Loading...
HomeMy WebLinkAboutNCS000528_Fact sheet binder_20230920 DEQ / DEMLR FACT SHEET FOR NPDES INDUSTRIAL INDIVIDUAL STORMWATER PERMIT DEVELOPMENT Basic Information for Permit Issuance and Renewals: Permit Writer/Date Brianna Young 9/20/2023 Permit Number NCS000528 Owner/Facility Name Premiere Fibers SIC AICS Code/Category 2824 (325220)/Manmade organic fiber Basin Name/Sub-basin number Yadkin Pee-Dee/03-07-10 Receiving Stream/HUC UT to Buffalo Creek/030401040205 Stream Classification/Stream Segment C/ 13-18-1 Is the stream impaired on 303 d list]? No Any TMDLs? No Any threatened and/or endangered species? No Any compliance concerns? See Section 2 below Any perinit mods since lastpermit? No New expiration date 10/31/2028 Comments on Draft Permit? See Section 6(below) Section 1. Facility Activities and Process: Premiere Fibers produces manmade organic fiber that converts Nylon-Type 6,Nylon-Type 6.6, and polyester pellets into a wound fiber. Synthetic oils are applied for future processing. There are approximately 35 motoring wells located across the site. Per the SWPPP submitted with the permit application, the dumpsters, storage silos, and shipping and receiving bays are the only areas where pollutants could potentially enter the stormwater drainage system. Per information in the permit file, materials that could potentially be exposed to stormwater include yarn, finish oils, degreasing soap, metal powder, boiler chemicals,perchloroethylene, refrigerant oils, coil cleaners, and maintenance supplies. These materials are shipped/received in closed containers, loaded and unloaded in covered loading docks, and stored inside. Outfall SW001: Drainage area consists of a parking lot,part of the facility, diesel fuel tank, propane tank, trash and metal dumpsters, hydrogen cylinders, wooden pallet storage, loading/unloading dock, and drum storage. Outfall SWO02: Drainage area consists of a driveway, part of the facility, and grassy areas. Outfall SWO03: Drainage area consists of a loading/unloading dock, driveway, and grassy and forested areas. Outfall SWO04: Drainage area consists of a loading/unloading dock, mechanical storage trailers, and part of the facility. Outfall SWO05: Drainage area consists of raw materials silos (polyester chips), nitrogen tank, diesel fuel tank, transformers, and part of the facility. Page 1 of 7 Why Industrial Sites with Stormwater are Subject to a Permit: Federal NPDES regulations define stormwater discharge associated with industrial activity in 40 CFR §122.26 (b)(14) as: "the discharge from any conveyance that is used for collecting and conveying storm water and that is directly related to manufacturing,processing or raw materials storage areas at an industrial plant. The term does not include discharges from facilities or activities excluded from the NPDES program under this part 122. For the categories of industries identified in this section, the term includes, but is not limited to, storm water [sic] discharges from industrial plant yards; immediate access roads and rail lines used or traveled by carriers of raw materials, manufactured products, waste material, or byproducts used or created by the facility; material handling sites; refuse sites; sites used for the application or disposal of process waste waters (as defined at part 401 of this chapter); sites used for the storage and maintenance of material handling equipment; sites used for residual treatment, storage, or disposal; shipping and receiving areas; manufacturing buildings; storage areas (including tank farms) for raw materials, and intermediate and final products; and areas where industrial activity has taken place in the past and significant materials remain and are exposed to storm water. For the purposes of this paragraph, material handling activities include storage, loading and unloading, transportation, or conveyance of any raw material, intermediate product, final product, byproduct or waste product. The term excludes areas located on plant lands separate from the plant's industrial activities, such as office buildings and accompanying parking lots as long as the drainage from the excluded areas is not mixed with storm water [sic] drained from the above described areas." Section 2. Monitoring Information and Compliance History: • February 2015 to March 2023,benchmarks exceeded for: o Spring 2021 sampling event missed due to sampling technician contracting long-term Covid(per info provided 6/23/2023) o SW001: TSS 3x, pH min not reached 5x o SW002: pH min not reached 4x o SW003: pH min not reached 6x o SW004: COD 3x, pH min not reached Ix o SW005: TSS 3x, pH min not reached 3x • NOD issued February 2015 as site inspection noted qualitative and analytical monitoring had not been conducted and recorded • Per June 2023 inspection report: o SWPPP not implemented per permit requirements o Qualitative and analytical monitoring not conducted per permit requirements o Several benchmark exceedances noted in data available, but appropriate tiered response actions not taken o BMP summary and feasibility study not included in SWPPP o Erosion was observed near the outlet of Outfall 4 with recommendations of repair and groundcover stabilization • NOV issued June 2023 for violations of the SWPPP, qualitative monitoring, and analytical monitoring Page 2 of 7 Threatened/Endangered Species: There are not threatened/endangered species in the nearby vicinity of the facility, however, there is a species of concern: Copper Emerald(Somatochlora georgiana; NC status: SR) Section 3. Proposed Monitoring for Stormwater Discharges: The Division considered potential pollutants from past and present industrial activities and data was submitted for February 2015 to March 2023. Quantitative sampling included pH, TSS, COD, and one sample each of O&G, total phosphorus, TKN, and total nitrogen. Parameters are based on potential pollutants in the drainage area, sampling results, and in some cases, dependent upon future activities (e.g., ash removal through the drainage area). Below is a table of the proposed monitoring for each outfall at the Premiere Fibers site. Outfall SWO01 Quarterly monitoring Total Suspended Solids BASIS: Potential pollutant from drainage area and BMP effectiveness (TSS) indicator. Quarterly monitoring pH BASIS: Pollutant indicator Quarterly monitoring Total Rainfall BASIS: Discharge potential indicator Quarterly monitoring Non-Polar Oil &Grease BASIS: Potential pollutant from lubricants; Method 1664 SGT-HEM targets petroleum-based O&G Quarterly monitoring Monthly Oil Usage BASIS: Potential pollutant from drainage area Quarterly monitoring BOD BASIS: Discharge potential indicator Quarterly monitoring COD BASIS: Discharge potential indicator Page 3 of 7 Outfalls SW002, SW003, and SWO04 Quarterly monitoring Total Suspended Solids BASIS: Potential pollutant from drainage area and BMP effectiveness (TSS) indicator. Quarterly monitoring pH BASIS: Pollutant indicator Quarterly monitoring Total Rainfall BASIS: Discharge potential indicator Quarterly monitoring Non-Polar Oil &Grease BASIS: Potential pollutant from lubricants; Method 1664 SGT-HEM targets petroleum-based O&G Quarterly monitoring Monthly Oil Usage BASIS: Potential pollutant from drainage area Quarterly monitoring COD BASIS: Discharge potential indicator Outfall SWO05 Quarterly monitoring Total Suspended Solids BASIS: Potential pollutant from drainage area and BM? effectiveness (TSS) indicator. Quarterly monitoring pH BASIS: Pollutant indicator Quarterly monitoring Total Rainfall BASIS: Discharge potential indicator Quarterly monitoring Non-Polar Oil &Grease BASIS: Potential pollutant from lubricants; Method 1664 SGT-HEM targets petroleum-based O&G Quarterly monitoring Monthly Oil Usage BASIS: Potential pollutant from drainage area Quarterly monitoring COD BASIS: Discharge potential indicator Quarterly monitoring Total Nitrogen BASIS: Potential pollutant from drainage area Page 4 of 7 Stormwater Benchmarks and Tiered Response: Rather than limits,North Carolina NPDES Stormwater permits contain benchmark concentrations. Stormwater benchmarks are numerical action levels for stormwater monitoring. Benchmarks are not effluent limits, and benchmark exceedances are not permit violations. Benchmarks provide facilities a tool for assessing the significance of pollutants in stormwater discharges and the effectiveness of best management practices (BMPs). Benchmark concentrations are intended as guidelines for the facility's development and implementation of the Stormwater Pollution Prevention Plan (SWPPP). Benchmark exceedances require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater BMPs in a tiered program. The permit establishes a tiered approach to specify actions the permittee must take in response to analytical results above benchmark concentrations. The tiered structure of the permit provides the permittee and DEMLR wide flexibility to address issues that may arise with one or more parameters and/or outfalls. Metals benchmarks are calculated to mimic acute water quality standards and with the guidance of DWR. NC DWR follows established federal procedures for calculating acute standards when developing the benchmarks. Just like the acute standards, metals benchmarks normally reflect one half of the calculated Final Acute Value (the "1/2 FAV"). In most cases, translation into total recoverable values is based on an assumed hardness of 25 mg/L and a total suspended solids (TSS) concentration of 10 mg/L. Acute standards protect aquatic life from negative impacts of short-term exposure to higher levels of chemicals where the discharge enters a waterbody. The Stormwater Permitting Program applies this approach because of the ephemeral nature of rainfall events. The Division may evaluate results to determine if a smaller suite of parameters for some outfalls is adequate to characterize potential pollution or BMP effectiveness. For example, one or more metals or other parameters may serve as an adequate tracer for the presence of ash pollution during disturbance or ash removal in specific drainage areas at this site. For parameters that do not have a stormwater benchmark, the Division may develop a benchmark value if appropriate toxicity data become available or if rising trends in concentrations suggest a persistent source. A summary of the benchmarks in the draft permit, and their basis, is below: Parameter Benchmark Basis Total Suspended 100 mg/L National Urban Runoff Program(NURP) Study, 1983 Solids TSS H 6 s.u. —9 s.u. NC Water Quality Standard(Range) Non-Polar Oil & Review of other state's daily maximum benchmark Grease 15 mg/L concentration for this more targeted O&G;NC WQS that EPA Method 1664 does not allow oil sheen in waters SGT-HEM BOD 30 mg/L BPJ; Based on Secondary Treatment Regulation(40 CFR 133.03 COD 120 mg/L BPJ; Generally found at levels 4x BOD5 in domestic wastewaters Total Nitrogen 30 mg/L TKN +Nitrate+Nitrite Benchmarks (Expressed in mg/L of N Page 5 of 7 Stormwater Pollution Prevention Plan: The proposed permit conditions reflect the EPA and NC's pollution prevention approach to stormwater permitting. The Division's maintains that implementation of Best Management Practices (BMPs) and traditional stormwater management practices that control the source of pollutants meets the definition of Best Available Technology (BAT) and Best Conventional Pollutant Control Technology(BCT). The permit conditions are not numeric effluent limitations but are designed to be flexible requirements for implementing site-specific plans to minimize and control pollutants in stormwater discharges associated with the industrial activity. Title 40 Code of Federal Regulations (CFR) §122.44(k)(2) authorizes the use of BMPs in lieu of numeric effluent limitations in NPDES permits when the agency finds numeric effluent limitations to be infeasible. The agency may also impose BMP requirements which are "reasonably necessary" to carry out the purposes of the Act under the authority of 40 CFR 122.44(k)(3). The conditions proposed in this draft permit are included under the authority of both of these regulatory provisions. In essence, the pollution prevention and BMP requirements operate as limitations on effluent discharges that reflect the application of BAT/BCT. Flexibility in Tier Responses: Tier Two actions provide an opportunity for the permittee to propose an alternative monitoring plan for approval by the Region: • Alternatively, in lieu of steps 2 and 3, the permittee may, after two consecutive exceedances, exercise the option of contacting the DEMLR Regional Engineer as provided below in Tier Three. The Regional Engineer may direct the response actions on the part of the permittee as provided in Tier Three, including reduced or additional sampling parameters or frequency. • If pursuing the alternative above after two consecutive exceedances, the permittee may propose an alternative monitoring plan for approval by the Regional Engineer. The permit therefore allows the permittee to petition the Regional Office for monitoring changes sooner than Tier Three (upon any four benchmark exceedances) and gives guidance on one option to take. For example, the permittee may request that mercury only be monitored semi-annually under the tiers, or that only parameters over the benchmark be monitored more frequently. In this way, changes to the monitoring scheme for any outfall could be handled outside of a permit modification. Other Proposed Requirements: • It is standard for Stormwater Pollution Prevention Plan(SWPPP)requirements to include an annual certification that stormwater outfalls have been evaluated for the presence of non- stormwater discharges, and if any are identified, how those discharges are permitted or otherwise authorized. • Requirement to submit a request for permit modification if the facility identifies or creates any new outfalls, removes outfalls, or alters any drainage area that changes potential pollutants. • The Division expects the permittee to apply best professional judgment and consider the safety of its personnel in fulfilling sampling obligations under the permit. • Federal regulations require electronic submittal of all discharge monitoring reports (DMRs). If a state does not establish a system to receive such submittals, then permittees must submit DMRs electronically to the EPA. • Quarterly QualitativeNisual Monitoring to assure regular observation of outfalls throughout year. Section 4. Chances from previous permit to draft: • Monitoring increased from semi-annually to quarterly for all parameters (qualitative and quantitative) Page 6 of 7 • "No discharge" clarifications made • Feasibility study requirement removed per updated stormwater program requirements • eDMR requirement added • Boilerplate language moved into body of the permit; boilerplate no longer attached • Outfall-specific monitoring been implemented to reflect industrial activity and potential pollutants specific to each discharge area • Monitoring for BOD added to SW001 due to storage of wooden pallets in drainage area • Benchmarks updated for parameters per guidance from DWR Standards group on stormwater benchmarks Section 5. Changes from draft to final: • None Section 6. Discussions with the Facility and Regional Office: • Initial contact with facility: 3/3/2023 (requested permit application be submitted); acknowledgement sent 6/6/2023; Add info request sent 6/8/2023 • Initial contact with Regional Office: 6/8/2023 • Draft sent to CO peer review: N/A • Draft sent to Regional Office: 7/26/2023 • Final permit sent for supervisor signature: N/A Section 7. Comments received on draft permit: • Melissa Joyner(DEMLR FRO; via email 7/27/23): The NCS000528 draft permit for Premiere Fibers looks good. I do not have any further comments. Page 7 of 7 LOCALiQ StarNewsl The lispatchlTimes-News PO Box 631697 Cincinnati,OH 45263-1697 Sun Journal I The D IY News I The Star The Free Press I Gaston Gazette The Fayetteville Observer NORTH CAROLINA PROOF OF PUBLICATION ENVIRONMENTAL MANAGEMENT COMMISSION INTENT Brianna Young TO ISSUE Brlanna YoungNPDES STORMWATER DISCHARGE PERMITS Ncdeq Dernh The North Carolina Environ- 1612 Mail Service CTR mental Management Commission proposes to Raleigh NC27699-1600 issue NPDES stormwater discharge permits) to the person(s) listed below. Public comment or oblecticn STATE OF NORTH CAROLINA,COUNTY OF CUMBERLAND to Invited. Written W itten Permitshe draft comments regardingregarding the proposed The Fayetteville Observer,a newspaper distributed in the county permit will be accepted until YtY 30 daft after the publish date of Cumberland,published in the City of Fayetteville,County of of this notice and considered Cumberland,State of North Carolina printed and published and In the final determination P P regarding Permit Issuance personal knowledge of the facts herein state and that the notice and Permit provisions. The hereto annexed was Published in said newspapers in the issues Director of the NC Division of Energy, Mineral, and dated on: Land Resources (DEMLR) may hold a Public hearing Oa/02/2023 should there be a significant degree of public interest. Please mail comments and/or Information requests and that the fees charged are legal. The Fayetteville Observer to DEMLR at 1612 Mail was a newspaper meeting all the requirements and qualifications Service Center, Raleigh, NC prescribed by Sec. No. 1-597 G.S,of N.C. 27699-1612.. Premiere Fibers, LLC [PO Sworn to and subscribed before on 08/02/2023 Box 8930, Bristol, VA 2e203) has requested renewal of Permit NCS000528 for the Premiere Fibers facility in Anson County. This facility discharges to an unnamed tributary to Buffalo Creek In the Yadkin Pee-Dee River Basin. Interested Persons may visit DEMLR at 512 N. Salisbury Street, Raleigh, NC 27606 to review Information on file. Additional information on Legal Clerk NPDES permits and this s notice may be found on our website: httm://dea.nc.9ov/obout/dlvls Nota ,State of W1,County f Brown lons/ener9y-mineral-and- ry, LY land-resources/stormwa- ter/stormwater- /7�2 PrograMstormwater-public. notices, or by contacting My CAR1mISlOD expires Brlanna Young at Publication Cost: $207.89 9i9 nno.yvao7 noOdea.nc.gov or Order No: 9101575 a= 9101575 #of Copies: Customer No: 929332 ) PO#: THIS IS NOT AN INVOICE! Pfeare do not use thisform for pgytuear remittance. DENISE ROBERTS Notary Public t�CCj , State of Wisconsin C AUG 12013 E® 6X R•StormwaterPro9rarrt Page 1 of 1 Compliance Inspection Report Permit:NCS000528 Effective: 06/01/15 Expiration: 05/31/20 Owner: Premiere Fibers SOC: Effective: Expiration: Facility: Premiere Fibers County: Anson 10056 US Hwy 52 N Region: Fayetteville Ansonville NC 28007 Contact Person:Dewey Fulton Title: Phone: 276-645-9719 Directions to Facility: System Classifications: SWNC, Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): On-site representative Chris Fowler 910-995-0740 Related Permits: Inspection Date: 06/16/2023 Entry Time 10:30AM Exit Time: 12:45PM Primary Inspector:Melissa A Joyner Phone: Secondary Inspector(s): Denise Bruce Kelly Jonas Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Stormwater Discharge, Individual Facility Status: ❑ Compliant Not Compliant Question Areas: Storm Water (See attachment summary) Page 1 of 3 Permit: NCS000528 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for Visit: Routine Inspection Summary: The current permit expired on May 31, 2020. An application for the permit renewal has been submitted and is being processed with the renewed permit currently under draft review. An inspection was conducted to determine compliance with the conditions of the current/expired permit. Melissa Joyner, Denise Bruce and Kelly Jonas met with Mr. Chris Fowler, EHS Manager. The facility's Stormwater Pollution Prevention Plan (SWPPP), including the Analytical and Qualitative Monitoring records was reviewed. The SWPPP did not have documentation of the annual review and update which should include all items listed under Part Il,Section A, Item 8 of the current permit. The site map needed to be updated to include all items as listed under Part ll,Section A, Item 1 c of the permit. The Spill Prevention and Response Procedures (SPRP)did not include the dated names and signatures of the facility personnel responsible for implementing the SPRP. No records were available for review of the required semi-annual facility and stormwater system inspections. There was no documentation of the required annual Employee Training available for review during the inspection.A Best Manangement Practices Summary and Feasibility Study was not included in the SPPP. The Analytical and Qualitative Monitoring records were reviewed. In 2019, during Period 1, there were exceedances of the benchmark values for Total Suspended Solids(TSS), at Outfall 1 and for Chemical Oxygen Demand (COD) at Outfalls 4 and 5. Tier One response actions were not initiated in response to these exceedances. No Analytical and Qualitative Monitoring occurred during Period 1 in 2020. Qualitative Monitoring also did not occur during Period 2 in 2020 and Period 1 in 2021. During Period 2, in 2020 there was another exceedance of the benchmark value for TSS at Outfall 1. During Period 1 in 2022, at Outfall 4, there was an exceedance of the benchmark value for COD. In Period 2 in 2022, no discharges occurred at Outfalls 1-5. No monitoring occurred for Period 1 in 2023. At Outfall 4, during Period 2, in 2023, there was an exceedance of the benchmark value for COD.Tier One and Tier Two response actions have not been initiated for these benchmark exceedances. There have been two consecutive exceedances of COD at Outfall 4, not including the periods of non-dischargE and non-sampling. Therefore, per the Tier Two response actions, immediately initiate at Outfall 4 monthly Analytical and Qualitative Monitoring of all parameters until three consecutive sample results are below the benchmark value or within the benchmark range. Observations were made of site conditions including Outfalls 1-5. Erosion was observed near the outlet of Outfall 4 with recommendations of repair and groundcover stabilization. An open, uncovered container with liquid contents was observed on a pallet. Page 2 of 3 Permit: NCS000528 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? ❑ ❑ ❑ #Does the Plan include a General Location (USGS) map? ❑ ❑ ❑ #Does the Plan include a"Narrative Description of Practices"? ❑ ❑ ❑ #Does the Plan include a detailed site map including outfall locations and drainage areas? ❑ ❑ ❑ #Does the Plan include a list of significant spills occurring during the past 3 years? ❑ ❑ ❑ #Has the facility evaluated feasible alternatives to current practices? ❑ ❑ ❑ #Does the facility provide all necessary secondary containment? ❑ ❑ ❑ #Does the Plan include a BMP summary? ❑ ❑ ❑ #Does the Plan include a Spill Prevention and Response Plan (SPRP)? ❑ ❑ ❑ #Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ❑ ❑ ❑ #Does the facility provide and document Employee Training? 