Loading...
HomeMy WebLinkAboutNCS000541_MONITORING INFO_20181017STORIGIWATER-DIVISfON-CODfNG-SHEET - - -- PERMIT NO. �GS �O CJ Lf DOC TYPE [I FINAL PERMIT MONITORING INFO APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE awa (c) � YYYYMMDD RECEIVED STORMWATER DISCHARGE OUTFALL (SDO)O 20 f$ r n .Kv� .� MONITORING REPORT PERMIT NUMBER NCS 000541 SAMPLES COLLECTED DURING v� i �' 2018 (This monitoring report shall be received by a s� no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _Southern States Cooperative — Lumberton Fertilizer COUNTY Robeson PERSON COLLECTING SAMPLE(S) Joshua Bass PHONE NUMBER CERTIFIED LABORATORY(S) ESC Lab Sciences LAB## ENV375 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Part A: Specific Monitoring Requirements Outfall Date T9img1L mg1L m mg1L m No. Sample Collected pH, Standard Units Sulfate, 9056 BOD, SM5210B COD, 410.4 Ammonia Nitrogen, 350.1 Nitrate- Nitrite, 9056 Total Phosphorus, 365.1 Benchmark mo/dd/yr (6.0-9.0) 500 30 120 7.2 10 2 001 10/17/18 7.28 16.4 3.9 20.7 0.315 8.02 1.59 Outfall Date m m m No. Sample Collected pH, Standard Units Kjeldahl Nitrogen, TKN, 351.2 Suspended Solids, 2540D Total Nitrogen Benchmark mo/dd/ 6.0-9.0 20 100 30 001 10/17/18 7.28 <0.50 152 8.02 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ Yes X No (if yes, complete Part 13) _ r Part H: Vehicle Maintenance ActivitY Monitoring Reouirements �Outfall! Date' 50050 6 X li. z€se 00556 :_i_ 00530 00400 �< No Sample' Total Flo " Toia! Oil &Grease Non -polar- Total pH ,New. Motor, Collected (lf apipucable) Rainfall app., E " I) O&G/TPH :, Suspended is Oil Usage , ' E (Method 1664 Solids 3 F SGT-HEM),if p1. x a „ mo/dd/ r „ .MG >_ inches m nt unif aUmo N/A N/A N/A N/A NIA N/A N/A NIA STORM EVENT CHARACTERISTICS: Date: 10/ 17/ 18 Total Event Precipitation (inches): 0.3 Event Duration (hours): N/A (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1111afoq0[8 (Date) Form SWU-247, last revised 21212012 Page 2 of 2 'Permit Number NCS 000541 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Southem States Cooperative - Lumberton Fertilizer PERSON COLLECTING SAMPLE(S) Joshua Bass CERTIFIED LABORATORY(S) ESC Lab Sciences Lab # ENV37 P Lab # TN R `� 5 2018 pwR SEC EKES Part A: Specific Monitoring Requirements SEES Part COUNTY Robeson PHONE NO. ( SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall pK Standard Units Total Nitrogen B 30 mwL ® Total Phosphorus osp 20 raa ® spin Total Suspended solids 100 mB/L Kjeldahl Nitrogen 20 mrJL Ammonia Nitrogen 7.2 mg/L mo/dd/yr MG inches (6.0-9.0) 001 1l291201$ nla 0.5$ 6.4$ <.I .264 c2.5 <.25 <A Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes Qlo (if yes, complete Part B) Part B. Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 60400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches mo m knit al/mo 001 1 /29/2018 n/a n/a n/a n/a n/a n/a n/a Form SWU-247, last revised 21212012 Pagel of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 'Permit Number NCS 000541 FACILITY NAME Southern States Cooperative - Lumberton Fertilizer PERSON COLLECTING SAMPLE(S) Joshua Bass CERTIFIED LABORATORY(S) ESC Lab Sciences Lab # ENV375 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Robeson PHONE NO. ( SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Date Sample Collected Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? [:]yes E]no (if yes, complete Part B) Part B: Vehicle Maintenance Activi Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM); if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/yr MG inches mgn m unit gallmo 001 1 /29/2018 nla nla nla nla n/a n1a nla Form S WU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable— see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines mprisowent for knowing violations." of Permittee) Form SWU-247, last revised 21212012 Page 2 of 2 Outfall 001 Visual Data for Southern States Lumberton Fertilizer Plant Permit Permit # NCS000541 tAAv.,a iting'- k I Eloatinj',-� FM I speagea ViAble "_m-7 E f(diares. I(Infi %Ihie or Solids 0 i J, 1 ds WMD�jqh Fda—,L1 en Opep.. RA infa-11 Zrj'� � M JYLesjN_p M 4v c s 1. poq� IM 6YM_o WNPAM en 1/29/2018 0.58 clear none I I I No No No 3/22/2017 0.39 clear none I I I No No No 7/20/2016 1 clear none 1 2 1 No No No 1/18/2016 3.7 clear none 1 2 1 No No No 9/24/2015 1.3 clear none 2 2 2 No No No 1/5/2015 2 clear none 1 3 3 No No No 8/4/2014 5.3 clear none 3 4 3 No No No 2/5/2014 4 clear none 1 3 3 No No No 2/13/2013 0.75 clear none 2 1 2 No No No 3/12/2013 0.4 4/29/2013 1.75 8/19/2013 2.1 4/6/2012 1.5 clear none 2 9/9/201 0.9 Notes: ESC ANALYTICAL REPORT m ESC February 05, 2018 EHC, Inc. Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L966301 01/30/2018 17-MI0113-1 Southern States Coop LUMBERTON, NC Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Entire Report Reviewed By: r Heather J Wagner Technical Service Representative Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except In full, without written approval of the laboratory. Where applicable, sampling conducted by ESL is performed per guidance provided In laboratory standard operating procedures: 060302, 060303, and 060304, r TABLE OF CONTENTS ONE LAB. NATIONWIDE. V Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr. Sample Results OUTFALL 001 L966301-01 Qc: Quallty Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 350.1 Wet Chemistry by Method 351.2 Wet Chemistry by Method 365.4 Wet Chemistry by Method 410.4 Wet Chemistry by Method 5210 B-2011 Wet Chemistry by Method 9056A GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 FP2 3 4 rs5 S 5 6 FCn 6 FSr 7 g rQ C 9 10 [GI 11 F 12 14 9SC 15 16 ACCOUNT; PROJECT: S DG: DATE/TIME: PAGE: OUTFALL 001 L966301-01 GW SAMPLE SUMMARY Collected by Joshua Bass Method Batch Dilution Preparation date/time Calculated Results WG1068976 1 01/3011816:41 Gravimetric Analysis by Method 2540 D-2011 WG1068063 1 01/30/18 21:10 Wet Chemistry by Method 350.1 WG1069081 1 02/02/1814:29 Wet Chemistry by Method 351.2 WG1068976 1 01130/1816:41 Wet Chemistry by Method 365.4 WGIO68324 1 01130/1816:41 Wet Chemistry by Method 410.4 WG1068181 1 01130/1819:50 Wet Chemistry by Method 5210 B-2011 WG1067888 1 01/30/1815:58 Wet Chemistry by Method 9056A WGIO67896 1 01/30/1817:08 ONE LAB. NATIONWIDE, 4V Collected date/time Received datettime 01129/tB 12:21 01/30/18 08:45 FP Analysis Analyst date/time E 02/01/1812:03 KK 0113011E: 2 EG 02102l18141429 JER 02101A612:03 KK 01/31/1809:51 KK F 01/30/18 22:05 MZ 02/04/1810:43 CM 01130/1817:08 DR E rQ—C F eAl F ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: CASE NARRATIVE ONE LAB. NATIONWIDE. JR All sample aliquots were received at the correct temperature, in the proper containers, with the EP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples C FT have been corrected for the dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by the client. All Method and Batch Quality Control are within established Ss criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. E ro-C F, Heather J Wagner 8AI Technical Service Representative 9SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: OUTFALL 001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dateltime: 01129118 12:21 L966301 Additional Information Result Units FP Analyte pH (On Site) 6.48 su F Temperature (on -site) 14 Deg. C Calculated Results FS Result Qualifier RDL Dilution Analysis Batch 4 Analyte ug11 ugA date 1 time FCn Total Nitrogen ND 100 1 02/011201812:03 WG1068976 Gravimetric Analysis b Method 2540 D-2011 Y Y Result Qualifier RDL Dilution Analysis Batch rQc Analyte ugA ug11 date! time Suspended Solids ND 2500 1 01130/201821:42 WG1068063 F, Wet Chemistry by Method 350.1 a Result Qualifier RDL Dilution Analysis Batch AI Analyte ugA ugA date! time Ammonia Nitrogen ND 100 1 02102/201814:29 WG1069081 FC Wet Chemistry by Method 351.2 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugA date 1 time Kjeldahl Nitrogen, TKN ND 250 1 02/01/201812:03 WG1068976 Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugll date 1 time Phosphorus,Total 264 100 1 01/31/2018 09:51 WG1068324 Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugll date I tim e COD 28000 10000 1 01130/2018 22:05 WG1068181 Wet Chemistry by Method 5210 8-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugA date 1 time BOD 3700 81 J- 1020 1 02104120181043 WG1067888 Wet Chemistry by Method 9056A Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugA date 1 time Nitrate ND 100 1 011301201817:08 WG1067896 Nitrite ND P1 100 1 01/301201817:08 WG1067896 Sulfate ND 5000 1 01/301201817:08 WG1067896 ACCOUNT: PROJECT: SDG: DATEM ME: PAGE: WG1068063 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Gravimetrlc Analysis by Method 2540 D-2011 L966301-01 Method Blank (MB) (MB) R3283050-1 01/30/18 21:42 Ep MB Result MB Qualifier MB MDL MB RDL Analyte ugAugA ugA FTc Suspended Solids U 350 2500 F L966320-01 Original Sample (OS) • Duplicate (DUP) (OS) L966320-01 01/30/18 21742 • (DUP) R3283050-4 01/30/18 21:42 Fn Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits s Sr Analyte ugA ugA % % Suspended Solids 1820000 1780000 1 2.22 5 L966349-02 Original Sample (OS) • Duplicate (DUP) �GI (OS) L966349-02 01/30/18 21:42 • (DUP) R3283050-5 01/3OA8 21:42 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits a AI Analyte ugA ugA % % Suspended Solids 69300 73300 1 5.61 J3 5 FSC Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3283050-2 01/30/18 21:42 • (LCSD) R3283050-3 01/30/18 21:42 Spike Amount LCS Result LCSD Result LCS Rec, LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugA ugA % % % % % Suspended Solids 773000 736000 752000 95.2 97.3 85.0-115 2.15 5 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1069081 QUALITY CONTROL SUMMARY ONE LAB, NA-PONWIDE. Wet Chemistry by Method 350.1 L966301-01 Method Blank (MB) (MB) R3283702-1 02/02/1814:02 MB Result MB Qualifier MB MDL MB RDL Anatyte ugA ugA ugA Ammonia Nitrogen U 31.7 100 L965766-01 Original Sample (OS) • Duplicate (DUP) (OS) L965766-01 02/02/1814:07 • (DUP) R3283702-4 02/02/1814:09 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ugA % % Ammonia Nitrogen 1100 1070 1 2.86 10 L966334-02 Original Sample (OS) • Duplicate (DUP) (OS) L966334-02 02/02/1815:24 • (DUP) R3283702-6 02/02/1815:26 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Anatyte ugA ugA % % Ammonia Nitrogen 22200 22500 5 1.14 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3283702-2 02/0211814:04 • (LCSD) R3283702-3 02102M 14:05 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec, Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Anayte ugA ugA ugA % % % % % Ammonia Nitrogen 7500 7330 7390 97.8 98.6 90-110 0.829 20 L966023-01 Original Sample (OS) • Matrix Spike (MS) (OS) L966023-01 02/02A814:10 • (MS) R3283702-5 02/02/1814:12 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Anayte ugA ugA ugA % % Ammonia Nitrogen 5000 ND 4990 99.9 1 90-110 L966334-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L966334-03 02/02/1815:27 • (MS) R3283702-7 02/02/1815:29 • (MSD) R3283702-8 02/02/1815:31 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Anayte ugA ugA ugA ugA % % % % % Ammonia Nitrogen 1000 22900 27300 27800 86.7 98.2 5 90410 V 2.09 20 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG1068976 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method 351.2 L966301-01 Method Blank (MB) FP - (MB) R3283326-1 02/OM li 56 MB Result MB Qualifier MB MDL MB RDL Analyte UgA UgA UgA C F Kieldahl Nitrogen, TKN U 35.0 250 Fs L965954-01 Original Sample (OS) • Duplicate (DUP) (OS) L965954-01 02/01/1812:00 • (DUP) R3283326-4 02101/1812:02 F Original Result DUP Result Dilution DUP RPD DUP Quallfier DUP RPD Limits Fr Analyte ugA ugA % % Kjeldahl Nitrogen, TKN 8720 9300 1 6.44 20 L966319-01 Original Sample (OS) • Duplicate (DUP) El(OS) L966319-01 02/01/1812:19 • (DUP) R3283326-6 02/01/1812:21 a AI Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ugA % % Kieidahl Nitrogen, TKN 4510 4760 1 5.39 20 Fc Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3283326-2 02/01/1811:57 • (LCSD) R3283326-3 02/01/1811:58 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugA ugA % % % % % Kjeldahl Nitrogen, TKN 10000 9760 9620 97.6 96.2 90-110 1.44 20 L966315-01 Original Sample (OS) • Matrix Spike (MS) (OS) L966315-01 02/01A812:04 • (MS) R3283326-5 02/OV1812:05 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte UgA ugA ugA % % Kjeldahl Nitrogen, TKN 5000 2980 7250 85.4 1 90410 J6 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG1068324 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Well Chemistry by Method 365.4 L966301.01 Method Blank (MB) (MB) R3282967-1 01/31M 09:43 MB Result MB Qualifier MB MDL MB RDL Analyte ugA ugA ugA Phosphorus,Total U 35.0 100 L965954-01 Original Sample (OS) • Duplicate (DUP) (OS) L965954-01 01/31/18 09:47 • (DUP) R32829674 01/31/18 09:48 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte UgA ugA % % Phosphorus,Total 2620 2820 1 7.35 20 L966319-01 Original Sample (OS) • Duplicate (DUP) (OS) L966319-01 01/31/1810:09 • (DUP) R3282967-8 01131/1810:10 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte UgA ugA % % Phosphorus,Total 671 701 1 4.37 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3282967-2 01/31/18 09:45 - (LCSD) R3282967-3 01/31/18 09:46 Spike Amount LCS Result LCSD Result LCS. Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte um ugA ugA % % % % % Phosphorus,Total 2000 1860 1840 93 92 90-110 1.08 20 L966315-01 Original Sample (OS) • Matrix Spike (MS) (OS) L966315-01 01/31/18 09:54 • (MS) R3282967-5 01/31/18 09:55 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte ugA ugA ugA % % Phosphorus,Total 2500 270 2390 84.8 1 90-110 J6 L966408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L966408-01 OV3111810:02 • (MS) R3282967-6 01131/1810:04 • (MSD) R3282967-7 01/31/1810:05 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec, Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ugA ugA ug/l % % % % % Phosphorus,Total 2500 ND 2210 2160 87 85 1 90410 J6 J5 2.29 20 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG1068181 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method 410.4 L966301-01 Method Blank (MB) FP (MB) R3282852-1 01/30/18 22:01 MB Result MB Qualifier MB MDL MB RDL Analyte ugA ugA ugA C FT COD U 3000 10000 F L966261-01 Original Sample (OS) • Duplicate (DUP) (OS) L966261-01 01/30/18 22:04 • (DUP) P3282852-4 01/30/18 22:04 En: Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits 5 Sr Analyte ugA ugA % % COD 246000 237000 1 3.97 20 L966545-01 Original Sample (OS) • Duplicate (DUP) F (OS) 1-966545-01 0V30/18 22:09 • (DUP) R3282852-7 01130/18 22:09 s AI Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ugA % % COD 330000 335000 1 1.39 20 E Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3282852-2 01/30/18 22:01 • (LCSD) R3282852-3 01/30/18 22:01 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugA ugA % % % % % COD 242000 245000 245000 101 101 90-110 0.249 20 L966362-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L966362-01 01/30/18 22:07 • (MS) R3282852-5 01/30/18 22:07 • (MSD) R3282852-6 01/30118 22:07 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec, Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ugA ugA ugA % % % % % COD 400000 50700 453000 445000 101 98.5 1 W120 1.87 20 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG1067888 QUALITY CONTROL SUMMARY ONE LAS, NATIONWIDE. 4V Wet Chemistry by Method 5210 B-2011 L966301-01 Method Blank (MB) FP (MB) R3283904-1 02/04tiB 11:48 MB Result MB Qualifier MB MDL MB RDL Analyte ugA ugA ugA ITC BOD U 61 1000 1000 Fs Laboratory Control Sample (LCS) (LCS) R3283904-2 02/04/18 09721 F Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ugA ugA % % Sr BOD 198000 162000 81.6 84.6-115 J- 0 Laboratory Control Sample (LCS) (LCS) R3283904-3 02104AB 11:09 GI Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ugA ugA % % E BOD 198000 214000 108 84.6-115 Fc ACCOUNT. PROJECT: SDG: DATEMME: PAGE: WG1067896 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Ja Wet Chemistry by Method 9056A L966301-01 Method Blank (MB) FP WEI) R3282839-1 01/30/18 06:40 MB Result MB Qualifier MB MDL MB RDL Analyte ugA ugA ugA FTc Nitrate U 22.7 100 Nitrite U 27.7 t00 FsSulfate U 77.4 5000 En L966282-01 Original Sample (OS) • Duplicate (DUP) (OS) L966282-01 01/30118 12:2 0 • (DUP) R3282839-4 01/30/1812:34 F Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ugA % % Nitrate 981 1010 1 2.56 15 Nitrite ND 0.000 1 0 15 F Sulfate ND 2560 1 0 15 F L966301-01 Original Sample (OS) • Duplicate (DUP) (05) L966301-01 OV3011817:08 • (DUP) R3282839-7 01/30/1817:23 F Original Result DUP ResultDilution DUP RPD DUP QualifierDUP RPD Limits Analyte ugA ugA % % Nitrate ND 39.2 1 0 15 Nitrite ND 135 1 200 P1 15 Sulfate ND 1220 1 0 15 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3282839-2 01/30/18 06:54 • (LCSD) R3282839-3 01/30M 07;09 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugA ugA % % % % % Nitrate 8000 8160 8140 102 102 80-120 0.211 15 Nitrite 8000 7940 7940 99,2 99.2 80-120 0.0441 15 Sulfate 40000 40800 40600 102 101 80-120 0.433 15 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1067896 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9056A L966301-01 L966282-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. V (OS) L966282-01 01/30/1812:20 - (MS) R3282839-5 01/30/1812:49 - (MSD) R3282839-6 01130/1813:03 ' Cp Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD limits Analyte ugA ugA ugA ugA % % % % % rTc Nitrate 5000 981 6010 6090 100 102 1 80-120 1.37 15 Write 5000 ND 5070 5070 101 101 1 80-120 0.077 15 Sulfate 50000 ND 53300 53200 101 101 1 80-120 0.114 15 L966301-01 Original Sample (OS) • Matrix Spike (MS) (OS) L966301-01 01/30/1817;W • (MS) R3282839-8 01/30/1817:37 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte ugA ugA ugA % % Nitrate 5000 ND 5030 99.8 1 80-120 Nitrite 5000 ND 5270 105 1 80-120 Sulfate 50000 ND 52800 103 1 80-120 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: GLOSSARY OF TERMS ONE LAB. NATIONWIDE. .V Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not FP intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions FTC MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). E RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. Fn SDG Sample Delivery Group. U Not detected atthe Reporting Limit {or MDL where applicable). sSC Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. s If the sample matrix contains an interfering material, or if concentrations of analytes in the sample are higher than the QC Dilution highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target `.G recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control 8Al sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. F The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, Including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Oc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description 61 The blank depletion was greater than the recommended maximum depletion of 0.2mg/L. J3 The associated batch QC was outside the established quality control range for precision. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. J- The associated batch QC was outside the lower control limits; associated data has a potential negative bias. Pf RPD value not applicable for sample concentrations less than 5 times the reporting limit. V The sample concentration is too high to evaluate accurate spike recoveries. ACCOUNT: PROJECT: SDG; DATE/TIME: PAGE: I F• .� .r� 6: I ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences Is the only environmental laboratory accreditedlceniBed to support your work nationwide from one location. One phone cal). one point of contact, one laboratory. No other lab 1s as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our Industry. The most significant bereft to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turnaround time, and preventing crass contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. ` Not all certifications held by the laboratory are applicable to the results reported In the attached report. State Accreditations Alabama 40660 Nevada TN-03-200 2-34 Alaska UST-080 New Hampshire 2975 Arizona AZ0612 New Jersey—NELAP TNO02 Arkansas 88-0469 New Mexico TN00003 California 01157CA New York 11742 Colorado TN00003 North Carolina Env375 Connecticut PH-0197 Florida E87487 Georgia NELAP Georgia 923 Idaho TN00003 Illinois 200008 Indiana C-TN-01 Iowa _ _ 364 Kansas E-10277 Kentucky' 90010 Kentucky' 16 Louisiana A130792 Maine TN0002 Maryland 324 Massachusetts M-TNO03 Michigan 9958 Minnesota 047-999-395 Mississippi TN00003 Missouri 340 Montana CERT0086 Nebraska NE-OS-15.05 Third Party Federal Accreditations North Carolina' DW21704 North Carolina = 41 North Dakota R-140 Ohio—VAP CL0069 Oklahoma 9915 Oregon TN200002 Pennsylvania 6"2979 Rhode Island 221 South Carolina 84004 South Dakota nla Tennessee " 2006 Texas T 104704245.07•TX Texas' LA80152 Utah 6157585858 Vermont VT2006 Virginia 109 Washington C1915 West Virginia 233 Wisconsin 9980939910 Wyoming QLA A21.A— ISO 17025 1461.01 AIHA-LAP,LLC 100789 A21-A— ISO 17025 s 1461.02 DOD 1461.01 Canada 1461.01 USDA S-67674 E PA—Crypto TN00003 ' Drinking Water ' Underground Storage Tanks 3 Aquatic Toxicity ' ChemicallMlcroblologlcal 9 Mold nib Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup andlor the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. WA OR ID NV UT CA T A Tz a AK p 0 B r•P ACCOUNT: MT WY r— — T CO NM 016 NO MN SD ? vvf NY MI NE IA * PA IL 1J7� OH WV VA� KSMO KY T� aTc AR � s a MS AL T GA T TX T LA T FL r PROJECT: $DG: DATE/TIME: ME PAGE: EHC, Inc. PO Box 902 Red Springs, NC 29377 BiM4 Information: pros Analysis / Container / Preservative Gain or Cmuldr fte _,_• of *ESC ti � 1 d m =_ o N � • Z O O "M' q! z & _ <n � Z C) O .z 4 0 N Y * a m 4 Q In P ' hors , w •eowa mr a rw;�,:: „y w+au; ans rsa sass rhaeraG?1fi•9e54 I r.�ass isa sass 0 Rupert to: Mr. "otnas Amrttens Email To: ehCttnrnrnans@tsrddhd net. ; Prajett Description: southern States Coop utr/Scats A Collected: L LR �!)bQ Al37 ce�num;ElliVF iQ TertipiataT7i661 Prelogin: P63262S° TSli.. W3: Hea"w J Wadrter -' L L Phone, 910-843-4456 Fax: 914.843=5376 1i3-1 EMIi1YO-11-MIDS18-3 I (pint}: �._...,_ ry 5lu�•1T�..lO.if WMBERTON,•NC ± Cq fl pzcd by (slgnatur4; Immediate / Packed on let N_ Y V Rush? (lab MUST Be Notified) Quote a Same Day _ RM Day Nerd Day _ S C* Lead Oebl Date Results Needed : Two Day 10 Day Vw aryl No, _ lhres Day l Sample ID Comp/Grab Matrix Depth Date Time trs Shipped Via: FedEX Groin aeati:ilr simpl. a 1 o"h9 a �o �j ►v w 5 x.,x x x x _: • Matrix; SS -Soil AIR -Air F-Fiber GW-Groundwater B-Bloassay WW •WasteWater DW - Drinking Water T -Other Rimarks. +' 6 l f ON `_. � Temp�t•i, Flow Other Santptes returnod vial r�1 UPS _ FCili11 -C*Aer Ttarting1,14 L/ ligg a ft i rb- wc-AL-kri.t CDC 6"1 Prei*ti;lfntaCtt —wPX- _0 CDC SighedllK+Giiralr:. S tiprct setive •fp=_watt N Ccrrre�t boi6lra #txllyd: � Hu:itC,;e, i Yptus .6ehC: Zf H_ VCA Eeea Hf.43iP4eet _Y ;1 Pi4�OSVXt�"Jfl L`arxecG�i�eC _7 ��,'� Re l' tUr y : el Date: Time: x rIt q Receivtdb . S tulp} ,� (�, - Trip Mfkk Retelvedt :Yes r Hcc/ mom T6q - Relinq Wed by : (Signature} Date: Time: R—Aved by; {Signature} ienfp��G� . f �► - , 4Epreservatfan requiEeii by tagbt:Dateji maT Relir4Lkhed by: (Signntwe} Date: De ' 7 K Hold; yeond itinrt ((%h �.. e I.:'nvlrvnmenlal Qualify Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance onfilling out thisform, please visit httasJ/deg.nc.goy/abQu divisions/energy-mineral-land- resources/enerr ,ry-mineral land-Krznits/stormwater-pgrmiWnRdes-industrial-sw#tAb4 Permit No.: N/C/ 5 / dl �l �l�l Ill or Certificate of Coverage No.: N/C/G/ I 1 1 1 Facility Nam : 6 County: 0 kSOA Inspector: 705 � Lk Date of Inspection: I I 4Y 1 16 Time of Inspection: [ t 7- f Total Event Precipitation (inches): 0 . S P No. AfhA _ , T/YC All permits require qualitative monitoring to be performed during a "measurable storm event." i A "measurable storm event" is a storm everts that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Offices By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 0 d ( Structure (pipe, ditch, etc.): Receiving'., C [ ti5) C. 5'(A/VA P1,P-C -h t-!, C L V, 4r k"V-(>r Rov I -\ ibe the industrial activities chat occur within Vip outfall drainage ttL:st,- b -P4:4VL..k*w . a 1-4 ►h R?