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HomeMy WebLinkAboutNCS000049_MONITORING INFO_20180824--STORIVIINATER-DIVISfON-CODING-SHEET-' PERMIT N0. DOC TYPE El FINAL PERMIT MONITORING INFO APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ YYYYMMDD Permit Number NCS000049 STORMWATER DISCHARGE OUTFALL (SDO) MO RING REPORT RIEO\lSAMPLES COLLECTED DURING CALENDAR YEAR* WGS4ZM GEN"TRAL FILES FACILITY NAME _IGM Resins n�LIOK SEG�t��` PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental Lab # 329 Lab # Part A: Specific Monitoring Requirements (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenburg PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE READ ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MG/L MG/L 001 8/02/2018 0.6 29 3.0 62 7.3 002 8/02/2018 0.6 15 8.4 300 7.2 003 8/02/2018 0.6 6.7 ND ND 7.1 004 8/02/2018 0.6 2.7 ND ND 6.7 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appi. Total Suspended Solids pH New Motor Oil Usage mo/d r MG inches m m unit al/mo Form SWU-247, last revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date _8/02/2018 Total Event Precipitation (inches): 0.6 Event Duration (hours): _3.0_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Scott Massey Plant Manager qklolix (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: William Gordon Project Name: SW Lot Number:TH02044 Date Completed:08/14/2018 M�fmz"-' 08/15/2018 9:54 AM Approved and released by: Project Manager: Kelly M. Nance The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (603) 791-9111 www.shealylab.com Page 1 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. 5C DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: TH02044 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. 106 vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: TH02044 Sample Number Sample ID Matrix Date Sampled Date Recelved 001 001 Aqueous 08102/20181100 08/02/2018 002 002 Aqueous 08/02/20181110 08/02/2018 003 003 Aqueous 08102120181115 08/02/2018 004 004 Aqueous 08/02120181120 08/02/2018 (4 samples) Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (B03) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID:TH02044-001 Description: 001 Matrix: Aqueous Date Sampled:08102I2018 1100 Date Received:0810212018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/02/2018 1100 MLK 1 (Temperature ) SM 2550B-2000 1 08/02/2018 1100 MLK 1 (SOD, 5 day) SM 521 OB-2011 1 08/07/2018 2052 AMR 08/02/2018 2333 12175 1 (COD) SM 5220D-2011 1 08/07/2018 0811 AMM1 08/06/2018 1742 1 (TSS) SM 25400-2011 1 08/08/2018 2056 AMM1 80116 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4600-H B-2 7.3 su 1 Temperature - Field (NC) SM 2550B- 29.9 ° C 1 BOD, 5 day SM 52108- 3.0 2.0 mgJL 1 COD SM 6220D- 62 20 mg1L 1 TSS SM 2540D- 29 1.4 mg1L 1 LOQ - Llmit of Quantitation B = Detected in the method blank E = Quantlation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.ahealylab.com Page 4 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID:TH02044-002 Description:002 Matrix: Aqueous Date Sampled:0810212018 1110 Date Received:08/0212018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/02/2018 1110 MLK 1 (Temperature) SM 255OB-2000 1 08/02/2018 1110 MLK 1 (BOD, 5 day) SM 521 OB-2011 1 08/07/2018 2052 AMR 08/02/2018 2333 12175 2 (COD) SM 5220D-2011 1 08/10/2018 0753 AMM1 08/09/2018 1737 1 (TSS) SM 254OD-2011 1 08/08/2018 2056 AMM1 80116 CAS Analytical Parameter Number Method Result 0 LOQ Units Run pH - Field SM 4500-H B-2 7.2 su 1 Temperature - Field (NC) SM 2550B- 29.1 ° C 1 BOD, 5 day SM 5210B- 8.4 2.0 mg1L 1 COD SM 5220D- 300 20 mg/L 2 TSS SM 254013- 15 3.3 mg/L 1 LOQ = Limit of Quantitation B = Detected In the method blank E = Quantitatlon of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% h = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shenlylob.com Page 5 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID: TH02044-003 Description: 003 Matrix: Aqueous Date Sampled:08102120181115 Date Received:0810212018 Run Prep Method Analytical Method Dllution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/02/2018 1115 MLK 1 (Temperature) SM 25506-2000 1 08/02/2018 1115 MILK 1 (BOD, 5 day) SM 5210B-2011 1 08/07/2018 2052 AMR 08/02/2018 2333 12175 1 (COD) SM 5220D-2011 1 08/07/2018 0811 AMM1 08/06/2018 1742 1 (TSS) SM 254OD-2011 1 08/08/2018 2056 AMM1 80116 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H B-2 7.1 su 1 Temperature - Field (NC) SM 2550B- 28.7 ° C 1 BOD, 5 day SM 5210B- ND 2.0 mg1L 1 COD SM 5220D- ND 20 mg1L 1 TSS SM 2540D- 6.7 1.0 mglL 1 LOQ = Limit of Quantdabon B = Detected in the method blank E = Quantitetlon of compound exceeded the natibrallon range ND = Not detected at or above the LOQ N = Recovery Is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Page 6 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID: TH02044-004 Description: 004 Matrix: Aqueous Date Sampled:0810212018 1120 Date Received:0810212018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Preo Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/02/2018 1120 MLK 1 (Temperature ) SM 2550E-2000 1 08/02/2018 1120 MLK 1 (BOD, 5 day) SM 521OB-2011 1 08/07/2018 2052 AMR 08/02/2018 2333 12175 1 (COD) SM 5220D-2011 1 08/07/2018 0811 AMM1 08106/2018 1742 1 (TSS) SM 254OD-2011 1 08/08/2018 2056 AMM1 80116 CAS Analytical Parameter Number Method Result Q i_OQ Units Run pH - Field SM 4500-H B-2 6.7 su 1 Temperature - Field (Ni SM 2550B- 29.0 ° C 1 BOD, 5 day SM 5210B- ND 2.0 mi 1 COD SM 5220D- ND 20 ni 1 TSS SM 2541 2.7 1.0 ri 1 LOQ = Limit of Quantftation B - Detected In the method blank E = Quantitation of Compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shoolyleb.com Page 7 of 12 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 12 0 N 9 3 Chalrf of Custody Record Shealy Environmental Services, Inc. 186 vwftOe Point brie West Columba, South Carolhna 29172 Telephone Ala. (BOSj 791.97Oo Fax No. (M3) 791-9111 %".Eheelylsb.Com NUmher czera 3GM PAO= Fort fb Confact Mom Gordon 9WnjW (PdrtW Nam QUOR Na. $ Teiaphona Na_ I Fir No. 0 Emsll Wafto NO, PAP of j CRY State zF code Char k*o NG PieSefvairvs 1. Urnpres. 4. HUM 7. NNOH 2. NaOWrzr A 5. HDL. 3. H2SN e. Na Thta. co f 1 NA NA NA NWw*r Gf cor"htese K D Boma "� �e 891i t Presanrae;ua xnrra oTH02044 5 a n PmAd NWAW F.ra Nmnber 1 >< sample IDiMaWplfan (ContainersFaROMsempls mey b4 oamboned an a m roe) dace TFn cvi DM!WW S a D I 001 ap G x x X x x X Ef' .��. 002 O x% x X X �'.� 003 s x ;' x x x x "%. -r • 004 r; x.= x x x x I G• T TO rum ArmW T]kne MwWh ad (Prixlab ap=cvWraqUvcc scr TAT) Ittaae (Rma9pmM l Semptra DJBFWel [ ROW-n to Cudd !1 La'b QC Requir�merrtg (Prase spadm Fiarartl 1 1 lore iaan �UnlesoMrn ' trr)tant 5y W►� y �a1 Tie 3 b 1. FLaufted by h� GE4+�'r ? Th"M 2. Rem by -VA-' 2. Rerairea 4y L-10% Time :W,O,dby late 3. Ftec Wd by owe rme4q bhad by Date 4. UbMAMF4eMJWad tar p Tune !! Note: All samples are retained for rsa[ w9eits from remlpt uMeas other Arran is ane made LAB USE ONLY Racsnrea on rce (Ctret{kj N lae Pedr R n3spt Terrrp. 7, Z s C Blank r {N ER� Dace oar xo�x r W m n m C O z m z D il— YI M M C_^ m CA z 0 SHEALY ENVIRONMENTAL SERVICES, INC. steGiv Em irenmenw $svica. lrrG Pape I of I Nk:=W Ncr ber, M70018C.14 E11hvfn,: Dart- a WI$ Sample Receipt Checklist (SRC) Client: 'T('M 'P.f51 n 5 Csioler lnsmuNd byNate: LY 01 Q •l`) g Lal 4. —r�A na6k Cl Means ofreceipt; E51 ❑ Clinai Lj UPS red . Ej Other: Ycs n 1. were custody seals present on the cooler? FQ Yes 'J No A 2. if custody seats wcm prcscnt. were tlt g intact and irtrhroken? pl I Strip lb: Chlorine Snip 1D: N rj9 Towd bv: TH rfghml tempei-attire upon receipt; Dcdvod (Correctt:d) tempemiure upon receipt %Sol' Snup-Cup ID: 4cthad:,r5iemperature Rlank ❑Against Bottles 1R Gun ID: 1R Gun Correction Factor: Il °C 4ethod i2r ccrirlant: 120'5'et ice ❑ lce Packs C Drylcc L None ❑ Yes ❑ No CIA 3. If temperahQe of any cooler exceeded 6.0°C, wEis Project Manager Notified? PM was Notified by: p]wur,; euuiil I ftwc—to-facc (circle nne). [ Yes :..1 No A 4. Is the commorcia] courier's packin slip allircdtod to this fonu? .•1'es Cl Na 5. Wert rimiper custody procodumii relinquislic(t'received) followed? SSC3 No 6, Wcre sore le 1D,9 listed tin the COC? Yr� © Na 17. Were sam le 1r-s listed on all sample containers? es ❑ No 18. Was colketion date fi.tirne 16l,x3 on the COO _ Yea 0 No 9, Was collection elate & iimc listcd on all sample containers? Yes ❑ No 10. Did all cantaincr label infounatton (113, dote, time) nffee with the COC? PU es ❑ No 11. Were tests to be performed listed on the COC7 R Yes f_I Nu 12. Aid all samplena arrive in the proper comainers for each test af1d+'or in go*d cunditiim (unbroken, lids on, etc.)? es ❑ Na 113. Was adequate Sample volume available? Yes 1% 14. A'nrs all sore les received withtn'�i the holding time or 49 haum, whielrcrcr comes first? .- Yes u 15. Wcru any samples containers mlRsinLexoess (circle one) sam Ica Not listcd on C'oc ? ❑ Yes 1_ .i No 21NA 16. For VOA and RSK-173 samples, wcrc bubbles pneseni >"pea-si re" (!/Vor 6nun ur diameter) in any aflhe VOA vials? t es No ` NA 17. were im r)Kt)imctals+nutrient sarst les received at a H oF<2? G Yes U No A 18. Were all eyaukk wmplcs received at a pli :;- 12 and Rulfide sore les teceived of a H =• 97 L;eYes ❑ No I.1 NA 19. Were Fill app to le NHs/TKN!cyanr Grp rno s mg sarnp es fr+pe of residual chlorine? iJ Yes ❑ No .DNA 1cormoly 20. %Va-c client retuarks rquests (i.e. reg wttod di(udcrns. M5+1viSD designaiions, etc...) trmiscribed from the Mc, into the comment section in LIMS? ❑ Yes No 21. �Vaa the quoto number listed on tfte container label' If cs Quote 0 Sample Preservation (Muse FA, completed for any sample(s) incorrectly prescr%-cd of widh Ilelidy=c) Sample(s) were received incorratly preserved and were Ousted ucc»rclingly in sample meiving with nil_ of circle (re: 142804, H+1U3,110. NaOI I using SR #.- tme of ppnervadon _ i rmoine Ihnn one preservative is needed. please note in the comments below. sample(:,) were receiYed.vith buhblos>6 mm in diameter. Sanrples(S) were received with TRC ? 0.5 mso. (U 419 i3 nu) and were adjusted accordingly in sample receiving with sodium thiosuifate (KarS,b,) with Shealy ID: 5R baroode labels applied by. Dace: _• Corrrrncyih: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Si1F,Ai(_jf M4:nvironnxentnl I "IGH.InC. ~�:100YdMagsPuintSki-a•'AWColurn.*50-AhCArrirleiil71l ••.• ., r• — Phote7Z}].�31.➢?uo•Iwrc Ml:!i 771,QIl1+�+rwrulradlylyFxcam William Gordon IGM - Resins 3300 Westinghouse Blvd.. Charlotte, NC 28241 IGNI - Resins Charlotte, NC Stormwatt-r Qualitative Monitoring Requiremonts 2018 2nd SetniMMual parent August 2, 2019 1- Aane 2-Faint Pipe 001 outfall Calm- 1 Odor- 1 Clarity- 1 Floating Solids- 1 Suspended Solids- 1 Foam- I Oil Sheen- 1 3-Moderate 4-Strong Estitated Flow: 0.3 GIs per minute 10.6 Inches Estimated Event,' Discharge ; 3.O fhs Estimated Total Flow : 90 GIs Pipe O92 ontfall Color- 3 Odur- 2 Clarity- 3 Floating, Solids- 1 Suspended Mids- Foarn - 1 Oil Shun- 1 Estimalud Flow: 1.0 GIs per minute! Il.6 Inches Estimated Event%Discharge : 1.0 jars F%tirmatad Total Plow: ISO GIs Shealy Environmental Services, Inc, 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Page I of 12 SHEALY ENVIRONMENTAL SERVICES, INC. IGM - Resins Charlotte, hC. Stonnwnter Qualitative Monitoring Rcquirements 2018 2nd Semiannual Evettt .august 2, 2018 1- A'unv 2-Faint 3-Moderate 4-Strong Pipe 003 ijutfal:ll Color- 2 Od(tr- I Clarity- 2 Floating Solids- 1 SuspendW Solids- l Foam- 1 Oil Sheen- I Estimu W Flow, 0.5U Uls pur minute j 0.6 Jnches Fstitualed Evtmtl Discharge: 3.p Hrs Estimated Total Flow: 90 Oils Pipe 4104 outfall Color- 1 Odor- I Claily- I Floating Solids- I SuLspended Solids- I Foam- I Oil Sheen- I KstimalW How ; 2.0 Ols per minute 10.6 lncltcs F-91imntcd Events Discharge, 3.0 Ilrs Estimated Total Flow: 360 GIs Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Page 12 of 12 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental_ Part A: Specific Monitoring Requirements RECEIVED Lab # 329 MAR 2 12018 Lab # r•I-N T RAL FILES DWR SECTION COUNTY Mecklenburg PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/yr MG inches MG/L MG/L MG/L 001 2/26/2018 0.21 ND 2.4 83 7.08 002 2/26/2018 0.21 12 2.8 99 7.17 003 2/26/2018 0.21 6 2.9 100 6.99 004 2/26/2018 0.21 ND ND ND 6.9 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m m unit al/mo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 2/26/2018 Total Event Precipitation (inches): 0.21 Event Duration (hours): 4.0_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Scott Massey Plant Manager cS/iz// e (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: William Gordon Project Name: Stormwater Lot Number:TB27039 Date Completed:03/05/2018 i 03/08/2018 2:13 PM Approved and released by: Project Manager: Kelly M. Nance The electronic signature above is the equivalent of a handwritten signature, This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: TB27039 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Inorganic Non -Metals 1 - The G-G associated with BOD batch 11879 was out of range at 151.6 mg/L (valid range is 167.5 — 228.5 mg/L). The associated BOD results should be considered invalid and only used for estimation purposes. Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www,shealylab.com Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: TS27039 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 02126120181052 02/27/2018 002 002 Aqueous 02126120181040 02/27/2018 003 003 Aqueous 02126120181020 02/27/2018 004 004 Aqueous 02/26120181025 02/27/2018 (4 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.00m Page 3 of 12 Inorganic non-metals gIient:IGM Resins Laboratory I D: TB27039-001 Description:001 Matrix: Aqueous Date Sampled:0212612018 1052 Dale Received:0212712018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/26/2018 1052 MILK 1 (Temperature ) SM 2550E-2000 1 02/26/2018 1052 MLK 1 (130D, 5 day) SM 5210B-2011 1 03/04/2018 1735 AJG 02/27/2018 2038 11879 1 (COD) SM 5220D-2011 1 03/01/2018 1522 AMM1 03/01/2018 1216 1 (TSS) SM 254OD-2011 1 02/28/2018 2111 AJG 65750 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H B-2 7.08 su 1 Temperature - Field (NC) SM 26608- 28.3 ° C 1 SOD, 5 day SM 6210B- 2.4 1 2.0 mglL 1 COD SM 5220D- 83 10 mglL 1 TSS SM 2540D- ND 1.6 mglL 1 aotnote(s):Lower than valid range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantilatlon of compound exceeded the calibration range ND - Not detected at or above the LOO N = Recovery is out of criteria P - The RPD between two GC columns exceeds 4D% H = Out of holding lime w = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 12 Inorganic non-metals Yient:IGM Resins Laboratory I D: TB27039-002 Description: 002� Matrix: Aqueous Dale Sampled:0212612018 1040 Date Received:0212712018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/26/2018 1040 MLK 1 (Temperature) SM 2550B-2000 1 02126/2018 1040 MILK 1 (BOD, 5 day) SM 521 OB-2011 1 03/04/2018 1735 AJG 02/27/2018 2038 11879 1 (COD) SM 5220D-2011 1 03/01/2018 1522 AMM1 03/01/2018 1216 1 (TSS) SM 254OD-2011 1 02/28/2018 2111 AJG 65750 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H B-2 7.17 au 1 Temperature - Field (NC) SM 25508- 27.4 ° C 1 BOD, 5 day SM 5210B- 2.8 1 2.0 mg1L 1 COD SM 5221 99 10 n i_ 1 T88 SM 25400- 12 4.0 mg1L 1 ootnote s :Lower than valid range LOG = Limit of Quantitation B = Detected in the method blank E = Guantltation of compound exceeded the calibration range ND = Not defected at or above the LOG N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5of12 Inorganic non-metals Client:IGM Resins Laboratory ID:TB27039-003 Description: 003 Matrix: Aqueous Date Sampled:0212612018 1020 Date Received:0212712018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/26/2018 1020 MLK 1 (Temperature ) SM 255OB-2000 1 02/26/2018 1020 MILK 1 (BOD, 5 day) SM 521 