NCS000161_MONITORING INFO_20161116

STORIVIWATER DIVISION CODING SHEET
PERMIT NO.
MCC, pv-o
DOC TYPE
❑FINAL PERMIT
711% MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 70((o
YYYYMMDD

STORMWATER DISCHARGE OUT1rALL (SDO)
MONITORING REPORT
Permit Number NCS OOO f 4 /
FACILITY NAME
PERSON COLLECTING SAMPLE(S) c 1
CERTIFIED LABORATORY(S) s„�41r Lab # 3 z-Y
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: -� J / 6
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY At e e 1F /,- 61. r
PHONE NO. 7041 3 5/
SIGNATURE OF PERMITTEE Okt DESIGNEE
REOUIItED ON PAGE 2.
1 ,
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Dims this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _-no
(if (if yes, complete Fart B)
Part B: Vehicle Maintenance Activity Monitorin¢ Rea nirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Greasc
(if appl.)
Non -polar
O&G/ TPH
(Method 1664
SGT-HEMS if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mvp/ddlyr
MG
inches
unit
galtwo
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Bate A9 --7 —/ L-
Total Event Precipitation (inches); G• (o G
Event Duration (boars): (only if applicable — see pennI)
(if more than one storm event was sampled)
Date _
Total Event Precipitation (inches);
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality .
Atta: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. i am aware that there are significant penalties for submitting false information,
including the possibility of fknes and imprisonment for knowing violations."
7 luav_f&
(Signature of Permittee) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)1 SPPP Annual Update DATA REVIEW FORM
Calendar Year `Z m t i-
Individual NPDES Permit No. NcskldUL]UO or S',« •'� l,[�/ 9 c_� �.. � h L
Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑ I'
This monitoring report summary of the calendar year should be kepi on file on-shte with the fadifty SPPP. R E CO V D
Facility Name: �L,. �...L!�•��•k �•;�tnj L c. NOV 16 2016
County: M.e c. A /tee ors CENTRAL FILES
Phone Number: 70 `( Py4,fe Total no. of SDOs monitored IF DWR SECTtr)nr
Outfall No. a a'/ 47
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No a'
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No 9--�
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No
SWU-264 - Generic Annual DMR
Last revised 511712013

" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fyies and imprisonment for knowing violations."
Signature
Date i A-V V 6
For questions, contact your local Regional Office:
DWQ Realonal Office Contact Information:
2090 US Highway 70
Swannanoa, NC 28778
[phone]
3800 Barrett Drive
Raleigh, NC 27609
[phone]
585 Waughtown Street
Winston-Salem, NC 27107
[phone]
225 Green Street
Systel Building Suite 714
Fayetteville, NC 28301-5043
[phone]
943 Washington Square Mail
Washington, NC 27889
[phone]
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
610 Fast Center Avenue/Suite 301
Mooresville, NC 28115
[phone]
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
[phone]
T�,� , .. ,I , Ir-T f
SWU-264 - Generic Annual DNIR
Last revised SIM013

A-iA
Am"
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit.-
--Permit No.: K1C1E1_U1 o/0,/il11/ or Certificate of Coverage No.:
Facility Name: _ C [--C i.'n� C,C .- ,, (_U- C,
County: ✓► �_� pia►� h� Phone No. 070'() 39 — 6 Yq,$1
Inspector: I($.A `gym
Date of Inspection:
Time of Inspection: l q'3-r,
Total Event Precipitation (inches): �� • 6
Was this a "Representative Storm Event" or;.�l�C1 V Cr) Event" as defined by the permit?
(See information below.) C �/
Yes ❑ No NOV 16 2016
CENTRAL FILES
Please veMfy whether Qualitative Monitoring mRtR p'_-*A9U during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be w
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable. .
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the i
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee I
obLains approval from the local DWQ Regional Office. F
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Per`mittee or Designee)
Page 1 of 2
5WU-242, Last modified 7/31/2013

