HomeMy WebLinkAboutNC0000272_Analytical Results TOC WW_20230516 Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
May 12, 2023
Mr. Phil Teague
Evergreen Packaging
175 Main Street
P.O. Box 4000
Canton, NC 28716
RE: Project: WW CITY SEWER
Pace Project No.: 92665284
Dear Mr.Teague:
Enclosed are the analytical results for sample(s)received by the laboratory on May 02, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
ariel.fitzgerald@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Cintya Bailey, Evergreen Packaging
Charles Howell, Evergreen Packaging
Mr.Tracy Willis, Evergreen Packaging
�pQ AC�FO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
9eU �y without the written consent of Pace Analytical Services,LLC. Page 1 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
CERTIFICATIONS
Project: WW CITY SEWER
Pace Project No.: 92665284
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
SAMPLE ANALYTE COUNT
Project: WW CITY SEWER
Pace Project No.: 92665284
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92665284001 CITY SEWER EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 ANM 1 PASI-A
SM 5220D-2011 MAB2 1 PASI-A
SM 5220D-2011 JP1 1 PASI-A
92665284002 CITY SEWER EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 ANM 1 PASI-A
SM 5220D-2011 MA132 1 PASI-A
SM 5220D-2011 JP1 1 PASI-A
92665284003 CITY SEWER EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 ANM 1 PASI-A
SM 5220D-2011 MAB2 1 PASI-A
SM 5220D-2011 JP1 1 PASI-A
92665284004 CITY SEWER EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 ANM 1 PASI-A
SM 5220D-2011 MAB2 1 PASI-A
SM 5220D-2011 JP1 1 PASI-A
92665284005 CITY SEWER EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 ANM 1 PASI-A
SM 5220D-2011 MAB2 1 PASI-A
SM 5220D-2011 JP1 1 PASI-A
92665284006 CITY SEWER EPA 160.4/SM2540D-2011 JMH1 2 PASI-A
SM 521OB-2016 BIDE 1 PASI-A
SM 4500-P E-2011 JP1 1 PASI-A
92665284007 CITY SEWER EPA 160.4/SM2540D-2011 JMH1 2 PASI-A
SM 521OB-2016 BIDE 1 PASI-A
SM 4500-P E-2011 JP1 1 PASI-A
92665284008 CITY SEWER EPA 160.4/SM2540D-2011 JMH1 2 PASI-A
SM 521OB-2016 BIDE 1 PASI-A
SM 4500-P E-2011 JP1 1 PASI-A
92665284009 CITY SEWER EPA 160.4/SM2540D-2011 JMH1 2 PASI-A
SM 521OB-2016 BIDE 1 PASI-A
SM 4500-P E-2011 JP1 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
SAMPLE ANALYTE COUNT
Project: WW CITY SEWER
Pace Project No.: 92665284
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92665284010 CITY SEWER EPA 160.4/SM2540D-2011 JMH1 2 PASI-A
SM 5210B-2016 BIDE 1 PASI-A
SM 4500-P E-2011 JP1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 4 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284001 Collected: 05/01/23 08:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 19.6 mg/L 0.50 5 05/12/23 14:37 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 33.2 mg/L 10.0 1 05/11/23 14:50 05/12/23 07:20 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 0.25 mg/L 0.040 1 05/10/23 20:32
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 302 mg/L 25.0 1 05/05/23 13:30 05/06/23 09:53
5220D COD,Soluble Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
COD,Soluble 81.6 mg/L 25.0 1 05/09/23 00:45 05/09/23 04:58 P4
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284002 Collected: 05/01/23 10:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 24.3 mg/L 0.50 5 05/12/23 14:39 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 37.2 mg/L 10.0 1 05/11/23 19:00 05/12/23 07:48 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 0.20 mg/L 0.040 1 05/10/23 20:33
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 671 mg/L 25.0 1 05/05/23 13:30 05/06/23 09:54
5220D COD,Soluble Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
COD,Soluble 157 mg/L 25.0 1 05/09/23 00:45 05/09/23 04:59 P4
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284003 Collected: 05/01/23 12:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 16.5 mg/L 0.40 4 05/12/23 14:43 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 33.0 mg/L 10.0 1 05/11/23 14:50 05/12/23 07:21 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 0.30 mg/L 0.040 1 05/10/23 20:34
