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Home My WebLink AboutNC0002305_GW Well PFAS Lab Results Part 2_20240505North Carolina Division of Water Resources Water Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality PFAS Cover Page Order ID: Regional Date Office: Received: 00 00 0 0 E-AMICk 24051001 W I RO 05/10/2024 Project/Site: NC0002305 LIMS ID: Sample ID: Site: Date Collected: Collector: 24051001-01 TB-20240509-GK PFAS_WIRO_TB 05/09/2024 09:16 G. Kegley 24051001-02 NC0002305-WS-20240509 NC0002305-WS 05/09/2024 11:11 G. Kegley 24051001-03 NC0002305-EFF-20240509 NC0002305-EFF 05/09/2024 11:15 G. Kegley 24051001-04 NC0002305-FB-20240509 NC0002305-FB 05/09/2024 11:10 G. Kegley "Providing science -based environmental stewardship for the health and prosperity of ALL North Carolinians." North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-01 Delivery Method: NC Courier Sample ID: TB-20240509-GK Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 09:16 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFBA 375-22-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeA 2706-90-3 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxA 307-24-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpA 375-85-9 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFOA 335-67-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFNA 375-95-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFDA 335-76-2 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFUnA 2058-94-8 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoA 307-55-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFTrDA 72629-94-8 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFTeDA 376-06-7 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFBS 375-73-5 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeS 2706-91-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxS 355-46-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpS 375-92-8 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFOS 1763-23-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFNS 68259-12-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFDS 335-77-3 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoS 79780-39-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS EHenderson N-McFOSAA 2355-31-9 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 2 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-01 Delivery Method: NC Courier Sample ID: TB-20240509-GK Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 09:16 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By N-EtFOSAA 2991-50-6 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 4:2 FTS 757124-72-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 6:2 FTS 27619-97-2 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 8:2 FTS 39108-34-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson HFPO-DA 13252-13-6 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson ADONA 919005-14-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 9CI-PF30NS 756426-58-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 11CI-PF3OUdS 763051-92-9 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFMOAA 674-13-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF02HxA 39492-88-1 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF030A 39492-89-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF04DA 39492-90-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF05DA 39492-91-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 1 29311-67-9 1.8 < 1.8 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson Byproduct 2 749836-20-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 4 2416366-18-0 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 5 2416366-19-1 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 6 2416366-21-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PEPA 267239-61-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PMPA 13140-29-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 3 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-01 Delivery Method: NC Courier Sample ID: TB-20240509-GK Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 09:16 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFECA-B 151772-58-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFECA G 801212-59-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Hydro -EVE 773804-62-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson EVE Acid 69087-46-3 1.8 < 1.8 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson R-EVE 2416366-22-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson NVHOS 801209-99-4 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFEESA/PES 113507-82-7 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 4 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-02 Delivery Method: NC Courier Sample ID: NC0002305-WS-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WG Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:11 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFBA 375-22-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeA 2706-90-3 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxA 307-24-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpA 375-85-9 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFOA 335-67-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFNA 375-95-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDA 335-76-2 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFUnA 2058-94-8 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoA 307-55-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFTrDA 72629-94-8 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFTeDA 376-06-7 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFBS 375-73-5 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeS 2706-91-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxS 355-46-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpS 375-92-8 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFOS 1763-23-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFNS 68259-12-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDS 335-77-3 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoS 79780-39-5 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS EHenderson N-McFOSAA 2355-31-9 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 5 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-02 Delivery Method: NC Courier Sample ID: NC0002305-WS-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WG Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:11 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By N-EtFOSAA 2991-50-6 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 4:2 FTS 757124-72-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 