NCS000330_ATI Specialty Materials Monitoring_20220217

February 14, 2022
Attn: Central Files
�� 7 zozz
N.C. Division of Water Quality iandENR,oF
1617 Mail Service Center McOresprlleR sect,
Raleigh, NC 27699-1617 se'eloyeE
Central Files:
ATI
P.O. Box 5030
2020 Ashcmft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Attached, please find stormwater monitoring data for ATI Specialty Materials — Monroe Plant
Permit No NCS000330. The originals are included. A copy was also uploaded into the NPDES
Stormwater Individual Permits website. The monitoring data is for the following monitoring
schedule:
Monitoring Events
Sample Number
I Start
I End
Year 4 — Period 1
6
1 January 1st• 2022
1 June 301h 2022
The Zinc benchmark was exceeded but the state has granted relief on zinc.
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
"I certify, under penalty of law, that this document and all attachments were prepared
under my direction or supervision in accordance with a system designed to assure that
qualified personnel properlygather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly
responsible forgathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerel
Mike McManus
EHS Coordinator

AT[ Specialty Materials -Monroe Plant
ATIStormwater Monitoring Report Form
Sample Date&Time: 1/20/22 8:15am Stormwater Discharge Cutfall #2
Sample Location: SW02
Person('s) Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Drainage Area = 272'590sg. Ft. =6.25 acres
Impervious = 36% J�
Tommy Long /James Moser
Pace Analyticals°aoF2
40 CFR Part 136 �P'P
��
�PZ9 P
C O'
Parameter
Results (mg/1)
Benckmark Values (mg/1)
BOD
2.6
30
COD
36.0
120
TSS
16.8
100
Cadmium
ND
0.003
Chromium, total recoverable
0.0327
1
Lead, total recoverable
ND
0.03
Nickel, total recoverable
0.146
0.335
Zinc, total recoverable
0.448
0.126
Oil & Grease
ND
15
H
7.3
6-9 (std units)
Storm Date: 1/20/22 Storm Duration: 4.75 (Hrs.) Inches of Rainfall: 0.40"
Duration of time preceding rain event exceeding 0.1": 85.25 (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total)= Q(Pervious Area)+ Q(Impervious Area)
Q(tot, cfs) = (A x inches rain/12inches/ft. x 6.25 acres x .64)+.9 x inches rain/12inches/ft. x 6.25 x .36)
Q(Total, cfs)=.1333 X 0.40" (inches of rain) +.1688 X 0.40" (inches of rain) = 0.121 cfs

STORM EVENT CHARACTERISTICS:
Date 1 /22/22
Total Event Precipitation (inches): 0.40"
Event Duration (hours): 4.75 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
4547Z4Q lzl -�9u
(Signature of Permittee) (Date)
Form SW U-247, last revised 611212015
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000330 SAMPLES COLLECTED DURING CALENDAR YEAR: 2022
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME AT[ Speicalty Materials
COUNTY Union
PERSON COLLECTING SAMPLE(S)
Q o
PHONE N f704 1289- r 11
CERTIFIED LABORATORY S Pace Analytical
()
Lab # 12
Lab # bOr
�6
Q7
SIGNATURE OF PE ITTEE OR DESIGNEE
d m
O
REOUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
o
No.
I Sample
Collected
01/22/2022
----------
----------
----------
----------
----------
----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Dyes @. no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/fPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m
unit
al/mo
Form S W U-247, last revised 611212015
Page 1 of 2

1C.
Environmental
Quality1 L,
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report s� p2p
For guidance on filling out this form, please visit https://deq.nc.gov/i
npdes-stormwater-gps
Permit No.: N/C/ S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/ / / / / / /
Facility Name:
County: Union
ATI Specialty Materials - Monroe
inspector: Tommy Long
Date of Inspection: 1 /20/22
Time of Inspection: 10:35 am
Total Event Precipitation (inches): 0.40"
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 01 Structure (pipe, ditch, etc.): Pipe
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Metal Storage
Page I of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
light gray
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1' 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ? 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 V 3 4 5
Is there any foam in the stormwater discharge? O Yes M No.
Is there an oil sheen in the stormwater discharge? OYes M No.
Is there evidence of erosion or deposition at the outfall? o Yes 6 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242, Last modified Of/01 /201 S