-(V h fA Page l of 2 5WU-242, last modified OVUM17 2. Color: Describe the color of the discharge 7N)asic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C U, 3. Odor. Describe�distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: l 2 7. Is there any foarn in the stormwater discharge? o Yes f No. 8. Is there an oil sheen in the stormwater discharge? OYes 4 No. 9. Is there evidence of erosion or deposition at the outfall? o Yes WNo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe I V b 54 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 swU-242. Lwt modified OW10017 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000541 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Southern States Cooperative -Lumberton Fertilizer PERSON COLLECTING SAMPLE(S) Joshua Bass PHONE NO. (� CERTIFIED LABORATORY(S) ESC Lab Sciences Lab # ENV375 Lab # Part A. Specific Monitoring Requirements COUNTY Robeson SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Yes _ _ No X (if yes, complete Part B) Form SWU-247, fast revised 21212012 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall:k"'Date" _ Collected .. d�. =5050� 0556; `00530 00400 a (rf applicable) ' ;To Rainfallf a apply p O&GPH Method 1564 SGT :a 1. SuspendedOWAS Sands p--Sampe ey�- rNo� age mo/.d"d`4. ,? _ 1MG-. f inches m 11 fn-ig/I •_ ruffit-WIW4N M"aUpmo FN STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): _(only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, inc)dd�ng the possibility of fines and imprisonment for knowing violations." of 1-2- (Date) Form SWU-247, last revised 21212012 Page 2 of 2 Southern States Cooperative, Inc. 6606 West Broad Street Richmond, Va. 23230-1717 Mall Address: P.O.Box 26234 Richmond, Vs 23260-6234 Telephone (804)281-1000 SOUTHERN May 3`d, 2017 STATES North Carolina Department of Environmental Quality R EC E IV Division of Water Quality 1617 Mail Service Center MAY 0 8 2017 Raleigh, North Carolina 27699-1617 CENTRAL FILES Attention: Central Files DWR SECTION RE: March 2017 NPDES Discharge Monitoring Report for the Southern States Lumberton Fertilizer Plant (Permit #NCS000541) Dear whom it may concern, The Southern States Cooperative, Inc. (SSC) would like to submit this Discharge Monitoring Report (DMR) for the SSC Lumberton Fertilizer Plant. The Lumberton plant is located at 745 Old Whiteville Road in Lumberton, North Carolina and has been covered under an Individual NPDES Storm Water Permit (#NCS000541). The sample was collected by EHG Environmental on March 22°d, 2017. Included with this letter are two copies of the DMR forms and a copy of the analytical lab results. The DMR was signed by the Executive Vice President of the SSC Agronomy Division, Mr. Steve Beeraft on May 2"d, 2017. A renewal application was sent NCDEQ back in November of 2016 but we have not received a response or a copy of the new permit so we are still using the forms and referencing the benchmark limits that were listed in the previous permit that expired in 2016. If you have any questions or comments regarding this facility, feel free to give me a call at (804) 281-1189. Sincerely, �L�Y1 Lauren B. Faulkner Environmental Project Manager Attachments: Discharge A4onitoring Report (2 copies) STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS,,ODD(( FACILITY NAME _ 4�n S�AC_5 _l. urn 64on FiA A W Fla PERSON COLLECTING SAMPLE(S) L Lab . 37S CERTIFIED LABORATORY(S) Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: �c (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY _ O e SOn _ PHONE NOI } (SIGNATURE OF PERNIITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my lmowledge. f Date Does this facility, perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes no (if yes, complete Part B) Part B: Vehicle Maintenance Ac vity Monitoring Requirements Outfall No. Date Sample Collected. ; . ,: 50050 00556 00530 00400 Total Flow ,(If applicable):- Total- Rainfall,•,. : "` Oil & Grease (if.appl.)' Non -polar... U&GrT.PH* .: (1liethod'1664- - SGT-HEM), if apipl Total Suspended- Solids pH New Motor Oil Usage mo/4d1 MG inches En ,. , unit . al/mo Form SWU-247-062310 Page 1 of 2- STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled). Date Total Event Precipitation ('inches): Event Duration (hours):, (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the'system, or those persotis' dirktl -Jrespo6s� Ie inr-gathering iM iiifor'niation,, tt � informfion. submitted is; to the hest of my knowledge and belief, true, accurate, and complete: I am-awaie#t#t.there �e $Ignjl cant penaltieS.for submitting false. in�ormatioa, including the possibility of fines and imprisonment for.lmowing'violat}ons,'' '�' `4' `! . :. (Signature of Permittee) (Date) Form SWU-247-062310 A Page 2 of 2 Permit Number NCS QL00541 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME �9+��M1c1 S [i�es Larrig,6,1 i r PERSON COLLECTING SAMPLE(S) T s jam_ cs CERTIFIED LABORATORY(S) r5SC Lab # Lab # Part A: Specific Monitoring Requirements COUNTY keSO✓) PHONE NO. U (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. 1 1. II I 'I I I � I � c� fir � ♦. � a !I • :I� • � � • Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes —no (if yes, complete Part B) Part B: Vehicle Maintenance Ac ivity Monitoring Requirements Outfall,.�- 'No. Date Sample . Collected '50050i'. •00556 .00530 00400E . Total Flow: '(if applicable) Total y Rainfall . 'Oil;&Grease` (if,appl.) Non -polar O&G/TPH . (Method1664 SGT-HEM), if a. 1. Total Suspended' Solids pH- : " ;New Motor Oil Usage' . mo/dd/ r MG inches unit gaVmo.. Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: -Date 3- �Q-I i Total Event Precipitation (inches): Q e 3 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) ! Form SWU-247-062310 Page 2 of 2 .�. STORMWATER DISCHARGE OUTFALLf(SA�5- COP MONITORING REPORT Permit Number NCS t7D05 y SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACH,M NAME ! oOVAO PN SAAu L XM6--�n Fo-r 4 d iZci Pali` PERSON COLLECTING SAMPLES) Cro,&4/Dobson CERTIFIED LABORATORY(S) Lab # NGDi 73 Lab # Part A: Specific Monitoring Requirements COUNTY ►�Obe5c)r� PHONE NO. �1f I o) -g+3- `iq SIQ__. (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. • : Date mpl Collected ► If it • = _ � • DWR SECTION Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements DWR SECTION Outfall No. = .. Date Sample Collected:.:: - 50050 00556 00530 00400 Total Flow (if applicable) Total" Rainfall: Oil & Grease (if appl.)"". ', Non -polar.: ;O&GIPPH ':'r (iVletFiod 1664 SGT-HEM), If a 1. Total <Suspened. Solids pH New Motor Oil Usage . - moJd MG in :. - unit t '" al/mo Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date Attn: Central Files Total Event Precipitation (inches): 1617 Mail Service Center Event Duration (hours): (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours).' (only if applicable — see permit.) "I- certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the'system, or those person' ' dirgctly.f`espoOW6 for. g&theting the information; th infornifltion.,stibmitted is; ;to the best of my irnowledge and belief, true, accurate, and complete..I am-awa e#hat.th re,a_ re sign fic0t penalties.for subnllittiug-fatse'inlorn[ati' including the possibill of fines and imprisonment %r.lmo�ving'violatlons.'' (Signature of Permittee) (Date) 10 Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000 S 4 FACILITY NAME SOASM 540fe �60 n _ re4+ i_Z_er PERSON COLLECTING SAMPLE(S) n CERTIFIED LABORATORY(S) SC Lab # L!G D i $ r13 Lab # - Part A: Specific Monitoring Requirements copy SAMPLES COLLECTED DURING CALENDAR YEAR- 2-01 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY e5o n PHONE NO. (q 10) Kt y3- y 56 (SIGNATURE OF PERMIT TEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. 1Samplek 1 1 1" 1 1 1 1 - 1 • , Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ^ yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Ac vityMonito ' Requirements Outfall No. Date Sample Collected..;; 50050 00556 - . 00530 00400 Total Flow ,(if applicable) Total Rainfall; • Oil & Grease (if appL) ': ', Non -polar., . . t , •)&GnTH`• ':';' (Metliod 16d4 GT-HEM), if a0pl. Total -Suspe'ed. Solids yks1 pH New Motor Oil Usage . mo/dd/ MG i ches :- . unit : al/mo Form SWU-247-662310 Page I of 2 .STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 0005 4 ! _ SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no Iater than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SOAtrn s s Lum�je 4nT CQUNTY iZo6oso I PERSON COLLECTING SAMPLE(S) ' - E "o to E E 1 Vj�f E&ONE NO. (_ $)q) &I -- 11'�q CERTIFIED LABORATORY(S) Sc; "c s _ Lab # Lab # DEC Q 1 Z 0 1 RSIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate CENTRAL FILE@)mplete to the best of my knowledge. Part A: Specific Monitoring Requirements DWR SECTION • ,. �i Total. Flow + Does this facility, perform Vehicle Maintenance. Activities using more than 55 gallons of new motor oil per month? _yes no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date- - Sample Collected - :. ,: 50050 00556 00530 OD400 Total Flow ,(if.applicable) Total- Rainfall:- Oil &• Grease (if.apgk.)'.- Non -polar.. _ ;O&G/TPii�• -'r? C1!khod 16d4 • SGT-HEM}, if Total =Suspehded. Solids pH , New Motor Oil Usage . mo/dd/yr MG inches nig/l unit mo form SVVU-247-062310 Page 1 of 2- STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation ('inches): Event Duration (hours):' (only if applicable -- see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathdr and evaluate the information submitted. Based on my inquiry of the person or persons who manage the'system, or those persob `dirocgy;, eglopsOiie %r gatherjing`thb iidfoirntation, tl infor tion.:s"miitted is, io the best of my knowledge'and belief, true, accurate, and complete: I am.awa a that.tli re ire gigs cant penaltles.for sub mitting.false: fnformatiou, i chiding the possibility of fines and imprisonment for.irnowirig violat#ons.?' t (Signature of 'ttee) (Dat ) Form SWU-247-062310 Page 2of2 s STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS oO 6 S 4 L SAMPLES COLLECTED DURING CALENDAR YEAR: zD i (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SO"(0 SJ a^'t PERSON COLLECTING SAMPLE SS ! Lab # hyfC S !o 9' CERTIFIED LABORATORY(S) , iby Lab # Part A: Specific Monitoring Requirements COUNTY KOLE'SO PHONE NO. (S2V l - 1179 (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. • Date Sample Collected &11a i Does this facility, perform Vehicle Maintenance Activities using more than SS gallons of new motor oil per month? _ yes )! io (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date 50050 00556 00530 00400 Total Flow Total- Oil &• Grease Non-potar,. _ . , Total pH New Motor No. Sample Collected .: : ,(if.applicable}, Rai (it.appl.)". ,U&G/TPH-PH- Suspended. Oil Usage . (IVIethod I664 - Solids _SGT-HEM), if r ' mo/dd/ MG - inches m unit Form SWU-247-062310 Page 1 of 2•- STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation Cinches): Event Duration (hours):' (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the'systeny or those persotis'directly irespons(lile # r. ga er}ng`th) eiifoirmation; the inform tion,'subnutted is, :to the best of my knowledge'and belief, true, accurate, and, complete:.I am-aw*i #iat.there ate �igffncant penaltfes.fpr submi#ting-[aisd information, including the possibility of fines and imprisonmenf for. knowirig-violatjgns,!' :r&6�nw (Signature of P tee) (Date Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2016 Individual NPDES Permit No. NCS000541 or Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1' of the following year. Facility Name: Southern States Cooperative Lumberton Fertilizer Plant County: Robeson Phone Number: (91J0 739-7562 Total no. of SDOs monitored 1 Outfall No. 001 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ® � MAR 1 3 2017 If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? � � Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Parameter, (units) Total Rainfall, inches BOD mglL COD mg1L Total Ammonia mglL Total Nitrogen m IL TKN mglL Nitrate mglL Nitrite mg/L Total Phosphorus m IL Benchmark NIA 30 120 7.2 30 20 10 10 2 Date Sample Collected, mmlddlyy 01118/2016 3.7 2.0 13.1 <.25 2.12 0.6 1.52 BDL 0.28 07/20/2016 1.0 2.0 30 <.25 3.78 1.57 2.21 BDL 0.756 Additional Outfall Attachment SWU-264-Generic-251Vlay2010 Outfall No. 001- continued Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No Yes ❑ No Parameter, (units) Total Rainfall, inches Total Suspended Solids m IL Sulfate mg/L pH storm water pH rain gauge Benchmark N/A 100 500 6-9 6-9 Date Sample Collected, mmlddlyy MMMMM 01/18/2016 3.7 4.8 .6.26 6.04 6.04 07/20/2016 1.0 18.8 6.61 7.86 7.86 3 s I ' r SWU-264-Generic-25May2010 1� s I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, -to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature_ Date Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: 'ASHEVILLE REGIONAL OFFICE FAY_ ETTEVILLE REGIONAL_ OFFICE MOORESVILLE REGIONAL OFFICE 2090 US Highway 70 ., 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 . Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE_ ASHINGTON REGIONAL OFFICE WILMINGTON REGIONAL _OFFICE 127 Cardinal Drive Extension 3800 Barrett Drive 943 Washington Square Mall Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 •' WINSTON-SALEM REGIONAL OFFICE CENTRAL OFFICE 1617 Mail Service Center -"Topmseme,Winston-Salem, 585 Waughtown Street NC 27107 Raleigh, NC 27699-1617and Qua entia►rce(336) 771-5000 (919) 807-630D j Nvrh►i Carrtwater.:.'' SWU-264-Generic-25May2010 i i I � I i �� .,� � � } � � .�" �a k5 r r';E_ 3 '�.� i.� �.