0 ❑ ❑ ❑ #Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ # Is the Plan reviewed and updated annually? ❑ 0 ❑ ❑ #Does the Plan include a Stormwater Facility Inspection Program? ❑ 0 ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? ❑ 0 ❑ ❑ Comment: The Stormwater Pollution Prevention Plan has not been implemented per the conditions of the permit. Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring? ❑ 0 ❑ ❑ Comment: Qualitative Monitoring has not been conducted per the conditions of the permit. Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ❑ 0 ❑ ❑ #Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ 0 ❑ Comment: Analytical Monitoring has not been conducted per the conditions of the permit. Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ❑ ❑ ❑ #Were all outfalls observed during the inspection? ❑ ❑ ❑ # If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ ❑ #Has the facility evaluated all illicit(non stormwater)discharges? ❑ 0 ❑ ❑ Comment: Page 3 of 3 ROY COOPER :is Governor ELIZABETH S.BISER � 4Y Secretary DOUGLAS R.ANSEL NORTH CAROLINA interim Director Environmental Quality June 27, 2023 CERTIFIED MAIL: 7010 1870 0003 47751683 RETURN RECEIPT REQUESTED Premiere Fibers Attn: Dewey Fulton P.O. Box 8930 Bristol, VA 24203 Subject: NOTICE OF VIOLATION (NOV-2023-PC-0269) Premiere Fibers NPDES Stormwater Individual Permit NCS000528 Anson County Dear Mr. Fulton: On June 16, 2023, Melissa Joyner, Kelly Jonas and Denise Bruce from the Fayetteville Regional Office of the Division of Energy, Mineral and Land Resources(DEMLR), conducted a site inspection for the Premiere Fibers facility located at 10056 US Hwy 52 N, Ansonville, Anson County, North Carolina. A copy of the Compliance inspection Report is enclosed for your review. Chris Fowler, EHS Manager was also present during the inspection and his time and assistance is greatly. appreciated. The site visit and file review revealed that the subject facility is covered by NPDES Stormwater Individual Permit NCS000528. Permit coverage authorizes the discharge of stormwater from the facility to receiving waters designated as an UT(un-named tributary)to Buffalo Creek, a Class C stream in the Yadkin-Pee Dee River Basin. As a result of the site inspection, the following permit conditions violations are noted: 1) Stormwater Pollution Prevention Plan (SWPPP) Per Part II, Section A...A Stormwater Pollution Prevention Plan (SWPPP) has not been properly implemented. 2)Qualitative Monitoring Per Part II, Section C...Qualitative monitoring has not been conducted and/or recorded in accordance with permit requirements. 3)Analytical Monitoring Per Part I, Section B...Analytical monitoring has not been conducted and/or recorded in accordance with permit requirements. Other Observations Please refer to the enclosed Compliance Inspection Report for additional comments and observations made during the inspection. Requested Response You are asked to respond to this office, in writing,within 30 calendar days from receipt of this notice.Your written response should include a reasonable explanation as to why the aforementioned violations have occurred as well as a Plan of Action to prevent these violations from recurring. Action Items Immediately review and amend the facility's SWPPP as needed and begin incorporating documentation pertaining to the annual update requirements of the permit. Conduct and record monitoring per the conditions of the permit. R' North Carolina Department of Environmental Quality I Division of Energy,Mineral and Land Resources .'e: D E� Fayetteville Regional Office 1225 Creep Street.Suite 7141 Fayetteville,North Carolina 28301 N:1R?F'C:A6?CiFANi. �F Thank you for your attention to this matter. This office requires that the violations, as detailed above, be properly resolved. These violations and any future violations are subject to a civil penalty assessment of up.to$25,000 per day for each violation. Should you have any questions regarding these matters, please contact Melissa Joyner or myself at(910) 433-3300. Sincerely, Ti othY�L.. LaBou PE Regional Engineer DEMLR TLLlmaj Enclosure: Compliance Inspection Report ec: Chris Fowler, EHS Manager— Premiere Fibers (via email) Toby Vinson, Jr., PE, CPESC, CPM, Chief of Program Operations—DEMLR (via email) Brad Cale, PE, Chief of Regional Operations—DEMLR (via email) Michael Lawyer, CPSWQ—Stormwater Program Supervisor—DEMLR (via email) Kieu Tran, Environmental Specialist, Stormwater Program— DEMLR (via email) DEMLR NPDES Stormwater Permit Laserfiche File CC" FRO — DEMLR, Stormwater Files Compliance Inspection Report Permit:NCS000528 Effective: 06/01/15 Expiration: 05/31/20 Owner: Premiere Fibers SOC: Effective: Expiration: Facility: Premiere Fibers County: Anson 10056 US Hwy 52 N Region: Fayetteville Ansonville NC 28007 Contact Person:Dewey Fulton Title: Phone:276-645-9719 Directions to Facility: System Classifications: SWNC, Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): On-site representative Chris Fowler 910-995-0740 Related Permits: Inspection Date: 06/16/2023 Entry Time10:30AM Exit Time: 12:45PM/Primary Inspector:Melissa A Joyner Phone: Secondary Inspector(s): Denise Bruce Kelly Jonas Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Stormwater Discharge, Individual Facility Status: ❑ Compliant 0 Not Compliant Question Areas: Storm Water (See attachment summary) Page 1 of 3 Permit: NCS000528 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for Visit: Routine Inspection Summary: The current permit expired on May 31, 2020.An application for the permit renewal has been submitted and is being processed with the renewed permit currently under draft review.An inspection was conducted to determine compliance with the conditions of the currentlexpired permit. Melissa Joyner, Denise Bruce and Kelly Jonas met with Mr. Chris Fowler, EHS Manager.The facility's Stormwater Pollution Prevention Plan (SWPPP), including the Analytical and Qualitative Monitoring records was reviewed.The SWPPP did not have documentation of the annual review and update which should include all items listed under Part 11,Section A, Item 8 of the current permit.The site map needed to be updated to include all items as listed under Part 11,Section A, Item 1 c of the permit. The Spill Prevention and Response Procedures(SPRP)did not include the dated names and signatures of the facility personnel responsible for implementing the SPRP. No records were available for review of the required semi-annual facility and stormwater system inspections.There was no documentation of the required annual Employee Training available for review during the inspection.A Best Manangement Practices Summary and Feasibility Study was not included in the SPPP. The Analytical and Qualitative Monitoring records were reviewed. In 2019, during Period 1, there were exceedances of the benchmark values for Total Suspended Solids(TSS), at Outfall 1 and for Chemical Oxygen Demand (COD)at Outfalls 4 and 5. Tier One response actions were not initiated in response to these exceedances. No Analytical and Qualitative Monitoring occurred during Period 1 in 2020. Qualitative Monitoring also did not occur during Period 2 in 2020 and Period 1 in 2021. During Period 2, in 2020 there was another exceedance of the benchmark value for TSS at Outfall 1. During Period 1 in 2022, at Outfall 4, there was an exceedance of the benchmark value for COD. In Period 2 in 2022, no discharges occurred at Outfalls 1-5. No monitoring occurred for Period 1 in 2023.At Outfall 4, during Period 2, in 2023, there was an exceedance of the benchmark value for COD.Tier One and Tier Two response actions have not been initiated for these benchmark exceedances. There have been two consecutive exceedances of COD at Outfall 4, not including the periods of non-discharg( and non-sampling.Therefore, per the Tier Two response actions, immediately initiate at Outfall 4 monthly Analytical and Qualitative Monitoring of all parameters until three consecutive sample results are below the benchmark value or within the benchmark range. Observations were made of site conditions including Outfalls 1-5. Erosion was observed near the outlet of Outfall 4 with recommendations of repair and groundcover stabilization. An open, uncovered container with liquid contents was observed on a pallet. Page 2of3 Permit: NCS000628 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? 0 ❑ ❑ ❑ #Does the Plan include a General Location(USGS)map? 0 ❑ ❑ ❑ #Does the Plan include a"Narrative Description of Practices"? 0 ❑ ❑ ❑ #Does the Plan include a detailed site map including outfall locations and drainage areas? E ❑ ❑ ❑ #Does the Plan include a list of significant spills occurring during the past 3 years? ❑ W ❑ ❑ #Has the facility evaluated feasible alternatives to current practices? ❑ 0 ❑ ❑ #Does the facility provide all necessary secondary containment? N ❑ ❑ ❑ #Does the Plan include a BMP summary? ❑ 0 ❑ ❑ #Does the Plan include a Spill Prevention and Response Plan(SPRP)?. 0 ❑ ❑ ❑ #Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? E ❑ ❑ ❑ #Does the facility provide and document Employee Training? E ❑ ❑ ❑ #Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ #Is the Plan reviewed and updated annually? ❑ 0 ❑ ❑ #Does the Plan include a Stormwater Facility Inspection Program? ❑ 0 ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? ❑ 0 ❑ ❑ Comment: The Stormwater Pollution Prevention Plan has not been implemented per the conditions of the permit. Qualitative Monitorina Yes No NA NE Has the facility conducted its Qualitative Monitoring? ❑ E ❑ ❑ Comment: Qualitative Monitoring has not been conducted per the conditions of the permit. Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ❑ 0 ❑ ❑ #Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ E ❑ Comment: Analytical Monitoring has not been conducted per the conditions of the permit. Permit and Outfalis Yes No NA NE #Is a copy of the Permit and the Certificate of Coverage available at the site? ❑ ❑ ❑ #Were all outfalls observed during the inspection? 0 ❑ ❑ ❑ #If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ ❑ #Has the facility evaluated all illicit(non stormwater)discharges? 110 ❑ ❑ Comment: Page 3 of 3 Compliance Inspection Report Permit:NCS000528 Effective: 06/01/15 Expiration: 05/31/20 Owner: Premiere Fibers SOC: Effective: Expiration: Facility: Premiere Fibers County: Anson 10056 US Hwy 52 N Region: Fayetteville Ansonville NC 28007 Contact Person:Dewey Fulton Title: Phone: 276-645-9719 Directions to Facility: System Classifications: SWNC, Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): On-site representative Chris Fowler 910-995-0740 Related Permits: Inspection Date: 06/16/2023 Entry Time 10:30AM Exit Time: 12:45PM Primary Inspector:Melissa A Joyner Phone: Secondary Inspector(s): Denise Bruce Kelly Jonas Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Stormwater Discharge, Individual Facility Status: ❑ Compliant Not Compliant Question Areas: Storm Water (See attachment summary) Page 1 of 3 Permit: NCS000528 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for Visit: Routine Inspection Summary: The current permit expired on May 31, 2020. An application for the permit renewal has been submitted and is being processed with the renewed permit currently under draft review. An inspection was conducted to determine compliance with the conditions of the current/expired permit. Melissa Joyner, Denise Bruce and Kelly Jonas met with Mr. Chris Fowler, EHS Manager. The facility's Stormwater Pollution Prevention Plan (SWPPP), including the Analytical and Qualitative Monitoring records was reviewed. The SWPPP did not have documentation of the annual review and update which should include all items listed under Part Il,Section A, Item 8 of the current permit. The site map needed to be updated to include all items as listed under Part ll,Section A, Item 1 c of the permit. The Spill Prevention and Response Procedures (SPRP)did not include the dated names and signatures of the facility personnel responsible for implementing the SPRP. No records were available for review of the required semi-annual facility and stormwater system inspections. There was no documentation of the required annual Employee Training available for review during the inspection.A Best Manangement Practices Summary and Feasibility Study was not included in the SPPP. The Analytical and Qualitative Monitoring records were reviewed. In 2019, during Period 1, there were exceedances of the benchmark values for Total Suspended Solids(TSS), at Outfall 1 and for Chemical Oxygen Demand (COD) at Outfalls 4 and 5. Tier One response actions were not initiated in response to these exceedances. No Analytical and Qualitative Monitoring occurred during Period 1 in 2020. Qualitative Monitoring also did not occur during Period 2 in 2020 and Period 1 in 2021. During Period 2, in 2020 there was another exceedance of the benchmark value for TSS at Outfall 1. During Period 1 in 2022, at Outfall 4, there was an exceedance of the benchmark value for COD. In Period 2 in 2022, no discharges occurred at Outfalls 1-5. No monitoring occurred for Period 1 in 2023. At Outfall 4, during Period 2, in 2023, there was an exceedance of the benchmark value for COD.Tier One and Tier Two response actions have not been initiated for these benchmark exceedances. There have been two consecutive exceedances of COD at Outfall 4, not including the periods of non-dischargE and non-sampling. Therefore, per the Tier Two response actions, immediately initiate at Outfall 4 monthly Analytical and Qualitative Monitoring of all parameters until three consecutive sample results are below the benchmark value or within the benchmark range. Observations were made of site conditions including Outfalls 1-5. Erosion was observed near the outlet of Outfall 4 with recommendations of repair and groundcover stabilization. An open, uncovered container with liquid contents was observed on a pallet. Page 2 of 3 Permit: NCS000528 Owner-Facility:Premiere Fibers Inspection Date: 06/16/2023 Inspection Type:Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? ❑ ❑ ❑ #Does the Plan include a General Location (USGS) map? ❑ ❑ ❑ #Does the Plan include a"Narrative Description of Practices"? ❑ ❑ ❑ #Does the Plan include a detailed site map including outfall locations and drainage areas? ❑ ❑ ❑ #Does the Plan include a list of significant spills occurring during the past 3 years? ❑ ❑ ❑ #Has the facility evaluated feasible alternatives to current practices? ❑ ❑ ❑ #Does the facility provide all necessary secondary containment? ❑ ❑ ❑ #Does the Plan include a BMP summary? ❑ ❑ ❑ #Does the Plan include a Spill Prevention and Response Plan (SPRP)? ❑ ❑ ❑ #Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ❑ ❑ ❑ #Does the facility provide and document Employee Training? 0 ❑ ❑ ❑ #Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ # Is the Plan reviewed and updated annually? ❑ 0 ❑ ❑ #Does the Plan include a Stormwater Facility Inspection Program? ❑ 0 ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? ❑ 0 ❑ ❑ Comment: The Stormwater Pollution Prevention Plan has not been implemented per the conditions of the permit. Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring? ❑ 0 ❑ ❑ Comment: Qualitative Monitoring has not been conducted per the conditions of the permit. Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ❑ 0 ❑ ❑ #Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ 0 ❑ Comment: Analytical Monitoring has not been conducted per the conditions of the permit. Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ❑ ❑ ❑ #Were all outfalls observed during the inspection? ❑ ❑ ❑ # If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ ❑ #Has the facility evaluated all illicit(non stormwater)discharges? ❑ 0 ❑ ❑ Comment: Page 3 of 3 Young, Brianna A From: Phil Rahn <prahn@watersedgeenv.com> Sent: Thursday,July 20, 2023 1:44 PM To: Young, Brianna A; Dewey Fulton; Chris Fowler Subject: Fwd: [External]Fwd: [External] Additional Questions for Premiere Fiber NPDES Permit Application CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Answers to your circled questions below. Top center of the picture is a dry van trailer (empty), to the right of that in the field is a groundwater pump house for the groundwater. On the east side in the middle is a pad area with transformers sitting on it. On the west side, those are air accumulators. ---------- Forwarded message--------- From: Chris Fowler<cfowler@premierefibers.com> Date: Wed,Jul 19, 2023 at 2:03 PM Subject: RE: [External]Fwd: [External] Additional Questions for Premiere Fiber NPDES Permit Application To: Phil Rahn <prahn@watersedgeenv.com>, Dewey Fulton <dewey.fulton@universalfibers.com> Top center of the picture is a dry van trailer(empty),to the right of that in the field is a freshwater pump house for the ground water. On the east side in the middle is the ground with transformers sitting on it. On the west side,those are air accumulators. Chris Fowler EHS Manager Premiere Fibers 10056 US 52 Ansonville, NC 28007 Office: 704-826-1100 Cell: 910-995-0740 Email:cfowler@premierefibers.com i From: Phil Rahn <prahn@watersedgeenv.com> Sent:Wednesday,July 19, 2023 1:53 PM To: Dewey Fulton <dewey.fulton@universalfibers.com>; Chris Fowler<cfowler@premierefibers.com> Subject: [External]Fwd: [External] Additional Questions for Premiere Fiber NPDES Permit Application [EXTERNAL EMAIL] Will obviously rely on you guys to help respond to this request. Sent from my iPhone Begin forwarded message: From: "Young, Brianna A" <Brianna.Young@deq.nc.gov> Date:July 19, 2023 at 1:39:53 PM EDT To: Phil Rahn <prahn@watersedgeenv.com>, Dewey Fulton <dewey.fulton@universalfibers.com> Subject: RE: [External]Additional Questions for Premiere Fiber NPDES Permit Application Good afternoon, After reviewing the site map again in conjunction with your answers below,there are a few items/structures with unidentified purposes. Please see the attached map and identify the items outlined in red boxes. Thank you, Brianna Young, MS(she/her) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/Division of Energy, Mineral, and Land Resources (DEMLR) Brianna.Young@deg.nc.gov(e-mail preferred)PLEASE NOTE NEW EMAIL ADDRESS **DEQ is updating its email addresses to @deg.nc.aov in phases from May 1st to June 9th. Employee email addresses may look different, but email performance will not be impacted. 2 919-707-3647 (office) Mailing address: 1612 Mail Service Center, Raleigh, NC 27699-1612 Physical address: 512 North Salisbury Street, Raleigh, NC 27604 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. The Department of Environmental Quality has adjusted operations to protect the health and safety of the staff and public. Please check with the appropriate staff before visiting our offices,as we may be able to handle your requests by phone or email. From: Phil Rahn <prahn@watersedReenv.com> Sent:Tuesday,July 18, 2023 2:18 PM To:Young, Brianna A<Brianna.YounR@deg.nc.Rov>; Dewey Fulton <Dewey.Fulton @universalfibers.com> Subject: [External] Additional Questions for Premiere Fiber NPDES Permit Application CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- You had some additional questions which Dewey and I have tried to answer below: 1. There are used wooden pallets stored outside until an amount for pickup. Used pallets are stored on the North side of the facility, location reference see Figure 3 near E (trash dumpster). There are also 2 totally enclosed storage trailers on the East side of the building used to store electrical and mechanical materials, location reference see Figure 3 near MW-4. 2. There are utility transformers on the east side of the main building and one additional transformer on the south side of the main building. 3. The materials listed are all stored inside and loaded and unloaded in covered loading docks. I don't understand the possibility of contact with storm water. Perchloroethylene and refrigerant oils are no longer on site. 4. There is no industrial activity in storm water outfall areas. 5. Dumpsters are located on the north side of the building(see Figure 3 of the permit application). 3 Hope this provides additional clarification. Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third arties b an authorized state official. 5 s y i 5'.'k;A • 1LKi i i . 7 4 1 •11 k 4 Young, Brianna A From: Phil Rahn <prahn@watersedgeenv.com> Sent: Tuesday, July 18, 2023 2:18 PM To: Young, Brianna A; Dewey Fulton Subject: [External] Additional Questions for Premiere Fiber NPDES Permit Application CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- You had some additional questions which Dewey and I have tried to answer below: 1. There are used wooden pallets stored outside until an amount for pickup. Used pallets are stored on the North side of the facility, location reference see Figure 3 near E (trash dumpster). There are also 2 totally enclosed storage trailers on the East side of the building used to store electrical and mechanical materials, location reference see Figure 3 near MW-4. 2. There are utility transformers on the east side of the main building and one additional transformer on the south side of the main building. 3. The materials listed are all stored inside and loaded and unloaded in covered loading docks. I don't understand the possibility of contact with storm water. Perchloroethylene and refrigerant oils are no longer on site. 4. There is no industrial activity in storm water outfall areas. 5. Dumpsters are located on the north side of the building(see Figure 3 of the permit application). Hope this provides additional clarification. Young, Brianna A From: Phil Rahn <prahn@watersedgeenv.com> Sent: Tuesday, July 18, 2023 2:18 PM To: Young, Brianna A; Dewey Fulton Subject: [External] Additional Questions for Premiere Fiber NPDES Permit Application CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- You had some additional questions which Dewey and I have tried to answer below: 1. There are used wooden pallets stored outside until an amount for pickup. Used pallets are stored on the North side of the facility, location reference see Figure 3 near E (trash dumpster). There are also 2 totally enclosed storage trailers on the East side of the building used to store electrical and mechanical materials, location reference see Figure 3 near MW-4. 