OB-2011 1 03/04/2018 1735 AJG 02/27/2018 2038 11879 1 (COD) SM 5220D-2011 1 03/01/2018 1522 AMM1 03/01/2018 1216 1 (TSS) SM 254OD-2011 1 02/28/2018 2111 AJG 65750 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H 8-2 6.99 su 1 Temperature - Field (NC) SM 2550B- 28A ° C 1 BOD, 6 day SM 5210B- 2.9 1 2.0 mg/L 1 COD SM 5220D- 100 10 mg1L 1 TSS SM 2540D- 6.0 2.0 mg1L 1 0o notes : I-G:G Lower than valid range LOQ = Limit of Quantitabon B = Detected in the method blank E = Quantitation o1 compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of orlteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab.com Page 6 of 12 Inorganic non-metals glient:IGM Resins Laboratory ID:TB27039-004 Description: 004 Matrix: Aqueous Date Sompled:0212612018 1025 Date Received: 0212712018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/26/2018 1025 MLK 1 (Temperature) SM 255OB-2000 1 02/26/2018 1025 MLK 1 (BOD, 5 day) SM 521 oB-2011 1 03/04/2018 1735 AJG 02/27/2018 2038 11879 1 (COD) SM 5220D-2011 1 03/01/2018 1522 AMM1 03/01/2018 1216 1 (TSS) SM 254OD-2011 1 02/28/2018 2111 AJG 65750 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H B-2 6.9 su 1 Temperature - Field (NC) SM 2550B- 27.7 ° C 1 BOD, 5 day SM 521013- ND 1 2.0 mg1L 1 COD SM 5220D- ND 10 mglL 1 TSS SM 2540D- ND 1.4 mg1L 1 octnote(s): 1-Lower than valid range LOO = Limit of Quantitation B = Detected in the method blank E = Quentitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPO between two GC columns exceeds 40% H = Out of holding time W a Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Page 7 of 12 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 12 0 ..y N E� Chinn of CuStWy Record Shealy Environ rental Services, Inc. 106 Yentapa Point Drive West Calumbla, South Carolina M72 Telep WM No. (W3) T91-9700 Felx lNo. (aO3) 791-9111 aww.shglylabwom Number u, Canrrcl Semler (Ar1+11ed N-w) Cudeft 131.1 Reams wow Gordan L. 4 Ada Tebphune No. 1 KiY Na 1 Ema! Yayg111 No. page j of 1 CLY State ZV Cade PresenmWe 1 1 NA NA NA NumberorCerltardn Chadalle NC; 1. Un rot 4. HW)S 7. NaOH 2. NBOMCnA a HCx K 0 adge projed 1 8 P�awvali,ia SW S. H2504 a. Na Ttdo. "ad *m4er RO NurLber Ma* S y g TB27039 ID f Desaiptlfltt sample (C;artiatrtera %r em* =q* my 76 Dale TI1M OW DW WW $ _ m Y ola fin C=bbW on Ce)Q C 8 RPM m o m A I 001 l; ib, G x x x x X1 x I A 7 3 r -W• " 002 0 x x x x x T 7"1 ` 4r QQ3 Ja2n G x x x x x G9 �8. 004 c I P x Y_ x x x x r, uMArau,tlTine Rqumd (Plrorlsb �wrcnd regWrec ror ftWdud TA7i Sample OISPesal OC RaW imemetb (Please Speedy) P—`ble Hazard Identmraman nad [JRm, F-40*1 ❑ Retum to OW ❑ Dbpesal by Lao Hand j F4014n2Ck ❑Sion Gritazrt Poben Unbw n 1. Flabnqulstxi y FSam D.2 ` 24- Trmc i r. - d by F li j, `}� 76 6 2. Ibesrgsaltt ed by r 2 T(me e� E . Z / • / / [S *I O �t ! . /� 6XV0 a. Reliriquiehed by pater Time 3. RP=WW by Dare Time �•Z7.iIL of 4. Reanqulshed by r e 4 i)WM d Bx TimCL,-- c� LIvats y r� NOW. All aamplm are re#sined for sbt weeks from receipt unleas other LAB USE aVLY R13 TM Bionic ! a mauls am rude Reamed on Ice (Clly�g Y H WeParac . � C C Y N c t Effective OWe Qti-27,2rt12 Z 0 SHEALY ENVIRONMENTAL SERVICES, INC. Shelly iinVinLpgxarYl 9arim. rxz Dmumcal Numbs: AIUIC-12 pl: l of l RF=Hye naic•,0l10't+2018 Sample Receipt Checklist {SRQ Client: Ci 1' Cooler Inspected byldate: [_i3rU i Lot y: 1 t [S i c1 Means of receipt: ;. SES[ OClicitit UPS ? [red[N DOther, _ [jfwZ;2rNoj 1. Nave custody steak prewriL an the emlet'l Yca l WNrt 'NA 2. 1f awardy seals were present were they intact turd wlbrokcii? T1 Strip TD f �.} - Chlorine Strip IrX i b ^� c+ _ Cooler TD f Origitral tenlpt:ratum upon rcccipt: Derived (C:orriected) lempenatum upon receipt: l I 'C . r ; -C, i. 5 *ir . a .l^°C b7�; _,LDS;°C method J;.;Ifftnpemturn Blank l pinst Rattles M Cttn 1D; try IIt Ciuu Cutttt lieirt Pac(c�r. �) �C: mor11ar1 at'aoolonl: e, Wet lot, Q Ice packs 0 Du Tce ❑ None L Yea ❑ No DNA 3• if temperature of any twulor encccdcd 6VC. µw Project Manager Notifled? PM was Notifieti by: phone i email ! face-to-face (circle one). .,: Yes No I A 4. I31ho colnmcrclirl courier's puAirig clip attm:hodto this forte? Yes L-1 No 5. Wwo pmprr custody procodurm (mlinquishcd;reccivcd) tollowed? Yes L-1 No 6. Wem bvmplc 09 listed on the COC? . :Yesl © Nol 7. li4em Gam to Ws listed on all gwnpic containcre? Yeas 11 No 3. Wo fill lection date & time iisieA fill the CAC? No 9. NVU callcction date & time limed on all sample containem? Py.yy,e,s C1 No 10. laid all container label infirr motion (11), date,time) agree withthe COC? . Nn 11. Womr tests to be performed lisped on 11w COC? Ymrl !-I No 12. Did all smnpiwi arrive in the prn[tercontainers for each teat and+or in good condition (unbroken, lids on, eta.)7 _ Yes _j No 113, Was aduquitic %tn Ic volume available? Yoe Cl No 114. Wmro All sanlplesreaeivad within �4 dtc holdirlgilme ot'48 hours, whichever comes first'! Y+rs a 15. Were any sam les conlaiate,s rniasinl{rmlttxg>,(circle one) sample+* Net listed on (A "i r3 Yes ❑ No WNA 16. Fur VQA and MK-175 sitinples, were huhhles present: "pea -size" ('110oi 61tim in diameter) in any of the VOA vials? cs U No LJ NA 17, Wom all DRtl;metal#nutrirnr samples received of a pH uP < 21 Yes No A 19. %Yore all cyonido samp ks i*xivr d tit a plT:• 12 an d sulfide sans les received at a pH � 92 j2rYes rt No 0 NA 19. NVerezdlapplicable NHa 1'IKNfcyarritic ptit:nv l < UrVQ sampler, free or tem A chlorin? Cl Yea C No LXNA 20. Wane client rernarlm. requests (i.e. requested dilutiuna, NIVNISO designations. etc...) cormtsly transcribed from the COC into the ct,inment m=tion in I.IMS'l Yea Uj 121. Was the qvvw Tr4mbcr used taken frorn the cmtAiner latml? ample Preservation (Must he eompletrd for any sample() irnurrertly prcl;mcd or with head space.) tunple(s) were moccived incoriluctly pieswvW and wury adjuutcd accordingly in satuple i ecciving with (I12SO4, iTNO3, HGI. Naf?H) using SR 4 ime of peusenFation , ainple(s) wer'a 3*ceived with huhhlcs *-6 min in diaracmr, antpl08) were received with TRC y 0.5 InWL (If tits is nv) and weir djusted mccoidu11;1y 41 winplu rumiving with sodium thiosultate (KazS:ins) with Shealy ID:. R barcode labels applied by: Clr 1)laIC: j Comments: Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Page 10 of 12 fr�� `1 3HFALIY Environmental Services, Inc. 106 Vantage Point Drive -West Columbia, South Carolina 29172 r Phone. 803,791.9700 • Fax 803.791.9111 - wwwjheatylab.com William Gordon IGM - Resins 3300 Westinghouse Blvd.. Charlotte, NC 28241 IGM - Resins Charlotte, NC Stormwater Qualitative Monitoring Requirements 2018 1" Semiannual Event February 26, 2018 1- None 2-Faint Pipe 001 outfall Color- 1 Odor- 1 Clarity- 1 Floating Solids- 1 Suspended Solids- 1 Foam- 1 Oil Sheen- I 3-Moderate 4-Strong Estimated Flow: 0.50 GIs per minute / 0.21 Inches Estimated Event/ Discharge : 4.0 Hrs Estimated Total Flow: 120 GIs Pipe 002 outiall Color- 2 Odor- 1 Clarity- 1 Floating Solids- 1 Suspended Solids- Foam- 1 Oil Sheen- 1 Estimated Flow: 1.0 GIs per minute / 0.21 Inches Estimated Event/ Discharge: 4.0 Hrs Estimated Total Flow: 240 GIs IGM - Resins Charlotte, NC Stormwater Qualitative Monitoring Requirements 2018 1' Semiannual Event February 26, 2018 l - None 2-Faint 3-Moderate 4-Strong Pipe 003 outfall Color- 2 Odor- 1 Clarity- 2 Floating Solids- 2 Suspended Solids- 2 Foam- 1 Oil Sheen- 1 Estimated Flow: 0.50 GIs per minute / 0.21 Inches Estimated Event/ Discharge : 4.0 Hrs Estimated Total Flow: 120 GIs Pipe 004 outfall Color- 1 Odor- 1 Clarity- I Floating Solids- 1 Suspended Solids- 1 Foam- 1 Oil Sheen- 1 Estimated Flow : 1.5 GIs per minute / 0.21 Inches Estimated Event/ Discharge: 4.0 Hrs Estimated Total Flow: 360 GIs March 12, 2018 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Re: February 2018 Stormwater Outfall Monitoring Report Dear Sirs, Enclosed you will find the February 2018 Stormwater Outfall Monitoring Report for IGM Resins USA, Inc. The analytical data from this sampling period showed no benchmark exceedances. Please contact Mr. William Gordon at 704-945-8725, should anything further be required. My contact information appears below, if you need to contact me directly. Sincerely, Scott Massey Plant Manager IGM Resins USA Inc IGM Resins Charlotte, Inc. 3300 Westinghouse Boulevard Charlotte, NC 28273 United States of America t: +1 704 945 8738 f: +1 704 945 8721 e: b.stegall@igmresins.com is www.iamresins.com September 12, 2017 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Re: September 2017 Stormwater Outfall Monitoring Report Dear Sirs, Enclosed you will find the September 2017 Stormwater Outfall Monitoring Report for IGM Resins USA, Inc. The analytical data from this sampling period showed no benchmark exceedances. Please contact Mr. William Gordon at 704-945-8725, should anything further be required. My contact information is shown below, if you need to contact me directly. Sincerely, 406�MA&l Scott Massey Plant Manager IGM Resins USA Inc IGM Resins Charlotte, Inc. 3300 Westinghouse Boulevard Charlotte, NC 28273 United States of America t: +1 704 945 8738 f: +1 704 945 8721 e: b.stegall@igmresins.com is www.igmresins.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental Lab #_329, Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenburg PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MG/L MG/L 001 09/01/2017 0.52 9.1 2.4 15 6.20 002 09/01/2017 0.52 7.1 4.1 13 6.37 003 09/01/2017 0.52 15 3.1 41 6.18 004 09/01/2017 0.52 2.7 ND ND 6.44 ,.�., �,�, �„ e Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Acti ity MonitoringRe uirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches MgA m unit gallmo Form SWU-247, last revised 21212012 Page 1 of 2 �Ito] 901VAalaYI<y:F41IIXTallli 4"IF3Ncc; Date _9/01/2017 Total Event Precipitation (inches): _0.52 Event Duration (hours): 4_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Scott Massey Plant Manager 9/r z/i7 (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: William Gordon Project Name: Stormwater Lot Number:S101045 Date Completed:0911112017 U�fxz-.-' 09/11/2017 3:42 PM Approved and released by: Project Manager: Kelly M. Nance LABORATORY kAE� ACCREDITATION t� BUREAU .mw.a wtr) ro ACCREDITEDwlictmss The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealyleb.com Page I of 12 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: S101045 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmerial Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www,shealylab.com Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: SIGIO46 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 08/31120171620 09/01/2017 002 002 Aqueous 08/31120171625 09/01/2017 003 003 Aqueous 06/31/2017 1634 09/01/2017 004 004 Aqueous 08/31/2017 1643 09/01/2017 (4 samples) Shealy Environmental Services, Inc. 106 Ventage Point Drive West columbia, Sc 29172 (803) 791-9700 Fax (803) 791-9111 www.sheMylab.com Page 3 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID: S101 045-001 Description: 001 Matrix: Aqueous Date Sampled:0813112017 1620 Date Received:0910112017 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/31/2017 1620 MLK 1 (Temperature ) SM 25508-2000 1 08/31/2017 1620 MLK 1 (BOD, 5 day) SM 521OB-2011 1 09/06/2017 1602 KNF 09/01/2017 1933 11550 1 (COD) SM 5220D-2011 1 09/07/2017 0953 MGM 09/06/2017 1251 1 (TSS) SM 254OD-2011 1 09/06/2017 2031 AJG 50749 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4600-H B 6.2 su 1 Temperature - Field (NC) SM 2550B-20 26.7 ° C 1 BOD, 5 day SM 521OB-20 2.4 2.0 m91L 1 COD SM 5220D-20 15 10 mg/L 1 TSS SM 264OD-20 9.1 1.3 m91L 1 LOQ = Limit of Quantitation 6 = Detected in the method blank E = Quantitalion Of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab.com Page 4 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID: S101 046-002 Description: 002 Matrix: Aqueous Date Sampled:0813112017 1625 Date Received:0910112017 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/31/2017 1625 MLK 1 (Temperature) SM 255OB-2000 1 08/31/2017 1625 MLK 1 (BOD, 5 day) SM 521 OB-2011 1 09/06/2017 1602 KNF 09/01/2017 1933 11550 1 (COD) SM 5220D-2011 1 09/07/2017 0953 MGM 09106/2017 1251 1 (TSS) SM 254OD-2011 1 09/06/2017 2031 AJG 50749 CAS Analytical Parameter Number Method Result Q LOQ Units Run pH - Field SM 4500-H B 6.37 su 1 Temperature - Field (NC) SM 255DB-20 27.0 ° C 1 BOD, 6 day SM 521 OB-20 4.1 2.0 mg1L 1 COD SM 5220D-20 13 10 mglL 1 TSS SM 25400-20 7.1 1.3 mg1L 1 LOQ = Limit of Quantitation B = Oatecled in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weVght basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.shealylab,com Page 5 of 12 Inorganic non-metals Client:IGM Resins Laboratory ID:SI01045-003 Description:003 Matrix: Aqueous Date Sampled:08131120171634 Date Received:09101/2017 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/31/2017 1634 MILK 1 (Temperature ) SM 255OB-2000 1 08/31/2017 1634 MLK 1 (BOD, 5 day) SM 521 OB-2011 1 09/06/2017 1602 KNF 09/01/2017 1933 11550 1 (COD) SM 5220D-2011 1 09/07/2017 0953 MGM 09/0612017 1251 1 (TSS) SM 254OD-2011 1 09/06/2017 2031 AJG 50749 CAS Analytical Parameter Number Method Result Q LOQ Units Run PH - Field SM 4500-H B 6.18 su 1 Temperature - Field (NC) SM 266OB-20 27.4 ° C 1 SOD, 5 day SM 621 OB-20 3.1 2.0 mg1L 1 COD SM 5220D-20 41 10 mg1L 1 T88 SM 254OD-20 15 1.3 m91L 1 LOQ = Limit of Quanutauon 8 - Detected in the method blank E - Quantitation of compound exceeded the calibration ranga ND = Not detected at or above the Loa N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Pax (803) 791-9111 www.shealylab.com Page 6 of 12 Inorganic non-metals Client:IGM Resins Laboratory I1):S101045-004 Description:004 Matrix: Aqueous Date Sampled:08/31/20171643 Date Received:0910112017 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 08/31/2017 1643 MLK 1 (Temperature ) SM 255OB-2000 1 08/31/2017 1643 MILK 1 (BOD, 5 day) SM 521 OB-2011 1 09/06/2017 1602 KNF 09/01/2017 1933 11550 1 (COD) SM 52200-2011 1 09/07/2017 0953 MGM 09/06/2017 1251 1 (TSS) SM 254OD-2011 1 09/06/2017 2031 AJG 50749 CAS Analytical Parameter Number Method Result 0 LOQ Units Run pH - Field SM 4500-H B. 6.44 Su� 1 Temperature - Fleld (NC) SM 2550B-20 27.3 " C 1 SOD, 5 day SM 5214B-20 ND 2.0 mg1L 1 COD SM 5220D-20 ND 10 mg1L 1 TSS SM 254OD-20 2.7 1.4 mg1L 1 LOG = Limit of Quanfitation B = Detected In the method blank E = Quanfitation of compound exceeded the callbratlon range ND = Not detected at or above the LOG N = Recovery Is out of cnterla P = The RPD between two GG columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.shealylab.com Page 7of12 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.ahealyleb com Page 8 o f 12 4 N m 0 V m m V 0 m x 0 V ti T f6 CD 4• m 3 eChain of CustoW Record Shealy Environmental Servion. Inc. 108 ardw r{ard DrWe West Cohimbia. South Cmotina 29172 Telephane No_ (803) 791-9700 Fax No (803) 791r9111 ■wws1wWb.mn Number chens twRohs Report to Owbd Gordon Isr (PMnw Name) Quole No. Telephone N0.1 Fax NA I Final WaYMNO. Pyp at 1 O9 ChMIoma srafs MC D I. Lkww 4. HNO3 7. ftDH . N owmak 3_ kCL 3. FiZJ04 � "Iihio. 1 1 NA NA MA NteOber Of Cardairulm K D Elasstp l�`� ��iist�y�,�bar 4 h. PMiw Mane raw 1 3 o a � 1.0 T4i Am n @ PrOJO4 V� Mbsr P. Num Mabix &emPlr D i Descelptlorl (Carters for each sample may t o ntM"ned OD One @n!} Data Tmie my OW VEnAr S O N � 001 �3 ,, G J. x x x x x xo 002 G x x x x x 003 G x x x x x 004 . j G x x x x x sum Time RwAw d 01"u Isb npp wwvcqunW fur AT} (Pleaoe5pndf� 7 SwnPIa Ospout ❑Re(utn to Cca+! ish PwMftMwft {phase Si5 -M P IdentiAraaon rO HFIaran aMe DSkrt lrtdairi son �U-I L OUVOrn 1 byf ji 1 l 1 �] Time y 1. � ` T.- 2. Re rgtsshad is 2. Q� 3. KoHwAAft* by Dam rnnn a1- f— 7.