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Home My WebLink AboutNCG050041_DMR_20250307 EnvConmental Quality ENTHALPY Received A N A L Y I IC, AL MAR 072075 Winston-Salem 1941 Reymet Road 0 Richmond,Virginia 23237 0 Tel:(804)-358.8295 Fax:(804)•358-8297 Regional Office Certificate of Analysis Final Report N C G V J 0011 ^11 Laboratory Order to 25B1072 Client Name: Enviro-BEE Date Received: February 14, 2025 10:10 127 Red Hill Church Road Dale Issued: February 28, 2025 16:52 Dunn, NC 28334 Project Number: 49S Submitted To: Paul Spangenberg Purchase Order: Paul Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Enclosed are the results of analyses for samples received by the laboratory on 02/14/2025 10:10. If you have any questions concerning this report, please feel free to contact the laboratory. Sincerely, Sarah R. Endsley Laboratory Manager End Notes: The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory. Unless otherviise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen, temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler included in the Certificate of Analysis are done so at the client's request and are not included in the laboratory's fields of certification nor have they been audited for adherence to a reference method or procedure. The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified. For a complete list of the Laboratory's NELAC certified parameters please contact customer service. This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Enthalpy Analytical. TNI Accredited VEIAP to 460021 Page 1 of 14 ENTHALPY � � ANALY I' IC, AL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358.8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC ANALYTICAL REPORT FOR SAMPLES Laboratory Order ID 25B1072 Sample ID Laboratory ID Matrix Dale Sampled Date Received Oul(all 1 25B1O72-01 Waste Water 02/12/2025 08:00 02/14/2025 10:10 Page 2 of 14 ENTHALPY 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804).358.8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Laboratory Order ID: 25B1072 Analytical Results Sample I.D. Outfall 1 Laboratory Sample ID: 25131072-01 Grab Date/Time: 02/12/2025 08:00 Field Residual Cl: Field pH: Reporting Sample Prep Analysis Parameter Samp ID Method Result Qual Limit D.F. DaleTme DateRme Analyst Metals (Total)by EPA 200 Series Methods Copper 01 EPA200.7 R4.4 <0.0100 mg/L 0.0100 1 02/17/25 10:30 02/17/25 15:29 ACM Lead 01 EPA200.7 R4.4 <0.0100 mg/L 0.0100 1 02/17/25 10:30 02/17/25 15:29 ACM Zinc 01 EPA200.7 R4.4 0.0190 mg/L 0.0100 1 02/17/25 10:30 02/17/25 15:29 ACM Wet Chemistry Analysis COD 01 SM5220D-2011 26.7 mg/L 10.0 1 02/24/25 10:00 02/24/25 10:00 CET Oil and Grease 01 EPA1664B <5.0 mg/L 5.0 1 02/26/25 16:40 02/26/25 16:40 KJM pH 01 SM4500-HB-2021 6.0 Su H -- 1 02/18/25 14:40 02/18/25 14:40 DTB TSS 01 SM254OD-2020 20.8 mg/L 1.0 1 02/18/25 12:02 02/18/25 12:02 ACA Page 3 of 14 ENTHALPY ANA1,'YTJCA � , 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-35"297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Analytical Summary Preparation Factors Sample ID Initial/Final Method Batch ID Sequence ID Calibration 10 Metals(Total)by EPA 200 Series Methods Preparation Method: EPA200.2R2.81SW3005A-ICP 25BI072-01 50.0 mL/50.0 mL EPA200.7 R4.4 BIB0625 SIB0567 AB50212 Preparation Factors Sample ID Initial/Final Method Batch ID Sequence ID Calibration ID Wet Chemistry