2. There are utility transformers on the east side of the main building and one additional transformer on the south side of the main building. 3. The materials listed are all stored inside and loaded and unloaded in covered loading docks. I don't understand the possibility of contact with storm water. Perchloroethylene and refrigerant oils are no longer on site. 4. There is no industrial activity in storm water outfall areas. 5. Dumpsters are located on the north side of the building(see Figure 3 of the permit application). Hope this provides additional clarification. Young, Brianna A From: Young, Brianna A Sent: Friday, June 30, 2023 3:21 PM To: Phillip Rahn; Dewey Fulton Subject: RE: [External] Additional Questions for Premiere NPDES Permit Application Good afternoon, Thank you for providing this information. After reviewing everything, I have a few follow-up questions. 1. Are wooden pallets and/or storage trailers outside? 2. Is there an electrical transformer located onsite? If so, please indicate where. 3. What materials are shipped/received from the facility? Information in the permit history indicates materials that could potentially be exposed to stormwater include yarn,finish oils, degreasing soap, metal powder, boiler chemicals, perchloroethylene, refrigerant oils, coil cleaners, and maintenance supplies. 4. You provided information on what appears to be industrial activities in the drainage areas outside of the facility. I apologize if this was not clear in my last request. Please confirm the activities taking place in drainage areas for each outfall of the facility(SW001 through SW005). 5. Please confirm what drainage area the 2 dumpsters on east side of facility are in. Please let me know if you have any questions on this request. Thank you, Brianna Young, MS(she/her) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/Division of Energy, Mineral, and Land Resources (DEMLR) Brlanna.Young@deg.nc.gov(e-mail preferred)PLEASE NOTE NEW EMAIL ADDRESS **DEQ is updating its email addresses to @deq.nc.gov in phases from May 1st to June 9th. Employee email addresses may look different, but email performance will not be impacted. 919-707-3647 (office) Mailing address: 1612 Mail Service Center, Raleigh, NC 27699-1612 Physical address: 512 North Salisbury Street, Raleigh, NC 27604 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. The Department of Environmental Quality has adjusted operations to protect the health and safety of the staff and public. Please check with the appropriate staff before visiting our offices, as we may be able to handle your requests by phone or email. From: Phillip Rahn <prahn@watersedgeenv.com> Sent: Friday,June 23, 2023 4:29 PM To:Young, Brianna A<Brianna.Young@deq.nc.gov>; Dewey Fulton <Dewey.Fulton@universalfibers.com> Subject: [External] Additional Questions for Premiere NPDES Permit Application 1 CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- I have tried to answer the additional questions raised for the Premiere NPDES Permit Application from your earlier email.They are attached to this email. Have a good weekend. Phil Rahn P.G. President Waters Edge Environmental, LLC 1434 Chester Road Raleigh, NC 27608 919.219.5820 (cell) prahn@watersedgeenv.com (email) watersedgeenvironmenta1.net (website) 2 WATERS EDGE ENVIRONMENTAL,LLC 1434 CHESTER ROAD • RALEIGH, N.C.27608 • PHONE 919.219.5820 MEMORANDUM Date June 23, 2023 To Brianna Young, MS Industrial Individual Permits Coordinator Stormwater Permitting Program From Mr. Phil Rahn P.G. - Waters Edge Copy Mr. Dewey Fulton - Premiere Fibers Subject Additional DEQ Requests Premiere Fibers NPDES Permit Renewal 10056 US S.R. 52N Ansonville, North Carolina 28007 Stormwater Permit No. NCS000528 Waters Edge Job No. R9-21 You had sent an email requesting Premiere to provide additional information. We have provided answers to each request in italics as follows: • Description of chemicals stored onsite; Answer We have provided a list contained in Appendix A;however, we would state that the only chemicals stored outside the building is fuel oil used to fire the boilers. The remaining chemicals are stored inside and should not be subject to any stormwater runoff. • Description of industrial activity in each drainage area; Answer The drainage areas depicted in the May 23, 2023 NPDES permit application (Figure 1) are in an area outside ofAnsonville that has no development other than residential or farming so there would be no industrial activity. • An electronic spreadsheet summarizing all of the monitoring data (visual and analytical)that has been collected since the effective date of the current permit; Answer We have provided a spreadsheet of the analytical data since the effective date of the currentpermit in AppendixB. Please realize that some of the Outfalls do not have flow during rain events and we missed the Spring 2021 sampling interval since our sampling technician contacted long-term Covid. We could not make an Excel spreadsheet of the visual data, but it is included in all of our individual submittals to NCDEQ. Additional DEQ Requests Premiere Fibers NPDES Permit Renewal 10056 US S.R. 52N Ansonville,North Carolina 28007 June 23,2023 Page 2 of 2 • Table D of EPA Form 217; Answer We have included Table D in Appendix C. • Summary of onsite BMPs; Answer The onsite BMPs have not changed since what was stated in the February 24, 2009 Stormwater PPP which is contained in Appendix D. • Summary of significant changes that have occurred at the site since the last permit renewal. Answer There have been no changes since the last permit renewal. If there are any questions, please contact me at prahn(a,watersedgeenv.com or 919.219.5820. APPENDIX A List of Chemicals Stored at Premiere Fibers Ansonville, North Carolina Spin Finish Spin finish concentrate composition and the oil-in-water emulsion made from the concentrate for application for conventional speed or high speed melt spinning processes for producing polyester or polyamide yarns, consists essentially of oil lubricant component, pentaerythritol ester lubricant, ethoxylated sorbitan monooleate of HLB ranging from 6 to 15, anionic antistatic agent, water soluble sulfosuccinate wetting agent, and oil soluble ethoxylated polymethylsiloxane wetting agent having molecular weight of 400 to 700 and an aqueous surface tension value of less than 21 dynes/cm. The concentrate has long term stability. Dowtherm Versatile Heat Transfer Fluid that can operate in either liquid or vapor phases in order to collect,transport, and store heat in a variety of heat transfer applications, such as concentrated solar power(CSP)systems. DOWTHERMTM A Heat Transfer Fluid is designed to provide a consistent and reliable source of heat transfer at high temperature applications up to 400°C (750°F) Fuel oil No. 2 fuel oil (heating oil): A distillate fuel oil that has a distillation temperatures of 400 degrees Fahrenheit at the 10-percent recovery point and 640 degrees Fahrenheit at the 90-percent recovery point and meets the specifications defined in ASTM Specification D 396. Compressor oil A long life PAO oil, specifically developed for use in Atlas Copco oil injected screw compressors. (PAO) fluids are the most common major synthetic base oil used in industrial and automotive lubricants. These synthetic hydrocarbons are designed to provide superior lubrication performance over a wider operating- temperature range than petroleum oils and typically are less volatile. Listing of Individual Chemicals Contained Inside Building at Premiere Fibers Item No Description U/M Store Location THERMINOL Therminol LT, Heat Transfer Fluid 55 al drum DRUM 508716 Chemical, Air washer MG-200, 5 Gallon EA PART ROOM 508570 Chemical, Air washer CL-4005 , 5 Gallon EA PART ROOM 508569 Chemical, Corrosion lnhibitor,CL-6050MB EA PART ROOM Cooling Tower ,Chen 508568 Microguard, MG-906, Biocide Cooling Tower EA PART ROOM Chemical, 5-Gallon 508567 Chemical, Air washer CL-4550, 5 Gallon EA PART ROOM 508566 Peroxide, Chemical, CL-10, 5 Gallon EA PART ROOM 508391 Coverage Plus,NPD (4 X 1 Gallon Plastic Bottles) CASE - Fiberboard B- 507679 Cleaner, Alkaline, 55 Gallon Drum, Metal Medic G PROD.SERV 7035, Sodium Hydroxide 507621 Coil Cleaner, Evaporative Foam No Rinse EA PART ROOM Eva orator, 6 of Nu-Cal on 507562 Cleaner/Degreaser, 55 gallon Water-Based, Clear G PART ROOM Yellowish, For O 507534 Reagent,Hexane(s) ACS, Minimum Assay 95% n- EA PART ROOM Hexane 507255 Hydrogen Peroxide, 35%, 5 Gallon(20L) Drum, DRUM PART ROOM Technical Grade 506962 Reagent, C3270240-2.5Y, Phenol/1,1,2,2- EA Tetrachloro ethane, 506595 Acetone, 5 Gallon,20L Pail, CAS # 67-64-1, EA PART ROOM CH3COCH-3 506288 Petroleum Ether A.C.S Reagent, in Poly coated Ltr PART ROOM Bottles 506169 Solution, Godet Cleaner BGC 2009, 5Litre, EA PART ROOM F/Cleaning Godet SL 506067 Trieth lene Glycol LBS PART ROOM 505696 Argon Industrial Shielding Gas Mix, Size 300 EA PART ROOM C linder, CGA-580 505594 Hydrofluoric Acid, 48%, 1L EA PART ROOM 504925 Urethane Conformal Coating, Aerosol, 12 FL.OZ EA ELECT.SHOP 504752 Kit, Acid Treatment, Spill-X, 6 - 2-lb. Shaker EA PART ROOM Bottles 504439 Coil Cleaner, No Rinse, Aerosol, 18 Oz, EA PART ROOM Evaporator Cleaner 504198 Nitrogen Gas Cylinder, Nitrogen Industrial 300 EA PART ROOM Vol-608.00 FT 504152 Acid, Hydrochloric, Reagent ACS 21/2L EA PART ROOM 503740 1 Sodium Phosphate Monobasic,Reagentplus 500G I DRUM I PART ROOM 503556 lsopropyl Alcohol , 1 Gallon, 99% EA ELECT.SHOP 503536 Nitric Acid, 1% (V/V) Aqueous Volumetric EA PART ROOM Solution, 2.5L 503420 Biocide, Ultra Kleen Solution-2, 5G SXBSXS2- EA PROD.SERV 0047 503419 Biocide, Ultra Kleen Solution-1, 5G SXBI-0041 EA PROD.SERV 503411 Brakleen, 19 fl. oz,Brake Parts Cleaner Aerosol EA PART ROOM 503371 Sodium Hydroxide, Purified pellets, 500G/Case CASE PROD.SERV 503285 Chemical pump, with programmable timer EA PART ROOM 503217 Minimal Expansion Foam, 12 Wt. Oz, CRC- EA ELECT.SHOP 14077 502874 Parts-Wash Solution, Gen. Purpose, Liquid EA PART ROOM Formula, 5 Gallon Size 502745 Acid dye for Nylon,PERMALON VIOLET FBL LBS PART ROOM 180% 502587 Xceltherm LVI, Heat transfer Fluid 55 Gallon EA WNDR.SHOP Drum Dowtherm A E 502404 Acetic Acid, 2.5L, Poly-Coated Glass Bottle EA PART ROOM 502277 Solution, Rydlyme, Biodegradeable Descaler, 55 DRUM PART ROOM Gallon Drum 502273 Pyrophosphate Tetrasodium, 500G DRUM PART ROOM 501825 Soduim DiH dro en Phosphate Extra Pure EA PART ROOM 501620 Xceltherm MKI, Heat transfer Fluid 55 Gallon EA WNDR.SHOP Drum Dowtherm A 501360 Grease, AUTOL TOP 2000 EA PART ROOM 501260 Cleaner, Alkaline, EZE 2945, 50 Gallon Drum/ LBS PROD.SERV 598 LBS 501013 Hydrogen Peroxide, 35%, 15 Gallon Drum, DRUM PART ROOM Technical Grade 500945 Oxygen Gas Cylinder, OXY Industrial 282 CF EA PART ROOM 500944 Argon Gas Cylinder, ARGON Industrial 336 CF, EA PART ROOM 500675 Cleaner, Contact, CRC2000 QD EA ELECT.SHOP 500504 Cleaner, Contact, CRC2000 EA ELECT.SHOP 500299 Perchloro ethylene, Freon Grade (55Gal Drum), DRUM PART ROOM 700Lbs 500280 Solution, Cleaning, PRODAN (IOLitre) EA PART ROOM 500081 Super Rustripper, Oakite LBS PROD.SERV 500080 Biocide, Acticide LA LBS PROD.SERV 400117 Reprocess Dowtherm A LBS WNDRSHOP APPENDIX B Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 001 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 4/24/18 Threshold Total Suspended Solids mg/L 100 231 5.5 57.0 2.9 5.0 39.2 159 BDL pH SU 6.0-9.0 4.0 6.7 6.3 5.9 6.4 6.5 6.2 NA Chemical Oxygen mg/L 120 BDL BDL BDL 46.0 BDL BDL BDL NA T)Pmand NCDENR Analytical Parameter Units Permit 8/2/18 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 Threshold Total Suspended Solids mg/L 100 2.8 1,250 8.9 10.2 9.4 No Flow 2.6 BDL pH SU 6.0-9.0 6.0 5.4 NA 6.1 5.1 No Flow 5.1 6.2 Chemical Oxygen mg/L 120 BDL 45.7 NA BDL BDL No Flow BDL BDL n rl NCDENR Analytical Parameter Units Permit 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 No Flow No Flow pH SU 6.0-9.0 No Flow No Flow Chemical Oxygen mg/L 120 No Flow No Flow M-M!And SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 001 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 002 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 4.6 38.2 BDL BDL 5.5 BDL BDL BDL pH SU 6.0-9.0 6.1 6.5 6.3 6.5 6.5 6.6 6.3 6.3 Chemical Oxygen llPmnn mg/L 120 BDL BDL BDL BDL BDL BDL BDL BDL NCDENR Analytical Parameter Units Permit 6/7/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 BDL 5.3 34.0 7.7 5.7 BDL No Flow 3.7 pH SU 6.0-9.0 5.6 6.4 5.8 5.6 4.2 6.2 No Flow 6.2 Chemical Oxygen mg/L 120 BDL BDL 27.3 BDL BDL BDL No Flow BDL nt-mnnd NCDENR Analytical Parameter Units Permit Threshold Total Suspended Solids mg/L 100 pH SU 6.0-9.0 Chemical Oxygen mg/L 120 SU-Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 002 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 003 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 4.1 15.1 12.3 67.9 2.6 5.3 26.8 10.1 pH SU 6.0-9.0 6.1 6.0 6.0 6.2 5.9 6.5 6.2 5.5 Chemical Oxygen llPmnn mg/L 120 BDL BDL BDL BDL BDL BDL BDL BDL NCDENR Analytical Parameter Units Permit 6/7/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 9.2 5.0 8.9 4.0 10.6 23.6 No Flow 11.0 pH SU 6.0-9.0 5.5 6.3 6.2 5.0 5.3 6.1 No Flow 5.9 Chemical Oxygen mg/L 120 38.6 BDL BDL BDL BDL 30.3 No Flow 31.6 nt-mnnd NCDENR Analytical Parameter Units Permit Threshold Total Suspended Solids mg/L 100 pH SU 6.0-9.0 Chemical Oxygen 11,E 120 DPMnnfI SU-Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 003 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 004 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 19.8 6.5 54.8 35.2 23.2 BDL 16.9 24.6 pH SU 6.0-9.0 8.3 6.3 6.8 6.9 6.3 7.2 6.9 6.3 Chemical Oxygen mg/L 120 45 BDL 94.0 97.0 34.0 BDL 88.0 37.9 T)Pmanrl NCDENR Analytical Parameter Units Permit 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 Threshold Total Suspended Solids mg/L 100 18.0 NA 9.2 20.3 23.3 9.9 15.7 7.0 pH SU 6.0-9.0 6.1 NA 7.0 7.0 6.8 5.9 6.8 7.6 Chemical Oxygen mg/L 120 136 258 104 58.4 59.5 25.7 125 41.1 n rl NCDENR Analytical Parameter Units Permit 3/2/23 Threshold Total Suspended Solids mg/L 100 7.7 pH SU 6.0-9.0 6.7 Chemical Oxygen mg/L 120 90.2 ilPmanrl SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 004 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 005 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 10/23/17 3/1/18 Threshold Total Suspended Solids mg/L 100 54.5 5.9 33.0 15.9 51.3 115 24.7 27.9 pH SU 6.0-9.0 8.3 6.3 7.1 6.9 6.4 6.8 6.8 6.5 Chemical Oxygen mg/L 120 BDL BDL 97.0 107 63.0 BDL 310 107 T)Pmand NCDENR Analytical Parameter Units Permit 8/2/18 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 Threshold Total Suspended Solids mg/L 100 27.5 96.5 NA 100 19.6 187 39.8 3.8 pH SU 6.0-9.0 6.3 6.2 NA 4.3 5.9 6.9 5.9 6.5 Chemical Oxygen mg/L 120 28.4 148 275 85.0 51.7 78.9 28.0 BDL n rl NCDENR Analytical Parameter Units Permit 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 8.6 5.3 pH SU 6.0-9.0 7.4 6.6 Chemical Oxygen mg/L 120 48.3 76.2 ilPmanrl SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 005 APPENDIX C EPA Identification Number NPDES Permit Number Facility name Outfall Number Form Approved 03/05/19 NCD986230159 NCS000528 Premiere Fibers 001-005 OMB No.2040-0004 STORMTABLE D. • ' • I Provide data for the storm event(s)that resulted in the maximum daily discharges for the flow-weighted composite sample. Number of Hours Between Total Rainfall During Maximum Flow Rate Duration of Storm Event (in inches) Beginning of Storm Measured and (in gpm or specify units) Total Flow from Rain Event Date of Storm Event (in hours) Storm Event End of Previous Measurable Rain During Rain Event (in gallons or specify units) Event 06/19/2023 Approximately 1 hour .31" 4/23-4/27, approximately 96 hours 5GPM 300 gal.from each outfall Provide a description of the method of flow measurement or estimate. Flow from each outfall 001-005 are discharged at the invert of a reinforced concrete pipe. No flow meters or measuring devices are in use. However,the predominant flow originates from roof drains.The discharge is rapid flowing and the duration is very limited upon cessation of the rain event.Some laminar flow is caught in the outfall 003 catch basin from the asphalt drive.Minimal flow is observed on the gravel and asphalt areas and is captured within the grassy areas.This water is moved to drainage features along the North,South and West due to the grade of the landscape.Total flow was estimated at 5 GPM for 60 minutes. Click to go back to the beginning of Form EPA Form 3510-21F(Revised 3-19) Page 13 APPENDIX D STORM WATER POLLUTION PREVENTION PLAN PREMIERE FIBERS, INC. 10056 US HIGHWAY 52 NORTH ANSONVILLE , NORTH CAROLINA 1175/1176 :0.'s: Premiere jf��1 P I B E R S Pe•pa ..i I...I — STORM WATER POLLUTION PREVENTION PLAN PREMIERE FIBERS, INC. 10056 US HIGHWAY 52 NORTH ANSONVILLE, NORTH CAROLINA Prepared for: PREMIERE FIBERS, INC Prepared by: PREMIERE FIBERS, INC. ANSONVILLE, N.C. February 24th 2009 :s:'s: Premiere "ll F I B E R S 'P_P_..I Innovaion TABLE OF CONTENTS Page No. 1.0 INTRODUCTION 1 2.0 POLLUTION PREVENTION TEAM 1 3.0 COMPARISON WITH OTHER PLANS 2 4.0 DESCRIPTION OF POTENTIAL POLLUTION SOURCES 2 4.1 FACILITY SITE MAP 2 4.2 INVENTORY OF EXPOSED MATERIALS 2 4.3 NON-STORM WATER DISCHARGES 2 4.4 STORM WATER MONITORING DATA 5 4.5 POLLUTANT SOURCE IDENTIFICATION 5 5.0 MEASURES AND CONTROLS 6 5.1 GOOD HOUSEKEEPING 6 5.2 PREVENTIVE MAINTENANCE 7 5.3 INSPECTIONS 8 5.4 SPILL PREVENTION AND RESPONSE PROCEDURES 8 5.5 SEDIMENT AND EROSION CONTROL 9 5.6 MANAGEMENT OF RUNOFF 9 5.7 EMPLOYEE TRAINING PROGRAM 9 5.8 STORM WATER DISCHARGE MONITORING 9 6.0 IMPLEMENTATION 9 7.0 SITE COMPLIANCE EVALUATION 10 8.0 CERTIFICATION 11 LIST OF FIGURES 1 Site Map 3 2 Site Plan 4 3 Compliance Evaluation Form 12 LIST OF TABLES 1 Pollution Prevention Team Roster 1 2 Preventive Maintenance Schedule 8 3 Storm Water Sampling Parameters 10 LIST OF APPENDICES A Inventory of Significant Materials On-Site B Non-Storm Water Discharge Certification Premiere I B L; R S '['..p• ua! Innva�ion 1.0 INTRODUCTION This Storm Water Pollution Prevention Plan (SWPPP) has been prepared to comply with the provisions of 40 CFR Part 122. Its purpose is to control the discharge of pollutants in storm water runoff from the Premiere Fibers Plant at 10056 US Highway 52 North in Ansonville North Carolina. Premiere Fibers is engaged primarily in the conversion of Nylon and Polyester chips into partially oriented yarn through a heating and extrusion process This document represents the continuing effort of Premiere Fibers to insure compliance with environmental regulations and assist all Premiere Fibers employees in the performance of their duties. 2.0 POLLUTION PREVENTION TEAM Responsibilities of the Pollution Prevention Team leader include signatory authority, coordinating all stages of plan implementation, coordinating the employee training program, keeping all records, and ensuring reports are submitted. Team member responsibilities include noting changes affecting the environment, conducting inspections, implementing the preventive maintenance program, coordinating spill response, and overseeing good housekeeping. Table 1 presents the Premiere Fibers Pollution Prevention Team. Table 1 Pollution Prevention Team Roster Leader: Kevin Bowers Technical Manager. (704) -826-8321 Responsibilities include coordinating plan implementation; coordinating employee training program; ensuring records maintenance and report filing; overseeing inspections and "good housekeeping". Members: Joe Shelton Safety Manager (704)-826-8321 Responsibilities include notifying team leader of any changes affecting the environment and assisting with inspections. Ravi Thandayuthapani Maintenance Manager: (704)-826-8321 Responsibilities include coordinating spill response efforts and implementing the preventive maintenance program. Premie1, 1re ■■� page 1 3.0 COMPARISON WITH OTHER PLANS Premiere Fibers, Inc. does not maintain any management plans with elements that might overlap with the emergency response, inspection, and training portions of this SWPPP. 4.0 DESCRIPTION OF POTENTIAL POLLUTION SOURCES In this section, activities, materials, and physical features of the facility that may contribute significant amounts of pollutants to storm water runoff or, during periods of dry weather, result in pollutant discharges through the separate storm sewers or storm water drainage systems that drain the facility are described. 4.1 FACILITY SITE MAP Figure 1 is a general location map generated from the U.S. Geological Survey's Ansonville North Carolina, and provided by the North Carolina Department of Environment and Natural Resources showing the facility's location in relation to transportation routes and surface waters. Figure 2 presents a map of the facility depicting storm water drainage patterns and places where significant materials are exposed to rainfall and runoff. Figure 2 also depicts areas where loading and unloading activities occur. 4.2 INVENTORY OF EXPOSED MATERIALS Appendix A presents an inventory of materials that are or may have been handled, stored, processed, treated, or disposed of in a manner to allow exposure to storm water at the facility within the three years prior to February 24th 2009. This inventory was prepared by the Technica Manager at Premiere Fibers, Inc. who conducted an inspection of the site and related records. The inventory includes a description of the methods and locations of on-site storage and disposal and practices used to minimize contact of materials with rainfall and runoff. According to Premiere Fibers, Inc. records, no significant spills have occurred at the facility within three years prior to February 24th 2009. 4.3 NON-STORM WATER DISCHARGES Appendix B presents certifications, signed by the Technial Manager at Premiere Fibers, Inc., that discharges from the facility have been tested or evaluated for the presence of non-storm water discharges. The certifications include the results of any tests and/or evaluations (i.e. observation of outfalls during dry weather) conducted to detect such discharges, the test method used, the dates on which the tests and/or evaluations were performed, and the on-site drainage points directly observed during the test and/or evaluation. In I Premiere.2an Page 2 0 o .71W y' . 1 NJ .r3a'•.. ' 1 - , •� ..._ .yr+'-r'..� _...: � 1J is ' �-f Pr*-Ililere Fibers F+I.UAL + 5IfE a-e9fa - 4 ti I Cc'.Irty; ?5115Lj1 Rfi,,H 6vxj St,oa1.}; UT k6 Buffalo 5A•I' qn: l]y-rOM(Odin R"free RNA Bin) Facility Lot.-ilit�ll wo Z7M�%ORr154°Mr �y- 7rtai Page 3 . S . .