NCO
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-t04 s/ r3
npdes-stormwater-gps °0,o1
Permit No.: N/C/ S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/
Facility Name: ATI Specialty Materials - Monroe
County: Union Phone No. 704-289-4511
Inspector: James Moser
Date of Inspection: 1-20-22
Time of Inspection: 9:30am
Total Event Precipitation (inches): 0.40"
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 02 Structure (pipe, ditch, etc.): Pipe
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Metal Storage
Page 1 of 2
S W U-242, Last modified 06/012018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
very light gray
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1' 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge; where I is no solids and 5 is extremely muddy:
7.
8.
9.
1 2 3 4 5
Is there any foam in the stormwater discharge? 0 Yes ■ No.
Is there an oil sheen in the stormwater discharge? 0Yes ■ No.
Is there evidence of erosion or deposition at the outfall? 0 Yes 0 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified O601/2018

NIC.
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-re"�)1m�
npdes-stormwater-gps 'd 4
Permit No.: N/C/
Facility Name: .
county: Union
Inspector: Toirll
S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/
AT[ Soecialtv Materials - Monroe
Date of Inspection: 1 /20/22
Time of Inspection: 10:50am
Total Event Precipitation (inches): 0.40"
No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Reeional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 03 Structure (pipe, ditch, etc.): Pipe/Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Metal Storage, Hammer Repair Dust Collection
Page 1 of 2
SWU-242, Last modified 06/01/201 S

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1' 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
Y 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 # 3 4 5
Is there any foam in the stormwater discharge? O Yes M No.
Is there an oil sheen in the stormwater discharge? QYes r No.
Is there evidence of erosion or deposition at the outfall? O Yes M No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
none
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 0601/2018

KIC
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit
npdes-stomiwater-gps
Permit No.: N/C/ S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/ / / / / / /
Facility Name: AT[
County: Union
Inspector: Tommy Long
Date of Inspection: 1 /20/22
Time of Inspection: 11:10 am
Materials - Monroe
Total Event Precipitation (inches): 0.40"
No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Reeional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee
1. Outfall Description:
Outfall No. 04 Structure (pipe, ditch, etc.): Pipe/Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Shipping Staging, Turnings Storage, Truck Loading
Page I of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
medium brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 0 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 V 3 4 5
Is there any foam in the stormwater discharge? 4 Yes MNo.
Is there an oil sheen in the stormwater discharge? QYes MNo.
Is there evidence of erosion or deposition at the outfall? 0 Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Erosion present at outfa-11 P.O. has been issued to contractor to install rip -rap
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified OfJ0112018

Environmental R�
Quality
Stormwater Discharge Outfall (SDO) o� fi��
Qualitative Monitoring Report °
oLp2,p � /G
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resole Q
npdes-stonnwater-gps
Permit No.: N/C/ S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/
Facility Name: ATI Specialty Materials- Monroe
County: Union Phone No. 704-289-4511
Inspector: Tommy Long
Date of Inspection: 1 /20/22
Time of Inspection: 10:15 am
Total Event Precipitation (inches): 0.40"
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee
1. Outfatl Description:
Outfall No. 05 Structure (pipe, ditch, etc.): Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Metal Storage, Clean Empty Drums, Equipment Storage, Roll Off Containers
Page I oft
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
very light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 V 3 4 5
Is there any foam in the stormwater discharge? Q Yes M No.
Is there an oil sheen in the stormwater discharge? 9Yes ■ No.
Is there evidence of erosion or deposition at the outfall? 0 Yes ■ No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 0601/2018

Kra
Environmental
Qualify
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
m�0�2 t q2b Q
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-rd*.* S/
npdes-stormwater-gps oo�
Permit No.: N/C/ S/0/0/0/3/3/0 or Certificate of Coverage No.: N/C/G/
Facility Name: ATI Specialty Materials - Monroe
county: Union Phone No. 704-289-4511
Inspector: Tommy Long
Date of Inspection: 1 /20/22
Time of Inspection: 11:35arn
Total Event Precipitation (inches): 0.40"
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the petmittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 06 Structure (pipe, ditch, etc.): Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area:
Trash Compactor, Metal Storage, Parking Lot
Page I of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
medium gray
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ? 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 V 3 4 5
Is there any foam in the stormwater discharge? 0 Yes ■ No.
Is there an oil sheen in the stormwater discharge? DYes M No.
Is there evidence of erosion or deposition at the outfall? 0 Yes 0 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, on sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified O001/2018

aceAnalytical
anm.pacalabs.com
January 27, 2022
Mr. Larry Allen
Allvac
RE: Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Dear Mr. Allen:
Pace Analytical Services, LLC
9800 kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 20, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: David Ethridge
Mr. Tommy Long, Allvac
Mike McManus, ATI Specialty Metals
Rick Moore, An Specialty Materials
James Moser
David Pope, Allvac
td4Z•1Z4 aA_1101;7_-yl•1X7_1:/_1W&96I
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, U.C.
Page 1 of 19

