NCG030333_MONITORING INFO_20151214

W k,2 u
STORMWATER DIVISION CODING SHEET
NCG PERMITS -
PERMIT NO.
DOC TYPE
❑ HISTORICAL FILE
�. MONITORING REPORTS
DOC DATE
❑ (:g o6 u
YYYYMMDD

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ c�2,6 / / O 613
YYYYM M D D

Semi-annual Stormwater Discharge Monitoring Report Ice
for North Carolina Division of Water Quality General Permit No NCG030000
r - ;
- Oaf g submrRe¢ x,., . ='s .AM
.�w, ,:3....
:�.. .max.,»+-.u�.9�r > , c. _,.•Y ., _ ....
' CERTIFICATE OF COVERAGE NO. NCG634d 3 1 SAMPLE COLLECTION YEAR a Q 1's
FAdLITYNAME Shn o f L IVtr:)J5,el-oft gc+eJ1'f,4SAMPLEPERIOD ❑Jan•June ❑lulyDec
' h
COUNTY C, jC&jJ G a&
PERSON COLLECTING SAMPLES
LABORATORY.
Comments on
0 i 6Je V, V,�+"Cd, G IL l y
analysis:
or tim Monthly /moor 1
�[/u•eG LV;Svc� O�sscrVvfrcrt� DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
Cart. a ❑2ero-fiow ❑Water Supply []SA
❑Other
e1A.f,d ;Irs l er At, No r-rou> on i sus 62
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/Olt 3 -i
Part A: Stormwater Benchmarks and Monitoring Results'
RECEIVE®
DEC 14 CUiS Nodischoroethis Period?
Outfall No.
t
Date sample
Collected'
(mo/dd/yr)
24•hour ralnfail
amount,
Inches'
Total Suspended Solids
CENT
PHd1,N
Standard uniu
L FILES
Egrm
Lead
21nc
Non•PolarO&G/
Total Petroleum
Hydrocarbons
'
Total Toxic
Organics'
Benchmarks
1W mg/Cor 50 mg/L
6:0=9A'
0.007 mg/L
0.033 mg/L
-0.067 mg/L
1S mg/L
- l mg/L
'monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same ouuan.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge, monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended'sites may be eligible for a waiver of the rain gauge requirement.
`See General Permit, Table 3 identifying the especiallysensitive receiving water classifications where the more protective benchmark applies.
' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subjectto the requirement to sample (far metal finishing use the definition as found in 40 CFR 433,11; for semiconductor
Manufacture use the.definition astound in 40 CFR 4,69.12; far electronic crystal manufacture use the definition as found in 40 CFR469.22: and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
t. Permib0are: 11/1/2012.10/31/20i 7 S%VU.245, last revised 10/25/2012
- :. Page I of 3

I

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver. the, discharger shall sign the following certification statement;
'Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring repart. I further certify that this facility is implementing the all the provisions of the
_ solvent -management plan included to the Stormwater Pollution Prevention Plan:'
Name (Print nafne)
Title (Print title)
r X�l
ure) (Date)
Note: Results must be reported in numerical formaL Do not report Below Detection Limit, BDL, <PQI, Non -detect, ND, or other similar non -numerical
.formal.. When results are.below the applicable limits, they musCbe reported In the format. '<XX mit/L'. where XX is the numerical value of the detection
limit; reporting limit, etc. in,mg/L..
Note: if you report a sample value in.exeess of the benchhark, you must implement Ter 1, •Tier 2, or T1er3 responses. See General Permit text.
Part B: Vehicle Maintenance Aiea Monitoring Results: only for facilities averaging > 55 gal of new of per onth.
o ddischarge this period??
a
'
OuttaO No.
-
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
.amount
Inchesr
Non -polar O&G/TPH by
EPA 1664fSGT•HEM)
Total Sus ended Solids
p-
pH
Benchmarks u=a
_
-
IS mg/L
100 mg/L ar.50 mg/L'
6.0 - 9.0 SU
711
Footnotes from Part A also apply to this Part
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: I1/l/2012.10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

