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HomeMy WebLinkAboutNCS000370_COMPLETE FILE - HISTORICAL_20191217December 12, 2019 North Carolina Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 BRIDGESTONE AMERICAS TIRE OPERATIONS, LLC Wilson Plant P.O. Box 1139 Wilson, North Carolina 27894-1139 RECEIVED DEC 7 2018 CEN7i_ Fl b Wei SECTlO Re: Storm water Sampling Year 10, Period 1 Analytical Results Dear Sir or Madam. - Enclosed is an updated DMR for the Bridgestone Americas Tire Operations, LLC (BATO) Wilson Plant. On December 10, 2019, Bridgestone received an updated lab report from Pace Analytical. The reported result for TSS from the South outfall had been incorrectly reported on the original lab report. The DMR has been updated with the correct TSS for the South outfall. The BATO-Wilson facility operates under National Pollutant Discharge Elimination System (NPDES) permit number NCS000370. The permit requires semi-annual quantitative sampling of storm water at the facility's two outfalls. The outfalls are named by their geographic locations, South and East. Please find the analytical results and Storm Water Outfall Discharge Monitoring Reports for the Sampling Year 10 Period 1 for the South and East outfalls in the Attachment. The samples were collected on November 11, 2019. The analytical results were received from the laboratory via electronic mail at BATO Wilson on November 21, 2019. As required, the original and one copy are enclosed. If you have any questions concerning this report, please contact Tausha Fanslau at (252) 246-7485. Sincerely, Vergil Norrod Plant Manager BATO — Wilson Plant cc: BATO Wilson Environmental Department pAMy Documents\Water-Stormwater\Files19 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000370 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Bridgestone Americas Tire Operations, LLC PERSON COLLECTING SAMPLE(S) Tausha FansIau R EI �/ ED CERTIFIED LABORATORY(S Pace Analytical DEC 17 20l9 Part A: Specific Monitoring Requirements COUNTY Wilson PHONE NO. ( 252 j 246-7485 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected Total Flow. (if app.) Total Rainfall ZINC (t)' COD TSS TPH PH mo/dd/ r MG- inches Mg/L. M /L MIL" MIL East 11/12/2019 0.47 0.0246 <25 4.7 < 5 6.4 South 11/12/2019 0.47 0.154 <25 30.2* 5.0 6.2 *Updated due to a lab error, see attached corrected lab report Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date ;50054 40556 00530 00400 Total Flow (if applicable) Total, : Ra�nfalh `,Oil &-Grease :. {if-appC) Non -polar O&GITPH' (Method 1'664 - Total - Suspended Solids. pH New Motor Oil Usage No.- Sample- . Collected t SGT-HEM); if a 1 moiddi r MG inches ` m /L. mg/1 unit at/mo Form SWU-247, last revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date 11/12/2019 Total Event Precipitation (inches): _0.47 Event Duration (hours): 4.0 (only if applicable -- see permit.) (if more than one storm event was sampled) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date Form SWU-247, last remised 21212012 Page 2 of 2 (�IacieAnalyticalo www.pacelahs.com December 10, 2019 Tausha Fanslau Bridgestone Americas 3001 Firestone Parkway Wilson, NC 27893 RE: Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Dear Tausha Fanslau: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 14, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. This revision was issued on 12/10/19 to correctly report the TSS data for sample "SOUTH" (92453778001). The TSS data in the original report was reported due to an analyst error. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski for Amanda Payne amanda.payne@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, . without the written consent of Pace Analytical Services, LLC. Page f of 15 lacmnalyficalo wwarpacilats.cam CERTIFICATIONS Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Pace Analytical Services Charlotte Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certiflcation #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 laceAnalytrcal www.pecelds.cors SAMPLE ANALYTE COUNT Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92453778001 SOUTH EPA 1664B HH 1 PASI-C EPA 200.7 Rev 4.4 1994 KQ 1 PASI-A SM 2540D•2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92453778002 EAST EPA 1664B HH 1 PASI-C EPA 200.7 Rev 4.4 1994 KQ 1 PASI-A SM 2540D-2011 CJL 1 PAS I -A EPA 9040C ECH 1 PASI-A SM 52200-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3of15 acleAnalytical WM."Colabf.com ANALYTICAL RESULTS Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SOUTH Parameters Lab ID: 92453778001 Collected: 11/12/19 13:10 Results Units Report Limit DF Received: 11/14/19 09:04 Matrix: Water Prepared Analyzed GAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16646 Total Petroleum Hydrocarbons 5.0 mglL 4.8 1 11/20/19 15:17 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Zinc 154 ug1L 10.0 1 11/16/1912:39 11/18/1906:29 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 30.2 mglL 