NCS000329_MONITORING INFO_20190813

mWI
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
f�l � S 3)
DOC TYPE
❑FINAL PERMIT
C� MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ ��l � � ��
YYYYMMDD

August 8, 2019
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
�ATI
P.O. Box 5030
2020 Ashcmff Avenue
Monroe, NC 281 1 1-5030
Phamc: (704) 289-451 1
Fax: ( 704) 290-5 t 94
Email: Iylermiercer@;uimetal s.cortt
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
End
Year 10 — Period l
19
March 1, 2019
August 31, 2019
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non -Contact Cooling Water #1 - #8
FC�j\/ED
R
WG 19 M9
CENT AL F ILES
DWR SECTION
If you have any questions or need additional information, please contact me at 704-289-451 1.
Thank you.
sincerely,
* 7nM&��
Tyler Mercer
Manager, EMS

Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Non-ContactCooling Wastewater
pavIrz o r • / .�
-IDa ce i�i�sc�yf ea%
40 CFR Part 136
- T
sfty MatarlaLs
Non-
Contact
Cooling
Water # _
Sampling
©ate
ITotal
Sampling
Time
Estimated
Flow(MGD)
Residual
Chlorine
(mg/L)
Temperature
pH {std. units}
Effluent
Downstream
Upstream
-/3-
soa.
D.00v3-
7
3
lv -/S-
8:-Yo.
. oDa9
03.0°�
ZVD
aR.6°`
3•/°`
6
D. 60 ja
o23. 9°`
3.3°4-
8
/3 -l91
zo = 33.a.
D • o�od
D
a?a 9 °G
o?-�

aceAnalytical
www.pecelabs.com
f
June 26, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on June 14, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, 7� n
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

5a'cieAna1Vtica1"`
www,pa"bi.com
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
{704)875.9092
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: EB7627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #; 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 19

aceAnalytical
` � www.pacela6s.00m
r
SAMPLE ANALYTE COUNT
Project: NONGONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
{704}875-9092
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92433143001
NON-CONTACT#1
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143002
NON-CONTACT#2
EPA 1664E
ims
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143003
NON-CONTACT#3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143004
NON-CONTACT#4
EPA 16646
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143005
NON-CONTACT#5
EPA 16648
JMS
1
PASI-C
SM 4500-Cl G-2011
GC
1
PASI-A
92433143006
NON-CONTACT#6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143007
NON-CONTACT#7
EPA 16646
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143008
NON-CONTACT#8
EPA 16648
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of Pace Analytical Services, LLC.
Page 3 of 19

aceAnalytical
www.pacelabs.com
i
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#1 Lab ID: 92433143001 Collected: 06113/19 07:50 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: D612612019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

e
aceAnalytical
wr`wpacelabs.com
i
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#2 Lab ID: 92433143002 Collected: 06/13/19 08:15 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0,024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

_ ;a'cie Analytical
rww ,pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. SOe 100
Huntersville. NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#3 Lab ID: 92433143003 Collected: 06/13/19 08:40 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02A0 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnalytiW Services, LLC.
Page 6 of 19

aceAnalytical
—Pacelabs.cam
r
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#4 Lab ID: 92433143004 Collected: 06/13/19 09:00 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mglL 5.0 1 06/26/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0.024 1 06118/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

aceAna1j4Jca1
wxw.pscelebs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLG
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#5 Lab ID: 92433143005 Collected: 06/13/19 09:25 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 06/26/2019 02:40 PM
Analytical Method: EPA 1664B
ND mg/L 5.0 1 06/26119 06:44
Analytical Method: SM 4500-CI G-2011
ND mg/L 0 024 1 06/18/19 17:57 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page B of 19

aceAnalylical
WW pacelahs.C=
i
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#6 Lab ID: 92433143006 Collected: (16/13119 09:45 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 06/26/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0,24 10 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

aceAnalytical
www pecelabs, cam
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hun:ersville, NC 28078
[phone]
Sample: NON-CONTACT#7 Lab ID: 92433143007 Collected: 06/13/19 10:10 Received: 06/14119 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mglL 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

r
m
acmnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#8 Lab ID: 92433143008 Collected: 06/13/19 10:35 Received: 06114/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mgi 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7762-50-5 H3
Date: 06/26/2019 02A0 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

aceAnalytical6
www.pacelabs.00rn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
QC Batch: 483277 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007.
92433143008
METHOD BLANK: 2612203 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 4.8 06/26119 06:42
LABORATORY CONTROL SAMPLE:
2612204
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5 38.5
100
78-114
MATRIX SPIKE SAMPLE:
2612205
92433576001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
37.2
97
78-114
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuli,
Date: 06126/2019 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

1�55'ne Analytical
www.pect4abs.com
i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
QC Batch: 481875 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples. 92433143001,92433143002,92433143003,92433143004,92433143005,92433143006,92433143007,
92433143008
METHOD BLANK: 2605891 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 06/18/19 17:57
SAMPLE DUPLICATE: 2605892
Parameter Units
Chlorine, Total Residual mg/L
92432727001 Dup
Result Result
ND ND
RPD Qualifiers
H3
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0612612019 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

/5aC6Analj6cal
1WWW.pMJ8lJ8.o=
1
0
I
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
Ti - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services. LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 6270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TIN - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASk-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 06126/2019 02:40 PM without the written consent of Pace Analyticai Services, LLC- Page 14 of 19

aceAnalytical
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F
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92433143001
NON-CONTACT#1
EPA 1664B
463277
92433143002
NON-CONTACT#2
EPA 1664B
483277
92433143003
NON-CONTACT#3
EPA 1664B
483277
92433143004
NON-CONTACT#4
EPA 1664B
483277
92433143005
NON-CONTACT#5
EPA 1664B
483277
92433143006
NON-CONTACT#6
EPA 1664B
483277
92433143007
NON-CONTACT#7
EPA 1664B
483277
92433143008
NON-CONTACT#8
EPA 1664E
483277
92433143001
NON-CONTACT#1
SM 4500-CI G-2411
481875
92433143002
NON-CONTACT#2
SM 4500-CI G-2011
481875
92433143003
NON-CONTACT#3
SM 4500-CI G-2011
481875
92433143004
NON-CONTACT#4
SM 4500-CI G-2011
481875
92433143005
NON-CONTACT#5
SM 4500-CI G-2011
481875
92433143006
NON-CONTACT#6
SM 45DD-CI G-2011
481875
92433143007
NON-CONTACT#7
SM 4500-CI G-2011
481875
92433143008
NON-CONTACT0
SM 4500-CI G-2011
481875
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalyticaf Services, LLC.
Page 15 of 19