IN
A

Note: If you report o sample value in excess of the benchmark you must implement Tier I, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART A AND PARTS MONITORING RESULTS: -
• A BENCHMARK -E%CEEDAua TRIGGERS TIER I REQUIREMENTS.. SEE PERMIT PART 11 SECTION B. '
• 2 EXCEEDANCES.IN A ROW FOR THE SAME PARAMETER AT THE SAME-OUTFALL-FRIGGER xJEIb2 REQUIREMENTS: 3EEPERROT PART II SECTION B.
.. -- - • TIER 3: HASYOUR FACII& HAO d-OR MORE BENCHMARKEXCEEOENCES FOR THE SAME PARAMETER AT ANY ONE 011TFALL7 YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? - YES- 0 NO ❑ -
REGIONAL OFFICE CONTACT NAME.
Mail an original and one copy of this DMR. lncludina oil 'No Dischorae'reports. within 30 days of receipt of the lob results for at end olmonitarina period
in the case of'No Dischame'reoortsl to:
Division of Water Quality
Attn: DWQCentrat Files
1617 Mail Service Center
Raleigh, North Carolina 27699.1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
'I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or Persons who manage the system, or
"those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are signifrwntpenalties for submitting false Information, -including the possibility of fines and imprisopment'for knowing violations." '
Permit Date: l l/1/201240/31/2017
(Date)
SWU•245, last revised 10/25/2012
Page 3 of 3
°Tay

/SIMS �/
METAL
`0 MANAGEMENT
December 10, 2015
Division of Water Quality
Attn: DWQ Central Files
North Carolina Department of Environment and Natural Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Monthly Monitoring Report - August 2015
General Permit NCG03000
Certificate of Coverage N . NCG030333
To NCDENR Division of Water Quality,
SMM Southeast LLC (d.b.a., Sims Metal Management - New Bern Facility) herein provides
the Monthly Monitoring Report for August 2015 for the facility located at 2912 Neuse
Boulevard in New Bern, North Carolina. Monthly monitoring has been implemented under
Tier 11 requirements. .
A copy of the Discharge Monitoring Report, Qualitative Monitoring Report and associated
laboratory report is attached. Please contact Bobby Glenn or me at [phone] should
you have any questions or concerns.
Sincerely,
% Jeremy Tyree
Manager
Enclosures �Ft
14 2015
Monthly Stormwater Monitoring Report 4 BKr7e RE
Qualitative Monitoring Report FERPERM1iTN,
Pace Laboratory Report
Page I of I

A'
NCDEWR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: hnp://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
Permit No.: IN/C/A/O/ 3/ O/ 0/ O/ Of or Certificate of Covera a No.:
Facility Name: .5 M M S,� 6,4 k 2ae c-/ /. L C, /(/ e Ef--A 9
County: _rr , a d fd, Phone No. 2 5 d —G 3;P,--o d9
Inspector: ej > r -fit V I 1 Pl e t�i
Date of Inspection:
Time of Inspection: �Jl, Zq
Total Event Precipitation (inches): t , / 3
Was this a `Representative Storm Event" or "Measureable Storm Event' as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event' or during a `measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
Page i of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. 061
c
Receiving Stream: _() t, n ,
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: S rn Li
3. Odor: Describe any distinc of ors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): N �!t
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and S is very cloudy:
1 2 3 (� 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 0 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes �6
9. Is there evidence of erosion or deposition at the outfall? Yes �Nq�
10. Other Obvious Indicators of Stormwater Pollution: v
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWO-242, Last inodlfied 10/2S/2012

ace Analytical
aM+v.VacabEswm
September 29, 2015
Jeremy Tyree
Sims Metal Managment
2912 Neuse Boulevard
New Bern, NC 28560
RE: Project: SIM STORMWATER
Pace Project No.: 92265901
Pace Analytical Servicas, Inc.
98001Qncey Ave. Suite 100
Huntereville, NC 28078
[phone]
Dear Jeremy Tyree:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C-,-,/ - �J-A-11-�
Kevin Godwin
[e-mail]
Project Manager
Enclosures
u Armandina Padinha, Sims Metal Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 1 of 11

aceAnalytical e
w»w.pxela6a.cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 25078
[phone]
CERTIFICATIONS
Project: SIM STORMWATER
Pace Project No.: 92265901
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Flonda/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDS
2225 Riverside Drive, Asheville, INC 28804
Flonda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wnnen consent of Pace Analytical Services, Inc.. Page 2 of 11