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 846 mg/L 25.0 1 05/05/23 13:30 05/06/23 09:54
5220D COD,Soluble Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
COD,Soluble 225 mg/L 25.0 1 05/09/23 00:45 05/09/23 04:59 P4
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284004 Collected: 05/01/23 14:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 14.3 mg/L 0.40 4 05/12/23 14:48 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 18.1 mg/L 10.0 1 05/11/23 19:00 05/12/23 07:49 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 0.25 mg/L 0.040 1 05/10/23 20:35
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 463 mg/L 25.0 1 05/05/23 13:30 05/06/23 09:54
5220D COD,Soluble Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
COD,Soluble 150 mg/L 25.0 1 05/09/23 00:45 05/09/23 04:59 P4
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284005 Collected: 05/01/23 16:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 12.7 mg/L 0.40 4 05/12/23 14:49 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 18.4 mg/L 10.0 1 05/11/23 19:00 05/12/23 07:54 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 0.36 mg/L 0.040 1 05/10/23 20:36
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 598 mg/L 25.0 1 05/05/23 13:30 05/06/23 09:54
5220D COD,Soluble Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
COD,Soluble 216 mg/L 25.0 1 05/09/23 00:45 05/09/23 05:00 P4
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284006 Collected: 05/01/23 08:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 114 mg/L 25.0 1 05/03/23 11:47
Volatile Suspended Solids 91.0 mg/L 25.0 1 05/03/23 11:47
5210B BOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
BOD,5 day 79.1 mg/L 2.0 1 05/03/23 07:07 05/08/23 09:14
SM4500P-E,Phosphate,Ortho Analytical Method:SM 4500-P E-2011
Pace Analytical Services-Asheville
Orthophosphate as P 1.6 mg/L 0.50 10 05/03/23 05:46 F6,M1
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284007 Collected: 05/01/23 10:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 286 mg/L 59.5 1 05/03/23 11:47
Volatile Suspended Solids 245 mg/L 59.5 1 05/03/23 11:47
5210B BOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
BOD,5 day 311 mg/L 2.0 1 05/03/23 07:07 05/08/23 09:15
SM4500P-E,Phosphate,Ortho Analytical Method:SM 4500-P E-2011
Pace Analytical Services-Asheville
Orthophosphate as P 5.2 mg/L 1.2 25 05/03/23 05:56 F6
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284008 Collected: 05/01/23 12:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 255 mg/L 51.0 1 05/03/23 11:48
Volatile Suspended Solids 227 mg/L 51.0 1 05/03/23 11:48
5210B BOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
BOD,5 day 420 mg/L 2.0 1 05/03/23 07:07 05/08/23 09:19
SM4500P-E,Phosphate,Ortho Analytical Method:SM 4500-P E-2011
Pace Analytical Services-Asheville
Orthophosphate as P 4.7 mg/L 1.2 25 05/03/23 05:57 F6
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284009 Collected: 05/01/23 14:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 148 mg/L 50.0 1 05/03/23 11:48
Volatile Suspended Solids 132 mg/L 50.0 1 05/03/23 11:48
5210B BOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
BOD,5 day 196 mg/L 2.0 1 05/03/23 07:07 05/08/23 09:22
SM4500P-E,Phosphate,Ortho Analytical Method:SM 4500-P E-2011
Pace Analytical Services-Asheville
Orthophosphate as P 2.1 mg/L 0.50 10 05/03/23 05:54 F6
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
ANALYTICAL RESULTS
Project: WW CITY SEWER
Pace Project No.: 92665284
Sample: CITY SEWER Lab ID: 92665284010 Collected: 05/01/23 16:00 Received: 05/02/23 10:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 168 mg/L 50.0 1 05/03/23 11:49
Volatile Suspended Solids 160 mg/L 50.0 1 05/03/23 11:49
5210B BOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
BOD,5 day 381 mg/L 2.0 1 05/03/23 07:07 05/08/23 09:28
SM4500P-E,Phosphate,Ortho Analytical Method:SM 4500-P E-2011
Pace Analytical Services-Asheville
Orthophosphate as P 2.4 mg/L 0.50 10 05/03/23 05:55 F6
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 772017 Analysis Method: EPA 160.4/SM2540D-2011
