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HomeMy WebLinkAboutNCG060414_DMR_20210114STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 0 4 1 4 FACILITY NAME Amazon.com Services LLC. - DRT4 COUNTY Henderson PERSON COLLECTING SAMPLES Duncan Quinn LABORATORY Eurofins Test America Lab Cert. ## �fi9 Part A: Stormwater Benchmarks and Monitoring Results Date submitted 01-14-2021 SAMPLE COLLECTION YEAR 2020 SAMPLE PERIOD ❑ Jan -June ❑■ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply ❑SA Other B FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.8 or n No discharae this period' Outfall No. pate Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 501 Within 6.0 — 9.0 120 30 10001 5001 Parameter Code - C0530 00400 00340 00556 31616 61211 Sample Point 01 12/24/2020 28 8.15 9.0 2.5 NIA NIA Sample Point 02 12/24/2020 18 8.63 <5.0 <0.69 NIA NIA Sample Point 03 12/24/2020 <5.0 8.02 <5.0 <0.67 NIA NIA Sample Point 04 12/24/2020 13 7.52 27 <0.66 N/A NIA 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SMonthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes ❑■ no (if yes, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part S *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Q IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case Of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing v,4ations." Signature of Permittee Permit Date:11/1/2018-05/31/2021 /___ Date SWU-249, Last Revised 11/5/2018 Page 2of2 urofins Environment Testing America ANALYTICAL REPORT Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-193354-1 Client Project/Site: Storm Water - Amazon Warehouses (DRT4) For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 111212021 9:12:45 AM Lauren Evans, Project Manager 1 (615)301-5034 Lauren.Evans@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNl requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. c Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoDIDOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoDIDOE) LOQ Limit of Quantitation (DoDIDOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative 1 Absent POS Positive 1 Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-193354-1 11 Eurofins TestAmerica, Savannah Page 2 of 17 1/12/2021 Sample Summary Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 680-193354-1 DRT4_SAMPLE_POINT_01_20201224 Water 12/24120 09:54 12129/20 10:00 680-193354-2 DRT4 SAMPLE_POINT_02_20201224 Water 12/24120 09:37 12/29/20 10:00 680-193354-3 DRT4_ISAMPLE_POINT_03_20201224 Water 12/2412010:41 12129/2010:00 680-193354-4 DRT4 SAMPLE POINT 04 20201224 Water 12/24/20 08:42 1212912010:00 Eurofins TestAmerica, Savannah Page 3 of 17 1 /12/2021 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID: 680-193354-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job ID: 680-193354-1 C. JOq Narrative 680-193354-1 Comments No additional comments. Receipt The samples were received on 12/29/2020 10:00 AM; the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 4.1° C. General Chemistry Method SM 2540D! The sample duplicate precision for the following sample associated with analytical batch 680-650893 was outside control limits: (680-193357-A-1 DU). The associated Laboratory Control Sample 1 Laboratory Control Sample Duplicate (LCSILCSD) precision met acceptance criteria. Method SM 254OD: Insufficient sample volume was provided to produce results within the specifications of SM 25400 which requires at least 2.5 mg dried residue with a sample volume not to exceed 1 L. A sample volume less than 1 L, that yielded less than 2.5 mg dried residue, was provided for the following sample: DRT4_ SAMPLE_POINT_03_20201224 (680-193354-3). Methods 1664B: Insufficient sample volume was available to perform a matrix spikelmatrix spike duplicate/sample duplicate (MSIMSDIDUP) associated with preparation batch 680-651693. