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HomeMy WebLinkAboutNCS000183_MONITORING INFO_20200922STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. N CSDDD 113' DOC TYPE ❑ FINAL PERMIT X MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ 202D09 22 YYYYMMDD Chemical Solutions o division of Radiator Specialty Company Septo'inber 12, 2018 Central Files North Carolina Department of lnvironment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Report Radiator Specialty Company Radiator Road, Indian Trail, North Carolina NPI)ES Permit No. NCS000183 Dear Sirs: CENjRPt FILES U\PJR S— - Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge OUtfall Monitoring Report for monitoring period Year 9 — Period 2 as required by Part III Section E.(l.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If' you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company G. Stuart A. Kerkhoff. CH Y*1 Environmental Health and Safety Manager Attachments SI01WAI RIPD2-201 RCV1- I.DOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscbrands.com STORMWATER DISCHARGE OUTFALL (SDO) . MONITORING REPORT Permit Number NCS NCS000183 FACILITY NANIE Radiator Specialh•Company PERSON COLLECTING SAMPLE(S) Stuart Kcrkhoff CERTIFIED LABORAToRY(S)_Pacc Anal)-lical Services, LLC_La1) 9_12 Lab # Part A: Specific N'lonitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) n COUNTY Union PHONE 'O.L704��684-I815 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall Date 50050 Total No. Sample Collected Total Flow (if app.) Total Rainfall Suspended .Solids Oil and Grease - TPH DRO - - TPH GRO H nto/dd/vr MG inches m-1/L - m /L - ni /L m /L -Units 003 4/23/18 NA 1.87 <100 <30 <0.50 <0.08 7.48 (101 4/23/18 NA 1.87 <100 <30 <0,50 <0.08 7.47 002 4/24/18 NA 1.87 <100 <30 <0.50 <0.08 7.25 (I(14 4/24/18 NA 1.87 <100 <30 <0.50 <0.08 6.59 Docs this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X_no (if ves. complete Part f3) Part 13: Vehicle Maintenance Activitv Monitoring Reouirentents Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage nto/ddhvr MG inches m /1 nt /1 unit -,al/mo Form SWU-247. last revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date 4/23/18_-4/24/18 Total Event Precipitation (inches): _I.87 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluade the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief', true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." (Signature of Permittec) 9 oJ ( Date) Form S W U-247. lust revised 21212012 Pare 2 of 2 / /PaceAnalytical vwn pscela65.con, Pace Analytical Services, LLC 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 May 01, 2018 Stuart Kerkhoff Radiator Specialty Company 600 Radiator Road Indian Trail, NC 28079 RE: Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 f�% r _, L, MAl' - 1 'U, Dear Stuart Kerkhoff: Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Q_, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. L-C. Page 1 of 18 ��e Analytical wmvpecela0.t.rom i I Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 Charlotte Certification IDs Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LAI70028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification It E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC, Page 2 of 18 1�eAnalytical ~pacelabsrom i i Project: STORMWATER YR9, PD2 Pace Project No.: 92-182049 Lab ID Sample ID 92382049001 003 Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664E JMS 1 PASI-C EPA 8015 Modified NU7 2 PASI-C EPA 5030/8015 Mod. CAH 2 PASI-C SM 2540D MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 /71aceAnalytical vmwpacclabs,ccrn I 411 V1It"iI_1:4'L161a61Zk1xH1Eel Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, 128078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92382049001 003 SM 2540D Total Suspended Solids 24A mg/L 5.0 04/30/18 14:53 D6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in lull, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 ��PaceAnalyticaI / wwwpacelaDs.com r Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWATER YR9, P02 Pace Project No.: 93382049 Method: EPA 1664E Description: 1664 SGT-HEM, TPH Client: Radiator Specialty Company Date: May 01, 2018 General Information: 1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria,were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and rcletivo percent differences (RPD3) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall nor be reproduced, except in full, without the written consent of Pace Analytical Services. LLC. Page 5 of 18 /7PaceAnalytical s / w pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 I,:101xH2\Ia1G1CL•�9),94 Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 Method: EPA 8015 Modified Description: 8015 Diesel Low Volume Client: Radiator Specialty Company Date: May 01. 2018 General Information: 1 sample was analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3511 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. QC Batch: 408280 S0: Surrogate recovery outside laboratory control limits. LCS (Lab ID: 2265401) • n-Pentacosane (S) S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. • BLANK (Lab ID: 2265400) • n-Pentacosane (S) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 /�ace Analytical mvw pacelabs.wm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWtATER YR9, PD2 Pace Project No.: 92382049 Method: EPA 5030/8015 Mod. Description: Gasoline Range Organics Client: Radiator Specialty Company Date: May 01, 2018 General Information: 1 sample was analyzed for EPA 5030/8015 Mod.. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within OC limits with any exceptions noted below. Method Blank: All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 18 171aceAnalytical I vmwpavelabs.con, 1 i PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: 408412 D6: The precision between the sample and sample duplicate exceeded laboratory control limits. DUP (Lab ID: 2266119) • Total Suspended Solids CUP (Lab ID: 2266120) • Total Suspended Solids Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 18 1JeAnapical s l vmwpacelabs corn i Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersvilte, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER YR9, PD2 Pace Project No.: 92332049 Sample: 003 Lab ID: 92382049001 Collected: 04/23/18 11:25 Received: 04/24/18 12:05 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons NO mg/L 5.0 1 04/25/18 05:21 8015 Diesel Low Volume Analytical Method: EPA 8015 Modified Preparation Method: EPA 3511 Diesel Range Organics(C10-C28) NO mg/L 0.50 1 04/27/18 13:13 04/28/18 00:20 Surrogates n-Pentacosane (S) 125 % 70-130 1 04/27/18 13:13 04/28/18 00:20 629-99-2 Gasoline Range Organics Analytical Method. EPA 5030/8015 Mod. Gas Range Organics (C6-C10) NO mg/L 0.080 1 04/26/18 19:42 Surrogates 4-Bromofluorobenzene (S) 115 % 70-145 1 04/26/18 19:42 460-00-4 2540D Total Suspended Solids Analytical Method. SM 2540D Total Suspended Solids 24.4 mglL 5.0 1 04/30/18 14:53 D6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 05/01/2018 01:27 AM without the written consent of Pace Analytical Services, LLC Page 9 o1 18 /71aceAnalyficalo w»wparxi cone i Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 QC Batch: 407775 QC Batch Method: EPA 1664B Associated Lab Samples: 92382049001 METHOD BLANK: 2262543 Associated Lab Samples: 92382049001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2262544 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 04/25/18 05:06 Spike LCS LCS % Rec Cone. Result e/ Rec Limits Qualifiers 19.2 19.5 102 64-132 MATRIX SPIKE SAMPLE: 2262545 35387367001 Spike MS MS % Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.10U 19.2 19.4 101 64-132 Results preserved on this page are in the units indicated by the -Units" column ecept where ariait create unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/01/2018 01.27 AM without the willed consent of Pace Analytical Services. I.I.C. Page 10 of 18 17PaceAnalytical L wwwpacelaos.mm i QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 QC Batch: 407825 Analysis Method: EPA 5030/8015 Mod. QC Batch Method: EPA 5030/8015 Mod. Analysis Description: Gasoline Range Organics Associated Lab Samples: 92382049001 METHOD BLANK: 2262719 Matrix: Water Associated Lab Samples: 92382049001 Blank Reporting Parameter Units Result Limit Analyzed Gas Range Organics (C6-C10) mg/L NO 0.080 04/25/18 14:26 4-Bromofluorobenzene (S) % 113 70-145 04/25/18 14:26 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2262720 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/L 1 1.0 100 70-150 4-Bromofluorobenzene (S) e/ 115 70-145 MATRIX SPIKE SAMPLE: 2262721 92382047001 Spike MS MS % Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/L ND 1 0.91 90 70-150 4-Bromofluorobenzene (S) e/ 119 70-145 SAMPLE DUPLICATE: 2262722 Parameter Gas Range Organics (C6-C10) 4-Bromofluorobenzene (S) 92382048001 Dup Units Result Result mg/L NO ND p/ 118 118 RPD Qualifiers El Results presented on this page are in the umh, indicated by the "Units' column except where an alternate unit is presented to the right o1 the result. REPORT OF LABORATORY ANALYSIS This report snarl not be reproduced, except in full. Dale: 05/01/2018 01:27 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 1�laceAnalytical9 bxm.pacel365.mm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 QC Batch: 408280 Analysis Method: EPA 8015 Modified QC Batch Method: EPA 3511 Analysis Description: 8015 Diesel Low Volume Associated Lab Samples: 92382049001 METHOD BLANK: 2265400 Matrix: Water Associated Lab Samples: 92382049001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diesel Range Organics(C70-C28) mg/L NO 0,50 04/27/18 22:48 n-Pentacosane (S) % 139 70-130 04/27/18 22:48 S3 LABORATORY CONTROL SAMPLE: 2265401 Spike LCS 1-CS % Rec Parameter Units Cone. Result e/ Rec Limits Qualifiers Diesel Range Organics(C10-C28) mg/L 10 10 100 70-130 n-Pentacosane(S) % 135 70-130 SO Results presented on this page are in the units inuiceted by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale. 05/01/2018 01:27 AM without the written consent of Pace Analytical Services. LLC, Page 12 of 18 l aceAnalyticaI wwwpacelabs.cont i QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 923-32049 QC Batch: 408412 Analysis Method: SM 2540D QC Batch Method. SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382049001 METHOD BLANK: 2266117 Matrix: Water Associated Lab Samples: 92382049001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/18 14:53 LABORATORY CONTROL SAMPLE: 2266118 Spike 1-CS LCS e/ Red Parameter Units Cone. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 2266119 92382049001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 24.4 43.2 56 D6 SAMPLE DUPLICATE: 2266120 92382121001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 38.3 44.0 14 D6 Results presented on this page are in the units indicated by the "Units' column except where an from ate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, Date: 05/01/2018 01:27 AM without the written consent of Pace Analytical Services, LLC Page 13 of 18 /71aceAnalytical wxwascelatxs.mrrr Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOIL -Adjusted Method Detection Limit. POL - Practical Ouantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCSQ) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. - N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. SO Surrogate recovery outside laboratory control limits. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/01/2018 01:27 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 117PaceAnalytical .pacebbscon i I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER YR9, PD2 Pace Project No.: 92382049 Lab ID Sample ID QC Batch Method QC Batch 92382049001 003 EPA 1664B 407775 92382049001 003 EPA 3511 408280 92382049001 003 EPA 5030/8015 Mod. 407825 92382049001 003 SM 2540D 408412 Date: 05/01 /2018 01:27 AM REPORT OF LABORATORY ANALYSIS This report shall not oe reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite I o0 Huntersville. NC 28078 (704)875-9092 Analytical Method EPA 8015 Modified Analytical Batch 408291 Page 15 of 18 Document Name: Document Revised: February 7, 2018 2CBA�8(yllCd�Y Sample Condition Upon Recelpt(SCUR) Page 3 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Ralelgh❑ Mechanicsvllle❑ Q y V^ Client Name: (� 3,Qe2r®�«4'9. /? Projec I�lO#c# 9� IIY+ j Coutler: ❑Fed Ex ❑UPS . ❑USPS❑Client ❑ Commercial Space ❑Qther._ - 92382049,' Custody Seal Present? ❑� Yes 0. Sealsintact? []Yes QNo Date/Initials Person ExaminingContents/�� Packing Material: ❑Bubble Wrap Ql�ubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes []NO /A ❑tRGun10: 92TO36 Type of ice: Bmt ❑Blue Drone Cooler Temp ('C): Li ( Correction Factor: Add/Subtract (•0) }Q. j �, Temp should be above freezing to 6'C Cooler Temp Corrected (•C): ❑Samples out of temp criteria. Samples on Ice, cooling process has begun USDA Regulated Soil (Q-t1<water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source )internationally, nYes (1N0 ...." 17-1 . n.,_ Cum ments/Dts crepa nay: Chain of Custody Present? es ONO ❑N/A 1. Samples Arrived within Hold Time? es Quo N/A 2. Short Hold Time Analysis (<72 hr.)? Oyes ghff- ❑N/A 3. Rush Turn Around Time Requested? Oyes 9a-o— ❑N/A d. Sufficient Volume? I❑*� ONO ❑N/A S. Correct Containers Used? -Pace Containers Used? 2M QYtr ONO ONO ❑N/A ❑N/A 6. - Containers Intact? s ONO N/A 7. Dissolved analysis: Samples Field Filtered? Oyes E3rJo ❑N/A B. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Oyes ONO ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes ONO N/A 10. Trip Blank Present? Trip Blank Custody Se a Is Presen t? Oyes ❑YCS ONO ONO pN/A ❑N/A it. _ - COMMENTS/SAMPLE 015CREPANCY Field Date Rectulred? Dyes ONO Lot ID of split containers: CIIENT NOTIFICATION/pE50LUTION Person Contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Page 16 of 18 Document Name: Document Revised: February 7, 2016 3Ce/I nalyliLdl - Sample Condition Upon Recetpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA,Loliform, TOC, Oil and Grease, DRO/8015 (svaterl DOC, LLHg "Bottom half of box Is to list number of bottle Proje' W0#-,923:820;4.9 PM.;; KLHli,' , 'D'ue' Dace: 03%014.18 CLIENT: 92'R9C ijK a y y Z n 7 N E u as Z �en > IS E i 0 Z > V .N a E 7 el = u J V _ y J m' N O _ n E IA m N o i - n n E Z m Z " a Z Y m a E N m N x Z A a E V of m 9 y L 5 E v` LL 3 Z a c J a a m J a — u a ¢ a U U D y E < E M ¢ ry 9 o a E a y N a v $ u a ¢ E a U E E o ruj I m i 2 a O E P a z No n Z ¢ p E a1 > Z n J < 0 E P > a v 06 x a O E OI o a o Y a u s n n y > p z w N E ~ ~ vs I Z m ar ,n E f 'm P o i A n E o Q ,r{ as ¢ 9 2 c a E ¢ E S O ¢ ¢ z e e = ,G N o J ¢ 9 2 v w E ¢ E m 1 2 3 a s 6 7 8 9 10 11 12 PH Adjustment Log for Preserved Samples Sample to Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot Note- Wh^^aveahetP_Iga,d$¢epanCy.affprtla NpQh.Cd[PIIed.GPfPP6ance 5dmP7CS,aCPpY-nLINS12rD rvIII Q;sent tot e o a n�^�i"'�^""""•""" Out of hold, incorrect Oreservative, out of temp, incorrect containers. Page 17 of 18 v�! Face Analytical x rr.pacela Eitom Section A Required Chew Inlonnation' n rl OrC55: L' i micas Email To'.SI I I Pnon¢ Far: Roglleslptl Uup UTruffAT: l t: section B Required Pmjdct Information: Repart To: i MY CHAIN -OF -CUSTODY / Analytical Request Document The Chair OGCustody is a LEGAL DOCUMENT. All relevmtt fields musl be completed accurately. -L I,,, FF Lt Section C Invoice Info Ouclion o mmria codes Requlrod OlmonnPonnnanp MnrRlx r�1p� DnnLing wafer Dw wale, wr a O COLLECTED z waste wrier Ww C-110SITE conmeSrtE Produr:: P - Q START f.NnGFnp SoiGSolitl St SAMPLE ID Oil OL K yVj o wP (A-Z.U-9 r. 1 - U Kwrpe Air AF: Sample IDS MUST BE UNIQUE Tissue p a o. W TS Other OT U M A Z S ¢ a W O r DATE TIME GATE TIME �_ a a ADDITIONAL COMMENTS DATE I TII ORIt,,')DL SAMPLER NAME AND SIGNATURE PRINT Nnmp of SAMPLER: S SIGNATURE of SAMPLER: 'Lnpnn:nn Nulr.: 9v �irinrng II . ro n Ypu:nc:¢[apiing nacc -::Er N a:.. I.:.Yin .nl .....�.: ann ngrt'prn9 Ip Iplo [pa If., ql I's, pet monln for arty it CO _m W m Pagp: � of I a ,,,on A Name: I '•,CI :c'. iv.— S•rL7A/1 2 U a'' a� REGULATORY AGENCY. '�IdPDES GROUND WATER DRINKING WATER UST RCRA OTHER Duow porn: Pro,_, 9or. ( Vr: IM..t vrpwe a: Site Location STATE: A / !. Requested Analysis Filtered (YIN) Preservatives z r N 0 IdQ to y N' I C7V� z c m Pace Project No./ Lab I.D. i le s- R A CEPTED BY I AF nWr UATION DATE TIME SAMPLE CONDITIONS L , ;Ysf'r rlC�r` q,)q aw.—f e�lch•�(' I� DATE Slgnpd .G (MMlDD/YYI: II. TAU V oI,� -- e _ '3 ~ V v "— F-ALL,Q-020rev.0T. 15-ma,-9nn7 aceAnalytical w oacefshs.cam Pace Analytical Services, LLC 9800 Kincery Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 May 01, 2018 el L Stuart Kerkhoff I Radiator Specialty Company f L L JU11i nEC D 600 Radiator Road f 1 Indian Trail, NC 28079 j By RE: Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 Dear Stuart Kerkhoff: Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNl/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 1 � aceAnalj6cal f wwwpavelabs.min f Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntefsville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 [fla[ i9WWIN INl11K South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services. LLC, Page 2 of 18 aceAnalyticala wxwpacelabs. com I Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: STORMWATER YR9, PD2 92382051 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92382051001 001 EPA 166413 JMS 1 PASI-C EPA 8015 Modified NUT 2 PASI-C EPA 503018015 Mod. CAH 2 PASI-C SM 2540D MDW i PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 1�aceAnalytical mrwpacela6s.cam i Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville. NC 28078 (704)875-9092 SUMMARY OF DETECTION Project: STORMWATER YR9, PD2 Pace Project 1 92382051 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92382051001 001 SM 2540D Total Suspended Solids 2.6 mg/L 2.5 04/30/18 14:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Li Page 4 of 18 17PaceAnapical e I wwwpacclabs.com ' I PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 9,1382051 Method:EPA 1664E Description: 1664 SGT-HEM, TPH Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. M Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC Page 5 of 18 a 1�7aceAnalytical vmwpacelabs. rom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 Method: EPA 8015 Modified Description: 8015 Diesel Low Volume Client: Radiator Specialty Company Date: May 01, 2018 General Information: 1 sample was analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. H4: Sample re -extracted and analyzed outside of EPA method holding time. •001 (Lab ID:92382051001) Sample Preparation: The samples were prepared in accordance with EPA 3511 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 eAnalytical www pawlabs.com i PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: W382051 Method: EPA 5030/8015 Mod. Description: Gasoline Range Organics Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 5030/8015 Mod.. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Anatytical Services, LLC. Page 7 of 18 1 .. aceAnalytical v eacefabs earn i i Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: 408412 D6: The precision between the sample and sample duplicate exceeded laboratory control limits. DUP (Lab ID: 2266119) • Total Suspended Solids DUP (Lab ID: 2266120) • Total Suspended Solids Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 Of 18 /71aceAnaVical l w»wpatelabs.con, Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078, /(70a)875-9092 ANALYTICAL I Project STORMWATER YR9, PD2 Pace Project No.: 92382051 Sample: 001 Parameters Lab ID: 9239z051001 Collected: 04/23/18 13:55 Results Units Report Limit OF Received. 04/24/18 1205 Matrix: Water Prepared Analyzed CAS No, Qual 1664 SGT-HEM, TPH Analytical Method. EPA 1664E Total Petroleum Hydrocarbons NO mg/L 5.0 1 04/25/18 05:21 8015 Diesel Low Volume Analytical Method: EPA 8015 Modified Preparation Method: EPA 3511 Diesel Range Organics(C10-C28) ND mg/L 0.50 1 05/01/18 08.40 05/01/18 13:26 H4 Surrogates n-Pentacosane(S) 105 % 70-130 1 05101/1808A0 05/01/1813:26 629-99-2 Gasoline Range Organics Analytical Method: EPA 503018015 Mod. Gas Range Organics (C6-C10) ND mg/1- 0.080 1 04/25/18 17:34 Surrogates 4-BromoBuorobenzene (S) 111 % 70-145 1 04/25/18 17:34 460-00-4 25400 Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 2.6 mg/L 2.5 1 04/30/18 14:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 05101 /2018 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 ��eAnalytical �`vmwpecera6s.com r QUALITY CONTROL DATA Project: - STORMWATER YR9, PD2 - —Pace. Project No.: 92382051 \ QC Batch: \ 407775 Analysis Method: EPA 166413, QC Batch Method: EPA 16643 Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92382051001 METHOD BLANK: 2262543 Matrix: Water Associated Lab Samples: 92382051001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L NO 5.0 04/25/18 05:06 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2262544 Spike LCS -CS % Rec Parameter Units Conic. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.5 102 64-132 MATRIX SPIKE SAMPLE: _ 2262545 35387367001 Spike MS MS %Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L S.OU 19.2 19.4 101 64-132 I Results presented on this page are in the units truth rated by the "Units" column eacepl where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full. Date: 05/01/2018 04:51 PM without the written consent of Pace Analytical Services. LLC. Page 10 of 18 / JJ laceAnayllical9 I www paceldbs.com i I Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 QC Batch: 407825 OC Batch Method: EPA 5030/8015 Mod. Associated Lab Samples: 92382051001 METHOD, BLANK: 2262719 Associated Lab Samples: 92382051001 Parameter Gas Range Organics (C6-CIO) 4-Bromofluorobenzene (S) QUALITY CONTROL DATA Analysis Method: EPA 5030/8015 Mod. Analysis Description: Gasoline Range Organics Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg/L NO 0,080 04/25/1814:26 113 70-145 04/25/18 14:26 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2262720 Spike 1-CS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Gas Range Organics (CB-C10) mg/L 1 1.0 100 70-150 4-Bromofluorobenzene (S) % 115 70-145 MATRIX SPIKE SAMPLE: Parameter 2262721 Units 92382047001 Result Spike MS MS Conc. Result % Rec % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/L - ND 1 0.91 90 .70-150 4-Bromofluorobenzene (S) % 119 70-145 SAMPLE DUPLICATE: 2262722 92382048001 Dup Parameter Units Result Result RPD Qualifiers Gas Range Organics (C6-C10) mg/L ND NO 4-Bromofluorobenzene (S) p/ 118 118 0 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/01/2018 04.51 PM without the written consent of Pace Analytical Services. L-C. Page 11 of 18 1�aceAnalyiical / www pacelaos cam I QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 QC Batch: 408631 Analysis Method: EPA 8015 Modified QC Batch Method: EPA 3511 Analysis Description: 8015 Diesel Low Volume Associated Lab Samples: 92382051001 METHOD BLANK: 2267259 Matrix: Water Associated Lab Samples: 92382051001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diesel Range Organics(C70-C28) mg/L NO 0.50 05/01/18 12:17 n-Pentacosane (S) % 102 70-130 05/01/18 12:17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2267260 Spike LCS LCS % Rec Parameter Units Conc. Result %Rec Limits Qualifiers Diesel Range Organics(C-10-C28) mg/L 10 9.4 94 70-130 n-Pentacosane(S) % 116 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2267261 2267262 MS MSD 92382767001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Diesel Range Organics(C70- mg/L 0.45J 10 10 8.8 8.8 83 84 70-130 1 C28) n-Pentacosane(S) % 99 105 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full. Date: 05/01/2018 04:51 PM without the written consent of Pace Analytical Services. LLC. Page 12 of 18 ��PaceAnalytical w pawlabs. cram Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.. 92382051 QC Batch: 408412 Analysis Method. SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382051001 METHOD BLANK: 2266117 Associated Lab Samples: 92382051001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2266118 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2266119 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE 2266120 Parameter Units Total Suspended Solids ni Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2.5 04130/1814:53 Spike LCS LCS % Rea Cone. Result e/ Rec Limits Qualifiers 250 242 97 90-110 92382049001 Dup Result Result RPD Qualifiers 24.4 43.2 56 D6 - 92382121001 Dup Result Result RPD Qualifiers 38.3 44.0 14 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date. 05/01/2018 04:51 PM without the written consent of Pace Analytical Services. LLC. Page 13 of 18 1�eAnajfyfical w»wpacerabscom i Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER YR9, PD2 Pace Project No.. 92382051 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit - TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethytvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. . PaceAnalytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte I7il_L�IIX�T�fa7Utll�:i�9 D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H4 Sample re -extracted and analyzed outside of EPA method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/01/2018 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 �IaceAnalytical- i v�vpacelabamm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER YR9, PD2 Pace Project No.: 92382051 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92382051001 001 EPA 1664E 407775 92382051001 001 EPA 3511 408631 EPA 8015 Modified 92382051001 001 EPA 5030/8015 Mod. 407825 92382051001 001 SM 2540D 408412 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, Dale: 05/01/2018 04:51 PM without the written consent of Pace Analytical Services, LLC. Analytical Batch 408752 Page 15 of 18 Document Name: Document Revised: February 7, 2018 Sample Condition Upon RecelpI(SCUR) Page 1 of 2 1�52ceMa p11Cdj Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] i r Client NaIC�� Project) �Q 92382�51 Courier: L]Fe&Ex ❑UPS -❑USPS -❑Client ❑ Commercial C, .r QOther:, 923820 Custody Seal Present? ❑Yes [31q - Seals Intact? []Yes 'Df10 N I %-�l'-� Date/Initials Person Examining Conlent3s'"� Packing Material: ❑Bubble Wrap E]866ble Bags []None ❑ Other Biological Tissue Frozen? Thermometer: []Yes ❑No ❑N/A ❑IRGun ID: 92T036 Type of Ice: ❑Wet ❑Bale Bone Cooler Temp ('C): C) - I Correction Factor: Add/Subtract (°C) +0.1 (f Temp should be above freezing to 6°C Cooler Temp Corrected (°C): `f ' % []Samples out of temp niteria. Samples on ice, cooling process has begun USDA Regulated Soil (E3,WA, water sample( Did samples origina[ein a quarantine zone within the Uniled States: CA, NY, or SC (check mapsj7 Old samples originate from a foreign source (internationally, RlmV rlyos r INo VYes L-_fNO - --- - Comments/Discrepancy: Chain of Custody Present? es []No ❑N/A 3. Samples Arrived within Hold Time? es ❑No N/A 2. Short Hold Time Analysfs (<72 ha)? ❑yes [JKr [-]N/A 3. Rush Turn Around Time Requested? Dyes .8ff—o ❑N/A q. Sufficient Volume? j2fg ❑No []N/A S. Correct Containers Used? -Pace Containers Used? qfr,, es ❑No ONO []N/A [:INLA 6. Containers Intact? ei Q{NNo N/A 7. Dissolved analysis: Samples Field Filtered? ❑yes ' LfNo []N/A 8. Sample Labels Match COV -include s Date/Time/10/Analysis Matrix: . Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? es []Yes ❑Yes ❑Yes ❑No 4I3��r�, .pnP ENO ❑N/A N/A []N/A ❑N/A 9- 10. COMMENTS/SAMPLE DISCREPANCY Lot ID of split contalners: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Date Required? ❑Yes []NO Page 16 of 18 Document Name: Document No.: Page 1 of 2 .. . Issuing Authority: 'Check mark top half Of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. EaeptlPne: VOA, Colifofm; TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box Is to list number of bottle Project WOW. .9.2382051 PM (KLHl 7 s i'�Duel`Date, 03/.01L18 CLIENT�'92-RSC?;., Q 6J < a V a E 6 es a v t! o J E J 6 m a L d ii E 7 6 O Z a m J n 7 n m v d o 2 n E 1%i 1 us N n.�.. o 2 n E a. b p a Z N u E aL m n Z So Z E a. tll u " y $ E a ¢ L a c 7 E a v r'1 a N U x E a _ .Q Z Z v = n a of /,1 a V 2 o ry 2 E i N a 2 a N 2 W E ¢ of T Q Z 2 Z E a E o `,'� n M Q i a O) E P O Q o a O E C~i > z < O E N > a ? o a O E U CI .� y= o `u n '5 Q i '� n tJ Q 2 _ N n N Z _ ° .n a N O y a of y D < g O o .N �o 7 Z N j E a - p N 2 3 a 5 6 7 I 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Typepl Preaervative pH upon re<elpt Date preservation adjusted Time pr¢aervatlan Amount of Preservative Lol q adjusted added ...m rhr Nnrth Carolina DEHNR CenlOcatlon MCC (I.e. u°te-whecevett2le[LISa�isvePancY-aHe[Iin6NPMSuollnalolnPPancx� Out of hold, iocorron preservative, out of temp, incorrect containers. Page 17 of 18 o- PaceAnalytiical - •'✓�'A1cet,III,am Section A Section D Required CGen! Inlo,mat.on Roquimd P �. IT�} Ca - RePon To: Mdress: l /Cl;E bV GL) ac; � c Fury To'. o Ct Znd;gn%Gr 1, NC 3'J Yi t, 5 V -1 �1/S II -a,: rd Duo Dam/TAT: lU LM CHAIN -OF -CUSTODY / Analytical Request Document _12 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o m N Section C - Pago: I of I a Section D Regt Malrk codes Regwmdah, In:mrna:mn u>ISIX r OnF - _ .., n. COLLECTED _ Dnnhing Wale, Dw - P/e5ervalives 8 Waver .ryT `� V 2 - Wa51C W.T, Aw v CO. TE OMPOCT `LOMGp$nE O P,-f... P w Srwnl : W SOUSDIid SL SAMPLE ID I A.Z. 0.91.-) q;,0. nR W V a W N Samalc IDs MUST BE UNICUE Tissue TS p a o_ z m Ornn, OT O r ~ 2 a x W z O m o 10 ='^V y a 0 g C ✓1 CUO I DATE TIME DATE TIME 2 O y hr C Y 13 13:5o Y a3 13:�5 2 i 3 5 6 7 B 9 in /1 12 ADDITIONAL COMMENTS RELINDUISNED BY/AFFILIATION - DATE TIME:: ACCEPTEDBY/AF 'IATI 22296G/- REGULATORY AGENCY 1 NPDES GROUND WATER i- DRINKING WATER I UST '- RCRA I, OTHER Site.Location STATE: nalysis Filtered (Y/N) � =I a ¢ Pace Project Nod Lab I.D. ON ' - DATE I, TIME I SAMPLE CONDITIONS IL-� 17'v1�1 ? .--,r_r, ORIGINAL ''11nuC nIU 11111TURE U PRINT Nami of SAMPLER: SI�Qi_ I<C-I�t, E ' - r - 2 SIGNATURE of SAMPLER: / DATE Signed E 'Inporl:rrrl Nele:❑ r' V r:;glrnny nruomr nu anrn¢nprne P:ar.'s NEilDe:ry paynrunumms Ono:rgmn'�mom uwru�wel Lex pnrmmrh I—,im�kuanr,kn (MMIDD/YYI: 1;. SLT � w` y F-ALL-0-020rev.07. 15dda,2007 l -PaceAnalytical y www Pacelabs. corn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 May 01, 2018 Stuart Kerkhoff Radiator Specialty Company 600 Radiator Road Indian Trail, NC 28079 RE: Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 � �2 L-1q +1 LFE MAY -I RECD , Dear Stuart Kerkhoff: Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures Q PCf o �S c tom•: �� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 Pace Analytical Services, LLC te 100 _ aceAnalytical a 9800HuntesKincey vlle, C128078 i w wparelabs win (704)875-9092 i CERTIFICATIONS Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VtrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full. without the written consent of Pace Analytical Services. LLC Page 2 of 18 /�aceAnalyflca( www p3mfabs oom i Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project:' STORMWATER YR9, PD2 Pace Project No.: 92382047 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92382047001 002 EPA 1664E JMS 1 PASI-C EPA 8015 Modified NUT 2 PASI-C EPA 5030/8015 Mod. CAH 2 PASI-C SM 2540D MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC Page 3 of 18 1�aceAnalytical0 wuw pacelabs. com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SUMMARY OF DETECTION Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92382047001 002 SM 2540D Total Suspended Solids 37.5 mg/L 15.6 04/30/18 14:55 REPORT OF LABORATORY ANALYSIS This repon shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 ljeAnalytical wwn Pacelabscum i i 9Z10131xdliJ_1GU IPLC Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 Method: EPA 1664E Description: 1664 SGT-HEM, TPH Client: Radiator Specialty Company Date. May 01. 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. LLC. Page 5 of 18 /71aceAnalyfical a .pacelabs.corn 1 PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 I--Ii1tT.S.�g9ii:Iil&71 -11MVI Description: 8015 Diesel Low Volume Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3511 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. QC Batch: 408280 S0: Surrogate recovery outside laboratory control limits. • LCS (Lab ID: 2265401) • n-Penlacosane (S) S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. • BLANK (Lab ID: 2265400) • n-Pentacosane (S) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the w/glen consent o1 Pace Analytical Services, LLC. Page 6 of 18 9 lr�aceAnalytical wmvpacelabs.com I PROJECT NARRATIVE Project. STORMWATER YR9, P02 Pace Project No.: 92382047 Method: EPA 5030/8015 Mod. Description: Gasoline Range Organics Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 5030/8015 Mod.. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within OC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within OC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 18 I�FaceAnalytical rw'w pacelabs. cram Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No 92382047 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Radiator Specialty Company Date: May 01, 2018 General information: 1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold limes with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below_ Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services. LLC, Page 8 of 18 1 � aceAnalytical9 Oawla65.com i ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 Sample: 002 lab ID: 92382047001 Collected: 04/24/1809:07 Received: 04/24/1812:05 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons NO mg/L 5.0 1 04/25/18 05:20 8015 Diesel Low Volume Analytical Method. EPA 8015 Modified Preparation Method. EPA 3511 Diesel Range Organics(C10-C28) NO mg/L 0.50 1 04/27/18 13:13 04/27/18 23:34 Surrogates n-Pentacosane (S) 124 % 70-130 1 04/27/18 13:13 04/27/18 23:34 629-99-2 Gasoline Range Organics Analytical Method. EPA 5030/8015 Mod. Gas Range Organics (C6-C10) ND mg/L 0.080 1 04/25/18 15:22 Surrogates 4-Bromofluorobenzene (S) 116 % 70-145 1 04/25/18 15:22 460-00-4 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 37.5 mg/L 15.6 1 04/30/18 14:55 Date: 05/01/2018 01:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in lull, without the written consent of Pace Analytical Services. LLC. Page 9 of 18 1 � aceAnalytical vmwpacelabs com i Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville. NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 QC Batch: 407775 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92382047001 METHOD BLANK: 2262543 Matrix: Water Associated Lab Samples: 92382047001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 04/25/18 05:06 LABORATORY CONTROL SAMPLE: 2262544 Spike LCS LCS e/ Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.5 102 64-132 MATRIX SPIKE SAMPLE: 2262545 35387367001 Spike MS MS %Rec Parameter Units Result Conc. Result e/ Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU 19.2 19A 101 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS Phis report shall not be reproduced, except in full, Date: 05/01/2018 01:55 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 11 aceAnalytical £ wwwpacelaDs. rom i Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, P02 Pace Project No.: 92382047 QC Batch: 407825 OC Balch Method: EPA 5030/8015 Mod. Associated Lab Samples: 92382047001 METHOD BLANK: 2262719 Associated Lab Samples: 92382047001 Parameter Units Gas Range Organics (C6-C10) mg/L 4-Bromofluorobenzene (S) % QUALITY CONTROL DATA Analysis Method: EPA 5030/8015 Mod. Analysis Description: Gasoline Range Organics Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 0.080 0412511814:26 113 70-145 0412511814:26 LABORATORY CONTROL SAMPLE: 2262720 Spike LCS LCS e/ Rec Parameter Units Conc. Result e/ Rec Limits Qualifiers Gas Range Organics (C6-C 10) mg/L 1 1.0 100 70-150 4-Bromofluorobenzene (S) % 115 70-145 MATRIX SPIKE SAMPLE: - Parameter 2262721 Units 92382047001 Result Spike Conc. ' MS MS Result % Rec % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/L ND 1 0.91 90 70-150 4-Bromofluorobenzene (S) % 119 70-145 SAMPLE DUPLICATE: 2262722 92382048001 Cup Parameter Units Result Result RPD Qualifiers Gas Range Organics (C6-C10) mg/L ND ND 4-Bromofluorobenzene (S) % 118 118 0 Results pre sound on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full. Date: 05/01 /2018 01:55 AM without the written consent of Pace Analytical Services. LLC. Page 11 of 18 ��PaceAnalytical vmwpacela0.s.com i i QUALITY CONTROL DATA Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 QC Batch: 408280 Analysis Method: EPA 8015 Modified QC Batch Method: EPA 3511 Analysis Description. 8015 Diesel Low Volume Associated Lab Samples: 92382047001 METHOD BLANK: 2265400 Matrix: Water Associated Lab Samples: 92382047001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diesel Range Organics(C 10-C28) mg/L ND 0.50 04/27/18 22:48 n-Pentacosane (S) % 139 70-130 04/27/18 22:48 S3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2265401 Spike LCS LCS % Rec Parameter Units Conic. Result %Rec Limits Qualifiers Diesel Range Organics(C10-C28) mg/L 10 10 100 70-130 n-Pentacosane(S) % 135 70-130 SO Results presented on this page are in the units inaiceted by the 'Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in lull. Date: 05/01 /2018 01:55 AM without the written consent of Pace Analytical Services, -LC. Page 12 of 18 ljeAnalytical / vfww pacefabs. com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlenwille, NC 28078 (704)B75-9092 QUALITY CONTROL DATA Project: STORMWATER YR9. PD2 Pace Project No.: 92382047 QC Batch: 408413 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382047001 METHOD BLANK: 2266121 Matrix: Water Associated Lab Samples: 92382047001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/18 14:55 LABORATORY CONTROL SAMPLE: 2266122 - Spike LCS LCS % Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 2266123 92382169001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 15.6 15.9 2 SAMPLE DUPLICATE: 2266124 92382308001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND 5.8 Results presented on this page are in tire units ine mated by the "Uni ls' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/01/2018 01:55 AM without the written consent of Pace Analytical Services, LLC, Page 13 of 18 1171aceAnalytical9 www pacelabs.crom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER YR9, PD2 Pace Project No.: 92382047 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS SO Surrogate recovery outside laboratory control limits. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 05/012018 01:55 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 ��PaceAnalytical wrx pacelabs cam Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER YR9, PD2 Pace Project No.: 92.382047 Lab ID Sample ID QC Batch Method QC Batch 92382047001 002 EPA 1664E 407775 92382047001 002 EPA 3511 408280 92382047001 002 EPA 5030/8015 Mod. 407825 92382047001 002 SM 2540D 408413 Date. 05/01 /2018 01:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. Analytical Method EPA 8015 Modified Analytical Batch 408291 Page 15 of 18 Document Name: Document Revised: February 7, 2018 aceAnalylica! Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Oftice Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsvllle❑ r Client Name.- // r , .g ,3.82 47.. _. . 7 rS Gl r Pro ec Wo Courier: ❑Fed Ex ❑UPS : ❑USPS ❑Client ❑ ar �I YII� I I �lI'I e�'' - ` -'- '"'` ❑ Commercial `❑Other:_ Custody Seal Present? ❑Yes ❑R, seats Intact? ❑Yes ONO (� K� Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap Dgubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes [—]NOt A ❑IRGun ID: 92TO36 Type of Ice: -[]Wet []Blue ❑Ngne Cooler Temp ('C): O Correction Factor: Add/Subtract ('C) +O, ) U I Temp should be above freezing to 6Y Cooler Temp Corrected ro: ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Sell (- /A, water sample) Did samples originate "in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, 1­1ve 1-11ki.. - ..,.o�nine Nawall and Puerto Rimy ayes FINo Comments/ DIs a re panty: Chain of Custody Present? Fjilrs ❑No N/A 1. Samples Arrived within Hold Time? es []NO N/A 2. Short Hold Time Analysis (<72 hr.)? Over 29-0— ❑N/A 3. Rush Turn Around Time Requested? []Yu [or- ❑N/A d. Sufficient Volume? ❑Yei ONO ❑N/A 5. Correct Containers Used? -Pace Containers Used? es oYes, ONO ❑No []N/A ❑tan 6. Containers Intact? RM QNO QNIA 7. Dissolved analysis: Samples Field Filtered? ❑Yes QNo []NIA B. Sample Labels Match COC? -Includes Dale/Time/ID/Anal sis Matrix: OW-1 ❑No ❑N/A 9. " Headspace in VOA Vials (>5.6mm)? ❑Yes 39'0— N/A 30. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑Ho [.}46 pN/A ❑N/A 11. _ COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Date: Date: Field Date Required? ❑Yes []NO Page 16 of 18 Document Name: Document Revised: February 7, 2018 aXAnalyfical' Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office `Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box Is to list number of bottle Projec W0# a 923820.47 PN.: KLH1 Due Date: 05/01/18- CLIENT: 92-RSC, E g ¢ = W 6 E o m 2 G E J 'm 2 R E J ou a 4r n m O E v m v O E Z m O1 O `a Q E a m 2 n Q E a m a u JTs q E o " 3 u t a i ti a - a E a m •_• a u z C E ¢ E n a O a E i .�i a _ vl E < E m a — D rh- „¢s a Z 0> GGE a o z D O > m > Z 0 E m i P O O E m o O N _ i ¢ > > p i n z— E N v', n ,„j a E N O x Z n E m a iO w G J E c a - C p r E OU > a — n Z G J ¢ E m o 1 2 3 a 5 6 7 6 9 10 11 12 PH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative - added Lot d Not, Whenevecthere.is.a. discrepancy -affecting North.Camlina.compfiancesamples, a_copy_of_thI5_fotrrt will bijttqrjm thgNorth Carolina DEHNR Certlllcatlon Otnce 0.e. _ Out of hold incorrect preservative, out of temp, Incorrect containers. Page 17 of 18 v, PkeAnalytical w w.pn[eldpx.[om Section A Required Client Inlormatio¢ a,nlpany: (( - �CtL' msl To rlronc Fn.: C cr t°qunsletl Duo DatcITAT: SeCcPn e R°gvlred Projeq Information' oo()' Regwree Cucnl lnbrmIDlm Matrl+Cpdos a LM1tt RikfODP — c OnnY.irg Wafer OW 9 iJ Wn:cr T W E V WoSlc Watar WW COMPOSITE PrMupl "' SAMPLE ID sp"elo-, oL Oil u (A-Z, 0-9 y-) Wipe Wp y l7 Sample DIMUSTBE, UNIQUE Air AR w w Tissue 00 011icr OT X w r r a ADDITIONAL COMMENTS Lid CHAIN -OF -CUSTODY If Analytical Request Document The Chain-of-CuSlody is a LEGAL DOCUMENT, All relevam fields mull be comPleted accurately. _o m N Section C Pago: �—�— Pf Invoice InlOrmalipn; Allcn(on; CPmpany Namc: / �A�'LCiv! '(.C, (f. REGULATORY AGENCY 7 Address: // 4 00 'P ! `idPDES _ GROUND WATER DRINKING WATER Y •X Rcrr u"cu: r CRA UST - R Paco Prp(aa l/ t - wrm!iec �i �- OTHER yr-t�f!`..•r r Site Locator, Paco Preldo 0; STATE: C Requested Anaiysfs Filtered (YIN) :TED Preserva(ives COM1IPOSIiE i O 1- eun mao J. N � L DATE OYPace Project Ned Lab LD. DATE TIME ACCEPTED By FILIATION DATE TIME u (� rr. it .. SAMPLE CONDITIONS � �� � J� 1 ORIGINAL-u-IF11 NAMEAND SIGNATURE PRINT'Namo of SAMPLER: S I rrII����,1 (((/C,,. SIGNATURE or SAMPLER: r� l�ll`VrJ 'IrnpnrL�m Nul¢ nS wyrhyl lni .Inrtn you :uu prc'aplbg Pam'x NO]p Cry W ymurn "I's ano a9rceiny ro pie cM1mpps of l SY. per rronN l: nn y mrol4r5 na R i0 rnlnin a— cu N 1�aceAnalytical0 v^pacelabs. cam 1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 May01, 2018 Stuart Kerkhoff Radiator Specialty Company 600 Radiator Road Indian Trail. NC 28079 RE: Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 JUN 14 RCC'D I Dear Stuart Kerkhoff: Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Bonnie Vang for Kevin Herring kevin,herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures FPCClu r REPORT OF LABORATORY ANALYSIS x N' This report shall not be reproduced, except in full, q; Qq without the written consent of Pace Analytical Services. LLC. soE�O, Page 1 of 18 -PaceAnalytical wwwparRlabS.artr Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # 1A170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification If 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 � ceAnalyticaly l vrowpecela6scon, i Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Lab ID Sample ID 92382046001 004 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664B JMS 1 PASI-C EPA 8015 Modified NU1 2 PASI-C EPA 5030/8015 Mod, CAH 2 PASI-C SM 2540D MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 ��e Analytical vmvrpacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (704)875-9092 611111611TIGl:4061911117l9x01IrroPI Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92382048001 004 SM 2540D Total Suspended Solids 6.5 mg/L 2.5 04/30/18 14:55 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 �1ace Analytical ~oacelsbs com i PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Method: EPA 1664E Description: 1664 SGT-HEM, TPH Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Hunlenw lle, NC 26078 (704)875-9092 General Information: 1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in lull, without the written consent or Pace Analytical Services, LLC. Page 5 of 18 17PaceAnapical E wwwpacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Method: EPA 8015 Modified Description: 8015 Diesel Low Volume Client: Radiator Specialty Company Date: May 01, 2018 General Information: 1 sample was analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3511 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any.exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 ll aceAnalytical e w wpacelabs.cam i I PROJECT NARRATIVE Project: , STORMVVATER YR9, PD2 Pace Project No: 92382048 Method: EPA 5030/8015 Mod. Description: Gasoline Range Organics Client: Radiator Specialty Company Date: May 01, 2018 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 1 sample was analyzed for EPA 5030/8015 Mod.. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: AI( criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within OC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 18 1 � aceAnalytical p xuw pacelabs.con Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Radiator Specialty Company Date: May 01, 2018 General Information: 1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF. LABORATORY ANALYSIS This report shall not be reproduced. except in for, without the written consent of Pace Analytical Services. LLC. Page 8 of 18 1�laceAnalytical I wwwpaceUbs.mm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 ANALYTICAL RESULTS Project:STORMWATER YR9, PD2 Pace Project No.: 92382048 Sample: 004 Lab ID: 92382048001 Collected: 04/24/18 09:17 Received: 04/24/18 12:05 Matrix: Water Parameters 1664 SGT-HEM, TPH Total Petroleum Hydrocarbons 8015 Diesel Low Volume Diesel Range Organics(C10-C28) Surrogates n-Penlacosane(S) Gasoline, Range Organics Gas Range Organics (C6-C10) Surrogates 4-BromoBuorobenzene (S) 2540D Total Suspended Solids Total Suspended Solids Date. 05/01/2018 04:50 PM Results Units Report Limit OF Prepared Analyzed CAS No. Oual Analytical Method: EPA 1664B - - NO mg/L 5.0 1 _ - 04125 Analytical Method: EPA 8015 Modified -Preparation Method: EPA 3511 NO mg/L 0.50 1 0510111808:40 05/01/1813:03 81 % 70-130 1 05/01/180840 05/01/181103 629-99-2 Analytical Method: EPA 5030/8015 Mod. NO mg/L 0.080 1 04/25/1815:50 118 % 70-145 1 04125/1815: 50 460-00-4 Analytical Method. SM 2540D 6.5 mg/L 2.5 1 04/30/18 14:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 18 1�eAnalytical a wvmparelabs.can j Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 QC Batch.- 407775 QC Batch Method: EPA 16646 —Asscoiotod.Lab Samples: 92382048001 METHOD BLANK: 2262543 Associated Lab Samples. 92382048001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2262544 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank -- Reporting Result Limit Analyzed Qualifiers ND 5.0 04/25/18 05:06 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 19.2 19.5 102 64-132 MATRIX SPIKE SAMPLE: 2262545 35387367001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L S.OU 19.2 19.4 101 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full. Date: 05/01/2018 04:50 PM without the written consent of Pace Analytical Services, U.C. Page 10 of 18 JaceAnalyfical b 1 wwx pacelabs.rorn I � QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 9?382048 1 OC Batch: 407825 Analysis Method: EPA 5030/8015 Mod QC BatchiMethod: EPA 5030/8015 Mod. Analysis Description: Gasoline Range Organics Associated Lab Samples. 92382048001 METHOD BLANK: 2262719 Matrix: Water Associated Lab Samples: 92382048001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Gas Range Organics (C6-C10) mg/L ND 0.080 04/25/18 14:26 4-Bromofluorobenzene (S) I % 113 70-145 04/25/18 14:26 LABORATORY CONTROL SAMPLE: 2262720 Spike LCS 1-CS % Red Parameter Units Conc. Result %Rec Limits Qualifiers Gas Range Organics (C6-C70) mg/L 1 1.0 100 70-150 4-Bromofluorobenzene (S) % 115 70-145 MATRIX SPIKE SAMPLE: 2262721 1 92382047001 Spike MS MS %Rec Parameter 1. Units Result Conc. Result %Rec Limits Qualifiers Gas Range�Organics (C6-C10) mg/L ND 1 0.91 90 70-150 4-Bromofluorobenzene (S) 1 % 119 70-145 SAMPLE DUPLICATE: 2262722 92382048001 Dup Parameter Units Result Result RPD Qualifiers Gas Range Organics (C6-CIO) mg/L ND ND 4-Bromofluorobenzene (S) i II % 118 118 0 I I Results presented on this page are I in the units t indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/01/2018 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 ��eAnayical � wWwp3CCIdbS.tplll i QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 - QC Batch: 408631 Analysis Method: EPA 8015 Modified QC Batch Method: EPA 3511 Analysis Description: 8015 Diesel Low Volume Associated Lab Samples: 92382048001 METHOD BLANK: 2267259 Matrix: Water Associated Lab Samples: 92382048001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diesel Range Organics(C10-C28) mg/L ND 0.50 05/01/18 12:17 n-Pentacosane (S) % 102 70-130 05/01/18 12:17 LABORATORY CONTROL SAMPLE: 2267260 Spike LCS LCS % Rec Parameter Units Conic. Result %Rec Limits Qualifiers Diesel Range Organics(C10-C28) mg/L 10 9.4 94 70-130 n-Pentacosane(S) % 116 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 2267261 MS 92382767001 Spike Parameter Units Result Conc. Diesel Range Organics(C10- mg/L 0 45J 10 C28) n-Pentacosane (S) % 2267262 MSD Spike MS MSD MS MSD e/ Rec Conc. Result Result % Rec e/ Rec Limits RPD 10 8.8 8.8 83 84 70-130 1 99 105 70-130 Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 05/01/2018 04:50 PM without the written consent of Pace Analytical Services, LLC. Dual Page 12 of 18 1J1 1 eAna1yfica1 vnrnpacelaEs.cnm i I Project: STORMWATER YR9, PD2 Pace Project No.: 9?382048 QC Batch; 408413 QC Batch lMethod: SM 2540D Associated Lab Samples: 92382048001 METHOD�BLANK: 2266121 Associatetl Lab Samples: 92382048001 1 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: I 2266122 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 25 04130/1814:55 Spike LCS LCS Conc. Result %Rec 250 244 98 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersedle, NC 28078 p041875 9092 % Rec Limits Qualifiers 90-110 SAMPLE DUPLICATE: 2266123 92382169001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 15.6 15.9 2 SAMPLE DUPLICATE: 2266124 92382308001 Cup Parameter Units Result Result 'RPD Qualifiers Total Suspended Solids mg/L NO 5.8 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result I i Date: 05/01/2018 04:50 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 13 of 18 �,PaceAnalytical xwM'.parRlabS.COT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huniersville. NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER YR9, PD2 Pace Project No.: 92382048 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05101 /2018 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 1�aceAnalytical y vmwpacelabs corn I QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunterwite. NC 28078 (704)875-9092 Project: Pace Project No.-. STORMWATER YR9, PD2 92382048 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92382048001 004 EPA 1664B 407775 92382048001 004 EPA 3511 408631 EPA 8015 Modified 408752 92382048001 004 EPA 5030/8015 Mod. 407825 92382048001 004 SM 2540D 408413 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/01/2018 04:50 PM without the written consent of Pace Analytical Services, LLC, Page 15 of 18 �aceAnalyi`101 Document Name: Sample Condition Upon Recelpt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality 0f0ce Laboratory receiving samples: Asheville ❑ Eden[—] Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Client Name: / Project H Courier. []Fed Ex ❑UPS . ❑LISPS ❑Client ❑ ❑Ca'Imerciaf V7rz :other:_ Custody Seal Present? ❑Yes [�Nll— Seals Intact? ❑yes .Ejao Date/Initials Person Examining Canlents: L' —' Y -d—T s " Packing Material: ❑Bubble Wrap ❑15—,bble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: [)Yes❑No ❑IRe�n10:92/T036 Type of et ❑slue ❑None Cooler Temp ('C): Correction Factor: Add/Subtract ('C) +0. ] � Temp should be above freezing to 6'C Cooler Temp Corrected( []Samples out of temp criteria. Samples on ice, coaling process has begun USDA Regulated Soli N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC(check maps)? Did samples originate from a foreign source (internatlanally, ._... ...... .,.n 000nn nimV flyer ITYa ' Comments/Discrepancy. Chain of Custody Present? E< ON. ❑N/a 1. Samples Arrived within Hold Time? es ONO N/A 2. Short Hold Time Analysis (<72 hr.)? Oyes to- ❑N/A 3. Rush Turn Around Time Requested? ❑yes ffrN. ❑N/A 4. Sufficient Volume? es ONO ❑N/A 5. Correct Containers Used? -Pace Containers Used? ❑-rs ONO ONO ❑N/A ❑N A 6. Containers Intact? faYe, ONO N/A 7. Dissolved analysis: Samples Field Flhered7 Oyes [21%fa— ❑N/A a. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: J:JV, Ui,i" ` ONO ❑N/A 9. . Headspace in VOA Vials (>5-6mm)? es ❑No N/A �-1 7 Trip Blank Present? Trip Blank Custody Seals Present? Oyes Oyes ]ftp, ENO pN/A ❑tl/A COMMENTS/SAMPLE DISCREPANCY Lot IDof split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Field Data Required? ❑Yes ONO Page 16 of 18 Document Name: Document Revised: February 7, 2010 Sample Condition Upan Recelpt(SCUR) Page 1 of 2 aceAnalyticsl y Document No.: Issuing Authorlty: F-CAR-CS-033-Rev.05 Pace Carolinas QualityOffice ----!Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (-.eater) DOC, LLHg "'Bottom half of box Is to list number of bottle . 2 on v T ¢ ¢ ¢ a ¢' x0 _ u < ¢ ¢ <• a n d n Z 2 Z A Ti v x x a ? ¢ Z O v z t Z y ? — fl a o o B o g i N v .i c' a. a a J E Oa Z J J J J N I Z N 2 u C J U_ N_ 2 `u 6 _ N 6 1 y d u p J _ M u .. .3 .. J u — Y .. := c .. u E x Z x y = 'u L '� a E a a a E E a a E o ¢ 0 ¢ 0 < 0 ¢ 0 a H ! S ¢ c E a a aE ¢ y E ,E 'E E E v 5 m `w E E n E E E E i° n E E E o- g E E = = o 'r yob O O o i i i o ° n ` m < c' 2 3• s x ._ 5 6 7 R 9 10 11 11 \ pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon recelpt Date pieservallon adjusted Time preservation adjusted Amount of Preservative added Lot x [Jnlr_lVherever.thecLiSailisaepaoty.dHetting Clnct[sSazelinJ_cetonliances am Ales-, opY9Lthis fc r will r rent to the North Carolina DEHNR Cen l llc a tloo Om o h.e. Out of hold, into ,ocl preservative, out of temp, incorrett containers. o Page 17 f 18 t �d Pace Analytical Section A Required Cliunl lnlurmalion: :aapany: c, itc�l;a- S nnm—:z 1 CHAIN -OF -CUSTODY / Analytical Request Document The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be compleled accurately. Section B Required Project Inlorm,s, Section C Pace, of Report i7 jj Invoice Information' N0.,�r I<1•_ICiT+iY Attention- Cc Email To:i _, I:+^r�',aCS.t',, AS. Panne: Purchd.Older No.: Cl ()Vv CI(�y 1 Ad Per Requested Dun c_ox: Project NamC: .� ` r ` •^ - 1 V '7 Yn+rxT�W C 'K I r Rel Pn[ Dat OITAT: ( 0 I Project Number: I C� :+( q Y Pn[ Section D Raouirad Gmnurtlormnrinn Manlx Codes 4 pin Tntz r 1,,f� - COLLECTEDWeer Drinking Water DL4 - o U 'rYdSIC Water WT WW Q U co"pos II C6MVOynE O Prwnfl arA r EN eck,,D SAMPLE ID SOiL'Golid Dil SL DL Ld o 1/M ST 1 Wife Air }VP AR u U smnplC IDS MUST 0E UNIOUc Tissue O m Z a Omer P o w X u Z ¢ Le ,O t Cif/ DATE TIME .DATE .TIME w O a W G V dY `(.•( 9 1y ((:(� 2 J ADDITIONAL COMMENTS RELINQUISHED BY/ DA'TE/ TIME e _229j ,'U REGULATORY AGENCY 'l+l'a r- O<L L/ 'NPOES (— GROUNDWATER r DRINKING WATER UST I— RCRA i- OTHER u e T, h c - Site Location STATE: - :Requested,Analysis Filtered (Y/N) z DS T z N _•. C re 0 y N e Pace Project No./ Lab I.D. G�BGtNr;L SAMPLER NAME AND SIGNATURE N PRINT Name of SAMPLER: Ed SIGNATURE of SAMPLER: - - O- 'Imnnn.nn tlole:ep`ulrurul lWS lvm Yauero Uoceytinq P:,, NE1 J00:ry neYmenl rorms:md agrr, to tale crev r. l - Gina 9 .yels^u Iwnnwrn M anY invoicre eo, pe. —,e, 90 days. 'DATE: I TIME �'g j lit ALL-C-020rev.07.15-1,a y.2007 /Or Chemical Solutions o division of Radiator Speclalfy Company March 21. 2018 Central Piles North Carolina Department of Environmental Quality Division of Energy, Mineral and Land Resources Stormwater Program 1617 Mail Service Center Raleigh, North Carolina 27699 c m; RE: Stormwater Discharge Outfall Monitoring Report � Z- " i t Radiator Specialty Company CO n.a Radiator Road, Indian Trail, North Carolina in r- �7 rl NPDES Permit No. NCS000183 o r- C' z n a, JTl D Dear Sirs: Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outlall Monitoring Report for monitoring period Year 9 - Period 1 as required by Part 111 Section E.(1.) and (2.) of Nalional Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company �Cut� G. l Stuart A. Kerkhoff, CHMM Environmental Health and Safety Manager Attachments S IRMWA IWR919 I -2018CVL IDOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscbronds.com STORM WATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS NCS000183 FACILITY NAME Radiator Specialty Company 13EIZSON COLLECTING SAMPLE(S) Stuart Kcrkhoff CERTIFIED LABORATORY(S)_Prisnt Laboratories, Inc. -Lab # 402 Lab # ]'art A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days front the date the facility receives the sampling results from the laboratory.) COUNTY Union PHON .�0. L704� 68J-I8F5 SIGNATURE OF PERKIITTEE OR DESIGNEE REQUIRED ON PAGE 2. Oulfall Date 50050 y ±t T3-- u_ a� ,_ , ;• - No. Sample, , , ;, Collected - Total *,. -Flow, if'a Total i' a •Ratnfall^' Suspended rSohilsw,�.,..� aQ Otliand f °Greaser }T,P,H# DRO T;PH. GRO,. H mo/dd/ r MG inches :.. i'-Kti'/Lz" s&,`P3+'S m-%14 ;x,."`r a m4/Ly ' Ak/L Units 002 9/12/17 NA 1.79 <100 <30 <0.53 <0.20 6.50 004 9/12/17 NA 1.79 <100 <30 - <0.53 <0.20 6.30 003 10/16/17 NA' 0.30 <100 `'<30 <0.55 <0.20 6.40 001 12/20/17 NA 1.27 <100 <30 <0.52 <0.20 6.77 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _,yes X_no (if vcs. complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Oulfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SCT=HEM), if Total Suspended Solids pH Nov Motor Oil Usage mo/dd/ yr MG inches m /I. m /I unit;,`, +al/mo Form SWU-247, last revised 2/1/?0/2 Page I of 2 STORM EVENT CHARACTERISTICS: Date 9/12/17 Total Event Precipitation (inches): _1.79 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date _10/16/17 Total Event Precipitation (inches): 0.30 Event Duration (hours): (only if applicable — see permit.) Date 12/20/17 Total Event Precipitation (inches): _1.27 Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleig-h, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best or my knowledge and belief, true, accurate, and complete. I ant aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit(ce) (Dat ) Form SWU-247. last revised 21212012 Paee 2 of 2 .1 PRISM 2=OIABOflATOPIE$ Wa Radiator Specialty Cc Stuart Kerkhoft 600 Radiator Rd. Indian Trail, NC 28079 NC Certification No. 402 Full -Service Analytical 8 NC Drinking Wale, Cert No. 37735 Environmental Solutions SC Certification No, 99012 Project: 2017 Stormwater Project No.: NGS000183 Lab Submittal Date: 09/14/2017 Prism Work Order: 7090244 Case Narrative 09/27/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference SEN g 2'U17 Reviewed By Cara C. Rusmisell Project Manager Results reported to the reporting limit. All other.results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced. except in Its entirety, without the written consent of prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-8001529.6364-Fax: 7041525-0409 Page 1 of 8 jb. R I S M Full -Service nalylical A Eu.!ronme tat set !,e = Sample Receipt Summary 09127/201 7 Prism Work Order- 7090244 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 002 004 7090244-01 7090244-02 Water Water 09/12/17 09/12/17 09/14/17 09/14/17 Samples were received in good condition at 4.0 degrees C unless otherwise noted. This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525.0409 Page 2 of 8 P ISM n„SOW'a QP. Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: 2017 Stormwater Project NO.: NCS000183 Sample Matrix: Water Laboratory Report 09/27/2017 Client Sample ID: 004 Prism Sample ID: 7090244-02 Prism Work Order 7090244 Time Collected: 09/12/17 08:30 Time Submitted: 09/14/17 17:33 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dale/Time ID Diesel,Range Organics by GC/FID Diesel Range Organics BRL mg/L 0.53 0.19 1 '8015C 9/16/17 14:42 ZRC P710238 Gasoline Range Orc Gasoline Range Organics o-Terphenyl 74 % 50-144 GC/FID BRL mg/L 0.20 0.026 1 '8015C 9119/17 19:57 ANG P710288 General Chemistry Parameters Oil & Grease (HEM) Total Suspended Solids a,a,a-Trilluorotoluene 106 % 57-132 BRL 4A mg/L m91L 5.0 0.98 1 2.5 0.40 1 '16648 9/26/17 13:05 'SM2540 D 9118117 10:23 SLS SLS P710411 P710263 This report should not be reproducedexcept in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte. NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525-0409 Page 4 0f 8 �PRISM Laboratory Report /� Fu1LServrcc Analyneal R d q environrnenmr Solutions 09/27/2017 6" �"�Ciw, m. u m x u s . c Radiator Specialty Co Project: 2017 Stormwaler Client Sample ID: 002 Attn. Stuart Kerkhoff Prism Sample ID. 7090244-01 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7090244 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 09/12/17 08:20 Time Submitted: 09/14/17 17:33 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch Limit Factor Daterl-ime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 0.53 0,19 1 '8015C 9/16117 15,19 ZRC P710238 Surrogate Recovery Control Limits o-Terphenyl 70 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.026 1 -8015C 9/19117 19.29 ANG P710288 __.____-- Surrogate Recovery Control Limits General Chemistry Parameters Oil 8 Grease (HEM) Total Suspended Solids a,a,a-Trilluorotoluene 103 % 57-132 BRL 18 mg/L mglL 5.0 0.98 1 17 0.40 1 '16648 926/17 12'11 'SM2540D 9118M7 10:23 SLS SLS P710411 P710263 This report should not be reproducedexcept in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 7041529-6364- Toll Free Number: l-8D01529.6364-Fax: 7041525-0409 Page 3 of 8 AC m R. I S M % .5�,.,� 4Ia.I.,i. 4 . 6n „enm r t Set rlen= Level II QC Report 9127117 Radiator Specialty Co Project: 2017 Stormwater Prism Work Order: 7090244 Attn: Stuart Kerkhoff Time Submitted: 9/14/2017 5:33:OOPM 600 Radiator Rd. Project No: NC3000183 Indian Trail, NC 28079 Gasoline Range Organics by GCIFID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710288 - 5030B Blank (P710288-BLK1) Gasoline Range Organics Surrogate: a,a,a-Trilluomtoluene LCS (P710288-657) Gasoline Range Organics Surrogate: a.a, a- Tri/luorotoluene LCS Dup (P710288.BSD1) Gasoline Range Organics Surrogate: a,a,a-Tri/luorotoluene Matrix Spike (P710288-MS1) Gasoline Range Organics Surrogate: a,a,a-Trilluomtoluene Matrix Spike Quip (P7I0288-MSD1) Gasoline Range Organics Surrogate: a.a.a-Trlllucrotoluene Prepared & Analyzed: 09/19/17 BRL 0.20 m /L 0.0980 mg/L 0,1000 98 57-132 Prepared & Analyzed. 09/19/17 1.26 0.20 mg/L 1.000 126 60-138 0.111 mg/L 0.1000 ill 57-132 Prepared & Analyzed: 09/19/17 1.20 0.20 mg/L 1.000 120 60-138 5 20 0.104 mg/L 0. 1000 104 57-132 Source: 7090244-01 Prepared & Analyzed: 09/19/17 1.24 0.20 m /L 1.000 0.0370 120 69-130 0.102 ri 0,1000 102 57-132 Source: 7090244-01 Prepared & Analyzed: 09/19/17 1.22 0.20 mg/L 1.000 0.0370 118 69-130 1 24 a 105 mg/L 0.1000 105 57-132 This report should not be reproducedexcept in its entirety, without the written consent of Prism Laboratories, Inc. 444 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: l-8001529.6364-Fax: 7041525-0409 Page 5 of 8 ��s PRISM Full -Service r,laoa do romtas al Envinenl Solutions �v..no..ra,>..c Radiator Specialty Co Project 2017 Stormwater Alin: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Level II QC Report 9/27/17 Prism Work Order: 7090244 Time Submitted: 9/14/2017 5:33:OOPM Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710238 - 3510C GC Blank (P710238-BLK1) Prepared & Analyzed: 09/16/17 Diesel Range Organics BRL 0.50 mglL Surrogate: o-Terphenyl 0.0532 mg/L 0.08000 67 50-144 LCS (P710238-BSI) Prepared & Analyzed: 09/16117 Diesel Range Organics 1.95 0.50 mglL 2.000 98 53-135 Surrogate: o-Terphenyl 0.0318 mg/L 0.04000 80 50-144 LCS Dup (P710238-BSD1) Prepared & Analyzed: 09/16/17 ........ .._... Diesel Range Organics 1.64 0.50 mg/L 2,000 82 53-135 17 20 Surrogate.' o-Terphenyl 0.0256 mg/L 0.04000 66 50-144 This report should not be reproduced. except in its entirety. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 6 of 8 a, Level II QC Report �PrR I S M I F Service Analytical One ylI a 9/27/17 Env mt So �vM'uNxWls+XC Radiator Specialty Co Project: 2017 Slormwater Prism Work Order: 7090244 Attn: Stuart Kerkhoff Time Submitted: 9/14/2017 5:33:00PM 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710263 - NO PREP Blank (P710263-BLK1) Prepared & Analyzed: 09/18/17 Total Suspended Solids BRL 5o mg/L LCS (P710263-BSI) Prepared & Analyzed: 09/18/17 Total Suspended Solids 490 5.0 mg/L 477a 103 90-110 Duplicate (P710263-Di Source: 7090244-01 Prepared & Analyzed: 09/18/17 Total Suspended Solids 17 5.0 mg/L 18 4 20 Batch P710411 - NO PREP Blank (P710411-BLK1) Prepared & Analyzed: 09/26/17 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P710411-BS1) Prepared & Analyzed: 09/26/17 Oil & Grease (HEM) 39.2 5.0 mg/L 40.00 98 78-114 Matrix Spike (P710411-MS1) Source: 7090244-02 Prepared & Analyzed: 09/26/17 Oil & Grease (HEM) 47.1 5o mg/L 50.63 2.78 88 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Date/rime 7090244-01 P710238 940 mL 1 mL 09/16/17 8:45 7090244-02 P710238 940 ml- 1 mL 09/16/17 845 Prep Method: 5030E Lab Number Batch Initial Final DateRime 7090244-01 P710288 5 mL 5 mL 09/19/17 1529 7090244-02 P710288 5 mL 5 mL 09/19/17 15:29 This report should not be reproduced except in its entirely. without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte. NC 28224.0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525.0409 Page 7 of 8 PraLSel vice An.rlyllcalE C.HAON OF CUSTODY RECORD y 9 Environmental Solutions PACE_ 1 .OF _ OUOTE N TO ENSURE PROPER BILLING: ec cM) apr'ngh <,or Road - Charlotte, NC 28217 Project t Name: PI >,r )gels2q;5tr4 Fe.: Tgs g2s g4oe Short Hold Analysis: (Yes) (k) UST Project: (Yes) ;,t: is 'Please ATTACH any project specific reporting (QC LEVEL 1 If III IV) Client Company Name: Lk I� f )i �.'� 1% I— provisions andlor QC RequirementsReport To/Contact Name: _� f ,.,-- V CC q l t Invoice To: lj CC f t L ,; 6; Reporting Address �,,_(I Q, 1J (_ J. 9 Address: liar gill•• h ;�C I n -, :; ul" r O Rr itrt nnr/L-TI r _ � (n r r(' 'w,4 al I(a L rr{IIJ Lrlll TI!Yh - m P'Po r l ,�1/AII If L +ui rnone: r. Purchase Order No.IBillin Reference -r. `i' f: j �: �,. 1. i g �..,. t'k. TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: �(�i, ;', �.1•r ,ix. is-• Requested Due Dale ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days U 5 Days CertlticatiOn: NELAC DOD FL NC ••� FUD Type: PDFy`ExCel Other "Working Days" ❑ 6-9 Days Q13tandaro 10 days ❑Rush Work Must Be — — Site Location Name: li \ 'L Pre -Approved Samples received after 14:00 will be processed next business day. SC OTHER NIA — Site Location Physical Adess: +- C/C' r<°<`. C(. 11 3,._ Turnar000d time is based on business days, excluding weekends and holidays. dr Water Chlorinated' YES NO✓ ') - (SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES q•_;3 I n;(r 0.'�{� ;' . ! aft < �I S-" !"! RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) _ Sample Iced Upon Collection: YES =NO_ TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, WATER OR PRESERVA- TIVES "-F i-� i �. ,�'_ ,^ --1� /• / REMARKS PRISM LAB •TYPE HOURS SLUDGE) SEE BELOW IJO. SIZE n' :� -; J " / \��� / ID NO. I Kit Sampler's Signature' V',t ,r IRfi'�jo�� Sampled By (Print Name) J111.c, Affiliation APFiiation i``tt Its. Upon relinquishing, this Chain of Custd6y leyour authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. _ __'-y�' ..,•�'w: Relinat she0 y: ( :gnat))p R) e + -�i, L. ) Receiv 8y; ISignature) Dale 1,1111tarylHours „� Additional Comments ItIT`fO rT.1� i ""f,�/l-� C ".nrlc_._ iL('�J I�.t ,�,C•��:� �.--/ y f;:ht,,"n .._ Relmqu s - Y: ISig store) '/ ,- Rea Y IS ture 1 ale ' \ i ti-1n L .t r: n-- / Relmqu gd y:(Signature) Receive or Prim omlarias Sy: Date f 't r b lh Meod cl SM1ipment NOTE: ALL SAMPLE COOLERS SHOOED BE TgPED SNUT WITH CUST DY LS FOR TRANS T SAMPLES ARE IJOT ACCEPTED AND VERIFIED AGAINST COC UNTI RECEIVED AT THE LABORAT RY. D Fed E. ❑ UPS O Hand -delivered v'P;ism Field Service ❑ Other tJ i�t; ✓� t'f NPOES: UST: GROUNDWATER: i DRINKING WATER: SOLID WASTE: ; RCRA: CERCLA LANDFILL OTHER: - ff" C❑SC ❑NC ❑SCI ❑NC ❑SC ' ❑NC ❑SC ONC ClSC ` El SC ❑NC ❑SC ❑NC ❑SC ❑NC OSC 1 ❑ __ ❑ ❑ ❑ cl -_. ❑ ❑ n n 1 'CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) /j"R ISM �OLAOOPATOWES I.0 Radiator Specialty Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 NC certification No. 402 Full -Service Analytical & NC Drinking Water Cen No. 37735 Environmental Solutions SC Certification No. 99012 Project: 2017 Stormwater Project No.: NCS000183 Lab Submittal Date: 10/18/2017 Prism Work Order: 7100361 Case Narrative 1 1 /01 /2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference NOV 8 2011 IU 6- Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 1 Of 7 Sample Receipt Summary vu • En iro Service Analytical s 11/Ol/2017 P'R I S M I env ronmcoim Solutions Prism Work Order: 7100361 Client Sample ID Lab Sample ID Matrix -Date Sampled Date Received 003 7100361-01 Water 10/16/17 10/18/17 Samples were received in good condition at 3.9 degrees C unless otherwise noted. This report should not be reproduced. except in its entirely. without the written consent of Prism Laboratones, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 281 Phone: 704/529-6364 - Toll Free Number: 1-600/529.6364-Fax: 704/525-0409 Page 2 of 7 nun.6enAnalytical Environm,n.J S.lmnas/AfikRI S M l Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: 2017 Slormwater Project No.: NCS000183 Sample Matrix: Water Laboratory Report 11/01/2017 Client Sample ID: 003 Prism Sample ID: 7100361-01 Prism Work Order: 7100361 Time Collected: 10/16/17 08:25 Time Submitted: 10/18/17 15:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch Limit Factor Daterrime ID Diesel Range Organics by GCIFID Diesel Range Organics BRL mg/L 0.55 0.20 1 18015C 10/23/17 20:08 ZRC P7J0394 Surrogate Recovery Control Limits Gasoline Range Orc Gasoline Range Organics GC/FID BRL General Chemistry Parameters Oil & Grease (HEM) Total Suspended Solids o-Terphenyl 95 % 50-144 mg/L 0.20 0.026 1 '8015C 10/30/17 15.46 ANG P7J0568 Surrogate Recovery Control Limits a,a.a-Trifluorotoluene 91 % 57-132 BRL 32 mg/L mg/L 5.0 0.98 3.8 0.40 1 •1664B 10/26/17 10:39 1 'SM2540 D 10/20/17 11:37 SLS SLS P7.10524 P7J0374 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: l-8001529-6364-Fax : 7041525-0409 Page 3 of 7 �E--Dzml AR ISM I Environmental nvir nmen nomrutio 4 Full -Service Analytical Level II QC Report 11/l/17 Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkholf 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Prism Work Order: 7100361 Time Submitted: 10/18/2017 3:00 OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7JO568 - 5030B - Blank (P7J0568-BLKt) Prepared & Analyzed: 10/30/17 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Tnfluomtoluene 0.0830 mgfl. 0.1000 83 57-132 LCS (P7J0568-BS1) Prepared & Analyzed: 10/30/17 Gasoline Range Organics 1.12 0.20 mg/L 1.000 112 60-138 Surrogate: a, a, a-Tritluorofoluene 0.0970 mg1L 0.1000 97 57-132 LCS Dup (P7J0568-BSDt) Prepared & Analyzed: 10/30/17 Gasoline Range Organics 1.13 0.20 mg/L 1.000 113 60-138 0.5 20 Surrogate: a,a,a-Tnfluomtoluene 0,101 mg/L 0.1000 101 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041625.0409 Page 4 of 7 A 6 MISM FWLServiee Analytical 8 Environmental Solutions Level II QC Report 11/l/17 Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Reporting Analyte Result . Limit Units Batch P7J0394 - 351 DC GC Prism Work Order: 7100361 Time Submitted: 10/18/2017 3:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7J0394-131-K1) __—_--_.-...__._.-..___.-___._..__. _..-_____. Prepared & Analyzed: 10/23/17 Diesel Range Organics BRL 0.50 mg/L Sunrogale: o-Terphenyl 0.0334 mg1L 0.04000 84 50-144 LCS (P7J0394-BS1) Prepared & Analyzed: 10/23/17 Diesel Range Organics 2.09 0.50 mg/L 2.000 104 53-135 Surrogate: o-Terphenyl 0.0365 mgQ 0,04000 91 50-144 LCS Dup (P7J0394-13SDt) Prepared & Analyzed: 10/23/17 Diesel Range Organics 2.02 0.50 mg/L 2.000 101 53-135 3 20 Surrogate: o-Terphenyl 0.0360 mg1L 0,04000 90 50-144 Matrix Spike (P7J0394-MS1) Source: 7100361-01 Prepared & Analyzed: 10/23/17 Diesel Range Organics 4.53 1.1 mg/L 4.255 BRL 107 51-145 Surrogate: o.Terphenyl 0.0603 mg1L 0,08511 94 50-144 Matrix Spike Dup (P7J0394-MSD1) Source: 7100361-01 Prepared & Analyzed: 10/23/17 Diesel Range Organics 4,41 1.1 mg/L 4.255 BRL 104 51-145 3 22 Surrogate: o-Terphenyl 0,0784 mg1L 0,08511 92 50-144 II This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spnngbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 5 of 7 1 r. 2PISM r4�9uwn.TonIas 11c Full -Service Analytical & Environmental Solutions Level II QC Report 11/1117 Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Analyse Result Limit Units Batch P7JO374 - NO PREP Prism Work Order: 7100361 Time Submitted: 10/18/2017 3:00:OOPM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes Blank (P7J0374-BLK1) Prepared & Analyzed: 10/20/17 Total Suspended Solids BRL 5.0 mg/L LCS (P7J0374-BSI) Prepared & Analyzed: 10/20/17 Total Suspended Solids 470 5.0 mg/L 477.0 99 90-110 Batch P7JO524 - NO PREP Blank (P7J0524-81-K1) Prepared & Analyzed: 10/26/17 Oil & Grease (HEM) BRL 5o mg/L LCS (P7J0524-13SI) _ ...... ...... ... __... ..._ ..____.__ ---- Prepared & Analyzed: 10/26/17 —...__—. .._._. ._... __._....... Oil & Grease (HEM) 38.4 5.0 mg/L 40.00 96 78-114 Duplicate (P7J0524-DUP1) Source: 7100361-01 Prepared & Analyzed: 10/26/17 Oil & Grease (HEM) BRL 5.0 mg/L BRL 18 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Dale/Time 7100361-01 P7J0394 910 mL 1 mL 10/23/17 10:00 Prep Method: 50308 Lab Number Batch Initial Final Date/Time 7100361-01 P7J0568 5 mL 5 mL 10/30/17 12:30 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-8001629-6364- Fax: 704/525.0409 Page 6 of 7 Full -Service Analytical & Environmental SOIUUons ... i,. •nun. Im ^. irvc. 419 gpmllbrook Road - Charlene, NC 28217 Pnono 7041529-G364 - Faz: 7041525-0409 Client Company Name: j(tdV0.r-i"r - �77)` �Y Report To/Contact Name: S t-L - F- Reporting Address: L._N '3d �t i ;�.` Ii v 'fit )•' PAGE— OF —L QUOTE N TO ENSURE PROPER BILLING: Project Name: ,'�of .Mw ..i^KI" I zc.."i, I_f . Short Hold Analysis: (Yes) UST Project: (Yes) (FW 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions and/or QC Require megts Invoice To: A CCf} G-.k- Address: i'I ;✓I ` z-,J'fe, i- -I :, r I !f Salnpl s INTAC; 1upor w r'.d" Re aved ON WE I' k F' PROPER PRFSFdRb'ATIVF.-S mcliroted? Pcr-ived fflIHIP1 HOLDINGTIMES'' CU It Y -FILL.: INIAIII"- VnLAI IF c' OW)OL) T HEADSPACI? PPl FR CONIAINFRS �Scd` 1 E —NONIA IA r— O Phone: ( f `/ 'f Y; 'i' Fax (Yes) ([bq): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: Requested Due Date D 1 Day ❑ 2 Days ❑ 3 Jays ❑ 4 Days O 5 Days Certification: NELAC DOD FL NC EDD Type: PDF ,., ;" Excel Other "Working Days" " ❑ 6-9 Days EFStany dard 10 days ❑ Rush Work Must Be Pre -Approved Sc OTHER NIA Site Location Name: I' C_ Samples received after 14:00 will be processed next business day. Site Location Physical Address: �- CC.1 •IZai(I .C.F:`— Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO Sr(SEE TI REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ NO_ ([_.l T, J �' RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, WATER OR PRESERVA- TNES i, .7 REMARKS !\�� `11u `- !'`, LAB ID NO. 'TYPE SLUDGE) NO. SIZE kJ SEE BELOW l.rL ,i Fo IL i l ((HOURS 'S •,25 L� � � 1` L (=iL'- 1 L!G,�S [� I — C U. /i 3 a., L L I A- i 'i ,'t: rr,' r r 1- % SIP J kc.- R•kk CL-- Sampler's Signature .�-1 '�• s✓ Sampled By (Print Name) v,� .Or Affiliation , Upon relinquishing, this Chain of C6tody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must beu��'r +era submitted In writing to the Prism Project Manager. There will be charges for an hanges after analyses hive been Initialized. a Olin edB atur / Recervetl 6Y (Slgnatw y, ` Date Meitarprl.,e Additional Comments 9n /. 9 �' d- A,,,al C Lc /c (.( ! 7 1. 6G' U ✓�' r� lV i 1 Jv — _ .G Relinquished By: (S,nature O Received by (Signature) Date Relinqushed By: ISignatura) 7 Receivetl For Prism Legerpo/njy� By: Date Meld r i - Me1M1od o15M1ipmenL NOTE:ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUbI U EALS FOR TRANSPORTATION TO THE LABORATORY CDC Group N .., �.......-._._.....___._.___._ ' SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTILPICEIVED AT THE LABORATORY. ❑ Fed Ex U UPS ❑ Hand-aelivered ism Feld Service ❑ Other 1` V ii l� I yr7 NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: 2�fACJ SC 0NC OSC 0NC ❑SC 0NC ❑SC 0NC ❑SC ❑NC❑SC 0NC ❑SC 0NC 0SC El INC 0SC Case Narrative FISM Y u60RATOMEs INC Radiator Specialty Cc Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cen No. 37735 Environmental Solutions SC Certification No. 99012 By 'AN Project: 2017 Stormwater Project No.: NCS000183 Lab Submittal Date: 12/21/2017 Prism Work Order: 7120401 01 /09/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. - Please call if you have any questions relating to this analytical report. Respectfully PRISM LABORATORIES, INC. u1 f (m�.a�Cl� Cara C. Rusmisell Project Manager Data Qualifiers Key Reference Reviewed By Cara C. Rusmisell Project Manager L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced. except in its entirety. without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-800/529-6364-Fax: 704/526-0409 Page 1 of 7 { �'Fi I S M I En'y1n omen Analytical s Sample Receipt Summary ®� ❑ Envhonmemal Solutions 01/09/201� V...nrnu...Rn iw. Y Prism Work Order: 7120401 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 001 7120401-01 Water 12/20/17 12/21/17 Samples were received in good condition at 4.5 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories.. Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364-Toll Free Number: l-8001529-6364- Fax: 704/525-0409 Page 2 of 7 &w. Full -Service Analytical a I SM I Env,ronmenla Solutions LT3Vu n, ,n es ,c Laboratory Report 01/09/2018 Radiator Specialty Co Project: 2017 Stormwater Client Sample ID: 001 Attn: Stuart Kerkhoff Prism Sample ID: 7120401-01 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7120401 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 12/20/17 09:40 Time Submitted: 12/21/17 15:00 Parameter Result Units Report MOL Dilution Method Analysis Analyst Balch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 0.52 0.19 1 '8015C 12/28/17 4:01 ZRC P71-0407 Surrogate Recovery Control Limits o-Terphenyl 77 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.026 1 18015C 1/3118 1:22 ANG P8A0007 Surrogate —--- _ Recovery Control Limits a,a,a-Tnnuorotoluene 104 % 57-132 General Chemistry Parameters Oil 8 Grease (HEM) Total Suspended Solids BRL mg/L 5.0 7.1 mg/L 2.9 0.98 1 '1664B 1/8/18 9:08 SLS P8A0080 0.40 1 'SM2540 D 12/22/17 12:15 EGC P71_0389 This report should not be reproduced.. except in its entirety, without the written consent of Prism Laboratones. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 3 of 7 I PRISM ®Vr.