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
- - Emerald Carolina Chemical
8309 Wilkinson Blvd.
Charlotte, NC 28214
Attention: Charlie StromRECEIUED
NOY 16 2016
CENTRAL FILES
Project Name: Stormwater 20160WR SECTION
Lot Number:RJ08099
Date Completed: 1012012016
Kelly M. Nance
Project Manager
LABORATORY
Ali ACCREDITATION
BUREAU .. �,; ACCREDiE61e"n
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: i of 11
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC. No: E87653 NC. DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Emerald Carolina Chemical
Lot Number: RJ08099
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 11
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Emerald Carolina Chemical
Lot Number:'RJ08099
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
001
Aqueous
10/07/20161443
10108/2016
002
002
Aqueous
10107/20161450
10108/2016
003
003
Aqueous
10107120161454
10/08/2016
004
004
Aqueous
10/07/20161500
10/08/2016
005
005
Aqueous
10/07/20161506
10/08/2016
006
006
Aqueous
10107/20161512
10/08/2016
007
007
Aqueous
10/07/20161518
10108/2016
008
008
Aqueous
10107/20161435
10108/2016
(8 samples)
Shealy Environmental Services, Inc. Page: 3 of 11
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID:RJOB099-001
Description: 001 Matrix: Aqueous
Date Sampled:10107/20161443
Date Received:10/08/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH - Field) SM 4500-H B-2011 1 10/07/2016 1443 "
1 (COD) SM 5220D-2011 1 10/18/2016 1531 CLM 10/18/2016 0933
1 (TSS) SM 2540D-2011 1 10/12/2016 1738 DMA 24272
1 (SGT - HEM (n) 1664B 1 10/19/2016 0000 ARP 24689
CAS Analytical
Parameter
Number Method
Result Q
POL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
ND
10
mg1L
1
TSS
SM 254OD-20
2.0
1.0
mg1L
1
SGT - HEM (non -polar material)
1664B
ND
4.5
mg/L
1
Footnote(s): "Tim McCorkle/ARM
POL = Practical quantitation limit S = Oetecled in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result c PQL and? MDL P • The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all sail sample analysis are reported on a dry weight basis unless Flagged with a "W"
Shealy Environmental Services, Inc. Page: 4 of 11
.106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Clienl:Emerald Carolina Chemical Laboratory ID: RJO8099-002
Description: 002 Matrix: Aqueous
Dale Sampled:10107120161450
Date Received: 1010812016
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
10/07/2016 1450
1
(COD) SM 5220D-2011
1
10/18/2016 1531 CLM 10/18/2016 0933
1
(TSS) SM 2540D-2011
1
10/12/2016 1738 DMA 24272
1
(SGT - HEM (n) 1664B
1
10/19/2016 0000 ARP 24689
CAS Analytical
Parameter
Number Method
Result Q
PQL
U nits
Run
pH - Field
SM 4500-H B
_
6.5
_ -
su
1
COD
SM 5220D-20
27
10
mg/L
1
TSS
SM 2540D-20
9.2
1.5
mg/L
1
SGT - HEM (non -polar material)
1664B
ND
4.5
mg1L
1
Footnote(s): "Tim McCorkle/ARM
PQL - Practical quant{tation limit B = Detected in the method blank f - OuanGlation of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the POL J - Estimated result � PQL and � MEX P - The RPD between two GO columns exceeds 40% N = Recovery is out of c6terla
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
Shealy Environmental Services, Inc. Page: 5 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory iD; RJ08099-003
Description: 003 " Matrix: Aqueous
Date Sampled1010712016 1454
Date Received:10/08/2016
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 10/07/2016 1454
1
(COD) SM 5220D-2011
1 10/18/2016 1531 CLM
10/18/2016 0933
1
(TSS) SM 2540D-2011
1 10/12/2016 1738 DMA
24272
f
(SGT - HEM (n) 1664B
1 10/19/2016 0000 ARP
24689
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5 �.
su
1T
COD
SM 5220D-20
15
10
mg1L
1
TSS
SM 254OD-20
8.0
1.0
mg1L
1
SGT - HEM (non -polar
material)
1664E
ND
4.5
mglL
1
Footnote(s); "Tim McCorkle ARM
POL = Practical quantltation limit B = Detected it the method blank E = Quanlltation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < PO4 and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless (lagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID:RJ08099.004
Description: 004 Matrix: Aqueous
Date Sampled: 10107120161500
Date Received;1010812016
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 10/07/2016 1500 •'
1
(COD) SM 5220D-2011
1 10/18/2016 1531 CLM
10/18/2016 0933
1
{TSS) SM 2540D-2011
1 10/12/2016 1738 DMA
24272
1
(SGT - HEM (n) 1664B
1 10/19/2016 0000 ARP
24689
CAS Analytical
_Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
22
10
mg1L
1
TSS
SM 254OD-20
15
1.4
mg1L
i
SGT - HEM (non -polar
material)
1664B
ND
4.8
mg1L
1
Fooinote(s): **Tim McCorkle/ARM
POL = Practical quantltation limit S = Detected in the method blank E = Ouantitatlon of compound exceeded the calibration range H - Out of holding time
ND - Not detected at or above the POL J = Estimated result < POL and? INDL P = The RPD between two GO columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry waight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory 1D: RJO8099.005
Description: 005 Matrix: Aqueous
Date Sampled:1010712016 1506
Date Received:1010812016
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1
10/07/2016 1506
1
(COD) SM 5220D-2011
1
10/18/2016 1531 CLM
10/1812016 0933
1
(TSS) SM 254OD-2011
1
10/12/2016 1738 DMA
24272
1
(SGT - HEM (n) 16648
1
10/19/2016 0000 ARP
24689
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
20
10
mg1L
1
TSS
SM 254OD-20
7.8
1.0
mg1L
1
SGT - HEM (non -polar
material)
1664B
ND
4.5.
mg1L
1
Footnote(s): "Tim Mc orkle ARM
POL = Practical quanbtation limit 0 = Detected in the method blank E = 4uanlitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < POL and? MDL P = The RPO between two GC columns exceeds 40% N = Recovery fs cut of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID:R,i08099-006
Description: 006 Matrix: Aqueous
Date Sar led:l0/0712016 1512
Date Received:1010812016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH - Field) SM 4500-H B-2011 1 10/07/2016 1512 "
1 (COD) SM 5220D-2011 1 10/18/2016 1531 CLM 10/1812016 0933
1 (TSS) SM 254OD-2011 1 10/12/2016 1738 DMA 24272
1 (SGT - HEM (n) 1664B 1 10/19/2016 0000 ARP 24689
CAS Analytical
Parameter _ _
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
all
1
COD
5M 5220D-20
19
10
fill
1
TSS
SM 254OD-20
16
1.0
ri lL
1
SGT - HEM (non -polar material)
16648
ND
4.7
mg1L
1
Footnotill "Tim McCorkle ARM
POL - Practical auantitation limit B - Detected in the method blank E - Ouentitatlon of compound exceeded the calibration range H = Out of holding time
NO • Not detected at or above the POL J = Estimated result < PQL and? l P = The RPD between two GC columns exceeds 40% N = Recovery is out of c4tena
Where applicable• all soil sample analysis are reported an a dry weight basis unless flagged with a -W"
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Inorganic non-metals
Client: Emerald Carolina Chemical - Laboratory ID: RJO8099-007
Description: 007 Matrix: Aqueous
Hate Sampled:10107120161518
Date Received:1010812016
Run Prep Method
_ Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
10/07/2016 1518
1
(COD) SM 5220D-2011
1
10/18/2016 1531 CLM 10/18/2016 0933
1
(TSS) SM 2544D-2011
1
10/12/2016 1738 DMA 24272
1
(SGT - HEM (n) 1664B
1
10/19/2016 0000 ARP 24689
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
32
10
mg1L
1
TSS
SM 254OD-20
8.6
1.0
mg1L
1
SGT - HEM (non -polar material)
16643
ND
4.5
mg/L
1
Footnote(s): "Tim MCCOrklei
PQL = Practical quantitation limit 8 = Detected In the method blank E - Ouantitallon of compound exceeded the calibration range H - Out of holding time
NO = Not detected at or above the POL J = Estimated result c PO4 and > i P - The RPD between two GC columns exceeds 40% N - Recovery is out of cnteria
Where applicable, all sail sample analysis are reported on a dry weight basis unless Flagged with a "W"
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Inorganic non-metals
Client: Emerald Carolina Chemical laboratory ID:RJ08099-008
Description: 008 Matrix: Aqueous
Date Sampled:10107/20161435
Date Received: 1010812016
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
10/07/2016 1435
1
(COD) SM 5220D-2011
1
10/18/2016 1531 CLM 10/18/2016 0933
1
(TSS) SM 2540D-2011
1
1011312016 1231 KWP 24339
1
(SGT - HEM (n) 1664B
1
10/19/2018 0000 ARP 24689
CAS Analytical
Parameter
Number Method
Result Q
PAL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
28
10
mg/L
1
TSS
SM 254OD-20
4.7
1.4
mg/L
1
SGT - HEM (non -polar material)
1664B
ND
4.7
mg/L
1
Footnote(s): ""Tim Mc oNe/ARM
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitabon of ecmpound exceeded the calibration range H = Out of holding time
ND - Not detected at or above the POL J = Estimated result < POL and i MDL P 2 The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where appllcable, all soil sample analysis are reported on a dry weight basis unless Nagged with a'W-
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Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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SHEALY ENVIRONMENTAL SERVICES INC.
5nroh, Emuuonmeer-,l Se * Icn, Inc E ae I aF I
Do.;nr,2nl Nurmh2r N(Pii"Al SC-Y E!IucUve rota _.I;R0016
�1 S4mp1z Rcceipt Chccklisl (SRC) �l
Client: �J� l L t: ,7�. <".� _ Cooler inspected byldnte: 6 4 +% 6 Lot fir:
Mewls of receipt: a-Sn, [ 3 Client n UPS ❑ FtdEx c Other I
Yes a
I I
1 1. Were custody seals present on the oonler? f
Yes (7
I NO u NA ❑
2. If custody Seals were Eresent, were they intact and unbroken?
pH strip ID: lb J �� ] � , _ C 1 strip Ifs:
Gooier 113106gIna]�tc rature upon receipt,'1}erivcd (corroctadl temperature upon receipt:
_ 11'+„ ' );C pe1 I . 04' i I 'C i J GC
Method: ❑ Turriperature Blank gainst Bottles IR Gun JD; _ IR Gun Correction Factor: _ _ { -C
Method of coolali(: ru cc ❑ Blue Ice r.. Dty Ice ❑ Notre
Yes 0
No n
NA ey—
3• if tempaniturc of any cooler exceeded 6.0^C, was Project ManatrrNulifred?
PM was Notified hy: phone , email I face -to -foci: (circle one). -
las ❑
No c
777e
4. Is the commercial courier's packiq& slip ullacluai to lhis form?
Yes
No ❑
{. WEreRropet cuslady prmMures relin isherl/received) followed?
yesy
No a
6. Wvrr. sample 10s listed on the COC?
Yeses
No c
7. tit -rc sample 1Ds listed on all same containers?
Yes
;Vo r
N. WAS [OIIOCtiall date & tilUe IiSted on the C"CiCY
Ye -a d
No ❑ . �
9. Wes collection date & time listed on all sample tnnleineris
Yes 01"
Nn n
10_ Did all container label information (ID, date, time) agree with tha COC?
1rs
No o
11. Were texts to be partbrwed li3tr d va the COC? �
Yes 7
No 0
12. rid all samples arrive in the pruper conlainw^s for each test and! or in good condiliori
unbroken lids nn, etc, ? i
Ye
`No ❑
II Was ade ante sanlpie valuate avvilablc?
Yes c►
No ❑
Id. Werc all samples received within VS the holding. time or ilS hours. whichever comes
first?
Ycs ❑
Nc.er�""-
W. _
15. Were any satrrp)r.13 cunttriners missinglexcaa5 (circle one samples Not listed rot C(l{
7
Yes 0
Nu n
v
16. Were hubbles present >` ea-siz&' /V'or 6min in diameter • in an VOA vials?
Yr
o ❑
11A n
17. Weit all DRCihrleirrlslnutrient iron ir_s received at a PH of -f 2?
Ycs 0
No ❑
N
18. were all c -anide an(Ifur sulfide samples received at a pH >12r!
_
VCR -1
No c
19, Were all applicable 1VI-t3Pl'KN1ganidepbenol:13N?t (•-0.2mg!L) samples free of its -dual
chlorine?
Yes n
Vn a
NAA2f"
20, Ware collection temperatures documented on the COC for NC samples'!
Yes n
No n
NA o,""
21. Were clienl mrDar"Imgtrests (l.e. requeswd dilutions, aN S M311 designations, etc...
correctly uwanscribed from die COC irlo the coinniew suction in LIMS7
Ycs Cl
Na in 1
Mis the quote number usod taken from the container label?
Seul tic PrCSL'rl'ati13n (Must be cam pleted for n sam le(s) ilien rrect} prascrved or with headspace)
SHmplc(s)
sans le recr~iving with
wire rccciyrd incorrectly prest:rvv4 and were adjwsted arcord
(HaSO4. HNO3, HCI, Na011) using SR Jff
ngly in
'iars7 ids)
were received with bubbles 56 mm in diameter,
Samples(s) _ were received with TRC X0.2 ntv+I_ (if #21 is No) told wen:
adjusted wcoazlinbly iir sllmplc rrccivinj with sodium thiosulfate (?`IA_S;03) with Shear ID:
SC Drinking, Wtitcr Project Sample(s) pH verified to be. 2 by I Date:
Sant le(s) were Not I 'ved kit u pH of <, 2 and were adiusted a000rd1n I r usisr
Sample labels applied by:
Verified hV: Date:
Comments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] tww ,shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC._
ENVIRONMENTAL
INC.
h SS'J� ti.!'Mf-N 1 ,+c Hf—Mtf.�fgf_vtKV1f.:��
Emerald Cafolinn C:heeminnln
0309 Wilkinson Blvd.
CinA lutte, NU 28214
Ernnreild Carolina Chemicals farlllty Charlotte, NC
Stormwater Qualitativa Monitoring Requirements Octolici 2111t3
For Ssmplinrl fnr ?_nd 2016 Scntl-Arrrrual Serrrpling (Performed '10R/16)
1- NCnli 2-1=uint 3-Moderate 4-5tronQ
Pipe 001 outfall
C: nln r- 1
Oour- 1
Clarity- 1
Floating Solidi- 1
Susperidccd Solids- 1
Fnsam- '1
Oil Sheen- 1
Fluw- :5.0 (Sal par minute
Rein Event (Total PreelpitationlDuration of Fveot)-0-66 inuhus! 8 tiours
Total Flow- 1,440 Gallon;; (Witwd on the gallons per Minute at time of sampling)
pip-0 002 outfall
Color- -1
Odor- 1
Clarity- f
Floating 0INF,- 1
Suspurided Solid9- 1
F04111- 1
Oil Sheen 1
FIGW- 0,5 Gal por mirrutu
RAin Event (Tntal PmelpltatlonlDuration of Event)-0.66 inche.^,J 8 Iwurs
Total Raw- 240 Gallurr;�; (tjuwLud on they galJona Crr minfrtA rat tlmf!� of sampling)
11164 DOWNS J7QAD, PINE-VILLE, NC 26134 / [phone] f,�ix (704).4t121-fJH'::f J YV.Vwoonenv.00m
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com