aceArralytical
f www.pacelabs.com
I
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification It 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 19

aceAnaiyticaf
www pacelabLCOM
SAMPLE ANALYTE COUNT
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92583541001
MONROE SW02 TSS
SM 254OD-2015
MAB2
1
PASI-A
92583541002
MONROE SW02 BOD
SM 521OB-2016
NFW
1
PASI-A
92583541003
MONROE SW02 COD
SM 5220D-2011
JP1
1
PASI-A
92583541004
MONROE SW02 O+G
EPA 1664B
ICO
1
PASI-C
EPA 1664B
ICO
1
PASI-C
92583541005
MONROE SW02 METALS
EPA 200.7 Rev 4.41994
CBV
5
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalytical
f www.pacelabs.com
ANALYTICAL RESULTS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MONROE SW02 TSS Lab iD: 92583541001 Collected: 01/20/22 09:50 Received: 01/20/22 11:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Performed by
Collected By
Collected Date
Collected Time
pH
Temperature
2540D Total Suspended Solids
Total Suspended Solids
Date: 01/27/2022 04:58 PM
Analytical Method:
Pace Analytical Services - Charlotte
ATI SM
1
01/20/22 09:59
TL
1
01/20/22 09:59
01/20/22
1
01/20/22 09:59
09:48
1
01/20/22 09:59
7.3 Std. Units
1
01/20/22 09:59
11.9 deg C
1
01/20/22 09:59
Analytical Method: SM 254OD-2015
Pace Analytical Services -Asheville
16.8 mg/L
5.0 1
01/24/2210:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

aceArtalytical
www.pacelabs com
ANALYTICAL RESULTS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MONROE SW02 BOD Lab ID: 92583541002 Collected: 01/20/22 09:52 Received: 01/20/22 11:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day Analytical Method: SM 521OB-2016
Pace Analytical Services -Asheville
BOD, 5 day 2.6 mg/L 2.0 1 01/21/22 06:25 01/26/22 06:02 132, B3
Date: 01/27/2022 04:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

aceArfalytlCal
rrwra PUSIOLCOm
ANALYTICAL RESULTS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MONROE SW02 COD Lab ID: 92583541003 Collected: 01/20/22 09:53 Received: 01/20/22 11:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand 36.0 mg/L 25.0 1 01/27/22 02:10 01/27/22 05:31
Date: 01/27/2022 04:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aceAnalyticalC'
www.pacelabs.com
ANALYTICAL RESULTS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: MONROE SW02 O+G Lab ID: 92583541004 Collected: 01/20/22 09:55 Received: 01/20/22 11:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
HEM, Oil and Grease Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease ND mg/L 5.0 1 01/21/22 09:11
1664 SGT HEM, TPH Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons ND mg/L 5.0 1 01/21/22 09:11
Date: 01/27/2022 04:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
Page 7 of 19

aceAna1j4ica1
t www.pacelab&ccm
ANALYTICAL RESULTS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MONROE SW02 METALS Lab ID: 92583541005 Collected: 01/20/22 09:57 Received: 01/20/22 11:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.41994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Cadmium
ND ug/L 1.0
1
01/21/22 11:52
01/24/22 20:54 7440-43-9
Chromium
32.7 ug/L 5.0
1
01/21/22 11:52
01/24/22 20:54 7440-47-3
Lead
ND ug/L 5.0
1
01/21/22 11:52
01/24/22 20:54 7439-92-1
Nickel
146 ug/L 5.0
1
01/21/22 11:52
01/24/22 20:54 7440-02-0
Zinc
448 ug/L 10.0
1
01/21/22 11:52
01/24/22 20:54 7440-66-6
Date: 01/27/2022 04:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 19

lance aljdical
www.pacelabs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 672895
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and Grease
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92583541004
METHOD BLANK: 3522301
Matrix: Water
Associated Lab Samples: 92583541004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
ND 5.0 01/21/22 09:11
LABORATORY CONTROL SAMPLE:
3522302
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mg/L
40 37.3
93 78-114
MATRIX SPIKE SAMPLE:
3522303
92583541004 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg/L
ND 39.6
33.6 82 78-114
SAMPLE DUPLICATE: 3522304
92583186002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Oil and Grease
mg/L
ND 1.81
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19