5.0 1 11/18/19 18:56 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.2 Std. Units 0.10 1 11/17/19 14:50 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 52200-2011 Chemical Oxygen Demand ND mg/1- 25.0 1 11/19/19 16:37 11/19/19 23:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/10/2019 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 (�IaneA'nalyfical' www.pacataftsxam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntorsville, NC 28078 (704)875-9092 Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Sample: EAST Lab ID: 92453778002 Collected: 11/1211913:30 Received: 11/14/1909:04 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 11/20/19 15:17 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Zinc 24.6 ug1L 10.0 1 11/16/19 12:39 11/18/19 06:33 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 4.7 mg/L 2.5 1 11/18/19 18:57 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 1 11/17/19 14:55 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 11/19/19 16:37 11/19/19 23:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/10/2019 1218 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 Pace Analytical Services, LLC aceAnalytical 9eoaKinoeyAve. Suite Huntersville, NC 2807878 www.potollbs.com (704)875-9092 QUALITY CONTROL DATA Project: SLormwaler Sampling -Revised Report Pace Project No.: 92453778 QC Batch: 510729 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92453778001, 92453778002 LABORATORY CONTROL SAMPLE: 2739945 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 22.1 110 64-132 MATRIX SPIKE SAMPLE: 2739946 35510490004 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 51.4 19.6 88.9 192 64-132 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/10/2019 12:18 PM without tho written consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalyltical www.picalabs.com Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 QC Batch: 509903 QC Batch Method: EPA 200.7 Rev 4.4 1994 Associated Lab Samples: 92453778001, 92453778002 METHOD BLANK: 2736512 Associated Lab Samples: 92453778001. 92453778002 Parameter Units Zinc ug1L QUALITY CONTROL DATA c Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 10.0 11/18/19 05:07 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntorsville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2736513 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Zinc ug/L 500 478 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736514 2736515 MS MSD 92452973001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Zinc ug/L 153 500 500 619 640 93 97 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736516 2736517 MS MSD 92453397008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Zinc ug/L 0,23 500 500 733 715 101 98 70-130 2 mg/L Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 12/10/2019 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 7 o1 15 aceAnalytical www.paeataba.eon QUALITY CONTROL DATA Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 QC Batch: 510251 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92453778001, 92453778002 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2737978 Matrix: Water Associated Lab Samples: 92453778001, 92453778002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/18/19 18:51 LABORATORY CONTROL SAMPLE: 2737979 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE: 2737980 92453632001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 44.9 51.7 14 SAMPLE DUPLICATE: 2737981 92453776004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 40.2 39.4 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12110/2019 12:18 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 15 aceAnalXical www,jmcgllbs.com QUALITY CONTROL DATA Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 QC Batch: 509994 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92453778001, 92453778002 SAMPLE DUPLICATE: 2736835 92452727001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.9 7-7 2 H3 SAMPLE DUPLICATE: 2736836 Parameter pH at 25 Degrees C 92453279001 Dup Units Result Result Std. Units 5.9 5.4 RPD Qualifiers 8 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12110/2019 12:18 PM without the written consent of Pace Analytical Services, L.L.C. Page 9 of 15 (�15'ne Analytical wrww.