/SIMS
M ETAL
MANAGEMENT
December 10, 2015
Division of Water Quality
Attn: DWQ Central Files
North Carolina Department of Environment and Natural Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Monthly Monitoring Report - October 2015
General Permit NCG030000
Certificate of Coverage No. NCG030333
To NCDENR Division of Water Quality,
SMM Southeast LLC (d.b.a., Sims Metal Management- New Bern Facility) herein provides
the Monthly Monitoring Report for October 2015 for the facility located at 2912 Neuse
Boulevard in New Bern, North Carolina. Monthly monitoring has been implemented under
Tier 11 requirements. Please note "no flow" was recorded for this time period.
A copy of the Discharge Monitoring Report is attached. Please contact Bobby Glenn or me
at [phone] should you have any questions or concerns.
Sincerely,
Je my Tyree
Manager
Enclosures
RRcz�-/�R®
DEC14 2015
Dw>z RFc 16ty
Monthly Stormwater Monitoring Report
Page I of I

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03.a 9 a 3
FACILITY NAME 5ftM 5Ou��ea�Y'f•4G Nt�6rCw RGGq(ilid-�
COUNTY. C rrt r/,e A --
PERSON COLLECTING SAMPLES�—
LABORATORY Lab Con. p
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR 1 n - 7 - / ��
SAMPLE PERIOD ❑ Jan -June ❑ July-Oec
or In Monthly' [month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑2ero•0ow []WaterSupply ❑SA
[]Other
/D- 91- l q,- R tnt °se i fr`d Gs'F d M NO Fl ou/ 0brserdLf,',m ei1
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period?'
• ou"all No.
'Date Sample
Collected'
(mo/dd/yr)
24-hour ralnfatl
amount,
Inches' _
r
Total Suspended Solids
PH,;
pH,;
units
Copper
trod
r
Zinc
Non -Polar 09G/
Total Petroleum
Hydrocarbons
Total r Toxic
Orgaalcss
Benthrtwrks==i
- 100 mg/L or 50 mg/L
6.0-9.0-
'0.007 mg/L
0.033 mg/L
0.067 mg/L
IS mg/L -
I mg/L
' Monthlysampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same paiameterat the same outfall.
'For sampling periods with no discharge at any single oulfall, you must still submit this discharge.monitoring report with acheckmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for awaiver of the.rain gauge'requirement..
.4 See GeneraLPermit, Table 3 identifying the especially sensitive receiving water classifications where the more Prot ective.benchmark applies.. .
s Total Toxic Organics sampling is applicable only for those facilities which peiform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines.for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31►. —
Permit Date: It/t/2012.10/31/2017 5WU•245, last revised 10/25/2012
Page 1 of 3 - -

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
'Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
070),1 certify that to the best of my knowledge and belief• no dumping of concentrated tout organics into the stormwater or areas which are exposed to rainfall or
slormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan.'
Name (Printname)
Title (Print id(!)
(Date)
Note: Results must be reported In numerical format. Do not report Below Detection Limit. BDL, <PQL, Non•deted, ND, or other similar non numerical
format.. When results are below the applicable limits, they most be reported In the format.'<XX mR/L". where XX is the.numerical value of the detection
limit; reporting limit, etc. in mg%L - -
value in excess cj the benchmark
must implement fer I, Tier 2 of Tier 3 responses: See General Permit text.
Nate: ljyoureport a somple
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil psytnonth.
No discharge this period?'
' OulfaU No:
Date Sample
Collected'
(moldd/Yr) .
24•hout rainfall
-amount,
Inches .. _ _
Mon -polar O$G/TPN by
..EPA.1664 fSGhNEM)_
"
Total Suspended Solids
pH
Benchmarks rua
- -
-
15 mg/L
1W mg/L or 50 ing/L� --
6.0 - 9.0 SU
Footnotes from Part A also apply to this Part 6
• See General Permit text. Table S. identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Dale: 11/l/2012.10/31/2017 SWU-245,last revised 10/25/2012
Page 2 of 3'

'L
Note: If you report a Sample value in CXCess of the benchmark, you must implement'T"rer 3, 77er 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART 11 SECTION 0.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETERAT THE SAME OLFTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION 0.
• TIER 3: HAS YOUR FACILITY HAD A OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO
IF YES, HAVE YOU CONTACTEDTHE.OWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Moif on original and one copy of this 0MR In "I&ng all 'No Dischome'repaMt within 3f) days of recelpt of the lob results (or at end of moniforina period
in the case of No Oischome'repom) to:
Division of Water Quality
Alto: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699.1617 -
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
'I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
-am aware that there are significant penalties for submitting false Information, including the possihilityol fines and imprisonment for knowing violations.'-
(Dort¢)
Permit Date: II/IR012-10/31/2017
SWU445, last revised 10/25/2012
Page 3 613- - -