ID
aceAnalytCal
www.pacelabs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
QC Batch: 672897 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92583541004
METHOD BLANK: 3522312 Matrix: Water
Associated Lab Samples: 92583541004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 01/21/22 09:11
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
3522313
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 16.5 82
64-132
MATRIX SPIKE SAMPLE:
3522314
92583541004 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 19.8 15.0
72
64-132
SAMPLE DUPLICATE: 3522315
92583536002 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 19

acpAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 673044
Analysis Method:
EPA 200.7 Rev 4.41994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92583541005
METHOD BLANK: 3522907
Matrix: Water
Associated Lab Samples: 92583541005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
01/24/22 20:05
Chromium
ug/L
ND
5.0
01/24/22 20:05
Lead
ug/L
ND
5.0
01/24/22 20:05
Nickel
ug/L
ND
5.0
01/24/22 20:05
Zinc
ug/L
ND
10.0
01/24/22 20:05
LABORATORY CONTROL SAMPLE:
3522908
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Cadmium
ug/L
500
470
94 85-115
Chromium
ug/L
500
482
96 85-115
Lead
ug/L
500
476
95 85-115
Nickel
ug/L
500
470
94 85-115
Zinc
ug/L
500
464
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3522909
3522910
MS
MSD
92583252001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
319
473 64 95
70-130
39 M1,R1
Chromium
ug/L
ND
500
500
334
487 66 97
70-130
37 M1,R1
Lead
ug/L
19.1
500
500
336
489 63 94
70-130
37 M1,R1
Nickel
ug/L
ND
500
500
318
470 63 94
70-130
39 M1,R1
Zinc
ug/L
23.1
500
500
339
490 63 93
70-130
36 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3522911
3522912
MS
MSD
92583707001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
476
465 95 93
70-130
2
Chromium
ug/L
ND
500
500
494
481 98 96
70-130
3
Lead
ug/L
ND
500
500
477
466 95 92
70-130
2
Nickel
ug/L
13.8
500
500
484
472 94 92
70-130
3
Zinc
ug/L
731
500
500
1230
1200 99 93
70-130
3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

1�
15a
www.pacelabs.com
j,
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 673309
Analysis Method: SM 254OD-2015
QC Batch Method: SM 2540D-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92583541001
METHOD BLANK: 3524348
Matrix: Water
Associated Lab Samples: 92583541001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 01/24/22 10:28
LABORATORY CONTROL SAMPLE: 3524349
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 234 94 90-110
SAMPLE DUPLICATE: 3524641
92583541001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
16.8 17.8 6
SAMPLE DUPLICATE: 3524642
92583674001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
45.0 44.0 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

5ac
1�
uMnalytical
wm.pacelabs.com
I
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 672981
Analysis Method:
SM 521OB-2016
QC Batch Method: SM 521OB-2016
Analysis Description:
5210B BOD, 5 day
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92583541002
METHOD BLANK: 3522786
Matrix: Water
Associated Lab Samples: 92583541002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 01/26/22 02:45 B3
LABORATORY CONTROL SAMPLE: 3522788
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 210
106 84.6-115 B3
SAMPLE DUPLICATE: 3522789
92583677001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
776
812 5 B3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 674143
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92583541003
METHOD BLANK: 3528521
Matrix: Water
Associated Lab Samples: 92583541003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
01/27/22 05:28
LABORATORY CONTROL SAMPLE: 3528522
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 760
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3528523 3528524
MS MSD
92583514001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 125
100 100 223
226 98 101
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3528525 3528526
MS MSD
92583514002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 106
100 100 209
212 103 105
90-110 1
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 19

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
www pacelabs.com
[phone]
QUALIFIERS
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2022 04:58 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 19

aceAnalXical
WWW.pacelab&C0M
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MONROE STORMWATER SW02
Pace Project No.: 92583541
Lab ID
Sample ID
92583541001
MONROE
SW02 TSS
92583541004
MONROE
SW02
O+G
92583541004
MONROE
SW02
O+G
92583541005
MONROE
SW02
METALS
92583541001
MONROE
SW02
TSS
92583541002
MONROE
SW02
BOD
92583541003
MONROE
SW02
COD
Date: 01/27/2022 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA1664B
672895
EPA 1664B
672897
EPA 200.7 Rev 4.41994
673044
SM 2540D-2015
673309
SM 521OB-2016
672981
SM 5220D-2011
674143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994 673119
SM 521OB-2016 672996
SM 5220D-2011 674165
Page 16 of 19