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 17 1/12/2021 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID: 680-193354-1 Client Sample ID: DRT4_SAMPLE_POINT_01_20201224 Lab Sample ID: 680-193354-1 Date Collected: 12/24/20 09:54 Matrix. Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac Oil & Grease (HEM) 2.5 2.4 0.67 mglL 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand 9.0 J 10 5.0 mglL 01/07/21 10:54 1 Total Suspended Solids 28 6.5 6.5 mglL 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 5 of 17 1/12/2021 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID: 680-193354-1 Client Sample ID: DRT4WSAMPLE_PO1NT_02_20201224 Lab Sample ID: 680-193354-2 Date Collected: 12/24/20 09:37 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fan Oil & Grease (HEM) <0.69 2.5 0.69 mg1L 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand <5.0 10 5.0 mg1L 01/07/21 10:54 1 Total Suspended Solids 18 5.0 5.0 mg1L 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 6 of 17 1/12/2021 Client Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample 10: DRT4_SAMPLE_POINT_03_20201224 Lab Sample ID: 680-193354-3 Date Collected: 12/24/20 10:41 Matrix: Water Date Received: 12/29/20 10:00 General Chemistry Anatyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac Oil & Grease (HEM) <0.67 2.4 0.67 mg1L 01/11/21 07:55 01/11/21 10:48 1 Chemical Oxygen Demand <5.0 10 5.0 mg/L 01/07/21 10:54 1 Total Suspended Solids <5.0 5.0 5.0 mg/L 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 7 of 17 1/12/2021 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_SAMPLE_POINT_04_20201224 Date Collected: 12/24/20 08:42 Date Received: 12/29/20 10:00 General Chemistry Analyte Result Qualifier RL MDL Unit Oil & Grease (HEM) <0.66 2A 0.66 mglL Chemical Oxygen Demand 27 10 5.0 mglL Total Suspended Solids 13 5.7 5.7 mglL Job ID: 680-193354-1 Lab Sample ID: 680-193354-4 Matrix: Water D Prepares! Analyzed Dil Fac 0111112107:55 01/11/2110:48 1 01/07/21 10:54 1 12/30/20 14:43 1 Eurofins TestAmerica, Savannah Page 8 of 17 1/12/2021 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Method: 1664B - HEM and SGT-HEM Lab Sample ID: MB 680-651693/1-A Matrix: Water Analysis Batch: 651719 ME ME Analyte Result Qualifier Oil & Grease (HEM) <1.4 Lab Sample ID: LCS 680-65169312-A Matrix: Water ,Analysis Batch: 651719 Analyte Oil & Grease (HEM) Lab Sample ID: LCSD 680-65169313-A Matrix: Water Analysis Batch: 651719 Analyte Oil & Grease (HEM) Spike Added 40.0 Spike Added 40.0 Method: 5220D-2011 - Chemical Oxygen Demand Lab Sample ID: MB 680-651574/3 Matrix: Water Analysis Batch: 651574 MB MB Analyte Result Qualifier Chemical Oxygen Demand <5.0 Lab Sample ID: LCS 680-651574/4 Matrix: Water Analysis Batch: 651574 Spike Analyte Added Chemical Oxygen Demand 50.0 Job ID: 680-193354-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 651693 RL MDL Unit D Prepared Analyzed Dil Fac 5.0 1.4 mg/L 01/11/2107:55 01111/2110:48 1 Client Sample ID: Lab Control Sample Prep Type: TotalINA Prep Batch: 651693 LCS LCS %Rec. Result Qualifier Unit D %Rec Limits 33.20 mglL 83 78- 114 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 651693 LCSD LCSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 34.40 mglL 86 78-114 4 18 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac 10 5.0 mglL 01/0712110:54 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec. Result Qualifier Unit D %Rec Limits 52.1 mg/L 104 90 - 110 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 680-650893/1 Matrix: Water Analysis Batch: 650893 ME ME Analyte Result Qualifier RL Total Suspended Solids <2.5 2.5 Lab Sample ID: LCS 680-650893/2 Matrix: Water Analysis Batch: 650893 Spike Analyte Added Total Suspended Solids 951 Client Sample ID: Method