Document Name:
Document Revised: February 7, 2018
aceAnafytical
Sample Condition Upon Recei t(SCUR
Page 1 of 2
Document No.:
Issufng Authority:
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑
Client Name: 97433143
• j � � Project #.—Wo' • ' �
Courier: —❑Fed Ex []UPS ❑Usps [:]Client
❑ Commercial QPace ❑Other: � �}ii 1111I111 UUU
92433143 - t
-_-Custody Sea] Present? _ _._❑Yes.- - []No Seals intact? ❑Yes ❑No
Date/initials Person Examining Contents.
Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
i
❑Yes []No ❑NIA
Thermometer:' 92TO48 Type of ice: I]� [:]Blue❑None
QIR Gun ID:
/? ',
Cooler Temp ('Cj: C.- �(*C��:�
ection Factor: Add/Subtract ('C) 0.0
�Temp should be above freezing to 6'C
Cooler Temp Correctedr ❑Samples out of letup criteria, samples on ice, cooing process
has begun
USDA Regulated Sail (© N/A, water sample)
Oid samples originate in a quarantine zone within the United 51ates: CA, NY, or SC (check mapsl? Did samples originate from a foreign .source (internationally,
nYes Mo including Hawaii ant! Puerto Rlcol7 CIYes 11N0
Comments/Discre ancy:
/
Chain of Custody Present?
des
❑No
N/A
1.
Samples Arrived within Hold Time?
. Yes
[]NO
❑N/A
2,
Short Hold Time Analysts L<72 hr.)?
GJVes
011.
N/A
3,
Rush Turn Around Time Requested?
Yes
4.
Sufficient Volume?
r Yes
No
N/A
S.
Correct Containers lased?
C3Ycs
❑No
[]N/A
6.
-Pace Containers Used?
01--
No
[]N/A
Containers intact?
❑kes
QNo
N/A
7.
Dissolved analysis: Samples Field Filtered?
©Yes,.
[]NO
N/A
fl.
Sample Labels Match COC?
0 es
❑No
❑N/A
9.
-Includes Date/lime/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Yes
❑No_
ON/A
10.
Trip Blank Present?
❑Yes
QNo
[)N/A
21.
Trip Blank Custody Seals Present?
Yes
NO
COiyEMENTS/SAMPLE DISCREPANCY
Field Data Required? []Yes [:]NO
Split Containers:
., . ,_._.. _... _. Lot € of sp„
CLIENT NOTIFICATIONIRESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review: L
Dale/Time:
Date: _ L' Will, X11
�
Date:
Page 16 of 19

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BP31J-250 mL Plastic Unpreserved (NIA)
SP2U-500 mL Plastic Unpreserved (N/A)
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8P1U-1 liter Plastic Unpreserved (N/A)
BP4S-125 mL Plastic H2SO4 {pH e 2) (Cl-)
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BP3N-250 mL plastic HNO3 (pH < 2)
8P4Z-12S mL Plastic ZN Acetate & NaOH (
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BM-125 mL Plastic NaOH (pH > 12) (Cl.)
vuGFU-wide-mouthed Glass jar Unpreserved
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AG1U-1 liter Amber Unpreserved INIA) ja)
I
AG1N-1 liter Amber Hb (pH < 2)
\
AG31J-250 mL Amber Unpreserved (N/A)
I
(C1-)
AG1S-1 liter Amber H2SO4 (pH < 2)
AMS-250 mt Amber H2SO4 (pH < 2)
AG3AjDG3A)-250 mL Amber NH4C1 [N/A)(el-)
OG9N-40 mL VOA HCl (N/A)
VGST-40 mL VOA Na2S203 IN/A)
VG9U-40 mL VOA Unp (N/A)
DG911-00 mL VOA H3PO4 IN/A]
l
VOAK (6 viats per W*5035 kit (N/A)
I
V/GK (3 vials per ki*VPH/Gas kit (N/A)
SPST-125 ml Sterile Plastic (NIA — lab)
SPZT-2SO mL Sterne Plastic (NIA —lab)
BP3A-250 mt. Plastic (NH2)2SO4
AGOU-100 mL Amber Unpreserved vials (l1/A)
J
VSGU-20 mL Scintillation vials (N/A)
DGSU-40 rnL Amber Unpreserved vials (NJA)
i
„ rA t A
a
0 rn
G � y
o 3 d
X S
y O ro O
w tv
G O n Cr
m x
CL
G1 7 V
Cr
ro m 7
CL
o P oa
Cr
O O p
15 a
a_ M O
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iw
O a
z � w
a
to
C.
A
ro
r1
A

170TATI
Specialty ftatr,,iah
Storrs dilater Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
napr
Project Number/Name: NonContact Cooling Water
Project Location: ATI SM
- Bakers
Sampler's Signature:
Date: 6
64
.'
u
E
a
CL
a
L
z
U
CA
co
40
�,
Requested Test
;'
o
iwE-.
E
Parameters
G`
y
++
CL
U
a
C
o
a331
o
G
G/d)
None
Y
Residual Chlorine
Say
G
G/41
None
Y
j
Residual Chlorine
n acf 3
Q,�
G
G/0
None
Y
Residual Chlorine
Co
00._
G
G/(9
None
Y
Residual Chlorine
on -Con acf,4i
= f.�
G
G/dY
None
Y
r5
Residual Chlorine
Alon-C6
G
G
None
Y
g
Residual Chlorine
No.1-C
/0,..
G
G/®
None
Y
%ta
�.S
Residual Chlorine
An-CeeAe,4$
j
0 35,
G
I G*M
I None
Y
y
Residual Chlorine
Meter Calibrated: f N IThermometer Callbra N
Sampling and Field analysis completed by:
Relinquished By:
Received By:
Date :-6 ITime: /S`�._
Date: OA - PI -h?
Relinquished By: 17:L—LLtag,
Received By:
Date
ITime: f ;,,,,_
Dater • �`f'F I Tlme: II Ica
EHS Baker South SW REV 4 2 S/10/2016
Page 18 of 19

')FF
specially Malerials
Storm dater Mont®rlr��
(NON CONTACT)
Bakers North
Chain of Custody Record
naee ff2
Project Number/Name: NonContact Cooling Water
Project Location: AT] SM - Bakers
Sampler's Signature:
Date:
Y,
ECa
v,
�
�
01
a
w
�
0LACL
U
Gl
a
�
�.
0
or-E
0
CL
w
o
Requested Test
Parameters
-Cp
/3-9
G
G
HCL
Y
/
Oil & Grease
- 04,J, dAq
G
G
HCL
Y
J ,
Oil & Grease
Dq-C'DR
(,
G
G
HCL
Y
Oil & Grease
0 IV
q •'G1pr.
G
G
HCL
Y
Oil & Grease
,,,_
G
G I
HCL
Y
Oil & Grease
6
G
G
HCL
Y
dj. q
Oil & Grease
Gy! C�' ctcl�
' I2,
G
G
HCL
Y
%. �
Oil & Grease
Dn Comma B
/0 S•—
G
G
HCL
I Y
Oil & Grease
Meter Calibrated: / N
IThermometer Calibrated: / N
Sampling and Field analysis completed by:
Relinquished By:
Relinquished By:
Date: - y-
Time:
Date :(J °f y f'i
Time:
Relinquished By:
4 -i
Relinquished By:
Date: & .j
ITime: fll.'.� ,
Date : (*�.,)'j - '-,
Time: I l :1 r47
EH5 Baker 5outh 5W REV N 2 5/10/2016
*[
:1.7'L
rcr�
Ct rL.
VIX
uou
cJ?
Page 19 of 19

aceftpicalm
wwwPecefabs.com
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall#01(B)
Pace Project No.: 92438396
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNVNELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, AT] Specialty Materials
David Pope, Allvac
ppCC:7F0
TN1,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC-
Page 1 of 15

I aceAnalXical
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Protect: SW Outfall#01(B)
Pace Project No.: 92438396
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiafVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
r
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 15