<un.owes rxc Full-Snrvicc Analytical & Environmental Solutions Level II QC Report 1/9/18 Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Analyte Batch P8A0007 - 5030B Reporting Result Limit Units Prism Work Order: 7120401 Time Submitted: 12/21/2017 3:00:OOPM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes Blank(PBA0007-BLK1) _ Prepared: 01/02118 Analyzed: 01/03/18 Gasoline Range Organics BRL 0.20 mg1L Surrogate: a,a,a-Tdfluorotoluene 0,0940 mgA- 0.1000 94 57-132 LCS (PSA0007-BS1) Prepared & Analyzed: 01/02/18 Gasoline Range Organics 1.29 0.20 mg/L 1.000 129 60-138 Surrogate: a,a,a-Tdfluorotoluene 0.103 mg/L 0.1000 103 57-132 LCS Dup (P8A0007-BSD1) Prepared & Analyzed: 01/02118 Gasoline Range Organics 1.43 0.20 mg/L 1.000 143 60-138 10 20 12 Surrogate: a,a,a-Trifluorotoluene 0.102 mglL 0.1000 102 57432 Matrix Spike (P8A0007-MS1) Source: 7120401-01 Prepared & Analyzed: 01/02/18 Gasolirie Range Organics 1.03 0.20 mg/L 1.000 0.0500 98 69-130 Surrogate: a,a,a-Trilluorotoluene 0,0680 mgA. 01000 88 57-132 Matrix Spike Cup (PBA0007-MSD1) Source: 7120401-01 Prepared & Analyzed: 01/02/18 Gasoline Range Organics 1.25 0.20 mg/L 1.000 0.0500 120 69-130 20 24 Surrogate: a,a,a-Trifluorotoluene 0.0890 mgA_ o1000 69 57-132 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 4 of 7 N ®P`Rnf,u service Anaryrcaia I S M I E�°ironmeutal Solut,ons Level II QC Report 119/18 Radiator Specialty Co Project: 2017 Stormwater AUn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Prism Work Order: 7120401 Time Submitted: 12/21/2017 3:00 OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P71_0407 - 351 OC GC Blank(P7L0407-BLK1) Prepared: 12/27/17 Analyzed: 12/28/17 Diesel Range Organics BRL 0.50 mg/L Surrogate: o-Terphenyl 0.0284 mg/L 0,04000 71 50-144 LCS (P71-0407-BS1) Prepared: 12/27/17 Analyzed: 12/28/17 Diesel Range Organics 1.51 0.50 mg/L 2.000 75 53-135 Surrogate: o-Terphenyl 0.0285 mg/L 0,04000 71 50444 LCS Dup (P7L0407-BS01) Prepared: 12/27/17 Analyzed: 12/28/17 Diesel Range Organics 1.58 0.50 mg/L 2.000 79 53-135 5 20 Surrogate: o-Terphenyl 0.0275 mgA. 0.04000 69 50-144 This repon should not be reproduced, except in its entirety, without the written consent of Prism Laboratories.. Inc. .i 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 I Phone: 7041529-6364 - Toll Free Number: 1.800/629-6364 - Fax: 704/525-0409 Page 5 of 7 AP'RISM �9u res .c Full -Service Analytical A Environmental Solu Gem Level II QC Report 1 /9/18 Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Analyle Project: 2017 Stormwater Prism Work Order: 7120401 Time Submitted: 12/21/2017 3:00:00PM Project No: NCS000183 Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7L0389 - NO PREP Blank (P71-0389-BLKt) Prepared & Analyzed: 12/22/17 Total Suspended Solids BRL 5.0 mg/L LCS (P7L0389-BS1) Prepared & Analyzed: 12/22/17 Total Suspended Solids 470 5.0 mg/L 477,0 99 90-110 Batch PBAD080 - NO PREP Blank (P8A0080-BLK7) Prepared & Analyzed: 01/08/18 Oil & Grease (HEM) BRL 5.0 . mg/L LCS (P8A0080-BS1) Prepared & Analyzed: Ot/08/18 Oil & Grease (HEM) 35.0 5.0 mg/L 40.00 88 78-114 Matrix Spike (P8A0080-MS1) Source: 7120401-01 Prepared & Analyzed: 01/08/18 Oil & Grease (HEM) 42.4 5.0 mg/L 47.06 BRL 90 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final DatelTime 7120401-01 P710407 970 mL 1 mL 12/27/17 10:59 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 7120401-01 PBA0007 5 mL 5 mL 01/02/18 15: 10 This report should not be reproduced.. except in its entirety, without the written consent of Prism Laboratones, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364-Toll Free Number: 1-800/529-6364- Fax: 7041525-0409 Page 6 of 7 I, ..,. :. Anal V�� ".i }.-.-vae�n nint2li SOIUiipr,5 PAGE �. .OF II! Client Physical Address Phone !_,. (_ t(=l 1' 1 i — Faxx�—l� •1 _ - P.O.S/Billing Reference _._!.�(-:-(- WASTEWATER CHAIN OF CUSTODY RECORD 449 Spiingbrook Road e Charlotte, NC 28217 P.O. Box 240543 � Charlotte, NC 282 4 0543 Phone:704l529-6364 a Fax 704/525-0409 REPORT TO: Name .--� Address K BILL TO: Name J Address �" U Requested Due Dale U Sanpler INTACT I. pon arrrv1l9 Received ON WEI CE?rLnp PROPER PRESERVATIVES indiCited! Received WITHIN ROl01NG TIMES? CUS 1O iY SEAT$ IN rAGT? VOLA PILES r , 0 W/Ol.11HL-ADSPACE.7 PROPEI, CON rAINERS used? State Certification YFPr NO N/A Requested NC Z. SC_. Other _._NA Water Chlorinated Yes — No i_ NA —. Sample Iced Upon Collection Yes No — CMUD—.—.—NPDES ^�.— OTHER -.--.- Project Name— I..- SAMPLE TYPE CONTAINER TYPE AND SIZE (ML) laor:ncrcr,.�­­ PRESERVATIVES USED .... ........._........-_.-_.___, ANALYSES TO BE PERFORMED ON THE SAMPLES SUB LAB CERT. PRISM LAB CLIENT SAMPLE I.D.NH3`-� Comp Grab Plastic Glass 01her None Iced HCI NaOH HNO3 FIeSO4 pH BOD TSS Cu Pb Ni Ag Zn O&G CN- as N (Y 'J C4 ID NO. 10 NO. Fi. I -- % x - - - -- -- -- - --� (crc.5 r>r-,f� r I - - - ---- - -- -- =- -- X Sampler's Signature=•!— -4- Jle lohoi ..— - --.... Sampled By (Print Name) ---—.------- -- — -- 41- Composite Type: FLOW TIME HAND (circle one) Start Date & Time for Composite Sampler:_ / / His St op Date& Time for Composite Sample: _--- I __ / —___ .—.—.— Hrs Dale & Time Composite Sample Collected:__ _ / _—! _-- — _ His -Total Hours Composite Collected Over: —_ Hours. End Flow: —_—._ Gal / Cu Feet Start Flow:_ (circleone) Total: — ..---- Affiliation_U� � ' �_7?C.`e r:•.- Additional Comments: Pipe 4 _ A-i �I:fYj -7 i Date & Time Grabls) Taken: / -� U I ! 4 " U Hrs. Field pH Meter Calibrated: Yes _ No_ —_- Field pH Result: _—.—_ _ Analyst's Initials:._—._-- Field Temp. ResuB: Analyst's Initials: --_. Sampler Interrupted: Yes No —. If Yes, Why?_-- --- RSC • ,Chemical Solutions L� a division of Radiator Speclohy Company September 14, 2017 Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Report Radiator Specialty Company Radiator Road, Indian Trail, -North Carolina NPDES Permit No. NCS000183 Dear Sirs: Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outfall Monitoring Report for monitoring period Year 8 — Period 2 as required by Part ❑I Section E.(1.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely. Radiator Specialty Company 0- 1( Stuart A. Kerkhoff. CHM� Environmental Health and Safety Manager Attachments SI'K M" 2% 1 WR8 PD2-2017C V 1. 1. DOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscbrands.corn STORM WATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS NCS000183 FACILITY NAME Radiator Specialty Company PERSON COLLECTING SAMPLE(S) Stuart Kerkhoff CERTIFIED LA13ORATORY(S)_Prisnt Laboratories, Part A: Specific Monitoring Requirements Ine._Lab 4402. Lab # SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY %Union P /J E�L/ /� 84?j 815 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall Date- 50050 Total No. Sample Collected Total : Flow (if-app.) Total Rainfall Suspended. Solids Oil and ; Grease TPH, DRO TPH GRO) PH, mo/dd/vr MG inches m /L m /L. - m'/L m 7L Units - -" - 003 2/15/17 NA 0.56 <100 <30 <1.0 <0.20 6.99 001 2/15/17 NA 0.56 <100 <30 <1.0 <0.20 6.62 004 4/24/17 NA 3.20 <100 <30 <0.50 <0.20 6.72 002 4/24/17 NA 3.20 <100 <30 <0.52 <0.20 6.84 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes Xno (ifyes, complete Part 13) Part 13: Vehicle Maintenance Activitv Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 F, 00530 00400:;". Total Flow - (if applicable) , Total Rainfall Oil & Grease (if appl:)- Non -polar _ O&G/TPH '(Method 1664 SGT-HEM), if Total Suspended Solids PH - New.Motor,. Oil. Usage mo/dd/vr MG inches In /I mg/1 unit - al/mo Form SWU-247, lust revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date 2/15/17 Total Event Precipitation (inches): _O.56 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date 4/24/I7 Total Event Precipitation (inches): _4.52 Event Duration (hours): (only ifapplicable — see permit.) Datc Total I:rent Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of nry knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perntittee) c!11311-) (Date) Form SWU-247, last revised 21212012 Page 2 of 2 1! i /PRISM ®"' � ©taeonprORES INC. Radiator Specialty Cc Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 NC Cenific Lion No. 402 Full -Service Analytical 8 NC Drinking Water Can No, 37735 Environmental Solutions SC Cenification No. 99012 Project: 2017 Slormwater Project No.: NCS000183 Lab Submittal Date: 02/16/2017 Prism Work Order: 7020332 Case Narrative 03/02/2017 G�fPG'�C^ MAR - o 2017 ID This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MOIL with values between MOIL and reporting limit indicated with a J. This report should not be reproduced except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Spnngbrook Road - P.O. Box 240543 - charlotte, NC 28224.0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525-0409 Page 1 Of 8 V� P� o I ` I Fulltr envied al Analytical s J Environmental Solutions - w�wurones n+c Sample Receipt Summary, 03/02/2017 Prism Work Order: 7020332 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 003 001 7020332-01 7020332-02 Water Water 02/15/17 02/15/17 02/16/17 02/16/17 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, mthoul the ontlen consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 2 of 8 PRISM rn „,1n 4 Env mnntm Soiminns o,a Laboratory Report 03/02/2017 Radiator Specialty Co Project: 2017 Stormwater Client Sample ID: 003 Attn: Stuart Kerkhoff Prism Sample ID. 7020332-01 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7020332 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 02/15/17 08:31 1 Time Submitted: 02/16/17 13:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch - Limit Factor DatelTime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg1L 1.0 0.18 1 '8015C 2/22/17 18:36 ZRC P780401 Surrogate Recovery Control Limits c-Terphenyl 80% 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 2/21/17 18:36 AND P7130385 Surrogate Recovery Control Limits a.a,a-Tnfl.orotoluene 96 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 1.0 1 '1664B 2127117 9:34 TJV P780495 Total Suspended Solids 27 mg/L 5.0 0.80 1 'SM2540 D 2/21117 12:54 SLS P780390 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 3 of 8 �Po ISM I FmLunm E�� ��,ot 6olurion, Radiator Specialty Co Alin: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: 2017 Stormwater Project No.: NCS000183 Sample Matrix: Water Laboratory Report 03/02/2017 Client Sample ID: 001 Prism Sample ID: 7020332-02 Prism Work Order: 7020332 Time Collected: 02/15/17 08:39 Time Submitted: 02/16/17 13:40 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.18 1 '8015C 2122/17 19:13 ZRC P7B0401 o-Terphenyl 62 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 OA25 1 '8015C 2/21/17 19:04 ANG P780385 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 94 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 1:0 1 '1664B 2127/17 10:07 TJV P7130495 Total Suspended Solids 14 mglL 3.4 0.80 1 'SM2540 D 2121117 12:54 SLS P780390 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 4 of 8 �PS© n r•r R � tI S M I FenNronmen,a$soluio"s Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail. NC 28079 Gasoline Range Organics by GC/FID - Quality Control Level II QC Report 312117 Prism Work Order: 7020332 Time Submitted: 2/16/2017 1:40:o0PM Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7130385 - 5030B Blank (P780385-131-1<1) Prepared 8 Analyzed: 02/21/17 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a.a-Trirluorotoluene 0.0970 mg1L 0.1000 97 57-132 LCS (P7130385-13SI) Prepared 8 Analyzed: 02/21/17 Gasoline Range Organics 1.06 0.20 mg/L 1,000 106 60-138 Surrogate: a.a,a-Trilluorotoluene 0.0920 mg1L 01000 92 57-132 LCS Dup (P7B0385-BSD1) Prepared 8 Analyzed: 02/21/17 Gasoline Range Organics 1.11 0,20 mg/L 1.000 ill 60-138 5 20 Surrogate: a,a,a-Trilluorotoluene 0.0860 mg1L 01000 86 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbroc k Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 5 of 8 �Fi I S M Full -Se -ire Anat r; a ai Sd cal mV,. Radiator Specialty Co Project: 2017 Stormwaler Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Level II QC Repoli 312/11 Prism Work Order: 7020332 Time Submitted: 2/16/2017 1:40:OOPM Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7130401 - 3510C GC Blank (P780401-BLK7) Diesel Range Organics Surrogate. o-Terphenyl LCS(P7B0401-BS1) Diesel Range Organics Surrogate: o-Terphenyl LCS Oup(P7B0401-BSD1) Diesel Range Organics Surrogate: o-Terphenyl Prepared & Analyzed: 02/22/17 BRL 1.0 m /L 0.0296 mg/L 0.04000 74 50-144 Prepared & Analyzed: 02/221/7 1.87 1.0 mg/L 2.000 94 53-135 0.0332 r mg/1- 0.04000 83 50-144 Prepared & Analyzed: 02/22/17 2.21 1.0 mg/L 2,000 110 53-135 16 20 0,0368 mg/L 0.04000 92 50-144 This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543.- Charlene, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 6 of 8 Full, Seance Analytical a e�. Radiator Specialty Co _ Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail. NC 28079 General Chemistry Parameters - Quality Control Analyze Project: 2017 Stormwater Project No: NCS000183 Reporting Result Limit Units Level II QC Report 3/2/17 Prism Work Order: 7020332 Time Submitted: 2/16/2017 1:40:OOPM Spike Source %REC RPD Level Result %REC Limits RED Limit Notes Batch P7BO390 - NO PREP Blank (P7B0390-BLK7) Prepared & Analyzed: 02/21/17 Total Suspended Solids BRL 5.0 mg/L LCS (P7B0390-BS1) Prepared & Analyzed: 02/21/17 Total Suspended Solids 480 So art 477.0 101 90-110 Batch P7130495 - NO PREP Blank (P7B0495-BLK7) Prepared & Analyzed: 02/27/17 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P7130495-BS-I) Prepared & Analyzed: 0227/17 ' Oil & Grease (HEM) 33.7 5.0 mg/L 40,00 84 78-114 Duplicate(P7B0495-DUP1) Source: 7020332-01 Prepared & Analyzed: 02/27/17 Oil 8 Grease (HEM) BRL 5.0 mg/L 1.24 18 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Dalemme 7020332-01 P780401 1000 mL 1 mL 02/22/17 9:00 7020332-02 P780401 1000 mL 1 rnL 02/22/17 9.00 Prep Method: 5030E I Lab Number Balch Initial Final Daterrime 7021 P7130385 5 mL 5 mL 02/21/17 14.26 7020332-02 P7B0385 5 mL 5 mL 02/21/17 14:26 This repon should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 7'of 8 CHAIN OF CUSTODY RECORD YES NO NIA Samples INTACT UPOT1 arrival'? Zz, P R I S M! E,,-rori ScAutio,IS PAGE I OF __ QUOTE # TO ENSURE PROAR BILLING: Project Name; tA 1, " Lit, Rec.,ed ON %VF T ICE? P! ionc . 1041529-636.1 Frx: 70415254),109 Short Hold Analysis: (Yes) (I)< LIST Project: (Yes) (rV PROPER PRESERVATIVES irtnicdt�d? 0 *Please ATTACH any project specific reporting (QC LEVEL 111111 IV) Receiveo WITHIN HOLDING TIMES9 M Client Company Name, Provisions and/or CC Requirements CUSIODY SEALS INTACT? Invoice To: 4(' Phone: Fax'Yesj (N.4): Purchase Order NodBilling Reference 0 Q TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Addre J Requested Due Date 0 1 Day CI 2 Days 0 3 Days 0 4 Days 0 5 Days Certification: NELAC DOD FIL NC �Z EDD Type; PDF I/ Exce�I_Othher "Working Days" 0 6-9 Days "reard 10 days (3 Rush Work Must Be Sit., Location Name: i� �( Pre -Approved Samples received aller 14:00 will be processed next business day. SIC OTHER N/A Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays, Water Chlorinated: YES— NO m C_ (SEE REVERSE FORTERMS & CONDITIONS REdARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES --�NO TIME MATR SAMPLE CONTAIN ANALYSIS REQUESTED SAMPLE DESCRIPTION COLLECTED mILI TARY WATER OR TIVES REMARKS 2,/, SM LA TYPE URS SLUDGE SIZE ID N7 IT Sampler's Signature Abm,,,J� I Sampled By (Print Name) S � I Affiliation PL�. ilj.. Upon re I inqu is hing, this Chain of C us tody*'your aWhorizati on for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Projec anager. There will be charges for any changes after analyses have been initialized. od ol Sh,pment NOTE: ALL SAMPLE COOLERS SHOULD HE TAPED SHUT Wilih CU51OVY St� . L. 'OR IHANSPORTATION TO 1111ti _AIJU�TUKY. UU Ul..p N., SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CoC UNTIL RECEIVED AT THE LABO"TORY. mpocu: vor sxnomnmoA/Ex: DRINKING WATER: un�ovv*xrE: nunA: osncLa |Lxwop/LL ornsn: cr"NC OSC| UwC oSC| owu �SC | uwC oSC | �wC qSC | owC�oC| UwC OSC; Owc OSc|��wC Q SC o �-----|o-------| 0-| Q | o- o—.---_� o_'-----iEl tl_—_�-- *CONTAINER TYPE CODES: x=Amber r=Clear G=Glass p=Plastic: Tz=Teflon-Lined Cap VOA =uuoueo�aoipAnalysis (Zero Head Space) ill A-�INR I S M l d®tABOaATOBIES INa Radiator Specialty Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Full -Service Analytical 8 Environmental Solutions Mll LJ LS MAY i 0 2017 NC certification No. 402 NC Drinking Water Cen No. 37735 SC Certification No. 99012 Project: 2017 Stormwater Project No.: NCS000183 Lab Submittal Date: 04/25/2017 Prism Work Order. 7040466 Case Narrative 05/09/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. �' Cara C. Rusmisell Project Manager Data Qualifiers Key Reference G� Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Pnsm Labormones. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1.8001529.6364-Fax: 7041525-0409 Page 1 of AMR.isM ` °""°A° Sample Receipt Summary, E .,re�me�tal s l,t,e�s 05/09/2017 Prism Work Order: 7040466 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 004 7040466-01 Water 04/24/17 04/25/17 002 7040466-02 Water 04/24/17 04/25/17 Samples were received in good condition at 1.9 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 2 0f 8 e^ Laboratory Report /42 v' --r R I S M BS,Bg,2D,7 Radiator Specialty Cc Project: 2017 Stormwater Client Sample ID: 002 Attn: Stuart Kerkhoff Prism Sample ID: 7040466-02 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7040466 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 04/24/17 08:25 Time Submitted: 04/25/17 15:15 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date[Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 0.52 0.19 1 '8015C 4I28/17 15A9 ZRC P7D0446 Surrogate Recovery Control Limits o-Terphenyl 82 % 50./44 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 5/8/17 1235 ANG P7E0120 Surrogate Recovery Control Limits a,a,a.Tnfluorololuene B9 % 57-132 General Chemistry Parameters Oil& Grease (HEM) BRL mg/L 5.0 0.98- 1 '1664B 518117 11:05 TJV P7E0138 Total Suspended Solids 20 mg/L 12 0.80 1 'SM2540 0 4128117 9:59 SLS P700493 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Frce Number: 1-8001529-6364 - Fax: 7041525-0409 Page 4 Of 8 ®P'R I S M Env o mental 5olullons Laboratory Report 05/09/2017 Radiator Specialty Co Project: 2017 Stormwater Client Sample ID: 004 Attn: Stuart Kerkhoff Prism Sample ID: 7040466-01 600 Radiator Rd. Project NO.: NCS000183 Prism Work Order: 7040466 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 04/24/17 08:08 Time Submitted: 04/25/17 15:15 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateTme ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 0.50 0.18 1 'SOiSC 4128117 14:35 ZRC P7D0446 Surrogate Recovery Control Limits c-Terphenyl 66 % 50-144 Gasoline Range Organics by GC/FID - - Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 518/17 12:07 ANG P7E0120 i - Surrogate Recovery Control Limits a,a,a-TnfIuorotoluene 92 % 57-132 General Chemistry -Parameters - OilB Grease (HEM) BRL mg/L 5.0 0.98 1 '1664B 5/8/17 10:29 TJV P7E0138 Total Suspended Solids 6.1 mglL 2.6 0.80 1 'SM2540 D 4/28117 9:48 SLS P7D0490 This report should not be reproduced, except in its enbrery,'without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number 7-800/529.6364 - Fax: 704/525-0409 Page 3 of 8 ' IS,M . F„ o m 4oaiyu[a 4 FG—dcn� rai sowuo„: Dv. Radiator Specialty Co Project: 2017 Stormwater AUn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail. NC 28079 Gasoline Range Organics by GC/FID - Quality Control Reporting Result Limit Units In Level II QC Report 519/17 Prism Work Order: 7040466 Time Submitted: 4/25/2017 3: 15:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7E0120-BLKI) __—..-_.. _._. _... _ ... ..... ...... _ Prepared & Analyzed: 05/08/17 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Trl/luoretoluene 0.100 mall 0.1000 100 57-132 LCS (P7E0120-BS1) Prepared & Analyzed: 05/08/17 Gasoline Range Organics 0.933 0.20 mg/L 1.000 93 60-138 Surrogate: a,a,a-Trilluoronnoene 0,0820 mg/L 01000 82 57-132 Matrix Spike (P7E0120-MS1) Source: 7040466-01 Prepared & Analyzed: 05/08/17 Gasoline Range Organics 1.09 0.20 mg/L 1.000 0.0430 104 69-130 Surrogate: a,a,a-Tniluorotoluene 0.0860 1. mg/L 0.1000 86 57.132 Matrix Spike Dup (P7E0120-MSD1) Source: 7040466-01 Prepared & Analyzed: 05/08/17 Gasoline Range Organics 1.25 D.20 mg/L 1.000 0.0430 121 69-130 14 24 Surrogate: a,a.a-Trilluorotoluene 0.107 mglL 01000 107 57-132 This report should not be reproduced, except in its entirety, without the wntten consent of Prism Laboratories, Inc. a 449 Springbrook Read - P.O. Box 240543 - Charlotte, INC 26224.0543 Phone: 7041529.6364 - Toll Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 5 of 8 1 service Anaiyrcni en.,,onmen,a 60 ,.enP�M ua Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Analyte Reporting Result Limit Units Level If QC Report 5/9%17 Prism Work Order: 7040466 Time Submitted: 4/25/2017 3:15:00PM Spike Source oREC RPD Level Result %REC Limits RPD Limit Notes Blank (P71)(1446-BLKI) Prepared: 04/27/17 Analyzed: 04/28/17 Diesel Range Organics BRL 0.50 mg/L Surrogate: o-7erpheny/ 0.0283 mg/L 0,04000 7/ 50-144 LCS(P7D0446-BSI) Prepared: 04/27/17 Analyzed: 04/28/17 Diesel Range Organics 1.74 0.50 mg/L 2.000 87 53-135 Surrogate: o-Terphenyl 0.0451 ri 0.04000 113 50-144 LCS Dup (P7D0446-13SDI) Prepared:_ 04/27/17 Analyzed: 04/28/17 _ Diesel Range Organics 1.76 0.50 mg/L 2.000 88 53-135 1 20 Surrogate: o-Terphenyl 0,0432 mg/L 0,04000 108 50-144 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springl rook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 11-8001529.6364 - Fax: 7041525-0409 F Page 6 of 8 Pa Fniien AnalyticalI S M I Environmental soluionst�d•.ue♦m ra xr. Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Duality Control Analyle Batch P7D0493 - NO PREP Project: 2017 Storrnwater Project No: NCS000183 Reporting Result Limit Units Level II QC Report 5/9117 Prism Work Order: 7040466 Time Submitted: 4/25/2017 3:15:OOPM Spike Source %REC RPO level Result %REC Limits RPD Limit Notes Blank (P7DO493-BLK1) Prepared 8 Analyzed: 04/28/17 Total Suspended Solids BRL 5.0 mg/L LCS (P7DO493-BS1) Prepared 8 Analyzed: 04/28/17 Total Suspended Solids 470 5.0 mg/L 47TO 9B 90-110 Duplicate (P7DO493-DUP1) Source: 7040466-02 Prepared 8 Analyzed: 04/28/17 Total Suspended Solids iB 5.0 mg/L 20 5 20 Batch P7E0138 - NO PREP Blank(P7EO138-BLK1) Prepared 8 Analyzed: 05/08/17 Oil 8 Grease (HEM) BRL 5.0 mg/L LCS (P7E0138-BS1) Prepared 8 Analyzed: 05/08/17 Oil& Grease (HEM) 35.2 5.0 mg/L 40,00 BB 78-114 Sample Extraction Data Prep Method: 351DC GC Lab Number Batch Initial Final Daterrime 7040466-01 P7D0446 1000 mL 1 mL 04/27/17 er55 7040466-02 P7D0446 960 mL 1 mL 04/27/17 er55 Prep Method: 5030E Lab Number Balch Initial Final Daterrime 7040466-01 P7E0120 5 mL - 5 mL 05/08/17 8:07 7040466-02 P7EO120 - 5 mL 5 mL 05/08/17 8:07 This report should not be reproduced. except in its entirety, without the written consent or Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlene, NC 28224-0643 Phone: 704/529-6364- Toll Free Number: 1-8001529-6364 - Fax: 7041525-D409 Page 7 of 8 rrrr���+++p a CHAIN OF CUSTODY RECORD -ppa��^+�yy'gLr^ya.i9 �/)�� Full -Service Analytical C p�5"., Q/ Y tl i Environmental Solutions PAGE— OF_ QUOTE a TO ENSURE PROPER BILLINGr — `p-yy 449 Spri lgnrook Rued • Charlotte, NC 28217 Project Name:' 'J 'N i"n,1 c• Kam' 1 i �y`� �ojecet: (Yes) (NO) f Phan. 7Ga1525-Glen - Fax: 7041525-0409 Short Hold'Analysls: (Yes) (No) UST Pr 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) Client Company Name: Zc,rl:'c', ie! o «�� �' < <� . provisions and/or CIC'Requirements , Report To/Contact Name' S hnoi �$-('l-, F' _ Invoice To: yi cL{` r: t S�e J Reporting Address: (; V !Z ,a rv+�- 17 ar :! Address: i- C'It 12 'n L,- Z T`_ A,, T�..�I NI, �F.0 )(i r 1 ! .I nrf ')(%u lG . Sadlples INTACT upon arrival? y _ Received ON WET ICE?' O PROPER PRESERVATIVES indicated? Receivad WITHIN HOLDING TIMES? '� C, m . - CUSTODY SEALS INTACT VOI.ATILES reed W/OUT HEADSPACE? PROPER CONTAINERS Used? TEMP'/'hewn lUT T--J Observed:-j_,(. "C/Cui, Phone: (. •i • (k+ 1- Fax Yes) purchase Order No./Billing Reference 4/ S 11 C7 Cl 1 3 S TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: �dt�")�`�' (<'�')(+'J%�l, jv % Requested Due Date O l Day ❑2Days 03 Days'U4 Days 05 Days Certification: NELAC_ DoD_ FL_ NC EDD Type: PDF yvy Excel Other "Working Days" U 6-9 Days er!�tandard 10days Dpre h Work Must Be pproved SC OTHER NIA Site Location Name: 7 (. Samples received after 14:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO .f Site Location Physical Address: •� [ (SEE REVERSE FOR TERMS a CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES /NO P P RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) — TIME MATRIX SAMPLE CONTAINER � PRESERVA- ANALYSIS REQUESTED � PRISM NT 7SAMPLE DATE COLLECTED (SOIL TIVES L"F Vr y'y tti / j' r� REMARKS LAB -TYPE CRIPTION COLLECTED MILITARY WATER OR l NO. SIZE .� t t'l ID NO. HOURS SLUDGE)' SEE BELOW I `((2`+lI7 k�_uY �✓ I i�C i-_L L`cz 14c( _ _C,r:.l, 01--- - Grc.ir 1- C f"A< 1_ Sampler's Signature �•'f% /0: Sampled By (Print Name) irivcJ- I�g �tj"1o1�- I Affiliation G .:, . /J_ �.. Upon relinquishing, this Chain of Cu,;OTy is your authorization for Prism to proceed with the analyses as requested above. Any changes must be �•' submitted in writing to the Prism Pr lect Manager. There will be charges for any c gas after analyses have been initialized. - Rein tmd Y I awre) "/ Received By: (Slgnalure) Data Mi ilarylHours Additional Comments: Si;o Arrival Tirna' 00 ff Date Sile Depadura TIn1a'. Relinquished By: (a7 Received By'. (Signature) Relinquished By: (Stgnalure) Received For P La lori f y: Dale [ . Field /ech Fee: Method of Shipment'. NOTE' ALL SAMPLE COOLE SHOVED BE TAPED SHUT WIT USTOD SEALS FOR TRANSPORTATION TO THE LABORATORY. CO rwp No RECEIVED THE LABORATORY. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL AT ❑ Fed Ex ] UPS ❑ Haw delivered QPeftm Field Service ❑ Other_ NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: ,CERCLA LANDFILL OTHER: 13NC 0 SC ® NC O SC ❑ NC ❑ SC O NC ❑ SC 13 NC ❑ SC O❑ NC O SC ❑O NC ❑ SC O NC ❑ SC 0 NC ❑ SC13 'CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) Chemical Solutions a division of Radiator Specialty Company March 24, 2017 Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Report Radiator Specialty Company Radiator Road, Indian Trail, North Carolina NPDES Permit No. NCS000183 Dear Sirs: RECEIVED MAR 3 0 2017 CENTRAL FILES DWR SECTION Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outfall Monitoring Report for monitoring period Year 8 — Period 1 as required by Part III Section E.(I.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company Stuart A. Kerkhoff, CHMM l/ Environmental Health and afety Manager Attachments S I MWA'IlYR8PDI-2017CVL'rDOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscldrands.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCSNCS000183 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Radiator Specialty Company PERSON COLLECTING SAMPLE(S) Stuart Kerkhoff CERTIFIED LABORATORY(S) _Prism Laboratories, Inc._Lab #_402 Lab # Part A: Specific Monitoring Requirements COUNTY Union PHONE NO: L�4 /,&T C.,Fdll// ISIGNATURE OF PERMITTEE OR DESIGNEE I REQUIRED ON PAGE 2. Outfall'_ Date" 50050 Total ;; 3, �`.._ ."�.x a s ,x!u.e< r No.Sample -Total Collected Flow' if a Totul ,',,--Suspended Rainfall - Solids Oil andsv Crease 4`�R x *$.'