%` : • � { . � Q � » ----------- mB@ . @¥ --- \ : --;GzC-Sn, ----' �� . _ � - - I §) \� ��� ~ � ^ f " 4.4 STORM WATER MONITORING DATA At present, no data are available on the quality or quantity of storm water discharges from the facility. However,the North Carolina Department of Environment, Health and Natural Resources(NCDEHNR)considers Premiere Fibers, INC.to be a Manufacturing facility,and requires visual monitoring of storm water discharges at such facilities(see Section 5.8). 4.5 POLLUTANT SOURCE IDENTIFICATION This section is a narrative assessment of the risk potential that sources of pollution at the facility pose to storm water quality.Specific activities,materials,and physical features at the facility are clearly pointed to. For this assessment,loading and unloading practices,outdoor storage, manufacturing,and processing activities,significant dust or particulate generating processes,and on-site waste disposal practices are considered.The pollutant parameters associated with each source are included in the assessment. The dumpsters,storage silos,and shipping and receiving bays appear to be the only areas where pollutants could potentially enter the storm water drainage system. These areas were inspected. An enclosed garbage dumpster is located on the North side of the facility. Solid waste from manufacturing and office activities awaiting off site disposal is stored in this dumpster.These types of waste would not be expected to leach if exposed to storm water.The risk for exposure of pollutants to storm water from this activity is low. Six storage silos are located on the West side of the facility.These silos store Polyester chips,raw materials to Premiere Fibers, INC. manufacturing process. Although the silos are closed,chips could potentially be released and exposed to storm water during loading/unloading activities. Materials that could potentially be exposed to storm water during loading/unloading activities at the shipping and receiving bays are yarn,finish oils,degreasing soap, metal powder, boiler chemicals, perch loroethylene, refrigerant oils,coil cleaners,and other maintenance and janitorial supplies.Because these materials are shipped or received at the facility in closed containers,the risk for exposure of pollutants to storm water from this activity is low. Two dumpsters are located on the East side of the facility.Solid waste from manufacturing awaiting off site disposal is stored in these dumpsters.These types of waste would not be expected to leach if exposed to storm water.The risk for exposure of pollutants to storm water from this activity is low. :eus Premiere Page 5 iiDC� 5.0 MEASURES AND CONTROLS This section presents an evaluation, selection, and description of pollution prevention measures, best management practices(BMPs), and other controls which will be implemented at the facility. 5.1 GOOD HOUSEKEEPING All Premiere Fibers, Inc. employees will use common sense to identify ways to maintain a clean and orderly facility and keep contaminants out of separate storm sewers. Ppemiere Fibers, Inc. has established protocols to reduce the possibility of mishandling chemicals or equipment and trains employees in good housekeeping techniques. These protocols are described as follows: Operation and Maintenance • Management will ensure that dry and clean floors and ground surfaces are maintained by providing brooms, shovels, vacuum cleaners, or cleaning machines. • Management will ensure that garbage and waste material are regularly picked up and disposed of. No more than 50 empty 55-gallon metal or polyethylene drums will be located on-site at any time. • Management will ensure that equipment is working properly(see Section 5.2 on preventive maintenance). • Management will routinely inspect for leaks or conditions that could lead to discharges of chemicals or contact of storm water with raw materials, intermediate materials,waste materials, or products (see Section 5.3 on inspections). • Management will ensure that spill cleanup procedures are understood by employees(see Section 5.4 on spill prevention and response procedures). Material Storage Practices • Management will provide adequate aisle space to facilitate material transfer and easy access for inspections. • Management will ensure that containers, drums, and bags are stored away from direct traffic routed to prevent accidental spills (see Section 5.4 on spill prevention and response procedures). • Management will ensure that containers are stacked according to manufacturers instructions to avoid damage to them from improper weight distribution. Management will ensure that containers are stored on pallets or similar devices to prevent corrosion of the containers which can result when they come in contact with moisture on the ground. Premiere Page 6 • Management will assign the responsibility of hazardous material inventory only to people who are trained to handle hazardous materials. Material Inventory Procedures Premiere Fibers, Inc. will keep an up-to-date inventory of all materials (hazardous and non- hazardous). During the inventory, the following tasks will be performed: • Management will identify all chemical substances present in the workplace by reviewing purchase orders. • Management will ensure that all containers are labeled to show the name and type of substance, expiration date, health hazards, suggestions for handling, and first aid information. This information will be obtained from the Material Safety Data Sheet (MSDS) maintained at the facility. • Management will ensure that hazardous materials requiring special handling, storage, use, and disposal considerations are clearly marked on the inventory. Employee Participation Premiere Fibers,lnc. will train employees in good housekeeping techniques. Employee training will occur as follows: • Management will incorporate information sessions on good housekeeping practices into the facility's employee training program. • Management will discuss good housekeeping at employee meetings. • Management will publicize pollution prevention concepts through postings. • Management will post bulletin boards with updated good housekeeping procedures, tips, and reminders. 5.2 PREVENTIVE MAINTENANCE Premiere Fibers, Inc. has developed a preventive maintenance program that involves regular inspection and maintenance of storm water management devices and other equipment and systems. The devices, equipment, and systems that will be inspected, the inspection and testing schedule, and the appropriate adjustments, cleaning, repair, or replacement actions are discussed on Table 2. :s�'s: Premiere Page 7 9r®�� l , B L a s T—P,1u l Innovation 5.3 INSPECTIONS The Pollution Prevention Team members identified in Section 2.0 will inspect the equipment and areas of the facility as discussed in Table 2. Complete and detailed records of routine preventive maintenance inspections and associated corrective action, repairs, or replacements will be provided to the Pollution Prevention Team leader who will file them with other visual inspection records. Table 2 Preventive Maintenance Schedule Inspection Device, equipment or systems Frequency Corrective action Enclosed Dumpster Monthly Contain, divert, and cleanup any spill: Two Dumpsters Monthly Contain, divert, and cleanup any spill; Storage Silos Monthly Contain, divert, and cleanup any spill; Shipping and receiving bays Monthly Dry and sweep area Paved areas Monthly Move potential pollutants under coves and out of storm water flow paths; cleat up any spill: Unpaved areas Monthly Seed any areas lacking vegetation mulch and stabilize any sodded area: plant vegetative buffer strips, a! necessary; install structural controls, a necessary 5.4 SPILL PREVENTION AND RESPONSE PROCEDURES Based on an assessment of possible spill scenarios, the following material handling procedures, storage requirements, containment/diversion equipment, and spill cleanup procedures are specified because they will minimize the potential for spills and, in the event of a spill, enable proper and timely response. If a leak develops or a spill occurs, the employee who discovers the discharge will contact his/her supervisor who will in turn contact the Pollution Prevention Team leader. The Pollution Prevention Team leader will obtain the following information: • Location of the spill or leak, material involved, and source (valve, pipe, drum, etc.). • The approximate amount spilled or an estimate of the discharge rate, and the direction of discharge flow. 'sE�'s: Premiere 0��It r 1 1i e a s Page 8 Pr.,.r.. The Pollution Prevention Team leader will dispatch facility personnel to the spill site to try to stop the leak and contain, divert and clean up the spill. 5.5 SEDIMENT AND EROSION CONTROL Landscaped areas at the facility have a high potential for significant soil erosion. It is the responsibility of the Pollution Prevention Team leader to ensure that vegetation of these areas is maintained. 5.6 MANAGEMENT OF RUNOFF Traditional storm water management practices that divert, infiltrate, reuse, or otherwise manage storm water runoff so as to reduce the discharge of pollutants do not appear to be reasonable and appropriate for the facility at this time. 5.7 EMPLOYEE TRAINING PROGRAM Employees and contractor personnel at all levels of responsibility will be informed of the components and goals of the SWPPP. Good housekeeping, materials management, and spill response procedures will be incorporated into the existing annual training program. Specific training topics are as follows: Good Housekeeping -Vacuuming and sweeping, prompt spill cleanup, locations of spill response equipment, securing drums and containers, checking for leaks and spills, perform daily. Materials Management Practices - Store materials neatly, identify and discuss handling of toxic and hazardous substances. Spill Prevention and Resnonse - Identify potential spill areas and drainage pathways, reporting spills to maintenance supervisor, practice with spill response equipment. 5.8 STORM WATER DISCHARGE MONITORING The NCDEHNR considers Premiere Fibers, Inc. to be a Manufacturing facility, and requires semi-annual visual monitoring of storm water discharges at such facilities. Table 3 identifies the characteristics which must be observed at each outfall. 6.0 IMPLEMENTATION The selected new BMPs and the training described above will be implemented by April 1 2009. :::'s: Premiere //�1, P I B E R S T"p-.1 I......... Page 9 Table 3 Storm Water Discharge Characteristics to be Observed Color Odor Clarity Floating Solids Suspended Solids Foam Oil Sheen Other obvious indicators of storm water pollution 7.0 SITE COMPLIANCE EVALUATION Pollution Prevention Team members will perform comprehensive site inspections to (1) confirm the accuracy of the description of potential pollution sources, (2) determine the effectiveness of the plan, and (3)assess compliance with the terms and conditions of the permit on a semi annual basis. This comprehensive evaluation will include: • Inspecting the storm water drainage areas for evidence of pollutants entering the drainage system. • Evaluating the effectiveness of measures to reduce pollutant loadings and whether additional measures are needed. • Observing structural measures, sediment controls, and other storm water BMPs to ensure proper operation. • Inspecting any equipment needed to implement the plan, such as spill response equipment. • Revising the plan as needed within two weeks of inspection. • Implementing any necessary changes within twelve weeks of the inspection. • Preparing a report summarizing inspection results and followup actions, if any. Include the date of the inspection and the name of the person who conducted the inspection. Identify incidents of non-compliance or certify that the facility is in compliance with plan. The report must be signed and kept with this SWPPP. sill Premiere It P I 1l I. R 5 Pag 10 Records of spills, leaks, or other discharges that will be maintained with the SWPPP include the following: • The date and time of any incident, weather conditions, duration, cause, environmental problems, response procedures, parties notified, recommended revisions to the BMP program, operating procedures, and/or equipment needed to prevent recurrence. • Formal written reports on any spills of a reportable quantity called in to the National Response Center. • A list of procedures for notifying the appropriate plant personnel and the names and telephone numbers of responsible employees. Records of inspections and maintenance activities include the following: • Field notebooks. • Dated and timed photographs. • Video tapes. • Drawings and maps. All records relating to storm water pollution prevention will be kept on file at the facility. 8.0 CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Kevin Bowers Technical Manager ss Premiere elect r 1 1; e a s Page 11 Figure 3 COMPLIANCE EVALUATION FORM Date and time of inspection: Inspector: (name and title) Pollutant potential to enter drainage system: Measures to reduce Measure(s) Pollutant loadings: Evaluated Status Equipment inspected: Status Action recommended as a result of this evaluation: Changes to SWPPP: Date: Comments: 9: s:Premiere 9/�_\F I B E R S P..p.i n.l Innoraon Page 12 APPENDIX A INVENTORY OF SIGNIFICANT MATERIALS ON-SITE on 11 Premiere Sheet of MATERIAL INVENTORY Completed by Title Date Instructions: List all materials used,stored,or produced onsite.Assess and evaluate these materials for their potential to contribute pollutants to Storm Water runoff.Also complete"Description of Exposed Material"worksheet if the material has been exposed during the last three years. Quality Past Significant (Units) Quality Exposed In Likelihood of Contact with Storm Water Spill or Leak Materials Purpose/Location Used Produced Stored Last 3 Years If yes,describe reason. Yes-7 No :Premiere ... . 1 APPENDIX B NON-STORM WATER DISCHARGE CERTIFICATION :::_: Premiere NON-STORM WATER DISCHARGE Sheet of ASSESSMENT AND CERTIFICATION Completed by Title Date Outfall Directly Observed Date of During theTest Method Used to Describe Results from Test for Name of Person Who Test or (identity as indicated on Test or Evaluate the Presence of Non-Storm Identify Potential Conducted the Test or Evaluation the site map) Discharged Water Discharge Significant Sources Evaluation CERTIFICATION I, (responsible corporate offical), certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or person's who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. Name&Official Title(type or Print B.Area Code and Telephone Number C.Signature. D. Date Signed '.��:Premiere Young, Brianna A From: Phillip Rahn <prahn@watersedgeenv.com> Sent: Friday, June 23, 2023 4:29 PM To: Young, Brianna A; Dewey Fulton Subject: [External] Additional Questions for Premiere NPDES Permit Application Attachments: 23-046 mem6.23.23 Premier NPDES Permit Renewal Additional Questions.pdf CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- I have tried to answer the additional questions raised for the Premiere NPDES Permit Application from your earlier email.They are attached to this email. Have a good weekend. Phil Rahn P.G. President Waters Edge Environmental, LLC 1434 Chester Road Raleigh, NC 27608 919.219.5820 (cell) prahn@watersedgeenv.com (email) watersedgeenvironmenta1.net (website) i WATERS EDGE ENVIRONMENTAL,LLC 1434 CHESTER ROAD • RALEIGH, N.C.27608 • PHONE 919.219.5820 MEMORANDUM Date June 23, 2023 To Brianna Young, MS Industrial Individual Permits Coordinator Stormwater Permitting Program From Mr. Phil Rahn P.G. - Waters Edge Copy Mr. Dewey Fulton - Premiere Fibers Subject Additional DEQ Requests Premiere Fibers NPDES Permit Renewal 10056 US S.R. 52N Ansonville, North Carolina 28007 Stormwater Permit No. NCS000528 Waters Edge Job No. R9-21 You had sent an email requesting Premiere to provide additional information. We have provided answers to each request in italics as follows: • Description of chemicals stored onsite; Answer We have provided a list contained in Appendix A;however, we would state that the only chemicals stored outside the building is fuel oil used to fire the boilers. The remaining chemicals are stored inside and should not be subject to any stormwater runoff. • Description of industrial activity in each drainage area; Answer The drainage areas depicted in the May 23, 2023 NPDES permit application (Figure 1) are in an area outside ofAnsonville that has no development other than residential or farming so there would be no industrial activity. • An electronic spreadsheet summarizing all of the monitoring data (visual and analytical)that has been collected since the effective date of the current permit; Answer We have provided a spreadsheet of the analytical data since the effective date of the currentpermit in AppendixB. Please realize that some of the Outfalls do not have flow during rain events and we missed the Spring 2021 sampling interval since our sampling technician contacted long-term Covid. We could not make an Excel spreadsheet of the visual data, but it is included in all of our individual submittals to NCDEQ. Additional DEQ Requests Premiere Fibers NPDES Permit Renewal 10056 US S.R. 52N Ansonville,North Carolina 28007 June 23,2023 Page 2 of 2 • Table D of EPA Form 217; Answer We have included Table D in Appendix C. • Summary of onsite BMPs; Answer The onsite BMPs have not changed since what was stated in the February 24, 2009 Stormwater PPP which is contained in Appendix D. • Summary of significant changes that have occurred at the site since the last permit renewal. Answer There have been no changes since the last permit renewal. If there are any questions, please contact me at prahn(a,watersedgeenv.com or 919.219.5820. APPENDIX A List of Chemicals Stored at Premiere Fibers Ansonville, North Carolina Spin Finish Spin finish concentrate composition and the oil-in-water emulsion made from the concentrate for application for conventional speed or high speed melt spinning processes for producing polyester or polyamide yarns, consists essentially of oil lubricant component, pentaerythritol ester lubricant, ethoxylated sorbitan monooleate of HLB ranging from 6 to 15, anionic antistatic agent, water soluble sulfosuccinate wetting agent, and oil soluble ethoxylated polymethylsiloxane wetting agent having molecular weight of 400 to 700 and an aqueous surface tension value of less than 21 dynes/cm. The concentrate has long term stability. Dowtherm Versatile Heat Transfer Fluid that can operate in either liquid or vapor phases in order to collect,transport, and store heat in a variety of heat transfer applications, such as concentrated solar power(CSP)systems. DOWTHERMTM A Heat Transfer Fluid is designed to provide a consistent and reliable source of heat transfer at high temperature applications up to 400°C (750°F) Fuel oil No. 2 fuel oil (heating oil): A distillate fuel oil that has a distillation temperatures of 400 degrees Fahrenheit at the 10-percent recovery point and 640 degrees Fahrenheit at the 90-percent recovery point and meets the specifications defined in ASTM Specification D 396. Compressor oil A long life PAO oil, specifically developed for use in Atlas Copco oil injected screw compressors. (PAO) fluids are the most common major synthetic base oil used in industrial and automotive lubricants. These synthetic hydrocarbons are designed to provide superior lubrication performance over a wider operating- temperature range than petroleum oils and typically are less volatile. Listing of Individual Chemicals Contained Inside Building at Premiere Fibers Item No Description U/M Store Location THERMINOL Therminol LT, Heat Transfer Fluid 55 al drum DRUM 508716 Chemical, Air washer MG-200, 5 Gallon EA PART ROOM 508570 Chemical, Air washer CL-4005 , 5 Gallon EA PART ROOM 508569 Chemical, Corrosion lnhibitor,CL-6050MB EA PART ROOM Cooling Tower ,Chen 508568 Microguard, MG-906, Biocide Cooling Tower EA PART ROOM Chemical, 5-Gallon 508567 Chemical, Air washer CL-4550, 5 Gallon EA PART ROOM 508566 Peroxide, Chemical, CL-10, 5 Gallon EA PART ROOM 508391 Coverage Plus,NPD (4 X 1 Gallon Plastic Bottles) CASE - Fiberboard B- 507679 Cleaner, Alkaline, 55 Gallon Drum, Metal Medic G PROD.SERV 7035, Sodium Hydroxide 507621 Coil Cleaner, Evaporative Foam No Rinse EA PART ROOM Eva orator, 6 of Nu-Cal on 507562 Cleaner/Degreaser, 55 gallon Water-Based, Clear G PART ROOM Yellowish, For O 507534 Reagent,Hexane(s) ACS, Minimum Assay 95% n- EA PART ROOM Hexane 507255 Hydrogen Peroxide, 35%, 5 Gallon(20L) Drum, DRUM PART ROOM Technical Grade 506962 Reagent, C3270240-2.5Y, Phenol/1,1,2,2- EA Tetrachloro ethane, 506595 Acetone, 5 Gallon,20L Pail, CAS # 67-64-1, EA PART ROOM CH3COCH-3 506288 Petroleum Ether A.C.S Reagent, in Poly coated Ltr PART ROOM Bottles 506169 Solution, Godet Cleaner BGC 2009, 5Litre, EA PART ROOM F/Cleaning Godet SL 506067 Trieth lene Glycol LBS PART ROOM 505696 Argon Industrial Shielding Gas Mix, Size 300 EA PART ROOM C linder, CGA-580 505594 Hydrofluoric Acid, 48%, 1L EA PART ROOM 504925 Urethane Conformal Coating, Aerosol, 12 FL.OZ EA ELECT.SHOP 504752 Kit, Acid Treatment, Spill-X, 6 - 2-lb. Shaker EA PART ROOM Bottles 504439 Coil Cleaner, No Rinse, Aerosol, 18 Oz, EA PART ROOM Evaporator Cleaner 504198 Nitrogen Gas Cylinder, Nitrogen Industrial 300 EA PART ROOM Vol-608.00 FT 504152 Acid, Hydrochloric, Reagent ACS 21/2L EA PART ROOM 503740 1 Sodium Phosphate Monobasic,Reagentplus 500G I DRUM I PART ROOM 503556 lsopropyl Alcohol , 1 Gallon, 99% EA ELECT.SHOP 503536 Nitric Acid, 1% (V/V) Aqueous Volumetric EA PART ROOM Solution, 2.5L 503420 Biocide, Ultra Kleen Solution-2, 5G SXBSXS2- EA PROD.SERV 0047 503419 Biocide, Ultra Kleen Solution-1, 5G SXBI-0041 EA PROD.SERV 503411 Brakleen, 19 fl. oz,Brake Parts Cleaner Aerosol EA PART ROOM 503371 Sodium Hydroxide, Purified pellets, 500G/Case CASE PROD.SERV 503285 Chemical pump, with programmable timer EA PART ROOM 503217 Minimal Expansion Foam, 12 Wt. Oz, CRC- EA ELECT.SHOP 14077 502874 Parts-Wash Solution, Gen. Purpose, Liquid EA PART ROOM Formula, 5 Gallon Size 502745 Acid dye for Nylon,PERMALON VIOLET FBL LBS PART ROOM 180% 502587 Xceltherm LVI, Heat transfer Fluid 55 Gallon EA WNDR.SHOP Drum Dowtherm A E 502404 Acetic Acid, 2.5L, Poly-Coated Glass Bottle EA PART ROOM 502277 Solution, Rydlyme, Biodegradeable Descaler, 55 DRUM PART ROOM Gallon Drum 502273 Pyrophosphate Tetrasodium, 500G DRUM PART ROOM 501825 Soduim DiH dro en Phosphate Extra Pure EA PART ROOM 501620 Xceltherm MKI, Heat transfer Fluid 55 Gallon EA WNDR.SHOP Drum Dowtherm A 501360 Grease, AUTOL TOP 2000 EA PART ROOM 501260 Cleaner, Alkaline, EZE 