SHEALY ENVIRONMENTAL SERVICESI-INC.
_ FNVIFIONMFN'FAI.
SERVICES, INC.
ASSCSSIt}I;NT & REMEDIAL SERVICES
Pipe 003 outfoll
Color- 1
C3dor- 1
Clarity- 1
Floating Sviid;;- 1
Suspended Snlidq- 1
Foam- 1
011 shkuull- 1
Flow- 2.0 Gal per minute
Rain Event (Total PrerlipitatiorgDuration of Evoot)-0.66 invhiuu 8 hluurs
TcAul [=low- 960 Callons (based can the gallons per minute at lima of sampling)
Pipe 004 outfafl
Color- 1
Odur- 1
Clarity- 'I
Floating Solid 2
Susprinded Solids- 2
Foam. 1
Oil Sheen 1
Flow- 1.0 Gal per minute
Rain Evnnt (Tnt,al Pre0ipit3ti0nlf]umti0n of Evurd)-0.643 iric:h u*w 8 hours
Tidal Flow- +4,90 Gallons (based on the gallons per minute at time of sampling)
Pipe 005 outfall
Cvlrar- 1
Odor- 1
charity-1
Floating Solids-2
Si.mpe,nded Sollde..2
Foam- 7
Oil Shnan-1
Plow- 0.5Gsal per minute
Kwin Evoni (Tatel PreclpitatianIOUrntinn of FWent)-0.06. Inches/ d hours
Total !"'low- 210 Gallons (hAFwrl nn the gallons per minuto Lit tiiriu Of sampling)
11164 DUVM/ S ROAD, PINEVILLE, NC. 281,74 (704),'Iran 062 f r;ix YVWW.erFrter1V.001n
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealy)ab.com

SHEALY ENVIRONMENTAL SERVICES INC.
Arm EN'VIRONW 1AI
SERVICES. INC.
ASSESGML4 Af74, REI ELDIAL SEttVOG't
Pipe 009 outfall
Color- 1
Odor- 1
(31-wity- 1
Floating Solid&- 1
{u'1J;.purlded Solids- 1
r,oarr)- i
Oil Sheen- 1
Flow- 0.5 Gal per minute
Pain Event (Tntat Precipitation/Duration of Everrt)-Q,60 irlchest t3 hours
otral Flow-240 Gallons (based on the garlons per minute at time of samplingl)
Pips 007 outfail
Color- 1
Odor- 1
Clarity- 1
Floating EDIAn- I
Suspended Solids- 1
Foam I
Oil .helm« 1
Flow- 1.0 Gal per minute
Rain Event (Total r'recip'rtationlDuraIlan of Event)-0.56 innhp:J R hour::
Total Flow- -180 Gallons (haled on the gallorrt; µex rniriute at time of sampling)
Pipe 008 Outfwll
Color- 1
Odor- -t
Ctartty- I
Floatbnr'l Solids • 2
Suspended Solids- 2
Foam- 1
Oil Sheen- 1
Irfow- 0.5 Gal per minutes
Raln Event (Total Precipitation/Duration of Event)-0.66 inuhuarl 8 hours
rotol Flow- 240 Gallons (based on the pallonc per minute at time of sampling)
i 1? 54 DOWN ; POAD, PINEVILLE, NC 26134 / (70-1)313:7 DFiPY F.ex (/fit) <r; } b�U�3 / wwlv.Bnner v.cum
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

..
's
STORMWATER DISCHARGE OUTFAUL (SDO)
MONITORING REPORT
Permit Number NCS /Mo)(Q) SAMPLES COLLECTED DURING CALENDAR YEAR: 01.1eb
(This monitoring report shall be received by the Division no later than 30 days "Mq
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME L.LC/ COUNTY�,tr3ccRf3-
PERSON COLLECTING SAMPLE S) CkLe — PHONE NO. (-W) 391 - <p-5+f9c
CERTIFIED LASORATORV(S) ✓. ah# +p 4-001
l.ah #
Part A. Specific Monitoring Requirements
—1 COD
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PACE 2. MMO
F-44
/
Date
Sample
�..
��MKISSOM
tV v r�
I mo♦
L.
r
ram•%%{//��
��C�%�LJi/
` �/
I� •
L
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes -X no
(if yes, complete Part B)
Part S: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
OO556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPII
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/M r
MG
inches
me]
m l
unit
allmo
Dorm SWU-247, Iasi revised 21212012
Page 1 of 2

STORM EVENT CUARACTERISTICS:
Date
Total vent Precipitation (inches):
Event Duration (hours): 13 (only if applicable — set permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
6
a3 asa��
lure Perm' ee) (Dat )
Dorm SWU-247, It revised 21212012
Page 2 of 2

Emerald Nrfo"make Materiab
March 51h, 2015
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Stormwater Discharge Monitoring Reports
NPDES Stormwater Permit
Permit NCS000161
Emerald Performance Materials
Mecklenburg County
To Whom It May Concern:
RECEIVED
MAR 0 6 2015
CENTRAL FILES
DWR SECTION
Enclosed you will find the Stormwater Discharge Outfall Monitoring Report for
Emerald Performance Materials located at 8309 Wilkinson Blvd, Charlotte, NC.
The report contains the analytical results for sampling during Year 6 - Period 1 of
the subject permit. As noted in the report, Benchmark values for TSS were
exceeded at Outfall No. 7 and Benchmark values for Oil and Grease were
exceeded at Outfall No. 4. Emerald has established a Tier One Response
Procedure as a result of this finding. If you have any questions please do not
hesitate to contact me at [phone].
Health, Safety, Security & Environmental Manager
Emerald Carolina Chemical, LLC
8309 Wilkinson Blvd. 1 Charlotte, NC 282141 Phone: [phone] Fax: [phone]
www.emeraidmaterials.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Emerald Carolina Chemical
8309 Wilkinson Blvd.
Charlotte, NC 28214
Attention: David Sikes
Project Name: First Semi -Annual 2015 SW Sampling
Lot Number:01310105
Date Completed:0212312015
Date Revised:0212412015
Kelly M. Nance
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 11
106 Ventage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Lavel 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Emerald Carolina Chemical
Lot Number: QB10105
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shoolyleb.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Emerald Carolina Chemical
Lot Number: OB10105
Sample Number
Sample ID
Matrix
Date Sampled
Data Received
001
001
Aqueous
02/09/20151418
02/10/2015
002
002
Aqueous
02109/20151423
02/10/2015
003
003
Aqueous
02/09/20151430
02/10/2015
004
004
Aqueous
02/09120151433
02/10/2015
005
005
Aqueous
02/09/20151437
02/10/2015
006
006
Aqueous
02/09/20151443
02/10/2015
007
007
Aqueous
02109/20151445
02/10/2015
008
008
Aqueous
02/09120151405
02/10/2015
(8 samples)
Shealy Environmental Services, Inc. Page: 3 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: QB1010S-001
Description: 001 Matrix: Aqueous
Date Sampled:02l0912015 1418
Date Received:02/10/2015
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1418
1
(COD) SM 5220D-2011
1 02/19/2015 1520 DRB1
02/19/2015 1157
1
(TSS) SM 254OD-2011
1 02/16/2015 0908 AMM1
67877
1
(HEM (oil and) 1664B
1 02/23/2015 0910 RIPS
68393
CAS Analytical
Parameter
_
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
30
10
mg/L
1
TSS
SM 254OD-20
5.2
1.0
mg/L
1
HEM (oil and grease)
1664E
N❑
4.4
mglL
1
ootnote(s): "'Tim McCorkle/ARM
PQL - Practical quantitatlon limit B = Detected in the method blank E a Quantitatlon of compound exceeded the callbratlon range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and? MDL P = The RPD between two GC columns exceeds 40% N a Recovery is out of criteria
Where applicable, all loll sample analysis are reported on a dry weight basis unless flagged with a'W
Shealy Environmental Services, Inc. Page: 4 of 11
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: OB10105-002
Description! 002 Matrix: Aqueous
Date Sampled:0210912015 1423
Date Received :02110/2015
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1423
1
(COD) SM 5220D-2011
1 02/23/2015 0942 AMM1
02/20/2015 1527
1
(TSS) SM 254OD-2011
1 02/16/2015 0908 AMM1
67877
1
(HEM (oil and) 1664E
1 02/23/2016 0910 RPB
68393
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 52200-20
34
10
mg1L
1
TSS
SM 254OD-20
38
3.3
ril
1
HEM (oil and grease)
1664B
ND
4.3
mg/L
1
ootnote s : '"Tim McCorkie/ARM
PQL = Practical quarttalion limit 0 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H - Out of holding time
ND = Not detected at or above the POL J = Estimated result < PQL and � MDL P = The RPD between two GC columns exceeds 40% N - Recovery Is out of criterla
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W'
Shealy Environmental Services, Inc. Page: 5 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Leval 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: QB10105-003
Description:003 Matrix: Aqueous
Date Sampled:0210912015 1430
Date Received:02110 /2015
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1430
1
(COD) SM 5220D-2011
5
1 02/23/2615 0942 AMM1
02120/2015 1527
1
1 SM 2540D-2011
1 02/16/2015 0908 AMM1
67877
1
(HEM (oil and) 1664E
1 02/23/2015 0910 RPB
68393
CAS Analytical
Parameter
__.
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
34
10
mg1L
1
TSS
SM 25400-20
29
2.5
mg1L
1
HEM (oil and grease)
1664B
ND
4.4
ni
1
Footnote(s): '"Tim McCarkle/ARM
PQL - Practical quantdation limit 8 =Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time
NO = Not detected al or above the PQL J = Estimated result a PQL and i MOIL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a'W'
Shealy Environmental Services, Inc. Page: 6 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: QB10'105-004
Description:004 Matrix: Aqueous
Date Sampled:0210912015 1433
Date Received: 02110/2015
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1433
1
(COD) SM 5220D-2011
1 02/1912015 1520
DR61 02/19/2015 1157
1
(TSS) SM 254OD-2011
1 02/16/2015 0908
AMM1 67877
1
(HEM (oil and) 1664B
1 02123/20150910
RPB 68393
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
20
10
mg1L
1
TSS
SM 25400-20
43
2.0
mg1L
1
HEM (oil and grease)
1664E
18
4.6
mg1L
1
Footnotes : "Tim McCorklelARM
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding b'me
NO a Not detected at or above the POL J - Estimated result a PQL and > MDL P = The RPD between two GC columns exceeds 411% N - Recovery is out of criteria
Where applicable, all soil sample aralysls are reported on a dry weight basis unless flagged with a "W
Shealy Environmental Services, Inc. Page: 7 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyiab.com Level 1 Reportv2.t

