NCS000330_MONITORING INFO_20190717

AA'T0
STORMWATER DIVISION CODING SHEET
NCS PERMITS
NO.
�vv-�3�
NLSPERMIT
DOC TYPE
❑FINAL PERMIT
MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
0 OTHER
DOC DATE
❑ � � I l U 1 l 7
YYYYMMDD

3*ATI
July 13, 2019
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
P.O. Box 5030
2020 Asheraft Avenue
Moram, NC 28111-5030
Phone: (7N)289.4511
Fax: [phone]
Email: Tyler Meraer@X11metals,cum
RECEIVED
JUL 17 2019
CENTRAL FILES
DWR SECTION
Attached, please find stormwater monitoring data for Permit No NCS000330. "Ilw originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Numberl
Start
I End
Year 10-11eriod 2
1 20
IMarch 1, 2019
August 31, 2019
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
"I certify, under penalty of law, that this document and all attachrne►►ts were prepared
under my direction orsupervision in accordance with a system desig►►ed to assure that
rlitalif <ed personnel properly Slather and evaluate the information suhnritted. Based on my
inquiry of the person or persons who manage the system, or those persons directly
respeinsible forgathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. l ant aware that there are significant
penalties forsubrnitting false information, including the possibilityof'fines and
imprisonment fbrknowbW violations."
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
* 'h�"`."
Tyler Mercer
El IS Manager

aceAnalytrcal
wnvw.PKelabs.eom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Ytuntors,Ale, NC 28078
[phone]
June 17, 2019
Tyler Mercer
AT) Specialty Materials
2020 Ashcraft Avenue
Monroe, NC 28110
RE: Project: Monroe Stcrmwater
Pace Project No.: 92432139
Dear Tyler Mercer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
Mike McManus, ATI Specialty Metals
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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aceAnaIXical
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Pace Analytical Services, LLC
9800 Kincey Aye. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Monroe Stormwater
Pace Project No.: 92432139
Charlotte Certification IDs
9800 KinceyAve, Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #'. 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
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aceAnalytical ffi
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Monroe Stormwater
Pace Project No.: 92432139
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92432139001
Monroe SW02
SM 2540D-2011
MJP
1
PASI-A
92432139002
Monroe SW02
SM 521OB-2011
JM1
t
PASI-A
92432139003
Monroe SW02
SM 5220D-2011
GC
t
PASI-A
92432139004
Monroe SW02
EPA 200.7 Rev 4.4 1994
DS
5
PASI-A
92432139005
Monroe SW02
EPA 1664B
JMS
t
PASI-C
REPORT OF LABORATORY ANALYSIS
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aceAnalytrcal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92432139
Sample: Monroe SW02 Lab ID: 92432139001 Collected: 06/07/19 09:15 Received: 06/07/19 11:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
Field Data Analytical Method
Collected By
TL
1
06/07/19 09:34
Collected Date
06/07/19
1
06/07/19 09:34
Collected Time
09:25
1
06/07/19 09:34
pH
7.5 Std. Units
0.10 1
06/07/19 09:34
Temperature
22.4 deg C
0.50 1
06/07/19 09:34
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Total Suspended Solids 20.1 mg/L 3.6 1 06/13/19 12:33
REPORT OF LABORATORY ANALYSIS
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Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18

(!;a'cie Analytical�
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ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92432139
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersvitte, NC 28078
[phone]
Sample: Monroe SW02 Lab ID: 92432139002 Collected: 06l0711909A7 Received: 06/07/19 11:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Clual
521OB BOD, 5 day Analytical Method: SM 521 OB-2011
BOD, 5 day 18.2 mg?L 2.0 1 06/08/19 02:59 06/12/19 22:46 L2
Date: 06/17/2019 06:23 PM
REPORT OF LABORATORY ANALYSIS
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Page 5 of 18