2945, 50 Gallon Drum/ LBS PROD.SERV 598 LBS 501013 Hydrogen Peroxide, 35%, 15 Gallon Drum, DRUM PART ROOM Technical Grade 500945 Oxygen Gas Cylinder, OXY Industrial 282 CF EA PART ROOM 500944 Argon Gas Cylinder, ARGON Industrial 336 CF, EA PART ROOM 500675 Cleaner, Contact, CRC2000 QD EA ELECT.SHOP 500504 Cleaner, Contact, CRC2000 EA ELECT.SHOP 500299 Perchloro ethylene, Freon Grade (55Gal Drum), DRUM PART ROOM 700Lbs 500280 Solution, Cleaning, PRODAN (IOLitre) EA PART ROOM 500081 Super Rustripper, Oakite LBS PROD.SERV 500080 Biocide, Acticide LA LBS PROD.SERV 400117 Reprocess Dowtherm A LBS WNDRSHOP APPENDIX B Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 001 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 4/24/18 Threshold Total Suspended Solids mg/L 100 231 5.5 57.0 2.9 5.0 39.2 159 BDL pH SU 6.0-9.0 4.0 6.7 6.3 5.9 6.4 6.5 6.2 NA Chemical Oxygen mg/L 120 BDL BDL BDL 46.0 BDL BDL BDL NA T)Pmand NCDENR Analytical Parameter Units Permit 8/2/18 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 Threshold Total Suspended Solids mg/L 100 2.8 1,250 8.9 10.2 9.4 No Flow 2.6 BDL pH SU 6.0-9.0 6.0 5.4 NA 6.1 5.1 No Flow 5.1 6.2 Chemical Oxygen mg/L 120 BDL 45.7 NA BDL BDL No Flow BDL BDL n rl NCDENR Analytical Parameter Units Permit 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 No Flow No Flow pH SU 6.0-9.0 No Flow No Flow Chemical Oxygen mg/L 120 No Flow No Flow M-M!And SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 001 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 002 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 4.6 38.2 BDL BDL 5.5 BDL BDL BDL pH SU 6.0-9.0 6.1 6.5 6.3 6.5 6.5 6.6 6.3 6.3 Chemical Oxygen llPmnn mg/L 120 BDL BDL BDL BDL BDL BDL BDL BDL NCDENR Analytical Parameter Units Permit 6/7/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 BDL 5.3 34.0 7.7 5.7 BDL No Flow 3.7 pH SU 6.0-9.0 5.6 6.4 5.8 5.6 4.2 6.2 No Flow 6.2 Chemical Oxygen mg/L 120 BDL BDL 27.3 BDL BDL BDL No Flow BDL nt-mnnd NCDENR Analytical Parameter Units Permit Threshold Total Suspended Solids mg/L 100 pH SU 6.0-9.0 Chemical Oxygen mg/L 120 SU-Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 002 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 003 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 4.1 15.1 12.3 67.9 2.6 5.3 26.8 10.1 pH SU 6.0-9.0 6.1 6.0 6.0 6.2 5.9 6.5 6.2 5.5 Chemical Oxygen llPmnn mg/L 120 BDL BDL BDL BDL BDL BDL BDL BDL NCDENR Analytical Parameter Units Permit 6/7/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 9.2 5.0 8.9 4.0 10.6 23.6 No Flow 11.0 pH SU 6.0-9.0 5.5 6.3 6.2 5.0 5.3 6.1 No Flow 5.9 Chemical Oxygen mg/L 120 38.6 BDL BDL BDL BDL 30.3 No Flow 31.6 nt-mnnd NCDENR Analytical Parameter Units Permit Threshold Total Suspended Solids mg/L 100 pH SU 6.0-9.0 Chemical Oxygen 11,E 120 DPMnnfI SU-Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 003 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 004 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 3/1/18 8/2/18 Threshold Total Suspended Solids mg/L 100 19.8 6.5 54.8 35.2 23.2 BDL 16.9 24.6 pH SU 6.0-9.0 8.3 6.3 6.8 6.9 6.3 7.2 6.9 6.3 Chemical Oxygen mg/L 120 45 BDL 94.0 97.0 34.0 BDL 88.0 37.9 T)Pmanrl NCDENR Analytical Parameter Units Permit 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 11/11/22 Threshold Total Suspended Solids mg/L 100 18.0 NA 9.2 20.3 23.3 9.9 15.7 7.0 pH SU 6.0-9.0 6.1 NA 7.0 7.0 6.8 5.9 6.8 7.6 Chemical Oxygen mg/L 120 136 258 104 58.4 59.5 25.7 125 41.1 n rl NCDENR Analytical Parameter Units Permit 3/2/23 Threshold Total Suspended Solids mg/L 100 7.7 pH SU 6.0-9.0 6.7 Chemical Oxygen mg/L 120 90.2 ilPmanrl SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 004 Table 1 Historical Stormwater Outfall Analytical Results Premier Fibers Ansonville, North Carolina OUTFALL # 005 NCDENR Analytical Parameter Units Permit 2/23/15 11/3/15 5/5/16 9/21/16 4/6/17 9/12/17 10/23/17 3/1/18 Threshold Total Suspended Solids mg/L 100 54.5 5.9 33.0 15.9 51.3 115 24.7 27.9 pH SU 6.0-9.0 8.3 6.3 7.1 6.9 6.4 6.8 6.8 6.5 Chemical Oxygen mg/L 120 BDL BDL 97.0 107 63.0 BDL 310 107 T)Pmand NCDENR Analytical Parameter Units Permit 8/2/18 6/7/19 7/24/19 10/16/19 2/11/20 11/11/20 8/3/21 6/17/22 Threshold Total Suspended Solids mg/L 100 27.5 96.5 NA 100 19.6 187 39.8 3.8 pH SU 6.0-9.0 6.3 6.2 NA 4.3 5.9 6.9 5.9 6.5 Chemical Oxygen mg/L 120 28.4 148 275 85.0 51.7 78.9 28.0 BDL n rl NCDENR Analytical Parameter Units Permit 11/11/22 3/2/23 Threshold Total Suspended Solids mg/L 100 8.6 5.3 pH SU 6.0-9.0 7.4 6.6 Chemical Oxygen mg/L 120 48.3 76.2 ilPmanrl SU- Standard Units NA -Not Analyzed BDL -Below Detection Limit Bolded numbers exceed NCDENR Permit Threshold OUTFALL 005 APPENDIX C EPA Identification Number NPDES Permit Number Facility name Outfall Number Form Approved 03/05/19 NCD986230159 NCS000528 Premiere Fibers 001-005 OMB No.2040-0004 STORMTABLE D. • ' • I Provide data for the storm event(s)that resulted in the maximum daily discharges for the flow-weighted composite sample. Number of Hours Between Total Rainfall During Maximum Flow Rate Duration of Storm Event (in inches) Beginning of Storm Measured and (in gpm or specify units) Total Flow from Rain Event Date of Storm Event (in hours) Storm Event End of Previous Measurable Rain During Rain Event (in gallons or specify units) Event Approximately 1 hour .31" 4/23-4/27, approximately 96 hours SGPM 300 gal.from each outfall Provide a description of the method of flow measurement or estimate. Flow from each outfall 001-005 are discharged at the invert of a reinforced concrete pipe. No flow meters or measuring devices are in use. However,the predominant flow originates from roof drains.The discharge is rapid flowing and the duration is very limited upon cessation of the rain event.Some laminar flow is caught in the outfall 003 catch basin from the asphalt drive.Minimal flow is observed on the gravel and asphalt areas and is captured within the grassy areas.This water is moved to drainage features along the North,South and West due to the grade of the landscape.Total flow was estimated at 5 GPM for 60 minutes. Click to go back to the beginning of Form EPA Form 3510-21F(Revised 3-19) Page 13 APPENDIX D STORM WATER POLLUTION PREVENTION PLAN PREMIERE FIBERS, INC. 10056 US HIGHWAY 52 NORTH ANSONVILLE , NORTH CAROLINA 1175/1176 :0.'s: Premiere jf��1 P I B E R S Pe•pa ..i I...I — STORM WATER POLLUTION PREVENTION PLAN PREMIERE FIBERS, INC. 10056 US HIGHWAY 52 NORTH ANSONVILLE, NORTH CAROLINA Prepared for: PREMIERE FIBERS, INC Prepared by: PREMIERE FIBERS, INC. ANSONVILLE, N.C. February 24th 2009 :s:'s: Premiere "ll F I B E R S 'P_P_..I Innovaion TABLE OF CONTENTS Page No. 1.0 INTRODUCTION 1 2.0 POLLUTION PREVENTION TEAM 1 3.0 COMPARISON WITH OTHER PLANS 2 4.0 DESCRIPTION OF POTENTIAL POLLUTION SOURCES 2 4.1 FACILITY SITE MAP 2 4.2 INVENTORY OF EXPOSED MATERIALS 2 4.3 NON-STORM WATER DISCHARGES 2 4.4 STORM WATER MONITORING DATA 5 4.5 POLLUTANT SOURCE IDENTIFICATION 5 5.0 MEASURES AND CONTROLS 6 5.1 GOOD HOUSEKEEPING 6 5.2 PREVENTIVE MAINTENANCE 7 5.3 INSPECTIONS 8 5.4 SPILL PREVENTION AND RESPONSE PROCEDURES 8 5.5 SEDIMENT AND EROSION CONTROL 9 5.6 MANAGEMENT OF RUNOFF 9 5.7 EMPLOYEE TRAINING PROGRAM 9 5.8 STORM WATER DISCHARGE MONITORING 9 6.0 IMPLEMENTATION 9 7.0 SITE COMPLIANCE EVALUATION 10 8.0 CERTIFICATION 11 LIST OF FIGURES 1 Site Map 3 2 Site Plan 4 3 Compliance Evaluation Form 12 LIST OF TABLES 1 Pollution Prevention Team Roster 1 2 Preventive Maintenance Schedule 8 3 Storm Water Sampling Parameters 10 LIST OF APPENDICES A Inventory of Significant Materials On-Site B Non-Storm Water Discharge Certification Premiere I B L; R S '['..p• ua! Innva�ion 1.0 INTRODUCTION This Storm Water Pollution Prevention Plan (SWPPP) has been prepared to comply with the provisions of 40 CFR Part 122. Its purpose is to control the discharge of pollutants in storm water runoff from the Premiere Fibers Plant at 10056 US Highway 52 North in Ansonville North Carolina. Premiere Fibers is engaged primarily in the conversion of Nylon and Polyester chips into partially oriented yarn through a heating and extrusion process This document represents the continuing effort of Premiere Fibers to insure compliance with environmental regulations and assist all Premiere Fibers employees in the performance of their duties. 2.0 POLLUTION PREVENTION TEAM Responsibilities of the Pollution Prevention Team leader include signatory authority, coordinating all stages of plan implementation, coordinating the employee training program, keeping all records, and ensuring reports are submitted. Team member responsibilities include noting changes affecting the environment, conducting inspections, implementing the preventive maintenance program, coordinating spill response, and overseeing good housekeeping. Table 1 presents the Premiere Fibers Pollution Prevention Team. Table 1 Pollution Prevention Team Roster Leader: Kevin Bowers Technical Manager. (704) -826-8321 Responsibilities include coordinating plan implementation; coordinating employee training program; ensuring records maintenance and report filing; overseeing inspections and "good housekeeping". Members: Joe Shelton Safety Manager (704)-826-8321 Responsibilities include notifying team leader of any changes affecting the environment and assisting with inspections. Ravi Thandayuthapani Maintenance Manager: (704)-826-8321 Responsibilities include coordinating spill response efforts and implementing the preventive maintenance program. Premie1, 1re ■■� page 1 3.0 COMPARISON WITH OTHER PLANS Premiere Fibers, Inc. does not maintain any management plans with elements that might overlap with the emergency response, inspection, and training portions of this SWPPP. 4.0 DESCRIPTION OF POTENTIAL POLLUTION SOURCES In this section, activities, materials, and physical features of the facility that may contribute significant amounts of pollutants to storm water runoff or, during periods of dry weather, result in pollutant discharges through the separate storm sewers or storm water drainage systems that drain the facility are described. 4.1 FACILITY SITE MAP Figure 1 is a general location map generated from the U.S. Geological Survey's Ansonville North Carolina, and provided by the North Carolina Department of Environment and Natural Resources showing the facility's location in relation to transportation routes and surface waters. Figure 2 presents a map of the facility depicting storm water drainage patterns and places where significant materials are exposed to rainfall and runoff. Figure 2 also depicts areas where loading and unloading activities occur. 4.2 INVENTORY OF EXPOSED MATERIALS Appendix A presents an inventory of materials that are or may have been handled, stored, processed, treated, or disposed of in a manner to allow exposure to storm water at the facility within the three years prior to February 24th 2009. This inventory was prepared by the Technica Manager at Premiere Fibers, Inc. who conducted an inspection of the site and related records. The inventory includes a description of the methods and locations of on-site storage and disposal and practices used to minimize contact of materials with rainfall and runoff. According to Premiere Fibers, Inc. records, no significant spills have occurred at the facility within three years prior to February 24th 2009. 4.3 NON-STORM WATER DISCHARGES Appendix B presents certifications, signed by the Technial Manager at Premiere Fibers, Inc., that discharges from the facility have been tested or evaluated for the presence of non-storm water discharges. The certifications include the results of any tests and/or evaluations (i.e. observation of outfalls during dry weather) conducted to detect such discharges, the test method used, the dates on which the tests and/or evaluations were performed, and the on-site drainage points directly observed during the test and/or evaluation. In I Premiere.2an Page 2 0 o .71W y' . 1 NJ .r3a'•.. ' 1 - , •� ..._ .yr+'-r'..� _...: � 1J is ' �-f Pr*-Ililere Fibers F+I.UAL + 5IfE a-e9fa - 4 ti I Cc'.Irty; ?5115Lj1 Rfi,,H 6vxj St,oa1.}; UT k6 Buffalo 5A•I' qn: l]y-rOM(Odin R"free RNA Bin) Facility Lot.-ilit�ll wo Z7M�%ORr154°Mr �y- 7rtai Page 3 . S . .%` : • � { . � Q � » ----------- mB@ . @¥ --- \ : --;GzC-Sn, ----' �� . _ � - - I §) \� ��� ~ � ^ f " 4.4 STORM WATER MONITORING DATA At present, no data are available on the quality or quantity of storm water discharges from the facility. However,the North Carolina Department of Environment, Health and Natural Resources(NCDEHNR)considers Premiere Fibers, INC.to be a Manufacturing facility,and requires visual monitoring of storm water discharges at such facilities(see Section 5.8). 4.5 POLLUTANT SOURCE IDENTIFICATION This section is a narrative assessment of the risk potential that sources of pollution at the facility pose to storm water quality.Specific activities,materials,and physical features at the facility are clearly pointed to. For this assessment,loading and unloading practices,outdoor storage, manufacturing,and processing activities,significant dust or particulate generating processes,and on-site waste disposal practices are considered.The pollutant parameters associated with each source are included in the assessment. The dumpsters,storage silos,and shipping and receiving bays appear to be the only areas where pollutants could potentially enter the storm water drainage system. These areas were inspected. An enclosed garbage dumpster is located on the North side of the facility. Solid waste from manufacturing and office activities awaiting off site disposal is stored in this dumpster.These types of waste would not be expected to leach if exposed to storm water.The risk for exposure of pollutants to storm water from this activity is low. Six storage silos are located on the West side of the facility.These silos store Polyester chips,raw materials to Premiere Fibers, INC. manufacturing process. Although the silos are closed,chips could potentially be released and exposed to storm water during loading/unloading activities. Materials that could potentially be exposed to storm water during loading/unloading activities at the shipping and receiving bays are yarn,finish oils,degreasing soap, metal powder, boiler chemicals, perch loroethylene, refrigerant oils,coil cleaners,and other maintenance and janitorial supplies.Because these materials are shipped or received at the facility in closed containers,the risk for exposure of pollutants to storm water from this activity is low. Two dumpsters are located on the East side of the facility.Solid waste from manufacturing awaiting off site disposal is stored in these dumpsters.These types of waste would not be expected to leach if exposed to storm water.The risk for exposure of pollutants to storm water from this activity is low. :eus Premiere Page 5 iiDC� 5.0 MEASURES AND CONTROLS This section presents an evaluation, selection, and description of pollution prevention measures, best management practices(BMPs), and other controls which will be implemented at the facility. 5.1 GOOD HOUSEKEEPING All Premiere Fibers, Inc. employees will use common sense to identify ways to maintain a clean and orderly facility and keep contaminants out of separate storm sewers. Ppemiere Fibers, Inc. has established protocols to reduce the possibility of mishandling chemicals or equipment and trains employees in good housekeeping techniques. These protocols are described as follows: Operation and Maintenance • Management will ensure that dry and clean floors and ground surfaces are maintained by providing brooms, shovels, vacuum cleaners, or cleaning machines. • Management will ensure that garbage and waste material are regularly picked up and disposed of. No more than 50 empty 55-gallon metal or polyethylene drums will be located on-site at any time. • Management will ensure that equipment is working properly(see Section 5.2 on preventive maintenance). • Management will routinely inspect for leaks or conditions that could lead to discharges of chemicals or contact of storm water with raw materials, intermediate materials,waste materials, or products (see Section 5.3 on inspections). • Management will ensure that spill cleanup procedures are understood by employees(see Section 5.4 on spill prevention and response procedures). Material Storage Practices • Management will provide adequate aisle space to facilitate material transfer and easy access for inspections. • Management will ensure that containers, drums, and bags are stored away from direct traffic routed to prevent accidental spills (see Section 5.4 on spill prevention and response procedures). • Management will ensure that containers are stacked according to manufacturers instructions to avoid damage to them from improper weight distribution. Management will ensure that containers are stored on pallets or similar devices to prevent corrosion of the containers which can result when they come in contact with moisture on the ground. Premiere Page 6 • Management will assign the responsibility of hazardous material inventory only to people who are trained to handle hazardous materials. Material Inventory Procedures Premiere Fibers, Inc. will keep an up-to-date inventory of all materials (hazardous and non- hazardous). During the inventory, the following tasks will be performed: • Management will identify all chemical substances present in the workplace by reviewing purchase orders. • Management will ensure that all containers are labeled to show the name and type of substance, expiration date, health hazards, suggestions for handling, and first aid information. This information will be obtained from the Material Safety Data Sheet (MSDS) maintained at the facility. • Management will ensure that hazardous materials requiring special handling, storage, use, and disposal considerations are clearly marked on the inventory. Employee Participation Premiere Fibers,lnc. will train employees in good housekeeping techniques. Employee training will occur as follows: • Management will incorporate information sessions on good housekeeping practices into the facility's employee training program. • Management will discuss good housekeeping at employee meetings. • Management will publicize pollution prevention concepts through postings. • Management will post bulletin boards with updated good housekeeping procedures, tips, and reminders. 5.2 PREVENTIVE MAINTENANCE Premiere Fibers, Inc. has developed a preventive maintenance program that involves regular inspection and maintenance of storm water management devices and other equipment and systems. The devices, equipment, and systems that will be inspected, the inspection and testing schedule, and the appropriate adjustments, cleaning, repair, or replacement actions are discussed on Table 2. :s�'s: Premiere Page 7 9r®�� l , B L a s T—P,1u l Innovation 5.3 INSPECTIONS The Pollution Prevention Team members identified in Section 2.0 will inspect the equipment and areas of the facility as discussed in Table 2. Complete and detailed records of routine preventive maintenance inspections and associated corrective action, repairs, or replacements will be provided to the Pollution Prevention Team leader who will file them with other visual inspection records. Table 2 Preventive Maintenance Schedule Inspection Device, equipment or systems Frequency Corrective action Enclosed Dumpster Monthly Contain, divert, and cleanup any spill: Two Dumpsters Monthly Contain, divert, and cleanup any spill; Storage Silos Monthly Contain, divert, and cleanup any spill; Shipping and receiving bays Monthly Dry and sweep area Paved areas Monthly Move potential pollutants under coves and out of storm water flow paths; cleat up any spill: Unpaved areas Monthly Seed any areas lacking vegetation mulch and stabilize any sodded area: plant vegetative buffer strips, a! necessary; install structural controls, a necessary 5.4 SPILL PREVENTION AND RESPONSE PROCEDURES Based on an assessment of possible spill scenarios, the following material handling procedures, storage requirements, containment/diversion equipment, and spill cleanup procedures are specified because they will minimize the potential for spills and, in the event of a spill, enable proper and timely response. If a leak develops or a spill occurs, the employee who discovers the discharge will contact his/her supervisor who will in turn contact the Pollution Prevention Team leader. The Pollution Prevention Team leader will obtain the following information: • Location of the spill or leak, material involved, and source (valve, pipe, drum, etc.). • The approximate amount spilled or an estimate of the discharge rate, and the direction of discharge flow. 'sE�'s: Premiere 0��It r 1 1i e a s Page 8 Pr.,.r.. The Pollution Prevention Team leader will dispatch facility personnel to the spill site to try to stop the leak and contain, divert and clean up the spill. 5.5 SEDIMENT AND EROSION CONTROL Landscaped areas at the facility have a high potential for significant soil erosion. It is the responsibility of the Pollution Prevention Team leader to ensure that vegetation of these areas is maintained. 5.6 MANAGEMENT OF RUNOFF Traditional storm water management practices that divert, infiltrate, reuse, or otherwise manage storm water runoff so as to reduce the discharge of pollutants do not appear to be reasonable and appropriate for the facility at this time. 5.7 EMPLOYEE TRAINING PROGRAM Employees and contractor personnel at all levels of responsibility will be informed of the components and goals of the SWPPP. Good housekeeping, materials management, and spill response procedures will be incorporated into the existing annual training program. Specific training topics are as follows: Good Housekeeping -Vacuuming and sweeping, prompt spill cleanup, locations of spill response equipment, securing drums and containers, checking for leaks and spills, perform daily. Materials Management Practices - Store materials neatly, identify and discuss handling of toxic and hazardous substances. Spill Prevention and Resnonse - Identify potential spill areas and drainage pathways, reporting spills to maintenance supervisor, practice with spill response equipment. 5.8 STORM WATER DISCHARGE MONITORING The NCDEHNR considers Premiere Fibers, Inc. to be a Manufacturing facility, and requires semi-annual visual monitoring of storm water discharges at such facilities. Table 3 identifies the characteristics which must be observed at each outfall. 