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
-CERTIFtCATEOF COVERAGE No. NCG030 3 3 3
FAauTYNAME 5Mh SDu+A•Po?oj" 7,,70.,/r/
COUNTY C ra v, :. _
PERSON COLLECTING SAMPLES e o '
LABORATORY Lab Bert.
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR (? tl
SAMPLE PERIOD ❑ Jan•June ❑ JulyDec
or Monthly' [month)
DISCHARGINGT CLASS QORW OHQW ❑Trout QPNA
QZero-flow Owater supply DA
QOther
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
F1 No dischorae this period?'
ovdall No.
t
'Date Sample
Collected'
(mo/dd/
24-hourr2lnf2ll
m
aount.
Inches
t
Total Suspended Solids
PH,
pH,
units
Copper
lead
r
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
'
TotalToxlc
Organics'
Benchmarks ==> -
100 mg/L or So mg/l.
- --6.0-9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L'
-- - 1S ma/L
- I mg/L
Q
' Monthly sampling (instead of semi-annual) mus( begin with the second consecutive benchmark exceeoance for the same parameterat the same outtdu,
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with checkmark here.
-'The total precipitation must be retorded using.data from an rain gauge. Unattended sites may be eligible for a waiver of the rain gauge -requirement.
`See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requiremenDto sample (for metal finishing use the definition as found in 40 CFR 433.1 Y, for semiconductor
manufacture use the definition as -found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22i and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: I ljlh012.10/31/2017 SWU•24S, last revised 10/25/2032
Page i of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shalt sign the following certification statement:
'Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best at my knowledge and belief• no dumping of concentrated toxic organics into the stormwatecor areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print nam )
� AA
- _ Title (Print title)
f gnatur , Vlate)
Mote: Results must be reported in numerical formal Do not retort Below Detection Limit, BOL, <PQL, Non -detect, ND, or other similar non -numerical
_ format. When results are below the applicable limits,, they must be reported In the format.'<XX mtt V where XX is the numerical value of the detection
IimA; reporting limit, etc. In mg/L.
Ndtr.'1Jyou report's ampfe'va/ue in excessoJthe benchmark, you rust implement rrrer 1, Tiei 2, or 77er 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Resultsi only for facilities averaging > SS gal of new oil peymonth.
No dischorae this oeriodra
'
OuNaU No.
_ ....
.Date Sample
Collected'
(mo/dd/Yr). ..
24•hour rainfall
- amount,
.., r
_ .Inches _. __ .._
Non -polar 08G/TPH by
EPA 1664 (SGi-HEM).
Total Suspended Solids
pH
Benchmarks a:J
_
LS arg/L
- 100 mg/L or 50 mg/L•
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part
See General Permit text, Table 5, identilying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012.10/31/2017 - - SWU-245, last revised 10/25/2012
Page 2 of 3

Note:, l u report a sample vcfue in exteis Of -the bertchmar[, you.must implement Tier 1, tier I, or tier 3 responses. See General. Permit tent: -` a
f you -
.-'FOR PART AAND -PART'RMONITORINGAESUIIS - - - -
_ .A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11SECTION B.
_2 E%CEEDANCES IN A ROW FORTHkSAME PARAMETERAT-THE SAMEOUTFAil:TRIGGEA4aEH 2 REQUjAEMWS• SEE PERMIT PART 11 SECTION a.
• TIER 3: 'HAS YOUR FACILITY. HAD a OR MORE BENCHMARK E%CEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE OWQ REGIONAL OFFICE? 'YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail on ortolnal and one toav of this OMR. lnNudina oil Na Discharge" reports, within 30 days of receipt o/ the rob results for at end al monitoring Period
in the case of No Dischame'reaortsl to:
Division of Water Quality
Altn: DW Q Central Res
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
'I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel property gather and evaluate the information submitted.,Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is: i6-iii ties[ of myknowfe`dge 5od�liellef,-tEu-e;-aiiuiale, and complete. I
am aware that there are significant penalties tar submitting false information, including the possibility of Fines and imprisonment for knowmgviolations.* -
Permit Date: Il/i/2012.10131/2017
SWU-245, last revised 10/25/2012
Page303 '