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92432139
Sample: Monroe SW02 Lab ID: 92432139003 Collected: 06/07/19 09:19 Received: 06/07/19 11:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quai
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand 114 mg/L 25.0 1 06/12/19 17:45 06/13/19 16:43
Date: 06/1712019 06:23 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 KinceyAva, Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92432139
Sample: Monroe SW02 Lab 1D: 92432139004 Collected: 06/07/19 09:20 Received: 06107/19 11:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4A 1994
Cadmium
ND
uglL
1,0
1
06/12/19 21:43
06/16/19 00:45
7440-43-9
Chromium
28.7
uglL
5.0
1
06/12/19 21:43
06/16/19 00:45
7440-47-3
Lead
NO
uglL
5.0
1
06/12/19 21:43
06/16/19 00:45
7439-92-1
Nickel
202
uglL
5.0
1
06/12/19 21:43
06/16/19 00:45
7440-02-0
Zinc
628
ug1L
10,0
1
06/12/19 21:43
06/16/19 00:45
7440-66-6
REPORT OF LABORATORY ANALYSIS
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aceAnalytrcal
wuw.pacebbs.c=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92432139
Sample: Monroe SW02 Lab ID: 92432139005 Collected: 06/07/19 09:22 Received: 06/07/19 11:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
Date: 06/17/2019 06:23 PM
Analytical Method: EPA 1664E
ND mg1L 4.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, l.l.C.
06/13/19 06:16
Page 8 o1 18

0
acmnaVical
wit wpacelabs,corn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92432139
QC Batch: 480855 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92432139005
METHOD BLANK: 2601096 Matrix: Water
Associated Lab Samples: 92432139005
Blank
Parameter Units Result
Total Petroleum Hydrocarbons mg/L ND
LABORATORY CONTROL SAMPLE: 2601097
Spike
Parameter Units Conc,
Total Petroleum Hydrocarbons mg/L 19.2
Reporting
Limit Analyzed Qualifiers
4.8 06/13/19 06:05
LCS LCS % Rec
Result % Rec Limits Qualifiers
21.3 111 64-132
MATRIX SPIKE SAMPLE: 2601098
35473817002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 4.8U 19.2 20.7 107 64-132
Reautts presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 18

acmnalytical
www,pacerabs. com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersvitle, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92432139
QC Batch: 480800
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
'Analysis Description:
200.7 MET
Associated Lab Samples: 92432139004
METHOD BLANK: 2600952
Matrix: Water
-.
Associated Lab Samples: 92432139004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0 06/15/19 23:33
Chromium
ug/L
ND
5.0 06/15/19 23:33
Lead
ug/L
ND .
5.0 06/15/19 23:33
Nickel
ug1L
ND
5.0 06/15/19 23:33
Zinc
ug1L
ND
10.0 06/15/19 23:33
LABORATORY CONTROL SAMPLE: 2600953
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Cadmium
ug/L
500 472
94 85-115
Chromium
ug/L
500 483
97 85-115
Lead
ug/L
500 466
93 85-115
Nickel
ug/L
500 470
94 85-115
Zinc
ug/L
500 468
94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2600954
2600955
MS
MSD
92431476001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cono.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
485
510
97
102
70-130
5
Chromium
ug/L
ND
500
500
495
518
99
104
70-130
5
Lead
ug/L
ND
500
500
476
496
95
99
70-130
4
Nickel
ug/L
ND
500
500
484
505
97
101
70-130
4
Zinc
ug1L
ND
500
500
495
518
98
102
70-130
5
MATRIX SPIKE & MATRIX SPIKE DUPLICATE;
2600956
2600957
MS
MSD
92431578001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
494
490
99
98
70-130
1
Chromium
ug/L
12.4
500
500
523
519
102
101
70-130
1
Lead
uglL
ND
500
500
489
486
98
97
70-130
1
Nickel
ugJL
ND
500
500
498
496
100
99
70-130
0
Zinc
Ug/L
18.1
500
500
513
512
99
99
70-130
0
Results presented on this page are In the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