Blank Prep Type: Total/NA MDL Unit D Prepared Analyzed Dil Fac 2.5 mg/L 12/3012014:43 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec. Result Qualifier Unit D %Rec Limits 926 mg/L 97 80 -120 Eurofins TestAmerica, Savannah Page 9 of 17 1/12/2021 QC Sample Results Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Method: SM 2540D - Solids, Total Suspended (TSS) (Continued) - Lab Sample ID: LCSD 680-65089313 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 650893 Analyte _Total Suspended Solids Spike LCSD LCSD Added Result Qualifier Unit 951 964 mg/L %Rec. RPD D %Rec Limits RPD Limit 101 80-120 4 25 Eurofins TestAmerica, Savannah Page 10 of 17 1 /12/2021 QC Association Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DRT4) General Chemi Analysis Batch: 650893 Lab Sample ID Client Sample ID Prep Type Matrix 680-193354-1 DRT4_SAMPLE_POINT_01_20201224 TotaUNA Water 680-193354-2 DRT4_SAMPLE_POINT_02_20201224 Total/NA Water 680-193354-3 DRT4 SAMPLE POINT_03_20201224 TbtalINA Water 680-193354-4 DRT4^_SAMPLE^_POINT_04_20201224 Total/NA Water MB 680-65089311 Method Blank TotalINA Water LCS 680-650893/2 Lab Control Sample Total/NA Water LCSD 680-65089313 Lab Control Sample Dup Total/NA Water Analysis Batch: 651574 Lab Sample ID Client Sample ID Prep Type 680-193354-1 DRT4_SAMPLE POINT 07 20201224 Total/NA 680-193354-2 DRT4_SAMPLE_POINT 02 20201224 TotaltNA 680-193354-3 DRT4_SAMPLE_POINTW_03_-20201224 TotallNA 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 TotaIINA MB 680-651574/3 Method Blank Total/NA LCS 680-65157414 Lab Control Sample Total/NA Prep Batch: 651693 Job ID: 680-193354-1 Method SM 2540D SM 2540D SM 2540D SM 2540D SM 2540D SM 2540D SM 2540D Prep Batch Matrix Method Prep Batch Water 522OD-2011 Water 5220D-2011 Water 5220D-2011 Water 5220D-2011 Water 5220D-2011 Water 5220D-2011 Lab Sample ID Client Sample ID Prep Type Matrix 680-193354-1 DRT4 SAMPLE POINT 07 20201224 TotaVNA Water 680-193354-2 DRT4_SAMPLE POINT 02 20201224 TotaitNA Water 680-193354-3 DRT4 SAMPLE—POINT-03-20201224 TotaUNA Water 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 TotaUNA Water MB 680-651693/1-A Method Blank TotaUNA Water LCS 680-65169312-A Lab Control Sample TotaUNA Water LCSD 680-651693/3-A Lab Control Sample Dup TotaUNA Water Analysis Batch: 651719 Lab Sample ID Client Sample 1D Prep Type Matrix 580-193354-1 DRT4 SAMPLE_POIN7_01 20201224 Total/NA Water 680-193354-2 DRT4—_SAMPLE_POINT_02—_20201224 Total/NA Water 680-193354-3 DRT4_SAMPLE_POINT_03_20201224 Total/NA Water 680-193354-4 DRT4_SAMPLE_POINT_04_20201224 Total/NA Water MB 680-65169311-A Method Blank Total/NA Water LCS 680-65169312-A Lab Control Sample Total/NA Water LCSD 680-65169313-A Lab Control Sample Dup TotaUNA Water Method Prep Batch 1664B 1664E 1664B 1664 t3 1664B 1664B 1664B Method Prep Batch 1664B 651693 1664B 651693 1664B 651693 1664B 651693 1664E 651693 1664B 651693 1664B 651693 Eurofins TestAmerica, Savannah C Page 11 of 17 1/12/2021 Lab Chronicle Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Client Sample ID: DRT4_ SAMPLE_POINT_01_20201224 Lab Sample ID: 680-193354-1 Date Collected: 12/24/20 09:54 Matrix: Water Date Received: 12/29/20 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664E 1050 mL 500 mL 651693 01/11/21 07:55 JAS TAL SAV Total/NA Analysis 1664B 1 651719 01/11/2110:48 JAS TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 Instrument ID: SPC7 Total/NA Analysis SM 2540D Instrument ID: NOEQUIP 1 1 2 mL 384 mL Client Sample ID: DRT4_ SAMPLE_POINT_02_20201224 Date Collected: 12/24/20 09:37 Date Received: 12/29/20 10:00 Batch Batch DO Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 1016 mL Total/NA Analysis 1664B 1 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 500 mL Instrument ID: NOEQUIP Client Sample ID: DRT4_ SAMPLE_POINT_03_20201224 