NCG020854_2016 Analytical Results Wastewater_20160511

aceAnalXical"
www.pnWabs com
May 11, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Basid 6 SW 515/16
Pace Project No.: 92296568
RECEIVED
ED
GENTR.6;L FILE
DWrR SECTION
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 1 of 15

aceAnalytical
wwwpacalabaomn
tj
Project: Basid 6 SW 5/5/16
Pace Project No. 92296568
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 633
UrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 15

aceAnalytical o
wwwpaceJa6scom
SAMPLE ANALYTE COUNT
Project: Basid 6 SW 5/5/16
Pace Project No 92296568
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92296568001 Sed 6 SM 2130B
KCE
1
PASI-E
SM 2540D
DWJ
1
PASI-E
SM 254OF
KCE
1
PASI-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 3 of 15

r ceAnalytical
i www.paceiabs.cam
Project: Basid 6 SW 5/5/16
Pace Project No: 92296568
Lab Sample ID Client Sample ID
Method Parameters
92296568001 Sed 6
SM 2130B Turbidity
SM 2540D Total Suspended Solids
SUMMARY OF DETECTION
Result Units
34.5 NTU
14.1 mg/L
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Report Limit Analyzed Qualifiers
0,50 05/06/1611:00
2.5 05/0611612:44
Page 4 of 15

aceMalytical
www.pacelabs oom
PROJECT NARRATIVE
Project: Basid 6 SW 5/5/16
Pace Project No : 92296568
Method: SM 2130B
Description: 2130E Turbidity EDN
Client: Charah
Date: May 11, 2016
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc Page 5 of 15

aceAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Basid 6 SW 5/5/16
Pace Project No,: 92296568
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: May 11, 2016
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration.
All criteria were within method requirements with any exceptions noted below
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN/22744
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1727831)
• Total Suspended Solids
• DUP (Lab ID: 1727832)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 6 of 15

acemalXicai
wwwpecelabscom
PROJECT NARRATIVE
Project: Basid 6 SW 5/5116
Pace Project No : 92296568
Method: SM 2540F
Description: 2540F Total Settleable Solids
Client: Charah
Date: May 11, 2016
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2540F All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc Page 7 of 15

aceAnalytical
wwwpacefabs com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project: Basid 6 SW 5/5/16
Pace Project No.: 92296568
Sample: Sed 6
Lab iD: 92296568001 Collected: 05/05/16 12:00
Received: 05/05/16 16:15 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Quaff
2130E Turbidity EDN
Analytical Method: SM 2130B
Turbidity
34.5 NTU
050 1
05/06/16 11:00
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
14.1 mg/L
2.5 1
05/06/16 12:44
2540F Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mUUhr
0.10 1
05/06/16 11:30
Date: 05/11/2016 10:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 8 of 15

11!;ac6Ana1j&a10
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project: Basid 6 SW 5/5/16
Pace Project No., 92296568
QC Batch: EDEN/22739
Analysis Method: SM 2130B
QC Batch Method: SM 2130B
Analysis Description: 2130E Turbidity EDN
Associated Lab Samples: 92296568001
METHOD BLANK: 1727811
Matrix: Water
Associated Lab Samples: 92296568001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Turbidity __.
NTU
ND 0.50 05/0611611:00
SAMPLE DUPLICATE: 1727812
92296260001 Dup
Parameter
Units
Result Result RPD Qualifiers
Turbidity
NTU
4.5 4.4 0
Results presented on this page
are in the
units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11 /2016 10:18 AM
without the written consent of Pace Analytical Services, Inc . Page 9 of 15

ace'Malytical
F --
www.pacalabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project:
Basid 6 SW 5/5/16
Pace Project No .
92296568
QC Batch:
EDEN/22744 Analysis Method: SM 2540D
QC Batch Method:
SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92296568001
METHOD BLANK: 1727829
Associated Lab Samples: 92296568001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 1727830
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 1727831
Parameter
Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2 5 05/06/16 12:38
Spike LCS LCS % Rec
Conc Result % Rec Limits Qualifiers
250 228 91 90-110
92296282001 Dup
Units Result Result RPD Qualifiers
mg/L 99.0 114 14 D6
SAMPLE DUPLICATE: 1727832
92296535001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 56.5 47.5
RPD Qualifiers
17 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 10:18 AM without the written consent of Pace Analytical Services, Inc Page 10 of 15

y ;alceAnalytical
www.pecefabscom
QUALITY CONTROL DATA
Project: Basid 6 SW 5/5/16
Pace Project No.: 92296568
QC Batch: EDEN/22738 Analysis Method: SM 2540F
QC Batch Method: SM 254OF Analysis Description: 2540F Total Settable Solids
Associated Lab Samples: 92296568001
METHOD BLANK: 1727809
Associated Lab Samples: 92296568001
Parameter Units
Total Settleable Solids mL/L/hr
SAMPLE DUPLICATE: 1727810
Parameter Units
Total Settleable Solids mtJIJhr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 05106/1611:30
92296568001 Dup
Result Result RPD Qualifiers
ND ND
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 10:18 AM without the written consent of Pace Analytical Services, Inc.
Page 11 of 16