C
w ;- aceAnaIXical
www pecWahs.wn
Project: SW Oulfall#01(8)
Pace Project No.: 92438396
Lab ID Sample ID
92438396001 SW OUTFALL #01 (B)
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
$Ii1
5
PAS -A
SM 2540D-2011
MJP
1
PASI-A
SM 4500-CI G-2011
GC
1
PASI-A
SM 521OB-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ace Analytical 0
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ANALYTICAL RESULTS
Project SW Outfall#01(B)
Pace Project No.: 92438396
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW OUTFALL #01 (B)
Parameters
Lab ID: 92438396001 Collected: 07/23/19 16:12
Results Units Report Limit DF
Received: 07/24/19 11:45 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 16:27
Collected Date
07123/19
1
07/23/19 16:27
Collected Time
16:15
1
07/23/19 16:27
pH
6.9 Std. Units
0.10
1
07/23/19 16:27
Temperature
20.1 deg C.
0.50
1
07/23/19 16:27
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mglL
5.0
1
07/31/19 05:43
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND ug/L
1.0
1
07/31/19 13:56
08/01/19 21:55
7440-43-9
Chromium
ND ug1L
5.0
1
07/31/19 13:56
08/01/19 21:55
7440-47-3
Copper
30.2 ug/L
5.0
1
07/31/19 13:56
08/01/19 21:55
7440-50-8
Nickel
5.0 ug1L
5.0
1
07/31/19 13:56
08/01/19 21:55
7440-02-0
Zinc
10.5 ug/t_
10.0
1
07/31/19 13:56
08/01/19 21:55
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
7.2 mg1L
4.2
1
07/29/19 13:06
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual
0.16 mg1L
0.024
1
07/29/19 18:48
7782-50-5 H3
5210E BOD, 5 day
Analytical Method: SM 521OB-2011
BOD, 5 day
10.4 mg1L
2.0
1
07/25/19 03:10
07/30/19 04'.33
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Chemical Oxygen Demand
67.0 mg1L
25.0
1
07/26/19 15:30
07/29/19 17:10
Date: 08/02/2019 11:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 15

aceAnalyticalm
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r
I
QUALITY CONTROL DATA
Project: SW Outfall#01(B)
Pace Project No.: 92438396
QC Batch: 489444 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92438396001
METHOD BLANK: 2641152
Associated Lab Samples: 92438396001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 2641153
Parameter Units
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 4.8 07131/19 05:42
Spike LCS
Conc, Result
38.5 37.0
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersvte, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
96 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15

m
1�;MeAnapili
..pacQb8.com
1
QUALITY CONTROL DATA
Project: SW Outfali(B)
Pace Project No.: 92438396
QC Batch: 489431 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 201 MET
Associated Lab Samples: 92438396001
METHOD BLANK: 2641114
Associated Lab Samples: 92438396001
Parameter
Units
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Nickel
uglL
Zinc
uglL
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed
ND
1.0
08/01/19 21:11
ND
5.0
08/01/19 21:11
ND
5.0
08/01/19 21:11
ND
5.0
08/01/19 21:11
ND
10.0
08/01/19 21:11
Qualifiers
Pace Analytical Services, Li
9800 Kincey Ave. Suite 100
Huntersville, 128078
[phone]
LABORATORY CONTROL SAMPLE:
2641115
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
489
98
85-115
Chromium
ug1L
500
494
99
85-115
Capper
ug1L
500
494
99
85-115
Nickel
ug1L
500
492
98
85-115
Zinc
uglL
500
497
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
MS
92437770001
Spike
Parameter
Units
Result
Conc.
Cadmium
uglL
ND
500
Chromium
uglL
ND
500
Copper
ug1L
22.4
500
Nickel
uglL
ND
500
Zinc
ug1L
133
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Conc.
Cadmium
uglL
ND
500
Chromium
uglL
ND
500
Capper
uglL
53.0
500
Nickel
ug1L
5A
500
Zinc
uglL
45.9
500
2641117
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc,
Result
Result •
% Rec
% Rec
Limits
RPD
500
503
499
101
100
70-130
1
500
503
497
100
99
70.130
1
500
517
516
99
99
70-130
0
500
600
493
99
98
70-130
1
500
640
632
101
100
70-130
1
2641119
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
500 502 504 100 101 70-130 1
500 502 512 100 102 70-130 2
500 547 555 99 100 70.130 1
500 496 502 98 99 70-130 1
500 544 551 100 101 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/0212019 11:30 AM without the written consent of Pace Analytical Services, i
Qual
Qual
Page 6 of 15

ace Analytrcalm
..Pacsfabs.com
QUALITY CONTROL DATA
Project: SW Outfall#01(B)
Pace Project No.: 92438396
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
HuntersO[e, NC 28075
[phone]
QC Batch: 488845
Analysis Method:
SM 2540D-2011
QC Batch Method: SM 2540D-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92438396001
METHOD BLANK: 2638666
Matrix:
Water
Associated Lab Samples: 92438396001
Biank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 07/29/19 13:04
LABORATORY CONTROL SAMPL3=- 2638667
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250
250
100 90-110
SAMPLE DUPLICATE: 2639441
92438421003
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg1L
58.7
57.3 2
SAMPLE DUPLICATE: 2639442
92438506002
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg1L
440
444 1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/0212019 11:30 AM without the written consent of Pace Analytical Services, L.C. Page 7 of 15

aceAnalytical
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1
1
QUALITY CONTROL DATA
Project: SWOutfall#01(B)
Pace Project No.: 92438396
QC Batch: 489113 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples. 92438396001
METHOD BLANK: 2639819
Associated Lab Samples: 92438396001
Parameter Units
Chlorine, Total Residual mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 07129/1918:44
SAMPLE DUPLICATE: 2639820
92438396001 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L 0.16 0.16
RPD Qualifiers
4 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9D92
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

1�5a'ceAnalytical-
www'pacdobs,com
i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SWOutfall#01(B)
Pace Project No.: 92438396
QC Batch: 488319
Analysis Method:
SM 52108-2011
QC Batch Method: SM 521OB-2011
Analysis Description:
5210E BOD, 5 day
Associated Lab Samples: 92438396001
METHOD BLANK: 2636157
Matrix: Water
Associated Lab Samples: 92438396001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 07/30/19 03:34
LABORATORY CONTROL SAMPLE: 2636158
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg1L
198 203
103 84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
ND
ND
Resuhs presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 15

aceAnalytrcal
wwwpacalabs.corn
l
QUALITY CONTROL DATA
Project: SW Outfall#01(B)
Pace Project No.: 92438396
QC Batch: 488767 Analysis Method: SM 5220D-2011
QC Batch Method: SM 52200-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92438396001
METHOD BLANK: 2638169
Associated Lab Samples: 92438396001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2638170
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville$NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 07/29/1917:06
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 3010 100 100 3090 3100 85 95 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 119 121 99 102 90-110 2
Results presented on this page are in the units indicaled by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

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aceAnalytical
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i
QUALIFIERS
Project: SW Outfall#01(B)
Pace Project No.: 92438396
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at of above adjusted reporting limit.
Ti - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, 128078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyse is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration,
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08102/2019 11:30 AM without the written consent of Pace Analytical Services, Li Page 11 of 15

1�l
;aceftljtcal'
/ wtim.pacelabsxom
i
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Outfall#o1(B)
Pace Project No.: 92438396
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92438396001
SW OUTFALL #01 (B)
92438396001
SW 0UTFALL #01 (B)
EPA 1664B
489444
92438396001
SW OUTFALL #01 (B)
EPA 200.7 Rev 4.4 1994
489431
EPA 200.7 Rev 4.4 1994
489630
92438396001
SW OUTFALL #01 (B)
SM 2540D-2011
488845
92438396001
SW OUTFALL #01 (B)
SM 4500-CI G-2011
489113
92438396001
SW OUTFALL #01 (B)
SM 521OB-2011
488319
SM 521OB-2011
488349
92438396001
SW OUTFALL #01 (B)
SM 52200-2011
488767
SM 5220D-2011
489096
Date: 08/02/2019 11:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 15