Date Collected: 12124/20 10:41 Date Received: 12/29/20 10:00 2mL 651574 01/07/21 10:54 ALG TAL SAV 1000 mL 650893 12/30/20 14:43 MS TALSAV Lab Sample ID: 680-193354-2 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 651693 01111/21 07:55 JAS TAL SAV 651719 01/11/2110:48 JA$ TAL SAV 2mL 651574 01/07/2110:54 ALG TAL SAV 1000 mL 650893 12/30/20 14:43 MS TAL SAV Lab Sample ID: 680-193354-3 Matrix: Water Batch Batch Dil Initial Final Batch Prep Type Type Method Run Factor Amount Amount Number Total/NA Prep 1664B 1048 mL 500 mL 651693 Total/NA Analysis 1664B 1 651719 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 Instrument ID: SPC7 Total/NA Analysis SM 2540D Instrument ID: NOEQUIP 1 1 2 mL 500 mL Client Sample ID: DRT4_ SAMPLE_POINT_04_20201224 Date Collected: 12/24/20 08:42 Date Received: 12129/20 10:00 Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 1053 mL Total/NA Analysis 1664B 1 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 440 mL Instrument ID: NOEQUIP Prepared or Analyzed Analyst Lab 01111/2107:55 JAS TAL SAV 01111/2110:48 JAS TALSAV 2mL 651574 01/07/2110:54 ALG TALSAV 1000 mL 650893 12/30/20 14:43 MS TALSAV Lab Sample ID: 680-193354-4 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 651693 01/11/21 07:55 JAS TALSAV 651719 01/11/21 10A8 JAS TALSAV 2mL 651574 01/07/2110:54 ALG TAL5AV 1000 mL 650893 12/30/20 14:43 MS TALSAV Eurofins TestAmerica, Savannah Page 12 of 17 1/12/2021 Lab Chronicle Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 €T�1 Eurofins TestAmerica, Savannah Page 13 of 17 1/12/2021 Accreditation/Certification Summary Client: ERM-West Job ID: 680-193354-1 Project/Site: Storm Water - Amazon Warehouses (DRT4) Laboratory: Eurofins TestAmerica, Savannah The accreditationslcertifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WVVISW) Slate 269 12-31-21 0 Eurofins TestAmerica, Savannah Page 14 of 17 1/12/2021 Method Summary Client: ERIVI-West Project/Site: Storm Water - Amazon Warehouses (DRT4) Job ID: 680-193354-1 Method Method Description Protocol Laboratory 1664B HEM and SGT-HEM 1664E TAL SAV 5220D-2011 Chemical Oxygen Demand SM TAL SAV SM 2540D Solids, Total Suspended (TSS) SM TAL SAV 1664E 'HEM and SGT'-H"EM ('Aqueous) 1664E TAL SAV Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 15 of 17 1/12/2021 T w rn 0 a IV N O IV _ r-.�MYV1La 3355 McLemore Drive Chain of Custody Record Pensacola. FL 32514 Phore:850-474-1001 Fax:850-478-2671 :h eurofins ' F wiranment Testing Anwdca SarnpW: p at �Q U' US PLt Carney Tracking No(s): CDC N0- Client Information u ^ Ni It h Evans. Lauren R 240-75870-28761.1 Cfenl Contact Phone: y I f y rJ E-I.O4. Pa Doug Wade I Lauren.Evans�Etrrofnsei.com Page 1 of 2 r: ERM-West Analysis Requested Address: Dud Dab Requeated: Preservation Codes: 1920 Main Street Suite 3r)0 A HCL M • Hexane a • - N" H - Nona City: TAT Raqueatod (loya): Irvine C - Ze AONaIa 0 - ASNO02 D - N&C And P - Ha204s SIMn Tip: CA, 92614 E - NaHSO4 a - Na2So3 F-k%OH R. W28203 PO s: 443.812-0046(Tel) Purchase Order Requested G • Arndrlor S - H2SO4 H-AacabcA[M T-TSP0Wecahydrate Emaa: wop ii J. Di Water V-MCAAe x-EDTA W-pH4.5 PMpodNdGug.wade�erm.eom Hama: Starl Storm Water - FUnazon Warehouses 2402PrOOCt 2 240242BD b $ L • EDA z- new (Veciy) other: Site: r.�c- ssovrs: Hasa .�of serv�eS pR i G x e Q E Sample Matrix Type Sample (Chomp. o+,rn.a o n Sam le Identffication Sample Date Time - Tabl Special Instruct)onslNots: Preservation Code: S IN S D(ZTq — 5nr+t �a _ PoL4 _ 01 Water Il -7t`! `tt> ic{ lr Water Jf ht A .pyfi_r.7-zLl-)o water N N .Z i 1 i'f — --- - -' v `�1 n0 y; it !+'� f'lttl ��Y_�O%t171�.7.