-,d'.. ' TP,H DRO s- kf P.H' GRO)i` _. nio/dd/vr, `, MG - inches m /L =,,; 003 10/7/16 NA 3.95 <100 <30 <1.0 <0.20 6.91 001 10/7/16 NA 3.95 <100 <30 <I.0 <0.20 6.90 002 1/23/17 NA 2.18 <I00 <30 <I.0 <0.20 6.51 004 1/23/17 NA 2.18 <100 <30 <1.0 <0.20 6.55 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X_no (if yes, complete Par B) Part R: Vehicle Maintenance Activitv Monitoring Requirements Outf�ll Date- 50050. :<" d00556fi,1,0)a 'ua•t 1100530=00400.= p a* ,. #s :(7.:' No. Sample Total Flow. y Totaf:x'4 �Od &Grease tNon polar Total fpH New Motot " �, , 5 .F s'��:ti za•�vwya .=+^ - iCsrar Collected _ (if applicable) Rainfall (tf apply OS ClTPH' �Suspehded ' Od Usage& `i , y� t Y�� y (IVlethod 1664 .Solids r - -mo/dd/ r.` .;MG- . .' inches , `:p; m /I.,:�ir`rJ'.E,'-., - aV M -i rii%L .. „ , .. , fuiirt,R.. -* `?Rtw aUn o t7, Form S W U-247, last revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date _10/7/16 Total Event Precipitation (inches): _3.95 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date 1/23/17 Total Event Precipitation (inches): _2.18 Event Duration (hours): (only if applicable — see permit.) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable —see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ll,t,tlt/ I (Signature of Permittee) 3 23 1� (Date) Form SWU-247, last revised 21212012 Page 2 of 2 7r dimisM �©LABOFATOFIM INC. Radiator Specialty Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail. NC 28079 NC Certification No. 402 Full -Service Analytical 8 NC Drinking Water Cert No. 37735 Environmental Solutions SC Certificelion No. 99012 Project: 2016 Slormwater Project No.: NCS000183 Lab Submittal Date: 10/07/2016 Prism Work Order: 6100179 Case Narrative 10/21/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are (lagged individually on each sample. A key reference for the data qualifiers pears�t t this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference OCT 27 2016 D Reviewed By Cara C. Rusmisell Project Manager MI Matrix spike outside of the control limits. Matrix interference suspected. BRL Below Reporting Limit MOIL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MOIL and reporting limit indicated with a J. This repel should not be reproduced.. except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone' 704/529.6364-Totl Free Number: l-800/529-6364- Fax: 704/525-0409 Page 1 of ®hk ISM I E=nn vice al Slyhoai a F 11-Semnm nl Sotical& �7L. —T. n&-c Sample Receipt Summary 10/2112016 Prism'Work Order: 6100179 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 003 6100179-01 Water 10/07/16 10/07/16 001 6100179-02 Water 10/07/16 10/07/16 Samples were received in good condition at 1.3 degrees C unless otherwise noted. 11 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364- Toll Free Number: l-8001529-6364-Fax : 7041525-0409 Page 2 of 8 Laboratory Report m r- Full-Scrvicc Analytical 0Pa-. A 8 R I SqM 6n�,roAm��to, 6ol�tion, RE 0/21/2018 Radiator Specialty Cc Project: 2016 Slormwater Client Sample ID: 003 Attn: Stuart Kerkhoff Prism Sample ID: 6100179-01 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 6100179 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 10/07/16 10:20 Time Submitted: 10/07/16 15:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dale/Time 10 Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.18 1 '8015C 10/13/16 15.17 ZRC P6J0216 Surrogate Recovery Control Limits o-Terphenyl 114 % 50-144 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 10/18/16 16:17 ANG P6J0314 Surrogate Recovery Control Limits a,a,a-TdOuorololuene 116 % 57-132 General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 1.0 1 '1664B 10/17/16 1100 TJY P6J0288 Total Suspended Solids 18 mg/L 2.6 0.80 1 'SM2540 D 10/13/16 15:42 SLS P6J0227 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Boa 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 3 0( 8 Laboratory Report oFull-ServiceAnalytical I��R I S M I 4 Environmnta 6olntions 10/21/2016 et Radiator Specialty Cc Project: 2016 Stormwater Client Sample ID: 001 Attn: Stuart Kerkhoff Prism Sample ID: 6100179-02 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 6100179 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 10/07/16 10:32 Time Submitted: 10/07/16 15:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GCIFID Diesel Range Organics BRL mg/L 1.0 0.18 1 '8015C 10/13/16 1691 ZRC P6J0216 Surrogate Recovery Control Limits - o-Terphenyl 90 % 50444 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 10/18/16 16:45 ANG '' P6J0314- Surrogate Recovery Control Limits a,a,a-Tdfluorotoluene 101 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 1.0 1 '1664B' - 10/17/16 1129' TJV 'P6J0288 Total Suspended Solids BRL mg/L 2.6 0.80 1 'SM2540 D 10/14/16 11:05 SLS P6J0267 This report should not be reproducedexcept in its entirety. without the written consent or Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-0409 Page 4 of 8 4♦f. �P'R I S M I Fu0 Service Analytical 6 E�v„onmerrat sot„r,on, Level II QC Report 10/21/16 Radiator Specialty Co Project: 2016 Stormwater Prism Work Order: 6100179 Attn: Stuart Kerkhoff Time Submitted: 10/7/2016 3:10:00PM 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6J0314 - 5030B Blank (P6J0314-BLK1) Prepared & Analyzed: 10/18/16 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Tritluorotoluene 0.114 mg1L 0.1000 114 57-132 LCS (P6J0314-BS1) Prepared & Analyzed: 10/18/16 _ Gasoline Range Organics 1.11 0,20 mg/L 1.000 ill 60-138 Surrogate: a,a,a-Tnlluorotoluene 0,0870 mgA- 0.1000 87 57-132 LCS Dup(P6J0314-BSD7)_ _ Prepared&Analyzed. 10/18/16 Gasoline Range Organics 1.23 0.20 mg/L 1.000 123 60-138 10 20 Surrogate: a,a,a-Trifluorotoluene 0,0930 mg1L 0.1000 93 57-132 This report should not be reproducedexcept in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525-0409 Page 5 of 8 �P R ISM I Fun,so,moe al Solucai 8 Env- o ee al Swtical & I�OLAM Aronrtc inc Level II QC Report 10/21/16 Radiator Specialty Co Project: 2016 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Analyte Batch P6JO216 - 351 OC GC Reporting Result Limit Units Prism Work Order: 6100179 Time Submitted: 10/7/2016 3:10:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P6J0216-BLK1) Prepared & Analyzed: 10/13/16 Diesel Range Organics BRL 1.0 mg/L Surrogate: o-Terphenyl 0.0508 mg/L 0.04000 127 50-144 LCS (PGJ0216-BS1) Prepared & Analyzed: -------- Diesel Range Organics 1.78 1.0 mg/L 2.000 89 53-135 Surmgele: o-Terphenyl 0,0418 mg/L 0.04000 105 50-144 LCS Dup (P6J0216-BSD1) Prepared & Analyzed: 10/13/16 Diesel Range Organics 1.89 1.0 mg/L 2.000 94 53-135 Sunogafer o-Terphenyl 0.0366 mg/L 0,04000 91 50-144 Matrix Spike (P6J0216-MS1) Source: 6100179-01 Prepared & Analyzed: 10/13/16 Diesel Range Organics 3.44 2.0 mg/L 4.000 BRL 86 51-145 Surrogate: o-Terphenyl 0.0720 nrl 0,08000 90 50-144 Matrix Spike Dup (P6J0216-MSD1) Source: 6100179-01 Prepared & Analyzed: 10/13/16 Diesel Range Organics 3.67 2.0 mg/L 4.000 BRL 92 51-145 Surrogate: o-Terphenyl 0.0732 mg1L 0.08000 92 50-144 6 20 7 22 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. _ 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364. Toll Free Number: 1-800/529-6364-Fax: 704/526-0409 Page 6 of 8 A n I `-Pn n FUILSucr nice Analylical8 n J' V' Env oeLA alytewnc Level II QC Report 10/21/16 Radiator Specialty Cc Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Analyle Batch P6J0227 - NO PREP Project: 2016 Stormwater Project No: NCS000183 Reporting Result Limit Units Prism Work Order: 6100179 Time Submitted: 10/7/2016 3:10:00PM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes Blank (P6J0227-BLK1) Prepared & Analyzed: IOlt 3116 Total Suspended Solids BRL 5.0 mg/L LCS (P6J0227-BS1) Prepared & Analyzed: 10/13/16 Total Suspended Solids 480 5o mg/L 477.0 102 90-110 Batch P6J0267 - NO PREP Blank (P6J0267-BLK1) Prepared & Analyzed: 10/14/16 Total Suspended Solids BRL 5.0 mg/L 'LCS (P6J0267-BSI) Prepared & Analyzed: 10/14/16 Total Suspended Solids 480 5.0 m /L 477o 101 90-110 Batch P6J0288 - NO PREP Blank (P6J0288-BLK1) Prepared & Analyzed: 10/17/16 Oil & Grease (HEM) BRL 5.0 mglL LCS (P6J0288-BS1) Prepared & Analyzed: 10/17/16 Oil & Grease (HEM) 33.9 5o mg/L 40.00 85 78-114 Matrix Spike (P6J0288-MSI) Source: 6100179-02 Prepared & Analyzed: 10/17/16 Oil & Grease (HEM) 36.8 5.0 mg/L 44.94 2.25 77 78-114 MI Prep Method: 3510C GC Lab Number Balch Initial Sample Extraction Data Final Date/Time 6100179-01 _ P6J0216 1000 mL 2 mL 10/13/16 9:10 6100179-02 P6J0216 1000 mL 2 mL 10/13/16 9,10 Prep Method: 5030E Lab Number Balch Initial Final Dale/Time 61OD179-01 P6J0314 5 mL 5 mL 10/18/16 12:18 6100179-02 PGJ0314 5 mL 5 mL 10/18/16 12,18 This report should not be reproduced. except in its entirety, without the written consent or Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 _, Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 7 of 8 Full -Service Analytical :3 _ py� Environmental Solutions "PRISM wr, 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6!3,64 • Fax: 7041525-0409 Client Company Name: IC P• ((1f-rtJ 1r?:'r i o, r'fY Report To/Contact Name: Reporting Address L L C Z i p .: Ivy. 1t•,c, d CHAM :OF CUSTODY RECORD PAGE_ OF — 01UOTE Is TO ENSURE PROPER BILLING: .Project Name: S 'kj rM L'J r.if,% LI/f, y ill I Short Holci Analysis: `(Yes) '.(l$l< UST Project: (Yes) "Please ATTACH any project specific reporting (QC LEVEL 111111 IV) provisions and/or QC; gR..equi))rements --Invoice To: ' / i i�� 1C,ti I',("- Address: (, 00 2L4, (J YES NC I.1F. 00 Samples INTACT upon on ival7 _ / w O Received OfJ JVr l ICI3? 00 PROPER FRk SFhJNI'I 'E� u J ":" ,/' , N RtcaivedWI-I iIN IULEM Jt, TIM / _ O a CUSTODY SFA:.S INL'-,.^'t" vourr I I r � i un rir a t< _.. PROPER c UNIAIN=n us. , T4 MP' I I.nr 1F1 ��-3� .',I 1 Li ` L•.f!]"'_:{ Phone: i. J Lf t ! % F/a), (Yes) (N�: Purchase Order No./Billing Reference i/ \ O0 LI 3 (, C; TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: N kt ` )tl• oh/ L' Y 1L Ij,'.',, Cl •i. C �M Requested Due Date El 1 Day ❑ 2 Days ❑ 3 Days O 4 Days ❑ 5 Days Certification: NELAC DOD_ FL_ NC t✓ EDD Type: PDF L.' Excel Other "Working Days" ❑ 6-9 Days FASrandard 10 days 0 Rush re h Work Mdust Be SC OTHER NIA Site Location Name: Samples received after 14:00 will be processed next business day. — Site Location Physical Address: G 1� hr. ; (, c-, to.- P rl Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO ✓ (SEE REVERSE FOR TERMS B CONDITIONS REGARDING SERVICES r,fl r.. 1 '.•.t 11(C J % %1 RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES ✓NO CLIENT DATE TIME COLLECTED MATRIX SOIL, SAMPLE CONTAINER PRESERVA- ANALYSIS REQUESTED /" (\� / / REMARKS I PRISM LAB 'TYPE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES j� /�j HOURS SLUDGE) NO.I SIZE - F� j I ID NO. SEE BE LOW V^—} CtC A. C, a ! - c i,,,G ELI �� ( r jr tt /• � ra r �� 11Y ��it'ki,o FJ" :(=kir. r!*- Sampler's Signature � - Sampled By (Print Name)= •-%'iLvGl/h' Affiliation f4o1 - Upon relinquishing, this Chain of Cu4y6y is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Prgl ct Manager. There will be charges for any changes after analyses have been initialized. %'ij ,`x�. �.-.,M. *t r,., •... elt aV;hed`By: ((S7..ture) Received By (Signature) -.„� Date MilitarylHours Additional Comments: r vA hn Relinquished 9y:(SI }10W Received By:(Synaturel Data <:•: Dcu,.r.,ue: hq.,: . Relinqu shed.By' (Signature) ceived r Prism Laeoratories By: - Date' I ...._.. /11 d Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT W CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No, t.__-__._.__... -___._ _ _—____.• SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST ?GIC UNTIL RECEIVED AT THE LABORATORY. {�I i U I ? l 0 Fedd Ex O UPS 0 Hand -delivered �sm Field Service 0 Other `% : FD DEl SCE CiP' O SC O NC O SC ❑ NOCU O SCTER: NC SCATERLl NC ❑ O NC E) SC O NRC El SC ❑ NC SC 0 NC O SC Radiator Specialty Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Full -Service Analytical 8 Environmental Solutions FEB - 8 2017' By NC Certification No. 402 NC Drinking Water Ced No 37735 SC Certification No. 99012 Project: 2017 Stormwater Project No.: NCS000183 Lab Submittal Date: 01/23/2017 Prism Work Order: 7010331 Case Narrative 02/03/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference Reviewed By Cara C. Rusmisell Project Manager 1 Samples for volatiles analysis received with headspace M Matrix spike outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference x Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364-T611 Free Number: 1.800/529-6364 - Fax: 704IS25-0409 Page 1 ci III® I M FW bSarvien al solutions s J Environmental Solutions -aavv. . Sample Receipt Summary 02/03/2017 Prism Work Order: 7010331 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 002 004 7010331-01 7010331-02 Water Water 01/23/17 01/23/17 01/23/17 01/23/17 Samples were received in good condition at 4.7 degrees C unless otherwise noted. a This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 t Phone: 7041529-6364- Toll Free Number: 1-3001529-6364 - Fax: 7041525-0409 Page 2 of 9 I S M environmental al Soiucal 8 Environmenml Solutions ®Vw�woomr6 ixc Laboratory Report 02/03/2017 Radiator Specialty Co Project: 2017 Stormwater Client Sample ID: 004 Attn: Stuart Kerkhoff Prism Sample ID: 7010331-02 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7010331 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 01/23/17 08:15 Time Submitted: 01/23/17 12:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L to 0.18 1 '8015C 1/26/17 15:39 ZRC P7A0384 Surrogate Recovery Control Limits o-Terphenyl 58% 50-144 Gasoline Range Organics by GC/FID 1 Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 2/2117 1933 ANG P780054 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 94 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 to 1 '1664B 211117 9:07 TJY P7130030 Total Suspended Solids 6.2 mg/L 2.5 0.80 1 'SM2540 D 1124117 14:02 SLS P7A0356 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1.8001529-6364 - Fax: 7041525-0409 Page 4 of 9 IR I S M FuibSarvico na0yiical a umn.raney .¢ Environmentnal $Olul1011s Laboratory Report 02/03/2017 Radiator Specialty Co Project: 2017 Stormwater Client Sample ID: 002 Attn: Stuart Kerkhoff Prism Sample ID: 7010331-01 600 Radiator Rd. Project No.: NCS000183 Prism Work Order: 7010331 Indian Trail, NC 28079 Sample Matnx: Water Time Collected: 01/23/17 08:02 Time Submitted: 01/23/17 12:30 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.10 1 '8015C 1/26/17 16:16 ZRC P7A0384 Surrogate Recovery Control Limits o-Terphenyl 54 % 50-144 Gasoline Range Organics by GCIFID 1 Gasoline Range Organics BRL mg/L 0.20 0.025 1 'BD15C 2/2/17 19:05 AND P7130054 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 91 % 57-732 General Chemistry Parameters Oil,& Grease (HEM( 5.3 mg/L 5.0 1.0 1 '1664B 211117 9:07 TJY P780030 Total Suspended Solids 14 mg/L 6.2 0.80 1 'SM2540 0 1/24/17 14:02 SLS P7A0356 This report should not be reproduced, except in its entirety, vnthout the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1.8001529-6364 - Fax: 704/525-0409 Page 3 of 9 APLo I S M I iu -.Senn er ai S01ulrO 4 Environmental Solutions �V.neo-mn,tz '.e Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Gasoline Range Organics by GCIFID - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2/3117 Prism Work Order: 7010331 Time Submitted: 1/23/2017 12:30:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7B0054 - 5030B Blank(P7B0054-BLK1) Prepared & Analyzed: 02/02/17 Gasoline Range Organics BRL 0.20 mg1L Surrogate: a,a,a-TriNuorotoluene 0.0920 mg/L 0,1000 92 57-132 LCS (P7B0054-BSl) Prepared_ & Analyzed: 02/02/17 Gasoline Range Organics 1.14 0.20 mg/L 1.000 114 60-138 Surrogate: a,a,a-Trifluorotoluene 0,0920 ni 0.1000 92 57-132 LCS Dup (P780054.BSD1) Prepared & Analyzed: 02/02/17 Gasoline Range Organics 1.17 0.20 mglL 1.000 117 60-138 2 20 Surrogate: a, a, a-Trifluomfoluene 0.0900 mg/L 0,1000 90 57432 Matrix Spike (P7B0054-MSI) Source: 7010331-01 Prepared & Analyzed: 02/02/17 Gasoline Range Organics 1.11 0.20 mgf- 1.000 BRL Ili 69-130 Surrogate: a,a,a-Trifluorotoluene 0,0870 mg1L - 0.1000 87 57-132 Matrix Spike Dup (P7B0054-MSDI) Source: 7010331-01 Prepared & Analyzed: 02/02/17 Gasoline Range Organics 1.31 0.20 mg/L 1.000 BRL 131 69-130 17 24 M Surrogate: a,a,a-Tnlluomtoluene 0.105 ni 0. 1000 105 57432 This report should not be reproduced, except in its entirely. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 2405431 Charlotte, NC 29224-0543 - Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041S25-0409 Page 5 of 9 ��C~ �n I S M r il-Service Analytical . umn ow a.n Environmental Sotuliona Radiator Specialty Co Project: 2017 Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 Diesel Range Organics by GC/FID- Quality Control Analyte P7AD384 - 3510C GC Reporting Units Level 11 QC Report 213/17 Prism Work Order: 7010331 Time Submitted: 1/23/2017 12:30:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7A0384-BLK1) _ Prepared_B Analyzed: 01/26/17 Diesel Range Organics BRL 1.0 mg/L Surrogate: o-Terphenyl 0.0275 mg/L 0.04000 69 50-144 LCS (P7A0384-BSI) Prepared 8 Analyzed: 01/26/17 Diesel Range Organics 1.96 1.0 mg/L 2.000 98 53-135 Surogate: o-Terphenyl 0.0303 mg/L 0.04000 76 50-144 LCS Dup (P7A0384-13SD1) Prepared 8 Analyzed: 01/26/17 _ 1 Diesel Range Organics 2.12 1.0 mg/L 2.000 106 53-135 8 20 Surrogate: o-Terphenyl _ 0.0293 - mg/L 0.04000 ,-, 73 50-144 Matrix Spike (P7A0384-MS1) Source: 7010331-01 Prepared 8 Analyzed: 01/26/17 _ Diesel Range Organics 3.71 2.0 mg/L 4.000 BRL 93 51-145 .' Surrogate: o-Terphenyl 0.0527 mg/L 0.08000 66 50-144 r Matrix Spike Dup (PM0384-li Source:.7010331-01 _ Prepared 8_Analyzed:__O7_/26_/17 Diesel Range Organics 3.47 2.0 mg/L 4.000 BRL 87 51-145 7 22 Surrogate: o-Terphenyl 0.0488 mg/L 0,08000 61 50.144 This report should not be reproduced. except in its entirety, wthout the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 281 Phone: 704/529-6364-To11 Free Number: 14J001529-5364-Fax: 7041525-0409 Page 6 0f 9 Y ePR I SpM Full-Sorvice Analytical 8 µ u S Environmental solutions Level II QC Report 2/3/17 Radiator Specialty Co Project: 2017 Stormwater Prism Work Order: 7010331 Attn: Stuart Kerkhoff Time Submitted: 1/23/2017 12:30:o0PM 600 Radiator Rd. Project No: NCS000183 Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7A0356 - NO PREP Blank (P7A0356-BLKt) Prepared 8 Analyzed: 01/24/17 Total Suspended Solids BRL 5.0 mg/L _LCS (P7A0156-BS1) Prepared &Analyzed_ Total Suspended Solids 490 5.0 Ell 477.0 102 90-110 Batch P71210030 - NO PREP Blank (P7B0030-BL_K_1_) Prepared 8 Analyzed: 02/01/17 Oil 8 Grease (HEM) BRL 5.0 mg/L _LC_S_(P_7B003_0-BS7_) _' Prepared 8 Analyzed: 02/01/17 Oil 8 Grease (HEM) 33.1 5.0 mg1L 40.00 83 78-114 Sample Extraction Data -Prep Method: 3510C GC Lab Number. Batch Initial Final Daterrime 7010331-01 P7A0384 1000 mL 1 mL 01/26/17 9:10 ' .7010331-02 P7A0384 1000 mL 1 mL 01/26/17 9t 10 Prep Method: 5030E Lab Number Batch • Initial Final Daternme 7010331-01 P7130054 5 mL 5 mL 02/02/17 15:19 7010331-02 P7B0054 5 mL 5 mL 02/02/17 15:19 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: l-800/529-6364-Fax: 7041525-0409Page 70f9 , CHAIN ®F CU1$TODV RECORD An 0lytical s .. I CP�� ISM -� Environmental pj/� ����st.�r �� Environmental So:utions pABE OF_aGUGTEp TO ENSURE PROPER BILLING, /vS.�M1.'ReN"L/.q(IHJION E]INC. � CC jj y ' 449 S Project Nar le:. ,_] ro rM,, L u IY' - �CI' I pri 7041529- 364A Chad one. NC 29217 (hone 704i529-G764 - Pas; '704;525-C40g •Short HoldrAn2lysis: (Yes)' (IW USTProject: (Yes) (N¢t' ^1 �� t _•� �� t ` L 'Ptease ATTACH any project specific reporting (QC LEVEL 1 II ill IV) Client Company Name: ict=c ,r•- . provisionsandlor OC Requirements Report To/Contact Name: $ }L.R/,f ;t ;Invoice To: - A (c ,, r. i k Reporting Address: it U rr - Ira. "Address: i (i l) ref r'•� lanA .1-.. C+,, a. f W L a k.o 11 yrl �fA. " , t,,:; �; ;.�,, .. .: _ �l t,l�.: YES NO' NIA Samples INTACT upon aidva? '~ Received ON WET ICE?! ''' PROPER PRESERVATIVES indicated? .Received WITHIN HOLDING TIMES? �_ CUSTODY SEALS INTACT? VOLATILES leo'd lV10UT HEADSPACE? f 7 PROPER CONTAINERS used'7 __L __ Them, r l Observed: , ( eC i Corr' 4r °C TEMP: TheID. ' ' m `p o� � d ll, 4� J. -(Lr L l .D .?Cj Phone: .:rU ' Lyt S' Faxles) (t t- Purchase Order No./Billing Reference .C-/ i 0 O J 3 CQ j Email Address: S 4'/' l� N .0�v CJ aft, Requested Due Date O 1 Day 02 Days 0 3-Days 04 Days :b 5 Days EDD Type: PDF ✓ Ex; at Other "Working Days" ❑ 69 Days 351t-andartl 10 days 0 Rush Work Must Be Site Location Name: f: �l- ISC_ Samples received after 14:00 wig be processed next business day. Site Location Physical Address: (a,ri j.P. Ci 'G�'fd.- Turnaround time Is based on business days. excluding weekends and holidays. J.ot , r r (SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES r ✓U�,_ ;},YOt.j RENDERED BY PRISM LABORATORIES, INC. TOCLIENTI ,L TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Certification: NELAC DoD FL NC OTHER NIA Water Chlorinated: YES_ NO�� Sample Iced Upon Collection:YES�ZNO_ CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA. TIVES ANALYSIS REQUESTED `"j - n p t') �- (ter N REMARKS % PRISM LAB ID NO. •7yPE $EE BELOW NO. SIZE Y; a t✓ I I I C ice. I r, 5 l C-1 Q 140 7 - -- A C-, Sampler's Signature a,I Sampled By (PrinFName) ��}l.tr;.Y ��c�-�s�oN' ,.Affiliation. 11?( -4., .11'ic�c; '. Upon relinquishing, this Chain of Custodyls your authorization for Prism to proceetl with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analysesl.have been initialized. Rollne 11h a By: (51 atw ) welveC y: Signature) Data MAita oars (- % / r /a f/(7 r j 4 ` r. "/ Additional Comments: Site Arrival Time: z �2 ( i 7i 13- t� Relinduished , (Signawre Racerved By: ,,rxtua, Date Ili Site. Depanut'a Tune: Ralirqulsged By: Signature) Rxeiv or abor ciao Date - Field Tech Fee: n ��. `•✓L. ..it") ..�1 Mileage: I Method! of Shipment: NOTE: ALL SAMPL OOLERS SHOULD BE TAPED SHUT WITH USTODY S FOR TRANSPORTATION TO THE LABORATORY. • COC Group W. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST LONTIL RECEIVED AT THE LABORATORY. 1 I '1 } O Fed Ex ❑ UPS ❑ Hand-eelivered 21<s m-Field Service ❑ Other_______ V V f) 1l NPDES: ! UST: GROUNDWATER: I DRINKING WATER: SOLID WASTE: RCRA::- CERCLA LANDFILL OTHER: I X1 c❑SC�I ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NCOISC CI ❑SC ❑NC ❑SC ❑NC ❑SC ❑ 1 ❑ ❑ 1 ❑__ _ ❑ ❑ ❑ n,. , "CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) '-PRISM CHAIN ®F CUSTODY RECORD Full -Service Analytical & l F_nvirmntanY.d Solutions PAGE l OF _�Z QUOTE a TO ENSURE PROPER BILLING: . <1': k..✓;- n.,.nn rs, nc. 1 iJ � ^) � 1 449 Spr ngbrook Road • Charlotte, NC 28217 Project Name: .� 1�'I"MW- r I cvr /c / Phone 7041529-6�364 - Fax: 7041525-0409 Short Hold Analysis: (Yes) (, UST Project: (Yes) I G ,� I ^ ( �� *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) Client Company Name: G L :4 �- rC a provisions and/or QC Req rement Report To/Contact Name: 1 t(- , } j04l),ir. / ' ` Invoice To: Reporting Address: (. cr C) 'l;a(l ati 7 , r, c( Address: I , n Trn I al ,F � 7 °i T_ .L'r - T ,. l ' At[ 7 Samples INTAGI upon arrival? Received ON WE"1 ICE? PROPER PRESERVATIVES indicateC? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEADSPACE? PROPER CONTAINERS used? TEMP: Therm ID:Ior_T I ( Observe YES NO N/A I O) Phone: -'(1- l,Yr S" Fax (Yes) (IN Purchase Order No./Billing Reference r/ UO (7 2 1,2 -?S TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: 1i0`.�-�<l0 1�-7�7 r�n�>, (n.^� Requested Due Dale O l Day 02 Days 03 Days 04 Days ❑5Days Certification: NELAC DOD FL NC✓ EDO Type: PDF ­1� Excel Other "Working Days" ❑ 6.9 Days I31-Kndard 10 days 0 Rush Work Must Be SC_ OTHER NIA Site Location Name: c Samples received after 14:00 will be processed next business day. Site Location Physical Address: G U'J j.c..j .c�',(.� Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_� c� 1 (SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES i'( I'l•� ,!'c�r .2J '>> RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES__�NO_ TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA. "'t vr' Q p REMARKS t� LAB SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE NO. SIZE TIVES �(^l (\ ID NO. HOURS SLUDGE) SEEBELOW `l 00q t a?fr� �:rS W l !-c T(Z f 6'1 �[ (c Ro 4o ---- -! A, L 41 i p7l _ Z 1- r. � 6 I� / �r lr r- . Sampler's Signature � � Sampled B Print Name -1 � hrG- (J L +� Affiliation r �, U-' -S : [ � P g P y( ) h Upon relinquishing, this Chain of CuStq4 Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be -• submitted in writing to the Prism Project Manager. There will be charges for ny changes after analyses have been initialized. RcLngul e7 By S!1 e) Received By: I g mreI - ale L iutlHa. Additional Comments: Site Arrival Time. Reungmshed By (Signawen Recelved By: (Signature) Date Site Departure Time: nN Relinquished By: (Signature) Received or )tsar bor es By: Date - Field Tech Fee: q 1 1 Mileage Method of Shignent NOTE: ALL 5AMPLE COOLERS 511D BE TAPED SNOT WI M USTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. OC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSTC UNTIL RECEIVED AT THE LABORATORY. % (? O Fed Ex ❑ UPS G Nand -delivered C-4nsm Flek Service D Other_- NPDES: - UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: 9- C0SC ❑NC OSC El NC El SC El NC OSC ZINC ❑SC ❑NCOSC ❑NC ❑SC ❑NC ❑SC ONC OSC I •., n n n n n n n n n ... �', 'CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCSNCS000183 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Radiator Specialty Company COUNTY _Union PERSON COLLECTING SAMPLE(S) Stuart Kerkhoff PH IE N . (,7 4, 6 31-1815 CERTIFIED LARORATORY(S)_Prism Laboratories, Inc._Lab4_402 CEIVE Lab # FEB 0 3 2016 1 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Part A: Specific Monitoring Requirements CENTRAL FILES nIA/R gcrtTIOnl Outfall .:•... No. Date ...� ..=_50050 Sample Collected ? .;,*"" `°s"`�.:.,,n. M PATacalomw IMEMMMINEW afflawifilim t ._. IFOR[ ..ORM ww ckr_," Total '` .Flow (if Total a a Rainfalh " " Suspendedp azaSolidss,,n..,4 Oil and ,[Grease,.. _ �TPH,DRO� TPHtGR0 � ` = t ,z l 1: " ` . •ii '' mo/dd/vrIVIC ,: -; d"n inches _ .fix .. „k rb » m 3 ;*,gym �/L•,r.x:4r"w;. I �, m /L, �:. -.i "^"` a 1 min /L����+ 5� I,t l i= min L $ ,`.t' s r a,^•' r.. �_�kt:Untts �, , :r t ti - 002 8/19/15 NA 4.61 16 <5.0 <1.0 <0.20 6.87 004 8/19/15 NA 4.61 <3.3 <5.0 <L0 <0.20 6.24 003 9/9/I5 NA 0.44 26 <5.0 <L0 <0.20 7.49 001 9/9/15 NA 0.44 7.1 <5.0 <1.0 <0.20 7.31 Does this facility perlbrm Vehicle Maintenance Activities using more than » gallons of new motor oil per month? ves X_no (ifyes, complete Part 13) Part 13: Vehicle Maintenance Activity Monitoring Requirements Oulfall - 50050 z'00556,x1-..,,�.� x., i`�'.> "._ -�'^' 90530 - r� (00400 ""r� .bate Total Flow Total' = g ,Odt�G,re"ase o )Nonlar �p� Total 3- •n"�, t�Ht6 No. Sample' Collected ifa applicable) C PP ) Rainfall s ( PP )_�` tfn 1 10&G/TPH _ ., OdUsa e g t k (Method 1664 Solid" k Y' r.. mo/dd/yr � MG , '��- inches ` a , m/1 '`"_-ntt.,,.