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID:OB10105-005
Description:006 Matrix: Aqueous
Date Sampled:0210912015 1437
Date Received: 0211012015
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) 5M 4500-H B-2011
1 02/09/2015 1437
1
(COD) SM 52200-2011
1 02/19/2015 1520
DRB1 02/19/2015 1157
1
(TSS) SM 2540D-2011
1 02/16/2015 0908
AMM1 67877
1
(HEM (oil and) 1664B
1 02/23/2015 0910
RPB 68393
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 522OD-20
19
10
mglL
1
TSS
SM 254OD-20
45
2.5
mglL
1
HEM (oil and grease)
1664E
HD
4.4
mglL
1
Footnote(s):"Tim cCarkle A M
PQL - Practical quanttation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result a POL and > MDL P = The RPD betweer two GC columns exceeds 40% N - Recovery is out of critaria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc: Page: 8 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.wm Level 1 Report v2A

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: Q610105-006
Description: 006 Matrix: Aqueous
Date Sampled:0210912015 1443
Date Received:0211012015
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1443 "
1
(COD) SM 5220D-2011
1 02I1912015 1520 DRS1
02/19/2016 1157
1
(TSS) SM 254OD-2011
1 02/16/2015 0908 AMM1
67877
1
(HEM (oil and) 1664B
1 02/23/2015 0910 RPB
68393
CAS Analytical
Parameter
Number _ Method
—
Result Q
PQL _
Units
—
Run
pH - Field
SM 4500-H B
6.5
su„
1
COD
SM 6220D-20
13
10
mg1L
1
TSS
SM 25400-20
5.6
1.0
mg1L
1
HEM (oil and grease)
1664E
ND
4.5
mg/L
1
Footnote(s): "Tim cCorklel M
PQL = Practical quartltation Ilmit B - Detected in the method blank E = Quantitatlan of compound exceeded the calibration range H = Out of holding time
ND - Not detected at or above the PQL ' J - Estimated result < POL and g MDL P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
Where applicable. all soil sample analysis are reported on a dry weight basis unless Flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 11
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: QB10105-007
Description:007 Matrix: Aqueous
Date Sampled:0210912015 1445
Date Received:0211012015
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
02/09/2015 1445
1
(COD) 5M 52200-2011
1
02/19/2015 1450
DR131 02/19/2015 1157
1
(TSS) SM 254OD-2011
1
02/16/2015 0908
AMM1 67877
1
(HEM (oil and) 1664B
1
02/23/2015 0910
RPB 68393
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
80
10
mg1L
1
TSS
SM 254OD-20
150
10
mg1L
1
HEM (oil and grease)
1664B
ND
4,7
mg/L
1
Footnote(s): "Tim cCQ e/A M
PQL = Practical quartitation limit B = Detected in the method blank E = Quantitatim of compound exceeded the callbratlon range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < POL and > MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where appllcable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Loyal 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: QB10105-008
Description:008 Matrix: Aqueous
Date Sampled:02109/2015 1405
Date Received: 0211012015
Run Prop Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 02/09/2015 1405
1
(COD) SM 5220D-2011
1 02/19/2015 1520
DRB1 02/19/2015 1157
1
(TSS) SM 254OD-2011
1 02/16/2015 0908
AMM1 67877
1
(HEM (oil and) 1664B
1 02/23/2015 0910
RPB 68393
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 52200-20
28
10
m91L
1
TSS
SM 254OD-20
15
1.7
mg1L
1
HEM (oil and grease)
16648
ND
4.5
mglL
1
Footnote(s): Tim cCor elAR
POL = Practical quantitation limit B = Detected in the method blank E = Ouarruation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < POI_ and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W
Shealy Environmental Services, Inc. Page: 11 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylal).corn Level 1 Report v2.1

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SHEALY ENVIRONMENTAL SERVICES, INC.
SHEALY 106 Vantage Point Drive s West Columtaa, Sr— 29172
�h81D Q� V SrOdi � Telephone No. 803.791-MO Fax M1ta_ 803-791-9111 Number 5 2
www.shodylab-com
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SHEALY ENVIRONMENTAL SERVICES, INC.
Slump Enwimntwrdal Servicm Iae,
Doci.werif Nwnhcr: F-AD•016
Rrvislon Number: 16
Petty 1 of I
R90MUCS Dale: 071WI4
Etfictk Drug 11101-114
Sample Receipt Checklist (SRC)
Client; A(1a Cooler inspected byidate- O_ AT-.%21tCAIS Loth: Q61tajQa
Means ofreceipt: ff�SRESI ❑ Client ❑ UPS ❑ FedEx ❑ Airborne Exp ❑ Other
Yes
No M
11. Were cusrody seals present on the cooler?
Yes
No NA
2. If custody souls were present, were flipy uttael and unbroken?
Cooler ID/Original temperature upon receiptq)erived (corrected) temperature upon receipt:
Method: ietnperature Wank 0 Against Bottles IR Gun ID: #4 lR Gun Correction tractor: VC
Method of coolant: [et lac ❑ Blue Ice ❑ Dry Ice ❑Atone
Yes ❑
No ❑
NA
3. Tf temperature of any cooler exceeded 6.0°C, was Prujcct Managcr notified?
PM notified by SRC:, phone, note (circle one), other;___
(For coolers received via commercial courier, PMs are to be notified
immediately.
Yes ❑
'o ❑
NA
4. Is the commercial courier's 2ack1n&sljg attached to this form?
Yea I
NO ❑
1
5. Were proper custody procedures(re lin uishedlreceived followed?
Yes ❑ I
Two ❑
NA Cal
5a Were samples relinquished by client to commercial courier!
Yes
'o ❑
6. Were sample 1Ds listed on the CDC?
Yec
No
7. Wart: stub is IDs listW on all yam lu conlainm?
Yes
No ❑
8. Was collection date & time listed on the COO:?
Yes
a ❑
9. Was collection datc & time listed on all sample containers?
Ycs
No LJ
10. Did all container label information ID, date, time agree with the COC?
Yes 01No
l 1. Were tests to be penfortned listed on the COC?
YcK OT
No ❑
1 12. Did all samples arrive in the proper eantainers for each test?
Yc3
No ❑
13. Did all containers arrive in good condition unbroken lids on etc.)?
Yet
No ❑
14, Was adequate sample volunte available?
Yes
No ❑
15. Were all samples received within !, the holding time or 48 hours, whiclmever
comes first?
Yes ❑
ha _
16. Were any samp leg wnlainers missin ?
Yes ❑ I
No
I
L 17_ Were there an • excess samples not listed on COC?
Yes
No
NA
19. Were bubbles present>" a•size" l/, orbmin in diameter in any VOA vials?
Yes
No
NA ❑
19. Were all meuilge"&GIFIEN1.1nulriont samples roceived at a p1l of =2?
Yes ❑
No ❑
NA
ud_ Were all cyanide and/or sulfide samples rc=ivcd at a pH >12?
Ycs ❑
No ❑
NA
21. Were all applicable NHWKNIcyanida phenol (<0.2mg(L) samples five of
residual chlorine?
Yes ❑ I
No ❑
NA
22. Were collection teen ralutes documented on the COC for NC samples?
Ycs ❑
No ❑
NA P'
23. Were client remarks/requests (i,e. requeskA dilutions, MSIMSD designations,
etc... correctly transcribed from die COC into the comment section in LIMS?
Yes Q
No
24, Was the quote number used taken from the container label?
Sample Preservation (Must be completed for any sample(s) iveim-rcOly pmser ved or with headspace.)
Sampie(s) were received incorrectly preserved and w= adjusted
according ly in gem lc rtxcivin with HzSC?i D,,HCI,NaOH) using SR 4
Sam le c were roccived with bubbles>6 mm in diameter.
Sam Ic(s) were te"Nud with TRC >0.2 m ., (If #21 is No
SC Drinking Water Project Sample(s) pH verified to be,> 2 by Date:
5artr *s) were not received at pH of <2 and were adjusted accord in Iv using SlifJ
11 Sample labels a lied by: Verified Date. 2 f5
Q Lments:
Shealy Environmental Services, Inc.
106 Vantage Point drive West Columbia, SC 29172 [phone] Fax [phone] www.shaalylab.com Leval 1 Report v2,1

-SHEALY ENVIRONMENTAL SERVICES, INC.
AwENVIRONMENTAL
SERVICES, INC.
A SSESSMENT & REMEDIAL SERVICES
Mr. David Sikes
Emerald Carolina Chemicals
8309 Wilkinson Blvd,
Charlotte, NC 28214
Emerald Carolina Chemicals facility Charlotte, NC
StormwaterQualltative Monitoring Requirements February 2015
For Re -Sampling for I'll 2015 Semi -Annual Sampling (Performed 219115)
1- None 2-Fahnt 3-Moderate 4-Strong
Pipe 001 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids-1
Foam- i
Oil Sheen- 1
Flow- 20 Gal per minute
Rain Event (Total PrecipitatiorVDuration of Event}0.86 inched 13 hours
Total Flow- 15,600 Gallons (based on the gallons per minute at time of sampling)
Pipe 002 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids-1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 1.0 Gal per minute
Rain Event (Total Precipitation0uralion of Event}0.85 inched 13 hours
Total Flow-780 Gallons (based on the gallons per minute at time of sampling)
11164 DOWNS ROAD, PINEVILLE NC 28134 / [phone] fax [phone] / 1w,ww.wmeriv.com
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www•shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC. ,
AWENVIRONMENTAL
SERVICES, INC,
ASSESSWNT& REMEDIAL SERVICES
Pipe 003 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Sands-1
Foam-1
OII Sheen- 1
Flaw- 0.5 Gal per minute
Rain Event (Total Preclpllatlon/Duration or Event)-0.86 inches! 13 hours
Total Flow-390 Gallons (based on the gallons per minute at time of sampling)
Pipe 004 outfall
Color- 2
Odor- 1
Clarity- 2
Floating Solids- 2
Suspended Solids- 2
Foam-1
Oil Shen- 1
Flow- 0.5 Gal per minute
Rain Event (Total PrecipttationtfOuration of Event)-0.86 inches/ 13 hours
Total Flow 390 Gallons (based on the gallons per minute at time of sampling)
Pipe 005 ouftll
Color- 1
Odor- 1
Clarity-1
Floating Solids-1
Suspended Solids-1
Foam- 1
Oil Sheen-1
Flow- 1.0 Gal per minule
Rain Event (Total Precipits tionlDuration o1 Eventr0.86 incheW 13 hours
Total Flow- 700 Gallons (based on the gallons per minute at time of sampling)
11164 aowuS ROAO. PNEVILLE NC 28124 / (704)369-01521 fax (704)369-M23 I www armenv.com
Shealy Environmental Services, Inc.
100 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylob.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
KmENVIRONMENTAL
SERVICES, INC.
ASSESSMENT d REMEDIAL SERVICE'S
Pipe 006 outfatl
Color- 2
Odor-1
Clarity- 2
Floating Solider 1
Suspended Solids-1
Foam- 1
011 Sheen- 1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-0.86 inches/ 13 hours
Total Flaw-390 Gallons (based on the gallons per minute at time of sampling)
Pipe 007 outfall
Color- 2
Odor- 1
Clarity- 2
Floating Solids- 2
Suspended Solids- 2
Foam- 1
Oil Sheen- 1
Flow- 1.0 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-0.86 inchesf 13 hours
Total Flow- 780 Gallons (based on the gallons per minute at time of sampling)
Pipe 008 outfall
Color- 2
Odor- 1
Clarity- 2
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 1.5 Gat per minute
Rain Event (Total PrecipitationlDuration of Event)-0.88 inches/ 13 hours
Total Flow- 1,170 Gallons (based on fhe gallons per minute at time of sampling)
} 1164 DOWNS ROAD, PINEWILL.E, NG 28134 ! (7D4)369-tI621 fax [phone] f www.turMrtv,c0rn
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheelylab.com Level 1 Report v2.1