- j F.: H Southern States Cooperative, Inc. 6606 West Broad Street ? Richmond, Va. 23230-1717 L/ Mall Address: P.Q.Box 26234 Richmond, Va 23260-6234 Telephone (804)281-1000 SOUTHERN October 23`d, 2015 STATES North Carolina Department of Environment and Natural Resources Division of Water Quality Attention; Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 • RE: DMR for Southern States Lumberton Fertilizer Plant located in Lumberton, NC (Permit #NCS000541) Dear whom it may concern, The Southern States Cooperative, Inc. (SSC) would like to submit the discharge Monitoring Report (DMR) for the second monitoring period of 2015 for the SSC Lumberton Fertilizer Plant. The Lumberton plant is located at 745 Old Whiteville Road in Lumberton, North Carolina and is covered under an Individual NPDES Storm Water Permit (#NCS000541) that requires the facility to collect semi-annual samples from one designated storm water outfall on the property. SSC hired EHC Environmental from Red Springs, NC to collect the semi-annual samples and to complete the Qualitative Monitoring Report. Two copies of each DMR form are included. If you have any questions or comments regarding this facility, feel free to give me a call at (804) 281-1189. Sincerely, � co), Lauren B. Faulkner Environmental Project Manager Il Attachments: DUR form M i STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS, 0005 FACILITY NAME - QtAern Si s TEr-1 [(-22r f PERSON COLLECTING SAMPLE(S) d a CERTIFIED LABORATORY(S) LSG r s Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 1�20f (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) r"�7 COUNTY r* RECEN NE NO. U OCT 2 8 20JESIGNATURE OF PERMITTEE OR DESIGNEE) . By this signature, I certify that this report is accurate CENTRAL FILESnplete to the best of my knowledge. DWR SECTION DateII I " # fir Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes -'-'no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall • 'Date- 50050 00556 00530'', 00400 No. Sample Total Flow Total Oil & Grease-T. ,Non-polarTotal �5, pH4 * > -New Motor wr Collected (if applicable) Rainfall (if appl.)=' O&GITPH Suspended ti Oil Usage;";'p '(Method 1664 Solids'_ SGT-HEM); if • a 1" ::. MG` °.'-- .: inches � ��I ' . 'm unit :� � al/mo *: iiu Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility offines and im?-is onment for knowing violations." (Date) Fornt SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ��// MONITORING REPORT Permit Number NCS Q706_# SAMPLES COLLECTED DURING CALENDAR YEAR: z017' (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Prn S Zf7 COUNTY - Ao6es n PERSON COLLECTING SAMPLE(S) PHONE NO. ( ) - CERTIFIED T ABORATORY(S) E C Lab it Lab # Part A: Specific Monitoring Requirements (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. DateII I Collectid Mill'' /1/ 1I - u f/MEN - Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓50 (if yes, complete Part B) Part R- Vphirlp Main1pnanre Artivity Mnnitnrinu RenuirpmentS �Outfall �,;: No.r ' Date Sample ;: - Collected = 50050 a00556 0 Total Flow (if applicable),,, r Total W Rainfall Oil & Grease .(if,appl:} Non -polar O&GlIPH. '(Method 1664-Solids' SGT-HEM), if . a l: Total Suspended pH New Motor F -Oil Usage mo/dd/yr MG inches m :unit al/mo Form SWU-247-062310 Page l of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-t617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete..I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonnDefit for knowing violations." 4&x (Signa ure o e tee (Date) Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT ` Permit Number NCS OM SAMPLES COLLECTED DURING CALENDAR YEAR: �� (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME a ouv,tfn 5 PERSON COLLECTING SAMPLE(S) i54- - rack CERTIFIED LABORATORY(S) C 5 ' Lab # F/PV r Lab # Part A: Specific Monitoring Requirements COUNTY Rn�og.sOc-% PHONE NO. (XPq ) c4I — f I S{`I' (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. ate I Collected. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Activitv Monitoring Requirements RECEIVED DENR-LAND QUALITY iwv Sri RMITf M- Outfall No. Date Sample- Collected' 50050; 00556 00530 00400 Total.Flow if a hcable C PP_ ) 9 Total: Rainfall Oil & Grease �f a L "' 0: pp) fNon-polar O&G/TPH '.(Method 1b64 SG T-HEM), if Total S 'ended . usp Solids pH' New Motor Oil,Usa a '.; g mo/ddl ' MG inches m unit al/mo Form SWU-247-062310 Page 1 of 2 MW STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitt(Date) v- Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS WO 5 FACILITY NAMES L�Ae,t-n) VP A-, \;-Lj PERSON COLLECTING SAMPLE(S) K-"C - aci,- C�bson CERTIFIED LABORATORY(S) F !Z 1_&b Sete r' rZA Lab # 3`75' Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: Q O I S (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY 90 � e So r� PHONE NO. (2tb j j Q91-1\ (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. 1 1, f DateI Sample -Collected I I 1 1 1 1 1 • up., MRim , 1 1 1 1• f, - 1� : �4 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Zo (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements OutfaU t• .' No. x' "' ' :Date° :: :n 'Sample Collected :50050,x,- - 00556 00530 00400 Total Flow (if applicable) Total Rainfall OR & Grease :(if appl.) Non -polar O&G/TPH (Method:1664:- SGT-HEM),-if appl. 'Total. Suspended Solids h pH t -New Motor •Oil Usage -mo/ddl e: - , :MG,- inches m unit.. al/mo Form 5WU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable -- see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of finesod imprisonment for knowing violations." (Signature of Permittee) (Date) Form SWU-247-062310 Page 2 of 2 Southern States Cooperative, Inc. 6606 West Broad Street Richmond, Va. 23230-1717 Mail Address: P.O.Box 26234 RECEIVED Richmond, Va 23260-6234 Telephone (804)281-1000 FEB 02 2015 January 27", 2015 DENR-LAND QUALITY SOUTHERN STORMWATER PE#RMITTfNC 57ATES North Carolina Department of Environment and Natural Resources Division of Energy, Mineral and Land Resources Attention; Central Files 1612 Mail Service Center Raleigh, North Carolina 27699-1612 RE: DMR for Southern States Lumberton Fertilizer Plant located in Lumberton, NC (Permit #NCS000541) Dear whom it may concern, The Southern States Cooperative, Inc. (SSC) would like to submit the discharge Monitoring Report (DMR) for the first monitoring period of 2015 for the SSC Lumberton Fertilizer Plant. The Lumberton plant is located at 745 Old Whiteville Road in Lumberton, North Carolina and is covered under an Individual NPDES Storm Water Permit (#NCS0 that requires the facility to collect semi-annual samples from one esignated storm water outfall on the property. SSC hired EHC Environmental from Red Springs, NC to collect the semi-annual samples and to complete the Qualitative Monitoring Report. Two copies of each DMR form are included. If you have any questions or comments regarding this facility, feel free to give me a call at (804) 281-1189. Sincerely, Lauren B. Faulkner Environmental Project Manager Attachments: DMR form STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS OM 5 4 I SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME 5 ouYhcM SIBS L",A-on eAI Alzer t' 6la ` PERSON COLLECTING SAMPLE(S) -i5 4c- - &rck& CERTIFIED LABORATORY(S) 4SC -Sc-, Lab # F• �✓V-3r75— Lab # Part A: Specific Monitoring Requirements COUNTY' PHONE NO. (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. -Da—te Sample Collected IWITILfl i ' . 1 • • Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Activitv Monitoring Requirements RECEIVED EI; 02 1JE5 Outfall 4 No. _ Date,'y ; •,_kw" Sannple Collected �50050f-' 00556 .00530 �00400 Total Flow (if. applicable) Total 'Rainfall' -Oil & Grease (if.appl:) Non -polar O&G/TPH: ' (Method!1664' -SGT-HEM);;if . .Total 'Suspended :Solids: '. pH New 1MR LAN O%TTSWWATE' .- mold -. SMG.x Tinches' -m m :unit-. - � :� al/mo D QUAUTY PERMITTING. Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date - Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of Imes and imprisonment for knowing violations." I2 (Signature of Permitte te) Form SWU-247-062310 Page 2 of 2 I STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000 cJ 1 FACILITY NAME -"yC(1 Smith '^",4er6n Ver v1 �i79 f PERSON COLLECTING SAMPLE(S) AMC- C,2, A, f lib Zn r, CERTIFIED LABORATORY(S) Eg1 lAL Lab # 2�iUV3-75' Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: I S (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Ro RS PHONE NO. ( i) t (SIGNATURE OF PERMITI'EE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. fSample Date Collected Oilipv 0Oil M1 Mal11 1 41 •.-q- ate. ■ 11 1 1 1 I�R• f� : 1L Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓-no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall V, ; No. iDate - -'50050; Sample Collected - - - - 00556 • :00530 `06400 Total Flaw (if applicable) Total Rainfall Oil•& Grease (if appi.) Non-polar'Total O&G/TPH (Method 1664 SGT-HEM); if Suspended rSolids pH New Motor Oil Usage inches unit. allmo Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of futesOd imprisonment for knowing violations." (Signature of Permittee) (Date) Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2015 Individual NPDES Permit No. NCS000541 or Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1" of the following year. Facility Name: Southern States Cooperative Lumberton Fertilizer Plant County: Robeson Phone Number: (910) 739-7562 Total no. of SDOs monitored 1 Outfall No. 001 t —, - Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ F No ® � Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ® FEB $ 206/l/ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? �d Enough consecutive samples below benchmarks to decrease frequency ❑ ' Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Parameter, (units) Total Rainfall, inches BOD mg/L COD mg1L Total Ammonia . mg/L Total Nitrogen m IL TKN mglL Nitrate mg/L Nitrite mglL Total Phosphorus m IL Benchmark NIA 30 120 7.2 30=- 20 10 10 2 Date Sample Collected, mmldd/yy 0' == 01/05/2015 2.0 2.0 37.0 BDL 19.0 0.5 18.0 .016 1.3 09/24/2015 1.3 10.8 245 .53 4.56 3.18 1.38 BDL 0.542 Additional Outfall Attachment SW U-264-Generic-25 May2010 Outfall No. 001- continued Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWO to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No ❑ Yes ❑ No�® Parameter, (units) Total Rainfall, inches Total Suspended Solids. .. Sulfate mglL pH storm water pH rain gauge. Benchmark N/A 100 500 6-9 6-9 -Date .Sample -T Collected, mmlddtyy 01105/2015 2.0 47 26.0 6.2 6.2 09/24/2015 1.3 15.7 14.1 7.44 7.44 4 - SWU-264-Generic-25May2010 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the passibility o nes and imprisonment for knowing violations." Signature Date 2 •� Mail Annual DMR Summary Reports to: DWQ Re ional Office Contact Information: ASHEV "LE_REGIONAL;.OF.FICE FAYETTEVILLE REGIONAL OFFICE MOORESVILLE=REGIONAL-OFFICE 225 Green Street 610 East Center Avenue/Suite 301 2090 US Highway 70 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 -(704) 663-1699 910 433-3300 RALEIGWREGIONXI ;OFF[CE WASHINGTON REGIONAL. OFFICE WILMINGTONREGIONAUOFFICE 943 Washington Square Mall 127 Cardinal Drive Extension 3800 Barrett Drive Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTO*SALEIVI_R_E_GIONAL.OFFICE CENTRAL -OFFICE 1617 Mail Service Center Raleigh, NC 27699-1617 76nd;ennence - 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 (919 807-6300 ,_` -+ina'water. 4 SWU-264-Generic-25May2010 y STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000 t i SAMPLES COLLECTED DURING CALENDAR YEAR: go) (This monitoring report shall be received by the Division no later than 30 days from `j_ ` y n the date the facility receives the sampling results from the laboratory.) FACILITY NAME SO+•A` AZI-1\ 5�� �,rY1�pr i�r+ �2r �; �iZ2>• 7' ���'l� COUNTY 4S0 r1 PERSON COLLECTING SAMPLE(S) &rn&4 lqpy-,x PHONE NO. (_8DA_) a$ CERTIFIED LABORATORY(S) E Lab #�5%f?f 70Y/ Lab # �. 13SG11 (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report Is accurate complete to the best of my kinpwledge. Part A: Specific Monitoring Requirements ISampleI Date Collected 1 i •. I s _ R• •' •' 1 I I �lu �� s �`}r• /E• A / I I Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements RECEIVED- SEP _ 5 2014 Outfall No. Date Sample Collected 50050 00556 00530 00400 D Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH §7~4WER Oil Usage mo/dd/yr MG inches m unit gallmo )UALITY 'ERMITTING Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date o B-DY-1N Total Event Precipitation (inches): 1. % Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS� I 1 SAMPLES COLLECTED DURING CALENDAR YEAR: di (This monitoring report shall be received by the Division no later than 30 days from ff� C ` the date the facility receives the sampling results from the laboratory.) FACILITY NAME StxnZ'h2er� J���QS L rn� eri-tn rer+Ais t�_ Phruf COUNTY 4OL-es6n PERSON COLLECTING SAMPLE(S) �a PHONE NO. (g0Y) - CERTIFIED LABORAT012Y(S) F_SC Sc , enr e s Lab # rcNVz-7s�o? 1 ��$j0(�y 1 Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of.my knowledge. Part A: Specific Monitoring Requirements • D. m .Collected Flow (if :pp ', , ' a • • + i + I Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ^ yes Xno (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&GArPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches EVA To unit al/mo Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 0 -0 -)q Total Event Precipitation (inches): �• / Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn. Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibilljy.-pf fines and imprisonment for knowing violations." 15.1 �f- (Signature of Permittee) (Date) Form SWU-247-062310 Page 2 of 2 j` c STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS Coo 51 SAMPLES COLLECTED DURING CALENDAR YEAR: �Oly (This monitoring report shall be received by the Division no later than 30 days from jf!� c L r the slate the facility receives thesamplingresults from the laboratory.) FACILITYNAME �f fi-,17 ?Yates 4u�0! �P��,%;zPr P/a�� COUNTY AOe5CYI PERSON COLLECTING SAMPLE(S) ra S PHONE NO. (&2N -EL IOC _ _ CERTIFIED LABORATORY(S) 15 C L.Qt, Su nce$ Lab # Y �S lJQ170�6Tg0�11 Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Part A: Specific Monitoring Requirements - a I Date 'Sample Collected CIO 11 I I '/ ! • r ' i III. N Does this facility, perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes kno (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Kt ;tl V CV SEP 5- 2014 DENR-LAND QUALITY WITTING Outfall No. . Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable): Total Rainfall:,-." Oil &• Grease (if appl.) `:: '; - Non -polar.. - "O&G,T H*• ':': 0 ethod 1664- Total <Suipended. Solids pH New Motor Oil Usage - mold MG inches m : ;:.. unit gzwmo Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours). (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly galber and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those personis'directl"y:i"ponij6ie for gathering"the information; tli� inform0'— on'sabmitted ls; io the best of my knowledge'and belief, true, accurate, and complete: I am awake 11iat.there ate signtficai it penalties.for subm tbri `Ialse-lfiforntation, ' . including the possibility of fines and imprisonment for.lcnowitig,violatlons.' (Signature of Permittee). (Date) Form SWU-247-062310 Page 2of2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 0206 i SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITYNAME 01A%ern S"S LQfrbn Fr lr'2er f hartL PERSON COLLECTING SAMPLE(S) CERTIFIED LABORATORY(S) G Lab e5 Lab#rNDWa170Q/BIoc)q/ Lab # Part A: Specific Monitoring Requirements COUNTY 06Wn - _ PHONE NO. LP! 1_Q81- IO2O (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. • ,. Date Sample, Collected + � 1 "W Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yesno (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfan No. Date Sample Collected 50050 00556 00530 00400 Total Flow .(if applicable),- Total- Rainfall,, _ Oil & Grease (IFappl.)":: ". Non -polar.. ;O&G/T H*- ':': fNfetiZod1664 sGT-HEM), If appl., .. _ Total -Suspended. Solids pH New Motor Oil Usage mo/M MG Inches M94 unit o Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 09- Total Event Precipitation (inches): 2, 5�7 Event Duration (hours): (only if applicable -- see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable - see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the'system, or those persons:dlrfetly- espoiiszIke Eor.gaWering'tlfe information; the lnform�tion.'submitted is-io.the best of my lnowledge'and belief, true, accurate, and complete: I am-awa�eihaith6r` e. re $i'gn cant penalties.fpr submitting-falso information, ".' including the po fines and imprisonment for. knowittg violatjonsr?' (Signature of Permittee) (Date) Form SWU-247-062310 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2014 Individual NPDES Permit No. NCS000541 or Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March !"t of the following year. Facility Name: _Southern States Cooperative Lumberton Fertilizer Plant County: Robeson Phone Number: 9( 10) 739-7562 Total no. of SDOs monitored Outfall No. 001 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ® Yes ❑ No ® ! - JXN 3 0 2015J t JAAN2 02ms Yes ❑ No ® -- -- - —� Parameter,`(units) OD COD Total,Ammonia Total. TKN Nitrate Nitrite Total Total Rainfall, ,> mglL mg1L mg11L, Nitrogen = mg/L mg1L ,., ' niglL Phosphorus inches m !L m -1L Benchmark' NIA 30 120. y = 7.2- 30 20 40 - io 2V Date Sample Collected, mmlddlyy 02105/2014 0,5 4,0 28.0 0.83 6.0 2.0 4.0 BDL 2.2 0810412014 5.3 38.0 0.78 13.0 2.6 9.9 0.48 0.70 Additional Outfall Attachment SWU-264-Gen a ric-25May2 010 Outfall No. 001 -continued Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier.2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No ❑ Yes ❑ No Total Rainfall, inches Parameter, (units) Total .Suspended Solids. m IL ;Sulfate - mglL pH. storm water ,. pH rain gauge n. .-. . Benchmark " N/A 100 500 6-9 6-9 Date Sample Collected, mmlddlyy 02/05/2014 69.0 13.0 5.64 5.32 08/04/2014 46.0 9.8 6.39 SW U -264-Generic-25M ay2010 4 , rify,r penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information; the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: ASHEVILLE REGIONAL OFFICE FAYET_T_EVILLE REGIONALDFFIC_E MOORESVILLE REGIONAL°OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE LW ASHINGTON REGIONAL OFFICE ,WILMINGTON=REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919)791-4200 (252)946-6481 (910)796-7215 WINSTON=SALEM REGIONAL'OFFICE CENTRAL OFFICE j 585 Waughtown Street 1617 Mail Service Center 'To ed Winston-Salem, NC 27107 Raleigh, NC 27699-1617 i ande harnprae� 336 771-5000 (919 $07-6300 North Caidina's +eater..." SWU-264-Generic-2510ay2010 ' STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2013 Individual NPDES Permit No. NCS000541 or Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1" of the following year. Facility Name: Southern States Cooperative Lumberton Fertilizer Plant County: Robeson Phone Number: 9( 10) 739-7562 Total no. of SDOs monitored 1 Outfall No. 001 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ® Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ® No ❑ FEB 2 # 2014 If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency Received approval from DWQ to reduce monitoring frequency Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Parameter, (units - Total,BO k :. _ : _ z Rainfall, ,D COD Total Ammonia Total TKN Nitrate Nitrite Total . mglL�:,. mg/L J m 11L= � �.. g w:� ,; Nitrogen , mg1L .},, ' mg1L ing1L = °Phosphorus inches =. F rn ..; Benchmark N/A : • .: : 30. l20 :: =7.2 30:, __ 20. _ _10 10 2, :. Date Sample `4Collected `; mmlddlyy 02/13/2013 0.75 BDL BDL 0.3 16.0 2.8 13.0 BDL 0.680 03/1212013 0.4 NA NA NA NA NA 2.4 NA NA 04/29/2013 1.75 NA NA NA NA NA NA NA NA 08/19/2013 2.1 4.4 22.0 1 1.2 5.4 3.8 1.6 BDL 0.68 Additional Outfall Attachment SW U-264-Generic-25 May2010 Outfall No. 001- continued Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ® No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency Received approval from DWQ to reduce monitoring frequency Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ' ; ' • . = • Parameter, 6nits) �x Total Total r Sulfate p H' = "Rainfall Suspended 1 -pH m IL storm water x inches Solids rain gauge: n . m IL .:.Benchmark N/A 100 500 6-9 6-9 Date'Sample Collected, mmlddlyy 02/1312013 0.75 32.0 26.0 7.05 7.42 03/12/2013 0.4 74 NA 6.35 04/29/2013 1.75 57 NA 6.66 6.74 08/19/2013 2.1 14.0 11.0 5.8 SW U-264-Generic-2 5 May2010 r ""I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the -possibility of fines and imprisonment for knowing violations." C � /--,- _ Signature a -- Date DWQ Recaional Office Contact Information: 2090 US Highway 70 Swannanoa, NC 28778 (828) 296-4500 RAIEIGH REGIONAL OF 3800 Barrett Drive Raleigh, NC 27609 (919)791-4200 585 Waughtown Street Winston-Salem, NC 27107 771-5000 Mail Annual DMR Summary Reports to: FAYET.TEVILLE REGIONAL OFFICE 225 Green Street Systel Building Suite 714 Fayetteville, NC 28301-5043 (910) 433-3300 WASHINGTON REGIONAL OFFICE 943 Washington Square Mall Washington, NC 27889 (252) 946-6481 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 807-6300 40ORESVII:LLEREGIONAL OFFICE 610 East Center Avenue/Suite 301 Mooresville, NC 28115 (704) 663-1699 [4MINGTON REGIONAL OFFICE 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910)796-7215 'To preserve, protect and enhance Wrth Carolina's water._.' SW U-264-Generic-25 M ay2010 Lawyer, Mike From: Lauren Faulkner <Lauren.Faulkner@sscoop.com> Sent: Wednesday, September 04, 2013 3:17 PM To: Lawyer, Mike Cc: Mark Gillis Subject: Southern States Lumberton Fertilizer Plant Attachments: 20130904150341479.pdf Attached is a scanned copy of the DMR for the Southern States Lumberton Fertilizer Plant for the second monitoring period of 2013. One original and one copy were mailed into NCDENR's central files but I wanted to send you a copy as well. All parameters are well within the permit limits other than the pH which was slightly below 6 but the pH of the rainwater was even lower so it does not appear to be caused by anything coming from the site. Thanks, Lauren Lauren A Faulkner Envirvnrnenta[Project MaruDer Sou tfienzStates Cooperative, Inc 804-281-1189 NOTICE: This e-mail message, including files attached to it, may contain confidential information or legally privileged information that is intended only for the use of the ADDRESSEE(S) named above. If you are not an intended recipient, you are hereby notified that any reading, distribution or copying of information contained in this message, or the taking of any action in reliance upon the information is strictly. prohibited. If you have received this message by mistake, please notify the sender immediately by reply e-mail, and immediately delete the message and attachments from your system. Thank you. STORMWATER DISCHARGE OUTFALL (SDO) MONI ORING REPORT Permit Number NCS a o5 11 FACII,ITY NAMES u n r ( L PERSON COLLECTING SAMPLE(S) J►- c- - CERTI>t'IED LABORATORY(S) CSCL,­tDas&SLab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: ao J�> (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY _P b"-_C -> - PHONE NO} — (SIGNATURE OF PE?Mi'I' M OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. 46 11 t Does this facility perform Vehicle Maintenance Acdvities using more than 55 gallons of new motor oil per month? _•,••, yes kno (if yes, complete Part )B) part R- Vehicle Mnintnnnnre Arlivity Manitnrino, Rcinnirr_mentm Outfall No. Date- Sample Collected 50050 00556 ' . 00530 00400 Total Flow .(ifappli(able)-, Total • Rainfall: .. Oil & Grease (.appl.)',: {• Non -polar. 'O&GITPS''� (Metliad 1664- SGT-HEM ), R alpipl. Total SuslieihYied- Solids pH :' New Motor Oil Usage - 'Molddlvr MG inches ale imit mo Form SWU-247-062310 Page I of 2 STORMIYATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Per at Number NCS Q d0 rJ y FAaor,=NAME Sou4,acn SiAps �umb�� an Fe�;ltz�r P64 PERSON COLLECTING SAl1IPLE(S) oroA,; Qnbscr, CERTITUM LABORATORY(S) ESC. L a 1 Se <o r,ce c Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAIL- 9Q 13 (Tb is monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY o e&X) PHONE NO. (SIGNATURE OF PERMITTEE OR DESIGNEE) By this f$nature, I certify that this report is accurate complete to the best of my knowledge. I i Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X-no (if yes, complete Part B) Part Re VphielP Maintpnan". Artivity Manitnrinv RemYirementC Oattail No. :.. Date Sample Collected:.:; 50050 00556 ' 00530 00400 Total Flow C4apjlicable) Total- Rainfall:' Oil & Grease G-appL)-:•. Non -polar.: , • S :O&C 'H ''= *1 tliod %64• SGT EMK, if Total Suspwded. Salida pH New Motor Oil Usage .. mo! MG inches 17WA,,. unit 9WMG Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date X 19-/ 3 Total Event Precipitation (inches): / Event Duration (hours): (only if applicable — see permit) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit) Mal Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigb, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that guaffled personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, in g the poWbiility fines and imprisonment for knowing violations." .