 50-150 23 PCB-1260 (Aroclor 1260) ug/L NO 10 10 6.0 6.8 60 68 50-150 12 Decachlorobiphenyl (S) % 50 48 10-132 Date: 10/22/2013 06:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 Paceces, Inc. Pace Analytical Services, Pace9800 Analytical 205East Meadow Roadt- Suite A Riverside Dr. K nciInc.cal ey Ave.A e. Suite 100 www.pwetebs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-B921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: SDX-3rd Quarter Pace Project No.: 92175150 QC Batch: WET127560 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92175150001 METHOD BLANK: 1064712 Matrix: Water Associated Lab Samples: 92175150001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/11/13 17:15 LABORATORY CONTROL SAMPLE: 1064713 Spike LCS LCS % Rec Parameter Units Conc, Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 80-120 SAMPLE DUPLICATE: 1064714 92175095001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 7970 7750 3 SAMPLE DUPLICATE: 1064715 92175176001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 31.0 30.0 3 Date: 10/22/2013 06:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 4 acmnalj6cal www.pecelabs.com Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QC Batch: WETA116767 QC Batch Method: EPA 351.2 Associated Lab Samples: 92175150001 METHOD BLANK: 1067246 Associated Lab Samples: 92175150001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 1067247 Parameter Units Nitrogen, Kjeldahl, Total mg/L Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: EPA 351.2 Analysis Description: 351.2 TKN Matrix: Water Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Blank Reporting Result Limit Analyzed Qualifiers ND 0,50 10/22/1311:09 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 10.7 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1067248 1067249 MS MSD 92175584001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.94 10 10 10.7 10A 98 95 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1067250 1067251 MS MSD 92175149002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.2 14.8 88 144 90-110 47 M1,R1 Date: 10122/2013 06:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 13 (/1a'neAna1j4ica1 wwwpweiabs.com Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27286 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 2a804 (62b)254-7176 QUALITY CONTROL DATA QC Batch: WETA116694 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92175150001 METHOD BLANK: 1063075 Associated Lab Samples: 92175150001 . Parameter Units Nitrogen, Nitrate mglL Nitrogen, Nitrite mg1L Nitrogen. NO2 plus NO3 mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 10/09/13 2107 ND 0.020 10/09/13 23:07 NO 0.020 10/09/13 23:07 Pace Analytical Services, Inc. 9000 Kinsey Ave. Suite 100 Huntenwifle, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1063076 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L 2.5 2.6 104 90-110 Nitrogen, Nitrite mg1L 1 1.0 101 90-110 Nitrogen, NO2 plus NO3 mg1L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1063077 1063078 MS MSD 92175076002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Nitrogen, Nitrate mg1L 1.5 2.5 2.5 4.2 4.1 108 106 90-110 1 Nitrogen, Nitrite mg1L 0.15 1 1 1.2 1.2 105 104 90-110 1 Nitrogen, NO2 plus NO3 mg1L 1.6 2.5 2.5 4.2 4.1 102 100 90-110 1 Date: 10/22/2013 06:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 9 of 13 aceAnalytical www.paoelabs,com Project: SDX-3rd Quarter Pace Project No.: 92175150 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvitte, NC 28078 (704)875-8092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrasodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. RI RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/22/2013 06:05 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 laceAnalytical www.pscelahs.c= Project: SDX-3rd Quarter Pace Project No.: 92175150 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27208 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)e75-9092 