Analysis Preparation Method: No Prep Wet Chem 2581072-01 750 mL/750 mL SM2540D-2020 BIB0698 SIB0616 Wet Chemistry Analysis Preparation Method: No Prep Wet Chem 2581072-01 1.00 mL/1.00 mL SM4500-HB-2021 BIB0707 SIB0629 Wet Chemistry Analysis Preparation Method: No Prep Wet Chem 25B1072-01 2.00 mL/2.00 mL SM5220D-2011 BIB0981 SIB0884 AB50163 Wet Chemistry Analysis Preparation Method! No Prep Wet Chem 25BI072-01 230 mL/230 mL EPA1664B BIB1105 SIB0996 Page 4 of 14 ' iii ENTHALPY 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC QC Analytical Summary Preparation Factors Sample ID Initial/Final Method Batch ID Sequence ID Calibration ID Metals(Total)by EPA 200 Series Methods Preparation Method: EPA200.2R2.8/SW3005A-ICP BIB0625-BLK1 50.0 mL/50.0 mL EPA200.7 R4.4 BIB0625 SIB0567 AB50212 BIB0625-BS1 50.0 mL 150.0 mL EPA200.7 R4.4 RIB0625 S180567 AB50212 BIB0625-MS1 50.0 mL/50.0 mL EPA200.7 R4.4 BIB0625 SIB0567 AB50212 BIB0625-MS2 EPA200.7 R4.4 BIB0625 SIB0567 AB50212 8I80625-MSDI 50.0 mL/50.0 mL EPA200.7 R4.4 BIB0625 SIB0567 AB50212 B1B0625-MSD2 EPA200.7 R4.4 BIB0625 SIB0567 AB50212 Preparation Factors Sample ID Initial/Final Method Balch ID Sequence ID Calibration ID Wet Chemistry Analysis Preparation Method: No Prep Wet Chem BIB0698-BLK1 1000 mL/1000 mL SM2540D-2020 BIB0698 SIB0616 BIB0698-BSI 100 mL/100 mL SM2540D-2020 BIB0698 SIB0616 B1B0698-DUP1 100 mL/100 mL SM2540D-2020 BIB0698 SIB0616 BIB0698-DUP2 30.0 mL/30.0 ml. SM2540D-2020 BIB0698 SIB0616 BIB0707-DUP1 1.00 mL/1.00 mL SM4500-HB-2021 BIB0707 SI80629 BIB0707-DUP2 1.00 ml./1.00 mL SM4500-HB-2021 BIB0707 SIB0629 81B0981-BLK1 2.00 mL/2.00 mL SM5220D-2011 BIB0981 SIB0884 AB50163 BIB0981-BSI 2.00 mL/2.00 mL SM5220D-20il BIB0981 SIB0884 AB50163 BIB0981-MRLI 2.00 mL/2.00 mL SM5220D-2011 BIB0981 SIB0884 AB50163 BIB0981-msl 2.00 mL/2.00 mL SM5220D-2011 BIB0981 SIB0884 AB50163 BI80981-MSD7 2.00 mL/2.00 mL SM5220D-2011 BIB0981 SIB0884 AB50163 BIB1105-BLK1 1000 mL/1000 mL EPA1664B BIB1105 SI80996 B1B1105-BS1 250 mL/250 mL EPA1664B BIB1105 SIB0996 BIB1105-DUP1 230 mL/230 mL EPA1664B BIBn05 SIB0996 BIB1105-MS1 250 mL/250 mL EPA1664B BIB1105 SIB0996 Page 5 of 14 ENTHALPY ►■iit ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358.8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Dale Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Page 6 of 14 ENTHALPY ►iiiiillil� A I J ,\ CA, �, 1941 Reymel Road•Richmond,Virginia 23230 •Tel:(804).358-8295 Fax:(804)-358.8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Metals (Total) by EPA 200 Series Methods -Quality Control Enthalpy Analytical Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit oust Batch BIB0625-EPA200.2R2.8/SW3005A-ICP Blank(SIB0625-BLK1) Prepared&Analyzed:02/17/2025 Copper <0.0100 mg/L 0.0100 mg/L Lead <0.0100 mg/L 0.0100 mg1L Zinc <0.0100 mg/L 0.0100 mg/L LCS(BIB0625-BS1) Prepared&Analyzed•02/17/2025 Copper 0,528 mg/L 0.0100 mg/L 0.500 mg/L 106 85-115 Lead 0.519 mg/L 0.0100 mg/L 0.500 mg/L 104 85-115 Zinc 0,526 mg/L 0.0100 mg/L 0.500 mg/L 105 85-115 Matrix Soi a(BIB0625-MS1) Source:25B0931.01 Prepared&Analyzed:02/17/2025 Copper 0.491 mg/L 0.0100 mg/L 0.500 0.0264 mg/L 92.9 75-125 Lead 0.480 mg& 0.0100 mg/L 0,500 <0.0100 mg/L 94.1 75-125 Zinc 0.546 mg/L 0.0100 mg/L 0.500 0.102 mg/L 88.7 75-125 Matrix Spike Dup(BIB0625-MSD1) Source:25BO931-01 Prepared&Analyzed:02/17/2025 Copper 0.495 mg/L 0.0100 mg/L 0.500 0.0264 mg/L 93.7 75-125 