Oocument Name:
Document Revised: February 7, 2018
aceArral ICdI e
Sample Condition Upon Recel t SCUp
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersviile Raleigh[] Mechanicsville❑
Client Name: Wo : 92438396
almlassm—Project tt;
Courier: (-]Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial Elpace ❑Other: / 92438396
Custody Seel Present? Dyes ©No Seals Intact? Dyes QIVo _
Date/InitiarsPerson ExaminingContentsi 7r4, of=+
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: 42I048 Type oFlce: ❑wet ❑Brae ❑None ❑Yes ❑No [tit/A
01R Gun tO;
Cooler Temp ('C): e cj,
- Correction Factor: Add/SubtraCt ('Cj 0.0
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (IT. MIA, water sample)
Did samples originate in a quarantine lane within the United States: CA, NY, or 5C {check maps)? Did samples originate from a foreign source {internationally,
MV— MN. inrtudin¢Hawaii and Puerto Rlcol?F-lYes 11No
Comments/niscre pancy:
Chain of Custody Present?
OYCS
ONO
❑N/A
1.
Samples Arrived within Hold Time?
E]Y/es
❑No
❑N/A
2.
Short Hold Time Anal sls <72 hr.)?
. Yes
Na
Nv A
3.
Rush Turn Around Time Requested?
OY.[DN.
N/A
4.
Sufficient Volume?
+ !es
UND
QN A
S.
Correct Containers Used?
-Pace Containers Used?
0:3�eS
dyes
[]NO
No
❑N/A
[]NIA
6.
Containers Intact?
ayes
Na
N/A
7.
Dissolved analysis: Samples Field filtered?
❑Yes
❑No
❑N/A
a.
Sample Labels Match COC?
-Includes Hate/Time/ID/Anal si9 Matrix:
©res
❑No
❑N/A
9,
Headspace in VOA Vials (>5.6mm)?
Elyes
[]No
N/A
10,
Trip Blank Present?
Trip Blank Custody Seats Present?
(]Yes
Yes
[]No
No
c N/A
Q N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: !•j� Date:
L� . —
Project Manager SRF Review: s {'�' - Date:
Page 13 of 15

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document Na.!
Issuing Authority:
1 aceArralyircal'
1
F-CAR-CS•033•Rev.06
Pace Carolinas quality Office
'Check mark top half of box if pH and/or dechlorination Is Project
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oii and Grease, DRO/8015 (water) DOC, LLHS
"Bottom half of box is to list number of bottle
WO#:92433396
PM: MW8 Owe Date: 08/02/19
CLIENT: 92-Allvac NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot d
Note: Whenever there is a discrepancy aftecVng North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEIINR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 14 of 15

Stormwater Monitorin
Chailtl of Custody Record
Project Number/Name: SW Outfall #01(13)
Project Location: ATI SNi - Bakers
Sample 's Signature:
Date: - �- 9
m
a�
c,
a
o
11
V
�
F-
G �'
a
PC
�,
>
Requested Test Parameters
1;
�
C7
O
WP
7 3-
.• •5'
G
G /©
HNO3
Y
Total Recoverahle: Chromium, Nickel, Copper. Zinc
J
G
G /0
1-1NO3
Y
_�
Cadmul.tttt
Q
G
/ 1'
I-1CL
Y
Oil SC Grease
Q
G
G /®
H2SO4
Y
COD
G
G IC
None
Y
BOD
G
G /d)
None
Y
TSS
G
G /©
None
Y
Residual Chlorine
Onsite Meld
111 Analysis
Onsite Field 'rent erature Analnis
111-1: G. 9 (S-u.) Sample `i'ilm. /s
Temp: J _(°C) SaIIII)Ic Tillie: _Y23�
Analysis Time-. �.' 7�
Analysis Tints: -
1vleter Calibrated: Ye,5
Therms}meter Calibrated: 0/ N
Sam lin , and field analysis completed by:
Relinquished By:
Received BiRAI&
Date:
Timtc: 6 ' f1.�
Date:Ting. ' 5
Relinquished By:
='
Received By:
Date: ' ,1 Time: 5i'
Date: 1 ,i `�j I'imc:
EHS-SW-Chain of Costody Outfall 01-Rev 001
Page 15 of 15

;aneAnalytical"
www.pacembs.com
i
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall #02 (B)
Pace Project No.: 92438403
Pace Analytical Services, LLC
4800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
ACCREO
iNI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of Pace Analytical Services, LLC.
Page 1 of 13

m
1�5acieAnalyfical
www.pacalaAs.cam
{
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NO 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersviile, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #! 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #; 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #; E87648
Massachusetts Certification #7 M-NC030
North Carolina Drinking Water Certification #; 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida{NELAP Certification #. E87627
Kentucky UST Certification #; 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

m
_ aceAnalytical
r_, mrw.pacelehs.com
r
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
Lab ID Sample ID
92438403001 SW OUTFALL #02 (8)
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
SM 254OD-2011
MJP
1
PASI-A
SM 521OB-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except ira full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytical
—Pacela8s.cam
r
I
ANALYTICAL RESULTS
Project: SW Outfal1 #02 (8)
Pace Project No.: 92438403
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: SW OUTFALL #02 (B)
Parameters
Lab ID: 92438403001 Collected: 07/23119 15:50
Results Units Report Limit DF
Received: 07/24/19 11:45 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 15:58
Collected Date
07/23/19
1
07/23/19 15:58
Collected Time
15:51
1
07/23/19 15:58
pH
7.1 Std. Units
0.10
1
07/23/19 15:58
Temperature
23.5 deg C
0.50
1
07/23/19 15:58
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND ug1L
1.0
1
07/31119 13:56 08/01/19 22:01
7440-43-9
Chromium
ND ug1L
5.0
1
07/31/19 13:56 08/01/19 22:01
7440-47-3
Copper
53.0 ug1L
5.0
1
07/31/19 13:56 08/01/19 22:01
7440-50-8
Nickel
5.4 ug1L
5.0
1
07/31/1913:56 08101/1922:01
7440-02-0
Zinc
45.9 ug1L
10.0
1
07/31/1913:56 08101/1922:01
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
26.7 mg1L
2.5
1
07/29/19 13:06
5210B BOD, 5 day
Analytical Method: SM 521 OB-2011
BOD, 5 day
4.6 mg/L
2.0
1
07/25/19 03:10 07/30/19 04:30
B2
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Chemical Oxygen Demand
45.8 mg/L
25.0
1
07/26/19 15:30 07/29/19 17:11
Date: 08/02/2019 11:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

ace Analytical
wwwpacelab&cam
QUALITY CONTROL DATA
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 489431 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92438403001
METHOD BLANK: 2641114
Matrix: Water
Associated Lab Samples: 92438403001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0
08101/19 21:11
Chromium
ug1L
ND
5.0
08/01119 21:11
Copper
uglL
ND
5.0
08101/19 21:11
Nickel
ug1L
ND
5.0
08/01119 21:11
Zinc
ug1L
ND
10.0
08/01119 21:11
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2641115
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
489
98
85-115
Chromium
uglL
500
494
99
85-115
Copper
uglL
500
494
99
85-115
Nickel
uglL
500
492
98
85-115
Zinc
uglL
500
497
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
MS
92437770001
Spike
Parameter
Units
Result
Cone.
Cadmium
uglL
ND
500
Chromium
uglL
ND
500
Copper
uglL
22.4
500
Nickel
uglL
ND
500
Zinc
uglL
133
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Cone.
Cadmium
ug1L
ND
500
Chromium
ug1L
ND
500
Copper
ug1L
53.0
500
Nickel
ug1L
5.4
500
Zinc
ug1L
45.9
500
2641117
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
500
503
499
101
100
70-130
1
500
503
497
100
99
70-130
1
500
517
516
99
99
70-130
0
500
500
493
99
98
70-130
1
500
640
632
101
100
70-130
1
2641119
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
500
502
504
100
101
70-130
1
500
502
512
100
102
70-130
2
500
547
555
99
100
70-130
1
500
496
502
98
99
70-130
1
500
544
551
100
101
70-130
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/0212019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

ace Analytical
www.p&ceiabs.com
QUALITY CONTROL DATA
Project: SW Outfal1 #02 (B)
Pace Project No.: 92438403
QC Batch: 488845 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples. 92438403001
METHOD BLANK: 2638666 Matrix: Water
Associated Lab Samples: 92438403001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 07/29/19 13:04
Pace Analytical Services, i
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2638667
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 250 100 90-110
SAMPLE DUPLICATE: 2639441
92438421003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
58.7
57.3 2
SAMPLE DUPLICATE: 2639442
92438506002
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mi
440
444 1
Results presented on this page are In the units Indicated try the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, Li Page 6 of 13