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03_j�9 3 3 j p
FACILITY NAME ri /1 /'j Sn g f
COUNTY r ,, ✓ fL
PERSON COLLECTING SAMPLES T r t r2 N T 7_�r
LABORATORY Lab CoA. Jf
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR ao r y
SAMPLEPERIOD ❑Jan•June ❑Julfy-Dec
or Omonthly' Sr/ month
DISCHARGING TO CLASS ❑ORW ❑ QW�❑PNA
Zero -flow ❑Watersupply ❑SA
�Olher
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -)
1LWo discharge this period?'
OuHall No.
Date Sample
Collected'
mo/dd/ r)
24•hour rainfall
amount,
Inches'
Total Suspended Solids
pH;
Standard units
Copper
lead
Zinc
Mon-Potar O&G/
Total Petroleum
Hydrocarbons
'
Total Toxic
Organics
0enchmorks ==>'
- -•
100 mg/L or 50 mg/L
6.0-9.0"
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1 mg/L
' Monthlysampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outran.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge, monitoring report with a checkmark here.
'The total precipitation must be recorded using data.frohi an on -site rain gauge. Unattended sites may be eligible fora waiver of the rain gauge requirement.
' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. - -
' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (far metal finishing use the definRion astound in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22: and. for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
e
Permit Date 11/112012•10/31/2017 _- SWU-24S, last revised 10/25/2012
Page I of 3

ti
4. •r.

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General �.
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organic
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan._"
Name (Print name
--ill`tY Ma-vL����
Title (Prim title)
(Agnature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported In the format,'<XX mR/L'. where XX is the numerical value of the detection
limit; reporting fimit;etc. Inmg/L
Note: If you report a sample value in excess of The benchmark, you must implement Titer 1, Tier 2, or Tiler 3 responses. See General permlt text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month.
' 'n No discharee this oeriode
-
OulfaU No.
Date Sample
Colrected'
(mo/dd/yr)
24•hour rainfall
a_ mount,
Inches'
Non..polar O&G/TPH by
EPA 1664 fSGT-HEM)
Total Suspended Solids
-
pH
Benchmarks rza
_
-
1S atg/L
100 mg/L or 50 mg1V
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part
See General Permit teat. Table .S• identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/3/2012.10/31/2017 _ SWU-245, last revised 10/25/2012
91 - Page 2 of 3

Note. If you report o sample value in excess of the benchmark, you must implement Tier 2, Tier 2, or Tier 3 responses. See General Permit text. .
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEOANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2ExCEEDANCESINA:ROW FOR THE SAhsEPARA FgRAT7HESAME .tlUTFAI4Ifg13GERTIER 2REOUtBEMEW9,-'6EEPtRMRP'AiT.itsicnou-&.
a TIER 3: HAS YOUR FAC,1fTY HAD 4 ORMORE BENCHMARK EKCEEDENCES-FOR THE SAME PAf�AR1ETER AT ANY ONE OUTFALL7 YFS ❑ NO
IF YES, HAVE YOU CONTACTEO THE OYIQ REGIONAL OfFICE1 YES ❑NO❑
REGIONAL OFFICE CONTACT NAME:
Division of Water Quality
Attn: DW Q Central Files
1617 Mail Service Center
Raleigh, ttorth Carolina 27699.1617
'I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
'those persons directly responsible for the information, the'information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am awarethat there are significant penaldesfor submitting falte information, including the possibility of rines and imprisonment lot knowing violations.'
(Date)
Permit Date: 1l/I/2012.10131/2017 SWU•245, last revised 10/2S/2012
• - • _ - Page 3 of 3

p /
SIMS
M ETAL
MANAGEMENT
August 1, 2015
Division of Water Quality
Attn: DWQ Central Files
North Carolina Department of Environment and Natural Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
a
RE: Monthly Monitoring Report - July 2015
General Permit NCG030000
Certificate of Coverage No. NCG030333 .
To NCDENR Division of Water Quality,
RECEIVED
AUG 17 2015
CENTRAL FILES
DWR SECTION
SMM Southeast LLC (d.b.a., Sims Metal Management - New Bern Facility) herein provides
the Monthly Monitoring Report for July 2015 for the facility located at 2912 Neuse
Boulevard in New Bern, North Carolina. Monthly monitoring has been implemented under
Tier II requirements. Please note "no flow' was recorded for this time period.
A copy of the Discharge Monitoring Report is attached. Please contact Bobby Glenn or me
at [phone] should you have any questions or concerns.
Sincerely,
Jeremy I YTyree
Manager
Enclosures
Monthly Stormwater Monitoring Report
i;
i
Page I of l
s