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS ��� (Q� _ SAMPLES COLLECTED DURING CALENDAR YEAR: 112101,11
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME MERAW-) r�?F>D tA�t�JG.� Mg71�,pugg.3LLc— COUNTY /►1F�kLF�/VE_1Z!',Zr _
PERSON COLLECTING SAMPLE(S) PHONE NO. (?D1f l mil/- 4,V4'41-
CERTIFIED LABORATORY(S) l Lab # 4-e-1ID&O-001
Lab #
SIGNATURE OF PERMCTTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
i00/mom
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��+�
+
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J
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Maia
�J
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��
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al •
,
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes Xno
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitorine Reauirements
':Outfall -, ' =
=Date � �
50Q50` _
r '-
:00555
_
0053©` .
004©0_ _
w
`No
�Sainple
Total'Flow :' -
Total,
Oil & GKease -Non
=po6r _'
Total=_ m
pH =New
Motor
Collected
(if applicable)
Ra�nfa[I
�(ifappE)�
:�O&GIIPF[
Suspended
Oil Usage
= G
s
{1Vlethoi 166
Solids'
u
SCT=HAM), if
-
appl. ,.
_..
-
r._
ono/dd/ r _. -:
MG
inches _
:m
-
unit
_
aI/mo e
Form SWU-247, last revised 21212012
Page 1 of 2
f

STORM EVENT CHARACTERISTICS:
Date Qy !l
Total Event recipitation (inches): 0,1(0
Event Duration (hours): !& (only if applicable -- see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Ann: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
/0�
%I a %f7
i re o -(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Emerald Carolina Chemical
8309 Wilkinson Blvd.
Charlotte, NC 28214
Attention: David Sikes
Project Name:2nd 2014 Semiannual Stormwater
Lot Number:P125042
Date Completed:1010712014
-71YU-11,
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 11
106 Vantage Point Drive West Coiumbia, SC 29172 [phone] Fax [phone] www.sheaiylab.com Laval 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Emerald Carolina Chemical
Lot Number: P125042
This Report of Analysis contains the analytical resull(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 11
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Emerald Carolina Chemical
Lot Number: P125042
Sample Number
Sample 1D
Matrix
Date Sampled
Date Received
001
001
Aqueous
09124120141405
09/25/2014
002
002
Aqueous
09124/20141410
09/25/2014
003
003
Aqueous
09/24/20141418
09/25/2014
004
004
Aqueous
09/24120141420
09/25/2014
005
005
Aqueous
09/24/20141424
09/25/2014
006
006
Aqueous
09/24120141428
09/25/2014
007
007
Aqueous
09124120141430
09/25/2014
OOa
008
Aqueous
09/24120141345
09/25/2014
(8 samples)
Shealy Environmental Services, Inc. Page: 3 of 11
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4
Inorganic non-metals
t
Client: Emerald Carolina Chemical Laboratory ID: P125042-001
Description: 001 Matrix: Aqueous
Date Sampled:0912412014 1405
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1405
"
1
(COD) SM 5220D-2011
1 10/02/2014 1540
HMA 10/01/2014 1928
1
(TSS) SM 254OD-2011
1 09/29/2014 1038
AMM1 57047
1
(HEM (oil and) 1664B
1 10/07/2014 0930
EWR 57659
CAS Analytical
Parameter
Number Method
Result a
PQL
Units
Run
PH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
20
10
mg/L
1
TSS
SM 2540D-20
3.5
1.0
mg1L
1
HEM (oil and grease)
16649
NO
4.4
mg1L
1
Footnote(s): **ARMrrim McCorkle
POL = Practical quantltabon Ilmlt B = Detected In the method blank E - Quartltation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and a MDL P =. The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 4 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: P125042-002
Description: 002 Matrix: Aqueous
Date Sampled:09124/2014 1410
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1410 **
1
(COD) SM 5220D-2011
1 10/02/2014 1540 HMA
10/01/2014 1928
1
(TSS) SM 25400-2011
1 09/29/2014 1038 AMM1
57047
1
(HEM (oil and) 1664E
1 10/07/2014 0930 EWR
57659
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
PH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
26
10
mg1L
1
TSS
SM 254OD-20
4.4
1.3
mg1L
1
HEM (oil and grease)
1664E
ND
4.4
mg1L
1
Footnote(s): **ARMrrim McCorkle
PO4 - Practical quanAtatlon limit B = Detected in the method blank E - Ouantllation of compound exceeded the calibration range H - Out of holding time
ND - Not detected at or above the PQL J = Estimated result a POL and? MDL P a The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 11
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S
Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: P125042-003
Description: 003 Matrix: Aqueous
Date Sampled:0912412014 1418
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
09/24/2014 1418
1.
1
(COD) SM 5220D-2011
1
10/02/2014 1540
HMA 10/01/2014 1928
1
(TSS) SM 254OD-2011
1
09/29/2014 1038
AMM1 57047
1
(HEM (oil and) 1664E
1
10/07/2014 0930
EWR 57659
CAS Analytical
Parameter
Number _Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
t
COD
SM 5220D-20
25
10
mg1L
1
TSS
SM 254OD-20
3.3
1.3
mg1L
1
HEM (oil and grease)
1664B
NO
4.6
mg1L
1
Footnote(s): "ARM/Tim McCorkle
POL • Practical quantitation limit B • Detected in the method blank E - Ouantitallon of compound exceeded the callbratlon range H = Out of holding time
ND = Not detected at or above the POL J Estimated result < POL and n MDL P - The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysts are reported on a dry weight basis unless Nagged with a -W-
Shealy Environmental Services, Inc. Page: 6 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: PI25042-004
Description: 004 Matrix: Aqueous
Date Sampled:0912412014 1420
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1420 **
1
(COD) SM 5220D-2011
1 10/02/2014 1540 HMA
10/01/2014 1928
1
(TSS) SM 2540D-2011
1 09/29/2014 1038 AMM1
57047
1
(HEM (oil and) 1664E
1 10/07/2014 0930 EWR
57659
CAS Analytical
Parameter
Number _ Method
Result_ Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
44
10
mg1L
1
TSS
SM 254OD-20
39
2.0
mg1L
1
HEM (oil and grease)
16648
NO
4.5
ni
1
Footnole(s): **ARMITim McCorkle
PQL - Practical quandtatlon limit B - Dalected in the method blank E = Quantltallon of compound exceeded the calibration range H - Out of holding time
ND . Not detected at or above the PQL J - Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
Where appllcable, all soil sample anal is are reported on a dry weight basis unless flagged with a -W"
Shealy Environmental Services, Inc. Page: 7 of 11
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t
Inorganic non-metals
ClienCEmerald Carolina Chemical Laboratory ID: P125042.005
Description: 005 Matrix: Aqueous
Date Sampled:09/24/2014 1424
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1424
"'
1
(COD) SM 5220D-2011
1 10/02/2014 1540
HMA 10/01/2014 1928
1
(TSS) SM 254OD-2011
1 09/29/2014 1038
AMM1 57047
1
(HEM (oil and) 1664E
1 10/0712014 0930
EWR 57659
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
22
10
mg1L
1
TSS
SM 254OD-20
5.6
1.0
nI
1
HEM (oil and grease)
1664E
ND
4.5
mglL
1
Footnote(s): A M im McCorkle
POL - Practical quantltation IlmIt B - Detected in the method blank E = Quanglation of compound exceeded the calibration range H - Out of holding time
ND - Not detected at or above the POL J = Estimated result t PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applioabte, all soil sample analysis are reported on a dry weight basis unless Hogged with a "W-
Shealy Environmental Services, Inc. Page: 8 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: P125042-006
Description:006 Matrix: Aqueous
Date Sampled:0912412014 1428
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1428
1
(COD) SM 5220D-2011
1 10/02/2014 1515 HMA
10/01/2014 1928
1
(TSS) SM 2540D-2011
1 09/29/2014 1038 AMM1
57047
1
(HEM (oil and) 1664B
1 10/07/2014 0930 EWR
57659
CAS Analytical
Parameter
Number [Method
Result Q �
Ill
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
56
10
mg1L
1
TSS
5M 2540D-20
15
1.0
mg1L
1
HEM (oil and grease)
16648
ND
4.4
mg1L
1
Footnote(s): "ARM/Tim McCorkle
POL - Practical cluantltation limit B - Detected in the methcd blank E - Ouanthation of compound exceeded the callbratlon range H = Out of holding time
ND - Not detected at or above the POL J - Estimated result < POL and g MDL P - The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, al} soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Shealy Environmental Services, Inc. Page: 9 of 11
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Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: P125042-007
Description: 007 Matrix: Aqueous
Date Sampled:0912412014 1430
Date Received:0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 09124/2014 1430
1
(COD) SM 5220D-2011
1 10102/2014 1540
HMA 10/01/2014 1928
1
1 5M 2540D-2011
1 09129/2014 1038
AMM1 57047
1
(HEM (oil and) 1664B
1 10/0712014 0930
EWR 57659
CAS Analytical
Parameter
Number Mg1hod
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 52200-20
23
10
mg1L
1
TSS
SM 254OD-20
7.7
1.0
mg1L
1
HEM (oil and grease)
1664E
ND
4.5
ril
1
Footnote(s): ' ARM im McCorkle
POL - Practical quangtation limit B - Detected In the method blank E - Duantitation of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the POL J - Estimated result < POL and ? MOL P v The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W-
Shealy Environmental Services. Inc. Page: 10 of 11
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: P125042-008
Description: 008 Matrix: Aqueous
Date Sampled:0912412014 1345
Date Received: 0912512014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 09/24/2014 1345 **
1
(COD) SM 5220D-2011
1 10/02/2014 1540 HMA
10/01/2014 1928
1
(TSS) SM 254OD-2011
1 09/29/2014 1038 AMM1
57047
1
(HEM (oil and) 1664B
1 10/07/2014 0930 EWR
57659
CAS Analytical
Parameter
Number Method
Result 0
POL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
55
10
mg1L
1
TSS
SM 254OD-20
6.6
1.0
mg1L
1
HEM (oil and grease)
1664B
NO
4.4
mglL
1
Footnote(s): **ARM1Tim McCorkle
PQI. = Practical quantilation limit B - Detected In the method blank E = Quantltatlon of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J - Estimated result < POL and } MOIL P = The RPD between two GC columns exceeds 4D% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a'W-
Shealy Environmental Services, Inc. Page: 11 of 11
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4
Lol Chain of Custody Record
Shealy Environmental Services, Inc.
I O Vantage Point DrW
West Columbia, South Carolina 28172
Telephone No. (803) 7913700 Pax No. l(SO T91 9111
'NW v sI1m8illlllab cum
Number 26409
Till
•presmative■�f1i�Lfra
MOM
■■MM■■
"'
MM■■■■
■■
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"
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M�
"
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.
125042
MICH11101
04.
IMMMMAM
- . . ,
N AU unmples are reUined :elpt 11FIV-1w.1
so �rmmemft are made.
M
C
C�
M
CAI