�j _ -4A (Signature of P ttee) (Date) Form SWU-246-112608 Page 2 of 2 24-HOUR SPILL RESPONSE NUMBER (9 t 0)843-445G ENVIRONMENTAL HYDR.OGEOLOGICAL'V Rain Volume Time Samnled CONSULTANTS, INC. Field Analytical Data - NC DENR Certificate # 5538 US EPA Lab Code #NCO1873 Client: Southern states Lumberton, NC Plant ire■��� Analyst: Grady Dobson ■■■■���� JOESC L-A•B 8•C•1-9-N-C-E•S MrThomas AmmonsEHi. , Inc. PO Box 902 Red Springs, NC 28377 Report Summary Tuesday August 27, 2013 Report Number: L652829 -.Samples Received: 08/20/13 Client Project: 13-MY10121-3 iption: Southern States Co 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 750-5850 1-800-767-5859 Fax {6151 758-5859 Tax I.D. 62-0814280 Est. 1970 The analytical results in this report are based upon information supplied by you, the client, and are for your.exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Revievied By: I J14 Hunt , ESC Representative La bona tol y Certifrca tion Numbers A2LA - 1461-01, AIRA - 100789, AL - 40660, CA -- 01157CA, CT - PH-0197, EL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TNO02, NJ NELAP - TNO02, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ -- 0612, MN - 047-999-395, NY - 11742, V!I - 998093910 NV -- TN000032011-1, TX - T104704245-11--3, OK - 9915, PA - 68-029�9, IA Lab #364 Accreditation is only applicable to the teat methods specified on each scope of accreditation held by ESC Lab Sciences, Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA EUP. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 8 Attachment A List of Analytes with QC Qualifiers Sample Work Sample Number Group Type Analyte L652829-01 WG677856 SAMP HOP Run ID qualifier R2791863 B1 Page 3 of 8 OESC J EHC, Inc, Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level 1S L652829 12065 Lebanon U. Mt. Juliet, TN 37122 (615) 758-5658 1-800-767-5859 Fax (615) 758-5859 Tax 1,D. 62-0814289 Eat. 1170 August 27, 2013 -.Laboratory Blank Analyte Result Units # Rec _ Limit Batch Date Analyzed Nitrate .. .:. mg/1 .. .:......':.-: ..:F7G677004 OVUM 09:45 Nitrite < ,1 mg/1 F7G677804 08/20/L3 06:45 Sulfate < 5 mg/1 WG677804 08/20/13 08:45 Phosphorus,Total < ,1 mg/1 WG677983 08/21/0 17:28 Suspended Salads 5 mg/1 ,- WG618157 08/23/13 08:36 COD < 10 mg/1 SOD 0.350 mg/l BOD 0.350 mg/1 Kjeldahl Nitrogen, TKN < ,1 mg/l WG678414 OB/23/13 13:57 WG677856 08/25/13 10:52 WG677856 08/25/13 10:52 W0678687 08/27/13 10r54 Ammonia Nitrogen <:,:1 m9/1 wG678391 08/27113 11:38 Analyte__ Units Result Duplicate Duplicate RFD Limit Ref Samp Hatch Nitrate ::.':;: }',j `::.:?:.sc J/1'• 21.0 19.0 '.'.`'.::::., 10 0:`{k'ii:'i4s1::;i[°.20 .:..., •. L652187-01 WG677604 Nitrite mgll 14.0 14.0 0 20 L652797-01 WG677604 Nitrate mg/1 1.90 1.90 4 20 L653001-01 HG677804 Nitrite :;'.i':;?49%1''. '0 D - {:.0--,: iiiiisisi:i:l.:: ;':,20.'::.': '1653001-01 WG677004 Phosphorus,Total mg/lk 2.80 2.50 3,51 20 1652934•-02 HG677983 Suspended Solids mg/l 2500 2500 1.21 5 L652803-03 WG678157 Suape7ded Solids mg/1 15.0 14.4 4,51 5 1652B29-01 WG678157 COD mg/1 12.0 15.0 22..2.e......^ 5 L652880-03 Y,G678414 COD mg/1 64.0 62,0 3.11 5 L652753-01 WG678414 Phaaphorus,Total mg/l 0.240 0,260 8.00 20 L651562-01 WG677903 SOD ,.::.^........... m9/i 0 0 ::'_::.: •::::'.:; •L:O.:;t`•:i::" :.':: .' 5 .L652803-02 ,::•?.':.rIG677854 BOD mg/l 0 0 0 5 L652805-05 WG677856 Kjaldahl Nitrogen, THN •.:.;=:;:i;_':::;:i.'-'-` :.mg/1 0.460:l::`..:,;,::O.BO.:.;y:-:.:[:::::?18.2.":' 20 :.:: i652996;03.::i(:'±>yG678667 Kjeldahl Nitrogen, TKN mg/1 0 0.140 24A 20 L651562-01 WG678687 Arfanonia Nitrogen •::':-.iy:: a::;;';..' mg/1 0.0520:i.;.:::::=;::;•:0f0780 <'::,'.` ' .39,01 20 Ammonia Nitrogen mg/1 D.0750 0.0740 1.08 20 L652810-01 WG6793RI • Performance of this Analyte is outside of eatablished.crlteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 5 of 8 OESCL.A.H H•C•I••N•C•E•8 ERC, Inc. Mr. Thomas Ammons PO Sox 902 Red Springs, HC 20377 Quality Assurance Report Level I1 L652829 12065 Lebanon Rd. Mt, Juliet, TN 37122 1615) 758-5058 1-800-767-5859 Fax 1615) 758-5B59 Tax I.D. 62-0814299 ESL. 1970 August 27, 2013 `':LaboratnrylControl,'§amplu Analyte Ifnit9 Knosm Val Result t Rec Limit Batch 8 '': _'..'..., :::: 8.34 • .:. 104, 90-110 4G677604 Nitrite mq/l 8 8.07 101. 90-110 WG677804 Sulfate mg/1 40 40.6 102. 90-110 UG677804 Phosphorus,Total mg/1 1 0.981 98.1 90•-110 47G677983 9u6pende.d:.5olld3.: mg/1 773.:''. :: :, 660: 109. 85-115 VIG678157 COD mg/1 183 194. 106. 90-110 WG678414 BOD mg/1 198 189. 95.5 84.6-115.9 WG677856 ROD mg/l 198 222. 112. 84.6-115.4 WG677856 ROD ' :','.`.. : ;mg/1 =, 198 :::, , , ..',:" ?02: `::'' . ... 102 84 ,6-115.4 ' :': 'WG677856 SOD mg/l 198 . 177. 89.4 Bt,6-115.4 10677856 Kjeldahl Nitrogen, TKN ""mgll "'; *.: .,,5, 5,::F ? 5:,6,9 10,3. .' 90-110;.','. :cWG67Bfi87 Ammonia Nitrogen m /l 7.5 7.39 98.5 90-110 WG67B391 Laboratory Control:'5ampleebuplicite Analyte Units .Result Ref %Rec Limit RPD Limit Batch Nitrate mg/ l 8.33 9.34 '' ' 104: .;.'..;: c..: :{ .::;;'90=110.:::::`:. ; :0 22R :=': ' ::;=20, ;:1:: • ii: KG577804 Nitrite m9/1 8.07 8.07 101. 90-110 0 20 WG677804 !fate m /l 40.8 40.6 102. 40-110 0.491 20 WG677804 Phosphorus,Total mg/1 0.981 0.981 98.0 90-110 0 2D WG677983 Suspended.?Solid s..{;:';:';;_.:?:;: [.: !W 8//. 840. 101)."'85-115 =.`.:.:?.0..475::::`:::.-J.:52::?-` °r:::' VIG678157 COD mg/l 196. 194. 107. 90-110 1.03 5 W0678414 Kjeldahl Nitrogen, TKN mg/1 5.84 5.69 106. 90-110 2.60 20 WG678687 Ammonia Nitrogen ::..::.:::::== <-:;;.`:;..:i::.'>..:::z:i_:.. mg/1 '- 7.64 7.39 102. 9D-110 '...' :-:'3.33 - i:.': ' ;:20 - =`.: i ,.:':WG678391 Matrix Spike Analvte Units i4S Res Ref Res TV I Rec Limit Ref Samp Batch Nitrate mg/1 9.11 4.40 5 94.2 80-120. ;;',L652810;01, hG677804 Nitrite mg/1 5.03 0 5 101. 80-120 L652810-01 WG617804 PhoSpharus,Tota1';; - ;':mg/1 2.56 0 2.5 •"10?. ....,9.0.-110: :;':'L6527.95-01'," i::"6779B3 Con mg/l 624. 220. 400 101. 90--110 L652801-01 WG678414 rformance of this Analyte is outside of established criteria. For additional information, please see Attachment,A 'List of Analytes with QC Qualifisrs.' Page 6 of 6 OESCL•A-B S•C•I•L'•H C•E•9 ENC, Inc. Mr. Thomas Ammons PC Box 902 Red Springs, NC 26377 Quality Assurance Report Level II L652829 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is affected is flagged with the appropriate qualifier in Appendix 8 of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytea above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. blatrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental aample that is spiked with known concentrations of target analytea. The percent recovery of the target analytea also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a "J5" or a "J6". The relative percent difference (4RPD} between the matrix spike and the matrix spike duplicate recoveries is all calculated, If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 8 of 8 12065 Lebanon Rd. t9t. Juliet, TN 37122 (6151 758-5058 1-800-767-5659 Fax (615) 758-5859 Tax I.D. 62-0814299 Est, 1970 August 27, 2013 Billing information; na WsislContainerlPreservattve Chain of Custody � ' ' 5 �� '° EHC, Inc. page —of Mr. Thomas Ammons PO Box 902 PO Box 902 s Red S rin s NC 28377 P g Red Springs,PiC 283Tf K OES , ra Y- i': L-A'B5-C•r•E•N•C•S-S i ' V l f `5• iN { y. 12055 Eci�amn Road Report �; Fina1F Mr. Thomas Ammons ehctammons@earthlink.net r r ���,' }`' a- : Mtlulict iN3712Z {, ' s; O ram,, {, .r . Phone: (OW) 767.5854'.. Project_ )eScription Southern States Coop cd :.. _ Z"&"'i Pa ra'` it >, �n cn rt O ry ' �;« ' rt Phone: (615)7s8-5658 Fax (615) 75$-5"9 "hwe: (910) 843-4456' rent r Joel # Lab Project" Ax:' %Z%— ENVHYD-11=MIQ51&3 _ , p� . C219 (910)843-5376 :. a !N. a by iP++nt) jf I- .,, / S,telFaoitty fD# P.O. lr h3rrL x'r'ca3A" r ,w., �,r sryi. L✓a w? ,S } nc iD f fig" I, BERT N ,' i ,rp�> # i+ - Q N F ` a - �-r ,- YEA^ �S�riw eaed by (slgnalurej: USA (t.anBe Not _ Same Day ............ ...2049E Date Results Isceded�a Rm4lediBtCt ice N Y Nwd DW ................ 100A Two Day ............. ... .50% , : " No.1'7- �+t i r+y'l� k CV say,aee1►nT'ir1G6�'P411Q9i 4 jQ� �a rc yv fah F T li . f x _171' r Jr"' •� [ ^S�' ry Ema3i? Ycs aCixd on -- ay...._ Three 259i �No FAX?�u5' No Yes S L N x Vic; tiSlil 11E;C'etiG t1q { ._ .... ...— CntrSr ❑ +c3, ., . �.,;�W. >.ti,.. .,... _ 0 E- sample ID ComplGrab ivlatrat' DePlh Date Tame U Z 1 RernarWGontarrinml Sample 0 flab only}. -I (vim, ���ry�y��•) J ��{{ 041 .`Metrlx SS - SOB GW • Groundwater W W - WasteWater DW - Drinking Water OT- Other. Rffami* r� Temp ) .� c i — ,z 7z3.yO&low Other Sul3 . (t?3 . SIB 7 RelFnq by Btu R Date: Time: ecety (Signature) esretur vma:.., FadF,.at C3Couner ❑ ,CondltmOn >i4 r ram( ) ., rr �"'�f G {�,�, , � �.�5r!,s � u��t �.� ate: tme emp a k t {lOtt 6s, ece F ` ,hod ece ( t r`� a : ?CE)C ScaS3ntaCt `��tt��1 5 nrNished E r s0o Yo j fa byr(Signal ` 4 k �S '�yax -- ii1 ': 'J .. rnr`.:�. %.Fy�•k5 ate rrne D8 .' ;+ hGy re �-Tim V IRAN _�1-r�u'x fi' 1.rip xp 1 /Y cBSd ar3 � �Ct`a �� lY 4{y 1•k-..'.7i.''' STORMWATER DISCHARGE OUTF'ALL (SDO) MONITORING REPORT Peru Number: NCS 00 0 5-1/ or Certificate of Coverage Number. NCG FACI7 m NAME u 6cn Sots Luyn6er6r, rer4j_aer N4 PERSON COLLECTING SAMPLE(S) -EHC CI+RTWM LABORATORY(S) 5C IoA 45 ,~ e S Lab # _ Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: CR(213 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY /l,r esOr7 PHONE NO. 10 ) '73 " ' S (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Outfall .. Date ......°.::.:.. :. ..... No Sample -.::Total Total .:•..OR -&`Grease ,Total Total Lead:.,:: pH coIlected Flow`(if app } Rainfall ._.. =: - Snspended mold :: ; MG : ::....: .... Units ­: . fb l r,14 laq (I r15 ,VIA 57 AIM (I I (_(� Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil par month? yes X-no (if yes, complete Part B) :Date Sample Total: Flow:..:: Total Rainfall:-; Oil&:Grease :._ -:Corrected `,.- . (if appElcable} inches . �xtxoJdd/v�r'.: ... . otal .pH New Motor Oil urspended Usage :. olids Form SWU-246-117M8 Page I of 2 0 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit-) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable -- see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, time, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C( AZ - D�&— 1:5—1-� (Signature of ermittee) (Date) Form SWU-246-112608 Page 2 of 2 NUMBER24-HOUR SPILL RESPONSE j ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, Ou#fall Rain Volume PH Temp, Time Sampled ° C (Inches) Field Analytical Data - NC DENR Certificate # 5538 US EPA Lair Code #NCO1873 001 1.75 6.66 18.60 12:00 PM DATE: 4/29/13 Client: Southern states Lumberton, NC PIant Analyst: Grad Dobson Rain Gau e 1.75 6.74 18.9° 12:05 PM Rain au a volume when sample was taken OESC I Mr. Thomas Ammons EHC, Inc. Po Box 902 Red Springs, NC 28377 Report Summary Thursday May 02, 2013 Report Number: L633102 Samples Received: 04/30/13 Client Project: 13-MI 0121-3 Description: Southern States 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814269 Est. 197C The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have an questions regarding this data package, please do not hesitate to caly l. Entire Report Reviewed By: Jimm# Hunt , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/810041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 64004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, Tx - T104704245-11-3, CK - 9915, PA - 68-02979, IA Lab #364 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences, Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA FLAP. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Whore applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 4 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 410ESC 1-800-767-5859 Fax (615) 758-5659 1-•A•B B•G•Y•E•N•C,E•S Tax I.D. 62-0814289 Est. 1970 REPORT CF ANALYSIS Mr. Thomas Ammons May 02, 2013 EHC, Inc. PO Box 902 Red Springs, NC 28377 ESC Sample # L633102-01 Date Received April 30, 2013 Description Southern States Site ID LUMBERTON, NC Sample ID OUTFALL 001 Project # 13-MI 0121-3 Collected By Grady Dobson Collection Date 04/29/13 12:00 Parameter Result Det. Limit Units Method Date Dil. pH (On Site) 6.66 su Temperature (on -site) 18.7 Deg C Suspended Solids 57. 2.5 mg/1 2540 D-2011 05/02/13 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 05/02/13 11:00 Printed: 05/02/13 11:19 Page 2 of 4 OESC I £HC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L6331C2 12065 Lebanon Rd. Mt. Juliet, TN 37122 f615) 75B-5858 1-800-767-5859 Fax (615) 758-5659 Tax I.D. 62-0814289 Est. 1970 May 02, 2013 Laboratory Blank Analyte Result Units % Rec Limit Batch Date Anal zed sus ended Solids < 2.5 mg/1 WG659017 05/02/13 09:42 Duplicate Analyte Units Result Duplicate RPD Limit _ Ref Samp _ Batch Suspended Solids mg/1 9.30 8.89 4.86 5 L632960-13 WG659017 Sus ended Solids mg/1 5500 6040 9.72` 5 L633052-01 WGG59017 Laboratory Control Sample Analyte Units Known Val Result % Rec Limit Batch Suspended _ Solids mg/1 773 808. 105. 85-115 WG659017 Laboratory Control Sample Duplicate Analvte Units Result Ref %Rec Limit RFD Limit Batch Suspended Solids mg/1 '780. 808. 101. 