Pace Analytical Services, LLC
;aceAnalXical0
9800 Kincey Ave. Suite 100
11�Hunlersville,
NC 28078
w^°w+.pecelabs,cam
(704 )875-9092
QUALITY CONTROL DATA
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 488319
Analysis Method: SM 521 OB-2011
QC Batch Method: SM 521OB-2011
Analysis Description: 521013 BOD, 5 day
Associated Lab Samples: 92438403001
METHOD BLANK: 2636157
Matrix: Water
Associated Lab Samples: 92438403001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
BOD, 5 day
mg/L
ND 2.0 07/30/19 03:34
LABORATORY CONTROL SAMPLE: 2636158
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
HOD, 5 day
mg1L
198 203 103 84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter
Units
Result Result RPD Qualifiers
BOD, 5 day
mg1L
ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an altemale unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

m
aceAnalytical
—pacerabs.com
l
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 488767
QC Batch Method: SM 5220D-2011
Associated Lab Samples: 92438403001
METHOD BLANK: 2638169
Associated Lab Samples: 92438403001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2638170
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5220D-2011
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 07129/1917:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 2638171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 3010 100 100 3090 3100 85 95 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 119 121 99 102 90-110 2
a
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8of13

Pace Analytical Services, LLC
aceAnalytical a 9800 Kincey Ave. to 100
Huntersville, NC
29078
www.pacewbs.com
[phone]
QUALIFIERS
Project: SW Outtall #02 (8)
Pace Project No.: 92438403
DEFINITIONS
DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 C hl oroethyl vinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
62 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAnalytical
~pacelabs.mn
r
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Outfall #02 (8)
Pace Project No.: 92438403
Lab 1D Sampie ID
92438403001 SW OUTFALL #02 (B)
92438403001 SW OUTFALL #02 (B)
92438403001 SW OUTFALL #02 (B)
92438403001 SW OUTFALL #02 (B)
92438403001 SW OUTFALL #02 (B)
Date: 0810212019 11:30 AM
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA 200.7 Rev 4.4 1994 489431 EPA 200.7 Rev 4.4 1994 489630
SM 2540D-2011 488845
SM 521OB-2011 488319 SM 521OB-2011 488349
SM 5220D-2011 488767 SM 5220D-2011 489096
REPORT OF LABORATORY ANALYSIS
Thls report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC-
Page 10 of 13

Document Name:
Document Revised: February 7, 2018
�170-AndllCr7la
--Document
Sam le Condition U on Recei t(SCUR
Pa c 3 of 2
No.;
Issuing Authority:
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑� Raleigh❑ Mechanicsville[]
• Client Name: WO# : 92438403
Project W
-,� tr Il�il� II IIIIII I III III
Courier: ❑Fcd EH [—]UPS ❑USPS []Client
❑ Commercial QPace ❑Other: 92436403
Custody Seal Present? Dyes Q o Seals Intact? Des Q(Vo
Packing Material: ❑Bubble Wrap ❑bubble Bags ❑None ❑ Other
Thermometejr,•,Gun rD: 92TO48 Type of ice: 0t/vet ❑Blue
©'t+
Cooler Temp ('C): -7 qCorrection Factor: Add/Subtract (°C) 0,0
—
/
Cooler Temp Corrected ('C}: v
i
USDA Regulated Soil (Q�N/A, water sample(
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
MY— nNn
Datellnitiafs Person Examining Contents:-7 11'M hi-�)
Biological Tissue Frozen?
❑Yes []No ❑t- N/A
❑None
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples an ice, cooling process
has begun
Old samples originate from a foreign source I#nternationally,
inrludinc Hawaii and Puerto Alm)? MYm F INn
Comments/biscre anc :
Chain of Custody Present?
12yes
[]NO
❑N/A
1.
Samples Arrived within Hold Tinge?
z ves
❑No
❑N/A
2.
Short Hold Time Anal sls 02hr.17
EJY&4
ONO
N/A
3.
Rush Turn Around Time Re nested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
JJVC5
Na
N A
5
Correct Containers Used?
-Pate Containers Used?
©Yes
. 4es
[]No
QNo
❑NIA
0 N/A
6.
Containers Intact?
©Yes
ONa
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
(]No
N(;A
8.
Sample Labels Match CC)C?
-Includes Date/Time/ID/Analysis Matrix:
❑Yeti
❑No
❑N/A
9.
Head space in VOA vials (5s-6mm)?
Qyes
❑No
❑L N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
`]Yes
Ljye3
ONO
014D
QN/A
I NIA
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes (—]No
Person contacted: Date/Tlme:
Project Manager SCURF Review: _4 /tip) Date:
Project Manager SRF Review: Vi,— Date:
Page 11 of 13

Document Name:
Document Revised: February 7, 2018
aceAnalj�tical
Sample Canditlon U on Receipt{SCUR)
Pa e.l of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
`Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 {water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # Wo# : 92438403
PM: MWB Due Dale: 08/02/19
CLIENT: 92-Rllvao NC
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pH Adjustment Log for Preserved Samples
Sample so
Type of Preservative
pH upon recefpt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot a
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm wlll be sent to the North Carolina DEHNR Certification Office (i.e.,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 12 of 13

Stormwa ter Mongt�lran
Chain of Custody Record
Project Number/Name:
SW Outfall #02 B
Pro-eci Location: ATI SM - Bakers
Sam ler's Sign. tipre-
Date:
E
a
Z u
v
U
�
o
u
E
i
Requested 'lest Parameters
1-7
- 3
S
G
G /<D
HNO3
Y
Total Recoverable: Chromium, N; kclt Co m )cr. Bile
G
G /O
1-1NO3
Y
Cadmium
y
G
G /S
1-12SO4
Y
COD
G
G /D
None
Y
BOD
3 "S
G
I G /0
Note TY
TSS
Onsite Field
II Analysis
Onsite Field Tem erature Analysis
pl-1: ZJ (s-1+.)
Sample Time:
Temp: anj, (0c) Sample Time: 3• y�
Analysis Time:
Analysis Tinic.- Sy�
Meter Cal;bratcc1: yES
Thermometer Calibrated: (Y / N
Sameling and field analysis completed by:
Relin uishc By: 29Q=2&A
Receivccl B i 'yam �ti.v7iC,71 777,
Date:
Tine S �.._
Date: L e
I'imc
Relll] lilSl Cd B
Received B �ij,.u� /';
Date: S
'I'ime: ILI .3 11
ate: 4- Time: L; 5 L¢
EHS-SW-Chain of Cosiody Outfall 02-Rev 001
Page 13 of 13

aceAnaIXical"
www.pacMbs.com
i
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 2BO78
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
pCCI? r�
44
iW ;
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

2cmnapical0
J "wpacelebs.cm
Project: SW Outfall #03 (8)
Pace Project No.: 92438402
Charlotte Certification lDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # t-4170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #. E87627
Kentucky UST Certification #: 84
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaA/ELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
f
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13

e
aceAnalytical
www.patelehs.c=
i
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HunlersviHe, NC 28078
[phone]
Project:
Pace Project No.:
SW Outfall #03 (B)
92438402
Analysts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92438402001
SW OUTFALL #03 (B)
EPA 200.7 Rev 4.4 1994
SH1
5
PASt-A
SM 254OD-2011
MJP
1
PASI-A
SM 521OB-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 13