acmnalytrcal ®
www.pecelabs.00m
1
QUALITY CONTROL DATA
Project: Monroe Stofmwater
Pace Project No.: 92432139
QC Batch: 480806 Analysis Method: SM 254OD-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92432139001
METHOD BLANK: 2600974
Associated Lab Samples: 92432139001
Parameter
Units
Total Suspended Solids
mg1L
LABORATORY CONTROL SAMPLE:
2600975
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersOle, NC 2BO78
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 06/13/1912:29
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 244 97 90-110
SAMPLE DUPLICATE: 2601060
92432194001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 618 666
SAMPLE DUPLICATE: 2601061
92432506001 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 150 150
RPD Qualifiers
7 D6
RPD Qualifiers
0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ava. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92432139
QC Batch: 479899 Analysis Method: - SM 521 OB-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92432139002
METHOD BLANK: 2597197 Matrix: Water
Associated Lab Samples: 92432139002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD, 5 day mg/L ND 2.0 06/12/19 22:14
LABORATORY CONTROL SAMPLE:
2597198
Spike
Parameter
Units
Conc.
BOD, 5 day
mg/L
198
SAMPLE DUPLICATE: 2597205
92432230001
Parameter
Units
Result
BOD, 5 day
mg/L
82.2
LCS LCS % Rec
Result % Rec Limits Qualifiers
126 64 84.6-115 L2
Dup
Result RPD Qualifiers
87.0 6 B1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92432139
QC Batch: 480787 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92432139003
METHOD BLANK: 2600860
Associated Lab Samples: 92432139003
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2600861
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 KinmyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 06/13/1916:37
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2600862
2600863
MS
MSD
92431794002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Chemical Oxygen Demand
mg/L
31.3
100
100
131
133
99
102
90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2600864
2600865
MS
MSD
92432237006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc,
Conc,
Result
Result
% Rec
% Rec
Limits RPD Qual
Chemical Oxygen Demand
mg/L
31.3
100
100
138
135
107
104
90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

aceAnaIX cal
www.pacWabs.corn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Monroe Stormwater
Pace Project No.: 92432139
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit. !
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-131phenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenyiamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B1 Less than 1.0 mglL DO remained for all dilutions set. The reported value is an estimated greater than value and is
calculated for the dilution using the least amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
REPORT OF LABORATORY ANALYSIS
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Date: 06/17/2019 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

aceAnalyfrcal
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I
DUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Monroe Stormwater
Pace Project No.: 92432139
Pace Analytical Services, LLG
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample
ID
QC Batch Method
QC Batch
Analytical Method
Batch
92432139001
Monroe
SW02
92432139ODS
Monroe
SW02
EPA 1664E
480855
92432139004
Monroe
SW02
EPA 200.7 Rev 4.4 1994
480800
EPA 200.7 Rev 4.4 1994
480840
92432139001
Monroe
SW02
SM 2540D-2011
480806
92432139002
Monroe
SW02
SM 521OB-2011
479899
SM 521 OB-2011
479909
92432139003
Monroe
SW02
SM 5220D-2011
480787
SM 522OD-2011
480835
Date: 0611712019 06:23 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