` a� Raft-AMMdby Date 1^� �r / T1me / r� 4. Re oa q Tkno 1 Mtn: AD samples am for sift wooks hoe„ ►sscelPt curlew other IL46 ME CW Sdr}@ oalvwd on !oe (cX+ec7s) r, N ke Pack � T 0 LOMP T N E ffmO a Date 05-Z7.2M2 Z n SHEALY ENVIRONMENTAL SERVICES INC. Roaly $NVtnmme W :Srrviom hie 179Nutrim[ Number: MEODISC-09 L'kK]ofi Effmiire Cate' 07-7VIO 17 Expn) Dow 07i2ar2022 Sample Receipt ChecWikit (SRC Clicnl: CmIer ltlipected by date: Means of receipt: p, n Client to UPS 0 FcdEx 0 011ter Ycs [3-1 Nn 1. Wcrc cusuxi_y seals prewit on the cooler? Ycs o No ❑ NA o 2. If custudv seals were present, were the ' Intact and Unbroken? pH strip ID- Cl strip [D: Cooler [D/Ori al temperature upon rcoeipt0cri►'ed (corrected) tempamfuru upon receipt: x r t_-Ij°c r �C i PC Method: perature B galnst Bottles IR (;,un ID: 1R Gun Currocn Factor: Method of caolanr. o< Ice o Blue Ice Cl Dry Ice o None Yes ❑ No o Tv:1 3. 1f temperature of any cooler cxtzcdcJ 6.0°C, was Project Manager Notified? PM was Notified by- Phone! email r face-to4we circle one). Yes ❑ No D AA 4. Is the eontmem>Gial murier's ackin sli aliachcd to this form? Ye No C- 5, Were pmr cos rowdurns Telir uishadlrecelved) followed? Ye$A,f No L, 6. Were sam le [Ds HOW on the COC7 Yes No Cl7. Were simple Ilh listed on all sample: containers? Yes No a S. Was collection date & time lislW Lin Qte COC7 Yes Nc ❑ 9. Was collection date & time listed on all %ample cnntaffim? Yes V No to 10. Did all cantalner label information ID, date, time agree with the COM Ycs No a 11. Were tests to be performed listed on the COC? Ye No 0 —No 12. Did all samples arrive in the proper containers for each test undror in good condition unbroken, lids o etc.)? Ya a 11. Wns ode uate sam le volume available) Yea o N 14. Werc all samples received within % the holdin lime or 48 Hours, whichever comes first? Yes a N 15. Were mny samples containers mis%ing/exaess (circle onc) samples Not listed on Ct C7 Yes a No a 16. Wane bubbles present >'"pell sige" 'I."nr 6mm in diarncicr in uny VOA vials? Yes o 0 NA o 17. Were all DRO/metats/nutrierl samples reccivcd at a CH of < 2? Yes o No t7 18. Were all cyanide samples received at a pH > 12 and Sulfide %am les received at a pH > 97 yes a No ❑ N 19, Were all applicable NH3.rrKNlcyanide!phenc11BNA (< 4.Smg/L) samples Brae of residual chlorin' Yes ,3 No ❑ NA 20. Were wlloa:tiein tem eratum documented on the COC for NC. sam IM? Ycs a No G N 21. Were client remarkslmqucsts (i.e, requested dilutions, MSIMSD designations, etc...) carrecay transcribed from the COC. into the comment section in [.IMS? Ycs rt N 22, Was tho quole number used taken from the container label? Sample Preservation ust be cam leted for an stun le s ijwArrectly preserved or %6h hcuds =. Saanplc(s) were received incorrectly preserved and were adjusted acensdingly in sample receivin with (1-12S,Q4- HNO,, HCI. NaOH) using SR 0 sample(s) were received with buhhles >6 ruin in diameter. Samples(s) wore rti=ived with 7'RC > 0.5 mg1L (If 1021 is Nu) and were adjusted accordlnglX in satn le receiving with tjodilml 1160suli4te NatS±Ut with Shealy 1D: SC Drinking Water Project Sample(s) pH verified to be <2 by Bate: sample(s) wcro Nol rme ived at a pH of c 2 and were all u+tted accordin .ly usinx SR# Sample labels ap liod by: Dote: Cornrntm Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Page 10 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. SH" ��+ rr `p Environmental F`J AL I t?1'YlOC9y I1tC+ 106 Vantage Point Drive • West Columbia, South Carolina 27172 [ 1 Phone. 803.791.9700 -Fax 803.791.9111 - www.shealoalaxom William Gordon IGM - Resins 3300 WestinAouse Blvd.. Charlotte, NCB 28241 IGM - Resins Charlotte, NC StorinwaLer Qualitative: Monitoring Rrquiremenls 2017 2"d Se;ttwannual Event Augmt 31, 2017 1-None 2-Faint 3-Moderate 4-Strong Pipe 001 out[all Color- 2 Odor- I Clarity- 1 Floating Solids- 2 Suspended Solids- -1 Foam- l Oil Sheen- 1 Estimated Flow : 0.50 GIs pex nlilmte 10.52 inches istimated Eveni/ Discharge : 4.0 His Estimated Total Flow: 120 GIs Pipe 002 outfall Color- 2 Odor- 1 Clarity- 1 Floating Solids-1 Suspended Solids- Foam- l Oil Sheen- 1 Estimated Flow - 1.5 GIs per minute J 0.521nches Estimated Evi nti Discharge : 4,t1 Hrs Estimated Total Flow, 360 013 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.sheaiylab.com Page 1 l of 12 SHEALY ENVIRONMENTAL SERVICES, INC. IGM - Resins Charlotte, NC Stonnwaber Qualitiative Monitoring Requirements 201? 2nd Semianrwal Event August 31, 2017 I- None, 2-taint 3-Moderate 4-Strong Pipe 003 outiall Color- 2 Odor- 2 Clarity- 2 Floating Solicly- 2 Suspended Solids- 2 Foam- I Oil Shctm- I Estimated Flow., 0.75 61.9 per minute ;' 0,52 Inches EstimateA Evend Discharge, 4,01drs Estimated 'Total Flow: 180 019 Pipe 004 outfall Color- 1 (Mor- I Clarity- 1 floating Solids- 1 Suspended Solids- 1 Foam- I Oil Sheen- 1 Estimated Flow. 2.0 GIs per minulc 10.52 Inches Estimated Event/ Discharge: 4.0 Hrs Estimated Total Flow: 480 GIs Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 12 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental Lab #_329 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenburg PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MG/L MG/L 001 09/01/2016 0.85 13 10 48 6.79 002 09/01/2016 0.85 37 2.6 16 6.81 003 09/01/2016 0.85 6.3 2.8 15 6.67 004 09/01/2016 0.85 6.6 2.7 14 6.17 ` Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity MonitoringR uirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m m unit gallmo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 09/01/2016 Total Event Precipitation (inches): 0.85_ Event Duration (hours): _3_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Scott Massey Plant Manager (Date) Form SWU-247, last revised 21212012 Page 2 of 2 September 15, 2016 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Re: October 2015 Stormwater Sample Dear Sirs, Enclosed you will find the September Stormwater Report for IGM Resins USA, Inc. The analytical data from this sampling period showed High TSS on outfall 001. This outfall was resampled twice, which is included, showed no high TSS. Please contact Mr. William Gordon at 704-945-8725, should anything further be required. My contact information is shown below, if you need to contact me directly, Sincerely, Scott Massey Plant Manager IGM Resins USA Inc IGM Resins Charlotte, Inc. 3300 Westinghouse Boulevard Charlotte, NC 28273 United States of America t: +1 704 945 8717 1: +1 704 945 8721 e: b.stegall@lgmresins.com is www.igmresins.com SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: William Gordon Project Name: Stormwater Lot Number:R102071 Date Completed:0811312016 Kelly M. Nance Project Manager r_ LABORATORY !ML� ACCREDITATION BUREA#1.,.,.,,. t ACCREDITED,no.urimu This report shall not be reproduced, except in Its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 7 106 Ventage Point Drive Wast Columbia, SC 29172 (803) 791-0700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. SC ❑HEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative iGM Resins Lot Number: R102071 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report, Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. It you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shenlylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: R102071 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 09101120161845 09/02/2016 002 002 Aqueous 09/01/20161857 09/02/2016 003 003 Aqueous 09/01/20161910 09/02/2016 004 004 Aqueous 09101/20161935 09/02/2016 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: R102071-001 Description: 001 Matrix: Aqueous Dale Sampled:0910112016 1846 Date Received:0910212016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prop Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/01/2016 1845 MLK 1 (Temperature ) SM 2550E-2000 1 09/01/2016 1845 MILK 1 (BOD, 5 day) SM 5214B-2011 1 09/07/2016 1932 KMR 09/02/2016 2031 10831 1 (COD) SM 5220D-2011 1 09/13/20161407 AMM1 09/13/2016 1037 1 (TSS) SM 254OD-2011 1 09/07/2016 0853 KWP 21417 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field T SM 4500-H B 6.79 T su 1 Temperature - Field (NC) SM 2550B-20 24.1 ° C 1 BOD, 6 day SM 521OB-20 10 2.0 mg1L 1 COD SM 522OD-20 48 10 mg1L 1 TSS SM 26400-20 13 2.0 mg/L 1 PQL = Practical quantitation limit 8 = Detected in the method blank E - Quantitation of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and 2 MDL P - The RPD between two GC columns exceeds 40% N - Recovery Is out of criteria Mora applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 9M Shealy Environmental Services, Inc. Page: 4 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sboalylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: R102071-002 Description: 002 Matrix: Aqueous Date Sampled:09101120161867 Date Received:0910212016 Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/01/2016 1857 MILK 1 (Temperature ) SM 2550E-2000 1 09/01/2016 1857 MILK 1 (BOD, 5 day) SM 521 OB-2011 1 09/07/2016 1932 KMR 09/02/2016 2031 10831 1 (COD) SM 5220D-2011 1 0911312016 1407 AMM1 09/13/2016 1037 1 (TSS) SM 254OD-2011 1 09/07/2016 0853 KWP 21417 CAS Analytical Parameter Number Method Result _Q PQL Units Run pH - Field SM 4500-H B 6.81 su 1 Temperature - Field (NC) SM 206OB-20 23.2 ° C 1 BOD, 6 day SM 521OB-20 2.6 2.0 mg1L 1 COD SM 6220D-20 is 10 mg1L 1 TSS SM 264OD-20 37 4.0 mg1L 1 PQL - Racket quentitafion Haig 9 - Detected In the method Wank E = Quentitation of compound exceeded the calibration range H - Out of holding Ilme NO a Not detected at or above the PQL J - Estimated result c PQL and > M DL P = The RPD between two GC columns exceeds 4a% N e Recovery Is out of criteria Mors applicable, all soil sample analysis are reported on a dry watght basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 5 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: R102071-003 Description: 003 Matrix: Aqueous Date Sampled:0910112016 1910 Date Received: 0910212016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/01/2016 1910 MLK 1 (Temperature) SM 255OB-2000 1 09/01/2016 1910 MLK 1 (BOD, 5 day) SM 52108-2011 1 09/07/2015 1932 KMR 09/02/2016 2031 10831 1 (COD) SM 5220D-2011 1 09113/2016 1407 AMM1 09/13/2016 1037 1 (TSS) SM 254OD-2011 1 09/07/2016 0853 KWP 21417 CAS Analytical Parameter Number _ Method— Result Q PQL Units Run pH - Field SM 4600-H B 6.67 su 1 Temperature - Field (NC) SM 2660B-20 23.9 ° C 1 BOD, 5 day SM 52108-20 2.8 2.0 mg1L 1 COD SM 6220D-20 15 10 mg1L 1 TSS SM 254OD-20 6.3 1.4 mg1L 1 PQL = Practical quantilation limit B = Detected In the method blank E - Quantitatlan of compound exceeded the calibration range H = Out of holding time ND - Not detected at or above the PQL J = Estimated result < PQL and > MDL P - The RPD between two GC columns exceeds 40% N - Recovery is out of criterta Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W' Shealy Environmental Services, Inc. Page: 6 of 7 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.bom Inorganic non-metals Client:IGM Resins Laboratory ID:R102071-004 Description: 004 Matrix: Aqueous Date Sampled:09/0112016 1935 Date Received:0910212016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/01/2016 1935 MLK 1 (Temperature ) SM 255OB-2000 1 09/01/2016 1935 MLK 1 (BOD, 5 day) SM 521OB-2011 1 09/07/2016 1932 KMR 09/02/2016 2031 10831 1 (COD) SM 5220D-2011 1 09/13/2016 1407 AMM1 09/13/2016 1037 1 (TSS) SM 254OD-2011 1 09/07/2016 0853 KWP 21417 CAS Analytical Parameter Humber Method Result Q PQL Units Run pH - Field SM 4600-H B 07 - su 1 Temperature - Field (NC) SM 25508-20 23.6 ° C. 1 BOD, 5 day SM 62108-20 2.7 2.0 mg/L 1 COD SM 6220D-20 14 10 mg1L 1 TSS SM 254OD-20 6.6 2.0 mg1L 1 PQL a Practical quanlltetlon limit B - Detacted in the method blank E - Quentitation of compound exceeded the calibration range H = Out of holding time ND a Not detected at or above the PQL J = Estimated result < PQL and ? MDL P a The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 7 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc, 106 Vantage Point Drive West Calumbla, SC 29172 (803) 791-9700 Fax (903) 791-9111 www.shealylab,com woo-gel/jee4s-mmAt MG-/8L (608) Xej 0018-W (E08) ME 9S 'el4wnlo3 -oul i ri R� Uhl h r •� t I I � r / •� E 1 I � i cr .I ISOM BAuO lulod QB%nUen 90l 'saaweS Il4U8wualnU3 AIMS rtl Rz m � cn m MCIm �b ra ±10 1 'ONI S33IAa3S -lVIN3WNOIIIAN3 A'lV3HS SHEALY ENVIRONMENTAL SERVICES, INC. Sh=l} ln:. Clicnt: -.�• t'age I ui' I 17Yac-1114nau (1741VAI)A PXPiq 11.1e: Qins'] D21 Sample Receipt Checklist (SRC ) -Cooler Inspected byldatc, ,;[V i gf1& I of 0: 12 :CO -- b i 1- Means orreceipl.: SITS[ ❑ Clicnt ❑ UPS ❑ FedEx ❑ Woos YcsI No 1, Were custody wily prewil oft the 000lcr' Yes LJ jNoUNA 2. If cusvAy nulls wcrc resent wcrc the • intact and ans. roken'? PH strip Ili:__ _ _ _ ('I strip 1D: N A Cvvlc-r IWOriginal temp mturc upon receiptiDerivcd Icarrcned) itmpm-mima upon receipt: `c, 1 aC 1 11 'G 'C: 1vMcthod: emprrtlllank A'Pillst BoLdes IR Oun ID: (a--IK(iunCori•cction F� c;Ior: Molhodofcooltlnt: ure Wet 1L'l' Q Blue lee ❑ Dry Icc ❑ Nale Yes ❑ No 11 AA 3. If L01uparulurc of any' cnoler excocdcd 6.0T, wua Project Manger n0l irieci'! NM was notified by: phonc i crimil! focc-lo•flice circle one). Yeas NCI El NA ff 4. Is the coilurtercinl couriir'y pocking slip attached to this forni? l'e�; No S, 1i4'Crr pro per oust tidy rorcduras rely ;ti8ltcdiaccivcd) frlllurwcd'.' Yu-1 No El 6. Were antrl IC IDs Ilsled on tllc CO ! Yes by 7. Were Sample IDS lisLed oil all eartiple cnniainers? Yc% No K. WAS ColICCtion date & flute Iiuwd on the CW? Ycl. NU _ 1 19. W ns collection date & time listed on all anti iv c0ntaiitorn? Y" Nu 10. Did all coiatainer Inbel itirornmtion f 10 date tittle a rec wilh (he COC? Y 1 Mi 0 1 11. Wcrc tests to be cl•fornied listed on the COC? Y . No ❑ 12• aid all salnl)ICS rttTiVC in the pl'UPCI cuntaincrs for cads test andror in good cvndition (unbroken lids on ctc. Yes No 13, Arab u ate sam le volumo gvailablo" Y1 ll 14. Wera all sn le9 rcccivcd witliin i4 the holdit tines or 49 hours, whichever comes first? Yes ❑ No 15. Were ally Samples containers misbina'cmess (circle one) samplers not IisIad on COC? Yes N41 NA I6. Wem bubbles resent61nm in dialncter in any 11n+1 vials? Yes Nu `4A lT. Were all mcts1s'0&G'KFMlnWrirnt cam leg ttiocivcd at o pH nr <2? Yrs No Q NA 1 tl. ware 41t c anidc an&or sul(idc sae lcs i•aclsiaed ai n H -12? Yo*' ❑ N"❑ vn ❑ M Wcrc all applicable Nl13fMN,cywflduphcnol (it7.2mk'L) samples li•co of csiduul chlorine? Yvs El No NA 0. Wcrc collection tam oritl.tircs docuinonted rn: the COC fan• NC sa lcs? Y, m ❑ ,4o ❑ NA 2 I. Wcrc client rclTmrkslrequcsts (i.c. rclucsted dilulions, MS,'MSD dcsigntuions, etc...) conrccily trajibcribed Crum, the COC into the comincnt section in LIMS? Yu� No :2. Wa€ the uolc ntunbei- used laken from the ennlainCr label? Sample Prewi- •B(no (Mtist be com)lctcd for any sanipltsl-;) incorrectly present d ur wish hcadxpace.) Sarnple(s) Carnplercicivilig went; received incorrectly prescrvcd and were adjusted accordingly in With I1,SQ IIN03, HC'I, NitOAT usin SR ii Samplelsi _ _ _ wcrc rvevived with bubbles --(s I= in diumigcr. Sampfes(s) _ sv= mccivcd with TRC >0.2 ing�L (Tree? I is No) and were a usl.ed occordirtly in su:liplc rcccivin with Sodium thiosulrato (Nn.Sj0A) wide Shealy ID:._ SC Drinkintr ►h/nl:r r'ro,lect Snmplc{g) pH .iciificd to be :12 by _ _ flute: Sarn I s mcre not received %_ a pH of Q and w•cro adjusted axortlirigly using Sli 4 Samlrlc Talmis upplicd Uy: %IcriGcd by: T)nl-.: fisLrlttmc�r ts: - - - Shealy Environmental Services, Inc. 106 Vantage Point Drive West.Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. rr ''� S HE AL E nvironmenhd it �, S1' Us, Inc. 106 Vantage Point Drive -West Columbi4 South Carolina 29172 � /� Phone 803.791.9700 - Fax 803.791.9111 - wwwshealylab.com Willimn Cordon IGM - Rcsins 3300 Wesdrighmace Blvd. Charlotte, NC 28241 IGM - Rc;sins Charlotte, NC Stormwater Qualitative Monitoring Requirements 2016 2" Semiannual Event Sep=ber 1,2016 1- None 2-Faial Pipe 001 outfall Color- 2 Odor- ] Clarity- 1 Floating Solids- 1 Suspended Solids- 1 Foam- 1 Oil Sheen- 1 3-Moderate 4-Strung Estimated Flow: 0.50 GIs per minute / 0.85 Inches Estimated Evente Discharge: 3.0 Hrs Estimated Total Flow: 90 Gis Pipe 002 outfall Color- l Odor- Clarity- 1 Floating Solids- 1 Suspended Solids- Foam- 1 Oil Sheen- i Estimated Flow: 2.5 Us per minute 10.85 Niches Estimated Event! Discharge: 3.0 Hrs Estimated Total Flow : 450 GIs Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com SHEALY ENVIRONMENTAL SERVICES, INC. IGM - Resins Charlotte. NC Stormwater QuAtative Monitoring Requirements 2111E 2nd Semiannual Event September 1, 2016 1- None 2-Faint 3-Moderate 4-Strong Pipe 003 outfall Color- 2 Odor- I Clarity- 2 Floating Solids- I Suapcndcd Solids- l Foam- 1 Oil Sheen- 1 Estimated Flow : 0.75 GIs per minute 10.85 Int;htz Estimated EvenvDischarge : 3.0 Hr1; Estimated Total Flow : 135 GIs Pipe 004 outfali Color-1 Odor- 1 Clarity- 1 Floating Solids- 1 SusptmJW Solids- 1 Foam- 1 O i I Sheen- I Estimated Flow : 7.0 GIs perminute / 0,93 Inches Estimated Even4'Mseharge : 3.0 Hrs Estimated Total Flaw: 1260 Gls Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com 9} .1 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Reid Smith Project Name: Stormwater Lot Number: RB03126 Date Completed:02/11/2016 Kelly M. Nance Project Manager LABORATORY Lck ACCREDITATION �',,., BUREAU . ACCREDITEDeaurinn This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shoolylab.com t SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: RB03125 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample, All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: RB03125 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 02103120161340 02/03/2016 002 002 Aqueous 02/03120161345 02/03/2016 003 003 Aqueous 02/03120161352 02/03/2016 004 004 Aqueous 02/03120161358 02/03/2016 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 7 106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: RB03125-001 Description: 001 Matrix: Aqueous Date Sampled:0210312016 1340 Date Received: 0210312016 Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/03/2016 1340 MLK 1 (Temperature) SM 2550B-2000 1 02/03/2016 1340 MLK 1 (BOD, 5 day) SM 521OB-2011 1 02/09/2016 1404 DMA 02/04/2016 1417 10395 1 (COD) SM 5220D-2011 1 02/11/2016 1012 BWS 02/10/2016 1836 1 (TSS) SM 2540D-2011 1 02/09/2016 0854 AMM1 96023 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4600-H B 7.34 au 1 Temperature - Field (NC) SM 26608-20 20.0 = C 1 BOD, 5 day SM 521OB-20 11 2.0 mg1L 1 COD SM 5220D-20 56 10 mg1L 1 TSS SM 2640D-20 32 6.0 mg1L 1 PQL = Practical quanfitation limit B = Detected in the method blank E = Quentitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and r MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 4 Of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fox (803) 791-9111 www.sheelylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: RB03126-002 Description: 002 Matrix: Aqueous Date Sampled1210312016 1346 Date Received, 02/03/2016 Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/03/2016 1345 MLK 1 (Temperature ) SM 255OB-2000 1 02/03/2016 1345 MLK 1 (SOD, 5 day) SM 521OB-2011 1 02/09/2016 1404 DMA 02/04/2016 1417 10395 1 (COD) SM 5220D-2011 1 02/11/2016 1012 BWS 02/10/2016 1 B35 1 (TSS) SM 254OD-2011 1 02/09/2016 0854 AMM1 96023 CAS Analytical Parameter Number Method _ Result Q PQL Units Run pH - Field SM 4500-H B 7.17 su 1 Temperature - Field (NC) SM 25SOB-20 20.0 " C 1 BOD, 5 day SM 521OB-20 2.1 2.0 mg1L 1 COD SM 6220D-20 12 10 mg1L 1 TSS SM 254OD-20 1s 2.5 mg1L 1 PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitetion of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result a PQL and > MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 5 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID:RB03125-003 Description: 003 Matrix: Aqueous Dale Sampled:0210312016 1352 Date Received:02/0312016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/03/2016 1352 MLK 1 (Temperature ) SM 255OB-2000 1 02/03/2016 1352 MILK 1 (SOD, 5 day) SM 521OB-2011 1 02/09/2016 1404 DMA 02/04/2016 1417 10395 1 (COD) SM 5220D-2011 1 02/11/2016 1012 BWS 02/10/2016 1835 1 (TSS) SM 254OD-2011 1 02/09/2016 0854 AMM1 96023 CAS Analytical Parameter Number Methog .. Result Q PQL Units Run pH - Field SM 4500-H B 7.21 su 1 Temperature - Field (NC) SM 2550B-20 21.0 ° C 1 SOD, 5 day SM 521 OB-20 ND 2,0 mg1L 1 COD SM 5220D-20 ND 10 mg1L 1 TSS SM 2644D-20 20 3,2 mglL 1 PQL = Practical cluantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result c PQL and > MDL P = The RPD between two GO Columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID: RS03126-004 Description: 004 Matrix: Aqueous Date Sampled:0210312016 1358 Date Received:0210312016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Data Batch 1 (pH - Field) SM 4500-H B-2011 1 02/03/2016 1358 MLK 1 (Temperature ) SM 255OB-2000 1 02/03/2016 1358 MLK 1 (BOD, 5 day) SM 521OB-2011 1 02/09/2016 1800 CLM 02/04/2016 1841 10396 1 (COD) SM 5220D-2011 1 02/11/2016 1012 BWS 02/10/2016 1835 1 (TSS) SM 2540D-2011 1 02/09/2016 0854 AMM1 96023 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 7.19 su 1 Temperature - Field (NC) SM 25508-20 21.0 ° C 1 BOD, 5 day SM 521OB-20 ND 2.0 mglL 1 COD SM 5220D-20 ND 10 mg1L 1 TSS SM 264OD-20 16 2.5 mg1L 1 PQL = Practleal quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out at criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W' Shealy Environmental Services, Inc. Page. 7 of 7 10e Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fox (803) 791-9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fox (803) 791-9111 www.shealylab.com 8 3 eol� SHEALY ENVIRONMENTAL SERVICES, INC. 91 SHFAL' Chain of Custody Record Tdephme hb.p803-791.9M u No. 990-79?9111 P*� WURVAtieafylab.com Number 51252 (wwf troop - gas'-+5 Fr1f =?lPLb►= A0_ %/�-- i' Tefaonon P& %F.mg f' ww" fyp, Adfsaa smnawrr, 8tiprawa �;++S.c r. A Wyats tN&VCh &t d MW *Me A A"*[q'� GAY 'tI' � }� IryCmia ` Q U r� s i C � p b RB03125 I Ramer Gbote� cn as l — PA*let hfa PC ANX rA f:C G i-Air9�fi ey P+wvvdirt r;�r 4--' it Mh r� MW w sumo W4M u e 7 ot!!r rfmp f Ig g : # k I 661 ab 2-1 Arewrd 16ria f7ngrNoraW jy7'r►Are srprpWJ q�rttl M 7r71 Svey.is f�4pt7tA1 9fandefa 1-: t9ued mpcotly) Im J R C-92v fRaf *L" �MB i{lrmr! Ibr+ W"hW J Rwama n 54in Irotar: I 1 Adnn URktmra aG fi801R1!'ralrfl� j�YraPj) . 7ile hpo"'w by !� C a- } 3 � rc,a 17. 2. f y Dsd9 rr„� 2. Ad"p-had by oars rrie z Raealea by Dab irae I adhq-*~ by film 78M 3. f awo ed by Data Tr+a ,,ft4'rgAWAdby f1we tans 4.LApOraWy li4iedby C?etc TNMe L 17 L40 USE ONLY /� �weiv�darr Gras i�1�►t ow sae Ph<a Racebt� -a-1—'G Note: All .:n we reta9d for four vmeJaorn maw 01—h-ss other afrdroa jmm ate now. MMMUf1UM WfWTE 3 YEILOWAEk M m f orM7 wiM Saqwh4W. PDX-Fhiv,! Copy DarmdafFfundcr. FADLJM €'rlfiOV00 fCOM-2 14 ch 2 m 1r z C X O ic m z n r M C_ m N Z n SHEALY ENVIRONMENTAL SERVICES, INC. ShalyEnviruntwital Survkz& Iac Dormeam Numhw.. NIFM l SC-Ul Pap t of 1 Ltrecliva Mac a V1fJ M4 Ex*y Date, 01AW103) Sample Receipt Checklist (SRQ Client: T (Tin '"Caolctsedbyldarc 1 6 Lul k: _7 Q Meansofreccirk 5B5I 0 Client ❑ ups ❑ redux ❑ other Yes Lj I No 1. Were cuss scull pircsent on the cooler? Yes tj I No U I NA Ld 1 2. if custot scaly wet: present, were tha itua4A and unbroken'! pH Arrip ID:_I S - CI strip TD: jt]A _ Oluler IDIC)ri&al temperature upon rrv, i l)erived (Corrected) temperature upon receipt: /$.I I °C r 1 —"C ! °C I l QC Method. Z Ternpemlur 13kilik ❑ Against Bottles IR (.lust ID: 4 I It Gttn Correction Factor: _o_ �c Method of coolant: Wet lce ❑ Blue Ice ❑ gg Ice: ❑ None Yes ❑ No i] NA .10 I If lemperature of any cooler exceedod bA°C, was Project Manta per notified? PM was natihod by phone/ email / face-to-faen circle ace). Y—es—r-TJ No NA 4, is the eottuncrcial �xwrier'ts packing slipattached to this IFarrn'.> Yes No El 5. Were grupci cusItody poxedures relit uishc&received followed? Yes No El NA 5a Were sainpics reflriquirthcd by cllew to commercial courier? Yes No 6. Were 4atn lc IDs listed on the COC? Yes No ❑ 7. Were slum lc We listed on all sample aunlaintxs`t Yes No A. Was collection date dt tiros listed c,n the COCY Yes No 4. Wes cnliaction date & time listed on all sample cvnlainex's? Yes Na 10. Did all coutainea label information @ date time) a with the COC? Yes Na t T . Were tests to be performed listed on the COC? Yes No 12. Did all test arrive in the containers 114vach test,' Yes No 13. Did all ocintainr� nrrivo in good condition unhnrk lids oil,etc,)? Y� No 14. Wass uate ram le voltutte mvilable? _ �, es No ❑ 15. Wtxe all samples tweivtad within'', the holding time or 48 holm, whichever col"M first? Yeti Np IG. Were an a les Containers miss)"? Yemt No 17. Were there an excess slam Ica not listed nn COU? Yes No NA 18. Were bubbles went -" -size" A"or 6rmn in diameter) in an VOA vials? Yes No NA 14. Were all tnetals/C) U/11EM nutrkrit sam lea received at a of <2? Yes No NA 20. Wen a all o tube andlar sulfide samples rtlnclved at a H 12': Yes ❑ No ❑ NA 21. Were all applicable WH: MNI/cyanid phenol (-0.2tngll,,) samples free of residual chlorine? Yes 0 No ❑ NA 22. Were collection teSwaturiw documejited on the COC for NC sam les? Yes ❑ No 9 NA 23. Wvrc client nemarks/requeals (i.e. requcsltad dilutions, MSAIASD designati ons, etc.,,) corTact ly transmibcd from the COC into theeotniumt section in LIMS? Yes Lj NoM 1 1 24. Was the uotc number used lakm from the: emktainer label? Sample Preservation (Must W completed for any aamplc(s) incorrectly prearved or wilts ltcadspace.) samples) were reoeived irx otroetly pmsenel attrl were adjusted accordingly in sample receiving with (H2SO4,11NO3, HCI, NcLOR) wing SIC # Samples) wee received with bubbles a6 mm in diantetex. Sample(&) were received with TRC >0.2 me. (if 021 is No) 3C Drinking Water Project Rarnplc(s) pH verified to be % 2 by Diner; sample(a) wwa not received at a pH of <2 and were adjusted accordingly using SR# Sample labels applied by:�� Verified by. Date ;v %! nts, Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. �-�Environmental SYMALL Servkes Ync. 10GVantagv Paint Ube -West Columbia, South Carolina 29172 Phone. 8+]3.751.47W • Fax. E03.391.911 f • wvir, shQBtylalb.cam Reid Sinith 1GM - Radius 3300 Westirghousa Blvd.. Charlotte, NC: 28241 IGM - Resins Charlotte, NC: 5t0rmwater Qualitative Monitoring Ret;u:rernalnts 2016 1st Seiniannual Fvtmt Fcbruary 3, 2016 1- ]None 2-Taint Pipe 001 outfall Color- 2 Oc1ur- 1 Clarity- 2 Floating Solids- 2 Suspended Solids- 2 Foam- 1 Oil Sbeen-1 3-Moderate 4-Strotlg Estimated Flow: 0.50 GIs perminW f 1.1 Liches Est'uluarod Fventl Discharge - 5.0 Hrs Estimated Total Flow : 150 GIs Pipe 002 nutfall' Color- I Odor- I Clal ity- 1 Nlod1bg Solids- 1 Suspended Solids- Foam- I Oil Sl een- 1 Estimated Flow , 1.5 (319 per mimitc 13 .l Inches Estimated Eventl Dischup : 5.0 His Estimated Total F14 1w : 450 G19 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com SHEALY ENVIRONMENTAL SERVICES INC. 1GN1- R oAns C:harIct c, NC Stonnwatar Qualitative Mattitwing Requirements 2016 1st Semiannual Evmnt Febiviiry 3, 2016 i- None 2-Filint 3-h4ndcrare 4-Sirnng Pipe 003 outfull Color- ? Odor- 1 Claiity- 2 Floating Solids- 1 Suspeaidcd Solids- 1 Foam 1 Oil Sheen-1 Fslinintri Flow: 0.50 GIs per mj;-,nte 11.1 inches Estimated 1 vmul Discharge: 5.0 Hrs Estimated Total Flow : 150 GIs Pipe 004 outfall Color- I Odor- 1 clarity- 1 Floating Solids- i Suspended Solids- 1 Foam- 1 Oil Sheen- 1 Estii imW Flow ; 4,0 Gla Tx7 minuwo' 1.1 Inuhcs Estimated Event/ Discharge : 5.0 Hrs EslitnatW TfAul Flow : 1200 G1.9 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-8111 www.shealylab.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _IGM Resins COUNTY Mecklenburg PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick PHONE NO. (704)945-8702 CERTIFIED LABORATORY(S) _Shealy Environmental Lab fCEW E FEB ���6 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Part A: Specific Monitoring Requirements CENTRAL FILES Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MG/L MG/L 001 02/03/2016 1.1 32 11 56 7.34 002 02/03/2016 1.1 19 2.1 12 7.17 003 02/03/2016 1.1 20 ND ND 7.21 004 02/03/2016 1.1 16 ND ND 7.19 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activitv Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/ddl r MG inches m m unit aVmo Form SW-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _02103/2016 Total Event Precipitation (inches): _i .1 Event Duration (hours): _5_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Scott Massey Plant Manager a//7/(a (Date) Form SWU-247, last revised 21212012 Page 2 of 2 December 16, 2015 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Re: October 2015 Stormwater Sample Dear Sirs, h cat coo q 9 RE!cE'IVED DEL 1 s.� uwR AI F14 oN RECEIVED DEC 18 ,,,j CENTRAL FILES DWR SECTION Enclosed you will find the October 2015 stormwater Report for IGM Resins USA, Inc. The analytical data from this sampling period showed High TSS on outfall 001. This outfall was resampled twice, which is included, showed no high TSS. Please contact Mr. Reid Smith at 704-945-8725, should anything further be required. My contact information is shown below, if you need to contact me directly. Sincerely, 40- Scott Massey Plant Manager IGM Resins USA Inc IGM Resins Charlotte, Inc. 3300 Westinghouse Boulevard Charlotte, NC 28273 United States of America t: +1 704 945 8717 f: +1 704 945 8721 e: b.stegall@igmresins.com ;1 is www.igmresins.com SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Andrew Brown Project Name:Stormwater Lot Number:QJ02038 Date Completed:10/1412015 Kelly M. Nance Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.ahaslytab.com Ll SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: 0J02038 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 7 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: 0J02038 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 10/02/2015 1200 10/02/2015 002 002 Aqueous 10102/20151209 10/02/2015 003 003 Aqueous 10/02/2015 1215 10/02/2015 004 004 Aqueous 10/02120151223 10/02/2015 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client: IGM Resins Laboratory ID: QJ02038-001 Description: 001 Matrix: Aqueous Date Sampled:1010212015 1200 Date Received:1010212016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 10/02/2015 1200 MLK 1 (Temperature ) SM 2550E-2000 1 10/02/2015 1200 MLK 1 (BOD, 5 day) SM 521OB-2011 1 10/08/2015 1253 HKB 10/02/2015 1013 10170 1 (COD) SM 5220D-2011 1 10/11/2015 1845 AEH2 10/08/2015 1451 1 (TSS) SM 254OD-2011 1 10/06/2015 0830 AMM1 86545 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 6.74 su 1 Temperature - Field (NC) SM 256OB-20 18.0 a C 1 BOD, 5 day SM 521 OB-20 4.3 2.0 mg1L 1 COD SM 5220D-20 59 10 mg1L 1 TSS SM 2544D-20 250 10 mg/L 1 PQL = Practical quantltation limit B = Detected in the method blank E = Quentitation of compound exceeded the calibration range H = Out of holding time NO a Not detected at or above the PQL J = Estimated result < PQL and y MDL P = The RPD between two GC columns exceeds 40% N a Recovery is out of critere Where applicable, all soll sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environments! Services, Inc. Page: 4 of 7 106 Vantage Point Drive West Columbia, SC 29W2 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Inorganic non-metals Client:IGM Resins Laboratory ID: QJ02038-002 Description: 002 Matrix: Aqueous Date Sampled:1010212015 1209 Date Received: 1010212015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 10/0212015 1209 MLK 1 (Temperature ) SM 2550E-2000 1 10/02/2015 1209 MLK 1 (BOO, 5 day) SM 52108-2011 1 10/08/2015 1253 HKB 10/02/2015 1013 10170 1 (COD) SM 5220D-2011 1 10/11/2015 1845 AEH2 10/08/2015 1451 1 (TSS) SM 2544D-2011 1 10/06/2015 0830 AMM1 86545 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 7.2 su 1 Temperature - Field (NC) SM 25508-20 18.0 ° C 1 BOO, 5 day 5M 521 