0.872 20 Lead 0.483 mg/L 0.0100 mg/L 0,500 <0.0100 mg/L 94.7 75-125 0.685 20 Zinc 0.542 mg/L 0.0100 mg/L 0.500 0.102 mg/L 88.1 75-125 0.570 20 Page 7 of 14 ENTHALPY � hNALYIIC, AL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)35"295 Fax:(804)-358.8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Wet Chemistry Analysis -Quality Control Enthalpy Analytical Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Qual Batch BIB0698 -No Prep Wet Chem Blank(BIB0698-BLK1) Prepared&Analyzed:02/18/2025 TSS <1.0 mg/L 1.0 mg/L LCS(BIB0698.BS1) Prepared&Analyzed:02/18/2025 TSS 92.0 mg1L 1.0 mg/L 100 mg/L 92.0 80-120 Duplicate(BIB0698-DUP1) Source:25B0894-03 Prepared&Analyzed•02/18/2025I TSS 35.0 mg/L 1.0 mg/L 39.0 mg/L 10.8 10 P Duplicate(BIB0698-DUP2) Source-25BI054-01 Prepared&Analyzed,0211 8/2 0 2 5 TSS 203 mg/L 1.0 mg/L 213 mg/L 4.80 10 Batch BIB0707 -No Prep Wet Chem Duplicate(8180707-DUP1) Source:25SO921.02 Prepared&Analyzed•0 211 8/2 0 2 5 PH 6.3 SU 0.0 SU 6.3 SU OA78 20 Duplicate(6180707-DUP2) Source:25B1073.02 Prepared&Analyzed:02/1 812 0 2 5 PH 6.6 SU 0.0 sU 6.7 SU 1.05 20 Batch BIB0981 -No Prep Wet Chem Blank(BIB0981-BLK1) Prepared&Analyzed:02/24/2025 COD <10.0 mg/L 10.0 mg/L LCS(BIB0981-BS1) Prepared&Analyzed:02/24/2025 COD 50.3 mg& 10.0 mg/L 60.0 mg/L 101 88-119 it Page 8 of 14 11"1110 Molow ENTHALPY 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax:(804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn INC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Wet Chemistry Analysis -Quality Control Enthalpy Analytical Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Quad Batch BIB0981 -No Prep Wet Chem Matrix Spike(BIB0981-MS1) _Source,25B1419-02 Prepared&Analyzed 02/24/2025 COD 83.5 mg/L 10.0 mg/L 50.0 26.3 mg/L 114 72.4-130 Matrix Spike Dup(BIB0981-MSD1) _.- Source:25B1419-02 Prepared&Analyzed:02/24/2025 COD 83.5 mg/L 10.0 mg/L 50.0 26.3 mg/L 114 72.4-130 0.00 20 Batch BIB1105-No Prep Wet Chem Blank(BIB1105-BLK1) Prepared&Analyzed 02/26/2025 Oil and Grease <5.0 mg/L 5.0 mg/L LCS(BIB1105-BS1) Prepared&Analyzed:02/26/2025 Oil and Grease 38.8 mg/L 5.0 mg/L 40.0 mg/L 97.0 78-114 Duplicate(BIB1105-DUP1) Source:25B1073.02 Prepared&Analyzed:02/26/2025 Oil and Grease <5.0 mg/L 5.0 mg/L <5.0 mg/L NA 18 Matrix Spike(BIB1105-MS1) Source:25B1054.02 Prepared&Analyzed:02/26/2025 Oil and Grease 38.7 mg/L 5.0 mg/L 40.0 <5.0 mg/L 96.7 78-114 Page 9 of 14 ENTHALPY 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Certified Analyses included in this Report Analyte Certifications EPA1664B in Non-Potable Wafer Oil and Grease VELAP,NCDEQ,WVDEP,SCDHEC EPA200.7 R4.4 In Non-Potable Water Copper VELAP,NCDEQ,WVDEP,SCDHEC Lead VELAP,NCDEQ,WVDEP,SCDHEC Zinc VELAP,NCDEQ,WVDEP,SCDHEC SM254OD-2020 in Non-Potable Wafer TSS VELAP,NCDEQ,PADEP,W VDEP,SCDHEC SM5220D-20111n Non-Potable Wafer COD VELAP,NCDEQ,PADEP,WVDEP,SCDHEC Code Description Laboratory ID Expires DURSC-NCDEQ NCDEQ Durham Service Center 703 12/31/2025 DURSC-NCDHHS NCDHHS Durham Service Center 37918 07/31/2025 MdDOE Maryland DE Drinking Water 341 12/31/2025 NCDEQ North Carolina DEQ 495 12/31/2025 NCDHHS North Carolina Department of Health and Human 51714 07/31/2025 NYDOH New York DOH Drinking Water 12069 04/01/2025 PADEP NELAP-Pennsylvania Certificate 4009 68-03503 10/31/2025 SCDHEC South Carolina Dept of Health and Environmental 93016 06/14/2025 TXCEQ Texas Comm on Environmental