Document Name:
Document Revised: February 7, 2018
s
.:ace Analytical
Sample Condition Upon Rece] t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersviile Raleigh[] Mechanicsville[]
Client Name: WO 92432139.
I.Project$
Tr Z2- I ��'� �, A
Courier: ❑fed x ❑UPS USPS — Client
❑ Commercial ❑Pate ❑Other: 9i43zi39 i 11 YY
�-
Custody Seal Present? IJyes LdNo Seals intact? VYes [JNa
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap. Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer:' Type of Ite: Wet ❑ []None
None ❑Yes []No QN/A
IR Gun 10. gl2Ta4a
Cooler Temp ('C)Correction Factor: Add/Subtract ('C) 0.0
n
Cooler Temp Car rected {d
USDA Regulated Sol] (Q N%A, water sample}
Did samples origi ate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
ayes o
Temp should be above freezing to 6'C
35amples out of temp criteria. Samples an ice, tooling process
has begun
Did samples originate from a foreign source {internatianally,
inctudinrr Hawaii and Puerto Rlcoi? nYes Fps o
Comments/01scre ancy:
Chain of Custody Present?
Ves
No
❑N/A
1.
Samples Arrived within Hold Time?
vas
[]NO
❑NIA
2.
Short Hold Time Analysis <72 hr.)?
L14S
LJNo .
N/A
3.
Rush Turn Around Time Requested?
—[]Yes
nfio
N/A
4,
Sufficient Volume?
Y-
EINo
IINIA
S.
Correct Containers Used?
❑No
❑N/A
6.
-Pace Containers Used?
,.,�Yes'
I%lves
No
N A
Containers intact?
Yes
No
N/A/
7.
Dissolved analysis: Samples Field Filtered?
❑Y -"' []No
[E[N/A
a.
Sample Labels Match COC?
r Yes
[]No
❑N/A
9.
i
-Includes Date/Time/ID/Anal sls Matrix:
ea space in VOA Vlals i>5-6mm)?
Yes
❑N
QN/A
10.
Trip Blank Present?
❑Yes
[3 o
❑N/A
.11.
Trip Blank Custody Seals Present?
Yes
No
/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review.
Project Manager SRF Review: L
Date/Time:
Fletd Data Required? ❑Yes ❑No
Dale:
Date:L�—
Page 16 of 18

Document Name:
Document Revised: February 7, 2018
+
Analytical
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
*"Bottom half of box is to list number of bottle
Project W9232139 .._,
PM: -MW8 Due Dale: 06/18/19
CLIENT: 92-A11vae NC
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Sample ID
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pH upon receipt
Date preservation adjusted
Time preservation
adjusted
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added
tot 9
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carc4na DEHNR Cenificailon Office 0.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 18

i
f PaceAnalytical `
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant Rods must be compteted accurately.
Section A , Section B Section C
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-Impormt Nate: By sigrwxl tm term you are ucceptmra Pace's NET 30 day p,Wmrnl tunny and aTuuoq to kea drirWs of 1.5% pc month W my v±.jrces nol��x7 /� �, - f 1 F-ALL-0-020rev.07. 15-May-2007

ATI Specialty Materials -Monroe Plant
Stormwater Monitoring Report form RATI
Sample Date&Time: 6/7/19 9:15am Stormwater Discharge Outfall #2
Sample Location: SW02 Drainage Area = 272'590sa. Ft. =6.25 acres
Impervious_= 36%
Person('s) Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
James Moser,David Ethridge,Tommy Long
Pace Analytical
40 CFR Part 136
Parameter
Results (mg/1)
Benckmark Values (mg/1)
BOD
18.2
30
COD
114
120
TSS
20.1
100
Cadmium
ND
0.003
0.0287
1
Chromium, total recoverable
Lead, total recoverable
ND
0.03
Nickel total recoverable
0.202
0.335
Zinc total recoverable
0.628
0.126
Oil & Grease
ND
15
H
7.5 (std units)
6-9 std units
Storm Date: 517119 Storm Duration: 87.5 (Hrs.) Inches of Rainfall: 1.35"
Duration of time preceding rain event exceeding 0.1": 576 (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Totai)= Q(Pervious Area)+ Q(Impervious Area)
Q(tot, cfs) = (A x inches rain/12inch es/ft. x 6.25 acres x .64) +.9 x inches rain/12inches/ft. x 6.25 x .36)
Q(Total, cfs)= .1333 X 1.35" (inches of rain) + .1688 X 1.35° (inches of rain) = 0.408 cfs

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000330
FACILITY NAME ATI Speicalty Materials
PERSON COLLECTING SAMPLE(S) Tommy Long, David Ethridge
CERTIFIED LABORATORY(S) ,Pace Analytical TT Lab # 12
~Lab ##
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Union
PHONE O. ��9-4511
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
1
FSample1
DateI!
Collected
t
1 1 1
1 1 /
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ()yes ono
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m I
m
unit
galAno
Form S W U-247, Iasi revised 611212015
Page I of 2