;a7c e A na ly No
www.pecelabscorn
f
QUALIFIERS
Project: Basid 6 SW 5/5/16
Pace Project No. 92296568
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270 The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD . Relative Percent Difference
NC - Not Calculable
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/11 /2016 10:18 AM without the written consent of Pace Analytical Services, Inc Page 12 of 15

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project:
Basid 6 SW 5/5/16
Pace Project No
92296568
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92296568001
Sod 6
SM 2130E
EDEN/22739
92296568001
Sod 6
SM 2540D
EDEN/22744
92296568001
Sed 6
SM 254OF
EDEN/22738
Date: 05111 /2016 10:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 13 of 15

uocument Name Document Revised; 26FE82016
i Sample Condkion U on Rece; t SCUfi Pape l of 2
c?CG' (lir7i}IGI p 1' ( $
f Document No.: Issuing Authority:
F•RAL-CS-CS-rev.05 Pace Raleigh quality Office __.•._
Paae 2 of 2 for Internal Use ONIv
• ,; ' • , • 4Clle�nt N�a�m�e: (`� /"�,+� Projec irti2296568
❑Courier: o ac Ex []tJPS Elothe Client
Commercial QPace ❑Other: t
•— saasesse
Custody Seal Present? []Yes 6No Seals intact? Ryes PNo
Date/Initials Person Examining Contents (
Packing Material;❑Bubble Wrap [Bubble Bags None ❑Other.
Thermometer: W IR SN: 122065387 ❑IR SN:122065371 Type of Ice: Wet ❑glue ❑None ❑Samples on ice, cooing pracess has begun
Correction Factor: O&C Cooler Temp Corrected ('C): f�, 2 Biological Tissue Frozen? []Yes ❑No N/A
Temp should be above fre ing to 61C
USDA Regulated Soil ( 0/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (int�ationaRy,
IlYes to
'IF, 11-1 i —11. mwl r l,_•l res rva
COMMENTS:
Chain of Custody Present?
Yes
❑No
❑NIA
1
Chain of Custod filled Out?
es
Eloo
NIA
2,
Chain ofCuslodyRelinquished?
es
ON.
rrJA
3.
Sampler Name and/or Signature on CAC?E��
Yes
No
NJA
4.
Samples Arrived within Hold Time?
yes
No
N/A
5,
Short Hold Time Analysis (a72 hr)?
Yes
Na
❑N/A
i
6.
Rush Turn Around71me Requested?
yes
No
NJa
7.
5ufflclentvolume?
es
No
[]N/A
8.
Correct Containers Used?
Yes
❑No
❑N/A
9.
-Pace Containers Used?
Yes
ENo
:NIA
Containers Intact?
[IN,
NIA
10.
filtered Volume Received for Dissolved Tests?
[]Yes
QNo
NIA
11. Note If sediment is visible In the dissolved container
Sample Labels Match COC?
Pes
❑No
(]N/A
12.
-Includes Date/Time/ID/Analysis Matrix:
All containers needtng acid/base presetvatlon have been
checked?
Q/JYes
❑No
❑N/A
13.
All containers needing preservation are found to be In
compliance with EPA recommendation?
(HNO3, H2SO4i HCI<2; NaOH>9 Sulfide, NaOH>12 Cyanide)
ess
[]NO
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLH
No
N A
Samples checked for dechlorinatior
Yes
t]Na
N/A
14,
Headspace In VOAVIaIs (>S-5mm)?
QYes
❑No
N/A
15,
Trip Blank Present?
[]Yes
[3No
NJA
16.
Trip Blank Custody Seals Present?
[)Yes
[]No
/A
Pace Trip Blank Lot 11(If purchased):
r
16LIr"l NUIrtIC [UN/RE59LUTlUN
Person Contacted:
Comments/Resolution;
Date/Tme:
Field Data Required? Dyes []No
Project Manager SCURF Review: , Date: -"f
l
Project Manager SRF Review: �< Date:
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolln2 DEHNR Certification Office p.e.
Out of holo, Incorrect preservative, out of temp, incorrect containers)
Page 14 of 15

ac, ceAnalytical'
1 6701 Conference Drive, Raleigh, NO 27tf07
ph: [phone], fax: [phone]
NCWW Cert"7, NCDW Cert#37731
Report Results To:
Company:
Address: M 71
Attn:
Phone:
Fax-,
Sampled by (signature):
Chain of Custody
W'O'#
Bill To:
Project Reference:
Project Number:
Purchase Order #:
CJ Standard Report Delivery
0 Rush Reporl Delivery (W/surcharge)
"Hush pmieds are akfePt to prior appmvW by
the laboratory
Requested Due Date:
]nature)
a
�rerin'qulshed by (signature)
[Ael
Tare
Relinquished by (signature)
Received by (signature)
Date
lime
Receipt Conditions (L IIly)
*
13 4*.2C I 1T
Res. Chlorine:
DAbswt OPrasent On/a
Acid preserv. <2?
0 Yes 0 No 0 n/a
Base preserv. s127
0 Yes 0 No 0 n/a
Page 15 of 15