OB-20 NO 2.0 mg1L 1 COD SM 6220D-20 26 10 mglL 1 TSS SM 254OD-20 17 1.0 mglL 1 PQL = Practical quentitation limit B = Qet&&ed In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and > MOL P = The l between two GC columns exceeds 40% N = Recovery Is out of criteria Whore applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services, Inc. Page: 5 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheaiyiab.com Inorganic non-metals Client:IGM Resins Laboratory ID:QJ02038-003 Description: 003 Matrix: Aqueous Date Sampled:1010212015 1215 Date Received: 1010212015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 10/02/2015 1215 MLK 1 (Temperature) SM 255OB-2000 1 10/02/2015 1215 MLK 1 (BOD, 5 day) SM 521OB-2011 1 10/08/2015 1628 HKB 10/03/2015 1246 10171 1 (COD) SM 5220D-2011 1 10/11/2016 1845 AEH2 10/08/2016 1451 1 (TSS) SM 254OD-2011 1 10/06/2015 1417 KML 86608 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 6.95 su 1 Temperature - Field (NC) SM 2660B-20 18.0 ° C 1 BOD, 5 day SM 52108-20 ND 2.0 mg1L 1 COD SM 6220D-20 22 10 mg1L 1 TSS SM 264OD-20 7.3 1.0 mg1L 1 PQL = Practical quantitabon limit B = Detected in the method blank E = Quanlilatlon of compound exceeded the cafibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria Where applicable, sit soil sample analysis are reported an a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:IGM Resins Laboratory ID:QJ02038-004 Description: 004 Matrix: Aqueous Date Sampled:1010212016 1223 Date Received: 1010212015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 10/02/2015 1223 MLK 1 (Temperature ) SM 25508-2000 1 10/02/2015 1223 MLK 1 (BOD, 5 day) SM 521OB-2011 1 10/08/2015 1628 HKB 10/03/2015 1246 10171 1 (COD) SM 5220D-2011 1 10/11/2015 1845 AEH2 10/08/2015 1451 1 (TSS) SM 254OD-2011 1 10/06/2015 1417 KML 86608 CAS Analytical Parameter NumberMethod Result Q PQL Units Run pH - Field SM 4600-H B 6.8 su 1 Temperature - Field (NC) SM 25SOB-20 18.0 ° C 1 BOD, 5 day SM 521OB-20 ND 2.0 mg1L 1 COD SM 6220D-20 19 10 mg/L 1 TSS SM 254OD-20 1.6 1.0 mg1L 1 PQL = Practical quantilation limb 8 = Detected in the method blank S = Quentitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J - Estimated result c PQL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all sail sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 7 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-970o Fax (803) 791-9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com sCn 4� C1 9 m m� m• T 3 3 v� WN v m � 0 3 a n c a N m N CWA f NPUiES Chain of Custody Record Shealy Environmental Servioes, Inc. 106 Varblage Point Drive West Columbia, South Carolina 29172 Telephone No_ 80-791-9700 Fax No. &03-791-9111 vninv,6 IyWCGre Number 37201 1 1JJ Report to cWtant sampler (Printed Name) � �. f �,t'I Quote Flo. Address Telephone No. EmIdl =lsld Parmelee (ua, pH, ramp, D4)osn b0 .*W d balsa ftge J _.•_ of L C/py� 4.t"' Stags fry Zlp [loos Pr usarveliva i.Htta] �i & 3. H250+1 6.802W.• li Mals „w �, < I + r.+q N,an6aol(aordslaeas 4lodernor Prtk �3dm Nam r w Mm=nWjm 0.% on& or,M j i I t1�� � iL �j fp Ff QJ02038 lr1•�' T f Pmjed NL:etti¢t P,ONtumber a t 3 :, ~ a i� Malrilt GW Ili wvrK* 5=5p1d ase�ree]of t]eara¢tfon fibre awn s Cdloftn pads � jr CogecciEon rowU Isunw i - 2, 1 �-"� FInW`FWD 2 sw i Tina O=nd -lam ftgr WJfttr r lab a$paara for -M ndwd a Furst►(.- bean .4podPrl Samlxe Otspeset ra rs" tDa F d Ql�asar d, lab w Requi--%- Ls (Sp�Y) P sma FT—wd Iderdi$rs�an •Ftaaid oFkmemie q.�1n Mnt C FMM Cthiatolm T. d L0Wj by) Sampler r� Date l-1-- -Ime 1. RecekW NJ Date /u&�J— Time r 3-'h— 2 Fiet>srq�n t:atb Time 2 Rooerved by Dabs Tiros 3. Rdpptdshed by Date rM 3_ ReaeFued by 1 Drle Time 4. ReingtFshed by Dst9 Title 4. l ebor>aWowy Raeived Date 'fnm Norte: All samples we retainod for Four weeks tram rec�L�t artfeas other aryl eatenla are matte w L48 ISE ONLY / }dbrsdred an tm ptYii -:)No d toe t'saR Tarp �. 'C Te.P. aantc'41 7 N 0WLn•W PI mlrr-r-16732 rw a 11 t Z r m C_ 0 M Cn Z 0 SHEALY ENVIRONMENTAL SERVICES, INC. 5ficcty Eorkantneoeat &n laea, lne, DaftnaniNambW MIA9IRC•01 SainpIc Receipt Checklist (SRC) Cheat: Cooler insperted byfdate: A&' A1—XX.r,_ Lot poor. I ar I Roptncec Daz 09+'i s S '- ti mlivo LIOW (41)U.'I S Means afreceipt: JTsrsi Q Cli_cat ❑ ups ❑ Fedix ❑ Other Ycs UJ No 1. ti�►ere CU9_tAd seals )resent on the 000la7 Yes U I -No NA 2. If custoi seals =a pment, Wom thuy intact and unbrokca? pli scrip 1D: 15 —164 51 „ Cl strip Ili: _ Cooler MfOirliginai temperature upon frc-eciptfDcrivcd (oorrected) temperature upon receipt; Method; 2rempemmirc Plank ❑ Against ldottim iR an ID: G 1R aunC:otrectipar IF -actor; , 6 °C Method of coolant: Wet Ice Q Bluc Ice ❑ Dry fee ❑ Non* Yra © No ❑ NA 3, jr tc aipcaaturc of any emler exceedetl 6.0°C, was Project Manager notified? PM notified by SRC, pltottr, iiutu (cirulc one), nther: (For eoobars received via oolimereini courier, PlAs are w be notiticd immodiatcl .) Yes No El NA 4. Is the commercial courier's packing slip attached to this furiit? Yes 16 No LJ J, S. Were proper custodl prareduraa tell ulsh t rvcc Foflowcd? Yes NCO NA E Sa Were satn lea relin uWied by cRejit toccirnmcircial eonrier? Yes No 6. Were sample IDs listed on the COV Yes 0Nc ❑ _ 7. Wcrc Sam la Ills IlAteii t at a Kam le vuntamers- Yes No _ S. Was collection data & little listed on the COC? Yes NU JJ 1 9. WAR onllectirin dlte & time listed on all salt! Ic containers? You No 10. Did all container Ihbel information ID dot time) agree with the COC7 Yes Nu- 11. were teats to be performed listed on the COC? Yea _ Nn 12, Did all as less arrive ill the pro eomtaiiwm for each test? Yaa NO U Did all containers arrive :n d condition (unbroken lids on, ato.)? Yes Na El I M. Was ads ate gate la votuinc available? Yes Tie ❑ 1 S. Wert all salnplcs naeived Within eA the holding '.imc or 48 hours, whichever camcs firs t? Yes No 16, Want any scut lea containers knissia ? Yes ❑ Na 17. Were them My txt:ess sum Ics not listed on COC? Yes No NA I S. Wen btib cx rest:nt >" :a -size" iS"ar (,tttm in diameter In au VOA vials? Yrs No El NA n 19. Wcre all metelW0&(x41R.Mtmirrie tunp Ica received at a pH of <27 Yea Tin ri A 20. Were all eye ni do and+or sulfide samples rweived at a 1"T > 127 Ycs ❑ No ❑ ` NA 21. Were all applivablo NH3 7YVcyanidelphenol (c0.2me) sAmples free of residual chlorine? Yes ❑ No El 'RX12r 'RA 22. Were collection lcmperaturrs documented no 14e ( = for NC samples? Yes f_l No ❑ NA 1 23, W=client remarks1requests (i,c rcquaatod dilutions, M& SD designatiars, etc..,) oonvUl ' irlinsrsiibcd from the CXX into the cosument section in LIMS? Yes QI_NoC3 1 24. Was the quote number used takai fruity the container label? Sant le Prraervation (Must he complow%1 fur any sturtple(S) incorrectly ewrved nr with heads oa) sample(s) — wcroroocivcd inoorri:ctlypresterved and were adjusted accardin I in last~ le receiving with fIIySD4, IW03,1{CI, NaCH using SR B Sam !e a were received with bubbles >6 nun in diumulLiz. Sample(s) wt7o r+.'"ived wi(h TRC >6.2 m (if #21 to Nn) SC Drinking Water Project Sample(s) pH verified to bt q 2 by Date: Sam 1 s wm: not rc civud nt a pH of <2 mid were adjusted ne000;din usiu SRN Sample labels applied by: Verified by: Dales 0 oanttFrals,: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelyleb.com SHEALY ENVIRONMENTAL SERVICES, INC. Environmental SHEALY Services, Ine. 106 ventage Pn1nt Drive -West Columbia, South Cardina 29172 Phnne, 803, 791.9700 - fax.803.741.91 i 1 - www.shealylab.com Andrew Brown , IGM - Resins 3300 Westinghouse Blvd.. Charlotte, NC 28241 IGM - Rcsins Charlotte, NC Stannwater Qualitative Monitoring Roquirmnonm 2015 2'4 Seeniaztmual FVC11t October 2, 2015 1- None 2-Fttint Pipe 001 outfall Color- 2 Odor- I Clarity- 2 floating Solids- 2 Suspended Solids- 2 Foam- 1 Gil Sheen-1 3-Moderate 4-Strong Utimated Flow: 0.25 Gla per minute 1 1.1 Inches Estimated Eveot/ Discharge : 7.0 IIrs Estimated Total Flow : 105 C1g Pipe 002 outfall Color- 1 Nor- 1 Clarity- I Floating Solids- l Suspended Solids- Femi- I Oil Sheen- 1 kgdmated flow : 1.0 GIs per minute 11.1 Inches Estimated Pvent/ Discharge : 7.0 Un Estimated Total Flow: 420 GIs .1 . Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Environmental� ` Services, anc. 106 Vantage Point Drivc -West Columbia, South Carolina 29173. Phonc.803,701.9700 • Fax,803,791.9111 •wuw�.thaalylahrrlm IGM - Rcsins Charlotto, NC Stormwater Qualitative Monitoring Requirements 2015 2''d Smitiatuival Event October 2, 2015 1-None 2-Faint 3-Moderate 4Stmng Pipe 003 outfall Color- 2 Odor- l � Clarity- 2 Floating Solids- 2 Suspertdod Solids- 2 Foam- I Off Sheen- 1 Estimated Flow : 0.75 Gh parr minute I '1.1 Inches Estimated Event/ Discharge : 7.01Ira Estimated Total Flow: 315 01:4 Pipe 004 outfall C: )hyr 1 Odor- 1 Clarity- 1 FloWng Solids- I Suspended Solids-1 Foam- 1 Oil Sheea. 1 Estimated Flow, 3,0 Gls porminutu 11.1 Inches Estimated bent! Discharge : 7.0 Hrs Estimated Total Flnw : 1260 GIs Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com rA STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental_ Part A: Specific Monitoring Requirements Lab #_329. Lab # COUNTY Mecklenburg PHONE NO. (704)945-8702 �CEIVE REQUIRED PAGE 2.�EE OR DESIGNEE f� DLL, , - 1 li LUl Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements O.otfall ,. —ate D z. i;00530. ,a_:`: :00400�.� 3 .� o-k ' pSample s3 Col' le�cted TotaleFlow y - - ' `F 'k if:a Ilcable Rif ) T.otal, ,ry J�`"."an�'e'- ' ] Rainfall �' Ulf&G er ase '2 tAwy�a-.'. a 1' pl? )' y m Nati paler i O&G/TPH Total ; �' 'L S. L *..i 3 .R Su�s�ended pI1 f '�6 :New.Motor; �}sryiMethod 1664� .i..A'21i Solids' r 4 4 x�r . r 4 3,- g t r, ast msr�•. a is aC s�a�xn 0mo, 7 Form S WU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _10/28/15 Total Event Precipitation (inches): —f applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Scott Massey Plant Manager iz%/& h (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Andrew Brown Project Name: Stormwater - TSS Resample Lot Number:QJ29052 Date Completed:11/03/2015 Kelly M. Nance Project Manager g� LABORATORY n�C ACCREDITATION BUREAU k ACCREa1TEi mweimn This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist, Shealy Environmental Services, Inc. Page: 1 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.ahealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: QJ29052 This Report of Analysis contains the analytical resutt(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: QJ29052 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 10128/20151643 10/29/2015 (1 sample) Shealy Environmental Services. Inc. Page: 3 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client!IGM Resins Laboratory I13:0J29052-001 Description: 001 Matrix: Aqueous Date Sampled:1012812016 1643 Date Received: 1012912015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (TSS) SM 254OD-2011 1 11/02/2015 1507 DMA 88547 CAS Analytical Parameter Number Method Result Q PQL Units Run TSS SM 254OD-20 16 1.7 mg1L 1 POL = Practical guantitation limit B = Detected in the method blank E = Quantllation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J = Estimated result a PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 4 Of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. 51anly F.nvireweaurdu1 Service!, Me. Vu,wr.cul Nu n,t%y ; h1 FIX I SC-02 Ya�t I o: I Replace Duke: O 2201 Sample Receipt Checklibt (SRQ . Cvulas r)enpacted by! date: *^+ 10 I_ot #: Mcnm ofmccipt: [2"S1:51 ❑ Clicat ❑ UPS ❑ Fed&x [] Mier N'M No t 1, WIXU �uswd St:ul3 resernt on the cooler? Yea N-n _ NA 2. If custad - suals +vere present, were they intact And ttnhmken? I1H rllrill rD: '0i ___ . . Cl strip ID: NA _ Cooler IWOriginal Icrnperature upon receipt+llcrivcd (commlvd) I01)l►rxalureupon receipt: +'7 1 I QA °t 1 r "C r + °t" + 'C Mel,od; Ternperv, turn : lank Against Bottles Ili Gun 1D:__� , IR Gun Cmiection Factor: '.C: Method of coolant: Wct lee Blue lue< Dry Ica D Ncroe Yes ❑ Na, ❑ KA Er 3. if tcmperattlrcto( >1ny 0001e exceeded GA°C; was Pr•o,jeat Metriager• notified! Plti? i1oliiiud by SRC, phone, note (cimlccrrre), other: (Tor cooler~ nzvived via twinurcrcial aauricr, PNI9 arc to be notified irmncdiatcl '.) Yrc Uj NoLjr i A 4. rs the enmmcreial rnurica•'s packin slip urtuelied it) dib Rva., Yes NeO 1 1 Were pMjer mioctrody prmedures (rclin uishcdi'rovciv0d) fullciwW? Yes ❑ Nu ❑ M ff 5a Were samples relinquished by client to commercial courier? Yes No ❑ 6. Wera sample iDs listcd on the CUC? Yes Na 7. Were :;am le IDs listed on all atu : curjltdnv s? Yes No S, Was collection date & time listed on the COC": Yea No _. 9. Was ctol lection date & timr listed on all sartr is ountamera? Yea N4 0 1 10. Lyrd all cuntaing land iTi fim-ivati in(AD, date, tilde) a girm%ith the C? 1'cs No El11. WmItta to he 'at7ned listed on the CDC? yes No ❑ 12. Did allmiriplo urrice itl the ro er containers for each test? t Ycv No _ 13. Did all corrtainc�5 trtrivr: lit urad c,luditioa itlli]1'DiCE fide en, na.1? YCS Na rl 14. Was ad ate sam :c volurnc arailabir? Y Nu 15. VLJero all samples received within'i, thcholding time or 48 luxury. whichevrs cantles fir'stry 16. Wet•e an ' 9mn les comainers tnissin ? Yr Nu V Yes No 17. Were Owe any excess sarn les not listed on C:(.K,? Yes El Va NA 18.1�+cxc bubUlea rsetrt �" -sine" (''A"or 6mtn in diprnetcr in aii• VOA %dale'? Ti_ No NA l y, Wcrc all rnt�Jilw'C)eSe{irHFM+'nutrient sam les reoei❑cd at a l3 rt <Z; Yes Nu Mi _ 20, Were all cyanide anclior sulfide l;Kns ilm rewired at a pH >12? Yon ❑ Nu ❑ N, 21. Woe ull applicable NH 3,TKNI'r,}iinirle/phenol (<Um�IL) samples fro: of -. residual chlorindr Yes ❑ Na D NA 22. W=%:gllectiun tens erarures documented nil ihB COC for NC icy? Yes ❑ Nn ❑ NA i• Were cli(atl rtxre►,rky rurluestta (i.& requested dilutions, MSWSl) designations, rtn,,.) correci1l trajiscribod from the CGC into the cowAnent section in LIMS? 77ff Rom 124, Was the quole nuinber used taken frcnn the comainur label? Sample Pmaerration (MLmt bs oumpleted for ruiy sample(s) inen"eclly preverved or with ltcaclspact:.) Sulriple(s) __-- _ wee received inaorrectiy prescrvcd and were adjusted 8ccardingly it xam lcrtwtizving With ftSC4,1Tl+ O3, IiCI, NaOH) uship SR Saln >'lei s wererteceived with babbles')-6 rnm in diamctcr, Sato Ic(s) wtxurwvived with TRC'r0.2 mvjrL (li'#7.1 is: Nol SC Thinking Watcr Projoct Sample(s) pal verifiod lr hu >� 2 by _ Data Sato Icry were not rsxcivesl al a jill of<.2 and were ad uatcd at cnrdin 1 ttsin SRfr Sato le labels applied by: I Verifiecl by: DR4 !4,11ltlf Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SH'ALY ENARONMENTAL SERVICES. INC. SHLALy Chaim Of "StOdy Record TW O p N . =-i9 q sx MO. ec r919ltl Number 5 318 81 www shaWylab.cam tiara' M C6nriCf 72 kPt m9 Pt0.l c'� cA�' Ginn Xft a�xas '.'- �vnre ARuya's fJuiau� � N rnow apxe � rc�leq; IOU A. Pfnifx,YNafT.A ` __ > ra Ij�aj� �oi�e:i z+w a o ) �-us!nx rw X � �r QJ29052 Ey Pc=V.1We lj{r► � i F nrpa rD: Uesa�ph�n Dad TA+ir g fl �rrs4+obi•s�+sarcNncsbecc�Snx.+r�a�taej ��� � � T Taun wOrldd TfmB A�+quhad FPPisr be a rcgoll�f 7AiC s8 rr� t�l Q Palwn w ! %? Y t!aNr�q•�d-rx+o � ��� 2. HsGrq�4r_•f r d. hv&v 4: j D LbES gate' A f am are r�fafri64 far lour rrevrs .*rum receipt T _ Unfoo �r arxa.OPOncrls arr; made. it'. ki-A u i A lye f tzm'.I.." rmtk r � � —�'• + AC Angr i��;sib dji 'D! MrrtHatwd;hnnls L 31dn rfr.-xt I I F3pon� 7 tA�kacw Rams f..R rune . ty MAP i A Latl0f2 rjF FOX+fYf by Tkra LAB WE;iwy Ppeeft e , n m ,` --i . §� Na doe Nf* L52�tTrrfa • I C -----' - JXSTitlBUflk' M WkD F a YC_it W I:L--% r• 1a .W•+-WWy vM •%wsp' ,r, MKfaakl-C iew C.W i r: u an"e: ,.r.. �PpxafmfMJl�:•r�lf]-.53 �ra:f+in+l.7lo:d.