6.0 IMPLEMENTATION The selected new BMPs and the training described above will be implemented by April 1 2009. :::'s: Premiere //�1, P I B E R S T"p-.1 I......... Page 9 Table 3 Storm Water Discharge Characteristics to be Observed Color Odor Clarity Floating Solids Suspended Solids Foam Oil Sheen Other obvious indicators of storm water pollution 7.0 SITE COMPLIANCE EVALUATION Pollution Prevention Team members will perform comprehensive site inspections to (1) confirm the accuracy of the description of potential pollution sources, (2) determine the effectiveness of the plan, and (3)assess compliance with the terms and conditions of the permit on a semi annual basis. This comprehensive evaluation will include: • Inspecting the storm water drainage areas for evidence of pollutants entering the drainage system. • Evaluating the effectiveness of measures to reduce pollutant loadings and whether additional measures are needed. • Observing structural measures, sediment controls, and other storm water BMPs to ensure proper operation. • Inspecting any equipment needed to implement the plan, such as spill response equipment. • Revising the plan as needed within two weeks of inspection. • Implementing any necessary changes within twelve weeks of the inspection. • Preparing a report summarizing inspection results and followup actions, if any. Include the date of the inspection and the name of the person who conducted the inspection. Identify incidents of non-compliance or certify that the facility is in compliance with plan. The report must be signed and kept with this SWPPP. sill Premiere It P I 1l I. R 5 Pag 10 Records of spills, leaks, or other discharges that will be maintained with the SWPPP include the following: • The date and time of any incident, weather conditions, duration, cause, environmental problems, response procedures, parties notified, recommended revisions to the BMP program, operating procedures, and/or equipment needed to prevent recurrence. • Formal written reports on any spills of a reportable quantity called in to the National Response Center. • A list of procedures for notifying the appropriate plant personnel and the names and telephone numbers of responsible employees. Records of inspections and maintenance activities include the following: • Field notebooks. • Dated and timed photographs. • Video tapes. • Drawings and maps. All records relating to storm water pollution prevention will be kept on file at the facility. 8.0 CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Kevin Bowers Technical Manager ss Premiere elect r 1 1; e a s Page 11 Figure 3 COMPLIANCE EVALUATION FORM Date and time of inspection: Inspector: (name and title) Pollutant potential to enter drainage system: Measures to reduce Measure(s) Pollutant loadings: Evaluated Status Equipment inspected: Status Action recommended as a result of this evaluation: Changes to SWPPP: Date: Comments: 9: s:Premiere 9/�_\F I B E R S P..p.i n.l Innoraon Page 12 APPENDIX A INVENTORY OF SIGNIFICANT MATERIALS ON-SITE on 11 Premiere Sheet of MATERIAL INVENTORY Completed by Title Date Instructions: List all materials used,stored,or produced onsite.Assess and evaluate these materials for their potential to contribute pollutants to Storm Water runoff.Also complete"Description of Exposed Material"worksheet if the material has been exposed during the last three years. Quality Past Significant (Units) Quality Exposed In Likelihood of Contact with Storm Water Spill or Leak Materials Purpose/Location Used Produced Stored Last 3 Years If yes,describe reason. Yes-7 No :Premiere ... . 1 APPENDIX B NON-STORM WATER DISCHARGE CERTIFICATION :::_: Premiere NON-STORM WATER DISCHARGE Sheet of ASSESSMENT AND CERTIFICATION Completed by Title Date Outfall Directly Observed Date of During theTest Method Used to Describe Results from Test for Name of Person Who Test or (identity as indicated on Test or Evaluate the Presence of Non-Storm Identify Potential Conducted the Test or Evaluation the site map) Discharged Water Discharge Significant Sources Evaluation CERTIFICATION I, (responsible corporate offical), certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or person's who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. Name&Official Title(type or Print B.Area Code and Telephone Number C.Signature. D. Date Signed '.��:Premiere Young, Brianna A From: Young, Brianna A Sent: Wednesday,April 19, 2023 10:53 AM To: Phillip Rahn Subject: RE: [External] Premiere Fiber NPDES Permit Application Renewal Questions- Stormwater Permit No. NCS000528 Good morning Phil, Please see below for responses to your questions. Section 4.1-Provide information on the facility's pollutant sources in the table below. Outfall Number Impervious Surface Area(within a mile radius of the facility) Total Surface Area Drained(within a mile radius of the facility) How can we be expected to calculate either impervious or total area drained within a mile radius of the facility. I can see if we are just concentrating on the property but a mile radius seems excessive The area offsite is helpful as it informs us of the surrounding land use area,which could affect runoff onto the permitted site.You can provide estimates for these values. Item 7.2 and Table A.All applicants must complete Table A. If the discharge is an existing discharge and your discharge is composed exclusively of stormwater(i.e., no process or nonprocess wastewater)then you only need to provide monitoring data for oil and grease, total phosphorus, total Kjeldahl nitrogen, and total nitrogen. Is this actually a requirement? I do not know if I will have a representative storm event between now and May 3 with my 30-day extension. Yes,this is a requirement.You may submit the application with all items except the monitoring so I can start reviewing information.Then you would just need to submit the monitoring data as soon as possible.The draft permit cannot proceed to public notice without all required information submitted. Please let me know if you have any other questions. Thank you, Brianna Young, MS(she/her/hers) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/Division of Energy, Mineral, and Land Resources (DEMLR) Brianna.Young@ncdenr.gov(e-mail preferred) 919-707-3647 (office) Mailing address: 1612 Mail Service Center, Raleigh, NC 27699-1612 Physical address: 512 North Salisbury Street, Raleigh, NC 27604 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. 1 Based on the current guidance to minimize the spread of COVID-19,the Department of Environmental Quality has adjusted operations to protect the health and safety of the staff and public. Please check with the appropriate staff before visiting our offices, as we may be able to handle your requests by phone or email.We appreciate your patience as we continue to serve the public during this challenging time. From: Phillip Rahn <prahn@watersedgeenv.com> Sent:Tuesday, April 18, 2023 4:21 PM To:Young, Brianna A<Brianna.Young@ncdenr.gov> Subject: [External] Premiere Fiber NPDES Permit Application Renewal Questions-Stormwater Permit No. NCS000528 CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Brianna- I am hung up on a couple items for our new permit application. In Form 4F, it asks: Section 4.1-Provide information on the facility's pollutant sources in the table below. Outfall Number Impervious Surface Area(within a mile radius of the facility) Total Surface Area Drained(within a mile radius of the facility) How can we be expected to calculate either impervious or total area drained within a mile radius of the facility. I can see if we are just concentrating on the property but a mile radius seems excessive Item 7.2 and Table A.All applicants must complete Table A. If the discharge is an existing discharge and your discharge is composed exclusively of stormwater(i.e., no process or nonprocess wastewater)then you only need to provide monitoring data for oil and grease, total phosphorus, total Kjeldahl nitrogen, and total nitrogen. Is this actually a requirement? I do not know if I will have a representative storm event between now and May 3 with my 30-day extension. Phil Rahn P.G. President Waters Edge Environmental, LLC 1434 Chester Road Raleigh, NC 27608 919.219.5820 (cell) prahn@watersedgeenv.com (email) watersedgeenvironmenta1.net (website) 2 Young, Brianna A From: Young, Brianna A Sent: Friday, March 3, 2023 3:57 PM To: dewey.fulton@universalfibers.com Cc: kbowers@premierfibers.com; tkalamatas@premierefibers.com Subject: Premiere Fibers stormwater permit NCS000528 Good afternoon, Premiere Fibers has stormwater permit NCS000528.This permit expired on May 31, 2020 and a renewal application was due by December 3, 2019.To date,the Stormwater Permitting Program has not received a renewal application. In order to keep this permit active, submit a renewal application by April 3, 2023. If an application is not received by this date, Premiere Fibers may be subject to enforcement action(s). The appropriate permitting forms can be found on our website here. In addition to submitting a renewal application, please enter your stormwater permit number into the Stormwater Permit Summary Report and you will see a form that includes the address of the facility, contact information for the permit, and the regulated stormwater outfall(s)for the facility. Please review the facility information to make sure it is correct. Information can be updated using the links provided below, where applicable: • Facility/Company name or ownership: Name/Ownership Change Form • Owner Affiliation (Legally responsible person; i.e., someone with the company who is designated to represent the company per signatory requirements or another authorized representative): Permit Contact Update Request Form • Delegation of Signature Authority(DOSA): Permit Contact Update Request Form • Billing contact: Permit Contact Update Request Form • Permit contact: Permit Contact Update Request Form • Facility contact: Permit Contact Update Request Form • Facility address only: Email Bethany Georgoulias • Stormwater outfall information: Email Bethany Georgoulias • Visit the eDMR Six Steps website and complete Steps 1 and 2. • Pay outstanding permit fees: Stormwater ePayment website Thank you, Brianna Young, MS(she/her/hers) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/Division of Energy, Mineral, and Land Resources (DEMLR) Brianna.Young@ncdenr.gov(e-mail preferred) 919-707-3647 (office) Mailing address: 1612 Mail Service Center, Raleigh, NC 27699-1612 Physical address: 512 North Salisbury Street, Raleigh, NC 27604 1 D- E- cl ; NORTH CAROLINA 7.AM Q Department of Environmental Quality Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Based on the current guidance to minimize the spread of COVID-19,the Department of Environmental Quality has adjusted operations to protect the health and safety of the staff and public. Please check with the appropriate staff before visiting our offices, as we may be able to handle your requests by phone or email.We appreciate your patience as we continue to serve the public during this challenging time. 2 wr }; af, ..W •�. i ,e' a ,:. Y � ILI ITI ` � n .^ F �� rr ` d - .t - LA" Young, Brianna A From: Young, Brianna A Sent: Wednesday,June 7, 2023 11:09 AM To: Dewey Fulton; Phil Rahn Subject: NCS000528 stormwater permit renewal acknowledgement Good morning, The Division of Energy, Mineral, and Land Resources (DEMLR) Stormwater Permitting Program acknowledges receipt of your renewal application for coverage under NPDES Permit Number NCS000528. Please continue to comply with all conditions and monitoring requirements in your current NPDES stormwater permit. As long as you have submitted a complete renewal request package and maintain compliance with those permit conditions, stormwater discharges from this facility are authorized by that permit until the Division issues a renewal permit or notifies you of an alternative action. Please let me know if you have any questions in the interim. Thank you, Brianna Young, MS(she/her/hers) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/Division of Energy, Mineral, and Land Resources (DEMLR) Brianna.Young@deg.nc.gov(e-mail preferred)PLEASE NOTE NEW EMAIL DEQ is updating its email addresses to @deq.nc.gov in phases from May 1st to June 9th. Employee email addresses may look different, but email performance will not be impacted. 919-707-3647 (office) Mailing address: 1612 Mail Service Center, Raleigh, NC 27699-1612 Physical address: 512 North Salisbury Street, Raleigh, NC 27604 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Based on the current guidance to minimize the spread of COVID-19,the Department of Environmental Quality has adjusted operations to protect the health and safety of the staff and public. Please check with the appropriate staff before visiting our offices, as we may be able to handle your requests by phone or email.We appreciate your patience as we continue to serve the public during this challenging time. 1 5/31/23,2:39 PM North Carolina Secretary of State Search Results • File an Annual Report/Amend an Annual Report • Upload a PDF Filing • Order a Document Online - Add Entity to My Email Notification List • View Filings • Print a Pre-Populated Annual Report form • Print an Amended a Annual Report form Limited Liability Company Legal Name Premiere Fibers, LLC Information Sosld: 1732139 Status: Current-Active O Date Formed: 7/27/2018 Citizenship: Foreign State of Incorporation: DE Annual Report Due Date: April 15th Currentgnnual Report Status: Registered Agent: CT Corporation System Addresses Mailing Principal Office Reg Office 10056 Us Highway 52 North 10056 Us Highway 52 North 160 Mine Lake Ct Ste 200 Ansonville, NC 28007 Ansonville, NC 28007 Raleigh, NC 27615 Reg Mailing 160 Mine Lake Ct Ste 200 Raleigh, NC 27615 Company Officials All LLCs are managed by their managers pursuant to N.C.G.S. 57D-3-20. President Chief Executive Officer Chief Financial Officer John T Amirtharaj Richard Marcus Ammen Greg Gentry 10056 Us Highway 52 North 10056 Us Highway 52 North 10056 Us Highway 52 North Ansonville NC 28007 Ansonville NC 28007 Ansonville NC 28007 https://www.sosnc.gov/online_services/Search/Business_Registration_profile?ld=14423878 1/2 5/31/23,2:39 PM North Carolina Secretary of State Search Results Secretary Greg Gentry 10056 Us Highway 52 North Ansonville NC 28007 https://www.sosnc.gov/online_services/Search/Business_Registration_profile?ld=14423878 2/2 '!%WATERS EDGE ENVIRONMENTAL, LLC 1434 CHESTER ROAD.RALEIGH, NC 27608• PHONE 919.219.5820 May 23, 2023 Brianna Young, MS (she/her/hers) Industrial Individual Permits Coordinator Stormwater Permitting Program NC DEQ/ Division of Energy, Mineral, and Land Resources (DEMLR) 1612 Mail Service Center, Raleigh,NC 27699 Reference: NPDES Stormwater Permit Renewal Application Premiere Fibers Facility 10056 US S.R. 52N Ansonville, North Carolina 28007 Stormwater Permit No. NCS000528 Waters Edge Job No. R9-21 Dear Ms. Young: �. We are attaching the NPDES Stormwater Permit Renewal application for the above-mentioned facility located in Ansonville, Anson County, North Carolina. We have the following attachments: • EPA NPDES Permit Summary Report-Appendix A • EPA NPDES Renewal- Certification- Appendix A EPA NPDES Supplemental Information Form- Appendix A • EPA Form 3510-1-Appendix B '• • EPA Form 3510-2f-Appendix C • Laboratory Documentation of Representative Sampling Event for parameters specified in Item 7.2 and Table A (oil & Grease, total P, total Kjeldahl N, and total N- Appendix D • Figure I- USGS Project Location Map with Outfall Drainage Areas • Figure 2- Project Location Map • Figure 3- Site Map with five (5) outfalls, groundwater monitoring well locations, and exterior structures including loading and unloading docks. If you have any questions, or if we may be of further assistance, please contact me at prahnL�watersedgeenv.com or 919.219.5820. Sincerely, Waters Edge Environmental, LLC Phillip L. Rahn QED .;� President .,a v .I I.tli.11 cc: Mr. Dewey Fulton and Mr. Chris Fowler- Premier Fibers D �ALR Stprm��ater Program 23-021 , { CaA6y AU- \ E, r _ � r `\ - r' 1: o z Leak Is& PEE DE E _A'CIUU / WILDLIFE REFCiGF. 44 77- se Ro CK haron ., S `• - f ! ~ .J �- E�endshiP CT�gqrch Of God LEGEND Ansonville t ) 1-mile Radius 43� 1 �' Property Boundary fo, 7:,;Iu Cs_, o Outfall 1-2 Drainage Area .:, AYLES 1000 0 1000 20DO 3000 4000 5000 6000 70M 8000 9000 SD000 Outfall 3-5 Drainage Area ; 6Pt: e,nr. FEET Job No. Tuljo Quad Bare Title Project Location Man�silh Outfall Drainage Areas ,MLWATERS EDGE ENVI RONM ENTAL, LLC R9-21 Ansonville 3.15.2023 File Name hi,qure 5'cale Prvjecr 1'rcn,iere Filers 23-023 I bar scale Ansonville.North Carolina _C2 LEGEND Property Boundary 0 5 1,000 500, Job No. Topo Quad Dare rifle Project Locafion map WATERS EDGE ENVIRONMENTAL, LLC AnsonvilIc 1 3 152023 I'de Name iFigure Scale Project Premiere Fibers 23-023 2 bar scale Ansonville.North Caerolina STORAGE LOCATIONS A Nitrogen Tank k '. Kx<�• B Raw Materials Silos C Diesel Fuel Tank D Propane Tank f" E Trash Dumpster ; F Hydrogen Cylinders G Receiving/Loading Dock + owl ,� H Metal Dumpster I Drum Storage 7. S - t 7 �' r � + R t- LEGEND Monitoring Well -in Deep Monitoring Well Outfall Sampling Location Outfall Boundaries job Image/Photo Date Title Site Map with Monitoring Wells and Oull'ail WATERS EDGE ENVIRONMENTAL. LLC R9-21 2022 Google Farth 3 20 2023 Locations File Name Figure Sc Premierrl,ihers 23-023 3 hat scale Anson isle.North Carolina NC Division of Energy, Mineral and Land Resources W NPDES Stormwater Permit Summary NC DCMLR has the following information in our Permit Database for vour perinit as of 3/28/2023. Permit Number: NCS000528 Permit Status: Expired Permit Type: Stormwater Discharge, Individual Facility Name: Premiere_Fibers Facility Addressi: 10056 US Hwy 52 N Facility Address2: City, State&Zip: Ansonyille, NC 28007 Owner Information Details: MUST submit a Change of Name/Ownership form to DEMLR to make any changes to this Owner information. .Click Here for "Change of Name/Ownership"Form) Owner Name: Premiere Fibers Owner Type: Non-Government Owner Type Group: Organization *** Legally Responsible for Permit*** (Responsible corporate officer/p rinci pie executive officer or ranking elected official/general partner or proprietor; or any other person with delegated signatory authority from the legally responsible person.) Owner Affiliation. Dewey Fulton Title: Addressi: PO Box 8930 v. Address2: City,State&Zip: Bristol, VA 24203 Work Phone: 423-306-7339 Fax: 276-669-3304 �. Email Address: dewev.fulton@universalfibers.com *** Permit Annual Fee Billing *** Billing Month: September Invoice Number Invoice Date Invoice Due Date Invoice Amount Invoice Status Owner Contact Person(s) Contact Name Title Address Phone Fax Email Facility Contact Person(s) Contact Name Title Address Phone Fax Email Kevin Bowers PO Box 436,Ansonville, NC 28007-0436 704-826-8321 704-826-6159 kbowers@premierFb ers.com Dewey Fulton PO Box 8930, Bristol, VA 24203 276-645-9719 Permit Contact Person(s) Contact Name Title Address Phone Fax Email 3/28/2023 Page 1 NC Division of Energy,, Mineral and Land Resources NPDES Stormwater Permit Summary NC DEMLR has the following information in our Permit Database for your permit as of 3/28/2023. Contact Name JW& Address Phone Fax EMU Dewey Fulton PO Box 8930,Bristol,VA 24203 276-645-9719 4 Type Contact Name 1-ft Address ne Fax Email air ........... R ..L NOW Tvae Contact Name Title Address one Fax do UP Outfall#: 001 Outfall Description: unknown Outfall Lattitude: 35.212780 Outfall Longitude: -80.110560 Represented by Outfall: %Stormwater: 100 %Industrial: Stream Waterbody Basin Waterbody Name Index Number Classification Yadkin Buffalo Creek 13-18-1 C r. Ad ,w, 3/28/2023 Page 2 r w STORMWATER POLLUTION PREVENTION PLAN DEVELOPMENT AND IMPLEMENTATION CERTIFICATION a North Carolina Division of Energy, Mineral, and Land Resources—Stormwater Program Facility Name: Premiere Fibms Permit Number NCs000528 Location Address: ,Goss us Highway 52 North lid Ansonvi0e,NC 28007 County: Anson I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all attachments were developed and implemented under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information required by the SPPP. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information gathered is, to the best of my knowledge and belief, true, accurate and complete." And "I certify that the SPPP has been developed, signed and retained at the named facility location, and the SPPP has been fully implemented at this facility location in accordance with the terms and conditions of the stormwater discharge permit." r And "I am aware that there are significant penalties for falsifying information, including the possibility of fines and imprisonment for knowing violations." .. Sign(according to permit signatory requirements)and return this Certification. DO NOT SEND STORMWATER POLLUTION PREVENTION PLAN WITH THIS CERTIFICATION. a.r Signature _ Da go„�Lkweo GU r A Print or type me of person signing above Itle a14 ems. �u SPPP Certification 10/13 ,r so we SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF INDIVIDUAL NPDES STORMWATER PERMIT Two copies of each of the following shall accompany this submittal in order for the application to be considered complete: (Do not submit the site Stormwater Pollution Prevention Plan) }4 Initials DF 1. A current Site Map from the Stormwater Pollution Prevention Plan. The location of industrial activities(including storage of materials, disposal areas, process areas and loading and unloading areas),drainage structures,drainage areas for each outfall, building locations and impervious surfaces should be clearly noted. DF 2. A summary of Analytical Monitoring results during the term of the existing permit (if your permit required analytical sampling). Do not submit individual lab reports. The summary can consist of a table including such items as outfall number, parameters sampled, lab results, date sampled,and storm event data. DF 3. A summary of the Visual Monitoring results. Do not submit individual monitoring reports.The summary can consist of a table including such items as outfall number, parameters surveyed, observations, and date monitoring conducted. DF 4. A summary of the Best Management Practices utilized at the permitted facility. Summary should consist of a short narrative description of each BMP's in place at .r the facility. If the implementation of any BMP's is planned, please include information on these BMP's. DF 5. A short narrative describing any significant changes in industrial activities at the permitted facility. Significant changes could include the addition or deletion of work processes, changes in material handling practices, changes in material storage practices, and/or changes in the raw materials used by the facility. DF 6. Certification of the development and implementation of a Stormwater Pollution Prevention Plan for the permitted facility(Sign and return attached form). If the final year analytical monitoring of the existing permit term has not been completed prior to filing the renewal submittal, then the last years monitoring results should be submitted within 30 days of receipt of the laboratory reports. (i.e.do not withhold renewal submittal w waiting on lab results) p EPA Identification Number NPDES Perm t Number Faality Name Form Approved 03105119 NCD986230159 NCSODOS28 Premiere Fibers OMB No.2040-0004 Form U.S.Environmental Protection Agency t t"YEPA Application for NPDES Permit to Discharge Wastewater NPDES GENERAL INFORMATION SECTION ! '• 1 1.1 Applicants Not Required to Submit Form 1 Is the facility a new or existing publicly owned Is the facility a new or existing treatment works 1.i.1 treatment works? 