Lab ID Sample iD QC Batch Method Analytical QC Batch Analytical Method Batch 92175150001 SPX-1 EPA 1664B GCSV/15717 92175150001 SPX-1 EPA 3510 OEXT124192 EPA 8082 GCSV115733 92175150001 SPX-1 SM 2540D WETl27560 9217515DDD1 SPX-1 40CFR PART 432.2 WET127590 92175150D01 SPX-1 EPA 351.2 WETA116767 92175150001 SPX-1 EPA 353.2 WETA116694 Date: 10/22/2013 06:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 13 �WceAnajYlcal' Client Name: Sample Condition Upon Recel Document Number: F-CH R-C S-03-rev.11 Page 1 of 2 Issuing Authority: Pace Huntersville Qualitv Office Where Received: [;� Huntersville ❑ Ashevilie ❑ Eden ❑ Raleigh Courier: 0-.Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pace Other Custody Seal on CoolerlBox Present: ❑ yes T no Seals Intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap DAfulble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 �' Type of Ice: Wet Blue None ❑ SaKples on Ice, cooling process has begun Temp Correction Factor T1102: No Correction T1301: No Correction Corrected Cooler Temp.: C Biological Tissue Is Frozen: Yes No N/A Date aaki tials c s tamining contdrt4 Temp should be above freezing to 6'C Comments: Chain of Custody Present: es ONO ❑NIA 1. Chain of Custody Filled Out: IaYes ❑No ❑NIA 2. Chain of Custody Relinquished: 0< ON, ❑NIA 3. Sampler Name & Signature on COC: es ONO ❑NIA 4, Samples Arrived within Hold Time: Yes ONO ❑NIA 5. Short Hold Time Mal Ia <72hr : E!fy'ea ONO ❑NIA 6. Rush Turn Around Time Requested: ❑Yea & ❑NIA 7. Sufficient Volume: bras ON, ❑NIA 8. Correct Containers Used: es ONO ❑NIA 9. -Pace Containers Used: 2iiredONO ❑wA Containers Intact: EfYe3 ❑No ❑ A 10. Filtered volume received for Dissolved tests ❑Yes ONO ❑NIA 11. Sample Labels match COC: Yes ONO ❑NIA 12. -Includes dateltime/ID/Anal sis Matrix: All containers needing preservation have been checked. ,LJYes ONO ❑N!A 13. All containers needing preservatlon are found to be In IZfYes ONO ❑NIA compliance with EPA recommendation. exceptions: VOA, collform, TOC, Or£O, WI-DRO water Yas C;No Samples checked for dechlorination: ❑ ea [IN, ❑NIA 14. Heads ace in VOA Vials >6mm : ❑vas ONO I<A 15. Trip Blank Present: ❑Yes ONO MA 16. Trip Blank Custody Seals Present ❑Yes ONO L7/WA Pace Trip Blank Lot # if purchased): Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: Date: SRF Review: Date: 0 1 Note. Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of tamp, Incorrect containers) �10t:92175150 j II17N9150�Id _;aceAtit trca!' �.Pacelahs.cam CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section G Page: of Required Client Information: Required Project Information: Invoice Information; Camp j'� 1, pan To - Attention: (� 1681929 l �J Copy To: Compaq Name: REGULATORY AGENCY Adder: r NPDES F GROUND WATER F DR1NK)NG WATER F UST r RCRA (- OTHER Email To: Purchase Order No.: Pace Qwte Phone: Fax Project Name: S �� Y 3 fR t +j' �- �^Pam er Site Location • SZATE: Requested Due Date1TAT: Project Number. ode e Requested Analysis Fiitered'(Y1N)' Section D Matrix Codes 8 a z RequiredCRaM Intannatiaa r coot Y COLLECTED Preservatives 's ikiMAiRIx Drirtg Water DW t0.17 O Water WT c Waste Water W W v START F w Z ct p iSo tisolid SL ig cy p. a, y SAMPLE ID Wipe �? , (A-Z 0-91.-) Air AR 4 a 'F; G "j0�1 ! ✓ Sample IDS MUST BE UNIQUE Tissue TS O Other OT . U ut r to 0. m o T m # 0. 0.° V 0 O CD _ ,cp; .0 ~ y' DATE TIME DATE TIME �' 2 X = Z Z4 O - :Pace.Project NoJ Lab F.D. t r c 2 •� - 3 4 -a - 5 6 7' 8: 9 11 12 ADDITIONAL COMMENTS REuNODISNED BY i AFFIt_tATION DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS AJ- SAMPLER NAME AND SIGNATURE a o 0 PRINT Name of SAMPLER:CEZ v E i> g a _ m ORIGINAL T SIGNATURE of SAMPLER: DATE Signed 1 3 (MMIDDNY): L' "t " { rEa n -Important mote: Sy so*V tNs form you are auxptarg Pace's NET 30 ray payrnent temp and agreeing Io late cheryes of 1.5% per Atanih far any in,oiras not Paid wmdn 30 days. F-ALL-0-020rev.07, 1 SMay-2007