QC Batch Method: EPA 160.4/SM2540D-2011 Analysis Description: 2540D TSS/TVSS
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
METHOD BLANK: 4007540 Matrix: Water
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/03/23 11:44
Volatile Suspended Solids mg/L ND 2.5 05/03/23 11:44
LABORATORY CONTROL SAMPLE: 4007541
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 252 238 95 90-110
SAMPLE DUPLICATE: 4007765
92664941002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 14900 20200 30 D6
Volatile Suspended Solids mg/L 10600 14200 29 D6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
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QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 771929 Analysis Method: SM 521 OB-2016
QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD,5 day
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
METHOD BLANK: 4007298 Matrix: Water
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD,5 day mg/L ND 2.0 05/08/23 09:06
LABORATORY CONTROL SAMPLE: 4007300
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
BOD,5 day mg/L 198 192 97 84.6-115
SAMPLE DUPLICATE: 4007301
92665293002 Dup
Parameter Units Result Result RPD Qualifiers
BOD,5 day mg/L 44.5 46.0 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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Asheville,NC 28804
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QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 773738 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284001
METHOD BLANK: 4015943 Matrix: Water
Associated Lab Samples: 92665284001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Ammonia mg/L ND 0.10 05/12/23 12:12
LABORATORY CONTROL SAMPLE: 4015944
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L 5 5.0 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4015945 4015946
MS MSD
92665935001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L 0.42 5 5 5.4 5.4 100 100 90-110 0
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4015947 4015948
MS MSD
92666042009 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L ND 5 5 5.0 5.0 100 100 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 774051 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284002,92665284003,92665284004,92665284005
METHOD BLANK: 4017486 Matrix: Water
Associated Lab Samples: 92665284002,92665284003,92665284004,92665284005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Ammonia mg/L ND 0.10 05/12/23 13:03
LABORATORY CONTROL SAMPLE: 4017487
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L 5 5.1 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4017488 4017489
MS MSD
92665284002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L 24.3 5 5 29.7 29.7 109 108 90-110 0
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4017490 4017491
MS MSD
92665284003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L 16.5 5 5 21.6 21.6 103 103 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 773834 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284001,92665284003
METHOD BLANK: 4016500 Matrix: Water
Associated Lab Samples: 92665284001,92665284003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl,Total mg/L ND 0.50 05/12/23 07:12
LABORATORY CONTROL SAMPLE: 4016501
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Kjeldahl,Total mg/L 10 9.7 97 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4016502 4016503
MS MSD
92666455002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 1.8 10 10 11.7 11.5 99 97 90-110 2
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4016504 4016505
MS MSD
92666455003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 2.6 10 10 12.6 12.6 100 100 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 773835 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284002,92665284004,92665284005
METHOD BLANK: 4016520 Matrix: Water
Associated Lab Samples: 92665284002,92665284004,92665284005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl,Total mg/L ND 0.50 05/12/23 07:52
LABORATORY CONTROL SAMPLE: 4016521
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Kjeldahl,Total mg/L 10 9.3 93 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4017337 4017338