6:2 FTS 27619-97-2 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 8:2 FTS 39108-34-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson HFPO-DA 13252-13-6 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson ADONA 919005-14-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 9CI-PF30NS 756426-58-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 11CI-PF3OUdS 763051-92-9 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFMOAA 674-13-5 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF02HxA 39492-88-1 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF030A 39492-89-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF04DA 39492-90-5 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF05DA 39492-91-6 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 1 29311-67-9 1.7 < 1.7 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson Byproduct 2 749836-20-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 4 2416366-18-0 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 5 2416366-19-1 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 6 2416366-21-5 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PEPA 267239-61-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PMPA 13140-29-9 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 6 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-02 Delivery Method: NC Courier Sample ID: NC0002305-WS-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WG Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:11 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFECA-B 151772-58-6 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFECA G 801212-59-9 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Hydro -EVE 773804-62-9 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson EVE Acid 69087-46-3 1.7 < 1.7 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson R-EVE 2416366-22-6 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson NVHOS 801209-99-4 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFEESA/PES 113507-82-7 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 7 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-03 Delivery Method: NC Courier Sample ID: NC0002305-EFF-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WW Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:15 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFBA 375-22-4 1.7 620 ng/L J1, J2, J7 5/30/2024 DWRPFAS EHenderson PFPeA 2706-90-3 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxA 307-24-4 1.7 43 ng/L 5/30/2024 DWRPFAS EHenderson PFHpA 375-85-9 1.7 7.4 ng/L 5/30/2024 DWRPFAS EHenderson PFOA 335-67-1 1.7 15 ng/L 5/30/2024 DWRPFAS EHenderson PFNA 375-95-1 1.7 2.7 ng/L 5/30/2024 DWRPFAS EHenderson PFDA 335-76-2 1.7 4.0 ng/L J1 5/30/2024 DWRPFAS EHenderson PFUnA 2058-94-8 1.7 < 1.7 ng/L U, A 5/30/2024 DWRPFAS EHenderson PFDoA 307-55-1 1.7 < 1.7 ng/L U, A 5/30/2024 DWRPFAS EHenderson PFTrDA 72629-94-8 1.7 < 1.7 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFTeDA 376-06-7 1.7 < 1.7 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFBS 375-73-5 1.7 21 ng/L J2 5/30/2024 DWRPFAS EHenderson PFPeS 2706-91-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxS 355-46-4 1.7 170 ng/L 5/30/2024 DWRPFAS EHenderson PFHpS 375-92-8 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFOS 1763-23-1 1.7 15 ng/L 5/30/2024 DWRPFAS EHenderson PFNS 68259-12-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDS 335-77-3 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoS 79780-39-5 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS EHenderson N-McFOSAA 2355-31-9 1.7 6.4 ng/L 5/30/2024 DWRPFAS EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 8 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-03 Delivery Method: NC Courier Sample ID: NC0002305-EFF-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WW Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:15 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By N-EtFOSAA 2991-50-6 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 4:2 FTS 757124-72-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 6:2 FTS 27619-97-2 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 8:2 FTS 39108-34-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson HFPO-DA 13252-13-6 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson ADONA 919005-14-4 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 9CI-PF30NS 756426-58-1 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson 11CI-PF3OUdS 763051-92-9 1.7 < 1.7 ng/L U 5/30/2024 DWRPFAS EHenderson PFMOAA 674-13-5 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson PF02HxA 39492-88-1 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF030A 39492-89-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF04DA 39492-90-5 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson PF05DA 39492-91-6 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 1 29311-67-9 1.7 < 1.7 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson Byproduct 2 749836-20-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 2416366-18-0 1.7 2.7 ng/L J1, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 5 2416366-19-1 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 6 2416366-21-5 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson PEPA 267239-61-2 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PMPA 13140-29-9 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 9 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-03 Delivery Method: NC Courier Sample ID: NC0002305-EFF-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WW Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:15 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFECA-B 151772-58-6 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFECA G 801212-59-9 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Hydro -EVE 773804-62-9 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson EVE Acid 69087-46-3 1.7 < 1.7 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson R-EVE 2416366-22-6 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson NVHOS 801209-99-4 1.7 < 1.7 ng/L U, J1, J13 5/30/2024 DWRPFAS2022 EHenderson PFEESA/PES 113507-82-7 1.7 < 1.7 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 10 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-04 Delivery Method: NC Courier Sample ID: NC0002305-FB-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:10 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFBA 375-22-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeA 2706-90-3 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxA 307-24-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpA 375-85-9 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFOA 335-67-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFNA 375-95-1 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFDA 335-76-2 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFUnA 2058-94-8 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFDoA 307-55-1 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFTrDA 72629-94-8 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFTeDA 376-06-7 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFBS 375-73-5 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFPeS 2706-91-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHxS 355-46-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson PFHpS 375-92-8 1.8 < 1.8 ng/L U, A 5/30/2024 DWRPFAS EHenderson PFOS 1763-23-1 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFNS 68259-12-1 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFDS 335-77-3 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson PFDoS 79780-39-5 1.8 < 1.8 ng/L U, J1, J13 5/30/2024 DWRPFAS EHenderson N-McFOSAA 2355-31-9 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 11 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-04 Delivery Method: NC Courier Sample ID: NC0002305-FB-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:10 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By N-EtFOSAA 2991-50-6 1.8 < 1.8 ng/L U, 11 5/30/2024 DWRPFAS EHenderson 4:2 FTS 757124-72-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 6:2 FTS 27619-97-2 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 8:2 FTS 39108-34-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson HFPO-DA 13252-13-6 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson ADONA 919005-14-4 1.8 < 1.8 ng/L U 5/30/2024 DWRPFAS EHenderson 9CI-PF30NS 756426-58-1 1.8 < 1.8 ng/L U, A 5/30/2024 DWRPFAS EHenderson 11CI-PF3OUdS 763051-92-9 1.8 < 1.8 ng/L U, A 5/30/2024 DWRPFAS EHenderson PFMOAA 674-13-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF02HxA 39492-88-1 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF030A 39492-89-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF04DA 39492-90-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PF05DA 39492-91-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 1 29311-67-9 1.8 < 1.8 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson Byproduct 2 749836-20-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 4 2416366-18-0 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 5 2416366-19-1 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Byproduct 6 2416366-21-5 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PEPA 267239-61-2 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PMPA 13140-29-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL Page 12 of 13 North Carolina Division of Water Resources Water ,f��D�E�C Sciences Section Laboratory Results NORTH CAROLINA _ Department of Environmental Quality P FAS Final Report LIMS ID: 24051001-04 Delivery Method: NC Courier Sample ID: NC0002305-FB-20240509 Received Date: 05/10/2024 07:15 Sample Matrix: WQ Temperature on Arrival (°C) 0.2 Collection Date: 05/09/2024 11:10 Report Print Date 07/15/2024 14:32 Sample processed during Reedy Creek Lab Campus Renovation and Expansion Project: Yes Analyte CAS # PQL Result Qualifier Analysis Date Method Reference Validated By PFECA-B 151772-58-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFECA G 801212-59-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson Hydro -EVE 773804-62-9 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson EVE Acid 69087-46-3 1.8 < 1.8 ng/L Z2 5/30/2024 DWRPFAS2022 EHenderson R-EVE 2416366-22-6 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson NVHOS 801209-99-4 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson PFEESA/PES 113507-82-7 1.8 < 1.8 ng/L U, J13 5/30/2024 DWRPFAS2022 EHenderson NCDEQ-WSS Chemistry Lab PFAS Qualifiers J1 Estimated - Surrogate or Internal Standard recovery limits have been exceeded. J2 Estimated - The reported value failed to meet the established quality control criteria for either precision or accuracy. J4 Estimated - Improper laboratory protocols, MDL studies are not completed for this analyte. J5 Estimated - Temperature limits exceeded (sample frozen or > 10 °C) during transport. J7 Estimated - Exceeded the upper calibration range. J13 Estimated - standards used for this analyte are from an uncertified source. These are the only standards available for the analyte. P Sample dilution occurred; Elevated PQL Q1 Holding time exceeded prior to receipt by lab. Q2 Holding time exceeded following receipt by lab. U Analyte was analyzed, but not detected above the reported PQL. V1 The analyte was detected in both the sample and the method blank. V2 The analyte was detected in both the sample and the field blank. X1 Sample not screened for this analyte. X3 Sampled, but analysis lost or not performed - lab error. y Elevated PQL due to insufficient sample volume. Z1 Inability to analyze the sample. Z2 Questions concerning data reliability. WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699 "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 13 of 13 ra T > P�� H G) 4D 2 m rL CD 3 ik ET lu sw rL kk Js� 0 Qs, 7T (Z) Cl -4Q cl -06 t3 r. w 4.+ 3 m 0 7-- CL �i 0 n (A mq. r+ . . . . . CL n.: " 4 - 7z 41 O S: n Lo n CL f7 M 2L >4 (D r. n 0 -4 rn Cl Sample Condition Upon Receipt (SOUR) questionnaire for PEAS Order ID: ZA 0 51001 Project/Site Name: _ 1" Instructions: Circle Yes or No for each question. If No, complete information below question. To be completed by Sampling Receiving: 17-0 rnrr,nlptad Bw aVi 1. Is there a COC security seal on transport container? ts'fi No / NA 2. For legal COC samples, is COC is properly signed in relinquished/received section . Yes / No / NA • Not relinquished • Other (describe) 3. Did samples arrive on ice? Yes No 4. Was the temperature blank bottle within (0 <_ 1000?(Yes No • No temperature blank bottle 5. is there a COC / analytical request form included with shipment? DYesNo Client contacted and provided form. To be completed by the PFAS Team: Completed By: 6. Are the number of samples the same as stated on the request form?oYes No 7. Do Sample IDS on COC match IDS on bottles? Yes / No n ' IDs impacted: C k6mO 5& r Y) t'w\ws `i'a '44C Sa'ry (f maS4f 5 ��1� -�Zvr. 8. Do dates & times on the COC match dates & times on bottles? Yes No • No dates on containers • No times on containers • Other (describe) 9. Are sample containers intact, with correct preservative & bottle type? Yes No • Damaged container • Leaking container • Wrong preservative • Wrong bottle type • Other (describe) Page 1 of 1 NCDEQ DWR Chemistry Laboratory Revision date: 8/28/2023 J:\UNITS\PFAS\ATL Sample Master LIMS\ATL LIMS - SCUR questions.docx