STORM EVENT CHARACTERISTICS:
Date W/19
Total Event Precipitation (inches): 1-85"
Event Duration (hours): 87-5 hrs. (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. l am aware that there are significant penalties for submitting false information,
including the possibility, of fines and imprisonment for knowing violations."
-26�� ell�.I. ;;x
A.
(Signature of Permittee) (Date)
Form SW U-247, last revised 611212015
Page 2 of 2

x
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Tar guidance on filling out thisform. please visit htt salde .nc, oviabout/divisions/ever-mineraldand-
resourceslenercy-m i neral-land-permits/stortnwater-permitshtpdes-industrial-sw#tab-4
Permit No.: NICI S/ 0 / 0 / 0 /3 / 3 /0 / or Certi€icate of Coverage No.: NICIGI—I_I / /_l_I
Facility Name: ATl Specialty Materials - Monroe
County: Union
inspector: James Moser
Date of Inspection: 617/19
Time of Inspection: 9:41 am
Total Event Precipitation (inches): 1.3510
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. SW06
Receiving Stream:
Richardson Creek
Structure (pipe, ditch, etc.): Ditch
Describe the industrial activities that occur within the outfall drainage area: Parking Lot,
Metal Storage, Trash Compactor
Page 1 of 2
S WU-242, Last modified 07r8120 f 7

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(Eight, medium, dark) as descriptors: very light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): Rorie
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 '2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 .3. 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
7.
8.
9.
1 2 3 4 5
Is there any foam in the stormwater discharge? () Yes 0 No. _
Is there an oil sheen in the stormwater discharge? ()Yes Q No.
Is there evidence of erosion or deposition at the outfall? O Yes O No.
14. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07128/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit htti2s://deq.nc.izov/abotit/divisioiis/energy .mineral-tand-
resources/ener -mineral-land- ermits/storm water- ermits/n des-industrial-sw#tab-4
Permit No.: N/C/ S /0 / 0 / 4 /3 / 3 /0 / or Certificate of Coverage No.: NICIGI—I—/—/—/ / 1
Facility Name: ATI Specialty Materials - Monroe
County: Union
Inspector: James Moser
Date of Inspection: 6/7/19
Time of Inspection: 9:49am
Total Event Precipitation (inches): 1.35"
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "treasurable storm event."
A "measurable storm event' is a storm event that results in an actual discharge from the permitted site
outfaii. The previous measurable storm event must have bean at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Desi
1. Outfall Description:
Outfall No. SW04 Structure (pipe, ditch, etc.): Pipe/Ditch
Receiving Stream:
Richardson Creels
Describe the industrial activities that occur within the outfall drainage area
turnings storage, truck loading
ipping staging ,
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2, 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
1 2- 3 4 5
G. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 12' 3 4 5
7. Is there any foam in the stormwater discharge? O Yes No.
8. Is there an oil sheen in the stormwater discharge? Oyes 0 No,
9. Is there evidence of erosion or deposition at the outfall? o Yes. o No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242. fast modified (17/2812017

Environmental
Qualify
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfrllingoul thisform, please Wsil httns://deq.nc.gov/about/divisions/energy-mineral-land-
resources/energy-mineral-land-permits/stormwater-permits/npdes ;industrial-sw#tab-44
Permit No.: NICI S / 0 / 0 / 0 / 3 / 3 /0 I or Certificate of Coverage No.: NICIGI_I_I_I_I 1_I
Facility Name: ATI Specialty Materials - Monroe
County: Union Phone No. 704-289-4511
Inspector: James Moser
Date of Inspection: 6/7/19
Time of Inspection: 9:13am
Total Event Precipitation (inches): 1.35"
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Desi
1. Outfall Description:
Outfall No. SW03 _ Structure (pipe, ditch, etc.): Pipe/Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area: Metal Storage,
Hammer Repair Dust Collection
Page 1 of 2
SWU-242, Lass modified 07/2812017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 .2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
'1" 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where 1 is no solids and 5 is extremely muddy:
1 •2 3 4 5
7. 1s there any foam in the stormwater discharge? Q Yes Q No.
8. 1s there an oil sheen in the stormwater discharge? QYes (E) No.
9. Is there evidence of erosion or deposition at the outfall? O Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 0712812017