1.1.2 treating domestic sewage? If yes,STOP. Do NOT complete 0 No If yes,STOP. Do NOT No Form 1.Complete Form 2A. complete Form 1.Complete Form 2S. 1.2 Applicants Required to Submit Form 1 1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing, E operation or a concentrated aquatic animal commercial,mining,or silvicultural facility that is a production facility? currently discharging process wastewater? Ej Yes 4 Complete Form 1 21 No ❑ Yes -* Complete Form 0 No z and Form 2S. 1 and Form 2C. 1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing, mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that commenced to discharge? discharges only nonprocess wastewater? C Yes 4 Complete Form 1 0 No ❑ Yes 4 Complete Form []✓ No R and Form 2D. 1 and Form 2E. d) 47 1.2.5 Is the facility a new or existing facility whose discharge is composed entirely of stormwater a associated with industrial activity or whose discharge is composed of both stormwater and non-stormwater? 0✓ Yes 4 Complete Form 1 ❑ No and Form 2F unless exempted by 40 CFR 122.26(b)(14)(x)or b 15 . SECTIOND•- AND LOCATION(40 2.1 Facilit y Name Premiere Fibers 0 2.2 EPA Identification Number u O NCD986230159 ro 2.3 Facility Contact Name(first and last) Title Phone number Dewey Fuiton Corporate Engineer (276)645-9719 to Email address dewey.fulton@universalfibers.com 2A Facility Mailing Address E Street or P.O.box R PO Box 8930 City or town State ZIP code Bristol VA 24203 EPA Form 3510-1(revised 3-19) Page 1 EPA Identification Number NPDES Permit Number Fa6lity Name Form Approved 03/05/19 NCD986230159 NCS000528 Premiere Fibers OMB No.204M004 y 2.5 Facility Location Street,route number,or other specific identifier Q �0 10056 US Highway 52 North a� 0 County name County code(if known) Anson E City or town State ZIP code E -o z m Ansonville NC 28007 SECTION • NAICS CODES1 3.1 SIC Code(s) Description(optional) 2824 Man made organic fiber N Gl 0 c.3 W u z 3.2 NAICS Code(s) Description(optional) �rs C 325220 U W _ 4.1 Name of Operator Premiere Fibers 0 4.2 Is the name you listed in Item 4.1 also the owner? E 0 ❑✓ Yes ❑ No w 4.3 Operator Status 0 �— 2 ❑ Public—federal ❑ Public—state ❑ Other public(specify) o IDPrivate ElOther(specify) 4.4 Phone Number of Operator (276)645-9719 4.5 Operator Address Street or P.O. Box E PO Box 8930 c .S City or town State ZIP code 0 o Bristol VA 24203 o Email address of operator 0 dewey.fulton@universalfibers.com SECTION • • ! 0 c 5.1 Is the facility located on Indian Land? ❑Yes ❑✓ Na EPA Form 3510-1(revised 3-19) Page 2 EPA IdenbficalJon Number NPDES Permit Number Facility Name Form Approved 03105119 NCD986230159 NC5000528 Premiere Fibers OMB No.2040-0004 SECTION •• I 6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each) d m NPDES(discharges to surface ❑ RCRA(hazardous wastes) ❑ UIC(underground injection of o water) fluids) NC5000528 NCD986230159 w ❑ PSD(air emissions) ❑ Nonattainment program(CAA) ❑ NESHAPs(CAA) �a X ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) ❑ Other(specify) LU SECTI• 1 7.1 Have you attached a topographic map containing all required information to this application?(See instructions for m specific requirements.) ` ❑/ Yes ❑ No ❑ CAFO—Not Applicable(See requirements in Form 213.) SECTIONOF I 8.1 Describe the nature of your business. Man-made organic fiber-SIC 2824 N a c 7 O Gl 7 2 SECTION •! I 9.1 Does your facility use cooling water? �- ❑ Yes ❑ No 4 SKIP to Item 10.1. v ' 9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at � 40 CFR 125,Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your o Y NPDES permitting authority to determine what specific information needs to be submitted and when.) ca SECTION1 VARIANCE REQUESTS 1 1 10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and when.) d ❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section x Section 301(n)) 302(b)(2)) d ❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a)) Section 301(c)and(g)) Not applicable EPA Form 3510-1(revised 3-19) Page 3 EPA ldentir:cat on Number WDES Permit Number Facihty Name Form Approved 03105119 NCD996230159 NCSr10052$ Premiere Fibers OMB No 2040-0004 SECTION1 CERTIFICATION STATEMENT(40 . . 111 In Column 1 below,mark the sections of Form t that you have completed and are submitting with your application. For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note that not all applicants are r uired to provide attachments. Column 1 Column 2 Section 1:Activities Requiring an NPDES Permit ❑ w/attachments ❑� Section 2:Name,Mailing Address,and Location ❑ wl attachments 0 Section 3:SIC Codes ❑ wl attachments 0 Section 4:Operator Information ❑ wl attachments ❑J Section 5:Indian Land ❑ wl attachments e 0 Section S:Existing Environmental Permits ❑ wl attachments ❑ Section 7:Map 0 w'topographic ❑✓ w/additional attachments 14map n 0 Section 8:Nature of Business ❑ wl attachments a ❑ Section 9:Cooling Water Intake Structures ❑ wi attachments V Section 10:Variance Requests El wi attachments c []� Section 11:Checklist and Certification Statement ❑ w/attachments Y 11.2 Cartificatlon Statement U t certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. t am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name(print or type first and last name) Official title 4074 � f Sign tufe Dale signed .R � Z5 ZVZ15 EPA Form 3510.1(revised 3-19) Page 4 EPA Identification Number NPDES Permit Number Facility Name Form Approved D3105119 NCD986230159 NCS000529 Premiere Fibers OMB No.2040-0004 Form U.S Environmental Protection Agency 2F 8,EPA Application for NPDES Permit to Discharge Wastewater NPDES STORMWATER DISCHARGES ASSOCIATED WITH INDUSTRIAL ACTIVITY LOCATIONr 1.1 Provide information on each of the facili 's outfalls in the table below Outfall Receiving Water Name Latitude Longitude Number 1 Buffalo Creek 35' 07' 14" N 80° 06' 20" W c a u 2 Buffalo Creek 35' 07 14" N 80' 06' 16" W 0 J 3 Buffalo Creek 35' 07' 11" N 80, 06' 15" W 4 Buffalo Creek 35' 07 08" N 80, 06' 16' W 5 Buffalo Creek 35` 07' 08" N 80, 06' 15 W SECTION - 1 s 2.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing, upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could affect the discharges described in this application? ❑ Yes [. No 4 SKIP to Section 3. 2.2 Briefly identify each applicable project in the table below. Brief Identification and Affected Outfalls Final Compliance Dates Description of Project (list outfatl numbers) Source(s)of Discharge Required Projected c m E 0 a. E 2.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects that may affect your discharges)that you now have underway or planned?(Optional Item) ❑ Yes ❑ No EPA Form 3510-2F(Revised 3-19) Page 1 w EPA Identification Number NPDES Permit Number Facility Name Fors Approved 03/05119 NCD986230259 NC5000528 Premiere Fibers OMB No.2040-0004 SECTION 3.SITE /'A 1 3.1 Have you attached a site drainage map containing all required information to this application?(See instructions for 0 cc C specific guidance.) in 'cc M ® Yes ❑ No r SECTIONPOLLUTANT SOURCESi 4.1 Provide information on the facility's pollutant sources in the table below. Outfall Impervious Surface Area Total Surface Area Drained ` Number (within a mile radius of the fadlity) (within a mile radius of the facility) specify units specify units 1 1.13 acres 30.13 acres —• specify units specify units 2 0.46 acres 30.13 acres specify units specify units 3 0.46 acres 54.54 acres specify units specify units 4 0.55 acres 54.54 acres •--• specify units specify units 5 0.07 acres 54.53 acres specify units specify units 4.2 Provide a narrative description of the facility's significant material in the space below.(See instructions for content requirements.) Premiere Fibers is a converter of Nylon-Type 6,Nylon-Type 6.6 and Polyester pellets into a wound fiber. Synthetic oils a) are applied for future processing. 0 0 4.3 Provide the location and a description of existing structural and non-structural control measures to reduce pollutants in stormwater runoff. See instructions fors ecific uidance. 5tormwater Treatment Codes from Outfall Number Control Measures and Treatment Exhibit 2F-1 list 1 No control measures 2 No control measures 3 No control measures 4 No control measures 5 No control measures EPA Form 3510-2F(Revised 3-19) Page 2 EPA Wenfificaton Number NPDES Permit Number racirrly Name Farm Approved 03105/19 NCD986230159 NC5000528 Premiere Fibers OMB No.2D40-OD04 SECTION •N STORMWATER 1 r 5.1 1 certify under penalty of taw that the outfall(s) covered by this application have been tested or evaluated for the presence of non-stormwater discharges. Moreover, / certify that the outfalls identified as having non-stormwater discharges are described in either an accompanying NPDES Form 2C,2D,or 2E application. Name(print or type first and last name) Official titte Dewey Fulton Signature Date signe 72� 2c�Z s' 5,2 Provide the testing information requested in the table below. OuNall Onsite Drainage Points Number During of Testing Method Used Dates)of Testing Directly Observed Duran Test i Direct Observation 04/25/2023 Yes 2 Direct Observation 04/25/2023 Yes 0 Z 3 Direct Observation 04/25/2023 Yes 4 Direct Observation 04/25/2023 Yes 5 Direct Observation 04/25/2023 Yes SECTIONOR 1 1 6.1 Describe any significant leaks or spills of toxic or hazardous pollutants in the last three years. w None n 0 se a ». c iA SECTION DISCHARGE INFORMATION1 See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must com lete.Not all applicants need to complete each table. 7.1 Is this a new source or new discharge? a ❑ Yes 4 See instructions regarding submission of ❑ No 4 See instructions regarding submission of estimated d ata. actual data. CE' Tables A,B,C,and D u 7.2 Have you completed Table A for each outfall? []✓ Yes ❑ No EPA Farm 3510-2F(Revised 3.19) Page 3 AM EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 NCD986230159 NCSOOO528 FPremiere Fibers OMB No.2040-0004 7.3 Is the facility subject to an effluent limitation guideline(ELG)or effluent limitations in an NPDES permit for its process y„F wastewater? ❑ Yes ❑✓ No 4 SKIP to Item 7.5. 7.4 Have you completed Table B by providing quantitative data for those pollutants that are(1)limited either directly or a� indirectly in an ELG and/or(2)subject to effluent limitations in an NPDES permit for the facility's process wastewater? ❑ Yes ❑✓ No 7.5 Do you know or have reason to believe any pollutants in Exhibit 2F-2 are present in the discharge? ❑ Yes ❑✓ No 4 SKIP to Item 7.7. 7.6 Have you listed all pollutants in Exhibit 2F-2 that you know or have reason to believe are present in the discharge and r� provided quantitative data or an explanation for those pollutants in Table C? ❑ Yes ❑ No 7.7 Do you qualify for a small business exemption under the criteria specified in the Instructions? ❑ Yes 4SKIP to Item 7.18. ❑ No 7.8 Do you know or have reason to believe any pollutants in Exhibit 2F-3 are present in the discharge? .� ❑ Yes ❑✓ No 4 SKIP to Item 7.10. 7.9 Have you listed all pollutants in Exhibit 2F-3 that you know or have reason to believe are present in the discharge in c Table C? 1 ,� �`o� ❑ Yes No 0 7.10 Do you expect any of the pollutants in Exhibit 2F-3 to be discharged in concentrations of 10 ppb or greater? ❑ Yes ❑✓ No-*SKIP to Item 7.12. �+ o 7.11 Have you provided quantitative data in Table C for those pollutants in Exhibit 2F-3 that you expect to be discharged in oM concentrations of 10 ppb or greater? sr El Yes ❑✓ No 7.12 Do you expect acrolein,acrylonitrile,2,4-dinitrophenol,or 2-methyl-4,6-dinitrophenol to be discharged in concentrations of 100 ppb or greater? &d ❑ Yes ❑✓ No 4 SKIP to Item 7.14. 7.13 Have you provided quantitative data in Table C for the pollutants identified in Item 7.12 that you expect to be discharged in concentrations of 100 ppb or greater? *p ❑ Yes [D No 7.14 Have you provided quantitative data or an explanation in Table C for pollutants you expect to be present in the discharge at concentrations less than 10 ppb(or less than 100 ppb for the pollutants identified in Item 7.12)? ❑ Yes ❑✓ No 7.15 Do you know or have reason to believe any pollutants in Exhibit 2F-4 are present in the discharge? ❑ Yes ❑✓ No 4 SKIP to Item 7.17. 7.16 Have you listed pollutants in Exhibit 2F4 that you know or believe to be present in the discharge and provided an explanation in Table C? r.� ❑ Yes 0 No 7.17 Have you provided information for the storm event(s)sampled in Table D? ❑ Yes ❑✓ No .w EPA Form 3510-2F(Revised 3-19) Page 4 ors EPA ideritEfication Number NPDES Permit Number Facility Name Form Approved 03/05/19 NCD986230159 NCS000528 Premiere Fibers OMB No.2040-0004 Used or Manufactured Toxics - 7.18 Is any pollutant listed on Exhibits 21 through 2F-4 a substance or a component of a substance used or 8 manufactured as an intermediate or final product or byproduct? a ❑ Yes �]✓ No 4 SKIP to Section 8. 0 7.19 List the pollutants below,including TCDD if applicable. 1. 4. 7. m cc 2. 5. 8. U c3 3. 6. 9. I SECTIONe eG ICAL TOXICITY TESTING DATA i 8.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on ro any of your discharges or on a receiving water in relation to your discharge within the last three years? ❑ Yes ✓❑ No 4 SKIP to Section 9. N 8.2 Identify the tests and their purposes below. Test(s) Purpose of Test(s) Submitted to NPDES gate Submitted x Permitting Authority? Q ~ ❑ Yes ❑ No U_ o ❑ Yes ❑ No m0 ❑ Yes ❑ No SECTION 9.CONTRACT ANALYSIS INFORMATIONi 9.1 Were any of the analyses reported in Section 7(on Tables A through C)performed by a contract laboratory or consulting firm? ❑ Yes ❑ No 4 SKIP to Section 10. 9.2 Provide information for each contract laboratory or consulting firm below. Laboratory Number 1 Laboratory Number 2 Laboratory Number 3 Name of laboratory/firm Pace Analytical 0 .a E 0 N Laboratory address 370 West Meadow Road U) ? Eden,North Carolina �a a U R 0 Phone number ca (336)623-8921 Pollutant(s)analyzed TSS,COD,and pH(analyzed semi-annually 0&G,Total P, Total Kjeldahl nitrogen,and Total Nitrogen were analyzed on 4/25/2023 EPA Form 3510-2F(Revised 3-19) Page 5 EPA IdenVication Number NPpES Permit Number raa_Ihy Name Farm Approved 03/05/19 NCD9S623p159 NCS000528 Premiere Fibers OMB No.2040-0004 SECTION 1 1 CERTIFICATION STATEMENT(40 and 10.1 In Column 1 below,mark the sections of Form 2F that you have completed and are submitting with your application.For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note that not all applicants are required to com fete all sections or provide attachments. Column 1 Column 2 ❑✓ Section 1 ❑ w/attachments(e.g„responses for additional outfalls) .....................__..........................._......... _._-----._._._........_....__--_......_...._.._._....._._.._................ ...._........_........._.......... ❑ Section 2 ❑ wi attachments Section 3 ❑ wl site drainage map �. Section 4 ❑ wi attachments ❑ Section 5 ❑ wl attachments .�. ✓n_ Section 6 ❑ wl attachments ❑� Section 7 El Table A ❑ wl small business exemption request .� _ ❑ Table B ❑ wl analyticai results as an attachment 0 ❑ Table C ❑ Table D '~ ❑✓ Section 8 ❑ w/afachments ❑ Section 9 ❑ wlattachments(e.g.,responses for additional contact laboratories or firms) �" ❑ Section 10 ❑ 10.2 Certification Statement l certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is,to the best of my knowledge and belief, true, accurate,and complete.l am aware that there are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations. Name(print or type first and last name) Official title Dewey Fulton Director-Health,Safety and Environment Signatur Date signedff o EPA Form 3510.2F(Revised 3-19) Page 6 EPA Identification Number NPDES Permit Number Facility Name 0utfall Number Farm Approved 03195119 NCD986230159 NCS000523 Premiere Fibers 001 0Mt3 No.2040-0004 TABLE A.CONVENTIONAL AND • • • r You must provide the results of at least one anal sis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (specify units) (specify units) Number of Storm information Pollutant or Parameter Grab Sample Taken Flow-Weighted Grab Sample Taken Flow-Weighted Events Sampled (new sourcelnew During First During First dischargers only;use 30 Minutes Composite 30 Minutes Composite codes in instructions) 1. Oil and grease ND 1 NA 2. Biochemical oxygen demand(BOD5) NA NA NA NA NA NA 3. Chemical oxygen demand(COD) NA NA NA NA NA NA 4. Total suspended solids(TSS) NA NA NA NA NA NA 5. Total phosphorus 0.082 mg/L NA NA NA 1 NA 6, Total Kjeldahl nitrogen(TKN) 1.1 mg/L NA NA NA 1 NA 7. Total nitrogen(as N) 1.4 mg/L NA NA NA 1 NA pH(minimum) NA NA NA NA t3. pH(maximum) NA NA NA NA Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2F(Revised 3-19) Page 7 EPA IdenKcation Number NPDES Permit Number Facility Name Outfall Number Form Approved 03 D5119 NCD986230159 NCS000528 Premier Fibers 002 OMB No.2040-OOD4 TABLE A. / / 1 NON CONVENTIONALr You must provide the results of at least one anal sis toreveTy pollutant in this table.Complete one table for each autfall.See instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (specify units) (specify units} Number of Storm Information Pollutant or Parameter Grab Sample Taken Flow-Weighted Grab Sample Taken Flow-Weighted Events Sampled (newsourcelnew During First During First dischargers only;use 30 Minutes Composite 30 Minutes Composite codes in instructions) 1. Oil and grease ND 1 NA 2. Biochemical oxygen demand(BOD5) NA NA NA NA NA NA 3. Chemical oxygen demand(COD) NA NA NA NA NA NA 4. Total suspended solids(TSS) NA NA NA NA NA NA 5. Total phosphorus 0.077m8/L NA NA NA 1 NA 6. Total Kjeldahl nitrogen(TKN) 1.3mg/L NA NA NA 1 NA 7. Total nitrogen(as N) 1.6 mg/L NA NA NA 1 NA pH(minimum) NA NA NA NA 8. pH(maximum) NA NA NA NA f Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter 1,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2F(Revised 3-19) Page 7 EPA Identificalion Number NPDES Permit Number Facility Name Outfall Number Form Approved 03 05119 NCD986230159 NC5000528 Premier Fibers 003 OMB No.2040-0004 TABLE A.CONVENTIONAL • • s r You must provide the results of at least one anal sis for every pollutant in this table.Complete ane table for each oulfall.See instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (specify units) (specify units) Number of Storm Information Pollutant or Parameter Grab Sample Taken Grab Sample Taken (new source/new During First Flow-Weighted During First Flow•Weighfed Events Sampled dischargers only;use 30 Minutes Composite 30 Minutes Composite ? codes in instructions 1. Oil and grease ND 1 NA 2. Biochemical oxygen demand(BOD5) NA NA NA NA NA NA 3. Chemical oxygen demand(COD) NA NA NA NA NA NA 4. Total suspended solids(TSS) NA NA NA NA NA NA b. Total phosphorus ND NA NA NA 1 NA 6. Total Kjeldahl nitrogen(TKN) 0.72 mg/L NA NA NA 1 NA 7. Total nitrogen(as N) 1.7 mg/L NA NA i NA NA pH(minimum) NA NA NA NA B, pH(maximum) NA NA NA NA 'Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2F(Revised 3-19) Page 7 EPA Identification Number NPDES Permit Number Facility Name outfall Number Form Approved 03+95119 NCD986230159 NCS000528 Premier Fibers 004 OMB No.204W004 TABLE A.CONVENTIONAL AND • • • t You must provide the results of at least one anal sis for every pollutant in this table.Complete one table for each out€all.See instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (specify unds) (Specltyt1flit,S) Number of Storm Information Pollutant or Parameter Grab Sample Taken Flow-Weighted Grab Sample Taken Flow-Weighted Events Sampled (new sourcelnew During First During First dischargers only;use 34 Minutes Composite 30 Minutes Composite codes in instructions) 1. Oil and grease ND 1 NA 2. Biochemical oxygen demand(BOD5) NA NA NA NA NA NA 3. Chemical oxygen demand(COD) NA NA NA NA NA NA 4. Total suspended solids(TSS) NA NA NA NA NA NA 5. Total phosphorus 0.080 mg/L NA NA NA 1 NA 6. Total Kjeldahl nitrogen(TKN) 0.70 mg/L NA NA NA 1 NA 7. Total nitrogen(as N) 1.5 mg/L NA NA Alili 1 NA pH(minimum) NA NA NA NA pH(maximum) NA NA NA NA ------------- 'Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3514-2F(Revised 3-19) Page 7 l I I b I I 1 1 I I 1 ! 