Pace Analytical Services, LLC
?ceAnalytical � 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpecafabamm [phone]
r
ANALYTICAL RESULTS
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Sample: SW OUTFALL #03 (S) Lab ID: 92438402001 Collected: 07/23/19 15:33 Received: 07/24/19 11:45 Matrix: Water
Parameters Results Units Report Limit of Prepared Analyzed CAS No. Quat
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 15:38
Collected Date
07/23119
1
07/23/19 15:38
Collected Time
15:26
1
07/23/19 15:38
pH
7.2 Std. Units
0.10
1
07/23/19 15:38
Temperature
23.8 deg C
0.50
1
07/23/19 15:38
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND ug/L
1.0
1
07/31/19 13:56 08/01/19 21:58
7440-43-9
Chromium
ND ug/L
5.0
1
07/31/19 13:56 08/01/19 21:58
7440-47-3
Copper
17.8 ug/L
5.0
1
07/31/19 13:56 08/01/19 21:58
7440-50-8
Nickel
ND ug/L
5.0
1
07/31/19 13:56 08/01/19 21:58
7440-02-0
Zinc
16.8 ug1L
10.0
1
07/31/19 13:56 08/01/19 21:58
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
19.8 mg/L
5.0
1
07/29/19 13:06
5210B SOD, 5 day
Analytical Method: SM 5210B-2011
BOD, 5 day
2.2 mg1L
2.0
1
07/25/19 03:10 07/30/19 04:29
52200 COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mg/L
25.0
1
07/26/19 15:30 07/29/19 17:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08102/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

0
aceAnalj&al
www. pacelehs.mm
i
QUALITY CONTROL DATA
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 489431
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description:
200.7
MET
Associated Lab Samples. 92438402001
METHOD BLANK: 2641114
Matrix: Water
Associated Lab Samples: 92438402001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Cadmium
ug1L
NO
1.0
08/01/19 21:11
Chromium
ug1L
ND
5.0
08/01119 21:11
Copper
ug1L
NO
5.0
08/01/19 21:11
Nickel
ug1L
NO
5.0
08/01/19 21:11
Zinc
ug/L
NO
10.0
08/01/19 21:11
Qualifiers
LABORATORY CONTROL SAMPLE:
2641115
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Cadmium
ug/L
500
489
98
85-115
Chromium
ug1L
500
494
99
85-115
Copper
ug1L
500
494
99
85-115
Nickel
ug/L
500
492
98
85-115
Zinc
ug1L
500
497
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
MS
92437770001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug1L
ND
500
Chromium
ug1L
ND
500
Capper
ug1L
22A
500
Nickel
ug1L
ND
500
Zinc
ug1L
133
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug1L
NO
500
Chromium
ug1L
NO
500
Copper
ug/L
53.0
500
Nickel
ug/L
5.4
500
Zinc
ug1L
45.9
500
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
Qualifiers
2641117
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
503
499
101
100
70-130
1
500
503
497
100
99
70-130
1
500
517
516
99
99
70-130
0
500
500
493
99
98
70-130
1
500
640
632
101
100
70-130
1
2641119
MSD
Spike MS MSD MS MSD % Rec
Conc, Result Result % Rec % Rec Limits RPD
500 502 504 100 101 70-130 1
500 502 512 100 102 70-130 2
500 547 555 99 100 70-130 1
500 496 502 98 99 70-130 1
500 544 551 100 101 70-130 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit lapresented to the right of the reautt,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Qual
Page 5 of 13

aceAnafytica!
Iwwwpacelabs.CM
r
I
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 488845
QC Batch Method: SM 254OD-2011
Associated Lab Samples: 92438402001
METHOD BLANK: 2638666
Associated Lab Samples: 92438402001
Parameter
Total Suspended Solids
QUALITY CONTROL DATA
Analysis Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 2.5 07/2911913:04
LABORATORY CONTROL SAMPLE:
2638667
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 2639441
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 2639442
Parameter
Units
Total Suspended Solids
mglL
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS %fl Rec
Conc. Result % Rec Limits Qualifiers
250 250 100 90-110
92438421003 Dup
Result Result RPD Qualifiers
58.7 57.3 2
92438506002 Dup
Result Result RPD Qualifiers
440 444 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

/ I '
;aceAnalXical"
www.patela6�.mm
i
QUALITY CONTROL DATA
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 488319 Analysis Method: SM 521 OB-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92438402001
METHOD BLANK: 2636157
Associated Lab Samples: 92438402001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2636158
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result limit Analyzed Qualifiers
ND 2.0 07/30/19 03:34
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 203 103 84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

aceftlytical0
—pacetabs.com
QUALITY CONTROL DATA
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 488767 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples'. 92438402001
METHOD BLANK: 2638169
Associated Lab Samples: 92438402001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2638170
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 07129/1917:06
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX'SPIKE & MATRIX SPIKE DUPLICATE: 2638171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 3010 100 100 3090 3100 85 95 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Reo % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L ND 100 100 119 121 99 102 90-110 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

aceAnapical
wwwpacelahs.com
QUALIFIERS
Project: SW Outfall #03 (8)
Pace Project No.: 92438402
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC, Page 9 of 13

aoAnalj tical
—pacelebs.crom
r
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Lab ID
Sample ID
92438402001
SW 0UTFALL#03 (B)
92438402001
SW 0UTFALL#03 (B)
92438402001
SW OUTFALL #03 (B)
92438402001
SW OUTFALL #03 (B)
92438402001
SW OUTFALL #03 (B)
Date: 08/02/2019 11:30 AM
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch Method - OC Batch Analytical Method Batch
EPA 200.7 Rev 4.4 1994 489431 EPA 200.7 Rev 4.4 1994 489630
SM 254OD-2011 488845
SM 521OB-2011 488319 SM 521OB-2011 488349
SM 5220D-2011 488767 SM 522OD-2011 489096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document Name:
Document Revised: February 7, 2018
�aceAnaljftal'
Sam le Condition Upon Recei t SCUR
Page 1 of 2
Document No.: I
Issuing Authority:
F-CAR•CS•033-ReV-06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden Greenwood ❑ Huntersville (] Raleigh❑ Mechanicsville[)
MI Client Name: .. Wp# : 92433402
Pr j ct ft
�I _i- � 1 JI: a I.i� '.R :.fit:: lry` . ... II � � 1 �I I I IM II ■ I�
Courier; ❑fed Ex ❑UPS❑U5P5 ❑Client
❑ Commercial ❑Pace []Other:
92438402
Custody Seal Present.? []Yes ❑No Seals Intact? ❑Yes QNo
Datelinitials Person Examining Contents:
Packing Material: []Bubble Wrap []Bubble Bags ©None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No ©N/A
Q18 Gun lo; 92TO48 Type of ice: ©Wet ❑Blue ❑None
Cooler Temp ('C): Correctlon Factor. Add/Subtract ('Cj 0.0
Temp should be above freezing to 6°C
Cooler Temp Corrected ('Qj c-', QSamples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sail (IRJ'N/A, water sample)
Did samples originate in a quarantine zone within the United States'. CA, NY, or SC (check maps)? Did samples originate from a foreign source linternatlonaay,
My— rlNn inrlridinc Hawaii and Puprtn Alrnl) F—Ivnc F-�lun
Comments/Discrepancy:
Chain of Custody Present?
[: Yes
QNO
❑N/A
1.
Samples Arrived within Hold Time?
QV/Cs
ONO
❑N/A
2.
Short Hold Time Anal sls 02hr.l?
+ Yes
ND
NA
3.
Rush Turn Around Time Requested?
Oyes
Q no
❑N/A
4,
Sufficient Volume?
10res
ONO
NJA
S
Correct Containers Used?
-Pace Containers Used?
QYes
yet
ONO
No
❑N/A
N A
6.
Containers Intact?
Dyes
EJNo
N/A
7.
Dissolved anal sis: Sam les Field PAered? y
❑Yes
_[]NO
N/A
S.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis MaWx:
❑Yes
ONO
❑N/A
9.
Headspace in VDA Vials (>5-6mm)?
Qyes
ONO
❑N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
Dyes
❑No
No
❑141A
N%A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes ONO
Person contacted; Date/Tlme:
Project Manager SCURF Review: �/l' , Date:
Project Manager SRF Review: f, /� Date:
Page 11 o113