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 510477 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92453778001, 92453778002 METHOD BLANK: 2738904 Matrix: Water Associated Lab Samples: 92453778001, 92453778002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 11/19/19 23:16 LABORATORY CONTROL SAMPLE: 2738905 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 757 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738906 2738907 MS MSD 92453323001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 100 100 106 103 103 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738908 2738909 MS MSD 92453776001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 327 100 100 444 444 118 118 90-110 0 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/10/2019 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 (�IacieAnalyfical" www.pacalabs.can QUALIFIERS Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzone using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/10/2019 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling -Revised Report Pace Project No.: 92453778 Analytical lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92453778001 SOUTH EPA 1664B 510729 92453778002 EAST EPA1664B 510729 92453778001 SOUTH EPA 200.7 Rev 4.4 1994 509903 92453778002 EAST EPA 200.7 Rev 4.4 1994 509903 92453778001 SOUTH SM 254OD-2011 510251 92453778002 EAST SM 2540D-2011 510251 92453778001 SOUTH EPA 9040C 509994 92453778002 EAST EPA 9040C 509994 92453778001 SOUTH SM 5220D-2011 510477 92453778002 EAST SM 5220D-2011 510477 Date: 12/10/2019 12:18 PM G REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. EPA 200.7 Rev 4.4 1994 509934 EPA 2007 Rev 4.4 1994 509934 SM 5220D-2011 SM 5220D-2011 510531 510531 Page 12 of 15 Laboratory receiving samples: Asheville 0 Eden[] Greenwood ❑ Huntersvlle ❑ Raleigh[g MechanicsvilleE Client Name: (WO 92458778 {{ • Project tip r`f. 11 Courier ❑Fed Ex UP5 ❑USP5 Client II Jill' fll]'.111 [] Commercial JDpace Other: 92453778 Custody Seal Present? []Yes gNo - Seals Intact? []Yes allo `_ Date/Initials Person Fxamfning Contents: N57- I f l /9 Packing Material: Bubble Wrap • []Bubble Bag_ s E]None ❑ Other Biological Tissue Frozen? Thermometer. Dyes []No BN/A AIR Gun ID: q ,. Type of ice: , Wet []Blue QNane Cooler Temp ('C). - 3 Correction Fact , u j ®• Q p { 1 _ 3 Temp should he shave freezing to 6'C Cooler Tem Corrected 'C : O • ❑Samples out of temp criteria. Samples on lie, coaling process has begun USDA Regulated Soil (® N/A, water sample) Did samples orlglnate In a quarantine zone within the United States: CA, NY, or SC (check maps)? ❑Yes ❑No Old samples orlginate from a foreign source (internationally, Ineludlne HawAll and Puerto RlcolT ayes r1bla Comments/Dlscrepanty: Chain of Custody present? Yea No N/A 1. Sames Arrived within Hold 7ime7 ❑No N/A 2. ld Time Anal Is (<72 hr.j? �Yeaj ESNo N/A 3. Rush Turn Around Time Re uested? QYes Na N/A 4. SufticlentVolume7 Joyes No EIKA 5. Correct Containers Used? -Pace Containers Used? )BYes es []NO No ❑N/A N A 6. Containers Intact? Yes []No N/A 7. Oissolvedanol :5am Ies Field Filtered? Dyes JDuo A I a. Sample Labels Match COC? -Includes Date/Time/ID/Analysts Matrix: Pes ❑No ❑H/A 9. Heads ace In VOA Vials (>5.6mm)7 QYF3 Na N/A 10. Trip Blank Present? Trip Blank Custody S61SPresent7 ❑Yes es ❑No QND /A /A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes []NO Person contacted: Date/Time: Project Manager SCURF Review: Date:, _ L_i Project Manager 5RF Review: 1, Date: Page 13 of 15 *Check mark top half of box If pH and/or dechlorinatlan Is verified and wlthln the acceptance range for preservation samples. - Exceptions: VOA, Collform, TOC, Oil and Grease, DROIB015 (water) DOC, LLHg "Bottom half of box Is to list number of bottle W0 22453??5 `y Project h , PM: AP Due Date: 11/21/19 CLIENT.. 92-BFUSA .Z.. C C c a V V U S u u - W n O. J vE c E 3 j a d i A a x 6 Z Q V �] n 7 % l7 FI -k }� J J �J gE E E ��, 2 N a per, er m m 3 y 9 Q d EE a 7 a '+ 2 l7 a z v 1n c rJ 131�rt l7 a N QL L H E a ° ., a ry y y$ N z u J 5�� ern! n'1 l7 a 2 J E `r� J. a e�5 17 a z Z (VOVj Y. 0 I Z a4 E E Y 7 x F- l9 _ •z C q 6 E l7 Q QQ Om. I O % E Y a m y y L ii p '°, 1'- X O a z j n' F' > .o A z yyZ�, a y •C E ` FF a Ln y d T y E AI N u ui a a qE ': I aa a m ? ywt. Z n i7 J p E g N 7 3 L7 a M A �i a E 4 5 t7 o 1 2 I 1 I 3 4 N \\N 5 6 7 9 10\�Ni ,11 i2 N '_M_ • pH Adjustment Log for Preserved Samples Sample ID Type of preservative pH upon receipt Date preservation adjusted Time preservation Adjusted Amount of preservative added tot # Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Ceruflcatlort Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect cantalners. Page 14 of 15 +.� a ., ti r•. _. 1� Section A Required aiwd kdorn adon: - _.� .: .. :.1:- -: o"Section BV Required Project Worrnuslat .. _.. .�--_.... ... _.. 1. .- . .. CHAIN -OF -CUSTODY! Analytical Request Document The Chaim -Of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed ac Sactioa C hraoice Irforrmfiom. 7. wmtely. Page: I _ Of 1 of on CO d iCw PwrY• Brbpwone Amfrj ha FansLau A�dorea>: 30p1 Firestone To: CornpartY Name: Wason. NC 27e53 F r: Saru usewfn Pxe Chula=324674M F— iUOrder Staffmvu er I Pecs Projocl Marf -, arnarda abe.mm. AzfZir ' OR2 Roquested Oue Dote: Pate PreSk 0: aso" _ MC SAMPLE ID One Character per box 1A-7. sample 41s meat be rarque LU LU �. SOUTH 'a`��:.� EAST 8 0 M+tsicc LY:oE n u C DM, wr aw VOW LY wawwas[ ww v' $ V Rma P OW939:tl SL a OL S p tti START W�. � A. ur W Cars OT is o V e E].TE T wr wr itlil5 ii z - O _ V i�+ t 0 mLU END u !O O z �' S r � � g ••- S o N 1J RE .i 4,4` or SAliILER: —� OI SAMMER: NEW F k: U ' 3 "776 -.f