4 ! r I 1 1 EPA Identification Number NPDES Permit Number Facility Name putfall Number Form Approved 03105119 NCD986230159 NC5000528 Premier Fibers 005 OMB No.2040-0004 TABLE A.CONVENTIONAL A • NON CONVENTIONAL You must provide the results of at least one anal sis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (specify units) (specify units) Number of Storm information Pollutant or Parameter Grab Sample Taken Flow-Weighted Grab Sample Taken Flow-Weighted Events Sampled (new sourcelnew During First During First dischargers only;use 30 Minutes Composite 30 Minutes Composite codes in instructions) 1. Oil and grease ND 1 NA 2. Biochemical oxygen demand(BOD5) NA NA NA NA NA NA 3. Chemical oxygen demand(COD) NA NA NA NA NA NA 4. Total suspended solids(TSS) NA NA NA NA NA NA 5. Total phosphorus 0.12 mg/L NA NA NA 1 NA 6. Total Kjeldahl nitrogen(TKN) 1.3 mg/L NA NA NA i NA 7. Total nitrogen(as N) 2.6 mg/L NA NA NA 1 NA pH(minimum) NA NA NA NA 8. pH(maximum) NA NA NA NA Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I:subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510.21'(Revised 3-19) Page 7 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03105119 NCD98623O159 NCSO0O528 Premiere Fibers 001 OMB No.2040-0004 TABLE B.CERTAIN CONVENTIONAL AND NON • • '• 41 CFR 122.26(c)(1)(i)(E)(4) 40 List each pollutant that is limited in an effluent limitation guideline(ELG)that the facility is subject to or any pollutant listed in the facility's NPDES permit for its process wastewater(if the facility is operating under an existing NPDES permit).Complete one table for each outfall.See the instructions for additional details and requirements. Maximum Daily Discharge Average Daily Discharge Source of (spec! units s units Number of Storm, Information Pollutant and CAS Number(ff available) Grab Sample Taken Grab Sample Taken (new sourcehiew During First Flow-Weighted During First Flow-Welghted Events Sampled dischargers only,use Composite During 30 Minutes 30 Minutes codes in instructions) Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2F(Revised 3-19) Page 9 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outtall Number Form Approved 03105I19 NCD986230159 NC5000528 Premiere Fibers 001 OMB No.2040-0004 TABLE C.TOXIC POLLUTANTS,CERTAIN HAZARDOUS SUBSTANCES,AND ASBESTOS(40 CFR 122.26(c)(1)(i)(E)(4)and 40 CIFIR 122.21(g)(7)(vi)(B)and(vii))' List each pollutant shown in Exhibits 2F-2, 2F-3,and 2F-4 that you know or have reason to believe is present.Complete one table for each outfall. See the instructions for additional details and requirements. Maximum daily Discharge Average Daily Discharge Source of s eci units s eci units Number of Storm Information Pollutant and CAS Number(if available) Grab Sample Taken Grab Sample Taken (new sourcelnew During First Flow-Weighted During First Ffow-Weighted Events Sampled dischargers only;use 30 Minutes Composite 30 Minutes Composite codes in instructions) Sampling shall be conducted according to sufficiently sens4ive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2F(Revised 349) Paoe 11 --I —This page intentionally left blank. an Pace Analytical Services,LLC ace Analytical 2]5 East Meadow Road-Suite A Eden,NC 27288 www.pacelabsxom {336}623-8921 May 10, 2023 Mr. Phil Rahn Waters Edge Environmental 1434 Chester Road Raleigh, NC 27606 RE: Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 Dear Mr. Rahn: Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures P p,CCAF�. ? '. REPORT OF LABORATORY ANALYSIS ;r+ This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 Of 16 Pace Analytical Services,LLC 205 East Meadow Road-Suite A aceAnalytieaf Eden,NC 27288 www,paceiabs.com (336)623-8921 i CERTIFICATIONS Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kil Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NEtAP Certification#:E87648 South Carolina Certification#:99030001 -- North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, wiftut the written consent of Pace Analytical Services,LLC. Page 2 of 16 Pace Analytical Services,LLC 1! '2ceAnalytical 205 East Meadow Road-Suite Eden,NC 27288 www.pacalabs.com (336)623-8921 SAMPLE SUMMARY Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 Lab ID Sample I❑ Matrix Date Collected Date Received 92664918001 OUTFALL 001 Water 04/25/23 11:00 05/01123 09:12 92664918002 OUTFALL 002 Water 04/25123 11:15 05/01/23 09:12 92664918003 OUTFALL 003 Water 04/25123 11:30 05/01/23 09:12 92664918004 OUTFALL 004 Water 04125/23 11:45 05/01/23 09:12 92664918005 OUTFALL 005 Water 04/25/23 12:00 05/01/23 09:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 16 Pace Analytical Services,LLC _ ace Analytical n 205 East Meadow Road-Suite A Eden,NC 27288 www.pacelabs.com (336)623.8921 SAMPLE ANALYTE COUNT Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 Analytes Lab ID Sample 10 Method Analysts Reported Laboratory 92664918001 OUTFALL 001 EPA 1664E REL 1 PASI-C TKN+NO3+NO2 Calculation MAB2 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A 92664918002 OUTFALL 002 EPA 1664E REL 1 PASI-C TKN+NO3+NO2 Calculation MAB2 1 PASI-A .. EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA305.1 Rev 2.01993 Zip 1 PASI-A 92664918003 OUTFALL 003 EPA 1664E REL 1 PASI-C TKN+NO3+NO2 Calculation MAB2 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A 92664918004 OUTFALL 004 EPA 1664B REL 1 PASI-C TKN+NO3+NO2 Calculation MA82 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A 92664918005 OUTFALL 005 EPA 1664B REL 1 PASI-C TKN+NO3+NO2 Calculation MA82 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A PAS I-A=Pace Analytical Services-Asheville PAS I-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in Full, without the written consent of Pace Analytical Services,LLC. Page 4 of 16 Pace Analytical Services,LLC ac /(n�f' tica J 205 East Meadow Road-Suite A r�t�l'1 I}/t11� l Eden,NC 27288 www.pacelabs.com (336)623-8921 ANALYTICAL RESULTS Project: PREMIERE FIBERS R9.21 Pace Project No.: 92664918 Sample; OUTFALL 001 Lab ID: 92664918001 Collected: 04/25/23 11:00 Received: 05/01/23 09:12 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method:EPA 1664B Pace Analytical Services-Chadotte Oil and Grease ND mglL 4.9 1.1 1 05/10/23 05:03 Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analytical Services-Asheville Total Nitrogen 1.4 mglL 0.040 0,040 1 05/09/23 12:21 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 1.1 mg1L 0.50 0.25 1 05/08/23 19:30 05/09/23 04:41 7727-37-9 353.2 Nitrogen,N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 0.28 mg1L 0.040 0.017 1 05/05/23 08:40 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2,0 1993 Preparation Method: EPA365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 0.082 mglL 0.050 0.025 1 05I10I2311:40 05I1012315:01 7723-14.0 Sample: OUTFALL 002 Lab ID: 92664918002 Collected: 04/25/23 11:15 Received: 05/01/23 09:12 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method:EPA 1664E Pace Analytical Services-Charlotte Oil and Grease ND mg1L 5.0 1.1 1 05/10/23 05:03 Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analytical Services-Asheville Total Nitrogen 1.6 mglL 0.040 0.040 1 05/09/23 12:21 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 1.3 mglL 0.50 0.25 1 05/08/23 19:30 05/09/23 04A2 7727-37-9 353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 0.27 mglL 0.040 0.017 1 05/05/23 08:43 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 0.077 mglL 0.050 0.025 1 05/1012311:40 05/10/2315:05 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05110/2023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 16 Pace Analytical Services,L LC �CBAnaly " 205 East Meadow Road-Suite A i G Il.�l^�f r Eden,NC 27288 www.pacelabs.com (336)623-8921 ANALYTICAL RESULTS Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 .r Sample: OUTFALL 003 Lab ID: 92664918003 Collected: 04/25/23 11:30 Received: 05/01/23 09:12 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services-Charlotte Oil and Grease ND mg1L 4.8 1.1 1 05/10/23 05:03 Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analyti cal Services-Asheville Total Nitrogen 1.7 mg1L 0.04D 0.040 1 05/09/23 12:21 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 0.72 mg/L 0.50 0.25 1 05/08/23 19:30 05/09/23 04:44 7727-37-9 353.2 Nitrogen,NO2/NO3 pros. Analytical Method: EPA353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 1.0 mglL 0.040 0.017 1 05/05/23 08:45 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville ^ Phosphorus ND mglL 1).050 0.025 1 05110/2311:40 05110/2315:07 7723-14-0 Sample: OUTFALL 004 Lab ID: 92664918004 Collected: 04/25/23 11 A5 Received: 05/01/23 09:12 Matrix: Water ^ Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services-Charlotte Oil and Grease ND mg1L 4.8 1.1 1 05/09/23 03:35 Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analytical Services-Asheville Total Nitrogen 1.5 mg1L 0.040 0,040 1 05109t23 12:21 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 0.70 mg/L 0.50 0.25 1 05/08/23 19:30 05/09/23 04:47 7727-37-9 353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 0.81 mg1L 0.040 0.017 1 05/05/23 08:46 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 0.080 mg/L 0,050 0,025 1 05/10/23 11 A0 05/10/23 15:08 7723-14-0 REPORT OF LABORATORY ANALYSIS "^ This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 16 Pace Analytical Services,LLC 1!2ce p��r,j�^ r' 205 East Meadow Road-Suite A H ly t� f Eden,NC 27288 a www.pacelabs.com (336)623-892 1 ANALYTICAL RESULTS Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 Sample: OUTFALL 005 Lab IQ: 92664918005 Collected: 04/25/23 12:00 Received: 05/01/23 09:12 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method:EPA 1664B Pace Analytical Services-Charlotte i Oil and Grease ND mg1L 4.8 1.1 1 05/10123 05:03 Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analytical Services-Asheville Total Nitrogen 2.6 mg/L 0.040 0.040 1 05/09123 12:21 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 1.3 mg1L 0.50 0.25 1 05/08/23 19:30 05/09/23 04:53 7727-37-9 353.2 Nitrogen,NO2IN03 pres. Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 1.3 mg/L 0.040 0.017 1 05/05/23 08:47 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 0.12 mg/L 0.050 0.025 1 05/10/2311:40 05110/2315:09 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 16 Pace Analytical Services,LLC accAnalyfical r 205 East Meadow Road-Suite AEden, Eden,NC 27288 www,pacela6s.com (336)623-8921 QUALITY CONTROL DATA ` Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 QC Batch: 773091 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease Laboratory: Pace Analytical Services-Charlotte .� Associated Lab Samples: 92664918004 METHOD BLANK: 4012808 Matrix: Water Associated Lab Samples: 92664918004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Oil and Grease mg1L ND 5.0 1A 05/09/23 03:35 LABORATORY CONTROL SAMPLE: 4012809 Spike LCS LCS %Rec ^ Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 34.2 86 78-114 MATRIX SPIKE SAMPLE: 4012810 92665487001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 38.8 32.5 82 78-114 ^ SAMPLE DUPLICATE: 4012811 357959520D1 Dup Max Parameter Units Result Result RPD RPD Qualifiers Oil and Grease mg1L 1.81 1.5J 30 Results presented°n this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS — This report shall not be reproduced,except in full. Date:05110/2023 04:39 PM without the written consent of Pace Analytical Services.LLC. Page 8 of 16 Pace Analytical Services,LLC aceAnalyticai` 205 East Meadow Road-Suite A Eden,NC 27283 a www.pacslahs.com (336)623-8921 QUALITY CONTROL DATA Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 QC Batch: 773286 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92664918001,92664918002,92664918003,92664918005 METHOD BLANK: 4013763 Matrix: Water Associated Lab Samples: 92664918001,92664918002,92664918003,92664918005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Oil and Grease mg/L ND 5.0 1.1 05/10/23 05:03 LABORATORY CONTROL SAMPLE: 4013764 Spike LCS LCS %Rec Parameter Units Cone. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 35.8 90 78-114 MATRIX SPIKE SAMPLE: 4014797 92665800001 Spike MS MS %Rec 4 Parameter Units Result Cone. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 39.2 35.0 83 78-114 SAMPLE DUPLICATE: 4013766 92665830001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Oil and Grease mg1L ND ND 30 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the tight or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 16 Pace Analytical Services,LLC aceAnalyrica1 Y 205 East Meadow Road-Suite A Eden,NC 27288 www.pacolabs.com (336)623-8921 QUALITY CONTROL DATA Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 QC Batch: 773107 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92664918001,92664918002,92664918003,92664918004,92664918005 METHOD BLANK: 4012953 Matrix: Water Associated Lab Samples: 92664918001,92664918002,92664918003,92664918004,92664918005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Nitrogen,Kjeldahl,Total mgJL ND 0.50 0.25 05/09/23 04:25 .� LABORATORY CONTROL SAMPLE: 4012954 Spike LCS LCS %Rec -- Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,Kjeldahl,Total mg1L 10 10A 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4012955 4012956 MS MSD 92664918003 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Nitrogen,Kjeldahl,Total mg/L 0.72 10 10 11.0 10.4 103 97 90-110 5 10 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4012957 4012958 MS MSD 92664918004 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc, Conc. Result Result %Rec %Rec Limits RPD RPD Qual Nitrogen,Kjeldahl,Total mg/L 0.70 10 10 10.7 11.5 100 108 90-110 6 10 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/1012023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 16 a� Pace Analytical Services,LLC �ce /!n�ry1ra 1 x 205 East Meadow Road-Suite A ,1! H!1 J !U r Eden,NC 27288 www.pacolabs.com (336)623-8921 QUALITY CONTROL DATA Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 QC Batch: 772073 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite,preserved Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92654918001,92664918002,92664918003,92664918004,92664918005 METHOD BLANK: 4008048 Matrix: Water Associated Lab Samples: 92664918001,92664918002,92664918003,92664918004,92664918005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Nitrogen,NO2 plus NO3 mg1L ND 0.040 0.017 05/05123 08:22 LABORATORY CONTROL SAMPLE: 4008049 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,NO2 plus NO3 mg1L 2.5 2.5 100 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4008050 4008051 Ms MSD 10651039001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc, Conc. Result Result %Rec %Rec Limits RPD RPD Qual Nitrogen,NO2 plus NO3 mg1L 0.58 2.5 2.5 2.9 3.0 94 95 90-110 1 10 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4008052 4008053 MS MSD 10651039002 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Nitrogen,NO2 plus NO3 mg1L 0.52 2.5 2.5 2.8 2.8 92 93 90-110 1 10 Results presented on this page are In the units indicated by the"Units'column except where an alternate unit is presented to the right of the result. '— REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services.LLC. Page 11 of 16 Pace Analytical Services,LLC aceAnalytrcal' 245 East Meadow Road-Suite R / Eden,NC 27288 www.pacelrabs.com (336)623-8921 QUALITY CONTROL DATA Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 �- QC Batch: 773403 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92664918001,92664918002,92664918003,92664918004,92664918005 METHOD BLANK: 4014363 Matrix: Water Associated Lab Samples: 92664918001,92664918002,92664918003,92664918004,92664918005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Phosphorus mg/L ND 0.050 0.025 05/1012315:00 LABORATORY CONTROL SAMPLE: 4014364 Spike LCS LCS %Rec Parameter Units Cone. Result %Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4014365 4014366 MS MSD 92664918001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual Phosphorus mg/L 0.082 2.5 2.5 2.7 2.7 106 106 90-110 0 10 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4014367 4014368 MS MSD 92664918002 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual Phosphorus mg/L 0.077 2.5 2.5 2.7 2.7 105 105 90-110 0 10 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS r' This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 16 Pace Analytical Services,LLC //*0"aceAnalXical r 2oe East Meadow goad-Suite A Eden,NC 27288 www.pacoiabs.cora (336)623-8921 QUALIFIERS Project: PREMIERE FIBERS R9-21 _. Pace Project No.: 92664918 DEFINITIONS OF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. NO-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count 3-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited anaiytes. TNI-The NEtAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/10/2023 04:39 PM without the written consent of Pace Analytical Services,I.I.C. Page 13 of 16 Pace Analytical Services,LLC _ aceAnalytical�� 205 East Meadow Road-Suite A Eden,NC 2728B www.pacelabs.com (336)623-8921 I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: PREMIERE FIBERS R9-21 Pace Project No.: 92664918 �^ Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92664918001 OUTFAL.L 001 EPA 1664E 773286 92664918002 OUTFALL 002 EPA 1664B 773286 92664918003 OUTFALL 003 EPA 1664B 773286 92664918004 OUTFALL 004 EPA 1664B 773091 92664918005 OUTFALL 005 EPA 1664B 773286 92664918001 OUTFALL 001 TKN+NO3+NO2 773293 Calculation 92664918002 OUTFALL 002 TKN+NO3+NO2 773293 Calculation 92664918003 OUTFALL 003 TKN+NO3+NO2 773293 Calculation 92664918004 OUTFALL 004 TKN+NO3+NO2 773293 Calculation 92664918005 OUTFALL 005 TKN+NO3+NO2 773293 Calculation 92664918001 OUTFALL 001 EPA 351.2 Rev 2.0 1993 773107 EPA 351.2 Rev 2.0 1993 773188 - 92664918002 OUTFALL 002 EPA 351.2 Rev 2.0 1993 773107 EPA 351.2 Rev 2.0 1993 773188 92664918003 OUTFALL 003 EPA 351.2 Rev 2.0 1993 773107 EPA 351.2 Rev 2.0 1993 773188 92664918004 OUTFALL 004 EPA 351.2 Rev 2.0 1993 773107 EPA 351.2 Rev 2.0 1993 773188 92664918005 OUTFALL 005 EPA 351.2 Rev 2.0 1993 773107 EPA 351.2 Rev 2.0 1993 773188 92664918001 OUTFALL 001 EPA 353.2 Rev 2.0 1993 772073 92664918002 OUTFALL 002 EPA 353.2 Rev 2.0 1993 772073 92664918003 OUTFALL 003 EPA 353.2 Rev 2.0 1993 772073 92664918004 OUTFALL 004 EPA 353.2 Rev 2.0 1993 772073 92664918005 OUTFALL 005 EPA 353.2 Rev 2.0 1993 772073 92664916001 OUTFALL 001 EPA 365.1 Rev 2.0 1993 773403 EPA 365.1 Rev 2.0 1993 773582 92664918002 OUTFALL 002 EPA 365.1 Rev 2.0 1993 773403 EPA 365.1 Rev 2.0 1993 773582 92664918003 OUTFALL 003 EPA 365.1 Rev 2.0 1993 773403 EPA 365.1 Rev 2.0 1993 773582 92664918004 OUTFALL 004 EPA 365.1 Rev 2.0 1993 773403 EPA 365.1 Rev 2.0 1993 773582 92664918005 OUTFALL 005 EPA 365.1 Rev 2.0 1993 773403 EPA 365.1 Rev 2,0 1993 773582 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full. Date:05/10/2023 0439 PM without the written consent of Pace Analytical Services.LLC- Page 14 of 16 i • ail # tl Pace'{NorborderN...beror � CHAIN-OF-CUSTODY Analytical Request Document , 4 �, o % .ft'aceAnatytical' X, -» �� t � � r 1 Chain-of-Custody is a LEGAL DOCUMENT-Complete all retevenl fields Coro ny: Billing Information: < a l.. WSE ONLY. Add s: Contatner PreservaEfve t Y ^sots ,c. nape Repor To: ! 1 Email To: ••Preservative types:(1)Mirk add,(?)sulfuric add,(3)bydroddon cad d,(4j sadn+m hydroxide,(5)zinc acetate, (6)methand.Q odlum bisulfate,(B)sodium thiosutfate,(9)hexan m m e,(A)atcorblcadd,(B)amoniu sullate, Copy)1r. (� Site Collection Info/Address: IC)ammonium 1prosddc,(0)TSP,(U)Unpreserved,(0)Other Jl� Analyses b;Proflte no - Custo er Project Name/Nu er, State: County/City: Zone Collected: Same a pi Checltliettt E /�-9-L-t : Time, 1 ,�N��,iJ t t PTt )mT{ )CT t eke t v$todp§¢aXg`Estiaeat7Itttact Y:N Phone SitelFacilityID p: Compliance Monitoring? : Cbgtody Sigaattsrets 4resent• Email: P%,Yes t ]No toliector.Sigaotitre Piengot' 9:•lltl - Bott).eN In.artt �.ill�y NA - Coil By(print): Purchase Order th OW PWs ID rt: - ccrrgct$otslca + �Y NA Quote# T—W DW Location Code r Lois t volttme tm Coitecde By(s' re): TumaraUnd Date R wired: mm iately P on Ice: a i samplesoc•svoa oa 1e0 mn e9 " • VeiC 8eadspnce.ZccbylabYn Y p p8aa.staglflnta�k se31a - Y t ( s [ ]NO ?� `s$ng+2cs 3n tasat3i>iq l�lmoit `Wt Sampl§Disposal: Rush: Field Filtered Iif applicable): , ttaaAdu•l.Cb2prsne.vrnaoat, T N t ., .* Di ' seas ap riate l 1 Return t )Same Day [ j Next Day t )Yes too Sgmpio ACCe bi [ )2 DaY [ 13 DaY t )4 DaY t )S Day Analysis �` ' °j Srtripet (EwpcdttQ Charges APP1Y) :Ld&recap t Z 13 • \ : 'a, rI ead AcrSr stet Stsi •. Matrix Codes(insert 3n Matrix box below):Drinking Water(DW),Ground Water(GW),Wastewater(WW), }•: e= t ? Product(P),Soil/Solid(SL),Oil(OL),Wipe(WP),Air(AR),Tissue(TS),B)oassay(B),Vapor(V),Other(OT) �;: r Y said os»tirlLfs ! Comp/ Collected(or Res #of Customer Sample ID Matrix' Grab Composite Start) Composite End Cl Ctns a, _ • 1: ( Date Time Date Time t ur 1 j ''" r f rAi 2 rl. .l `mil f I T .:Y .r Egg r =. ZN II i<'' 4: ..•3A: r..N'4. L7'!'iT. ' a4A l.f, -tr t.. t nit.; :±:'�-''• 'Xw:i �a `C<-_:s�4... ..c...C�--t.. � v. r Customer Remarks/Special Conditions/Possible Hazards: 7Y)te � � Blue` ':9 Df�3ie ,;. (tX {EjSPAESE�Yi( Z�Itoftr3) fff/A� �` E3b$atnill��@ttlperattJre Info F ''tV>1Ct _ a _ b;', .i , - t = xi i,. Temp BWrlk�tte t� o Y N `)`F '4nrJ.G.•YJ. ,t tr s• jy�� `r..^s}i2f1RI � ; • Carloterx;ielttp.(i�tttnt'tecelpr: •nQ �..Y-Sl-,. t. i r •r mp) u¢d- �'-'�_..} F t r ec t i' COnIeF'�?�1er111 Ctirr,F f'aC�O � Tiadyhemsatnple(Y),saeett�d{�c�00t 1,� N {� ■��"'�j{r /�,� _ ar /r�� �/ .l -..x.. ti t �- vy� }.. •4. tf'.��� t'"i.:.nij�-� i; s� �'6T,.�!• � ;WYtQ�i��d�e'"SI.-�W.�•• Refingi ished by/Comps tM W y:IS'ignature) Datemme: ceiv by/Company:(Signare) bate/f'une: ;tfY(T(t:t/x6 LJ$E 01y1 �+ ehtr» • � �w12 taf�� y� •� , + . Reiln ished ! an . I nature ime: eceiVCd b� gture): Sit Acctrium i �,• 4y g 1 Y t m Da e/Ttme: ( Terylplafe. TSp9(anlRectred ,=Y K' . prerogU, ktCf. McQH TSP °that Relinq 'Shed by/Company:(Signature) Date/Time: Received by/Company:(Signature) Date�me: PM Hon Cotif Page: " I DCi Tltte: ENV-FRM-HUNI.0084 v02 Tech Spec Sample Conditlon Upon 9tfo9Mace- i � Receipt I i11{TfL'i:Rih+Y Effective[)ate: two *Check mark top half of box if pH and/or dechiorination Project e Is verified and within the acceptance range for �n7irf preservation samples. PM ltWB Rus Date 6/23 Exceptions:VOA,Collform,TOC,Oil and Grease,DROJ8015(water)DOC,LLHg **Bottom half of box is to list number of bottles ` ' l�S=Wa ,e's Ed .. ***Check all unpreserved Nitrates for chlorine ; i 13 iI a a 0 a a O1 z v 2 Rro j Z N v Y 2 2 B I a a 9 v v a 3 a a > > T 0 t3 _ 2 N D e ro .f.4 z uo a a a i a a a a.l c Q ? E OQ O G 0¢ a u d E E E a E E E E� �_ u E E J J = Qy :: E E E oaE E E E Q 1pJE� $ o ROE rl i�v v�1 r1 „�. fV H H .q N .•�G ry A 7 N �. p N N ry aY� .. m m m m m m a 3 a a a a a o n a L" in m 1 -N s rr k11Q \\N I 2 2; Z 4 i 1 rr f \\N I 5 j �r ! 6 I i 7I N\ i 8 N\ I NMI i \N\\ iN\ It 10 ff f NEW 11 � i11 \N I 12 - N I I NNNW -N NNN 1 11 1 NN I L i pH Adjustment Log for Preserved Samples Sample lD Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservailve Lot a r r If adjusted added rr i ` Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(i.e. r.r i Out of hold,Incorrect preservative,out of temp,incorrect containers) Qualtrax Document ID:70677 Page 2 of 2 r. WATERS EDGE ENVIRONMENTAL, LLC 1434 CHESTER ROAD•RALEIGH, NC 27608•PHONE 919.219.5820 February 11, 2020 RECEIVED Mr. Bradley Bennett MAR 0 9 2020 SW NPDES Permit Coverage Stormwater Permitting Unit DEM7-LAND QUALITY 1617 Mail Service Center ST1,Mn'JVATE,R,r^E�'Ji�1 tPtii Raleigh,North Carolina 27699-1617 Reference: Stormwater Permit Renewal Premiere Fibers 10056 USW Highway 52 North Ansonville, Anson County, NC NC Stormwater Permit#NCS000528 Waters Edge Job No R9-21 Dear Mr. Bennett: The coverage for the above-mentioned permit is set to expire on June 30, 2020. We would like to request an extension of the existing permit and are hereby submitting this request to your office. If you have any questions, or if we may be of further assistance, please contact me at prahngwatersedizeenv.com or 919.859.9987. Sincerely, Waters Edge Environmental, LLC &_44Z ;�� Phillip L. Rahn President Cc: Mr. Dewey Fulton- Premiere Fibers NCDENR Central Files 20-012