SHEALY ENVIRONMENTAL SERVICES, INC.
Sbesly EcviromgerAil Scrims, inc.
Document Number; F-AD-016
Rvvbian Number: 11
essn t of r
Replaces C lure ff3,137f 14
Effw6vc flame' OVIN14
//�� Sample Receipt Checklist (SRC)
�Client: (Oaj'CsyLi-1C1 Cooler Inspected byldatc, C.Ntr 1911219k4 Lot # : ft�;2
Means of receipt'. SES1 ❑ .Client ❑ UPS ❑ FedEx ❑ Airbome ftp ❑ Other
Yes
No al
1 1. Werc custody acala pm=t on the cooler?
Yes
LJ
I No LJ I NA
2. If custody seals Were presemt, were they intact and unbroken?
Cooler i ,10riginal temperature upon reccipt0erived (corrected) temperature upon receipt:
Method: ❑ Temperature Wank Against Bottles IR Gun III: *3 iR Gun Corncctimt factor, 4oPC
Method of coolant, [30 1y et Ice M Blue lee Ice ❑ Nonc
Yes ❑
No ❑y,+l
9. if templerature of any cooler exceeded 6.41C, was Project Manager noaif ed ;'
PM nntifrod by SRC, phone, note (circle one), other
(For coolm received An commercial courier, PMs aft: to be notified
irIlulcdiatxl .
Yes ❑
o ❑
NA ff
4. is the commercial courier's packing slip attached to this fcxm?
Yea
No ❑
S. Were pmrE cimod ' 11mcedures rel inqLLishedlreceived followed7
Yes ❑
No ❑ I
NA
Sa Were sam les relinquished b • client to commercial courier?
Yes
No
6. Were sample Ms listed an the COL'?
7. Wcre sample IDs listed on all sample containers?
n ❑
8. Was cullcctlu4 chic &i 4um llsiml (m the CSC?
4r,N
c
9. Was collection date & time listed on all sample contaitlets?
n
10. Did all container labcl infrmnation ID, datc, time a me with the CDC?
o ❑
11. Wcra tests to be hsiod on the COC?
n ❑
I Ill Hit aim 1G:3 HmYC in IhG tf GI4ifIIINi11Cr5{ CUI CHCII IGat?
Yes
No ❑
13. Did all containers arrive iu-good condition unbroken, lids on etc.)?
Ycs
No ❑
14. Was ade uate sarri le vnlume available?
Yes
No ❑
l S. Were all samples received within 'A the holding time or 48 hours, whichever
comes first?
yea ❑
NU Er
16, it om any anal IGs cuntH>nGr� mrsun ? I
Yes
No le
17. Were there any excess samples not liAW on COC.'
Yes El
No
NA
18. Wen: bubbles pmscrit >` -sizu" 'f.' idr 6rnm in diameter) in an y VOA vials?
Yes
I+o 0_
NA❑
19. Were all meta &s O&GiH13hVnutrient samples received at a H of<27
Yes
Na
NA
20. Were a#1 cyarlidin arid/'or sulfide aim Icq ncceivl:d at a pIT >1?
Yes ©
No ❑
NA LJ
21. Were all applicable NH3JTKN+cyauidc1pheno1 (<Urn IL) samples free of
residual chlorine`'
Yes El I
Nu ❑
NA
22. Wcrc callcutlon lqn cramms documented on the COC for NC samples?
Yes ❑
No ❑
NA
23. Were client renlarks+'rcqucsts (i.e. roqucstcd dilutions, MStMSD designations,
etc. , . corrrxtl transcribed Crum the COC intothe comment srction in I.1MS?
Yes No 24. Was the.quote lumber used takes from the container label?
Sample Presemation (Miist bG oumpletcd for any snrnplc(s) inoorrectly pmsarvod or with headspaoe.)
Samples) 'ere Ieceit,ed incorrectly preservW and w= adjusicd
accordingb, in sample rGCGivin with SO HN43 CI NaOH' using SR A
Sample(s) were received with bubhlec >6 nim in diameter.
S 1 s wort✓ received with TRC }0.2 m T. If #21 is No
SC Drinking Water Project Sashplo(s) pH verified to be > 2 by Date:
Samples) were not received at a PH of <2 and ►ygrt: adiuslcd acconfingly using SR9
Sam le labels applied by- aiklcr Verified bY: Date;:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Repon v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
AWENVIRONME
SERVIGM IK
ASSESSMENT
Mr. David Sikes
Emerald Carolina Chemicals
8309 Wilkinson Blvd
Charlotte, NC 28214
Emerald 06
Stormwater Qualltai
For
1- None 2-Faint 3
Pipe 001 outfall
Color-1
Odor- 1
Clarity- 1
Floating Solids- 1
5uspertdlsd Solids- 1
Foam-1
09 Sheen- 1
Flow- 10 Gal per minute
Rain Event (Total Procipit
Total Fkwv- 4,800 Galloins
Pipe 002 outfall
Color- 1
Odor- 1
0arity- i
Floating Solids-1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 1.5 Coal per minute
Rain Event (Total Precipitation
Total Flow-720 Gallons (based
I
111M
-w Chemicals fall Charlotte, NC
Monitoring Requirements September 2014
l Semi -Annual 2014 Event
derate 4-Strong
wi 1plt of Event)-O. 16 inches/ 8 hours
on the gallons per minute at tame of sampling)
ration of Event)-O. 16 In0098 hours
the gallons per minute at lime of sampling)
faxt7(W)389.W23 / www.ermenv,mm
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
KMENVIRONMENTAL
SEAViCES, INC.
ASSt?SSMENT & R5i6r?t:DIAL SER MISS
Pipe 003 ouffall
Color- 1
Odor- 1
Clarity-1
Floating Sviids- 2
Suspended Solids- 2
Foam 1
ON Sheen- 1
Flow-1 Gel per minute
Rain Event (Total PrecipliationJoutation of Event)-0.18 inches/ S hours
Total Flow-480 Gallons (based on the gallons per minute at time of sampling)
Pipe 004 outfall
Color- 1
Odor- t
astity- 1
FWtirtg Solids- 1
Suspended Solids-1
Foam-1
Oil Sheen- 1
Flow-1.5 Gal per minute
Rain Event (Total Predpitation/I
Total Flow- 720 Gallons (based
Pipe 006 ouffall
Col)r--1
Odor- 1
clarity-1
Floating Solids-1
Suspended Solida-1
Foam- i
Oil Sheen-1
Flow- 1.0 Gal per minute
Rain Event (Total Predpitatlond
Total Flow- 480 Gallons (baked
ation of Event]-0,16 inches/ 8 hours
the gallons per minute at time of sampling)
anon of Even". ie lnches/ 8 hours
the gallons per minute at time of samping)
28134 / {704)369a2t fax C7N)389-1151W r Iwv.amrenv,aam
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
AWENVIRONMENTAL
SEROCES, INC.
ASSESSMENT 6 REVEDOL SERMIFS
Pipe 006 outfall
Color- 1
Odor- 1
Clarity-1
Floating Solids- 2
Suspended Solids- 2
Foam-1 ;
Oil Sheen- 1
Flaw- 0.6 Gal per minute
Rain Event Motel Precipitation/Duration of Event}0.16 inches/ 8 hours
Fotal Flow-240 Oellons (based an the gallons per rninute at time of sampling)
Pipe W? outfall
color- 1
odor- 1
Clarity- 1
Floating Solids- 2
Suspended Solids- 2
Foam-1
Oil Sheen- 1
Flow- fl.5 Gal per minute
Rain Event (Total Precipliation/Ciuration of Event)-0.16 ind*si 8 hours
Total Flaw- 240 Gallons (based bn the gallons per minute at time of sampling)
Pip 003 outfall
Color- 1
Odor- 1
Clarity- 4
Floating Solids-1
Suspended Solids-1
Foam- 1
Oil Sheen- 9
Flow-1.0 Gal per minute
Rain Event (Total Predpitation/Duration of Event)-0.16 Inches! 8 hours
Total Flow- 480 Gallons (based on the gallons per minute at dme of sampling)
11164 DOWNS ROAD. XNEVUX, NC 28134 / (7a4)369411621 fox (704W9-M3 / www.ennertv.0=
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

g:;eralldl Performance Materials
Carolina Chemical
October 10, 2014
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Stormwater Discharge Monitoring Reports
NPDES Stormwater Permit
Permit NCS000161
Emerald Performance Materials
Mecklenburg County
To Whom It May Concern:
Please find enclosed the Stormwater Discharge Outfall Monitoring Report for
Emerald Performance Materials located at 8309 Wilkinson Blvd, Charlotte, NC.
The report contains the analytical results for sampling during Year 5 - Period 2 of
the subject permit. As noted in the report, all results are within the benchmark
values as established in the permit. If you have any question please do not
hesitate to contact me at [phone].
Sincerely,
J. David Sikes
Health, Safety, Security and Environmental Manager
Emerald Carolina Chemical, LLC
8309 Wilkinson Blvd./ Charlotte, NC 282141 Phone: [phone] Fax: [phone]
www.emeraldmaterials.com