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-`
8P1U-1 liter Plastic Unpreserved (N/A)
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alAS-125 mL Plastic H2504 IPH < 2) IC$-)
X"
BP3N•250 mt plastic HNO3 (pH < 21
BP4Z-125 ML Plastic ZN Acetate & NaOH (>9)
9P4C-125 mL Plastic N20H (pH > 12) (CI-)
WGFU-WidC-mouthedGlass jar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (CI-)
AG1H-1 liter Amber HC) (pH < 2)
AG3U-250 nL Amber Unpreserved (N/A) (0)
AG1S 1literAmberH2SO4(pH<21
RG35.250 ml. Amber H1SO4 (pH < 2)
RG3A(DG3A)-250 mL Amber NH4CI (N/A)(Ct-)
DG9M-40 mL VOA HCI (N/A)
VG9T-40 mL VOA Na2S203 (N/A)
VG9U-40 mt VOA Unp IN/A)
DG9P-40 mL VOA H3PO4 (tJ/A)
VOAK IS Vials per kit)-5035 kit IN/A)
V/GK O Vials per kit)-VPH/Gas kit (N/A)
SPST-125 rnL Sterile Plastic (N/A — lab)
SM-250 mL Sterile Plastic (N/A — lab)
BP3A-250 mt Plastic (NH2)2504 (9.3.9.7)
ACiGU-100 mL Amber Unpreserved vials (N/A)
VSGU-20 mL Scintillation vials (N/A)
OG9U-40 mL Amber UnpreServed vials (N/A)
'9
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Stormwater M onitori��
Chain of Custody Record
Project Number/Name:
SW Outfall #43 B
Project Location: ATI SM - Bakers
Sampler's Si rrature:
Date:
f
l;
a
a
a•
a.
..
>,
6.
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E
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�
Requested '[jest Parameters
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a$
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FIN03
Y
Total Recoverable: ChrOMiLim, Nickel. Co pvr. Zinc
g
G
G /0
HNO3
Y
Cadmium :Ly
3
G
G /d)
i-I2SO4
Y
COD
G
G IQ
Notre
Y
BOD
3 3
G
I G /c
LNonc]Y
rSS
Onsite Vield
I -I Analysis
Onsite Field Tens verature Anaivsis
I)H:�_• R (S.U,)
Sample "rime:
,3•p�
Temp: 4, 3.8 ,(-C) Sample'I'i911C: 3• .
Analysis Time:
�
Analysis Time: J
Meter Calibrated: Yes
Thcrnx)n)et r Calibrated: / N
S;rm gin ► and field Analysis completed by:
Relinquished By:
Received
Date:
l It c: %D
Date;: '-) ,
Tii lc: jIIVj5
Relinquished B r
Received By: ,t-
Date: ` l l
Tinge:
LIL
Date:
EHS-SW-Chain at Costody Outfall 03-Rev 001
Page 13 of 13

July 23, 2019
Attn: Central Files EcEWE, D
N.C. Division of Water Quality IUL 8 6 2019
1617 Mail Service Center CEht7��i�!
Raleigh, NC 27699-1617 DWR Si C7lC)AI
Central Files:
-W'ATI
P.O. Box 5030
2020 Ashcrali Avenuc
Monroe, NC 291 1 1-5030
Phone: (704) 289•451 1
Fax: [phone]
Einail: 1ylcr.mcrccrC�alinmtal5.com
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitorin Period
sample Number
Start
End
Year 10 — Period 1
19
March 1, 2018
1 Au,ust 3 l , 2018
Analytical monitoring includes:
• Non Contact Cooling Water #I - #8
If you have any questions or need additional information, please contact me at 704-289-451 1.
Thank you.
Sincerely,
-a�L 'mom" --
Tyler Mercer
Manager, EH&S

Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
ikon-ContactCooling Wastewater
n2vd Pow �' , Alm 6%Aql�-
AlLe �ira /,rhea/
40 CFR Part 136
.A.
Non-
Contact
Cooling
Water#..
Sampling
Date
Sampling
Time
Estimated
Flow(MGD)
Total
Residual
Chlorine
(mg/L)
Temperature
pH (std. units)
Effluent
Downstream
Upstream
4
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7 $1

e
aceAnalytical
Iwwwpatxfab3.corrr
June 26, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersvVe, NC 28078
(704 )875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on June 14, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

0
/5a'cie Ana lj4ical
www.pacembs.com
1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification (Ds
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaA/ELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, LLC. Page 2 of 19

m
accAnalytical
H+ww,pacela�l,com
SAMPLE ANALYTE COUNT
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analysts
Reported
Laboratory
92433143001
NON-CONTACT#1
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143002
NON-CONTACT#2
EPA1664B
JMS
1
PASI-C
SM 4500-Cl G-2011
GC
1
PASI-A
92433143003
NON-CONTACT#3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143004
NON-CONTACT#4
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143005
NON-CONTACT#5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143006
NON-CONTACT#6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143007
NON-CONTACT#7
EPA 1664B
JMS
i
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143008
NON-CONTACT#8
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalytical
www.pacarabs.com
i
1
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#1 Lab ID: 92433143001 Collected: 06/13119 07:50 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. UC.
Page 4 of 19

aceAnalytical
—pecelebs.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#2 Lab ID: 92433143002 Collected: 06/13/19 08:15 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quai
HEM, oil and Grease Analytical Method: EPA 1664B
Oil and Grease NO mg/L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI 0-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 0612612019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

a
aceAnalytical
/ www.pacelabs.corn
E
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Nuntersville, NC 2BO78
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#3 Lab ID: 92433143003 Collected: 06/13/19 08:40 Received: 06/14119 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 , 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mglL 0,024 1 06/18/19 17:57 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2019 02A0 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19

ace Analytical
. paealaft com
i
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#4 Lab ID: 92433143004 Collected: 06113119 09:00 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease NO mg/L 5.0 1 06126119 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual NO mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 0612612019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

�;a'o Analyticale
/ wwwpacelebs-com
i
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#5 Lab ID: 92433143005 Collected: 06/13119 09:25 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 06/26/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 06126/2019 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

ace Analytical
www,pecAlabs.eam
E
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NO 28078
[phone]
Sample: NON-CONTACT#6 Lab ID: 92433143006 Collected: 06113119 09:45 Received: 06114/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 06/26/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual NO mg1L 0,24 10 06118l19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 9 of 19

1�5a'ne Analytical
www pacela�s.com
r
f
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#7 Lab ID: 92433143007 Collected: 06/13/19 10:10 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mglL 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50.5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAnalyticat
www.pacelabs.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#8 Lab ID: 92433143008 Collected: 06/13/19 10:35 Received: 06/14119 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06118/19 17:57 7782-50.5 H3
Date: 06126/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 11 of 19

aceAnaVical
wtwcpacelabs.corn
1
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 483277 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92433143001,92433143002,92433143003,92433143004,92433143005,92433143006,92433143007,
92433143008
METHOD BLANK: 2612203 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 4.8 06/26/19 06:42
LABORATORY CONTROL SAMPLE:
2612204
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mglL
38.5 38.5
100
78-114
MATRIX SPIKE SAMPLE:
2612205
92433576001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
37.2
97 78-114
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06126/2019 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