�[�.i»�201J Z 3 Z n rn C 7 n z n SHEALY ENVIRONMENTAL SERVICES, INC. SHEALY Enviri)nment$1 Services, Inc. Andrew Brown TC'TiVI -Resins 3300 Westinghousu 131vd,. Charlotte, NC. 28241 106 Vantage Point Dmre - Wesl Columbia, South Carolina 29172 Phone.W:1.791.9300 • Fax.803.791.3111 - wwwsheaMab-mm 1GM - Resins Charlotte, NC Stormwater QuLitnlivc Monitoring Requirements 2015 Resatnple TSS . Cictober 2.8, 201 S ' 1- None 2-Vaint Pipe 001 outfall Color- 2 Odor- I Clarity- 2 Floating Solid~- I Suspend Solids-1 Foam - Oil ShcC11- I 3-Moderate 4-Strong Eytimnicd Flow: 0.50 GIs per minute ; 0.45 inches Estimated Events Disuharge . 14 Hrs P-sitimac:d Total Flow : 420 GIs a Outfall 001 was rommPIC11 tier TSS bwau$e. initial 2015 2'selziannu,al evcan wa<s over the benclunark. During the first collection it ix hclicved that the sample might have had natural accruing mattar such as lenves and dirt which caused it to be bias high for *SS during collection. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.corn IN STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental Lab # 329 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenburg _- PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _x no (if yes, complete Part B) Part B: Vehicle Maintenance Activity MonitoringRe uirements Ouffall `Da§e,�5 00 50 ..= '. yam_ ,�00556 4°_ ems" s� LQ0530' � 0040 = 0� '` `'$` ; NoM .. - r..Collected. Sas � ; � �TotalFlow : �� ifs able) `.Rainfall `T,otai � ,� :' °Oil `& Gr e" (if ap L): �Non�' ol� P O& - PH ETotalfN SuspendedF 4 PH.r ew Motor OBI Usage Y. . �F' � '� � 1.{,� �� ®�� -� 4�,.' �?'� ;�•- :�,� to �:E rs.� � �.��._�� X Imo/d/' ; aMG>t Of Tinchesa s m��. „ F`e�`.' `f �* nit _L - h"`aUmo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _11/19/15 Total Event Precipitation (inches): _1.15 Event Duration (hours): _6_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Scott Massey Plant Manager Z (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Andrew Brown Project Name:TSS -001 Stormwater Resample Lot Number:QK19050 Date Completed:11/25/2015 Kelly M. Nance Project Manager LABORATORY �@a ACCREDITATION BUREAU .�'� M ACCREDW Drwae "' This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist, Shealy Environmental Services, Inc. Page: 1 Of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: OK19050 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: QK19050 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 11/19/2015 0855 11/19/2015 (1 sample) Shealy Environmental Services, Inc. Page: 3 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shoslylab.com Inorganic non-metals Client:IGM Resins Laboratory ID:QK19050-001 Description: 001 Matrix: Aqueous Date Sampled:11/1912015 0855 Date Received: 1111912015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (TSS) SM 254OD-2011 1 11/23/2015 2038 DMA 90414 CAS Analytical Parameter Number Method Result Q PQL Units Run TSS SM 254OD-20 33 3.3 mg/L 1 - POL = Practical cluantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services, Inc. Page: 4 of 4 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fox (803) 791-9111 www.shealyleb.com o s CWI1 ! NFDES Chain of Custody Record Shealy Environmental Servioes, Inc. 106 Vw t p Point Drive West Columbia(, South Caroline 29172 Telephone No. W2491-9700 Fax No. 803761-0T11 www.s 18a44ab x= Number 37521 Chard - /1j1t 1. Report to pp Corlf A-ctl Sampler _ (Printed Name) (ha-vuz.L I L� Quota ND. Addraas Teleown W Field Param4fers (iEmail,e., pH, temp. E q can be raoQded nalow ge PaOf CKV state i.K ZIP Code Preservative I. ump". 4. HNOS 2, NoW Z� KI HTSN f, Sadkns Thosidh —4 S (a � NrudbercfCofaelrtBrs� OWAW rye: P.M k s.s-aas Paojed 00 O-J" Pramnntlm (use cock m im � � � � OK19050 *%^ �' r11Pr f Daf PA fWlrt PMallix a a r U dS U l ate' 4i r MV IHilf , , SaScfil Semple ID t Descrlptlon FAnWrarsfor eadlsarrrplan>aybe eOMWAd fm one IMP ems.-ua+ Dela wledFa, Tune imelay} 1 $fall rj� ' Remiedis I ii}Oi9Y !U Flrids 5te1t Finish Flnbh Start Firi>k Smrf f�Zg1 Un AmwO Time RaQiiaad (Prier Izb ;�$ea*rimd is espadre i116 5tsrdrard M Rush Peaa ypaofy} Semple o Rel,an m CM by Lob QC Fteq **meta tsp-dyl Paaft Hazard td alien mw IJFId= eb. DS dM idifrd OPOSM oUiaw m ,. F61nq byr 3 _- �� �a� •�� itwe if: �' ,.Received by �/— �e-�. 2_ ReN qukshed by dale Recsi ed by DsJ: Time 3 RemquLehed by Vaba The I Reoehmd by Date Tinge t, R by Dale % - / J Time fieceirerd 8 ofe. All plim are retained for four weeks from receipt union atbwarimingemw t8 are nee. LOS USE ONLY HOWN-adonCe fc" Z. r3.110 nlmPmrk Da:UrMaN1mr F4U�61V W I Z4 M C_ 0 M U) Z 0 SHEALY ENVIRONMENTAL SERVICES, INC. Shealy EnOommW Senicsy. Inc. Documt.Ir Nuo*cr! M.E301ar-W Para I of 1 Rcldaccs Data:09,1115 Erraova No; I0.AI 15 Sample Receipt Checklist (SRC) Client: Cooler Inspected byrdste: �V\mwS Lot 4: r 6 - sesi ❑ Client ❑ ups D FodEx ❑ other psp Nn 1. Were custod seals cat on the cooler? 2. If custtxi &eels were resent, were the intact and unbrokcn? D: Cl strip ID: Cools �IW`Original temperature upon receipt/Derivccl (corrected) temperature upon receipt: QC Method: emperatu�lank 0 A&mI Bottles IR Outt ID: �-0 IR Gun Correction Factor. b •C�^C Method of cuolunc L Wet Ice El Blue Ice 7 Dry Ice ❑ Ntme Yes ❑ No ❑ NA 3. !f temperature of any cooler exceeded 6,0°C, was Project Manager notified? PM notified by SRC, phone, note (circle one), other: (For coolers received %ia commercial courier, PMs are to be notified immediately.) Yea Va NA Lodr 4, is the cnmmercial courier's packing sli atmchcd to this form? Yes 21 NO 0 4, Wcrc w2cr cuotody proced1ures `relin uiahe&recei followed? Yea LN. 0 NA Ur Wcrc samples relinquished by client to commereW courier'? Yee a 6. Woe sa Ie IN listed on the COC? Yes v 7. Were Ram le i Ds listed on all lc contain=? Yes o 9, Was collectiem Mte die time listed on the COO Yes o ❑ 9, Was collection date & time listed on all sample containers? Yes o 10. Did all container label inforrtwtion ID des time ee with the COC? Yea o 0 I I . Were tests to be perfDrmcd )uteri on the COC? Yes o 12. hid all samples arrive in the c[ conlainers fur each tell? Yra calallo 13, Did all containers arrive in good condition !unbroken. lids on, etc,)? Yea Iff a 14. Was ad ate sam k volume available? Yes gr No ❑ 15. Were all samples received within's the holding time or 48 hours, whichever comes first? Yea No 16. Wtrc any samples containers inissin ? Yea No 17. Wcrc these any vxvAs sat des riot listed an COC? Yea No N-A.0 I & Wcre t+trbhlca seem >" -size" I r4"or 6mm in diameter in Orly VOA vials? Yrr Na —N—A-7 19. Were all mettalOO&6 HEK'nulrient sunpics roccivcd at a PH of <27 Yes No NA 20. Were all gMide andior sulfide samplm received at a pH > 12? Yes ❑ No ❑ NA 21 • Were all applicable, NH31TKNIcyan id4'phennI (<10.2mg1L) samples free of residual chlorine'd Yes Na NA 7 22. Were collection temperatures documented on the CDC for NC sn 1m? Yzm ❑ No ❑ NA 23. Were client remarks'requc3ts (i.e. requested dilutions, MS/MSD designations, etc... coTr atl trdu n)xd froin the C UCf into the. comment acc:timi in ISMS? Yes N8 Uri 24. Was the quolc number uvW takat from the container label? Sample Preservation Must becompLetcd For any serer 1 a) inwnwly preserved or wilb hm idopmoc.) Sumplc(s) were rcceivcd incorrectly preserved and were adjusted accardine in so rnple recei ' with ("04 HNO3, HC! NaOil usin SR # Sam 1 s were received ,,with bubbles ?6 mm in diameter. sure l s ware received with TRC -0.2 m �,. 11' 1121 iR No SC Dritildng Watcr Project Sample(s) pH verified to be ? 2 by Dates Sa s were not rcocived at a pl I of £2 and wcrc adjusted acomdi n l • ua' SR# Sample labels Madicd b : Val fled b : Date: C[rmrrrants.1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Andrew Brown IGM - Resins 3300 Westinghouse Blvd.. Charlotte, NC 28241 IGM - Resins Charlotte, NC Stormwater Qualitative Monitoring Requirements 2015 Resample TSS November 19, 2015 1- None 2-Faint 3-Moderate 4-Strang Pipe 001 outfall Color- 1 Odor- 1 Clarity- 1 Floating Solids- 1 Suspended Solids- Foam- 1 Oil Sheen- 1 Estimated Flow : 1.5 GIs per minute 1 1.15 Inches Estimated Event/ Discharge : 6 Hrs Estimated Total Flow: 540 GIs STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 RECEIVED SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from DEC 18 2015 the date the facility receives the sampling results from the laboratory.) FACILITY NAME _IGM Resins CENTRAL F11 ES PERSON COLLECTING SAMPLE(S) _Micheal KilpatricWWR SECTION CERTIFIED LABORATORY(S) _Shealy Environmental Lab # 329 Lab # Part A: Specific Monitoring Requirements COUNTY Mecklenburg-_ PHONE NO. (704)945-8702 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MGIL MG/L 001 10/02/15 1.1 250 4.3 69 6.74 002 10/02/15 1.1 17 ND 26 7.2 003 10/02/15 1.1 7.3 ND 22 6.95 004 10/02/15 1.1 7.3 ND 22 6.95 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if a 1. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m m unit al/mo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _10/02/15 Total Event Precipitation (inches): _l.I Event Duration (hours): _7_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Scott Massey Plant Manager /21/1,h.� (Date) Form SWU-247, last revised 21212012 Page 2 of 2 Permit Number4NC5000049 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT RECEIVED SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from MAR 31 2015 the date the facility receives the sampling results from the laboratory.) FACILITY NAME _IGM Resins CENTRAL FILFS PERSON COLLECTING SAMPLE(S) _Micheal KilpWMMSECTION CERTIFIED LABORATORY(S) _Shealy Environmental Lab # 329 Lab # Part A: Specific Monitoring Requirements COUNTY Mecklenburg PHONE NO. (704)945-8702 r7 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. :1 0 •_ ! T Rr Mli' •-�. / i w�',€..jyt}�, �L 't� ''-" jzy��'{ ^""ate f :gn..#4da�.. �E# $ }� _ I MF -2 lftff&Mo ,� .,"'T II I I I I II I I I I 1 I Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes, complete Part B) Part R- Vehicle Maintenance Artivity Mnnitnrina Rennirementc �OutfAll No. I - q�_. rF, fk �. ., _�i ?'�l:�.::, Sample Collected .-.� ... -S ., tT.Y. .1Lwa'-.:. ,d y.'�"K Tot 1 Flow = (Iftapplicable)_ +i 3 -L iiv�i-'`.�°r�'i&i'5..:_'"i."-.�.-� Tot 1 !Rainfall i Y`•'3d � � t .ix: V.?,3K� x:•i.s-..i'd Oil &Grease (if apply, .:O&G/TPH` i 1 � L -: �o:�!d�.�i�. �1 6� polar i' 1 c�� :a 1. '�ic'4'".-�k-'_,.i.H. 530 ,' W408 � 3 = '9 Total i ' a� (Suspended ��" .,-A ��-r&� �'�-.F:s�.._4_ �H = h 'r, >- #� h ' -' -z�r5�[r'.:y.��d':J� New°'Motor ,OlI?IJsage.,�, 6 .. H (•.� �'�'D'Yx: 7�:.eilficS_':S. 'qy�� '(�i���F ttl�7} .:.,af. 61 yiTYW.'H'., _ �xx,y� V �' mo/ddL .r., g F- -�T. "... MG�.s.� ��.�,. _� y �,�g'�r �y�� �� C - 'K;"�1F1 ;inches, � �re�z ygaq� L� rt+'.Na �. "�, m -_.a-. . ;�� 2 FRg— -- ,m �- 4 - � un>I't �.�._ � allmo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _03/05/2015 Total Event Precipitation (inches): 0.32 Event Duration (hours): 8.5 (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and b lief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, g includinthe popib ftynof ftnes and imprisonment for knowing violations." (Signature Bryan Stegall Plant Manager 3 2 to r 5 (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis lGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Reid Smith Project Name: Stormwater Lot Number:QC06044 Date Completed:0312412016 Kelly M. Nance Project Manager o� i This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, inc. Page: 1 Of 7 106"Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shaalytab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: 0006044 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the DAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,sheelylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: QC05044 Sample Number Sample ID Matrix Date Sampled _Date Received 001 001 Aqueous 03105120151142 03/05/2015 002 002 Aqueous 03/05/20151153 03/05/2015 003 003 Aqueous 03105/20151200 03/05/2015 004 004 Aqueous 03/05/20151210 03/06/2015 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab.com Level 1 Report v2,1 Inorganic non-metals Client:IGM Resins Laboratory ID: QC05044-001 Description: 001 Matrix: Aqueous Date Sampled:0310512015 1142 Date Received: 0310512016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 03/05/2015 1142 MILK 1 (Temperature) SM 25508-2000 1 03/05/2015 1142 MILK 1 (BOD, 5 day) SM 52108-2011 1 03/11/2015 1540 ANG 03/06/2015 1039 9747 1 (COD) SM 5220D-2011 1 03/16/2015 1542 AMM1 03/16/2015 1057 1 (TSS) SM 25400-2011 1 03/10/2015 1011 BLO 69584 CAS Analytical Parameter Number _ Method____ _Result Q PQL Units Run pH - Field SM 4500-H B 7.6 su 1 Temperature - Field (NC) SM 265OB-20 18.0 a C 1 BOD, 5 day SM 621OB-20 4.7 2.0 mg/L 1 COD SM 5220D-20 38 10 mg/L 1 TSS SM 254OD-20 31 2.5 mg/L 1 PQL = Practical quantlletlon limit B = Detected in the method Wank E = Quanbtabon of compound exceeded the calibration range H = Out of holding time ND = Not detected at of above the PQL J = Estimated result < PQL and g MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all loll sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 4 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: QC05044-002 Description: 002 Matrix: Aqueous Date Sampled:03105120151163 Date Received:03105/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 03/05/2015 1153 MLK 1 (Temperature) SM 255OB-2000 1 03/05/2015 1153 MLK 1 (BOO, 5 day) SM 521OB-2011 1 03/11/2016 1540 ANG 03/06/2015 1039 9747 1 (COD) SM 5220D-2011 1 03/16/2015 1542 AMM1 03/16/2015 1057 1 (TSS) SM 254OD-2011 1 03/10/2015 1011 BLO 69584 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 7.45 su 1 Temperature - Field (NC) SM 2550B-20 18.0 ° C 1 BQD, 5 day SM 621OB-20 2.6 2.0 mg1L 1 COD SM 52200-20 22 10 mglL 1 TSS SM 25400-20 16 2.5 mglL 1 POL = Practical quentitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding tlme ND = Not detected at or above the PQL J = Estimated result c POL and a MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 5 of 7 106 Ventage Point Drive West Columbia, SC 29172 (003) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: QC05044-003 Description: 003 Matrix: Aqueous Date Sampled:0310512015 1200 Date Received: 0310512016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 03/05/2015 1200 MLK 1 (Temperature) SM 255OB-2000 1 03/05/2015 1200 MLK 1 (BOD, 5 day) SM 621OB-2011 1 03/11/2015 1540 ANG 03/06/2015 1039 9747 1 (COD) SM 5220D-2011 1 03/16/2015 1542 AMM1 03/16/2015 1057 1 (TSS) SM 254OD-2011 1 03/10/2015 1011 BLO 69584 CAS Analytical Parameter _ - Number Methg Result Q PQL Units Run pH - Field SM 4600-H B 7.51 su 1 Temperature - Field (NC) SM 2550B-20 18.0 ° C 1 BOD, 5 day SM 52108-20 3.0 2.0 mg1L 1 COD SM 5220D-20 26 10 mglL 1 TS8 SM 26400-20 16 2.6 mg1L 1 PQL = Practical quantitation limit B = Detected In the method blank E = Quantitallon of compound exceeded the calibration range H - Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and � MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 7 106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: 0005044-004 Description: 004 Matrix: Aqueous Date Sampled:0310512015 1210 Date Received: 0310512015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H 9-2011 1 03/05/2015 1210 MLK 1 (Temperature ) SM 25508-2000 1 03/05/2015 1210 MLK 1 (BOD, 5 day) SM 521OB-2011 1 03/11/2015 1820 AMM2 03/06/2015 1616 9748 1 (COD) SM 5220D-2011 1 03/16/2015 1542 AMM1 03/16/2015 1057 2 (TSS) SM 254OD-2011 1 03/12/2015 1019 BLO 69799 CAS Analytical Parameter Number Method Result 0 PQL Units Run pH - Field SM 4500-H B 7.09 su 1 Temperature - Field (NC) SM 25SOB-20 17.0 ° C 1 BOO, 5 day SM 521 OB-20 NO 2.0 mg[L 1 COD SM 5220D-20 ND 10 mg1L 1 TSS SM 26400-20 2.6 2.6 mg1L 2 PQL = Practcal quantlat6on limit B = Detected in the method blank E = Quentillation o1 compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria More applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'^W' Shealy Environmental Services, Inc. Page: 7 of 7 106 Vantage Point Drive West Columbia, SC 20172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2,1 jodoU tene-I woo'qulAIe949'A,AM L 6-LGL (£o8) xBd 0%6-lU (908) UW OS 'B!gwnlOD tSGM enuQ lulad eBB"uBA904 'ou! '900INaS IeIuawuonAu3 A1804S > ti L C or rm ir E cb 13 I 1 '9 �, 18 I (06. �. 