Emerald Performance Materials
March 26th, 2014
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Stormwater Discharge Monitoring Reports
NPDES Stormwater Permit
Permit NCS000161
Emerald Performance Materials
Mecklenburg County
To Whom It May Concern:
F?ECE1 VED
M4R 2 7 2014
CENTRAL F1LEQ
D V06bG
Please find enclosed the Stormwater Discharge Outfall Monitoring Report for
Emerald Performance Materials located at 8309 Wilkinson Blvd, Charlotte, NC.
The report contains the analytical results for sampling during Year 5 - Period 1 of
the subject permit, As noted in the report, Benchmark values for TSS were
exceeded at Outfali No. 7. Emerald has established a Tier One Response
Procedure as a result of this finding as required in our Permit. If you have any
questions please do not hesitate to contact me at [phone].
Sincerely,
J. David Sikes
Health, Safety and Environmental Manager
Emerald Carolina Chemical, LLC
8309 Wilkinson Blvd./ Charlotte, NC 28214/ Phone: [phone] Fax: [phone]
www.emeraidmaterials.com

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 0001(e / SAMPLES COLLECTED DURING CALENDAR YEAR: -
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME L COUNTY
PERSON COLLECTING SAMPLE S) of r PHO ! O �41- &4,41V
CERTIFIED LABORATORY(S) ✓ Lab #
Lab #
SIGNATURE OF PERMIT -FEE OR DESIGNEE
_ REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
•
1.
II I
empto
ml'�Em�
I—lr�y'7L�lF!!I
I r r
r
I i
I
■o JffYA�
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?. yes kno
(if yes, complete Part B)
Fart 15: Vehicle Maintenance Acrfvity MOnttOrift Ke ulrementS
Oiitfallr '
=Date �n
r.
50050ti_
. ;._ �� :
00555 _ -
m53©- -'.
-00400
_
Total -Flow
r _
'Total
Oil &'Grease
Nan -polar µ
Total-
pia-w
New Motor
_ . w.
No -=- :
'Sample- =
Collected _
(lf :applicable)
Rainfall
{if apply
- -
O&PH
Gif
-..
Suspended
- -
OEI Usage -
w
(Method 1464
Solids
-
ySGT'ITEM), if
=
v
.Form SWU-247, last revised 21212012
Page 1 of 2

��`
� 4
' w,
I
�r
� •.
�� � '

1
STORM EVENT CHARACTERISTICS:
Date 03 03 lq
Total Event Precipitation (inches): O- ff
Event Duration (hours): g (only if applicable — see permit.)
(if more than one storm event was sampled)
Date C
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of tpep and imprisonment for knowing violations."
1 03 a?�
izwAture &ermi ee (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Emerald Carolina Chemical
8309 Wilkinson Blvd.
Charlotte, NC 28214
Attention: David Sikes
Project Name: Stormwater
Lot Number.-PC04044
Date Completed:03118/2014
7W_`11
Kelly M. Maberry
Project Manager
�``"9 � xccogo a
Ao
u
K '1
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 11
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Sc
SHEALY ENVIRONMENTAL SERVICES, INC.
NEIAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Emerald Carolina Chemical
Lot Number: PC04044
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Emerald Carolina Chemical
Lot !Number: PC04044
Sample Number
Sample ID Matrix
Date Sampled
Date Received
001
001
Aqueous
03103120141455
03/04/2014
002
002
Aqueous
03103120141458
03/04/2014
003
003
Aqueous
03/03120141503
03/04/2014
004
004
Aqueous
03/03120141511
03/04/2014
005
005
Aqueous
03103120141518
03/04/2014
006
006
Aqueous
03103120141525
03/04/2014
007
007
Aqueous
03103120141,935
03/04/2014
008
008
Aqueous
03103120141440
03/04/2014
(8 samples)
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: PC04044-001
Description: 001 Matrix: Aqueous
Date Sampled:0310312014 1455
Date Received: 0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1455
1
(COD) SM 5220D-2011
1 03118/2014 1950 AMM1
03117/2014 1630
1
(TSS) SM 254OD-2011
1 03/06/2014 1223 AMM1
41704
1
(HEM (oil and) 1664E
1 03/14/2014 1630 TOT
42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 52200-20
10
10
mg1L
1
TSS
SM 254OD-20
3.6
1.0
mg1L
1
HEM (oil and grease)
1664E
NO
4.5
mg1L
1
Footnote(s): "Tim McCorkle ARM
PQL - Practical quantitatlon limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J - Estimated result c PQL and a MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 4 of 11
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Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: PC04044-002
Description: 002 Matrix: Aqueous
Date Sampled:0310312014 1458
Date Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1458
1
(COD) SM 52200-2011
1 03/18/2014 1950
AMM1 03/17/2014 1630
1
(TSS) SM 25400-2011
1 03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664B
1 03/14/2014 1630
TDT 42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
37
10
m91L
1
TSS
SM 254OD-20
6.8
1.0
mg/L
1
HEM (oil and grease)
16648
ND
4.5
mglL
t
Footnote(s):**Tim McCorkle/ARM
PQL - Practical quandtation limit 8 - Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND - Not detected at or above the PQL , - Estimated result < POL and a MDL P - The RPD between two GC columns exceeds 40% N - Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W-
Shealy Environmental Services, Inc. Page: 5 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: PC04044-003
Description: 003 Matrix: Aqueous
Date Sampled:0310312014 1503
Date Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1
03/03/2014 1503
"
f
(COD) SM 5220D-2011
1
03/18/2014 1950
AMM1 03/17/2014 1630
1
(TSS) SM 2540D-2011
1
03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664B
1
03/14/2014 1630
TDT 42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
39
10
mg1L
1
TSS
SM 2540D-20
4.0
1.0
mg1L
1
HEM (oil and grease)
1664E
ND
4.5
mglL
1
Footnote(s): 'Tim McCorkle/ARM
PQL = Practical quantitation limit a = Detected In the method blank E - L1uanlitalion of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < POL and > MOL P = The Roo between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all Soil sample analysis are reported on a dry weight basis unless flagged with a W
Shealy Environmental Services, Inc. Page: 6 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com bevel t Report Q.7