1 aceAnaij4ica!0
r-wwwpacela6s.rnm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
QC Batch: 481875 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
METHOD BLANK: 2605891 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143D08
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L NO 0.024 06/18/19 17:57
SAMPLE DUPLICATE: 2605892
92432727001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L NO ND H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shaA not be reproduced, except in full.
Date: 06/26/2019 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

15a'neAnalytical"
i
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydiazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether,
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NFLAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
❑ate: 06/26/2019 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

0
aceAnalytical
—pacelabs.crom
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Lab ID Sample ID QC Batch Method QC Batch
92433143001
NON-CONTACT#1
EPA 1664E
483277
92433143002
NON-CONTACT#2
EPA 16649
483277
92433143003
NON-CONTACT#3
EPA 1664B
483277
92433143004
NON-CONTACT#4
EPA 1664B
483277
92433143005
NON-CONTACT#5
EPA 1664B
483277
92433143006
NON-CONTACT#6
EPA 1664B
483277
92433143007
NON-CONTACT#7
EPA 16646
483277
92433143008
NON-CONTACT#8
EPA 16648
483277
92433143001
NON-CONTACT#1
SM 4500-CI G-2011
481875
92433143002
NON-CONTACT#2
SM 4500-CI G-2011
481875
92433143003
NON-CONTACT#3
SM 4500-CI G-2011
481875
92433143004
NON-CONTACT04
SM 4500-CI G-2011
481875
92433143005
NON-CONTACT#5
SM 4500-CI G-2011
481875
92433143006
NON-CONTACT#6
SM 4500-CI G-2011
481875
92433143007
NON-CONTACT#7
SM 4500-CI G-2011
481875
92433143008
NON-CONTACT#8
SM 4500-CI G-2011
481875
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
Page 15 of 19

Document Name:
Document Revised: February 7, 2018
- ace�nallrtlCrlj�
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Sample Condition Upon Receipt(SCUR
Page 2 of 2
Document No.:
Issuing Authority:
F•CAR•CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville L�I Ralelgh❑ Mechanicsville❑
Client Name:
433143
�-" Project
Courier: []Fed Ex []UPS ❑USPS []Client
❑ Commercial QPace ❑Other: �1 1y sill !l1111
2133143
i
Custody Seal Present?--QYes--- ❑No- ---Seals Intact? ❑Yes ❑No
Packing Material: ❑Bubble Wrap 08ubble Bags ❑None ❑ Other
Therrnom 25IR G 42T048 Type of Ice: Owe ❑slue
QIR Gun 10:
Cooler Temp ('C): ( ��. �.•� Correction Factor; Add/Subtract ('C) ().0
Cooler Temp Corrected ('C): "r�(+?
USDA Regulated Soil (0 N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, Or SC (check maps)?
❑Yes ONo
8 I
Date/tnitials Person Examining Contents:
alologicalTissue Frozen?
[]None [-]Yes []No ❑N/A
Temp should be above freezing to VC
❑Samples Out of temp criteria. Samples on ice, coobng process
hasbegun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto RICO)? ❑Yes []NO
Comments/Discrepancy:
Chain of Custodv Present?
,�
Yes
❑No
❑NIA
1.
Samples Arriuedwithin Hold Time?
Y
❑No
❑N/A
2.
Short Hold Time Analysis J<72 hr,)?
Yes
No
N/A
3,
Rush Turn Around Time Requested?
C]Yes
[DNO
[]N/A
4.
Sufficient volume?
.Yes
No
❑N/A
S.
Correct Containers Used?
❑Yes
[3NO
❑N/A
6.
-Pace Containers Used?
21Yres
No
NIA
Containers Intact?
Dyes„
QNo
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes„
❑No
❑ /
S.
Sample Labels Match CDC?
Eyes
❑No
[]N/A
9.
/ {
-Includes Date/Time/ID/Analysis Matrix:
S
Headsp ace in VOA vials (?5-6mm)?
Qyes
[]NO-
ON/A
10,
Trip Blank Present?
❑Yes
[QNo
❑N/A
11,
Trip Blank Custody Seals Present?
Yes
ONO
N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review: r✓
DatelTlme;
Field Data Required? []Yes ONO
Date: f, r 1 4!l!l
Date:
--ram
--
Page 16 of 19

Document Name:
Document Revised: February 7, 2018
aCeAnalytical
Sample Condition Upon Recei t SCURI
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pa cc Car olinos Quality Office
"Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Cofiform, TOC, 011 and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project #i ' WOR
pM : MW
-- c i ENT"
cftOI2.433143 B g
Due Date-. 06/2
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
PH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
lot $1
Note: Whenever there is a discrepancy affecting North Caroilna compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 17 of 19

s
gATI
Specialty IMT.:eats
Storm Tatar Montt ri
(NON CONTACT)
Bakers North
Chaim of Custody Record
Project Number/Name: NonContact Cooling Water Project Location: ATI SM
- Bakers
Sampler's Signature:
Date, (o
L
u
E
m
=
la
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u
0
.0
i—'
5
ti
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ca
'�
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�,
Requested Test
o
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as
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Parameters
a
g,
0
L
QJ
F
3--
a
iL
C!
«•
o
c
°
�l?f�331 "
p -(,o ac,J4�J
G
G/d)
None
Y
7, J
Residual Chlorine
G
G/O
None
Y
j
Residual Chlorine
G
GAD
None
Y
Residual Chlorine
Ca
•'00—
G
G/O0
I None
Y
Residual Chlorine
IVOA
9 5i,
G
G/19
None
Y
6
Residual Chlorine
don -Co.+tL,+ 6
*J%,
G
G/a
None
Y
dJ,9
Residual Chlorine
Aloe-C aztJl?
•-/0,
G
G/®
None
Y
� (�
7.3'
IResidual Chlorine
M-C"C-48
:S5�,J
G
I Gla
None
I Y
I Z.
Jd2, q
I Residual Chlorine
Meter Calibrated: f N Thermometer Calibra Q/ N
Sampling and Field analysis completed by:
Relinquished By:
Received By : rT-R . 7 e'a,
Date: - Time: /r...r
Date: fir! I'i Time:
Relinquished By:
Received By. -
Date L/ -Je' Time: t, ,,,,�
Date:(. ` '' j J Time: i' j j cj
EHS BakerSouth SW REV d 2 5/10/2016
bo i
f7 Vl
cstaz,�
Page 18 of 19

�0►�I I
Specialty Ai'Ilerials
Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
i
nage #2
Project Number/Name: NonContact Cooling Water
Project Location: ATE 5M - Bakers
Sampler's Signature:
Date:
Eo
`n
GJ
°'
i=
°.
c
CL
F
w
M,
C
u
GIw CL
?
LA
LA
a
V
0
v
�►
f'
�
0
Requested Test
Parameters
J
-/3`
S' o-
G
G
HCL
Y
f
Oil & Grease
G
G
HCL
Y
Oil & Grease
DA-Corr
OA
G
G
HCL
Y
U. q
Oil & Grease
D -G-
•'&V,
G
G
HCL
Y
Oil & Grease
Algp _C , T9
G
G
HCL
Y
Oil & Grease
off- ac f
5,..
G
G
HCL
Y
Oil & Grease
07 32yuf
Q
G
G
HCL
Y
7 S
Oil & Grease
Co�Ifa
/Q '
G
G
HCL
Y
Oil & Grease
Meter Calibrated: j N
Thermometer Calibrated: / N
Sampling and Field analysis completed by:
Relinquished By:
Relinquished By:
Date: - y
Time:
Date :01 11i-1 li
Time:
Relinquished By:
TV 77,775 777,7
Relinquished By: �r„��/%J.�
Date : UE 1'/ l
Time: /lf 1, ,,, ,�._
Date :
[Time:1
EH5 Baker South SW REV # 2 5/10/2036
Xl
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vu<
zoo,
GO x
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Page 19 of 19