85-115 3.53 5 WG659017 Batch number /Run number / Sample number cross reference WG659017: R2648960: 1,633102-01 * * Calculations are performed prior to rounding of reported values. Performance of this Analyte is Outside Of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 3 of 4 OESC f EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615)758-5858 1-Boo-767-5859 Fax (615) 758-5859 Tax I.D. 62-OB14289 Est. 1970 Quality Assurance Report Level II L633102 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix 3 of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a 11J5" or a "J6". The relative percent difference (%RPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 4 of 4 May 02, 2013 4 .STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NC5 Q 05 HL - _ _ sAmnys COLLECTED DURING cmimIDAR YEAR: Cis monitoring report shall be received by the Division no later than 30 days from t the date the facslity receives the sam� plk g results from the laboratory.) FACILITY NAME �u evn n �Oo� ��v¢- 1 uml��rOn �tfliZer PI4nk COUNTY Rp6s%gr� PERSON COLLECTING SA M E( -- E HC �-a bd a PHONE NO. (90'1) CERTIFIED LABORATORY(S) —Lab (SIGN[ATME OF PFRMTrrEE OR DESIGNER) By this signature, I certify that this report is acc arate complete to the best of my knowledge. Part A: Specific MonitorJug Requirements - 1 r �M �1 1 1 1 1 41 � � � • , 1 Z. 1 I 41 :. • .- Does this h6 ity perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes O (if yes, complete Part B) tfavt R- Vphirlp Mi%intpunurp Artivift UnnitnAmp Upwairp-menk Ont[all No. 1}! Date Sample Collected: ,. 50050 00556 ' . 00530 00400 Total Flow .(if.applecable) Total- •- RaInfa>l=• Oil &• Grease . CAP ap i.) ` Non -polar..- ; , ;�&Gl` H•• .`_ etiod• 16d4 Total < ided. Solids PH .. New Motor Oft Usage -. - mo/d MG inches ,, unit ;gykno Form SWU-247-0623I0 Pago 1 of 2 STORM EVENT CE AR A CTERiS UCS: Date _3_ �� - )3 Total Event Precipitation Cmcbes): QQq Event Duration (hours): (only if applicable — see p=mt.) (if more than one storm arcut was sampled) Date Total Event Precipitation Finches): Event Duration (hours): ' (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attu Ctotral Files 1617 Marl Service Center Raleigh, North Carolina 27699-1617 'Z certify, render penalty of law, that this doewment and all atta meats were prepared under my direction or supervision in accordance with a system desigged to assure that qualified personnel properly gafher and evaluate the informatign submitted. Based on my inquiry of tbe'person or persons who manage $re'systcm, or those person `dirne*:YVpo . .. for• t1 .. , , b iinlormatioh tt infox on�sUibriritted 4 �a the best of'my knowledge and belief, trae, necarate, and complete: am awAetat.th�re;a`gniicat penalties ibr sahmitiirip.fals�ortmatiom; iucriading dre 'ty of tines audimprisonment h►r.�mot�g�violat�7ons,!' r, , :,:' th , �w , ; _, ,'�. -:., .• - :=d (Signature of rmittee) (Date) Form, SWU-247 062310 Page 2 of 2 J 4utfa1l Rain PH I Temp, Time Volume ° C Sampled (Inches) Field Analytical Data - NC DENR Certificate # SS38 US EPA Lab Code #NC01873 00I 0.4 6.35 11.7° 10:00am DATE: 3/12/13 Client: Southern states Lumberton. NC Plant I I I I I I Analyst: Gradv Dobson Rain 10.4 16.42 116,7° I10:05am Rain gau.Re volume when sample was taken I I I I I Southern States Cooperative, Inc. 6606 West Broad Street Richmond, Va. 23230-1717 Mall Address: P.O.Box 26234 Rlohmond, Va 23260-6234 Telephone (804)281-1000 F?ECOVED 14AR 13 2013 March 81"2013 OENR-FAYa1EWLLEREGIONAL OFFICE , SOUTHERN STATES North Carolina Department of Environment and Natural Resources Fayetteville Regional Office 225 Green Street Systel Building Suite 714 Fayetteville, North Carolina 28301-5043 RE: DMR for Southern States Lumberton Fertilizer Plant located in Lumberton, NC (Permit #NCS000541) Dear Mr. Lawyer, The Southern States Cooperative, Inc. (SSC) would like to submit the discharge Monitoring Report (DMR) for the second monitoring period for the second year of the permit for the SSC Lumberton Fertilizer Plant. The Lumberton plant is located at 745 Old Whiteville Road in Lumberton, North Carolina and they have an Individual NPDES Storm Water Permit (#NCS000541) that requires the facility to collect semi- annual samples from one designated storm water outfall on the property. SSC hired EHC Environmental from Red Springs, NC to collect the semi-annual samples and to complete the Qualitative Monitoring Report. Copies of the DMR form, analytical data and visual inspection forms are included. This sample also should be considered the first sample of the Tier II monitoring for the elevated Total Suspended Solids (TSS) level that was detected during the last 2 sampling events. The TSS level for the sample that was just collected on February 13th, 2013 was 32 mg/L which is below the benchmark value of 100 mg/L for this location. EHC will continue to collect a monthly sample for TSS until there are 3 consecutive events where the level is below the benchmark value. If you have any questions or comments regarding this facility, feel free to give me a call at (804) 281-1184. Sincerely, Lauren B. Faulkner Environmental Project Manager .STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS ,0 0 D.9 LM I FACILITY NAME So A ern S a� s I km6r6nr an PERSON COLLECTING SAMPLES) - C n c - CERTIFIED LABORATORY(S)ce5 _,Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: a(-')13 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY � h esw PH_ ONE 1v9. 01— (SIGNATURE OF PE l T SEMI .E OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. D: 'Collected 1 •• I I 1 i , . • M. III I I 1 I w 4. �. �r Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per mouth? _ yes _✓no (if yes, complete Part B) Part R: Vehicle Maintennnre Artivity Mnnitnrinv RPnniremantc Oatm No. Date Sample Collected 50050, 00556 00530 00400 Total Flow (iiapplicable),- Total Rainfall:-:' Oil & Grease (if appl.)- _ Non -polar .'0&GTI'PH '' (1Vietliod'1"4- SGT-HEM), it Total =Susj�entled. Solids pH New Motor Oil Usage - moldffil MG inches UWA unit : ' - omo C) rrl --C m i m m � N o C.rrt rn� w 0 c7 M Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date -13 -13 Total Event Precipitation (inches): 0 - 75� Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): ' (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system desigi}ed to assure that qualified personnel properly gathdr and evaluate the informatipn submitted. Based on my inquiry of the person or persons who manage the'system, or those persons'd*06ffyr;i�poxis;ble for. Met4ng`tlie tfc rmatiun,�thg info on-stibmrtted h$ to the best of my knowledge and belief, true, accurate, and complete. J am -awes'] 4ai.th�re.' $igniilea it penaifies.f+or sating [ais� information, inch the possib' . of fines and imprisonmenf6r knowiiig•viol4tjoi sV' r' • , : L; '` ;' _ ^: , (Signature of P rmittee) (Date) Form SWU-247-062310 Page 2 of 2 Permit Number NC S 000-527 1 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from I I II the date the facility receives the sampling results from the laboratory.) FACILITY NAME �OUA l S_Aks Z Lel-kl , -�, IiZL! 0 � COUNTY ISO e5 n PERSON COLLECTING SAMPLE(S) _ C r�p_n- Z�JJG, T,c . PHONE NO. (rl I Q) ' 13 - l 5 (,, 7- CERTIFIL'D LABORATORY(S) S� e nce 5. _Lab Lab # (SIGNATURE OF PERNIITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge - Part A: Specific Monitoring Requirements mmim : . Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _n� (if yes, complete Part B) Part B: Vehicle Maintenance Activity Mnnitnrima RennirpmPntc Outfall No. Date- Sample Collected 50050 00556 00530 00400 Total Flow {if,applicable) Total" Rainfall:- Oil &" Grease (iiappl.)": `<< Non -polar ;O&G/TPg ; - (Method I664" SGT HEM), if a l.` Total =Suspeiitled. Solids pH New Motor " Oil Usage moldq/T MG inches mo unit o Form SWU-247-062310 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 2-13-15 Total Event Precipitation (incites): 0,75 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours):: (only if applicable — see permit.) Mail original and one copy to: Division of Water Quality Attu: Central Files 1617 Mail Service Center Raleigh, Noith Carolina 27699-1617 "I certify, under penalty of law,.that this document and all attachments .were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the informatign submitted. Based on my inquiry of the person or persons who manage the -system, or those persons'diVctl`y;kespo s ble for ttte ng.thb d6ri anatioh; tlf� infor on, stibrititted is; to the hest of my knowledge and belief, true, accurate, and complete. j am aw .there are gig cant penalties.ior submifting•#'alse, information, including the possibility of fines and imprisonmerif for knowing'viol4 onsr" r= . (Signature of ermittee) (Date) Form SWU-247-062310 Page 2 of 2 1 OESC I 12065 Lebanon Rd, Mt. Juliet, TN 37122 (6151 756-5058 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Mr. Thomas Arranons EHC, Inc. PO Box 902 Red Springs, EC 28377 . .- Report Summary Thursday February 21, 2013 Report Number: L620194 Samples Redeiv6d: 02/14/13 Client Project: 13-MI0121-3 Description: Southern States Coo The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to -call. Entire Report Reviewed By: I Jim4 Hunt , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375iDW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: D60302, 060303, and 060304. Page 1 of 6 H OESC I REPORT OF ANALYSIS Mr. Thomas Ammons EHC, Inc. PO Sox 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. 7uliet, TN 31122 015) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0914289 Est, 1970 February 21,2013 ESC Sample # : L620194-01 Date Received February 14, 2013 Description Southern States Coop Site ID LUMBERTON, NC Sample ID 001 Project # 13-M10121-3 Collected By Grady Dobson Collection Date 02/13/13 00:00 Parameter Result Det. Limit Units Method Date Dil. Nitrate 13000 2000 ug/1 9056 02/14/13 20 Nitrite BDL 100 ug/1 9056 02/14/13 1 Sulfate 26000 5000 ug/1 9056 02/14/13 1 BOO BDL 2000 ug/l 5210 B-201 02/19/13 1 COD BDL 10000 ug/l 410.4 02/15/13 1 Total Nitrogen 16000 100 ug/1 Calc. 02/21/13 1 Ammonia Nitrogen 300 100 ug/1 350.1 02/20/13 1 Phosphorus,Total 680 100 ug/1 365.4 02/18/13 1 Kjeldahl Nitrogen, TKN 2800 100 ug/1 351.2 02/16/13 1 Suspended Solids 32000 1000 ug/1 2540 D-201 02/19/13 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 02/21/13 17:43 Printed: 02/21/13 17:43 Page 2 of 6 12065 Lebanon Rd. Mt. Juliet, TN 37122 OESC (615) 758-585e 1-800-767-5859 Fax (615) 758-5859 L-A,B 5•C•1•E.N•C,E•9 Tax I.D. 62-08142e9 Est. 1970 EHC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red springs, NC 28377 February 21, 2013 L620194 Laboratory Blank Analyte Result Units Rec Limit Batch Date Analyzed Nitrate < .1 mg/1 WG636876 02/14/13 07:45 Nitrite < .1 mg/1 WG636876 02/14/13 07:45 Sulfate < 5 mg/1 WG636076 02/14/13 07:45 COD < 10 mg/l WG636944 02/15/13 13:13 Kjeldahl Nitrogen, TKN < .1 mg/l WG636861 02/15/13 16:13 Phosphorus,Total < .1 mg/1 WG637208 02/18/13 14:01 Suspended Solids < 1 mg/l WG637119 02/19/13 09:50 Bon -0.0500 mg/1 WG636842 02/19/13 10:46 Ammonia Nitrogen < .1 mg/1 WG636953 02/20/13 10:47 Duplicate Analyte Units Result Duplicate RPD Limit Ref S�u Batch Nitrate mg/1 0.200 0.200 0 20 L620170-02 WG636876 Nitrate mg/1 0.940 0.810 14.9 20 L620170-03 WG636876 COD mg/1 10.0 11.0 4.65 5 L620093-01 WG636944 COD mg/l 28.0 25.0 11.3* 5 L620227-Cl WG636944 Kjeldahl Nitrogen, TKN mg/1 0.270 0.200 29.1- 20 L618646-02 WG636881 Kjeldahl Nitrogen, TKN mg/1 0.220 0.160 30.2• 20 L618646-01 WG636881 Phosphorus,Total mg/l 2.70 2.70 0 20 L620247-01 WG637209 Phosphorus,Total mg/1 0.670 0.684 1.48 20 L620194-01 WG637205 Suspended Solids mg/l 2400 2370 0.423 5 L620182-03 wG637119 Suspended Solids mg/l 190. 203. 5.80* 5 L620265-01 WG637119 BCD mg/l D D 0 5 L620145-01 WG636B42 Ammonia Nitrogen mg/1 38.0 38.0 0 20 L620282-02 WG636953 Ammonia Nitrogen mg/1 0.510 0.550 7.55 20 L620176-01 WG636953 Laboratory Control Sample Analyte Units Known Val Result 4 Rec Limit Batch Nitrate mg/l 8 7.90 96.8 90-110 WG636876 Nitrite mg/l 8 7.80 97.5 90-110 WG636876 Sulfate mg/l 40 37.2 93.0 90-110 WG636876 • Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 3 of 6 Summary of Remarks For Samples Printed 02/21/13 at 17:43:52 TSR Signing Reports: 350 R5 - Desired TAT Report GW in ppb Sample: L620194-01 Account: ENVHYD Received: 02/14/13 09:00 Due Date: 02/21/13 00:00 RPT Date: 02/21/13 17:43 12065 Lebanon Rd. Mt. Juliet, IN 37122 *ESC (615) 75B-5858 1-800-767-5859 Fax (615) 758-5859 L•A•6 9-C-I-6-IV•C•M-8 Tax T.D. 62-0819289 r a Est. 1970 EHC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 February 21, 2013 L620194 Laboratory Control Sample Analyte Units Known Val Result Roo Limit Batch COD mg/1 183 184, 101. 90-110 WG636944 Kjeldahl Nitrogen, TKN mg/1 8.55 9.04 106. 90-110 WG636881 Phosphorus,Total mg/l 1 1.01 101. 90-110 WG637208 Suspended Solids mg/l 773 816. 106. 85-115 WG637119 BOD mg/l 198 193. 