Environmental
Quality
Stormwater Discharge Outfall (SD4)
Qualitative Monitoring Report
For guidance on filling out this form, please visil https://deg,nc.gov/about/divisions/energy-mineral-land-
resources/energy-mineral-land-permits/storrnwater-pernuts,/npdes; industrial-sw#tab-4
Permit No.: N/C/S / 0 / 0 / 0 /3 / 3 /0 / or Certificate of Coverage No.: N/C/GI�hI
Facility Name: ATI Specialty Materials - Monroe
County: Union
Inspector: James Moser
Date of Inspection: 6/7/19
Time of Inspection: 9.20am
Total Event Precipitation (inches): 1.35"
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. SW05_ Structure (pipe, ditch, etc.): Ditch
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area: Metal Storage,
Equipment Storage,clean empty drums, roll off containers
Page 1 of 2
SWU-242. Last modified 0728/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
,1', 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge_ where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Q Yes Q No.
8. 1s there an oil sheen in the stormwater discharge? QYes (E) No.
9. Is there evidence of erosion or deposition at the outfall? O Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/2812017

Environmental
Qualify
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out thisform, please visit htt salde .nc. ov/about/divisions/ener -mineral-land-
resources/energy-m ineral-1and -perm its/stornzwater-permits/npdes-ind ustrial--sw#tab-4
Permit No.: N/C/S/O /0 / 0/3 /3 /0 / or Certificate of Coverage No.: NICIGI hI I _1 __l�l
Facility Name: AT[ Specialty Materials - Monroe
County: Union
Inspector: James Moser
Date of inspection: 6/7/19
Time of Inspection: 9:05am
Total Event Precipitation (inches): 1,35"
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMi_,R
Rev-ional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee
1. Outfall Description:
Outfall No. SW02
Receiving Stream:
Richardson Creek
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the Outfall drainage area: Metal Storage
Page 1 of2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Eight brown
I Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where I is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Q Yes No.
8. Is there an oil sheen in the stormwater discharge? QYes 0 No.
9. Is there evidence of erosion or deposition at the outfall? O Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5WU-242, Last modified 07/2812017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out this form, please visit https://dec nc.gov/about/divisions/energy,-mineral-land-
resources/ever -mineral-land- ermits/stormwater-perm its/n des-industrial-s%v#tab-4
Permit No.: NICI S / 0 / 0 / 013 / 3 /0 / or Certificate of Coverage No.: NICIGI—I—I, /—/—l—1
Facility Name:
County: Union
inspector: James Moser
Date of Inspection: 6/7/19
Time of Inspection: 9:29am
Total Event Precipitation (inches): 1.35"
Phone No. 704-289-4511
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Des
1. outfall Description:
Outfail No. SW01 Structure (pipe, ditch, etc.): Pipe
Receiving Stream:
Richardson Creek
Describe the industrial activities that occur within the outfall drainage area: Metal Storage,
Equipment Storage,clean empty drums, roll off containers
Page l of 2
SWU-242, last modified 07/28t2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light gray
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): none
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
J. 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge. where 1 is no solids and 5 is extremely muddy:
1 21
3 4 5
7. is there any foam in the stormwater discharge? () Yes O No. _
8. Is there an oil sheen in the stonnwater discharge? ()Yes No.
9. Is there evidence of erosion or deposition at the outfall? O Yes U No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
Indicative of pollutant exposure. These conditions warrant further investigation.
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SWt1-242, Ust modified 97/28/2017