Quality#T10470r T104704576 05/31/2025 VELAP NELAP-Virginia Certificate#12969 460021 06/14/2025 WVDEP West Virginia DEP 350 11/30/2025 Page 10 of 14 ENTHALPY 6k'1A_ ANALY l 1CAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)358-8295 Fax:(804)-358.8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC, 28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Summary of Data Qualifiers H Analysis was performed outside of the method prescribed holding time. P Duplicate analysis does not meet the acceptance criteria for precision ' RPD Relative Percent Difference Qual Qualifers -RE Denotes sample was re-analyzed D.F. Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section. TIC Tentatively Identified Compounds are compounds that are Identified by comparing the analyze mass spectral pattern with the NIST spectral library.ATIC spectral match is reported when the pattern is at least 75%consistent with the published pattern. Compound concentrations are estimated and are calculated using an Internal standard response factor of 1. PCBs,Total Total PCBs are defined as the sum of detected Aroclors 1016,1221,1232,1248,1254,1260,1262,and 1268. Page 11 of 14 a T' O cN N o LL ¢ o q? U0 u N _ q tnn `o 'c Rd z z n E Q Z Z N �o>6 Y m U ' Q Z O w $a°?on wjcwi Fw v1 - a I o „a._= y�z o . 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F m n qe1E) x o 0 0 ' ° rn 0 tf c U a 0) w W o S m U U Z0 co `w O W m U) v 6a d d d h Q d N Q ggp U) RN Z o Z 3 F- .- o \ o o Y Q U (n W u W @ N m m Z p O " U O z z z 0 0 0 2 O U ¢ a L N U)i S M y n o n m rn 1w � IX Rd PYId ^ O '6 C o) co a Qxd PYu � N fJ m xdPYld Jill t xdPYld t IM U Rd c V P.Y...y c O xdmid ` n HN a Rd PYld � Jf CL v L$ g Q N lid I.YId n E O m E IL ' Z E ` s ! l�e/a� gm Y/ a Rd lwld m Rd PYW Rd P w LJ at Rd IOU Rd F.M so r N 4 W; Q I • 1 @erg 1 al.wmuoo R o 6 ® k = § f Q 2 al a�dwag — m yr cd >. L o z i x '� ENTHALPY 6it ANALYTICAL 1941 Reymet Road•Richmond,Virginia 23230 •Tel:(804)358.8295 Fax:(804)-358.8297 Certificate of Analysis Final Report Client Name: Enviro-BEE Date Issued: February 28, 2025 16:52 127 Red Hill Church Road Project Number: 49S Purchase Order: Paul Dunn NC,28334 Submitted To: Paul Spangenberg Client Site I.D.: 1112 Rt 49 South,Asheboro, NC Sample Conditions Checklist Samples Received at: 3.10•C How were samples received? UPS Were Custody Seals used? Yes Are the custody papers filled out completely and correctly? Yes Do all bottle labels agree with custody papers? Yes Is the temperature Wank or representative sample within acceptable limits or received on Ice,and recently taken? Yes Are all samples within holding Ume for requested laboratory tests? No Is a sufficlenl amount of sample provided to perform the tests Included? Yes Are all samples in appropriate containers for the analyses requested? Yes Were volatile organic containers received? No Are all volatile organic and TOX containers free of headspam? - NA Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011,EPA504,EPA6260,EPA624, NA EPA8015 GRO,EPA8021,EPA524,and RSK-175. Are all samples received appropriately preserved?Note that metals containers do not require field preservation but lab Yes preservation may delay analysis.In addition,field parameters are ahvays received outside homing Ume and will be marked accordingly. Work Order Comments ph to be analyzed out of hold as it is a field parameter.CSB 2/14/25 1213 Page 14 of 14