- ....z. -,":.,:" al/tno Form SWU-247, last revised 21212012 Paee I of 2 STORM EVENT CHARACTERISTICS: Date _8/ 19/ 15 Total Event Precipitation (inches): 4.61 Event Duration (hours): (only if applicable — see permit.) (if store than one storm event was sampled) Date 9/9/15 Total Event Precipitation (inches): _0.44 Event Duration (hours): (only if applicable — see permit.) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a _ system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (D e) Form SWU-247, last revised 21212012 Pare 2 of 2 nC6-006/93 dlr NC Certification No. 402 F.P.1 SC Certification No. 99012Case Narrative AI S M Full -Service Analytical 8 NC Ounkmq Water Cen No. 37735 Environmental Solutions VACer iftcalion No. 460211 09/Ol/2015 Q- OlAe0aAi0AIES INC. DoD ELAP: L-A-B Accredited Certificate No. L2307 ISOIIEC 17025: L-A-B Accredited Certificate No. L2307 Radiator Specialty Cc Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: Stormwater Lab Submittal Date: 08/19/2015 Prism Work Order: 5080335 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable conditionandprocessed according to the referenced methods. I Data qualifiers are (lagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. )� , J , ?�_ Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: H SEP 2.1.2015 it Reviewed By Robbi A. Jones President/Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced. except in its entirety. without the written Consent of Prism Laboratories. Inc. 449 Sprinybrook Road - P.O. Box 240543 - Charlotte, No 28224-0543 _ Phone: 7041529-63W -Toll Free Number: 14001529-6364 -Fax: 70415254409 Bag e''1? 6f 8 isloao ISM I Fulb Service Analytical Envi.onmen,al 6ol.,ions Sample Receipt Summary 09101 /2015 Prism Work Order: 5080335 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 002 5080335-01 Water 08/19/15 08/19/15 004 5080335-02 Water 08/19/15 08/19/15 Samples were received in good condition at 0.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 9. �p'RISM F - n .,.,,nr,nS.I [n.nonmemm sownoos Laboratory Report 09/01/2015 Radiator Specialty Co Project: Stormwaler Client Sample ID: 002 Attn: Stuart Kerkhoff Prism Sample ID: 5080335-01 600 Radiator Rd. Prism Work Order: 5080335 Indian Trail, INC 28079 Sample Matrix: Water Time Collected: 08/19/15 09:45 Time Submitted: 08/19/15 11:15 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch Limit Factor DateRme ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.082 1 '8015C 825115 14:53 ZRC P5110398 Surrogate Recovery Control Limits o-Terphenyt 107 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mglL 0.20 0.032 1 '8015C 826/15 11:22 ANG P5H0435 Surrogate Recovery Control Limits a.a,a-TriOuorotoluene 98% 57-132 General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 0.48 1 '1664B 8/26/15 14:50 ARC P51-10457 Total Suspended Solids 16 mg/L 12 0.80 1 'SM 2540 0 8121/15 10:35 EGC P5110360 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 P8g8 PRISM ` w,. n,6 Env c tat Solmions V . Laboratory Report 09/01/2015 Radiator Specialty Co Project: Stormwater Client Sample ID: 004 Attn: Stuart Kerkhoff Prism Sample ID: 5080335-02 600 Radiator Rd. Prism Work Order: 5080335 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 08/19/15 09:55 Time Submitted: 08/19/15 11:15 Parameter Result Units Report MOL Dilution Method Analysis Analyst Batch ' Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.082 1 '8015C 825/15 14:16 ZRC P5H0398 Surrogate Recovery Control Limits o-Terphenyl 91 % 50.144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.032 1 '8015C 8/26/15 11:50 ANG P51-0435 Surrogate Recovery Control Limits a.a a.TriBuorotoluene 96 % 57-132 General Chemistry Parameters Oil& Grease (HEM) BRL mg/L 5.0 0.48 1 '16648 8/27/15 10-00 ARC PSH0493 Total Suspended Solids BRL mg/L 3.3 0.80 1 'SM 2540 D 8/21/15 11-10 EGC P5H0360 This reporl should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704f529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 .,. Page 4. of 8 �p R. I S MI F,a o me a s yr, a Env m Sowuons Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Level II QC Report . 9/1/15 Prism Work Order: 5080335 Time Submitted: 8/19/2015 11:15:00AM Reporting Spike Source %REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Blank(P5H0435-BLK1) Gasoline Range Organics Surrogate: a,a,a-Trifluorotoluene LCS(P5H0435-BS1) Gasoline Range Organics Surrogate: a,a.a-Tri11U0rotolueno LCS Dup (P5H0435-BSD1) Gasoline Range Organics Surrogate: a.a,a-Trifluoromluene Matrix Spike (P5H0435-MS1) Gasoline Range Organics Surrogate: a,a.a-Trilluorotoluene Matrix Spike Dup (PSH0435-MSD1) _ Gasoline Range Organics Surrogate: a.a,a-Trl/luoromluena Prepared: 08/25/15 Analyzed: 08/26/15 BRL 0.20 mg/L 0,107 ni 0,1000 107 57-132 Prepared: 08/25/15 Analyzed: 08/26/15 1.00 0.20 mg/L 1.000 100 60-138 0.0990 mg/L 0.1000 99 57-132 Prepared: 08/25/15 Analyzed: 08/26/15 1.10 0.20 mg/L 1.000 110 60.138 0,0970 mg/L 0.1000 97 57-132 Source: 5080335-01 Prepared: 08/25/15 Analyzed: 08/26/15 1.25 0.20 mg/L 1.000 BRL 125 69-130 0.0980 mg1L 0.1000 98 57-132 Source: 5080335-01 Prepared: 08/25/15 Analyzed: 08/26/15 1.28 0.20 m /L 1.000 BRL 128 69-130 0,108 ni 0.1000 108 57-132 10 3 This report should not be reproduced, except in its entirely. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 20 24 Page 5 of 8 Foil-S Service Analyticalaku. I S MI Environmental Soltions Level II QC Rgport 9/1/15 Radiator Specialty Co Project: Stormwater Prism Work Order: 5080335 Attn: Stuart Kerkhof( Time Submitted: 8/19/2015 11:15:OOAM 600 Radiator Rd. Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P5HO398 - 3510C GC Blank fP5H0398-BLK1) Prepared: 08/24/15 Analyzed: 08/25/15 Diesel Range Organics BRL 1.0 mg/L Surrogate: o-Terphenyl 0.0373 mg/L 0.04000 93 50-144 LCS(PSH0398-B51) Prepared: 08/24/15 Analyzed: 08/25/15 Diesel Range Organics 2.04 1.0 mg/L 2.000 102 53-135 Surrogate: o-Terphenyl 0.0447 mg/I_ 0.04000 112 50-144 LCS Cup (P5H0398-BSD1) Prepared: 08/24/15 Analyzed: 08/25/15 Diesel Range Organics 2.01 1.0 mg/L 2.000 100 53-135 2 20 Surrogate: o-Terphenyl 0.0409 mg7L 0,04000 102 50-144 Matrix Spike (PSH0398-MS1) Source: 5080335-01 Prepared: 08/24/15 Analyzed: 08/25/15 Diesel Range Organics 4.10 2.0 mg/L 4.000 BRL 103 51-145 Surrogate: o-Terphenyl 0.0869 mg/L 0.08000 109 50-144 Matrix Spike Dup (P5H0398-MSD1) Source: 5080335-01 Prepared: 08/24/15 Analyzed: 08/25/15 Diesel Range Organics . _...... 4.09 .. ._ 2.0 . ... .. mg/L _. _...___. ... 4.000 BRL 102 51-145 0.2 22 Surrogate: 0-Terphenyl 0.0781 mg1L 0.08000 98 50-144 This repo" should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte. NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1.8001529-6364 -Fax: 7041525-0409 Pege',6iof i. rr r nserviae srica a no Envnmennwai SOuMions �OInIWN�IYni[s inc. Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Analyte Reloading Result Limit Units Level II QC Report 9/1/15 Prism Work Order: 5080335 Time Submitted: 8/19/2015 11:15:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P5HO360 - NO PREP Blank (PSH0360-BLK1) Prepared & Analyzed: 08/21/15 Total Suspended Solids BRL 5e mg/L LCS (P5H0360-BSI) Prepared & Analyzed: 08/21/15 Total Suspended Solids 520 5.0 mg/L 477.0 108 90-110 Batch P5H0457 - NO PREP Blank (PSH0457-BLK1) Prepared & Analyzed: 08/26/15 Oil & Grease (HEM) BRL 5.0 mg/L LCS (PSH0457-BS 1) Prepared & Analyzed: 08/26/15 Oil & Grease (HEM) 32.7 5.0 mg/L 40.00 82 78-114 Batch P5H0493 - NO PREP Blank (P5H0493-BLKI) Prepared & Analyzed: 08/27/15 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P5H0493-BS1) Prepared & Analyzed: 08/27/15 Oil & Grease (HEM) 32.1 5.0 mg/L 40.00 80 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Datorpme 5080335-01 P51-10398 1000 mL 2 mL 08/25/15 8:55 5080335-02 P5H0398 1000 mL 2 mL 08/25/15 8:55 Prep Method: 5030E Lab Number Batch Initial Final Daterfime 5080335-01 P5H0435 5 mL 5 mL 08/25/15 14:32 5080335-02 P51-0435 5 mL 5 mL 08/25/15 14:32 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 14100/529-6364 - Fax: 7041525-0409 -- -PBCje 7 OGS PRISM p CHAIN OF CUSTODY RECORD Full Scrvroe Analytical & Ar Envncnm .tal Solutions PAGE OF I QUOTE# TO ENSURE PROPER BILLING: /k NO NA �i �QJi' ..':.':� LAPORA70R FS wr CC 11. Sample. INTACT upon arrival? _ ✓_ - - ...0� Project Name: —9J N/M U a- V(! ? ) Received ON W E'f ICE? / 449 Springbrook Road - Charlotte, NC 28217 t ."". Wa '- - Phone 7041529-6064 • Fax 7041525-0409 Short Hold Analysis: (Yes) IN* UST Project: (Yes) ( PROPER PRESERVATIVES Indicated? 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) Received WITHIN HOLDING TIMES? mI Client Company Name: IC aciia /o- rc-<�-�, ��. -- O: provisions and/or QC Requirements CUS rOUY' SEAL.. wiACT? Report To/Contact Name. .S-hnc:. f � r� �r k 1^ .� t j Invoice To: Ce liar: [t rL VOLATILES reed W/OL'T HEAD ;PAC['% Reporting Address: %Qft R(,il 4- ?I( Address: n /�ri: rt IOC / PROPER CONTAINFRSgsed? C G (2 d -- C: C--- .. Obsen:e•.i. i j- °or. TEMP: ,44-- -rla.I LIS .M? TEMP: Thorn lO: t !�<. Phone: C-• htl -lyr 5 Fax (Yes) Purchase Order No./Bliling Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: e(;T(c) r5 cJ. G,M Requested Due Date O t Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NCB EDD Type: PDF --Excel—Other "Working Days" O 6-9 Days 9-515andard 10 days ❑ preSApporrovedusl Be — SiteLocationName: �cuia><! Sec la l{ (� Sc OTHER NIA -0 Samples recelved after 14:00 will be processed next business day. Site Location Physical Address: U'O I<ni -a Turnaround time is based on business days. excluding weekends and holidays. Water Chlorinated: YES_ NO ✓ (SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES ICl .In! I n. i�lC I,}37C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES NO TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT DATE COLLECTED (SOIL, PRESERVA- / ! PRISM SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR •TYPE BELOW NO(� /• j REMARKS LAB HOURS SLUDGE) SEE . SIZE ID NO. �/�/ Vv I4 IS S'y} w J 1 I C 11�0 L ► c'i v�� 1 q0. c rIc ( s I — I ��rdr IS J_�- L/ 7 I I '( I No"z I C C, 1-i I I'lu a Sampler's Signature /) -/ -�- Sampled By (Print Name) J PAC4- Kt?Ack-N- I Affiliation KC. iF f. ) al c. c, U Upon relinquishing, this Chain of Custody is your authorization for Prism proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges 1 Y any changes after analyaes-havo been initialized. Rew 4�ccXX�9�s.By: (Sgnaturx,,)//r 11 ecerved ey: ( I store) ( ` Date v7i MnitarylHours Additional Comments: %�/>:ri ��%.7 L�l7 I/T �Oiv0 /a'�'1 l_ n� (�"1-I�tS irl'_Lln Il SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC�UNTIL RECEIVED AT THE LABORATORY. NFULb: ub I: GRUUNUWAIER: URINKINGWATER: SOLIDWASTE: RC CERCLA LANDFILL OTHER: a'tiC❑SC ❑NC El SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SC ❑NC ❑❑ SC INC ❑SC ❑NC ❑SC D -- ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ 'CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) r' NC Cenification No. 402 P® ++RISM SCCenificationterCmN Case Narrative dl! Full -Service Analytical 8 NC Drinkino Water, 46 211 37735 11— Environmental Solutions VA Cenification No. 460211 09/23/2015 .M®ueonnroalr; INC. DoD FLAP: L-A-B Accredited certificate No. L2307 ISO/IEC 17025: L-A-B Accredited Cell No. L2307 �Radiator Specially Co Project: Stormwater TMT0TT[ StuartKerkhoff SEP 2 9 2015 600 Radiator Rd. Lab Submittal Date: 09110/2015 Indian Trail, INC 28079 Prism Work Order: 5090175 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A.Jones Presidenf/Project Manager Data Qualifiers Key Reference Reviewed By Robbi A. Jones President/Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in Its entirety. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 14100/529-6364 -Fax: 7041525-0409 Page 1 of 7 a� P'R I S M Full -Servile Annlyticul 8 Environmental SOIuu DrS �Vunun.rmiev r,e Sample Receipt Summary 09/23/2015 Prism Work Order: 5090175 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 003 001 5090175-01 5090175-02 Water Water 09/09/15 09/09/15 09/10/15 09/10/15 Samples were received in good condition at 4.3 degrees C unless otherwise noted. This report should not be reproduced. except in its enllrety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 2 O($^;: „ r Laboratory Report �P`RISM FullironrienanSolutions p ewboe�,�mai soimlens 09/23/2015 Radiator Specialty Co Project: Stormwater Client Sample ID: 003 Alln: Stuart Kerkhoff Prism Sample ID: 5090175-01 600 Radiator Rd. Prism Work Order: 5090175 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 09/09/15 14:50 Time Submitted: 09110115 15:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch Limit Factor DabuTme ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.082 1 'BO15C 9/16/15 23:56 ZRC P510257 Surrogate Recovery Control Limits o-Temhenyl 84% 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0,032 1 '801 SO 9117/15 21:22 ANG P510314 Surrogate Recovery Control Limits a,a,a-Trinuorotoluene 105 % 57-132 General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 OA8 1 '1664B 9/15/15 10:20 ARC P510266 Total Suspended Solids 26 mg/L 6.2 0.80 1 'SM 2540 0 9114115 11.20 EGO P510225 This report should not be reproduced, except in Its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte. NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001579-6364 - Fax: 7041525-0409 Laboratory Report m a Follse,��cn n�ayucal 8 �P�R�SM Enm,enmemal svmlenc 09/23/2015 Radiator Specialty Cc Project: Stormwater Client Sample ID: 001 Attn: Stuart Kerkhoff Prism Sample ID: 5090175-02 600 Radiator Rd. Prism Work Order: 5090175 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 09/09/15 15:00 Time Submitted: 09/10/15 15:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GCIFID Diesel Range Organics BRL mg/L 1.0 0o82 1 '8015C 9117115 0:34 ZRC P510257 Surrogate Recovery Control Limits o-Terphenyl 80 % 50-144 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0.20 0.032 1 'BO15C 9117/15 21:50 ANG P510314 Surrogate Recovery Control Limits a,a,a-Trifluorololuene 103 % 57-132 General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 0.48 1 '1664B 9/15/15 10:20 ARC P510266 Total Suspended Solids 7.1 mg/L 3.8 0.80 1 'SM 2540 D 9114/15 11:20 EGC P510225 This repon should not be reproduced, except in its entirely, without the written Consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 7041529-63U - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of.8 , . Environmental „vi emal Solutions Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Analyle Reporting Result Limit Units Level II QC Report ' 9/23/15 Prism Work Order: 5090175 Time Submitted: 9/10/2015 3:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P510314 - 5030B Blank (P510314-BLK1) Prepared 8 Analyzed: 09/17/15 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Triluorololuene 0,107 mg/L 0,1000 707 57-132 LCS (P510314.BS1) Prepared & Analyzed: 09/17/15 Gasoline Range Organics 1A3 0.20 mg/L 1.000 113 60-138 Surrogate: a, a. a-Tribuororoluene 0,106 mg/L 0.1000 106 57-132 LCS Dup (P510314.BSD1) Prepared 8 Analyzed: 09/17/15 Gasoline Range Organics 1.12 0.20 mg/L 1.000 112 60-138 1 20 Surrogate: e,,Ta-Trilluorololuono 0.106 mg1L 0.1000 106 57-132 Matrix Spike (P510314.MS1) Source: 5090175-01 Prepared 8 Analyzed: 09/17/15 Gasoline Range Organics 111 0.20 mg/L 1.000 BRL 121 69-130 Surrogate: a.a,a- Tri(luorotolueno 0.107 mg1L 0.1000 107 57-132 Matrix Spike Dup (P510314-MSD1) Source: 5090175-01 Prepared 8 Analyzed: 09/17/15 Gasoline Range Organics 1.24 0.20 mg/L 1.000 BRL 124 69-130 3 24 Surrogate: a,a,o-Trilluorololuone 0.111 mg4. 0.1000 111 51.132 This report should not be reproduced. except in its entirely, without the written consent of Prism Laboratories. Inc. 449 $pringbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529.6364 - Fax: 704152541409 Pagel'5 Of 8 r' e� ® s Full -Service Analytical 8 dP I S M uvbenmeNal S.ellens „e,,. —a..,.c Radiator Specialty Cc Project: Slormwater Alto: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Reporting Result Limit Units Batch P510257 - 3510C GC Level II QC Report 9123/15 Prism Work Order: 5090175 Time Submitted: 9/10/2015 3:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(P510257-BLKt) Prepared: 09/15/15 Analyzed: 09/16/15 Diesel Range Organics BRL 1.0 mg/L Surrogate: o-Terphenyl 0.0340 mg7L 0.04000 85 50-144 LCS (P510257-BS1) Prepared: 09/15/15 Analyzed: 09/16/15 Diesel Range Organics 1,95 1.0 mg/L 2.000 98 53-135 Surrogate: o-Terphenyl 0.0312 mg7L 0.04000 78 50-144 LCS Dup (PSI0257-BSDt) Prepared: 09/15/15 Analyzed: 09/16/15 Diesel Range Organics L92 1.0 mg/L 2.000 96 53-135 2 20 Surrogate: o-Torphenyl 0.0304 mg/L 0.04000 76 50-144 Matrix Spike (P510257-MS1) Source: 5090175-01 Prepared: 09/15/15 Analyzed: 09/16/15 Diesel Range Organics 4.08 2.0 mg/L 4.000 BRL 102 51-145 Surrogate: o-Terphenyl 0.0664 mg1L 0.08000 83 50-144 Matrix Spike Dup (P510257-MSD1) Source: 5090175-01 Prepared: 09/15/15 Analyzed: 09/16/15 Diesel Range Organics 3.95 2.0 mg/L 4.000 BRL 99 51-145 3 22 Surrogate: o-Terphenyl 0.0626 mg/L 0.08000 76 50-144 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 - Page 6 Of 8 AP'RJ 4 j FYtI$Cr C An ClyliCal B I S M 6nvnOnmOp,al $YIWICnS ®v. Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Level II QC Report 9/23/ 15 Prism Work Order: 5090175 Time Submitted: 9/10/2015 3:00:00PM Reporting Spike Source %REC RPO Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P510225 - NO PREP Blank (P510225-BLK1) Prepared & Analyzed: 09/14/15 Total Suspended Solids BRL 5.0 mg/L LCS (P510225-BS1) Prepared & Analyzed: 09/14/15 Total Suspended Solids 460 5o mg/L 477.0 96 90-110 Batch P510266 - NO PREP Blank (P510266-BLK1) Prepared & Analyzed: 09/15/15 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P510266-BSI) Prepared & Analyzed: 09/15/15 Oil & Grease (HEM) 35.3 5.0 mg/L 40,00 88 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Daterrime 5090175-01 P510257 1000 mL 2 mL 09/15M5 1230 5090175-02 P510257 1000 mL 2 mL 09/15/15 12:30 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 5090175-01 P510314 5 mL 5 mL 09/17/15 14:15 5090175-02 P510314 5 mL 5 mL 09/17/15 14:15 This report should not be reproduced, except in its entirety, whhoul the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page To CH IN ®F CUSTODY RECORD M:= 'z,2- hullService Analytical & I /._ yF NO NOi Envuv o rental Solutions PAGE OF QUOTE NTO ENSURE PROPER eILLINO: Sample,; WTAfI ul c t arival7 Project Name: 1 �f4.. Wr��� V 1�� (� I Recemked MJ WETh? T -- —x 449 `.prmgbrook Road • Charlotte NC 28217 Short Hold Analysis: (Yes) ( UST Project: (I PROPER. PRFSERVAI IVE < indirh en? -_. _ 1'Ihm . /041„ 29.6364 - Far: 7041525-0409 • , Soo,1 1� L 'Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV) Received VVTHIN HOLD114G TIM ? 7 Client Company Name: eJ i CJ-= I o or provisions and/or QC Regqquire/menf5� CUSTOnY SEALS INTACT Report To/Contact Name: S-I-.r./I' Kr+Ic�FT Invoice To: rY L'�T1 1'c,�0 �jle VOLAT ILES rec d tViOUT EALSPACE? f.S _� --,._-- Reporting Address: 6Ul7 IZAI(:r, i✓-' — Address: L7 1(rll ir, / �1L PROPER CONE IN Uved> /L i r TEMP Inen:ID r1n erveL, (Yes) (": Purchase Order No./Billing Reference 44 5000 3 00l 1 Email Address: �> 6? -10N ., tit- (� EDD Type: PDF to Excel_Othel Site Location Name: I cl I : r- ✓J' Site Location Physical Address: 1 CLIENT DATE SAMPLE DESCRIPTION I COLLECTED Oo 3 19/S. !"S(5•"^ tV Requested Due Dace ❑ 1 Day O 2 Days ❑ 3 Days ❑ 4 Days O 5 Days "Working Days" ❑ 6-9 Days 613landard 1D days O Rush Work Must Be Pre -Approved 5 +' icl Samples received after 14:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES C Z } v �i `I RENDERED BY PRISM LABORATORIES. INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER / C COLLECTED (SOIL, _ PRESERVA- MILITARY WATER OR -TYPE TIVES HOURS SLUDGE( SEE BELOW NO. SIZE ^ j C C� _ I-� I -ICI v�A 3 40-.,c Po I I Ivitna- I I TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC_ DoD_ FL_ NC SC_ OTHER NIA Water Chlorinated: YES_ NO--" Sample Iced Upon Collection: YES -�'NO_ PRISM o/• U / / REMARKS I LAB ID NO. z IS;0 ? i I-C I 1\101` CtLi I (-L I4CI I -- --- - I'iu -- I— — Sampler's Signature -�,..✓ I1-LJ 'Sampled By (Print Name) S 4 L-a+I KL-lch%rr Affiiation gcl ;L,L/ %�PC: Upon relinquishing, this Chain of Custody if your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Projec ager. There will be charges for any changes after analyses have been initialized. Hcl. ned By:1/T�igna urel ) Recet By:(i)nature) oat MintarylMgo_urs additional Comments: �[n/J9rlu�''Y C//re/(.! RO. i7(ryr5 tl Sy: (Signature Re rve By: (Signature) f Date ftelinO M1ed By: (Signawr J , Received F Prism LaW alor es By. Date boo Method Of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT/WYITH OUS OD SEAL FOR TRANSPORTATION TO THE LABORATORY. COC Group No. SAMPLES ARE NOT ACCEPTED AN D VERIFIED AGAINSICOCMNI/ RECEIVED AT THE LABORATORY. ❑ Fed Ea ❑ UPS O Hand-detive,W Wnsm Field Semce ❑ ONcr l v 0 NPD arlc ❑ SC. ❑ NC ❑ SC ❑ NOCU ❑ SCTER: ❑ NC I SCATER: CI NC ❑ SOLID SSCE ❑ NC ❑ SC ❑E1 L❑ SC ❑ NC F❑ SC Cl C ❑ SC ❑ ❑ ❑ ❑ —i ❑ ❑ ❑ ❑ _. — ❑ `CONTAINER TYPE CODES: A= Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) 3ile Anlval-rime- Site Departuro Time Reid lecit F'oe: Mileage: A .Vr Chemical Solutions a division of Radiator Specially Company .January 28, 2016 Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Report Radiator Specialty Company Radiator Road, Indian Trail, North Carolina NPDES Permit No. NCS000183 Dear Sirs: Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outfall Monitoring Report for monitoring period Year 7 — Period 1 as required by Part III Section E.(l.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company Stuart A. Kerkhoff Environmental I-icalth and Safety apger Attachments SIRMWAr\YR7PD 1-2015C V1- rDOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscbrands.conn STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 'w Permit Number NCS_NCS000183 FACILITY NAME Radiator Specialty Company PERSON COLLECTING SAMPLE(S) Stuart Kerkhoff CERTIFIED LABOR.ATORY(S)_Prism Laboratories, Ine._Lab#_402 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY _Union PHON NO. ( 7 4,_654-1815 _� FSIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PACE 2. Outfall No. Date Sample Collected 50050To[al, T low a t Flow (if Totnl`' Rai II .,�' Suspended . Solids ©ikand Grease TP,Hd DRO TtP,H GRO H' ME mo/dd/ r MG ='riche§ _ m /L m Ll Ermg/l m LL Units r"'� tl 003 7/28/15 NA 0.16 34 <5.0 <I.0 <0.20 6.25 001 No Flow NA No Flow No Flow No Flow No Flow No Flow No Flow 002 No Flow NA No Flow No Flow No Flow No Flow No Flow No Flow 004 No Flow NA No Flow No Flow No Flow No Flow No Flow No Flow Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X_no (ifyes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date 50050 00556 ?fir a <OOa30- �' . = 00700="? " # Total Flow Total Oil &Grease , Non=polar P,, ,Total "` pH'� New Motor — No. Sample Collected (if applicable) Rainfall {dappl) O&�GPH� St s� pend d' ?s OdUsage '(Methodr1664Sohds SGT HEM)' tf mo/dd/yr MG inches ;in `_ r•'g — .6ni—w=-o:-�,A .zo Form SWU-247, losi revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date _7/28/ 15 Total Event Precipitation (inches): 0.16 Eve at Duration (hours): (only if applicable —see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see pennit.) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — sec permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a System designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pernnittee) v / o ph/ - (Date) Form S W U-247, last revised 21212012 Pafle 2 of 2 NC Certification No. 402 SC Cenifcation No. 99012 Case Narrative API S M Full -Service Analytical 8 NC Drinkino water Ceo No 37735 r Environmental Solutions VACenifcationNo. 460211 08/12/2015 0ueoxatoaies ;xe. DoO ELAP: L-A-B Accredited Certificate No. L2307 ISO/IEC 17025: L-A-B Accredited Cenificate No. L2307 " Radiator Specialty Co Project: Stormwater Stuart Kerkhoff 600 Radiator Rd. Lab Submittal Date: 07130/2015 Indian Trail, NC 28079 Prism Work Order: 5070595 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A.Jones President/Project Manager 10 Data Qualifiers Key Reference a- U Reviewed By Robbi A. Jones President/Project Manager AUG 2 4 2015 BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference t Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirely. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-63U -Toll Free Number: 1-8001529.6364 - Fax 7041525-0409 P ®I S M Full-Seralce Analytical 8 6ovbenmeotal fiat uuuns �vuMvu.n,.x Sample Receipt Summary 08/12/2015 Prism Work Order: 5070595 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 003 5070595-01 Water 07/28/15 07/30/15 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Frea Number: 1-6001529.6364 -Fax: 7041525-0409 'PagB'2'Oi%7;='•', &P.R. I, S,M I [nJ coral solutions v, Radiator Specialty Cc Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Laboratory Report 08r12/2015 Project: Stormwater Client Sample ID: 003 Prism Sample ID: 5070595-01 Prism Work Order: 5070595 Sample Matrix: Water Time Collected: 07/28/15 13:45 Time Submitted: 07/30/15 15:50 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date7rime Batch ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0082 1 '8015C 8/4/15 17:01 ZRC P5110028 Surrogate Recovery Control Limits Gasoline Range Organics by GC/FID Gasoline Range Organics BRL General Chemistry Parameters Oil & Grease (HEM) Total Suspended Solids o-Terphenyl 78 % 50-144 mg/L 0.20 0.032 1 '8015C 8/11/15 11:29 ANG P5H0135 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 102 % 57-132 BRL 34 mg/L mg/L 5.0 0.48 6.2 0.80 1 '16646 814/15 16:15 1 'SM 2540 D 7131115 14:50 ARC EGC P5110047 P5130610 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 ®� m I S M I Full-serym ica Plyti[al 6 - Environmental Salwions Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: Stormwater Gasoline Range Organics by GC/FID - Quality Control Reporting Result Limit Units Batch P5HO135 - 50308 Level II QC Report 8/12/15 Prism Work Order: 5070595 Time Submitted: 7/30/2015 3:50:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P5H0135-BLK1) Prepared & Analyzed: 08/11/15 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a.a.a-TriOuorotoluene 0.0950 mg1L 0.1000 95 57-132 LCS (P5H0135-BS1) Prepared & Analyzed: 08/11/15 Gasoline Range Organics 1.01 0.20 mgtL 1.000 101 60-138 Surrogate: a,a,a-Tnlluorotoluene 0.0950 mg1L 0.1000 95 57-132 LCS Dup (P5H0135-BSD1) Prepared & Analyzed: 08/11/15 Gasoline Range Organics 1.11 0.20 mg/L 1.000 ill 60-138 10 20 Surrogate: a,a,a-Triduoretoluene 0.0990 mg7L 0.1000 99 57-132 Matrix Spike (PSH0135-MS1) Source: 5070595-01 Prepared & Analyzed: 08/11/15 Gasoline Range Organics - 0.997 0.20 mg1L 1.000 BRL 100 69-130 Surrogate: a,a,a-Trilluorotoluene 0.101 mgrL 0,1000 101 57-132 Matrix Spike Dup (PSH0135.MSD1) Source: 5070595-01 Prepared & Analyzed: 08/11/15 Gasoline Range Organics 1.17 0.20 mg/L 1.000 BRL 117 69-130 16 24 Surrogate: a,a,a-Tnlluomtoluene 0.110 mg/L 0.1000 110 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 s. of a ISM I Environmental nvi fn1al Sol urio 049 Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, INC 28079 Diesel Range Organics by GCIFID - Quality Control Analyte Reporting Result Limit Units Level It QC Report 8/12115 Prism Work Order: 5070595 - Time Submitted: 7/30/2015 3:50:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch'P5H0028 - 3510C GC Blank (PSH0028-BLK1) Prepared & Analyzed: 08/04/15 Diesel Range Organics BRL 1.0 mg/L Surmgale: o-Terphenyl 0.0273 mg/L 0,04000 68 50-144 LCS (1351-10028-13ST) _ Prepared & Analyzed: 08/04/15 Diesel Range Organics 1.92 1.0 mg/L 2.000 96 53-135 Surrogate: o-Terphenyl 0.0311 mg/L 0.04000 78 50-144 LCS Dup (PS110028-13SM) Prepared & Analyzed: 08/04/15 Diesel Range Organics 1.98 1.0 mg/L 2.000 99 53-135 3 20 Surrogate: o-Terphenyl 0.0293 mg7L 0.04000 73 50-144 Matrix Spike (PSH0028-MS1) Source: 5070595-01 Prepared & Analyzed: 08/04/15 Diesel Range Organics 2.34 1 0 mg/L 2.000 0.323 101 51-145 Surrogate: o-Terphenyl 0.0362 mg/L 0.04000 90 50-144 Matrix Spike Dup (P5H0028-MSD1) Source: 5070595-01 Prepared & Analyzed: 08/04/15 Diesel Range Organics 2.06 1.0 mg/L 2.000 0.323 87 51-145 13 22 Surrogate: o-Terphenyl 0.0296 mg7L 0,04000 74 50-144 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525.0409 �� ism J'vI� �I I Full -Service al Solutions eovlreorneurASO Analytical rwpuraa[i ixc Radiator Specialty Co Attn: Stuart KerkhoH 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Analyte Project: Stormwater Reporting Result Limit Units Level II QC Report 8/12/15 Prism Work Order: 5070595 Time Submitted: 7/30/2015 3:50:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P5G0610 - NO PREP Blank (P5G0610-BLK1) Prepared & Analyzed: 07/31/15 ------------ Total Suspended Solids BRL 5.0 mg/L LCS (PSGO610-BS1) Prepared & Analyzed: 07/31/15 Total Suspended Solids 470 5.0 mg/L 477.0 99 90.110 Batch P51-10047 - NO PREP Blank(P5H0047-BLKt) Prepared & Analyzed: 08/04/15 Oil & Grease (HEM) BRL 5e mg/L LCS (P5H0047-BS1) Prepared & Analyzed: 08/04/15 Oil & Grease (HEM) 31.7 5e mg/L 40.00 79 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 5070595-01 P51-10028 1000 mL 2 mL 08/04/15 8:10 Prep Method: 5030B Lab Number Batch Initial Final Daterrime 5070595-01 P51-10135 5 mL 5 mL OB/11/15 722 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 CH/AIM OF CUSTODY RECORD 'PRISM `°I1e^'^:`A"''"`<"F YES ,.NO WA F IS a e I w eu n •u,o - �� 93 d R E CM . IF .Name Shim Ie An ly IY ) IH 1 USTPmIecl (Yes) (NOI CV'E i ESE0.VAT LS car 4p ,. r1luAlsMEIF �- 5 �I �•' 91s ATTACH ypH, p Itic repene,(OC LEVEL 111111IV) Ws VADmG IK3 5 )11 5E 5 TA _ Client Company Name CSa pAdvidens mullor OCRq C Ra P. TWContac9 Name. 1—M i ) SIi vL—TILE q 9 I[ oC cF RepoilmB Aeerpss' GDh 1 t{--Rd -.. AddressI'� 1 RI PPCaERcplT 5 n .. n .fir O ..... s� r phone: 4}_!-ly (res) (tki: Purchase order Hdmining Ratennca /' L%cy TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Add.... cin i+.I Ra ndreynmaa Jtmr mWpp OT mw Dam» usmw COH.ficatlon: NELAC_DOO_FL_NC ✓ EDDTypv: PDF_Eail Olhn -wwside Oryf U69 m».>Su�ane town DNt. o..a'�e< SC OTHER NIA Site Location Name' IL 4- 1. S-1.1MLAYad aar, a corm vn Moue... n<n o,.�..0 — 311.Location Physicl!lAeeresa 1p: I. ". _ sunv�mtd Nre•urrtlm Wu,is. p. Lmunmeu •.+m."amvadar•. Wa9erLMorinatOe: YES_NO✓ r LI,. 'Gz �/ A(CA(C YY�h ouueoRnrwNaM is SamplekveUponCOlbction:YE5�N0— I 91.E lRl% 3 NhECONIYHER L SISREWESTE. pRRN CLIEN p E COLLECTED ISOL _ PPESERV L /J/ / / q[yaRIL3 LAp HLITAR $AMPLE OESC IIUN COLLEC E0 OURS E E O 36E TMES '�,rV /<�r M1/� mN0 OURS 3 UOiEI SEE OELGW _ _ - _... — v„A Upon nunauIshi, mNChaln oIC. Y'r.`nirto"th1m. pito to proceed with the enelpee ar,q... led agora ouManager.Tat, Any theme must as ' auamntee Namot. LeIMpMe pm»n WII pa cmryr. mt •my cesnO••.Ne,.ne, aura esm I mdslinto ANOnmal Cdrvrenl mi r_ n.. Ir — I'm i' /w.io ;4a AmL C061i ..nattjU5..A-1-1 Ls . In cVfLs?aE95FufrdTtinu Tm LA AT . Rc-1. A.'.I--Arco' orDF mn•5 t. n..�.n na vmn .__ --'L OUND.RTE. A DflINNIND VIATEfl: SOLID WAEIE: RCL I CICJ NPDES: UST: G.c ER.. LANDFILL OTHER. ,WATEP'.• 3FCOSC DNC 'J SL -J rvC JSC ONC ]SC ']NC JSC JNC LI SC' OrvC JSC IJ NC ]SC'ONC ]SC ll EI J _ J ._ 'J J ❑ Q.— _ .. _. _ 'CONTPINEAU IECODES: A=Arnite� C. Cloat G-Glaaa P. plasm; IL=TeRont"Im Cau VOA-I...i,l l W,a AnaN'-$(Zerol MSpace) i Chemical Solutions a division of Radiator Specialty Company AUflUst 4, 2016 Central riles North Carolina Department of Environment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Ralciah, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Rep, Radiator Specialty Company Radiator Road, Indian Trail, North Carolina NPDES Permit No. NCS000183 Dear Sirs: RECEIVED AUG 0 8 2016 CENTRAL FILES DWR SECTION Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outfall Monitoring Report for monitoring period Year 7 — Period 2 as required by Part III Section E.(1.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Environment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company Ami 01 ' Stuart A. Kerkhoff. CI-IMM Environmental Health and Safety anager Attachments S I RMWA 1)Yk71'1)2-2016CVI.I DOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — www.rscbrands.conn C'VEt) STORMWATER DISCHARGE OUTFALL(SDO) _ MONITORING REPORT _ Permit Number N'CSNCS000183 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 _ FILES RECEIVED C �'v�® (This monitoring report shall be received by the Division no later than 30 days from '1TION R CE the date the facility receives the sampling results from the laboratory.) FACILITY NAME Radiator Specialty Company PERSON COLLECTING SAMPLE(S) Stuart Kerkho_f[=NTRAL R FS CERTIFIED LABORATORY(S)_Prism Laboratories, Ine_lL�i'IS#DWZTKM Lab # Part A: Specific Monitoring Requirements COUNTY Union PH(� —NO j_704J 6 4-1815 / b 3 /G SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall Date 50050 Total No. Sample Collected Total Flow (if a Total Rainfall . Suspended Solids ,Oil and - Grease TPH DRO TPH GRO)_ PH mo/dd/vr MG inches m /L m /L m /L m /L Units 004 5/20/16 NA 1.79 <100 <30 <1.0 <0.20 6.95 002 6/6/16 NA 1.83 <25 <5.0 <I.0 <0.20 8.63 001 No Flow NA No Flow No Flow No Flow No Flow No Flow No Flow 003 No Flow NA No Flow No Flow No Flow No Flow No Flow No Flow Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X_no (ifyes, complete Part 6) Part B: Vehicle Maintenance Activity Monitornw. Requirements Outfall No. Date Sample Collected 50050 '00556 00530 "" 00400. 1' Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar'- O&G/TPH (Method 1664, SGT-HEM), if, a l- Total Suspended Solids pH New Motor Oil Usage mo/dd/ •r MG '. inches - 'm /I - m /I unit al/mo Form S W U-247, lost revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date _5/20/16 Total Event Precipitation (inches): _I 79 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date 6/6/16 Total Event Precipitation (inches): _1.83 Event Duration (hours): (only if applicable — see permit.) Date Total Event Precipitation (inches): Event Do ration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of n»Y knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm /� (Date) Form SWU-247, last revised 1/J2012 Page 2 of 2 wtaISeonnroaies nicM Radiator Specialty Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Full -Service Analytical & Environmental Solutions ? ' ll �� JUf\I 2 0 9016 I0 NC Certification No. 402 NC Drinking Water Carl No, 37735 SC Certification No. 99012 FL NELAC Cert No. E87519 VA NELAC Cen No. 460211 Project: Slormwaler r,C�-aoo/ 93 Case Narrative Lab Submittal Dale: 05/25/2016 Prism Work Order: 6050491 06/09/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. J�oneess President/Project Manager Data Qualifiers Key Reference 7��_ a_. (&� Reviewed By Robbi A. Jones President/Project Manager RECEIVED AUG 08 zolb CENTRAL FILES DWR SECTION BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MOIL with values between MOIL and reporting limit indicated with a J. This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-8001529-6364-Fax- 7041525-0409 Page 1 0f7 Sample Receipt Summary o w Full -Service .9 Srn r. x 06/09/2016 eP'R I S M S ;ro , n, t se , o, AvvArr,;,..,.c Prism Work Order 6050491 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 004 6050491-01 Water 05/20/16 05/25/16 Samples were received in good condition at 3.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Tall Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 2 of 7 Laboratory Report Aa:r a F.m-Scrvice Analytical a Po R I S M„ ;,e menr, so er e„= 06/09/2016 Radiator Specialty Co Project: Stormwater Client Sample ID: 004 Attn: Stuart Kerkhoff Prism Sample ID: 6050491-01 600 Radiator Rd. Prism Work Order: 6050491 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 05/20/16 08:25 Time Submitted: 05/25/16 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dale/Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L le 0.18 1 '8015C 5/25116 16:55 2RC P6E0490 Surrogate Recovery Control Limits o-Terphenyl 82 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.025 1 '8015C 6/2/16 1627 ANG P6F0055 Surrogate Recovery Control Limits a,a.a-Trifluorololuene 110 % 57-132 General Chemistry Parameters Oil 8 Grease (HEM) 5.6 mg/L 5.0 1.0 1 '16648 6/3116 10:44 TJY P6F0084 Total Suspended Solids 7.4 mg/L 3.6 0.80 1 'SM 2540 D 5/27116 11.46 SLS P6E0606 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, He 28224-0543 Phone: 7041529-6364- Toll Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 3 of 7 O Full -Service Awlytical & !Ql R.I S M 1 Environmental Solutions .'�Vuvo�.rnx�r>�„� Level II QC Report 619116 Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Analyte Batch P00055 - 5030B Reporting Result Limit Units Prism Work Order: 6050491 Time Submitted: 5/25/2016 11:00:OOAM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes Blank(P6F0055-BLK1) Prepared: 06/02/16 Analyzed: 06/03/16 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Trifluorotoluene 0.0990 mg/L 0.1000 99 57-132 LCS (P00055-BSI) Prepared & Analyzed: 06/02/16 Gasoline Range Organics 1.05 0.20 mg/L 1.000 105 60.138 Surrogate: a,a,a-Trifluorotoluene 0.0920 mg/L 0.1000 92 57-132 LCS Cup (PGF0055-BSDI) _ _ .. _ _ _ _ _.__-__ _ Prepared & Analyzed: 06/02/16 Gasoline Range Organtcs 1.12 0.20 mg/L 1.000 112 60-138 6 20 Surrogate: a,a.a-Trilluorotoluene 0.100 mg/L 0.1000 100 57-132 Matrix Spike (P6F0055-MS1) _ Source: 6050491-01 Prepared & Analyzed: 06/02/16 Gasoline Range Organics 1.13 0.20 mg/L 1.000 BRL 113 69-130 Surrogate: a,a,a-Tri/luomfoluene 0,107 ni 0. 1000 107 57-132 Matrix Spike Cup (P00055-MS01) _. Source: 6050491-01 Prepared & Analyzed: 06/02/16 Gasoline Range Organics ___________--__-_.--. 1.24 0.20 mg/L 1.000 BRL 124 69-130 10 24 Surrogate: a,a,a-Trinuorololuene 0,117 mg/L 0.1000 117 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 4 of 7 o Full -Service Analyfeal a ®PRISM e„ ,.enure ,at Solo inn. Level II QC Report 6/9/16 Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Analyze Batch P6EO490 - 3510C GC Reporting Result Limit Units Prism Work Order: 6050491 Time Submitted: 5/25/2016 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPO Limit Notes Blank (P6E0490-BLKt) Prepared & Analyzed: 05/24/16 Diesel Range Organics BRL l o mg/L Surrogate o-Terphenyl 0.0368 ngIL 0.04000 92 50-144 LCS (PGE0490-BS1) Prepared & Analyzed: 05/24/16 Diesel Range Organics 2.16 1.0 mg/L 2.000 108 53-135 Surrogate: o-Terphenyl 0.0421 mg/L 0,04000 105 50-144 LCS Dup (P6E0490-BSD1) Prepared & Analyzed: 05/24/16 Diesel Range Organics 1.96 1.0 mg/L 2.000 98 53-135 10 20 Surrogate: o-Terphenyl 0.0366 mg/L 0,04000 91 50-144 Matrix Spike (KE0490-MS1) Source: 6050491-01 Prepared & Analyzed: 05/25/16 Diesel Range Organics 4.77 2.0 mg/L 4.000 BRL 119 51-145 Surrogate: o-Terphenyl 0.0897 mg1L 0,08000 112 50-144 Matrix Spike Dup (P6E0490-MSD1) Source: 6050491-01 Prepared & Analyzed: 05/25/16 Diesel Range Organics 4.96 20 mgtL 4.000 BRL 124 51-145 4 22 Surrogate: o-Terphenyl 0,0814 mg/L 0.08000 102 50-144 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 5 of 7 Level II QC Report ens a . A smtical /06.3 1 S M Fulb$O'n'` a Analytical 8 6/9116 Radiator Specialty Cc Project: Slormwater Prism Work Order: 6050491 Attn: Stuart Kerkhoff Time Submitted: 5/25/2016 11:00:OOAM 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6E0606 - NO PREP Blank (P6EO606-BLK1) Prepared & Analyzed: 05/27/16 Total Suspended Solids BRL 5.0 mg/L LCS (P6E0606-BSI) Prepared & Analyzed: 05/27/16 Total Suspended Solids 470 5.0 mg/L 477.0 98 90-110 Batch P61`0084 - NO PREP Blank (P6F0084-BLK1) Prepared & Analyzed: 06/03/16 Oil & Grease (HEM) BRL 5o mg/L LCS (P6F0084-BS1) Prepared & Analyzed: 06/03/16 Oil & Grease (HEM) 35.8 5.0 mg/L 40.00 90 78-114 Prep Method: 3510C GC Lab Number Batch Initial Sample Extraction Data Final Date7Time 6050491-01 P6EO490 1000 mL 2 mL 05/25/16 12:30 Prep Method: 5030B Lab Number Batch Initial Final DateRime 6050491-01 P6F0055 5 mL 5 mL 06/02/16 12:28 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 140543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525-0409 Page 6 of 7 PRISMI Full -Service Analytical Environmental Solutions LeonmaomES. uuc. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 Fax: 7041525-0409 Client Company Name: iZs �- U�e+.ir• I S II. ��'v Report To/Contact Name: 1"1,.(.!i" Reporting Address: U,,L' �_.) ` /+q � Y g 4� ;- i k i� SP;, 'g ;.� r ;' rip )'•, 1)i PAGE r OF / QUOTE N TO ENSURE PROPER BILLING: Project Name: Short Hold Analysis: (Yes) (1,11< UST Project: (Yes) (NO) 'Please ATTACH any project specific reporting (OC LEVEL 111 If IV) provisions and/or OCR Requtrements /I Invoice To: cc_ l- 7cL. 117 re Address: (, L' V' J ct_,v, - 72J r-- ,.I _ �i,--'I A( YEry nip WA San n pies INTACT upon n,Iwal.1 Received ON VVEIICE" PROPER 'RE>;-RVAT 'VE.- nJc:n'-d V _ ROcLivedlNllI IN 1-I01, Ul['K INIF'9+' �'"� W OUST ODY SEALS IN U.0 : i VOLAI ILLS n;c t J L 1 I FAI Jli,'t I- L�'_. , PROPER GON IAINEr . oszd, V i Phone: ✓u 1J y I.�/ S Fax (Yes) (14): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL �� �n � r, h / Email Address: 1 (7� < - .1C . '^•�f p. C o'er Requested Due Date O 1 Day O 2 Days ❑ 3 Days 04 Days ❑ 5 Days Certification: NELAC DOD FL NC r� EDD Type: PDF -,'Excel Other "Working Days" ❑ 6-9 Days t3<andard 10 days 0 Rush Work Must Be Pre -Approved SC OTHER N/A Site Location Name: I Samples received after 14:00 will be processed next business day. — Site Location Physical Address: (,00 i2c:�I Ca!•+% 2i1 Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO,- nntgl �M ; I (L)L 99 // dY l) I (SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) P P Sample Iced Upon Collection: YES —"NO CLIENT DATE TIME COLLECTED MATRIX (SOIL, SAMPLE CONTAINER PRESERVA- ANALYSIS REQUESTED `-7 �^ O Q ! REMARKS / PRISM LAB 'TYPE NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES ft"? ID NO. HOURS SLUDGE) SEE BELOW lit- Pic — V 3 o ML He i 3 I I Sampler's Signature Sampled By (Print Name) J" l.v(J- \'t'�t'"' %`� Affiliation Upon relinquishing, this Chain / ody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism p o�ject Manager. There will be charges cr any changes after analyses have been initialized. Relinqu ed6 (S(gnature) ' 1��,,�,- Rece.,oi By: gnaWm) r (' Dale MIIllarwHOule -_. -� Additional Comments Relinguohed ay: ( gnnpare) Received By. (Signature) Dale S le p t,tu , T r r\ t {i Ref,nOu.ehed By ISlgnaluret Re. For Pnsm Lab IOries By: %�-Method Oala j� pl I 1 I' of nt NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No. SAMPLESARENOT AfCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.JS / G Hantl-0elivered Q Prism Field Service :J Other ILYY NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: ' I.T'NCOSC ONC 175C El OSC 0NC ❑SC ONC 0SC ❑NC❑SC El NC ❑SC ONC CI 0NC 0SC APRISM '®" VLABOBArORIE51Nc. Radiator Specially Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Full -Service Analytical & Environmental Solutions L l'!.' ? 1] N JUN 2 X 2w D NC Certification No. 402 NC Drinking water Cart No. 37735 SC Cenification No. 99012 FL NELAC Cen No. E87519 VA NELAC Cen No. 460211 Project: Stormwater Lab Submittal Date: 06/07/2016 Prism Work Order: 6060125 Case Narrative 06/21/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES. INC. ) t�_ a_. (?�__ RobbiA.Jones President/Project Manager Data Qualifiers Key Reference Reviewed By Robbi A. Jones President/Project Manager M Matrix spike outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference R Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax 7041525-0409 Page 1 of 7 Sample Receipt Summary n` fA fi R I S M I Eulbso,�,en nnaiyhtio x Env mSolutionsoneai Solutions 06/21 /2016 Prism Work Order: 6060125 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 002 6060125-01 Water 06/06/16 06/07/16 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 2 of 7 Laboratory Report ePR I S M I Funaervice Analytical o „ „o m n,a 6omr,ons 06/21/2016 Radiator Specialty Co Project: Stormwater Client Sample ID: 002 Attn: Stuart Kerkhoff Prism Sample ID: 6060125-01 600 Radiator Rd. Prism Work Order: 6060125 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 06/06/16 08:15 Time Submitted: 06/07/16 14:18 Parameter Result Units Repon MDL Dilution Method Analysis Analyst Batch Limit Factor Date/lime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mgA- 1.0 a18 1 '8015C 6114116 16:42 ZRC P6F0213 ___ .......... . ------- ---- . ._ .. Surrogate Surrogate Recovery Control Limits o-Terphenyl 75 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0,20 0.025 1 '8015C 6/16/16 18:33 ANG P6F0328 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 114 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 1.0 1 '1664B 6/15/16 10:21 TJY P6F0301 Total Suspended Solids BRL mglL 25 0.80 1 'SM 2540 D 618/16 16:06 SLS P61`0187 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: l-800/529-6364- Fax: 7041525-0409 Page 3 of 7 Level II QC Report �P© S. Full -Service Analytical8 R I S M I eunrenmentat solutions 6/21/16 m.4�ow, Radiator Specialty Cc Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: Stormwater Gasoline Range Organics by GC/FID - Quality Control Prism Work Order: 6060125 Time Submitted: 6/7/2016 2:18:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6F0328 - 5030B Blank (P6F0328-BLK1) Prepared & Analyzed: 06/16/16 Gasoline Range Organics BRL 0.20 rl Surrogate: a,a,a-Trifluorotoluene 0.104 ni 0.1000 104 57-132 LCS (P6F0328-BS1) Prepared & Analyzed: 06/16/16 Gasoline Range Organics 0.983 0,20 ni 1.000 98 60-138 Surrogate: a,a,a-Trifluorotoluene 0.0950 mg1L 0.1000 95 57432 LCS Cup (P6F0328-BSD1) Prepared & Analyzed: 06/16/16 Gasoline Range Organics 1.04 0,20 mg/L 1.000 104 60-138 6 20 Surrogate: a,a,a-Trifluorotoluene 0.0930 rl 0.1000 93 57-132 Matrix Spike (PGF0328-MS1) Source: 6060125-01 Prepared & Analyzed: 06/16/16 Gasoline Range Organics 1.14 0.20 mg/L 1.000 BRL 114 69-130 Surrogate: a,a,a-Trifluorotoluene 0.114 mg1L 0.1000 114 57-132 Matrix Spike Dup (P6F0328-MSD1) Source: 6060125-01 Prepared & Analyzed: 06/16/16 Gasoline Range Organics 1.23 0.20 mg/L 1.000 BRL 123 69-130 8 24 Surrogate: a,a,a-Tiifluomloluene 0.107 ni 0.1000 107 57-132 This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax 7041525-0409 Page 4 of 7 Level II QC Report �P R ISM nEwi15ue1 nnatyiicai 8 6/21/16 Env en4J Sahemns Radiator Specialty Cc Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: Stormwater Diesel Range Organics by GC/FID - Quality Control Prism Work Order: 6060125 Time Submitted: 5/7/2016 2:18:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6F0213 - 3510C GC Blank (P6FO213-BLK1) Diesel Range Organics BRL to mg/L Surrogate: o-Terphenyl 0.0279 mg7L Les (PGF0213-BS1) Diesel Range Organics 1.67 l o mg/L Surrogate: o-Terphenyl 0,0340 m97L' LCS Dup(P6F0213-BSD1) Diesel Range Organics 208 to mg/L Surrogate: o-Terphenyl 0,0364 mg7L Matrix Spike (P6FO213-MS1) Source: 6060125-01 Diesel Range Organics 371 2.0 mg/L Surrogate: o-Terphenyl 0.0665 mg7L Matrix Spike Dup (PGF0213-MSD1) Source: 6060125-01 Diesel Range Organics 3.56 2.0 mg/L Surrogate: o-Terphenyl 0.0669 mg/L Prepared: 06/10/16 Analyzed: 06/14/16 0.04000 70 50-144 Prepared: 06/10/16 Analyzed: 06/14/16 2.000 83 53-135 0.04000 85 50-144 Prepared: 06/10/16 Analyzed: 06/14/16 2.000 104 53-135 0,04000 91 50-144 Prepared: 06/10/16 Analyzed: 06/14/16 4.000 BRL 93 51-145 0.08000 83 50-144 Prepared: 06/10/16 Analyzed: 06/14/16 4.000 BRL 89 51-145 0.08000 84 50-144 22 20 M 4 22 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 5 of 7 rewn.i' oer11 o:nnsaelya„ cal naIJ �mop�3o,. N,«,I a Level II QC Report 6/21/16 Radiator Specialty Cc Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, INC 28079 General Chemistry Parameters - Quality Control Prism Work Order: 6060125 Time Submitted: 6/7/2016 2:18:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6F0187 - NO PREP Blank (PGF0187-BLK1) Prepared & Analyzed: 06/08/16 Total Suspended Solids BRL 5o mg/L LCS (P6F0187-BS1) Prepared &Analyzed: 06/08/16 Total Suspended Solids 470 5.0 mg/L 477.0 99 90-110 Batch P6F0301 - NO PREP Blank (P6F0301-Bl Prepared & Analyzed: 06/15/16 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P6F0301-BS1) ...___..._.....___..........______._._--__—___.—______._.__.._. Prepared & Analyzed: 06/15/16 ..... _. .._— .. .... ... Oil & Grease (HEM) 34.0 5.0 mg/L 40.00 85 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 6060125-01 P61`0213 1000 mL 2 mL 06/10/16 12:20 Prep Method: 50308 Lab Number Batch Initial Final Daternme 6060125-01 P6F0328 5 mL 5 mL 06/16/16 14:43 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 6 of 7 CHAIN OF CUSTODY RECORD Full -Service Analytical & PRISM I Environmental Solutions PAGE LOF ' QUOTE Y TO ENSURE PROPER BILLING: I A INC. ` 1-' 1 '? Project Name: )itrti"1 W f� ./ 449 Springbrock Road •Charlotte, 25 28217 C Phone 7041529-G;3�64 Fax: 704/526-0409 Short Hold Analysis: (Yell (f1�1 UST Project: (Yes) (I� Client Company Name: 2 L CI. ( , h ),.h,. 'Please ATTACH any project specific reporting (OC LEVEL 111111 IV) p y \r"Ii ' provisions and/or QC Requirements Report To/Contact Name- Invoice To: %i (c1) Reporting Address C CU If 4, l�'c.. (u d �c. c� " Address: W ( (,l(.) l-d C� ck'�d— / Samples IN'L:C T u1:on ; uia,d? Received VN WET I,-, PROPER PRESS R".rAl'IVE 6 ,I-U, Peceiv,vd lVl llil 4I IOI Dw(.i 1IM 4' CUS I OUV SEALS IN l I VOLAF1- r',ilWJ'1i 1 1'LP 1 ROPI I CUNT INI IENI Th n D yLr -'I Phone: l; "- - . J Fax (Yes) (I}ip�: Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: F--�.1� .Jlf �- r�; c �7'<%�d'.1. ! :-.'� Requested Due Dale O 1 Day U 2 Days ❑ 3 Days O 4 Days U 5 Days Certification: NELAC DOD FL NC EDD Type: PDF%Excel_Other "Working Days" U6-9 Days Qiftandard l0 days ClRRrueshh Work Must Be — .-� Site Location Name: t:. S C pproved Samples received after 14:00 will be processed next tusiness day. SC OTHER N/A Site Location Physical Address: L Ot-) k(:./ 1-: <,J- Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO ` I, (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES ---'NO CLIENT DATE TIME COLLECTED MATRIX (SOIL, SAMPLE CONTAINER PRESERVA- / ANALYSIS REQUESTED j O % REMARKS ti -�.L/� /� PRISM LAB SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE NO. SIZE TIVES �,\ / j ID NO. HOURS SLUDGE) SEE BELOW �(0 „c 14C1 -"-- r r Yk'ltl� Kd A J'�- I Z � t Sampler's Signature .t-L''� l.t Sampled By (Print Name) Affiliation U'le't, )<'�. Upon relinquishing, this Chain of Custo i our authorization 'sm for Prism to proceed with the analyses as requested above. Any changes must be f'r pp 5 (1c`'.rFCiT submitted in writing to the P Proje t Manager. There will be charges for any changes after analyses have been initialized. Reling etl By. (S au ) J i ilc'7 �Jrc �7 Received '(signature) � Date / IilarylHours Additional Comments �'S r' ,� 1�'/w, G�7%Ia 355 - - RelmquishedBy'!(Slgnawre Received By: (Signature) Dale wit-1h;;;.•.r'un: /nr-: ) Rol ngelseed By: (Signature Received I -Or HnSgaLaeeraic es By: Date I 61711 Me d Ol snipmem: NOTE: ALL sAhtCOOLERS SHOULD BE TAPED SHUT WITH TODY SEALS FOR TRANSPORTATION TC THE LABORATORY. CDC Group No. SAMPLES ARE NOT NOT��ACCEPTED AND VERIFIED AGAINST CDC IL RECEIVED AT THE LABORATORY. U red E. O UPS ❑ Hand -delivered WCcrism Field Service D O:her NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: t3 NC❑SC ❑NC ❑SC El NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC CI ❑NC CI ❑NC ❑SC ❑NC ❑SC 0 -❑ ❑ n 71 n n n n STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 0001 FACILITY NAME _Radiator Specialty Company PERSON COLLECTING SAMPLE(S) Stuart Kerkhoff CERTIFIED LABORATORY(S) Prism Laboratories, Inc. Lab 4 402 Lab 4 Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 . (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Union PHON NO. (�70 j) 6R4 181 U50N OF PERMITTEE OR DESIGNEE PACE 2. Outfall No. Date Sample Collected 50050 Total Total Flow ifa Total Rainfall Suspended Solids Oil and Grease. TPH (DRO) TPH (GRO) pH mo/dd/ •r MG inches -:m /L m /L "m g /L - m /L Units 002 4/7/14 NA 1.01 24 <5.0 <1.0 <0.20 6.58 004 4/7/14 NA 1.01 15 <5.0 <1.0 <0.20 6.34 003 5/15/14 NA 2.50 13 <5.0 <1.0 <0.20 6.50 001 5/15/14 NA 2.50 <5.0 <5.0 <1.0 <0.20 6.30 err C t- Does this facility Perim ill Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _X_no (if yes. complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements OCT 0 9 2014 CENTRAL FILES DWR SECTION Outfall No. Date Sample Collected 50050 00556 1 00530 — - 00400 Total Flow- (if applicable) Total Rainfall Oil & Grease. (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/yr MG inches m /I m /I unit al/mo - Form SWU-247, lost revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date 4/7/14 Total Event Precipitation (inches): L01 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date 5/15/14 Total Event Precipitation (inches): 2.50 Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pernti ich, IIq (Date) Fonn SWU-247, last revised 2/212012 Page 2 of 2 v Full -Service Analytical 8 I S M I Environmental Solutions A01 =-LABOPATORIM MG Radiator Specialty Cc Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 NC Certification No. 402 SC Certification No. 99012 NC Onnking Water Cent No. 37735 VA Certification No. 460211 DoD ELAP: L-A-B Accredited Certificate No. L2307 ISOIIEC 17025: L-A-B Accredited Certificate No. L2307 Project: Stormwater Project No.: 4500025790 Lab Submittal Date: 0410912014 Prism Work Order: 4040187 Case Narrative 04/23/2014 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data q s a ears at the end of this case narrative. D T ' T' W' D Please call if you have any questions relating to this analytical report. APR 2 3 tJ Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference Reviewed By Robbi A. Jones President/Project Manager BRL Below Reporting Limit MOIL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Servic I S M l roaronnnee Analytical a v.eonuw e: ac Environmental Solutions Sample Receipt Summary 04/23/2014 Prism Work Order: 4040187 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 002 4040187-01 Water 04/07/14 04/09/14 Samples were received in good condition at 3.