MS MSD
92665970002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 0.53 10 10 10.4 10.5 99 100 90-110 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4017339 4017340
MS MSD
92665970003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 0.93 10 10 11.4 10.7 105 98 90-110 6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 773621 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite,preserved
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
METHOD BLANK: 4015520 Matrix: Water
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0.040 05/10/23 20:03
LABORATORY CONTROL SAMPLE: 4015521
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4015522 4015523
MS MSD
92665754004 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.64 2.5 2.5 3.0 3.0 95 96 90-110 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4015524 4015525
MS MSD
92665754005 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.48 2.5 2.5 2.8 2.8 94 94 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 771950 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus,Ortho
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
METHOD BLANK: 4007370 Matrix: Water
Associated Lab Samples: 92665284006,92665284007,92665284008,92665284009,92665284010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 05/03/23 05:44
LABORATORY CONTROL SAMPLE: 4007371
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Orthophosphate as P mg/L 0.25 0.24 98 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4007372 4007373
MS MSD
92665284006 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Orthophosphate as P mg/L 1.6 0.25 0.25 1.9 1.9 96 112 90-110 2 F6,M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 22 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 772610 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
METHOD BLANK: 4010686 Matrix: Water
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 05/06/23 09:48
LABORATORY CONTROL SAMPLE: 4010687
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 762 102 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4010688 4010689
MS MSD
92664835001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 6430 100 100 6680 6680 257 257 90-110 0 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4010690 4010691
MS MSD
92664935001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 26.9 100 100 132 132 105 105 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA
Project: WW CITY SEWER
Pace Project No.: 92665284
QC Batch: 772797 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD,Soluble
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
METHOD BLANK: 4011852 Matrix: Water
Associated Lab Samples: 92665284001,92665284002,92665284003,92665284004,92665284005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
COD,Soluble mg/L ND 25.0 05/09/23 04:57
LABORATORY CONTROL SAMPLE: 4011853
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
COD,Soluble mg/L 750 774 103 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4011854 4011855
MS MSD
92665284001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
COD,Soluble mg/L 81.6 100 100 188 180 106 99 90-110 4 P4
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4013165 4013166
MS MSD
92665284003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
COD,Soluble mg/L 225 100 100 322 329 97 104 90-110 2 P4
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 24 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALIFIERS
Project: WW CITY SEWER
Pace Project No.: 92665284
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
F6 Sample was not filtered within 15 minutes of collection and does not meet sampling and/or regulatory requirements.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
P4 Sample field preservation does not meet EPA or method recommendations for this analysis.
REPORT OF LABORATORY ANALYSIS
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Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 29
Pace Analytical Services,LLC
leac, yficalAnal 2225 Riverside Dr.
Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WW CITY SEWER
Pace Project No.: 92665284
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92665284006 CITY SEWER EPA 160.4/SM2540D- 772017
2011
92665284007 CITY SEWER EPA 160.4/SM2540D- 772017
2011
92665284008 CITY SEWER EPA 160.4/SM2540D- 772017
2011
92665284009 CITY SEWER EPA 160.4/SM2540D- 772017
2011
92665284010 CITY SEWER EPA 160.4/SM2540D- 772017
2011
92665284006 CITY SEWER SM 5210B-2016 771929 SM 5210B-2016 771963
92665284007 CITY SEWER SM 5210B-2016 771929 SM 5210B-2016 771963
92665284008 CITY SEWER SM 5210B-2016 771929 SM 5210B-2016 771963
92665284009 CITY SEWER SM 5210B-2016 771929 SM 5210B-2016 771963
92665284010 CITY SEWER SM 5210B-2016 771929 SM 5210B-2016 771963
92665284001 CITY SEWER EPA 350.1 Rev 2.0 1993 773738
92665284002 CITY SEWER EPA 350.1 Rev 2.0 1993 774051
92665284003 CITY SEWER EPA 350.1 Rev 2.0 1993 774051
92665284004 CITY SEWER EPA 350.1 Rev 2.0 1993 774051
92665284005 CITY SEWER EPA 350.1 Rev 2.0 1993 774051
92665284001 CITY SEWER EPA 351.2 Rev 2.0 1993 773834 EPA 351.2 Rev 2.0 1993 774029
92665284002 CITY SEWER EPA 351.2 Rev 2.0 1993 773835 EPA 351.2 Rev 2.0 1993 774030
92665284003 CITY SEWER EPA 351.2 Rev 2.0 1993 773834 EPA 351.2 Rev 2.0 1993 774029
92665284004 CITY SEWER EPA 351.2 Rev 2.0 1993 773835 EPA 351.2 Rev 2.0 1993 774030
92665284005 CITY SEWER EPA 351.2 Rev 2.0 1993 773835 EPA 351.2 Rev 2.0 1993 774030
92665284001 CITY SEWER EPA 353.2 Rev 2.0 1993 773621
92665284002 CITY SEWER EPA 353.2 Rev 2.0 1993 773621
92665284003 CITY SEWER EPA 353.2 Rev 2.0 1993 773621
92665284004 CITY SEWER EPA 353.2 Rev 2.0 1993 773621
92665284005 CITY SEWER EPA 353.2 Rev 2.0 1993 773621
92665284006 CITY SEWER SM 4500-P E-2011 771950
92665284007 CITY SEWER SM 4500-P E-2011 771950
92665284008 CITY SEWER SM 4500-P E-2011 771950
92665284009 CITY SEWER SM 4500-P E-2011 771950
92665284010 CITY SEWER SM 4500-P E-2011 771950
92665284001 CITY SEWER SM 5220D-2011 772610 SM 5220D-2011 772842
92665284002 CITY SEWER SM 5220D-2011 772610 SM 5220D-2011 772842
92665284003 CITY SEWER SM 5220D-2011 772610 SM 5220D-2011 772842
92665284004 CITY SEWER SM 5220D-2011 772610 SM 5220D-2011 772842
92665284005 CITY SEWER SM 5220D-2011 772610 SM 5220D-2011 772842
92665284001 CITY SEWER SM 5220D-2011 772797 SM 5220D-2011 773186
92665284002 CITY SEWER SM 5220D-2011 772797 SM 5220D-2011 773186
92665284003 CITY SEWER SM 5220D-2011 772797 SM 5220D-2011 773186
92665284004 CITY SEWER SM 5220D-2011 772797 SM 5220D-2011 773186
92665284005 CITY SEWER SM 5220D-2011 772797 SM 5220D-2011 773186
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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Asheville,NC 28804
www.pacelabs.com (828)254-7176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WW CITY SEWER
Pace Project No.: 92665284
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/12/2023 04:48 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 29
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Page 28 of 29
_DC#j; #1G;_15NV-FR"UN1-0Q83 O;LSample Condition Upon Receipt
.
aC6,
Effe A(ve Datw.11/14/2024 8:18..so.AM
*060 mark top-half Of box If OH and/or dechlorl n.*
--loh siveritled and Project, k## : 92665284
within the-PmeM""1;4. ra qplw preservat lah samp!q$.
Rcepllon;-VOA,0111Wni:TOC,.l7ll- AdGreA%C, DOC, LH9 PM: ASF Due Date- 05/16/23
Bottom half of bowls U 114 number of bottles CLIENT: 93—BRPP
Check aJ1 unpi.e..�mrvo#Nltrates for chlorine
z a
A n M f
�t �V
A z
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Z5 CL Z
D M z
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Z,
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In n
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40 IS
> Ln V1
iD
-
7
V I—
-pH Adjustment Log for Preserved Samples
SOMP!e 10 TVpaqfP(vreFvadvE j;H.uponFecelpt Dglo,preserwatlol preservation kmo �tatp
I adjusted 71 me U reservatvi. I Lmut
adjusted
added
Note, Whenever there Is a d1screpancy affecting North(aroPria cornkande samples,a copy of thls fo rrn will be sew,to the Ncirth Cilro'li. ENR-C. OPIce (:,e,
Out afhold,incorrect presbrvalive,out of. T
Inqot Act cont-aW rs.
Page 29 of 29