� iz-r��-Z`� �r��`� tT Water 19 Water U Water o' Water c O L _ U. Water — �r co Water m Q„ Water eo Water Possible Hazard Idenlifkarlon Sample Disposal (A fee may be assessed If samples are renWried longer than 1 month} E] Nun -Hazard 1:3Flammable Skin Irritant � Poisnn B Unknown Radiological =Rerurn To Cl enf =Disposal By l.ab Archive For Months Deliverable Requested: I, II, lit. IV. Other (specify) Special InsinxtionsICC Requirements: Empty Kit Relinquished by: jDaw Time: Matrbd or SMpmenC R*wwpi arwed by: Dne/Rne , oO Cwnparry A Recewed 'i �- Rak quirk" try: Dale/Trme' Corrpwry RWAMOd by. Dalarrm 7 Company Refnqulehed by. Datw Tyne: Company Reedlrrrd try: Oalerrre: C- mpww Custody Seals Intact Custody Seal No.: Coaw Temperalwe(s)'C and Other Remarks: e Yes a t Login Sample Receipt Checklist Client: ERM-West Job Number. 680-193354-1 Login Number:193364 List Source: Eurofins TestAmerica, Savannah List Number: 1 Creator: Mooken, Darmal Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 17 of 17 1/12/2021 January 14, 2021 Wastewater Branch Water Quality Permitting Section Division of Water Resources 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Delegation of Signature Authority AMAZON.COM SERVICES LLC. - DRT4 NPDES Permit Number NCG060414 To Whom It May Concern: By notice of this letter, I hereby delegate signatory authority to each of the following individuals for all permit applications, discharge monitoring reports, and other information relating to the operations at the subject facility as required by all applicable federal, state, and local environmental agencies specifically with the requirements for signatory authority as specified in 15A NCAC 213.0506. Individual #1 Individual #2 (ifapplicable) Name: Michael Boese Title: Business Environmental Leader Mailing Address: Na Environmental Dept Po Box 80842 Seattle, Wa 98108 Physical Address: (if different) Email Address: boese@amazon.com Office Phone: 484 - 252 - 1748 - - Mobile Phone: - - - - If you have any questions regarding this letter, please feel free to contact me at 951-445-7785. Sincerely, see attached delegation authority Michael D. Deal President, Treasurer And Secretary cc: Asheville Regional Office, Water Quality Permitting Section DocuSign Envelope ID: 11f)ECCCC-4COB-4164-917A-E418C922A295 AMAZON.COM SERVICES LLC DELEGATION OF AUTHORITY (Boese, Nickens, Wilson, Vijoykumor, Sonches) I, Michael D. Deal, being the duly elected, qualified and acting President, Treasurer and Secretary of Amazon.com Services LLC (the "Company"), and having been authorized by resolutions duly adopted by the Board of the Company, do hereby sub -delegate my authority as follows: DELEGATION OF AUTHORITY 1. Effective September 10, 2020, authority is hereby delegated to Michael Boese, Amber Nickens, Paul Wilson, Vimal Vijaykumar, and Debora Sanches ("Authorized Representatives") to act on behalf of the Company and in its name and place to execute and file environmental and permitting applications, and related documents with government authorities. This Delegation of Authority shall not include any authority to commit spend on behalf of the Company. SUBDELEGATION 2. The Authorized Representatives are not authorized to subdelegate the authority granted to them in this delegation. TERM OF DELEGATION 3. The authority delegated hereby shall terminate upon the earlier of: (i) when revoked by the Company, the undersigned, any successor in responsibility to the undersigned, or any person to whom the undersigned reports; or (ii) immediately upon the cessation of the Authorized Representative's employment by Amazon.com, Inc. ("Amazon"), the Company, and Amazon's affiliates. 4. The authority delegated herein shall remain in full force and effect until terminated in accordance with Section 3 of this Delegation of Authority regardless of the appointment status of the undersigned with the Company. DATED: September 10, 2020 OocuS4n*d by: y-411 X Michael D. Deal President, Treasurer and Secretary