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Frea Number: 1-800/529-6364 - Fax: 7041525-0409 I Laboratory Report untia environmenal Soluuens 04/23/2014PR ISM r Radiator Specialty Co Project: Stormwater Client Sample ID: 002 Attn: Stuart Kerkhoff Prism Sample ID: 4040187-01 600 Radiator Rd. Project No.: 4500025790 Prism Work Order: 4040187 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 04/07/14 13:25 Time Submitted: 04/09/14 09:20 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GCIFID Diesel Range Organics BRL mg/L 1.0 0.042 1 18015C 4113/14 22,03 JMV P4D0236 Surrogate Rewyery Control Limits o-Terphenyl 71 % 50-144 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0.20 0.017 1 '8015C 4/17/14 20:02 ANG P4130378 Surrogate Recovery Control Limits a,a,a-Tdnuorotoluene 68 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 0.37 1 '1664A 4115/14 15:58 JAB P4D0326 Total Suspended Solids 24 mg/L 12 0.90 1 'SM 2540 D 4111/14 14:45 JAB P4D0252 This report should not be reproduced, except in its entirely. without the wd0en consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 i _ Phone: 7041529-6364-Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 ',', 1.1.Fag( J S M I runcryiee Analytical Bell,,onm:al Solutions "Ad...w.m�u,.c Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 Gasoline Range Organics by GCIFID - Quality Control Reporting Result Limit Units Level II QC Report 4/23/14 Prism Work Order: 4040187 Time Submitted: 4/9/2014 9:20:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P4D0378 - 5030B Blank (P4D0378-BLK1) Prepared & Analyzed: 04/17/14 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Trilluorololuene 0.0790 mg1L 0.1000 79 57-132 LCS (P4D0378-BS1) Prepared & Analyzed: 04/17/14 Gasoline Range Organics 1.03 0.20 mg/L 1.000 103 60-138 Surrogate: a,a,a-TriOuorofoluene 0,0890 mg/L 0.1000 89 57-132 LCS Cup (P4D0378-BSD1) Prepared & Analyzed: 04/17/14 Gasoline Range Organics 1.10 0.20 mg/L 1.000 110 60-138 7 20 Surrogate: a,a,a-Tnlluorotoluene 0.0900 ri 0.1000 90 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 23224-0543 Phone: 7041529-6364 -Tall Free Number: 1.8001529.6364 - Fax: 7041525-0409 ®" I S M I 4na., a s Enu.,ronmemai soiuuons Radiator Specialty Co Project: Slormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: 4500025790 Indian Trail, INC 28079 Diesel Range Organics by GCIFID - Quality Control Level II QC Report 4/23114 Prism Work Order: 4040187 Time Submitted: 4/9/2014 9:20:OOAM Reporting Spike Source °%REC RPD Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Blank(P4D0236-BLK1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics BRL 1.0 mg/L Surrogate: o-Terphenyl 0.0275 mg/L 0.04000 69 50-144 LCS(P4D0236-BS1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics 1.83 1.0 mg/L 2.000 92 53-135 Surrogate: o-Terphenyl 0.0294 mg1L 0.04000 74 50-144 LCS Dup (P4D0236-BSD1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics 1.76 1.0 mg/L 2.000 88 53-135 4 20 Surrogate: o-Terphenyl 0.0263 mg/L 0.04000 66 50-144 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number. 1.8001529.6364 - Fax: 704/525-0409 et �P o I S M l Fu ; en Analytical 4 ee. Solutions ®emu Radiator Specialty Co Attn: Stuart KerkhoH 600 Radiator Rd. Indian Trail, NC 28079 General Chemistry Parameters - Duality Control Project: Stormwater Project No: 4500025790 Level II QC Report 4/23/14 Prism Work Order: 4040187 Time Submitted: 4/9/2014 9:20:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4DO252 - NO PREP Blank(P4D0252-BLK1) Prepared & Analyzed: 04/11/14 Total Suspended Solids BRL so mg/L LCS (P4DO252-BS1) Prepared & Analyzed: 04/11/14 Total Suspended Solids 430 5.0 mg/L 426.0 102 90-140 Batch P400326 - NO PREP Blank(P4DO326-BLK1) Prepared & Analyzed: 04/15/14 Oil & Grease (HEM) BRL So mg/L LCS (P4DO326-BSI) Prepared & Analyzed: 04/15/14 Oil & Grease (HEM) 38.3 5.0 mg/L 40.00 96 78-114 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Daternme 4040187.01 P4D0236 1000 mL 2 mL 04/11/14 15:30 Prep Method: 5030B Lab Number Balch Initial Final Daternme 4040187-01 P400378 5 mL 5 mL 04/17/14 13:10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charitable, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 RI `- n n I Full -Service Analytical s J' V' Environmontal Solutions ' ////yy„cysnr- r. uaOMiOntES ING 449 Springbrook Road • Charlotte. NC 28217 Phone 7041529.6364 • Fax: 7041525-0409 Client Company Name: Radiator Specialty Report To/Contact Name: Stuart Kerkhoff Reporting Address: 600 Radiator Road T,`Ii nn Trail. NC 28079 CHAIN! OF CUSTODY RECORD 4 PAGE-1- OF 1 QUOTE a TO ENSURE PROPER BILLING: jarnples.INTACT upon arrivatT Stormwater Sample Yr 5 Pd 2 . Recewad ON WET ICE? Project Name: Short Hold Analysis: (Yes) (IMT DST Project: (Yes) (RLH PROPER PRESERVATIVES indicated? 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) 'Receiveq WITHIN NODDING TIMES? provisions andlor QC Requirements CUSTODY SEALS INTACT? " Invoice To: ACCts Payable '--VOLATILES iec'd,W/OUT.HEADSPACE -PROPER CONTAINERS used7'. .TEMP Therm ID:_z--ObseF Address: 600 Radiator Road T—A,',., mom=;l NTO -RTn70 YES NO NIA Phone: Fax(Yes)(M*- Purchase Order No./Billing Reference 9"500025790 TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Emall Address: skerkhofflirsvbrands.com Requested Dee Data Q l Day ❑2Days 03 Days Q4 Days ❑5Days Certification: NELAC -DoD_FL_NC EDD Type: PDFXExcel Other 'Working Days- ❑ 6-9 Days IN Standard 10 days Q Rush Work Must Be SC OTHER N/A Site Location Name: R a d i a t n r Spe r i a 1 t y Samples received after 14:00 mll be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO Site Location Physical Address: 600 Radiator (SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES ✓NO_ Rd Tndian Trail, NC 28079 RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED NIILfTARY (SOIL, WATER OR PRESERVA- TES N O O REMARKS LAB ID NO. -TYPE NO. SIZE �l� fT�. HOURS SLUDGE) SEE BELOW lJ oo q-�-iy �3;15 W I lot Nci i Sampler's Signature /V Sampled By (Print Name) Stuart Kerkhoff (Affiliation Radiator Special a Upon relinquishing, this Chain of Cust y I your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to thePrism Proct Manager. There will be cha gee for any changes after analyses have boon initialized. acsly SI &ure etc MletaryMoura Rel. sn_ ey:(s r� v:( (` Additional Comments: Site Arrival Time: . elinquisked By. (Slgnelure) ecery y: (SpnaNre) Data Site.. eIe Time: 1 Field TeFee: Gh Fe Retinqushed Y: (Sig tare) Reaelved Far groin Lsbe eterriiae By: Oat e jt- t, c'k 1 (/ Mileage: trodafShlpmenb NOTE: ALL SAMPOULLK4 SMOULO BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE IABORATORY. COC Graup No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CdCUNTIL RECEIVED AT TKE LABORATORY. rr-- O Feyyd Ex CUPS O Hen04aMered t3nilsm flab SaMu ❑Other SOLIDWASTCLA LANDFILL❑ OTHER: ES:TER: DIRINK1 UST. I NC ❑ SCATER: O NC ❑ SCE. 13�NC ❑ SC O NC I ❑ SC ❑ NC ❑ SCO NC ❑ O SC ❑ NRC ❑ SC ❑ NC SCI ❑ NC O SC 1 1 n n n ❑ ❑_ 10 ❑ ❑ ❑ 'CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL �< NC Certification No. 402 fit SC Certification No. 99012 Case Narrative ®I © Full -Service Analytical & NC Drinking Water Con No. 37735 I S M Environmental Solutions VA Certification No. 460211 04/23/2014 Dulwnnoniea tic DoD ELAP: L-A-B Accredited Certificate No. L2307 ISOIIEC 17025: L-A-B Accredited Cenificale No. L2307 - Radiator Specially Cc Project: Stormwater Stuart Kerkhoff Project No.: 4500025790 600 Radiator Rd. Lab Submittal Date: 04/09/2014 Indian Trail, NC 28079 Prism Work Order: 4040186 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM. LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference Reviewed By Robbi A. Jones President/Project Manager T M LS � U � N APR 232014 BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.80015296364 - Fax: 7041525-0409 PRISM E n, « AnSolutio 4 Env memos 9oiwions �fijv Sample Receipt Summary 04/23/2014 Prism Work Order: 4040186 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 004 4040186-01 Water 04/07/14 04/09/14 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525-0409 AID wn-so,. ce Analytical n I S M I Envl,un coca „on> 0IN Laboratory Report 04/23/2014 Radiator Specialty Co Project: Stormwater Client Sample ID: 004 Atin: Stuart Kerkhoff Prism Sample ID: 4040186-01 600 Radiator Rd. Project No.: 4500025790 Prism Work Order: 4040186 Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 04/07/14 13:35 Time Submitted: 04/09/14 09:20 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date7Time ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0,042 1 '8015C 4/12/14 12:54 JMV P4D0236 Surrogate Recovery Control Limits o-Terphenyl 58% 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0,017 1 '8015C 4117114 19:34 ANG P4D0378 Surrogate a,a,a-TriOuorololuene General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 0.37 Total Suspended Solids 15 mg/L 8.3 0.90 Recovery Control Limits 79 % 57-132 1 '1664A 4/15/14 10:35 JAB P4D0326 1 'SM 2540 D 4111114 14:45 JAB P4D0252 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Full-Sarvic� Analytical eovuonrevm Environmental Solutions Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Reporting Result Limit Units Level II QC Report 4/23/14 Prism Work Order: 4040186 Time Submitted: 4/9/2014 9:20:o0AM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P4D0376 - 5030B Blank (P4D0378-BLKt) Prepared 8 Analyzed: 04/17/14 Gasoline Range Organics BRL 0.20 mg/L Surrogate: a,a,a-Trifluomtoluene 0.0790 mg/L 0.1000 79 57-132 LCS (P4D0378-BS1) Prepared 8 Analyzed: 04/17/14 Gasoline Range Organics 1.03 0,20 mg/L loon 103 60-138 Surrogate: a,a,a-Trilluomtoluene 0.0890 mg1L 0. 1000 89 57-132 LCS Dup (P4D0378-BSD1) Prepared 8 Analyzed: 04/17114 Gasoline Range Organics 1.10 0.20 mgtL 1.000 110 60-138 7 20 Surrogate: a,a,a-Tdfluorotoluene 0,0900 nl 0.1000 90 57-132 Matrix Spike (P4D0378-MS7) Source: 4040186-01 Prepared 8 Analyzed: 04/17/14 Gasoline Range Organics 0.967 0.20 mg/L 1,000 BRL 97 69-130 Surrogate: a,a,a-Trilluorotoluene o0770 mgA 0.1000 77 57-132 Matrix Spike Cup (P4D0378-MSD1) Source: 4040186-01 Prepared 8 Analyzed: 04/17/14 Gasoline Range Organics 1.10 0.20 mg/L 1.000 BRL 110 69-130 13 24 Surrogatea,a,a-Trifluomtoluene 0.0860 mg7L 0.1000 66 57-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 6� ®Id�l] ISM u.w .on sz �c FuAnalytical En,anamallSowrian8z Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkho(f 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 Diesel Range Organics by GC/FID -Quality Control Analyse Batch P4100236 - 351 OC GC Reporting Result Limit Units Level II QC Report 4/23/14 Prism Work Order: 4040186 Time Submitted: 4/9/2014 9:20:OOAM Spike Source hREC RPD Level Result %REC Limits RPD Limit Notes Blank (P400236-BLK1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics BRL to mg/L Surrogate: o-Terphenyi 0.0275 mg/L 0.04000 69 50-144 LCS (P4D0236-BS1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics 1.83 1.0 mg/L 2.000 92 53-135 Surrogate: o-Terphenyl 0.0294 mg/L 0,04000 74 50-144 LCS Dup (P4D0236-BSD1) Prepared: 04/11/14 Analyzed: 04/12/14 Diesel Range Organics 1.76 1.0 mg/L 2.000 88 53-135 4 20 Surrogate: o-Terphenyl 0.0263 mg/L 0,04000 56 50-144 This report should not be reproduced, except in its entirety, without the written consent of Prism Lalwratories, Inc. 449 6pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: /-800/529-6364 - Fax: 704/525-0409 o, Level II QC Report �P�R ism I Fullnormcc al solutions 8 4,23„4 Environmental Solutions rgS= u- x.ro E.a— Radiator Specialty Co Project: Stormwater Prism Work Order: 4040186 Attn: Stuart Kerkhoff Time Submitted: 4/9/2014 9:20:OOAM 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes �It47SlaZrybi'a�[a79 7�: Blank(P4D0252-BLKI) Prepared & Analyzed: 04/11/14 Total Suspended Solids BRL 5.0 mg/L LCS (P4DO252-BSI) _ Prepared & Analyzed: 04/11/14 Total Suspended Solids 430 5.0 mg/L 426.0 102 90-110 Batch P400326 - NO PREP Blank (P4DO326-BLKI) Prepared & Analyzed: 04/15/14 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P4D0326-BS1) Prepared & Analyzed: 04/15/14 Oil & Grease (HEM) 38.3 5.0 mg/L 40.00 96 78-114 Duplicate (P4D0326-DUP1) Source: 4040186-01 Prepared & Analyzed: 04/15/14 Oil & Grease (HEM) 2.19 5.0 mg/L 2.38 8 18 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Daterr me 4040186-01 P4D0236 1000 mL 2 mL 04/11/14 15:30 Prep Method: 5030E Lab Number Batch Initial Final Date/rime 4040186-01 P4D0378 5 mL 5 mL 04/17/14 13:10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 P i CHAIN OF CUSTODY RECORD R I S M Full -Service Analytic al d Environmental Solutions PAGE 1 OFL-- QUOTE:- TO ENSURE PROPER BILLING: k I naonATONIF� Inc Project Name: Stormwater Sample Yr 5 Pd 2 449 one 70b 52 k Road • Charlotte, 25 2R217 gggg Phone 7041529-8364 Fax 704/525-0409 Short Hold Analysis: (Yes) t...r) UST Project: (Yes) W) Client Company Name: Radiator Specialty Please ATTACH any project specific reporting(CIC LEVEL I H III IV) provisions and/or CC Requirements Report To/Contact Name: Stuart Kerkhoff Invoice To: Acets Payable Reporting Address: 600 Radiator Road Address: 600 Radiator Road Tndian Trail. NC 28079 oon-rn Sarnpl s INTACT -upon arry I? Recmv d ON WF.T PROPER FRESERVAI VFo lnclua dr `-.Rec Ived WIl HIN.HOLDiNG TIMES? CUSTODY SEF1.5 IN ACt' - `VOLATILES:e:''d1NIOUT HEADSPACE' PROPEF 1014i AINER use61 T MIP Ihem:!D'. .Li -•a Obsera,.,�. O Phone: (A�.iq-/,Yff_ Fax (Yes)(%X Purchase Order No./Billing Reference 4500025790 TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: sly rkhnff`Rrsrhrandc_cnm Requested Due Date D 1 Day ❑2Days 03 Days 04 Days ❑5 Days Certification: NELAC DOD FL NC ✓ EDD Type: PDF,X_Excel_Other 'Working Days' ❑ 69 Days (�5tandard t0 days D Pre-Appro edust Be SC OTHER N/A Site Location Name: Radiator 9l:iC i d 1 .fir Samples received after 14:00 will be processed next business day. Site Location Physical Address: 600 Radiator Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO✓ Rd., Tndian Trail. (SEE REVERSE FOR TERMS A CONDITIONS REGARDING SERVICES NC 28079 RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES✓NO TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- O REMARKS LNa T'PE NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR nVES �` N iG I HOURS SLUDGE) SEE BELOW Cj (7 00Y y /Y 1 (3:3S w ? 11 1-4- 0.4 3 Vo. c ( Cr i I i \ e r Sampler's Signature `i Sampled By (Print Name) Staart Ke rY.hoff Affiliation Radiator SpeClal Upon relinquishing, this Chain of Custo Is lour authorization for P ' m to proceed with the analyses as requested shove. Any changes must be submitted in writing to the Prism Project Manager. There will be cha s for any changes after analyses have been initialized. Reel Ish ( lure ►l,2 ql k R By (Signs Date Mil ryMwrs Additional Comments: Sit(,,Animl lone: —' : p U�l- 1 t 1 RelingldshM y: (Sign Recelwd Bg (Sgnature) ` Date idle Departure Tung Rollnalushed{By,(SgMure) ` ,�� i Recakd For Laboratories 1D-ate __ Msthodaf5Npm& NOTE: ALLSAMPLE COOL ER SH ULOB PEDSNU WIN ST DY SEAIS FOR TRANSPORTATION TO THE LA ORATORY. LUUG PNo. SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COCCAfImL RECEIVED AT THE LABORATORY. (� tt''] V LI D 1 ❑ Fed a O UPS O HanddeWered Qr� F.1d Service ❑ Den.,-7 J(G NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: (H•tIrC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC El NC El SC ❑ NC ❑ SC ❑ NC O Sr ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC 1 n n n ❑ ❑ ❑ ❑ -_- ❑ ❑ 'CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ABIR. Full-Service Analytical & ISM I Environmental Solutions 7IABOnAtoPoES IN6 Radiator Specially Co Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 NC Certification No. 402 SC Certification No, 99012 NC Drinking Water Cert No. 37735 VA Certification No. 460211 DoD ELAP: L-A-B Accredited Certificate No. L2307 ISO/EC 170251 L-A-B Accredited Certificate No. L2307 Project: Stormwater Project No.: 4500025790 Lab Submittal Date: 05/16/2014 Prism Work Order: 4050357 Case Narrative 06/03/2014 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data. Qualifiers Key Reference RMUTT' JUN - 5 2014 r (o lcc-' Reviewed By Terri W. Cole For Robbi A. Jones Project Manager SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference k : Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 ®Ll I SnM Full-Sorvice Analytical 8 Env nm eaiuro ¢s c onantal Solutions Sample Receipt Summary 06/03/2014 Prism Work Order: 4050357 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received 003 001 4050357-01 4050357-02 Water Water 05/15/14 05/15/14 05/16/14 05/16/14 Samples were received in good condition at 2.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the wnften consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041525-0409 PRISM Full-o on f n Analytica rl en�ionmemal Solutions Laboratory Report 06/03/2014 Radiator Specialty Co Project: Stormwaler Client Sample ID: 003 Attn: Stuart KerkhoH Prism Sample ID: 4050357-01 600 Radiator Rd. Project No.: 4500025790 Prism Work Order. 4050357 Indian Trail, NC 28079 Sample Matrix: Water Time Collected. 05/15/14 08:27 Time Submitted: 05/16/14 12:15 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date rime ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0o34 1 '8015C 5123/14 19:10 JMV P4E0367 Surrogate Recovery Control Limits o-Terphenyl 104 % 50-144 Gasoline Range Organics by GCIFID Gasoline Range Organics BRL mg/L 0,20 0.034 1 '8015C 5/27/14 13,53 ANG P4E0536 Surrogate Recovery Control Limits a,lio-Triflucrotoluene 89 % 57-132 General Chemistry Parameters Oil & Grease (HEM) BRL mg/L 5.0 0.37 1 '1664A 5/30114 8'13 JAB P4Ee630 Total Suspended Solids 13 mg/L 5.0 1.0 1 'SM 2540 D 5120114 14:05 JAB P4E0393 This report should not be reproduced, except in its entirety, without the written consent o/ Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 {�.'1j1 Phone: 7041529-6364- Toll Free Number: 14001529-6364 - Fax: 7041525-0409 ;g>�Pagg,3jof,!8!� v. pService Analytical a Ev coral Solutions AhkYiism 1 Radiator Specialty Co Attn: Stuart Kerkhoff 600 Radiator Rd. Indian Trail, NC 28079 Project: Stormwater Project No.: 4500025790 Sample Matrix: Water Laboratory Report 06/03/2014 Client Sample ID: 001 Prism Sample ID: 4050357-02 Prism Work Order 4050357 Time Collected: 05/15/14 08:35 Time Submitted: 05/16/14 12:15 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dalerhme ID Diesel Range Organics by GC/FID Diesel Range Organics BRL mg/L 1.0 0.034 1 '8015C 5/23/14 19'46 JMV P4E0367 Surrogate Recovery Control Limits o-Terphenyl 100 % 50-144 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/L 0.20 0.034 1 18015C 5/27/14 14:21 ANG P4E0536 Surrogate a,a a-TnOuorotoluene General Chemistry Parameters Oil 8 Grease (HEM) BRL mg/L 5.0 0.37 Total Suspended Solids BRL mg/L 5.0 to Recovery Control Limits 96 % 57-132 1 '1664A 5/30/14 8:55 JAB P4E0630 1 'SM 2540 D 5/20/14 14:05 JAB P4E0393 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 23224-0543 Phone: 7041629-6364 - Toll Free Number; 1.8001529.6364 - Fax: 7041525-0409 Pagei4rof;8xrypf PRISM r , Ana „aa Ena coral Soimions Radiator Specialty Cc Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 Gasoline Range Organics by GC/FID - Quality Control Reporting Result Limit Units Batch P4EO536 - 5030B Level II QC Report 6/3/14 Prism Work Order: 4050357 Time Submitted: 5/16/2014 12:15:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P4E0536-BLK1) Prepared & Analyzed: 05/27/14 Gasoline Range Organics BRL 0,20 mg/L Sunogate' a,a,a-Trifluomtoluene 0.0840 mg/L 0.1000 84 57-132 LCS (P4E0536-BSI) Prepared & Analyzed: 05/27/14 Gasoline Range Organics 1.02 0.20 mg/L 1.000 102 60-138 Surrogate: ea,a-Trirluorotoluene 0. 100 mg/L 0,1000 100 57-132 LCS Dup (P4E0536-BSD1) Prepared & Analyzed: 05/27/14 Gasoline Range Organics 1.10 0.20 ni 1.000 110 60-138 8 20 Surrogate: a,a,a-Trirluorotoluene 0,0860 mglL 0,1000 86 57-132 Matrix Spike (P4E0536-MS1) Source: 4050357.01 Prepared & Analyzed: 05/27/14 Gasoline Range Organics 1.03 0.20 mg/L 1.000 BRL 103 69-130 Surrogate: a,a,a-Trirluorotoluene 0,0930 mg/L 0.1000 93 57-132 Matrix Spike Dup (P4E0536-MSD1) Source: 4050357-01 Prepared & Analyzed: 05/27/14 Gasoline Range Organics 1.11 0.20 mg/L 1.000 BRL Ill 69-130 7 24 Surrogate: a,a,a-Trirluorotoluene 0.0970 mg/L 0. 1000 97 57-132 This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 .A'. \ 1 Envu n a o$ s dP R I S M m ra, Solutions Radiator Specialty Co Project: Stormwater Attn: Stuart Kerkhoff 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 Diesel Range Organics by GC/FID - Quality Control Analyte Batch P4E0367 - 351 OC GC Reporting Result Limit Units Level II QC Report 6/3/14 Prism Work Order: 4050357 Time Submitted: 5/16/2014 12:15:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(P4EO367-BLK1) Prepared: 05/20/14 Analyzed: 05/23/14 Diesel Range Organics 6RL 1.0 mg1L Surrogate: o-Temhenyl 0.0356 mg/t. 0.04000 89 50-144 1-CS (P4E0367-BSI) Prepared: 05/20/14 Analyzed: 05/23/14 Diesel Range Organics 1.98 1.0 mg/L 2.000 99 53-135 Surrogate: o-ramhenyl 0.0576 mg/L 0,04000 144 50-144 1-CS Cup (P4E0367-BSD1) Prepared: 05/20/14 Analyzed: 05/23/14 Diesel Range Organics 1.99 1.0 mg/L 2.000 99 53-135 0.2 20 Surrogate: o-Terphenyl 0.0578 ni 0.04000 145 50-144 SR This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1.8001629-6364 - Fax: 7041525-0409 # FNb§0 *Ci!` Level II QC Report rra 6/3/14AI S M I Environmental nvionmenalsolutionns V.... n..oa... inc Radiator Specially Co Project: Stormwater Prism Work Order: 4050357 Attn: Stuart Kerkhoff Time Submitted: 5/16/2014 12:15:00PM 600 Radiator Rd. Project No: 4500025790 Indian Trail, NC 28079 General Chemistry Parameters - Quality Control Reporting Spike Source oREC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4E0393 - NO PREP Blank (P4E0393-BLKi) Prepared & Analyzed: 05/20/14 Total Suspended Solids BRL 5.0 mg/L Blank (P4E0393-BLK2) Prepared & Analyzed: 05/20/14 Total Suspended Solids BRL 5.0 mg/L Total Suspended Solids 480 5.0 mg/L 468.0 05120/14 103 90-110 LCS (P4E0393-BS2) Prepared & Analyzed: 05/20/14 Total Suspended Solids 450 5.0 mg/L 468.0 97 90-110 Batch P4E0630 - NO PREP Blank (P4E0630-BLK1) Prepared & Analyzed: 05/30/14 Oil & Grease (HEM) BRL 5.0 mg/L LCS (P4E0630-BS1) Prepared & Analyzed: 05/30/14 Oil & Grease (HEM) 33.4 5.0 mg/L 40.00 84 78-114 Duplicate (P4E0630-DUP1) Source: 4050357-01 Prepared & Analyzed: 05/30/14 Oil & Grease (HEM) BRL 5.0 mg/L 1.22 18 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final DaterTme 4050357-01 P4E0367 1000 mL 2 mL 05/20/14 8:45 4050357-02 P4E0357 1000 mL 2 mL 05/20/14 8:45 Prep Method: 5030E Lab Number Batch Initial Final Daterrime 4050357-01 P4E0536 5 mL 5 mL 05/27/14 10:19 4050357-02 P4E0536 5 mL 5 mL 05/27/14 10:19 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0S43 Phone: 7041529-6364 - Toll Free Number. 1-8001529-6364 - Fax: 7041525-0409 ISI�/II Cl AIN ®F CUSTODY RECORD Full -Service Analytical&Environmental Solutions PAGE 1 OF 1 OUOTE F TO ENSURE PROPER BILLING: /,V�gffi.&Rrs' - 160PA,DaiESINt Project Name: STormwgater Sampling, Yr 5 Pd2 449 Springbrook Road • Charlotte, NC 28217 $hort Hold Analysis: (Yes) l�'�xu ') UST Project: (Yes) M) Phone 7041529.6364 • Fax: 704)525-0409 'Please ATTACH any project specific reporting (DC LEVEL 1 II III IV) Client Company Name: Radiator Srecialty provisions and/or OC Requirements Report To/Contact Name: Stuart KerkhOff Invoice To: Accts Payable Reporting Address: 600 Rani ator Rnad Address: 600 Radiator Road Tndian Trail N(' 28079 Indian Trail, NC 28079 Samples INTACT upon arrival? Received ON' W ET ICE? PROPER PRESERVATIVES indicated? Receved WITHIN HOLDING TINIES? .CUSTODY SEALS INTACT? NCIATILES reed NJ/OUT HEADSPACE? eqn ID:VZ T � Observed'. YES NO NIA i Phone: i �Q- l jYl i Fax (Yes) (NOX Purchase Order No./Billing Reference 4500025790 TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: gkprkho f f ar gohra n d g . r:r1m_ Requested Due Date a 1 Day ❑ 2 Days O 3 Days 04 DayS O B Days Certification: NELAC_ DoD_ FL_ INC ✓ EDD Type: PDFXExcel_Other rk Must Be -Working Days" ❑ B-9 Days f,1 Standard 10 days O Rush Work SC_ OTHER NIA Site Location Name: D a r� t a t o rr 4nvr^ i l e a tv Samples received after 14:00 will be processed next business day. n Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO t/ Site Location Physical Address: 6 n n R a i a t r (SEE REVERSE FOR TERMS& CONDITIONS REGARDING SERVICES le Iced Sam Collection: YES NO P P �G Rd Tndian Trail NC 2an79 RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- L.J �. (Y.� Q) REMARKS LAB NO. SIZE SAMPLE DESCRIPTION COLLECTED MHOURICI—TARY WATEROR TIVES ` �(.-I Ok �� �(� ID NO. SLUDGE) SEE BELOW 003 Of C C, I-C NC VOA 3 Vp-MC 1-1C I t/A HcI 3 _3 Sampler's Signature - Sampled By (Print Name) GtUa rt. Yerkhoff Affiliation y Upon relinquishing, this Chain of st y Is your authorization for Prism to proceed with the analyses as uested above. Any changes must be submitted In writing to the Prism Project Manager. There will be charges for any than after analyse a e been initialized. eI rs ed (S et a s11s�Jy IS_ Received By: (SlgnoWre MiLmrY ours Additional Comments: Site Arrival Time: -r� h o Site Depantue Time'.Field Relim,wshed y: srg I ) R.ned By: (Sig- L Terh FeeReOnquonod Bg (Sgnewel Rec - or Prism b atadas By:�LI 1�� Mileage: Meta oShipment: NOT L SAMPL C SHOULD BE TAPED SHUT CUST YSEALS OR TRANSPORTATION TO THE LABORATORY. COc Group No. SA LESARE NOT AC EPTEDAND VERIFIED AGAINST CUNT ECEIVEDATTHE IABORATORY SOJW D O red Ea ❑ UPS ❑ Hand -delivered ❑ rism Field Servic ❑ ONer NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: Q'NC O SCI O NC O SC 0❑ NC ❑ SC NC ❑ SC O❑ NC ❑ SC 0❑ NC O SC El NC ❑ SC EI NC ❑ SC OO NC O SC Q 'CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (cero head space) ORf^,IN.AI IORSC Chemical Solutions a division of Radiator Specialty Company October 6, 2014 Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699 RE: Stormwater Discharge Outfall Monitoring Report Radiator Specialty Company Radiator Road, Indian Trail, North Carolina NPDES Permit No. NCS000183 Dcar Sirs: Enclosed please find two copies of Radiator Specialty Company's Stormwater Discharge Outfall Monitoring Report for monitoring period Year 5 — Period 2 as required by Part ❑1 Section E.(I.) and (2.) of National Pollutant Discharge Elimination System Permit Number NCS000183. Radiator Specialty Company appreciates the North Carolina Department of Fnvironment and Natural Resources cooperation and assistance in this matter. If you have any questions, or require any additional information, please call me at (704) 684- 1815. Sincerely, Radiator Specialty Company Stuart A. Kerkhoff Environmental Health and Safety Manager Attachments S'I'RM WA I \YRii'D2.20H DOC 600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: 800-438-4532 — Fax: 704-684-1975 — w .rscbrands.corn