aceAoalyllsala
Document Name:
Sample Condition Upon Receipt SCUR
0ocumen[ Revised: November 15, 2021
Page I of 2
Document No.:
F{AR-CS-033-Rev.08
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Ashevllle M IF en[I—lGreenwood Huntersville [ - RaleighQ-- Mechanicivlilea—AHantaB--Kernersville(D-----
• Client Name:
A- - A f I/cv PrD'e" W®I* 0 92583541
❑Courier: Fed Ex OUPS ❑LISPS t4CIient 'I'II"III II'III IIIIII
Commercial []Pace Mother:_
Custody Seal Present? []Yes (z3No Sealslntact? []Yes ONO 925831541
Dale/Inkfals Person Examining Contents:7(-1- -77C
Packing Material: RBubbie wrap ®Bubble Bags ❑None ❑ - Other Biological Tissue Frozen?
Thermometer: Dyes ❑No ❑N/A
®IR Dun to: QQT?bY Tyof ice: Qwet []Blue []None
pe
Correction Factor:
Cooler Temp: 2. Add/Subtract (°C) 0.0
Temp should be above freezing to 6°C
❑Samples out or temp criteria. Samples on ice, cooling process
rim vcauu
USDA Regulated Soll (N N/A, water samplel
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples atiginate from a foreign source (internationally, ri
flyes INa nrludin°Haaaall andnuannelrnl) r-1vae r—IM..
Comments Discrepancy:
Chain of Custody Present?
jffyes
QNO
N A
1.
Samples Arrived within Hold Time?
Des
No
N/A
2.
Short Hold Time Analysis 102 hr.)?
SlYes
No
N/A
3.
Rush Turn Around Time Requested?
yes
No
0 N/A
4.
Suff clent Volume?
BYES
NO
O N/A
S.
Correct Containers Used?
-Pace Containers Used?
Ye5
Yes
❑No
01,10
❑N/A
N/A
6.
Containers Intact?
ZVes
Otto
N/A
7.
Dissolved analysis: Samples Field Filtered?
ElVes
ONO
N/A
B.
Sample Labels Match COC?
•InGudes Date me/ID/Ana Is Matrlk:
14Yes
[]No
❑NIA
9.
Heads acein VOAVhIs >5.6mm1?
Over
No
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Des
[]Yes
ONO
ONO
❑N/A
NIA
It.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Field Data Required? ❑Ye5 []No
Page 17 of 19

Document Name:
document Revised: November 15, 2021
a
fl%al
Sample Condition Upon Receipt (SOUR)
Page 2 of 2
Document Nb.:
Issuing Authority:
aCeAga1j ..
F-CAR•CS•033•Rou.08
Pace Carolinas Quality Office
'Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance ranee for preservation
samples.
Exceptions: VOA, Conform, TOC, Oil and Grease, ORO/8015 (water) ROC, Wig
"Bottom half of box is to list number of bottles
Project
WN :'9 1
PM: Mt+l6 Due Dater 01 /31/22
CLIENT: 92—Allvae NC
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pH Adjustment Log for Preserved Samples
Sampia 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of preservative
added
Lot p
note: whenever there is a discrepancy anecung Nortn carmina compuance samples, a copy or rnvs corm ww oe sent to the North caroana of rtNK certification 0111ce (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 18 of 19

ATI Specialty Materials *ATI
. ...................... _. Specialty Materials
Monroe
Chain of Custody Record
Project Name/Number: Mon oe Stormwater SW02
Project Location: Monroe/Ashcraft Facility
Sampler(s) Signature: �-
awll-
Date:
CL
M
r^
V
M
�
L.
�-
�,
a,
w
�;
Requested
M
,E
�
IL
O
Parameters
-(�
G/(0
None
Y
TSS
'
-
rr
G
None
Y
BOD
G,}
H2SO4
Y
COD
Mij ' �,1
Q--
l a'1
G P
HCL
Y
Oil & Grease Non -Polar oil & Grease by
o (,A��
r
/ r
EPA Method 1664 SGT-HEM
air►COMM,
Chromium, Lead,
OonroC,,�u)
�'�
G
HNO3
Y
Nickel. i
Benchmarks
TSS
100 mg/L
BOD
30 mg/L
COD
120 mg/L
OIL & Grease
15 mg/L
Cadmium
0.003 mg/L
Chromium
0.905 mg/L
Nickel
0.33S mg/L
Lead
0.03 mg/L
Zinc
0.126 mg/L
Onsite Field Analysis
Onsite Field Temperature Analysis
pH: Sample Time: IA
Temp:OC Sample Time:_2.,Y.5.4.
Analysis Time: `
Analysis Time: r '-
Sampling and Field Analysis completed by:
Relinquished by:
Received by:,Z 11, &�L ! V�
Date: /• as - Time: ll ; -VD l4 41
Date: 1 / IQ/Z Time:I�cl_
EHS-ENV-SW-COC Rev.001
Page 19 of 19