4%) �� sir Ifi�t a � geo Irss p� ` Coo 24 1 FArd pits o f�, J A® I p 0 L' �J�� ©ago e 1-4 � 0m �j3s i p z c w w OD 'ONI S33IAH3S -ld1N3WNONIAN3 A-lV3HS SHEALY ENVIRONMENTAL SERVICES, INC. Shady F}nvirrxnnerMal Services. Inc. DiXt"ent Namher. R-AD-016 Revisloe tkfnbcr. 16 Waclotl Reylatxs Mtg6 074SM EiiacriveDaft; I1i07f14 Sample Receipt Checklist (SRC) Client: —=Pn 11A Cooler Inspected by/dace e A�&77 T Lot 4. 5QQSO u u MCitnS of receipt: SESI ❑ Client ❑ LIPS ❑ FedEx ❑ Airborne Exp ❑ Uther Yes No 1. Were custcAy seals pruent an the cooler? Yos No Lj I NA 2. if custody seals ware present, were thoy irttsct and unbroken'? Cooler ID/Original temperature uponmcriptiDwivcd (exsrrec(od) eatnpnratute uryypon reuipc; ` . r 0C J �L......-.L.....--.�cc i I Uc J 1' Method: Temperature Blank ] Against 3ottles iR Gun W. #4 At Gun Correction Factor: Method of coolant BVot Ice ❑ Blue} lot Q Ury Ice El None Yes ❑ No ❑ NA 3, If temperature of Any cooler exceeded fi,M, was Pmject Manager notified? PM notified by SKC:, phone, note (circle one), other. (For coolers received via cornmerciai courier, Phis are to be notified irrlmediatel . Yes ❑Wv❑ NA 4. is the commercial couricr'e packing slip attached to this form? Yes No S. Were proper custody rocodures relict uished/received) follower. Yes No NA 5a Were samples relin wished b client to commercial courier? Yes No 6. Were sam le Ws listed on the COC? Yes No ❑ 7, Were sample IM listed on all sam le containcrs? Yes No U. Was collection date &time listed on the COC? Yes Nn 9. WA; rrlleatinn date & time listed on all sam is cuntaierpm? Yes No ❑ 10. Did all container label imfomiation 1D date time a with the COC? Yes No 11. Were bests to be Prformcd listed on the COC? Yes No 12. Aid al I seta les arrive in the proper containers for each test? Yes No 13. Did al I containers arrive in and condition unbroken, lids un, cu-.17 Yes Nn ❑ 14. Was adequate sent le volume available? Yes ff No ❑ 15. Were all samples rawived within A dw holding time or 49 hours, whichever comes first? Yes I No 16. Wcrc an sa les containers lttissiu ? Yes No 17. Were there an.y excess samples not listed on COC? Yes ❑ Nn NA ! R. Were bubbles m-scnt >" ea -sine" r't"or bmm in diameter in any VOA vials? Yes No 0 NA El 19. Were all metlals/O&GeMWnutrient ssm les received ate pH of <? Yea TI No C IAA CF 20. Were all cyanide andfor sulfide samples received at a pR >127 Ycs ❑ No NA Ze 21. Were all applicable N1-UrrKN/cyanidetpht-.no1(N.2mg/L) ,*mplec free of residual chlorine? Yes No NA 22. Were collection temperatures ducumentod tm the COC: for NC samples? Yes ❑ Nn ❑ NA 23. Were client rernarkstrequests (i.e. requested dilutions, MSJMS0 designations, etc... correctly transcribed fi= the LW. into the comment section in LIMS? Yea No 24. Was the quote number usnd takcu from the onntainer label? Sample Preservation (Must be completed for any Fample(s incorrmLly prelicrved of with beadspace.) Samples) Were received incorrectly preserved and we c adj uslyd accordingly in sam la T=ivin with H2S0a H14Ua HC1.Na0T1 LLsinA SR# Sam I s were received with bubbles >6 man in diameter. Sam I s were received with TKC; >0 2 m If # 21 is Tk1 SC Drinking Water Projea Samples) pH verified to be > 2 by Sam I S wcm not rote ived at a pH of Q and were adjusted accordinglyaccm-4ingly asinx SRO Sam le labels applied h ; 0 NA-.VcnCied by: Date: Comments: Shealy Environmental Services, Inc. 10q Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. " Environmental SHEALYi Services, Inc— 106 Vantage Potnt Dflw • West Columbia, South CalrolIt1a 29172 Mona. 803.791.9700 - Fax 803.7919111 - www,shea lyla boom Reid Smith IGM - Resin 3300 Wcs1in8h0UW Blvd - Charlotte, NC 28241 IGM - Rcsins Charlotte, NC Stormwater Qualitative Monitoring Requirements 2015 1't Semiannual Event. March 5, 2015 1- None 2-Faint Pipe 001 outfull Color- 2 Odor- 1 Clarity- 2 Floating Solids- 1 Suspended Solids- l Foam- 1 Oil Sheen-1 3-Moderate 4-Strung E,atimatcd Flow: 0 25 GIs per minute 10, 32 inches Estimated Event' Discharge: 8.5 Hrs Estimated ToW Flow: 127,5 GIs Pipe 002 outfaD Color- 1 Odor- 1 Clarity- I Floating Solus-1 Suspended SDlids- Foacn- 1 Oil Sheen- 1 Estimated plow: 1.5 Gls pern%inute 10.32 Inches Estimated Event/ Discharge : 8.5 Hrs Estimated Total Flow : 765 GIs Shealy Environmental Services, Inc. 10r; Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. IGM - Resins Charlonc, NC Stormwater Qualitative Monitoring Requirements 2015 110 Semiannual Event March 5, 2015 1- None 2-Faint 3-Moderate 4-Strung Pipe 003 outfal2 Color- 2 Odor- 1 Clarity- 2 Floating Solids- 2 Suspended Solids. 2 FOW11- I Oil Sheen 1 Wmatai Flow : 0.75 GIs per minute / 0,321nches Estimated Event/ Discharge, 9.5 Hrs Estimated Total Flow: 382.5 GIs Pipe 004 autfau Color- 1 Odor- 1 Clarity- 1 Floating Solids- 1 Suspended Solids- Faam- 1 Oil Sheen- I Estimated Flow : 2.75 GIs per minute +' 0.321nche-4 Estimated Event/ Discharg:: 8.514ra Estimated Total blow : 1402.5 GIs Shealy Environmental Services, Inc. 10q Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) Micheal Kilpatrick CERTIFIED LABORATORY(S) Shealy Environmental Lab # 329 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenbur PHONE NO. 704 945-8717 FSIGNATURE OF PERMITTEE OR DESIGNEE QUIRED ON PAGE 2. �I�LY="..A�Fia`S!•Y.r; 'I1 r '�. I I I ' " < •L'ivy�; yes'. I 1 1 ' � .i - _ _ s �'� sL K � 0 1 �k: ��`� ,V �;� EI I'm' 51111, II I' I 1 I 1 11 I' 1 I 1 II• I' I I ' ! 1 1 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _x no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements CENTRAL FILES DWR SECTION O� fa'll Dat 1. W005§6ik ``"; .. � ZZ [00530 :00400 No N 'tip "Sample : Collected Total�Flow (if�a 'licable 'Y' Total; Yt"Oilw Rainfalls "t Grease a I.0&GJfTPH PP ): " Nonpc►la Total K 1pH New Motor _ _,�� (Method 1664. �So idsrs lam` =-mm ,. �`aal/mo- Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 09/24/2014 Total Event Precipitation (inches): 0.28 Event Duration (hours): _8.0_ (only if applicable —see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possib ity es and imprisonment for knowing violations." o t" Mw 101-74LI (SignAturelof rmitt ) (Dat ) Bryan Stegall Plant Manager Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Reid Smith Project Name: Stormwater Lot Number: P124072 Date Completed:10101/2014 7qR_rV1y Keily M. Maberry Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: P124072 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative, The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page, Shealy Environmental Services, Inc. Page: 2 of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (603) 791-9111 www.shealylab.com Level 1 Report v2,1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: P124072 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 09/24120141250 09/24/2014 002 002 Aqueous 09124/20141300 09/24/2014 003 003 Aqueous 09124120141305 09/24/2014 004 004 Aqueous 09124120141310 09/24/2014 (4 samples) Shealy Environmental Services, Inc. Page: 3 Of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab,com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary IGM Resins Lot Number: P124072 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 001 Aqueous COD SM 5220D- 11 mg/L 5 001 001 Aqueous TSS SM 25400- 6.4 mg/L 5 002 002 Aqueous BOD, 5 day SM 521013- 4.4 mg/L 6 002 002 Aqueous TSS SM 2540D- 4.0 mg/L 6 003 003 Aqueous BOD, 5 day SM 521013- 2.2 mg/L 7 003 003 Aqueous COD SM 5220D- 18 mg/L 7 003 003 Aqueous TSS SM 2540D- 11 mg/L 7 004 004 Aqueous TSS SM 2540D- 3.9 mg/L 8 (8 detections) Shealy Environmental Services, Inc. Page: 4 of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Level 1 Repon v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: P124072-001 Description: 001 Matrix: Aqueous Date Sampled:09124120141250 Date Received:09/2412014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/24/2014 1250 MLK 1 (Temperature) SM 255OB-2000 1 09/24/2014 1250 MLK 1 (BOD, 5 day) SM 521OB-2011 1 09/30/2014 0906 ANG 09/25/2014 1041 9374 1 (COD) SM 5220D-2011 1 09/27/2014 1738 HMA 09/26/2014 2118 1 (TSS) SM 254OD-2011 1 09/25/2014 1614 AAD 56882 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 6.69 su 1 Temperature - Field (NC) SM 255OB-20 24.0 ' C 1 BOD, 5 day SM 521OB-20 ND 2.0 mg1L 1 COD SM 5220D-20 11 10 mg1L 1 TSS SM 254OD-20 6.4 2.0 mg1L 1 POL = PraeUeal quantitation limit B = Detected In the method blank E a Quentitatlon of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the PQL J = Estimated result a POL and a MOL P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria Where applicable, ell soH sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 5 Of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2, t Inorganic non-metals Client:IGM Resins Laboratory ID: P124072-002 Description: 002 Matrix: Aqueous Date Sampted:0912412014 1300 Date Received:0912412014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/24/2014 1300 MILK 1 (Temperature) SM 2550B-2000 1 09/24/2014 1300 MLK 1 (BOD, 5 day) SM 521OB-2011 1 09/30/2014 0906 ANG 09/25/2014 1041 9374 1 (COD) SM 5220D-2011 1 09/27/2014 1738 HMA 09/26/2014 2118 1 (TSS) SM 25400-2011 1 09/26/2014 1614 AAD 56882 CAS Analytical Parameter Number Method Result 0 PQL Units Run pH - Field SM 4500-H B 6.58 su 1 Temperature - Field (NC) SM 2550B-20 24.0 ° C 1 BOD, 5 day SM 521OB-20 4.4 2.0 mg1L 1 COD SM 5220D-20 ND 10 1 1 TSS SM 25400-20 4.0 1.0 ni 1 PQL = Practical quantitation limit B = Detected in the method blank E = fluantitatbn of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result a PQL and > MDL P = The RPO between two GC columns exceeds 40% N = Recovery is out of criteria Mere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: P124072-003 Description: 003 Matrix: Aqueous ,Date Sampled:0912412014 1305 Date Received:09124/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/24/2014 1305 MLK 1 (Temperature ) SM 2550E-2000 1 09/24/2014 1305 MLK 1 (GOD, 5 day) SM 521OB-2011 1 09/30/2014 0906 ANG 09/26/2014 1041 9374 1 (COD) SM 5220D-2011 1 09/27/2014 1738 HMA 09/26/2014 2118 1 (TSS) SM 254OD-2011 1 09/25/2014 1614 AAD 56882 CAS Analytical Parameter Number Method Result Q POL Units Run ^ pH - Field SM 4600-H B 6.64 su 1 Temperature - Field (NC) SM 2550E-20 24.0 ° C 1 GOD, 5 day SM 521OB-20 2.2 2.0 mg1L 1 COD SM 5220D-20 18 10 mg1L 1 TSS SM 264OD-20 11 1.0 mg1L 1 PQL - Practical quentitailon limit a = Detected in the method blank E = Quanulation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and - MDL P = The RPD between two GO columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 7 of 8 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylob.com Level t Report v2,1 Inorganic non-metals Client:IGM Reslns Laboratory ID: PI24072-004 Description: 004 Matrix: Aqueous ,Date Sampled:0912412014 1310 Date Received; 09/24/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 09/24/2014 1310 MLK 1 (Temperature ) SM 2550E-2000 1 09/24/2014 1310 MLK 1 (BOD, 5 day) SM 521OB-2011 1 09/30/2014 0906 ANG 09/25/2014 1041 9374 1 (COD) SM 5220D-2011 1 09/27/2014 1738 HMA 09/26/2014 2118 1 (TSS) SM 254OD-2011 1 09/25/2014 1614 AAD 56882 CAS Analytical Parameter Number Method Result 0 POL Units Run pH - Field SM 4500-H B 6.71 su 1 Temperature - Field (NC) SM 2550B-20 24.0 ° C 1 BOD, 5 day SM 521OB-20 ND 2.0 mg1L 1 COD SM 5220D-20 ND 10 mg1L 1 TSS SM 264OD-20 3.9 1.0 mg1L 1 PQL = Practical quantltatlon limit B = Detected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result a PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of crlteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flogged with a "W' Shealy Environmental Services, Inc. Page: 8 of 8 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shaalylab.com Level 1 Report v2.1 C7 3 o� 3 iu l0 m N e 0 } N Chain of Custody Record Shealy Environmental Services, Inc. 106 Vantage Point Drive West Galttmbia, South Carolina 29172 Tetephona No. (8D3) 791 J70D Fax No. (603) ?91-9111 wAvzsheWab.mm Number 26418 CFgrtif Repert in Corded 5ar Ow (PvWod Name) Cfuda No. Address Ttitahom No. i Fax No. I Email Waybill No, Page C of / 0 ago Trz- Yip Code Presenrapva I- VrvreL * HM33 7. NuC H 2 HWp47M 5. RCL 3. H2sN s, N,iw. FW f4A Niodw d Quisko c ij Bottle lies br>I I eon bads Proievt Name 2-0 , 1Zft -►,GA 51..)' lacy I PfeservatiYa P124072 �r1 T. tJ 4 %M PKWI Nuuber P.D Hinher :1� e VI Matrix ��.�S�,aymp.��la ID II 0960%*ion (Caat* s tier Carl swch� be k* /�� Date Tk" /n V S //awbivdanam �-0 Q �% 14 l q J 00 aH t 0 k 1ph Z mte id FFM Atou d71MR Rsgdn d (PtEcr l# e}garel regiired `m a -;it -ad TA] 13 Rwh rowsaspoft Semple Digpvssl OC O Ram b Caad byLab Roge rsmo>rts (3perify) Nepard WeatlGcaliun niSiifn hA a OPOM OLkhran 1. ReG by Sampler T} ??i ! uoe! b � i. Recekned Qeh� f T /� f un@ 2 RaUrtq•.iishea by Dele i imn Z. R %xgiwed by Data Time 3. RalinquNt ed by Cale Time 3. RaoaiwO by pie Tina A. RaIngL a Dat Tim�(a' 4. ietrordtotY Racecvad try fl ,L �, 1.0 N : A ea mp r9 retained for six weeks from receipt unless other arm2gernents are made. LAD USE ONLY RSCai- an Ice (Chsdd 7Kes o No a ka PMk 79M."-, •C Tamp u Y 1zl� W m C_ n m U) z 0 SHEALY ENVIRONMENTAL SERVICES, INC. Shruly Fnvirraugcad services. Inc. lbcum&v Number F-A"l6 Revision Number is Sample Rcccipt Checklist (SRC} Pop t or r Rttaaes L1 w 03107r 14 El vahwDntr 07015/14 Client: Curler Inspected by; date: wvyw, ! •«y_ 1oi #: Q \'Z.N-1% 4Al— Means of receipt: [?SUSI ❑ C Bent ❑ UFS ❑ FeclFx ❑ Airborne Exp ❑ Other Yes No 1. Were custody seals present on the cooler? ices I I I No NA 2. If cmtody scats were pmevit, were they intact and tmbmken? Cooler IDIOrigival temperature upon receipt/Darivcd (corr+ectcd) temperr, tutic upon receipt: Method-. ❑ Tempe—mture Blank ,ErAgainst Bottic s IR Gun ID: #3— IR Gun Convctiom Factor: Method of coolant et lee El Blue Iec ❑ Dry h;e None Yes ❑ No ❑ NA 3. If te°mperature of any cooler exceeded 6.4°C, was Pmjcct Manager notified? PM nottltcd by SRC, phone, note (circle one), other: (For coolm received via commercial courier. PMs are to be nniified immediately.) Yea ❑ No ❑ NA 4. Is the commercial couritx s arakin $li attached to this fbrm7 Yes ❑ No ❑ 5. Were E2per custody oceduns relln uished%recdved followed? Yes L I No ❑ NA 5a Wen samples relinquished by client to co**+**+=ial courier? Yes No 0 6. W= saMple E)s listed on the COL? Yes Na 7. Wcr. sample IDs listed on all sample containers? Ycs No ❑ 8. Was collection date & time listed on thr COC? Yes Nn ❑ 9. Was collixtiou date R tune listed on all Sam le containers? Yea No 10. Did all container label infurrnaliorl ID, date, time? agree sith the COG'! Yes No ❑ 11. Were testa to be performed listed on the COC? Yea No 12. Did all samples. arrive in the propm cvnwincrs for each test'f Yes No ❑ 13. Did all containers arrive in g2od ocMitioll unhmken, lids on, Cluj? Yes No 14. Was adequate sam lc vol umcavailahle? Yes 7 10 No ❑ 15. Were all samples rcccived within'% the holding time or 48 hours, whichever comes first? Yas E]I No 16. Were any winples containers misain 7 Yes No 17. Were there any excess samples not listed on C X:'! Yes '❑ No ❑ NA 18. Were bubbles resent >' -sing" ti"or 6mm in diameter in any VOA vials? Yes No ❑ NA ❑ 1 19, Were all metalae0&G!KE1A,uWrient sarm les rcccivcd at n li of <2? Yet ❑ No ❑ NA 0' 20, Ware all cyanide and%nr sulfide sam Ics rcccived at a pH a12? Ycs ❑ No ❑ NA 21. Wtxc all applicable NH3.17,N,'cyanidefphemol (0.2mg,T.) samples free of residual chlorine? Yes ❑ No ❑ NA 22. Were collection ten matures documented on the COC for NC samples'? Yes ❑ No ❑ NA 23. Were client remark&1rcqucsls (i.e. requested dilutions, MS1MS13 designations, etc... correccly transcrihed from the COG ittto the comment serum in LIMiS' Yew 01 No ff 24_ Was tho 14ote number used taken from the containcr label? Sample Preservation (Must he completed fur any samples) incyor wdy preserved or with hcatlspace.) Sample(s) were received incorrwly preserved and were adjustrd accordingly -in sample rcceivinit with H2S0" HCl Na0H usinit SR 9 Sale lea were received with bubbles >6 mm . in dinmetor. S lc s wrre received with TRC'. >0.2 m 'I, Qf421 is No) SC Drinking Water Project Sample(s) pH verifrcd to be > 2 by hate: sample(s) were not received at a pH of =2 and were adjusted aeeordin usingSRO sample labels applied b : Verified b '. Date: Ct 11111 Comments: Shealy Environmental Services, Inc. 106 Vantage Point drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,sheelylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. " Environmental SHEALY Services., Inc. 106 Vantage Point Drive - West Columbia, South Carolina 29172 LL A Phone. 