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Home My WebLink AboutNCS000391_MONITORING INFO_20190213P� 0 STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO, !Y DOC TYPE ❑ FINAL PERMIT X MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTH ER OC DATE ❑ YYYYM M D D STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000391 SAMPLES COLLECTED DURING CALENDAR YEAR: 2020 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME The Goodyear Tire & Rubber Co. COUNTY Cumberland PERSON COLLECTING SAMPLE(S) Elijah Herrington PHONE NO. (_910_) 630-5678 CERTIFIED LABORATORY(S) Microbac Fayetteville Division Lab # 11 Lab 4 FQUI NATURE OF PERMiTTEE OR DESIGNEE REDON PAGE 2. Part A: Specific Monitoring Requirements (Tier 2 Sampling Event for Zinc) Outfall No. Date Sample Collected 50050 Total Flow (if app.) Total Rainfall COD, Total Oil & Grease Total Suspended Solids Zinc, Total Thiram pH, Field mo/dd/ yr MG inches M /l M /I M /l Mg/1 M Il S.U. 001 1/13/20 1 28.4 <5.0 20.4 0.142 7.42 002 1 /13/20 1 97.3 <5.0 11.2 0.074 7.58 E ZU J .r- f1Al Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _X_no (if yes. complete Part B) Part B: Vehicle Maintenance Activity Monitoring Re2uirements NIA Outfall Date 50050 00556 00530 00400 Total Flow Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if appl. mo/dd/vr MG inches mall m /i unit al/mo Form S W U-247 Page i of 2 STORM EVENT. CHARACTERISTICS: Date 1/13/20 Total Event Precipitation (inches): 1 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable —see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 2 (Date) Form SWU-247 Page 2 of 2 4,L#W M I C R 0 B A C @) Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOA0263 Project Description Stormwater Samples - Monthly For: Mr. Carlton Williams Goodyear Tire and Rubber Co. 6650 Ramsey Street Fayetteville, NC 28311 Administration Brittany Smith Friday, January 24, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. if you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received, Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 7 0MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOAO263 Goodyear Tire and Rubber Co. Project Name: Stormwater Samples - Monthly Mr. Carlton Williams Project 1 PO Number: NIA 6650 Ramsey Street Received: 01/16/2020 Fayetteville, NC 28311 Reported: 01/24/2020 Case Narrative Field pH (by client): 01:7.42 02:7.58 Rainfall: V Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Outfall #1, Grab KOA0263-01 Aqueous Grab Outfall #2, Grab KOA0263-02 Aqueous Grab Sample Begin Sample Taken Lab Received 01/13/20 09:10 01 /16120 14:29 01/13/20 08:55 01/16/20 14:29 Page 2 of 7 �VMICROBAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOA0263 Analytical Testing Parameters Wcsaaa3 Client Sample ID: Outfall #1, Grab Sample Matrix: Aqueous Collected By: Client Lab Sample ID: KOA0263-01 Collection Date: 01/13/2020 9:10 Wet Chemistry Result MDL RL Units Dilution Nate Prepared Analyzed Analyst Method: EPA 1664 Rev. B Oil & Grease (HEM) <5.0 5.0 mgJL 1 01/24/20 1020 TBM Method: SM 2540 0-2011 Total Suspended Solids 20.4 4.44 mglL 1 01/17120 1025 CLB Method: SM 4500 H+13-2011 pH at 25 °C 6.7 1.0 S.U. 1 H C1121120 1542 CLB Method: SM 5220 D-2011 COD, Total 28.4 10.0 mg1L 1 01121/20 0902 MT Metals Result MDL RL Units Dilution Note Prepared Analyzed Analy_ Method: Metals AqueouslEPA 200.7 Rev 4.4 1994 Zinc 0.142 0.005 mg1L 1 01122/20 1246 01/22/20 1246 TBM Client Sample ID: Outfall #2, Grab Sample Matrix: Aqueous Collected By: Client Lab Sample 10: KOA0263-02 Collection Date: 01/13/2020 8:55 Wet Chemistry Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: EPA 1664 Rev. B Oil & Grease (HEM) <5.0 5.0 mg1L 1 01/24120 1020 TBM Method: SM 2540 D-2011 Total Suspended Solids 11.2 4.17 mglL 1 01/17/20 1025 CLB Method: SM 4500 H+B-2011 pH at 25 'C 6.8 1.0 S.U. 1 H 01121/20 1542 CLB Method: SM 5220 D-2011 COD, Total 97.3 10.0 mg/L 1 01/21/20 0902 MT Metals Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: Metals AqueouslEPA 200.7 Rev 4.4 1994 Zinc 0.074 0.005 mg/L 1 01/22/20 1250 01/22/20 1250 TBM Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 3 of 7 VMICROBAC�' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOA0263 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD Wet Chemistry Result RL Units Level Result %REC Limits RPD Limit Notes Batch KA01519 - Wet Chem Aqueous - SM 2540 D-2011 Blank (KA01519-BLKI) Prepared &Analyzed: 0111712020 Total Suspended Solids <2.50 2.50 mg1L Blank (KA01519-BLK2) _ Prepared & Analyzed: 01/17/2020 Total Suspended Solids <2.50 2,50 mg1L Blank (KA01519-BLK3) Prepared & Analyzed: 01/17/2020 Total Suspended Solids <2.50 2.50 _ mg1L LCS (KA01519-BSI) Prepared &Analyzed: 01/17/2020 Total Suspended Solids 29.8 2.50 mg1L 30.7 97 94.5-105.4 Duplicate (KA01519-DUPI) Source: KOA0252-01 Prepared &Analyzed: 01/17/2020 Total Suspended Solids 78.0 2.50 mg1L 78.0 0 10 Duplicate (KA01519-DUP2) Source: KOA0255-01 Prepared & Analyzed: 01/17/2020 Total Suspended Solids 40.0 2.50 mg/L 44.0 10 10 Batch KA01718 - Wet Chem Aqueous - SM 5220 D-2011 Blank (KA01718-BLKI) Prepared &Analyzed: 01/21/2020 COD, Total <10.0 10.0 mg1L Blank (KA01718-BLK2) Prepared & Analyzed: 01/21/2020 COD, Total <10.0 10.0 mg1L LCS (KA01718-BS1) Prepared &Analyzed: 01/2112020 COD, Total 499 10.0 mg1L 500 100 90-110 Duplicate (KA01718-DUPI) Source: KOA0250-01 Prepared & Analyzed: 01/21/2020 COD, Total 31.4 10.0 mg1L 29.4 7 20 Matrix Spike (KA01718-MS1) Source: KOA0250-01 Prepared &Analyzed: 01/21/2020 COD, Total 54.4 10.0 mg1L 25.0 29.4 100 80-120 Batch KA01742 - Wet Chem Aqueous - EPA 1664 Rev. B Blank (KA01742-BLKI) Prepared & Analyzed: 0112412020 Oil & Grease (HEM) <5.0 5.0 mg/L LCS (KA01742-BS1) Prepared & Analyzed: 0112412020 Oil & Grease (HEM) 36.7 5.0 mg/L 40.8 90 83-101 Matrix Spike (KA01742-MS1) Source: KOA0338-01 Prepared &Analyzed: 01/24/2020 Oil & Grease (HEM) 30.0 5.0 mg/L 39.6 ND 76 78-114 Metals Result RL Batch KA01729 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 Spike Source %RI:C Units Level Result %REC Limits Blank (KA01729-BLK1) _Prepared & Analyzed: 01/22/2020 Zinc <0.010 � 0.010 mglL��__�_ RPD RPD Limit Notes Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7 �DMICROBACr' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOA0263 