Inorganic non-metals
Client:Emeraid Carolina Chemical Laboratory ID: PC04044-004
Description: 004 Matrix: Aqueous
Date Sampled:0310312014 1511
Date Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysis Data
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1511
1
(COD) SM 5220D-2011
1 03/18/2014 1950
AMM1 03/17/2014 1630
1
(TSS) SM 2540D-2011
1 03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664B
1 03/14/2014 1630
TDT 42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
20
10
mg1L
1
TSS
SM 254OD-20
8.6
2.0
mg1L
1
HEM (oil and grease)
1664B
ND
4.7
mg1L
1
Foolnote(s): "Tim McCorkle/ARM
POL = Practical quantitation limit B = Detected in the method blank E - Ouentitation of compound exceeded the calibration range H - Out of holding time
ND = Not detected at or above the POL J - Estimated result c POL and? MDL P - The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client:Emerald Carolina Chemical Laboratory ID: PC04044-005
Description: 005 Matrix: Aqueous
Date Sampled:0310312014 1518
Date Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1518 "
1
(COD) SM 5220D-2011
1 03/18/2014 1950 AMM1
03/17/2014 1630
1
(TSS) SM 254OD-2011
1 03/06/2014 1223 AMM1
41704
1
(HEM (ail and) 1664E
1 03/14/2014 1630 TDT
42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 5220D-20
54
10
mg1L
1
TSS
SM 254OD-20
39
1.0
mg1L
1
HEM (oil and grease)
1664B
ND
4.5
mg1L
1
Footnote(s): "Tim McCorkle ARM
9QL = Practical cluantitation limit B = Detected in the method blank E - Quanbtation of compound exceeded the catibrallon range H - Out of holding time
ND = Not detected at or above the PQL J = Estimated result < POL and a MDL P - The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W"
Shealy Environmental Services, Inc. Page: 8 of 11
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: PC04044-006
Description: 006 Matrix: Aqueous
Date Sampled:0310312014 1525
Dale Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysts Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1525
1
(COD) SM 52200-2011
1 03/18/2014 1950
AMM 1 03/17/2014 1630
1
(TSS) SM 254OD-2011
1 03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664B
1 03/14/2014 1630
TDT 42353
CAS Analytical
Parameter
T Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
34
10
mg1L
1
TSS
SM 254OD-20
9.7
1.0
mg1L
1
HEM (oil and grease)
1664B
ND
4.7
mg/L
1
Footnote(s): 'Tim McCorkle ARM
PDL = Pracdcal quantltalion Ilml1 a - Detected in the method blank E - Ouantitation of compound exceeded the callbratlon range H - Out of holding time
ND = Not detected at or above the PQL J - Estimated result a PDL and? MDL P = The RPD between two GC columns exceeds 40% N - Recovery Is out of crlteda
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a
Shealy Environmental Services, Inc. Page: 9 of 11
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: PC04044-007
Description: 007 Matrix: Aqueous
Date Sampled:0310312014 1535
Date Received; 0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1535
1
(COD) SM 5220D-2011
1 03/18/2014 1950
AMM1 03/17/2014 1630
1
(TSS) SM 254OD-2011
1 03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664E
1 03/14/2014 1630
TOT 42353
CAS Analytical
Parameter
Number Method
Result 0
P0L
Units
Run
pH - Field
SM 4500-H B
6.00
su
1
COD
SM 522OD-20
46
10
mg1L
1
TSS
SM 254OD-20
180
5.0
mg1L
1
HEM (oil and grease)
1664B
NO
4A
mg1L
1
Footnote(s): *:Tim McCorkle/ARM
PO4 - Practical puanbtallon limit B = Detected in the method blank E - Ouamtitation of compound exceeded the calibration range H - Out of holding time
No = Not detected at or above the PUL J = Estimated result < POL and? MDL P - The RPD between two GC columns exceeds 40% N - Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W"
Shealy Environmental Services, Inc. Page: 10 of 11
106 Vantage Point Drive West Golumbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Emerald Carolina Chemical Laboratory ID: PC04044-008
Description: 008 Matrix: Aqueous
Date Sampled:0310312014 1440
Date Received:0310412014
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(pH - Field) SM 4500-H B-2011
1 03/03/2014 1440
"
1
(COD) SM 52200-2011
1 03/18/2014 1950
AMM1 03/17/2014 1630
1
(TSS) SM 254OD-2011
1 03/06/2014 1223
AMM1 41704
1
(HEM (oil and) 1664B
1 03/14/2014 1630
TDT 42353
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
pH - Field
SM 4500-H B
6.5
su
1
COD
SM 5220D-20
70
10
mg1L
1
TSS
SM 254OD-20
5.3
1.0
mg1L
1
HEM (oil and grease)
1664B
ND
4.4
mg1L
1
Footnote(s): "Tim McCorkle ARM
POL - Practical quantitatlon limit B - Detected In the method blank E = Ouantitatien of compound exceeded the calibration range H - Out of holding time
ND - Not detected at or above the POL J - Estlmaled result r POL and > MDL P = The RPD between two GC columns exceeds 40% N - Recovery is out of c6tarla
Where applicable, all $oil sample analysis are reported on a dry weight basis unless flagged with a -W-
Shealy Environmental Services, Inc. Page: 11 of 11
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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106 Vantaye Pois,t Drive
I,Vest Cralumhia. South CCRmlina 79172
Telephone No. taG3} 791.9700 Fax Nof8,13} 791-9111
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unless other ;prrafr erriCnts are rrlBClr.
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SHEALY ENVIRONMENTAL SERVICES, INC.
$h"lyFn+imrRnrolnl5arsic ;.Ina.
Ucwumrnt Nur.,bw F-AL'-016
Rr- WnnM.inibet: 13
NgetofI
Replaers Daic OK•I p 13
F.IfrX13ve Due: 09 "2;111
// Sample Receipt Checklist (SRC]
Client: � }+..c71rf ii L.lfyli�y�a,,l. t"cxrler Inspcctod by.'tiate: �.�I I� Latit: _ i
Means of receipt: [. - SI ❑ Clicrlt ❑ UPS ❑ FedFat ❑ Airbclrne Lxp ❑ Othcr
Yes NO
1. WCr€ r"tudl ' seals present Oil We cuull7?
YCS No
2. If custody seals Wcrc present. were they intact turd unbroken?
Ctxwlcr ITN(lriginal temperaturc upon reset 1101erivcd (cornscted) temperature ur rn mccipt:
Mct tod:: ❑ Temperature Blank EPAgainst Bottles lit Gun ID. 4�3 IR Gun Comea-rion Factor:7L °C
Method of coolant: et ice a Blue Ice ay Ice ❑ None
If res ouse i3 No or Yes fur la, 15, 161, an ex lanatim,'resolution inurtl be ovided.
Yes ❑
No ❑
NA �
3. If temperature of any corpler -exceeded 6.0°C, was Prc1•j cct Manager notified?
� Y:'4>! uatificd by SRC, nhrane, note (circle one), other, _. (For
_
ceolcrs received via commercial euurirr, PMs are to be notilicd inimediylely.
Yes
:tio
❑
NA
4- Is the conuncrc.ial courier's packing slip attached 10 this form?
1`cs
0
5. Were proper custo mcr+lurrs (r*n ishetilreicivccl) follovcod?
Yes
❑�
Ku
NA
5a Were samples relinquished b • clirut to commercial courier?
Yes
No
h. Were son► le [Ds ligwd?
Yes
No
7. Was collection date & time listed?
Iles
No
8. Wcrc tests to bG performed listed on the COC?
Ycs ;
Nn
9. Did all sam t]es arrivr in the yoper containers foreacll test?
Yes
No
to. Did all container label infurmaiion (1P, date time a c with C()C ?
5'es
No
] 1. Did all containers arrive in gwd condition unbrukeu. lids on, etc.:?
1'c5
No
12. Wm adequate sam le ,volume available?
ycs
No
13. Were all samples mcvivc d within % the holding time ar 48 hours, whichever
comes first?
17cs
No
14- wele an v SII lcs containers missin "
Yes
No
15. Were there any excc.,:s Ram les not listed on COC? _
16, 'Wcrc bubbles preuml >"pea -size" (W'or 6mm in diameter) in,any VOA Ed
vials?
Ycs ❑
No ❑
N
Yes
No
NA ❑
17, Were ;ill rnGl.rils!O&G,'IIEhl:tnutrient samples received at a piT of � 2?
Yes
No
NA
18. Werr all c azMc and,'ar sulfide samples received at a pH >12?
I'ca El
NO 13
NA
Were all applicable NH3e1XK-,cyani&u hcnnl (41.2mg'L) samples free till
residual chlorine?
residual
Yes
NaEj
NA
24. Were collection temperatures docnrlienled on the COC for NC sans lus?
yc : []
No ❑
KA�_
21. Were client remarksfreyttests (i.e. requeyned dilutions,'MSAISD designations,
etc. , . I corrmtly transcribed from the COC into the comment section in LUVI-92
Sample. Preservation (Mu Lit be wmpleted for any sample(s) incorrectly pr•cstwvt:d or with headspace.)
_--were recrived incorrectly prq�scrved turd were adjusted
uccardingly iu sample rre -Mng with (14,904,1W0,,HCI,Nkj0H) with the SR 9 (number)
Sample(s) were rec ived with bubbles >6 mm in diameter.
5atnplC(s)_ _ - were received will' TRC >0.2 rig+1. fnr NI 13!
TKNlcyatltdel banal 1
Sam lc labels mrified Date;
Correetive Action taken if neceaaa 11
Was client. notified: Yet; ❑ No Did client rcbWnd. Yee ❑ Nit ❑
SLSI employee: Date of respcuxse:
(;nmrrtrllts: ��
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

F '.
ARAAENVIRONMENTAL
SERVICES, INC.
ASSESSMENT & REMEDIAL SERVICES
Mr. David Sikes
Emerald Carolina Chemicals
8309 Wilkinson Blvd.
Charlotte, NC 28214
Emerald Carolina Chemicals facility Charlotte, NC
Stormwater Qualitative Monitoring Requirements March 2014
For 1 st Semi -Annual 2014 Event
1- None 2-Faint 3-Moderate 4-Strong
Pipe 001 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 3.0 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-O. 15 inches/ 8 hours
Total Flow- 1,440 Gallons (based on the gallons per minute at time of sampling)
Pipe 002 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-O. 15 inches/ 8 hours
Total Flow-240 Gallons (based on the gallons per minute at time of sampling)
11164 DOWNS ROAD, PINEVILLE, NC 28134 / [phone] fax [phone] / www.armenv.com

ENVIRONMENTAL
A—RAASERVICES, INC.
ASSESSMENT & REMEDIAL SERVICES
Pipe 003 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 1 Gal per minute
Rain Event (Total PrecipitationlDuration of Event)-O. 15 inches/ 8 hours
Total Flow-480 Gallons (based on the gallons per minute at time of sampling)
Pipe 004 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-O. 15 inches/ 8 hours
Total Flow- 240 Gallons (based on the gallons per minute at time of sampling)
Pipe 005 outfail
Color- 1
Odor- 1
Clarity-1
Floating Solids-1
Suspended Solids-1
Foam- 1
Oil Sheen-1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-0.15 inches/ 8 hours
Total Flow- 240 Gallons (based on the gallons per minute at time of sampling)
11164 DOWNS ROAD, PINEVILLE, NC 28134 / [phone] fax [phone] / www,armenv.com

ENVIRONMENTAL
A-RAASERVICES, INC.
ASSESSMENT & REMEDIAL SERVICES
Pipe 006 outfall
Color- 1
Odor- 1
Clarity- 2
Floating Solids- 2
Suspended Solids- 2
Foam- 1
Oil Sheen- 1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-O. 15 inches/ 8 hours
Total Flow-240 Gallons (based on the gallons per minute at time of sampling)
Pipe 007 outfall
Color- 1
Odor- 1
Clarity- 2
Floating Solids- 2
Suspended Solids- 2
Foam- 1
Oil Sheen- 1
Flow- 1 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-O. 15 inches/ 8 hours
Total Flow- 480 Gallons (based on the gallons per minute at time of sampling)
Pipe 008 outfall
Color- 1
Odor- 1
Clarity- 1
Floating Solids- 1
Suspended Solids- 1
Foam- 1
Oil Sheen- 1
Flow- 0.5 Gal per minute
Rain Event (Total Precipitation/Duration of Event)-0.15 inches/ 8 hours
Total Flow- 240 Gallons (based on the gallons per minute at time of sampling)
11164 DOWNS ROAD, PINEVILLE, NC 28134 / [phone] fax [phone] / www.armenv.com