803.791.9700 - Fax. 803, 791.9111 - www.5bealyla b com Reid Smith 1GM - Resins 3300 westinghouse Blvd.. Charlotte, NC 28241 1GM - Rcsins Charlotte, NC Stormwatcr Qualitative Monitoring Requirements 2014 2"d Semiannual Ev=1 September 24, 2014 I- None 2-Faint Pipe 001 outfall Color- 1 Odor- 1 Clarity- 1 floating Solids-1 Suspended Solids- 1 Foam- I Oil Sheen- 1 3-Moderate. 4-Strong Estimated Flow: 0.25 GIs per minute! 0.28 Inca= Estimated Event/ Discharge : SA Hrs Estimated Total Flow: 120 GIs Pipe 002 outiall Color- 1 Odor- 1 Clarity- 1 Floating Solids- I Suspended Solids- Foam- 1 Oil Sheen- 1 Estimated Flow: l .0 GIs per minute 10.28 Inches F-Mimated Event/ Discharge : 8.01Irs Estimaled'rotal Flow : 480 GIs Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shoolylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Enviironmentnl SHEAil LY Serviel , Inc. 106 Ventage Point Drive , West Columble4 South Carolina 29172 Phone. 803,791,9700 - Fax-803.791.9111 - www.shealylah.com IGM - Resins Charlottc, NC Stormwater Qualitathv Monitoring Requirements 2014 2nd Semianll l EV�-nt September 24, 2014 1- None 2-Fault 3-elexatc 4-Struag Pipe 003 outfall Color- 1 Odor- l Clarity- I Floating Solids- 2 Suspc Tided Sn1idii- 2 Foam- 1 Oil Sheen- 1 Estimatod Flow : 1.0 GIs per minute 10,28 inches Estimated Event! Discharge: 8.0I3.r9 Estimated Total Flow : 480 Gis Pipe 004 ou#all Color- I Odor- 1 Clarity- l Floating Solids- 1 Suspended Solids-1 Foam- 1 Oil She =- I Estimated Flow: 2.5 GIs per minute / 0.28 Inches Eraimatesd Event/ Discharge : 8.0 Hrs Estimated Total Flow: 1200 GIs Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www.shealylab.com Level 1 Reportv2.1 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000049 FACILITY NAME _IGM Resins PERSON COLLECTING SAMPLE(S) _Micheal Kilpatrick CERTIFIED LABORATORY(S) _Shealy Environmental Lab #_329 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Mecklenburg PHONE NO. (704)945-8702 F NATURE OF PERMITTEE OR DESIGNEE QUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall TSS BOD5 COD pH mo/dd/ r MG inches MG/L MG/L MG/L 001 02/21/2014 0.25 51 3.8 23 7.09 002 02/21/2014 0.25 22 3.1 54 6.85 003 02/21/2014 0.25 33 ND 51 7.07 004 02/21/2014 0.25 11 ND 18 6.93 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _x no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m m unit al/mo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 02/21/2014 Total Event Precipitation (inches): _0.25 Event Duration (hours): —2.5_ (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Tim Tippett Plant Manager / 3 1-14 i (Date) Form SWU-247, last revised 21212012 Page 2 of 2 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis IGM Resins 3300 Westinghouse Blvd. Charlotte, NC 28241 Attention: Reid Smith Project Name: Stormwater Lot Number:PB21079 Date Completed:0310612014 7WIny Kelly M. Maberry Project Manager `Ea,H Accogp+ c • � u s= This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc, The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist, Shealy Environmental Services, Inc. Page: ! of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Leve! 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No, 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative IGM Resins Lot Number: PB21079 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date Is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shaalylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary IGM Resins Lot Number: PB21079 Sample Number Sample ID Matrix Date Sampled Date Received 001 001 Aqueous 02/21/2014 0845 02/21/2014 002 002 Aqueous 02/21/2014 0655 02/21/2014 003 003 Aqueous 02/21/2014 0900 02/21/2014 004 004 Aqueous 02/21/2014 0910 02/21/2014 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 7 106 Ventage Point Drive West Columbia, SC 29172 (903) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2,1 Inorganic non-metals Client:IGM Resins Laboratory ID: PB21079-001 Description: 001 Matrix: Aqueous Date Sampled:0212112014 0845 Date Received:0212112014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/21/2014 0845 MILK 1 (Temperature) SM 25508-2000 1 02/21/2014 0846 MILK 1 (BOD, 5 day) SM 521OB-2011 1 02/27/2014 1000 KES 02/22/2014 0930 8863 1 (COD) SM 5220D-2011 1 03/04/2014 1640 BLB 03/04/2014 1235 1 (TSS) SM 2540D-2011 1 02/27/2014 1545 AMM1 41254 CAS Analytical Parameter Number Method Result a PQL Units Run pH - Field SM 4500-H B 7.09 su 1 Temperature - Field (NC) SM 25508-20 17.0 ° C 1 BOD, 5 day SM 621OB-20 3.8 2.0 mg1L 1 COD SM 6220D-20 23 10 mg1L 1 TSS SM 264OD-20 61 2.9 mg1L 1 PQL - Practical quentitation limit B = Detected In the method blank 5 = Quantita[iOn of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < POL and? MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of Maria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 4 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Leval 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: P621079-002 Description: 002 Matrix: Aqueous Date Sampled:0212112014 0855 Date Received:0212112014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/21/2014 0855 MLK 1 (Temperature ) SM 255OB-2000 1 02/21/2014 0855 MLK 1 (BOD, 5 day) SM 521OB-2011 1 02/27/2014 1000 KES 02/22/2014 0930 8863 1 (COD) SM 5220D-2011 1 03/04/2014 1640 BLB 03/04/2014 1235 1 (TSS) SM 254OD-2011 1 02/27/2014 1545 AMM1 41254 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4500-H B 6.85 su 1 Temperature - Field (NC) SM 2560B-20 17.0 a C 1 BOD, 5 day SM 521OB-20 3.1 2.0 mg1L 1 COD SM 5220D-20 54 10 mg/L 1 TSS SM 254OD-20 22 1.0 mg1L 1 PQL = Practfeal quantitation limit 8 = Detected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result a PQL and > MDL P = The RPD between two GG columns exceeds 40% N = RebOvery is Out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: PB21079-003 Description: 003 Matrix: Aqueous Date Sampled:0212112014 0900 Date Received:02/21/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/21/2014 0900 MLK 1 (Temperature) SM 25508-2000 1 02/21/2014 0900 MLK 1 (BOO. 5 day) SM 521OB-2011 1 02/27/2014 1145 KES 02/22/2014 1229 8864 1 (COD) SM 5220D-2011 1 03/04/2014 1640 BLB 03/04/2014 1235 1 (TSS) SM 254OD-2011 1 02/27/2014 1545 AMM1 41254 CAS Analytical Parameter Number Method Result Q PQL Units Run pH - Field SM 4600-H B 7.07 su 1 Temperature - Field (NC) SM 2650B-20 17.0 a C 1 BOD, 5 day SM 521OB-20 ND 2.0 mg1L 1 COD SM 5220D-20 51 10 ni 1 TSS SM 254OD-20 33 2.0 ri 1 PQL = Practical quantltatlon limit 8 = Detected In the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result s PQL and i MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, ail soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:IGM Resins Laboratory ID: PB21079-004 Description: 004 Matrix: Aqueous Date Sampled:0212112014 0910 Date Received:0212112014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH - Field) SM 4500-H B-2011 1 02/21/2014 0910 MILK 1 (Temperature ) SM 2550E-2000 1 02/21/2014 0910 MILK 1 (BOD, 5 day) SM 521 OB-2011 1 02/27/2014 1145 KBS 02/22/2014 1229 6864 1 (COD) SM 5220D-2011 1 02/28/2014 2123 BLB 02/28/2014 1500 1 (TSS) SM 254OD-2011 1 02/27/2014 1545 AMM1 41254 CAS Analytical Parameter Number Method Result a PQL Units Run pH - Field SM 4500-H B 6.93 su 1 Temperature - Field (NC) SM 2550B-20 17.0 ° C 1 BOD, 5 day SM 521OB-20 ND 2.0 mg1L 1 COD SM 6220D-20 1s 10 mg1L 1 TSS SM 25400-20 11 1.0 mgli_ 1 PQL = Practical quantitallon limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the PQL J a Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, afl soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 7 of 7 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 WWW.shealylab.com Level 1 Report v2.1 9,7 M 40 0 -.3 a a 0 P 05 a 0 -4 -4 ZD 4 -n -4 T (6 N r,p .1-) ��HFALV Chain of Custody Record Shealy Ens/iron mental 'Servires, Inc 10FAlanip-ga Puirit D- ve VVe- Galmibia Soutl- Carolina 29172 Number i 0164 fAophone N c. 79'j-9?0,) Fax No (RCI'!) 7E1I -P I I I - F- iIE;! 4Jern.�o presetv atree —1" O-J 7 P, All V6 A HI, 154 '44 Prr ad Numbz' -Y r, f,. r N.0 'I III'! I] ri V, 1; > Eu C: < I- 10 C� ior 11'anlT-n `Isqji-Bd(PrL- lejair:dlcrEipel--7t M) w- Mr 'p-L up Ep.-T fl.k.1 SSIMSL C 3L11'-4 p tU , 2, Rga'Jvvlj II 2. 11 Dato IMP 3 R"-IIr Time to RF-F�t:-V.-A -r. f4— Re.,C.14ec L. 211 Mute; All jijitilpleS are retained Co[ MY weeks from receipL unless Other atrangentents are rnafle. LAQ USE nl)-11c ii1ce Page ut 3,3LJE fSp� It- 0 ru J.: L I d F-In u Rv.y.:h 1 D ,1'-7,01 -jF++ Date —T. -I 11 . 'I 1. I 'K— ZY6�0— Tim- Dijtu N, ;,a_1T'rt Tenn E!Iar'$I V .-/3 CA m M z 0 z ic M z M C_ ca z 0 SHEALY ENVIRONMENTAL SERVICES, INC. SIWNIIy IN WLI 111 auvuu.' SttvicCs. In;. nisi: i:oen[ F-AD,-`JUi R_vi•inn Muwnlivr: 13 Cage i aF I Replaces Or= iFq: Z4 i s Fffr:titc C7ate::ly@h,;; Sample Reeeipt Chwkli;t (SRC) Q "L1 ILot #: .i G (:;licni: M i CoolerInspectod by dale: t ___1 f Q.� h wITIS lif mcoipl: [--I SF.SI ❑ Client ❑ UPS ❑ FedLx ❑ Airborne Eap ❑ 01her Yes NO I I 1. Were cu.Rindy scalR pirwent on the cooler? Yes No I 2. Ifcusiody seals were present, wcrc they intact and unbroken? Cooler I )jOriginal letnpertrurc kipo t receiptMerived (crlrl•ectcd) temperature upon receipt: Wthnd: ❑ 'l'ernperalure Blank Kainst 1Bottlos TR C.run ITS: � TR Gun Correctiolt Factor f Q ' f "C Method cif coolant: h "ct Ice ❑ Blue I" n My Ice ❑ Notie If reS onSe is No for Yes for 11. 15, 16), roust he I,Itrvided. Yes F ] No ❑ NA Q` 3. If temperature of any cooler exceerIM t+.0°(.:, was Prmlex:t Manager notifrad? PM notified by SRG phone., note (circle one), oilier: , (or coolers rcccived via co=ricrcial coicier. FNIs ate to be nolilied immediately. Yes ❑ No U NA- A. Is the comnwrcit11 u+lurita',, Pasking all. HIIrIJIt:rl t(+ this form? Yes 0 5• Wwrc proper custody pruc:Aures (rolin uishcd;rcccivCd) tulluwrd? Yes Yes - NU No Ll-1 Lit Sa We= sam lrs rrlinc uisheAl hy client to 00MMercial anurier:' 6. Wart' :tarnPle IT)s I icted? Ye% NJ- s. 7. Was eollec�tion date. & time listed'? 1'es Yes -Nit Na S. Were. teas to he performed liFled nn the C;OM 9. Did all sawpieS arrive in the puler crintainers for each test? Ycs No'H M Did all container Jabel information 111), date, 6niel agree uith COC" Yes NU H 11. Did rill undairre-rsaitive rrl �s?nlI lCMlidltlrll: Ui117Iokcn. lids can, ctc. ? Y'cs Nn 11 Was weir uale sample volume available'! 1'rs ' No ❑ Nip -_ 13, Were.. all samples rerewed within'h the holding, r:me or ail !tours, whichever comers first?' Z'v5 14, Wom nrty sam Ice cc�ataincra miming? Yes F1 No _ NA 15, Wrte there any excess samples not listed on COC? Yvs U No ❑ 16' Wcre bubbles present >"pct�-si r" (1.0ow bloat in dianteter) in arty VOA vials? 'o NA _ _ 17, Wcrc all metals':0&GrHL•,'vL`nutncn1 samples re�cerived at a 11 of �• 7 EYes 1°e'+ Mil NA• .. n l S. Vt'ere all cyanide andkw sul ride samples received at a p11 >12'1 5'cs ❑ 1v 0 NA.� I9. Wcrc all applicable 1N'H3,?KNicyariide:''phvu,.-1 (•42ntg L) samples fiec iif residual chlorine? Yvs _ No i NA Iff ?f). Wc:e collection tc )cratures documented on the CUC; I'VT NC sarnplm? Yes ❑ \u ❑ NA T"WCie client remarks?ir+qucsts fix- rcquesied diltilionS, ltIVNISD designations. etc...) txuir4t1transcribed fi-nln the COC into the comincnt section in LVVI5? Sutttple Preservation (Must t bL: crnnplctcd for any samplc(sl incorrectly' preserved or with headspac;. l samplv(s) _ were rcccived inet=CLfy presLT%-vJ wi l wcry ad., usled acrardingly in ample iecei-,ing with__ • (I1�SfT,,}NC11,HC1,tiaOH) tr,:lh the Sly 4 tnurnhcr) s am . ic(x) were rcccived with bubble~ >(, runi in diameter. l Sampie(s) were Feceived with i'ItC'-0.2 tng,'L• fLn N143i 'I'K\Isr4tut:dc:+lthrrull i Sam Ic h1hrlS %-vtificrl by: date: Corrective ve Action taltcn it•arcetuar : Was client notified: Yee Lj Nn 1_1 SM.SI employee: _ i_ cmtmer,ls Did cltvul respund'. Yr5 LJ No U Date of responx.: Shealy Environmental Services, Inc. 106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleb.com Level 1 Report v2,I SHEALY ENVIRONMENTAL SERVICES, INC. i I Environmental SIBEALY Sell -Vices, Inc. 1UnVanlayePoint Drive-Vries,Columbia,SouthCarolina 29;72 � f l I'hone,803.791.97VU- Rix,803,?91.9111-wwv.:.shealylah.rom Reid Smith IGNI - Resins 3300 Westinghouse Blvd., Charlotte. NC 38241 1GNI - Resins C:harlottc, N(' Stom water Qualitative Monitoring Rcyuircinuttt3 2014 191 Semiannt131 Lkew February 21, 2014 1- None 2-Faint Pipe 001 outfull Color- 2 odm- 1 Clarity- 2 Floatine Solids- 1 SuspeildW Solids- kFoam- 1 Oil Shecn- 1 3-Ytnderate 4-Strong Fstitnatud Flow : 0.25 GIs per minute. r 0.25 htchus Csrfinnicd F:vLnt' Dischargc : 2.5 Hrs FsLiinaied Total Flow : 37.5 Gls Pipe 002 ontfull Color- 1 Odor- I f:lurity- 1 Floating solids- 1 Susllunded Solids- I Funi11- I Oil ShVett-.1 l.stimared Flow : 0.50 Gis per minute ? 0.25 Inches Estimated F+rut: Dischnrgc : 4.5 [Irs lstimated Total Flim : 75 GIs Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reporl v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. H F A l YEnvironmental (.. .Y Services, SRC. 106 Vantt+ge Point DriyA ONest CulumLia, South Carolina 29172 %= l Nione,80.791.9700 - Fix. $03.791.9111 •Www,5he1Iv1ah.CnM I0NI • Rcsins Charlottc, NC' Sk MIlWhIcr ()ualitalivc \lunitaring Rquirements 2014 1'' 5emialmual EVVIIt February 21.2U14 1- None 2-Faint 3-Moderate 4-Strong Pipe 003 outfall Color- 2 Odor. I Clarity- 2 F loaung Solids- 2 Suspended Solids- Fiown- I Oil Sheen- 1 Fs1ilnxtLd HOW : 1.0 Gls per minute .i 0?5 Inches Emimnted Event! Di,chargc :2.5 Mrs Estimated Total Flow : 150 Gls Pipe 004 outfall Color- I Oder- 1 (.1arity- I FiCItttiue Solids- I Suspended Solids- 1 Foam- I Oil Shun- I Estimatcd Flow : 2.0 Us per minute? 0.25 Inches Esrimmed Event♦ Dischar6c : 2.5 Hr.,; 1=stimu1ct1Tutul Flow : 300 GIs Shealy Environmental Services, Inc. 10e Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 3300 Westinghouse Blvd Charlotte, NC 28273 704-945-8725 LR APR 30Z014 March 12, 2014 Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Stormwater Discharge Outfall Monitoring Report February 21, 2014 Certified Mail 7009 3410 00013396 6505 Dear Sirs: Please find the Stormwater Discharge Outfall Monitoring Report for IGM Resins USA, Inc. (IGM), Permit #: NCS000049. The analytical data from this sampling is included. No Benchmark exceedances noted. If you have any questions or concerns please call Mr. Reid Smith at 704-945-8725. Respectfully yours, Tim Ttppett Plant Manager Reid Smith Ph:704-945-8725 Fax:704-945-8725 email j.smith@igmresins, corn �ww.t North Carolina Department of Revenue Pat McCrory Lyons Gray Governor . Secretary April 29, 2014 We have received the enclosed document at our Raleigh, North Carolina office. Since there is no information indicating that it was intentionally sent to us, we can only assume that it was received in error. Therefore, it is being returned to you. Regards, Margaret Plummer, Team Leaderldd Documents, Payments Processing Division (919) 814-1406 PO BOX 2628, RALEIGH, NC 27602 Website: www.domc.com An Equal Opportunity Employer L9 APR 3 0 2014 ! � iili�k_.._�._.- 3 ., J_ _�1�,.