97.5 84.6-115.4 WG636842 SOD mg/l 198 189, 95.5 84.6-115.4 WG636842 SOD mg/l 199 188. 94.9 84.6-115.4 WG636842 BOD mg/l 198 178. 89.9 84.6-115.4 WG636842 SOD mg/l 198 182. 91.9 84.6-115.4 WG636842 SOD mg/1 196 182. 91.9 84.6-115.4 WG636842 SOD mg/1 198 181. 91.4 B4.6-115.4 WG636842 SOD mg/1 196 175. 98.4 84.6-115.4 WG636842 Ammonia Nitrogen mg/1 7.5 8.12 108. 90-110 WG636953 Laboratory Control Sample Duplicate Analyte Units Result Ref %Rec Limit RPD Limit Batch Nitrate mg/1 7.90 7.90 99.0 90-110 0 20 WG636876 Nitrite mg/1 7.81 7.80 9B.0 90-110 0.128 20 WG636876 Sulfate mg/l 37.3 37.2 93.0 90-110 0.268 20 WG636876 COD mg/1 191. 184. 104. 90-110 3.73 5 WG636944 Kjeldahl Nitrogen, TKN mg/l 9.11 9.04 106. 90-110 0.771 20 WG636881 Phosphorus,Total mg/l 1.09 1.01 109. 90-110 7.62 20 WG637208 Suspended Solids mg/l 644. 816, 109. 85-115 3.37 5 WG637119 Ammonia Nitrogen mg/l 8.19 8.12 109. 90-110 0.858 20 WG636953 Matrix Spike Anal to Units MS Res Ref Res TV t Rec Limit Ref Samp Sat Nitrate mg/l 4.77 0 5 95.4 80-120 L620190-12 WG636876 Sulfate mg/1 47.6 0 50 95.2 80-120 L620190-12 WG636876 COD mg/1 415. 0 400 104. 90-110 L620083-02 WG636944 Kjeldahl Nitrogen, TKN mg/l 6.95 1.10 5 117.- 90-110 L620170-01 WG636881 " Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 4 of 6 OESCL•A•B a•c•i•e•1�t•c•E•9 EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L620194 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-900-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 February 21, 2G13 Matrix Spike Analyte Units MS Res Ref Res TV 4 Rec Limit Ref Samp Batch Phoaphorus,Total mg/1 3.95 1.50 2.5 98.0 90-110 L620162-02 WG63720B Ammonia Nitrogen mg/l 7.78 1.90 5 118.* 90-110 L620176-02 WG636953 Matrix Spike Duplicate Analyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch Nitrate mg/1 4.92 4.77 98.4 80-120 3.10 20 L620190-12 WG636876 Sulfate mg/l 49.1 47.6 98.2 80-120 3.10 20 L620190-12 WG636876 COD mg/l 410. 415. 102. 90-110 1.21 5 L620083-02 WG636944 Kjeldahl Nitrogen, TKN mg/l 6.79 6.95 114.* 90-110 2.33 20 L620170-01 WG636BOI Phosphorus,Total mg/1 3.97 3.95 98.8 90-110 0.505 20 L620182-D2 WG637208 Ammonia Nitrogen mg/1 7.62 7.7B 114.* 90-110 2.08 20 L620176-02 WG636953 Batch number /Run number / Sample number cross reference WG636676: R2543742: L620194-01 !, WG636944: R2544518: L620194-01 i WG636681: R2545217: L620194-01 WG637208: R2547299: L620194-01 WG637119: R2547737: L620194-01 WG636842: R2548339: L620194-01 WG636953: R2550099: L620194-01 WG638016: R2552597: L620194-01 • ' Calculations are performed prior to rounding of reported values. * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 5 of 6 *ESC i EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 12065 Lebanon Ad. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Quality Assurance Report Level II February 21, 2013 L620194 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix B of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a 11J5" or a "J6". The relative percent difference (6RPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 6 of 6 1 DENR_^F . STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) FEB 21 2�113 Calendar Year 2012 DYYO Individual NPDES Permit No. NCS❑c7 Q©❑S ©0 or Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1' of the following year. Facility Name: _Southern States Cooperative Lumberton Fertilizer Plant County: Robeson Phone Number: (91 Total no. of SDOs monitored 1 Outfall No. 001 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Parameter -(units) ' Total` r.x � , _ � ��COD= ' K;`jj = �` � � f ` Rainfall, -BOW, M ^Total=Ammonia- Total TKN Nitrate Nitrite Nitrite T,o# a inches : mglL y`, mglL mgllf=_ s Nitrogen mg1L rngL mg1L Phosphonus � �... .... ,. m IL 9endhmark N/A- - . 30- 1W 7.2 ` = 30 20 ;10 10 --2 = *Date:Sample Collected,. mmlddlyy,- 1.5 2.2 19 0.22 3.2 0.87 2.3 <0.1 1.1 0410612012 Additional Outfall Attachment SW U-264-Generic-2 5 M ay2010 Outfall No. 001L continued Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ® Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Parameter, (units) .Total Total -, Rainfall, Suspended Sulfate pH pH = .inches - Solids mgll storm water rain gauge m 1L a.. Benchmark N/A 100 500 6-9 6-9 Date Sample Collected, mmlddlyy 04/06/2012 1.5 12 119 6.13 15.79101 SWU-264-Ge neric-2 5 May2 010 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including thy-ppssibility of fines and imprisonment for knowing violations." Signature Date T S i�_ DWQ Regional Office Contact Information: Mail Annual DMR Summary Reports to: 'ASHEVILLE:REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESVILL&REGIONAL:OFFICE 2090 US Highway 70 E 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 910 433-3300 RALEIGH REGIONAL OFFICE WASHINGTON€REGIONAL'OFFICE WILMIN(TON REGIONAL OFFICE 127 Cardinal Drive Extension 3800 Barrett Drive 943 Washington Square Mall Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4204 (252) 946-6481 (910) 796-7215 WINSTON=SALEM REG[ONAL�OFFICI+ CENTRAL OFFICE ;. 585 Waughtown Street Winston-Salem, NC 27107 1617 Mail Service Center Raleigh, NC 27699-1617 'To preserver prated and enhance (336) 771-5000 j 919 807-6300 North Carolina water..." SWU-264-Genedit-25May2010 AY!i;-'O�t NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Governor Director June 18, 2012 Mr. Mark Gillis Southern States Lumberton Fertilizer Plant PO Box 1485 Lumberton, NC 28359 Subject: COMPLIANCE EVALUATION INSPECTION Southern States Cooperative Inc. Lumberton Fertilizer Plant NPDES Stormwater Permit-NCS000541 Robeson County Dear Mr. Gillis: Dee Freeman Secretary On May 31, 2012, I, Hughie White, from the Fayetteville Regional Office of the Division of Water Quality, conducted a site inspection for the Southern States Fertilizer Plant facility located at 745 Old Whiteville Road in Lumberton, Robeson County, North Carolina. I would like to thank you for your assistance during this insepction. A copy of the inspection report is attached for your review. Stormwater from the facility drains to Lee Pond, a Class C: Sw water located in the Lumber River Basin. The site visit and file review revealed that the subject facility is covered by NPDES Stormwater General Permit-NCS000541. Accordingly, the following observations were note&during the Division of Water Quality inspection (please see the attached addendum for information about your permit): 1) Stormwater Pollution Prevention Plan (SPPP) A Stormwater Pollution Prevention Plan (SPPP) has been developed, recorded, and properly implemented. es■ No❑ 2) Qualitative, Monitoring Qualitative monitoring has been conducted and recorded in accordance with permit requirements. es■ No❑ Location: 225 Green Street, Suite 714, Fayetteville, North Carolina 28301 Phone: 910-433.33001 FAX: 910.486-07071 Customer Service: 1-877.623-6748 Internet: www rimatergualitv.ofa An Equal OpponuMy 1 Affirmative Aclion Employer one NorthCarolina )Vaturally 3) Analytical Monitoring Analytical monitoring has been conducted and recorded in accordance with permit requirements. es ■ N Please be advised that violations of the NPDES Individual Permit are subject to a civil penalty assessment of up to $25,000 per day for each violation. If you or your staff has any questions, comments, or needs assistance with understanding any aspect of your permit, please do not hesitate to contact me at (910) 433-3308. Sincerely, `Y1 /, &' r Hughie White Environmental Specialist Enclosure cc: FRO -Surface Water Protection WBS Compliance and Permits Unit ij Permit: NCS000541 SOC: County: Robeson Region: Fayetteville Compliance Inspection Report Effective: 05/01/11 Expiration: 04/30/16 Owner: Southern States Cooperative Inc Effective: Expiration: Facility: Southern States Cooperative - Lumberton Fertilizer Plant 745 Old Whiteville Rd Contact Person: Danny Dillion Title: Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related • Permits: Inspection Date: 05/3112012 EntryTime: 10:00 AM Primary Inspector: Hughie White Secondary Inspector(s): �1I�cI Mike Lawye Reason for Inspection: Routine Permit Inspection Type: Stormwater Discharge, Individual Facility Status: ■ Compliant ❑ Not Compliant Question Areas: Storm Water (See attachment summary) Lumberton NC 28358 Phone: Certification: Exit Time: 11:30 AM Phone: Phone: 910-433-3300 Ex 3a Phone: 910-433-3300 Ext,Z29' Inspection Type: Compliance Evaluation 3309 Page: 1 JN Permit: NCS000541 Owner - Facility: Southern States Cooperative Inc Inspection Date: 05/31/2012 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: The stormwater pollution prevention plan has been developed and implemented. The plan appeared to be complete and contain all the necessary components. The plan is also being updated annually. Qualitative monitoring and analytical monitoring is being performed, as required. This facility does not meet the requirement to perform analytical monitoring from vehicle maintenance areas. The previous sampling results revealed a benchmark exceedance for Total Suspended Solids. As a reminder, a benchmark exceedance of a parameter requires the facility to implement the Tier One requirements for monitoring and evaluation of the facility BMP's, housekeeping, etc. Also, benchmark exceedances of the same parameter for two consecutive sampling periods will result in the facility being required to implement the Tier Two sampling, monitoring, and evaluation requirements outlined within the stormwater permit. All possible sources of suspended solids need to be evaluated and preventive actions need to be put in place to eliminate the discharge of high levels of solids. The outfall was observed during this inspection. Page: 2 Permit: NCS000541 Owner - Facility: Southern States Cooperative Inc Inspection Date: 05/31/2012 Inspection Type: Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? ■ ❑ ❑ n # Does the Plan include a General Location (USGS) map? ■ ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices"? ■ ❑ ❑ ❑ # Does the Plan include a detailed site. map including outfall locations and drainage areas? ■ ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? ❑ Cl ■ ❑ # Has the facility evaluated feasible alternatives to current practices? ■ ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? ■ ❑ ❑ ❑ # Does the Plan include a BMP summary? ■ ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ■ ❑ ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ■ ❑ ❑ ❑ # Does the facility provide and document Employee Training? ■ ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? ■ ❑ ❑ ❑ # Is the Plan reviewed and updated annually? ■ ❑ ❑ Cl # Does the Plan include a Stormwater Facility Inspection Program? ■ n ❑ n Has the Stormwater Pollution Prevention Plan been implemented? ■ n n n Comment: Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ■ ❑ ❑ ❑ Comment: Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ■ ❑ ❑ ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ■ ❑ Comment: This facility does not meet the requirements for monitoring from vehicle maintenance areas. Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ■ ❑ ❑ ❑ # Were all outfalls observed during the inspection? ■ ❑ n ❑ # If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ ■ ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ■ Cl ❑ ❑ Comment: Page: 3 I- (S) F_ m Lo 01) Ic CP Tr v CD tv m CV) L0 CD Individual NPDES Permit No. Certificate of Coverage (COG) No. DENR-FRO STORMWATER DISCHARGE OUTFALL (SDO) � �i ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year zo Il Dwo or This monitoring report summary of the calendar year is due to the DWO Regional Office no later than March is' of the following year. Facility Name: s �C_ -L+A,o,�er�:<<zer County. - Phone Number: i 9zo ?39 - 7SG Z Total no. of SDOs monitored Outtall No. Do 1 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No D' Was this outfali ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No [�!' if this outtall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease hequency ❑ Received approval from DWO to reduce monitoring frequency ❑ Other ❑ Was this SOO monitored because of vehicle maintenance activities? Yes ❑ No [ Pr®nee=unlis) ti_s i - V. -." fj i1 ors .�l� �.. ._�"�_ t' - = I 6.1 !Q•d 33 ,2 p 3 SW U-264-Generic�-25M ay�2010 0 E- r__ CD E_ CD 00 m m 0 a w Additional Outfall Attachment OutfalI No. 0 U Is this outfali currently in Tier 2 (monitored monthly)? Yes ❑ No B--- Was this outtall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No [q--' If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWO to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No [J -r ?"•.:+� - `-rye, � aci���&R. :�"''rt - a, i -.+C �i .�l �r'!s%-- �. _ 7- �cR _ _. AR Wi �,. Gam. L..t. 11 x `..,,, •t. .,- UD m M m O CD 0. 0 w SW Ll-264-Generic-25May201 a