Spike Source %REC RPD Metals Result RL Units Level Result %REC Limits RPD Limit Notes Batch KA01729 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 LCS (KA01729-BSI) Prepared &Analyzed: 01/22/2020 Zinc 0.250 0.010 mg/L 0.250 100 85-115 --� LCS (KA01729-BS2) Prepared & Analyzed: 01/22/2020 Zinc 0.255 0.010 mg/L 0.250 102 85-115 Duplicate (KA01729-DUPI) Source: KOA0196-01 Prepared &Analyzed: 01/22/2020 Zinc 0.050 0.005 mg1L 0.048 4 10 Duplicate (KA01729-DUP2) Source: KOA0298-01 Prepared & Analyzed: 01/22/2020 Zinc 0.050 0.005 mglL 0.059 17 10 Matrix Spike (KA01729-MSI) Source: KOA0196-01 Prepared & Analyzed: 01/22/2020 Zinc 0.303 0.005 mglL 0.250 0.048 102 70-130 Matrix Spike (KA01729-MS2) ............ ---.--.-----------.----....................... _...-......_......_._._....._.__._...-----.___.--------- Source: KOA0298-01 ------------ - ------------ Prepared & Analyzed: 01/22/2020 - _..._ — - ------ — Zinc 0.314 0.005 mglL 0.250 0.059 102 70-130 Matrix Spike Dup (KA01729-MSDI) —..---------------- ---- - -- ----.... Source: KOA0196-01 -----------------.-.-.-.-.,..,..-.-.,..---------------,..,..,._ Prepared & Analyzed: 01/2212020 .............................----------- -- ------------- ---- -- --- --- --- Zinc 0.291 0.005 mglL 0.250 0.048 97 70-130 4 30 Matrix Spike Dup (KA01729-MS02) Source: KOA0298-01 Prepared & Analyzed: 01/22/2020 Zinc 0.287 0.005 mg1L 0.250 0.059 91 70-130 _ 9— 30 — Reference (KA01729-SRMI) Prepared & Analyzed: 01/22/2020 Zinc 1.98 0.010 mglL 2.00 99 95-105 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 7 VMICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOA0263 Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time mg/L: Milligrams per Liter RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Cooler Receipt Log Cooler 10: Default Cooler Temp: 3.2°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to 1 applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) anaWed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 0112412020 21 A2 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 7 1 I Fayetteville Division 2592 Hope Mills Road -- Fayetteviile, NC 28306 (910) 864-1920 / 864-8774 fax CHAIN OF CUSTODY RECORD 111111111,1111511191 PAGE 1 OF i CLIENT NAMESADDRESS: PO# Goodyear Tire and Rubber Company 6650 Ramsey Street Fayetteville, NC 28311 PROJECT fLOCATION: Goodyear - fa etteville S T T L E TYPE OF ANALYSIS PRESERVATION CODE # O i i � }— 6 O 0- d r C IV CODE: A =None B = HNO3f(PH<2) + <4°C G= H2SO4'(pH<2) + <4°c D= NaOH + <4°CG E __ZN Acetate.+ <4'C F = HCI CONTACT PERSON: Elijah Herrington PHONE 910-630-5678 SAMPLER: CMS DATE 1 METHOD OF SHIPMENT: LAB ID # SAMPLE�TYPE DATE TIME COMP GRAB pH D.O. TEMSP•C RES' CHLORINE outfall # 1 Stormwater �� ` iD x x x x x x z 1_2 Outfal #2 Stormwater 1/1 '?%r x x I x x x x Relinquished by: 1 Date 11 Time ; 5 Received by: {Signature) ,7 z Date /-1f 1() Time l2;2.6 Relinquish d 1by- Date / firn. Recei y: { gnu _ 4 Date Time Rel:ngtrip�hed y: ��VV Date 7p Time Recei ed by: nature Da e !, Time, 3 3 5 -lG 1-3 6cJ Comments or Special Hazards: REVIEWED a-4. f ( of I Page 7 of 7