rD,

FACItTTYNAM%,J_Mtl sn.Ii`f-t!tfo sF LIi( ,ll%C✓DfY'/1. Il
COUNTY, G/ ¢.v, e.�ti_
PERSON COLLECTING SAMPIM'�� a
UtBORATORY' . _
La .C_ei4li
Corninentsan iampte collection oranIy11
s7t -
Pai4A _.,an Monito ingResult
y t>atoSimpla` °24.bourraln}all: 1
QGtfallNo-., a��,.-ice Nam: ,�i,TotnlSutPededSoll�r '
Collected amount . Sung
_ _ .fine/ee/w1.. '2623
Permit Date,ll/3%2072.10/31/2D17
' ' Noo•Polsr t3!
�PD�r Lead RTint i TOWIPotrolc
- _ rNyaiocaitio
sameoutfallF
ugeiequir''e"meoC -.
EPA
.manufacture`
twined inlh-e
seinicanducto!
it or(a Yiotle'r`a'y. .
51VU•2aS, ISitiairicd 10)25/2012
7agc I of3
7
1

J
Oared upon my intjuiry of the Person r rsw� rde�tly responsible toi managlrig compparue +ash the peimn moms onng�req (reJr ic�it7toial tor7[ organics; { (TTOJ I:cendy that rotha best ofmy>edge and belief,mo dumping of concentrated toxic organics mtoa oatormwater or areasiuhtch�arc eposed to in_fallon. ' t
sturtnwat raleot� has octunetfsfrtce hlrn tha`la T sc! aigc man tonng�repo`rt �`ctl�,ei ce`rt�fy, that,this to ty rs �mplementing,the5il the provisions of t c ! soh ent managem`en_t'pJan
inNudep mthe SiorrtmwaterPollubon.Preveotion Plan "
mm
Note'Results must be reported to nurnuriwl format Do not resort Below Deteeron t(mmt 9DL;<pQt, Non;deted ND; or othet;dtmmlacnon�numerifal
lvhlt
• format When resifts are* ,tielovr the appljcable limits; then'muse be reiio led iri the"torniat' "<7iic`mv/L"''ui}iere><X is'the riunieri[al value ofthe detedioh
limit, reporting Ifrimn etc mmmg/L': -
R A. 7'1
Notei.IJyaa report a sample volue In'excess of the benchmorfy you musEmmplemegt Tier 1,.Te '2,'�or1%r3 respon a Ste G_ eeeiol permit text
Part'B: Vehide;N151ntenancaArea Monitoring Resulu; only for facilities ayeragtng > SS;gal of.new oil per month:
oatnotr s fr
y 3
Sec General Pemillexi; tattle 5 ldenufy n e especially s nsri vc reccrving water clasfiouons wharf tAe more `pip erti4e ticmchmarli applies`;
Per'mi[Datec_71/1/20I2=10/31/2017 SW,U-2a5'Jastreviied 70/25/2012
q... -
Page 3
[—,-Irvo alscnor
e, tnfs periodT
Oiitf511 No.
'6sicSampic
M
24rhuurralnfa0,1:
m
CoilcRcd. '.
r)
amount
ches
Non.
Iay(mod
EPA.or1-1,"..,Toti*s-p
_ Q)
.-.
endedW-- 66
... - .
DH
;Oenchmorks tea.
_. _ -.
>
.:
--= . ,
. 15(mg/4 -
"100 m g/
.. -_ g/L`or 50 m t•
6.0 9 O SU
,8
om PbR A also apply

m
M&I On bpi -inot crut 01011
Orvrsron f
inter
I Ir
SWU-245; last i6visid-IMS/2012
'Pap of 3­
"r.'6
I

/SIMS
METAL
MANAGEMENT
8/01/2015
Division of Water Quality
Attn: DWQ Central Files
North Carolina Department of Environment and Natural Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Semi -Annual Discharge Monitoring Report - Year 3 Period 1
General Permit NCG030000
Certic fiate of Coverage No. NCG030333
To NCDENR Division of Water Quality,
RECEIVED
AUG 17 2015
CENTRAL FILES
DWR SECTION
SMM Southeast LLC (d.b.a., Sims Metal Management- New Bern Facility) herein provides
the Year 3 Period 1 Semi -Annual Discharge Monitoring Report and Qualitative Monitoring
Report for the facility located at 2912 Neuse Boulevard in New Bern, North Carolina.
Its Sims understanding that although outfall 001 is technically sealed preventing a
concentrated discharge of stormwater runoff to the adjoining drainage ditch, the NCDENR
has requested a representative sample be collected from the overflow that intermittently
permeates though the riprap at the northwestern corner of the property. This request was
verbally communicated during a site inspection by the NCDENR (Mr. Vernon Riggs) and
subsequent Compliance Inspection Report dated August 29, 2014.
In response, Sims has collected a representative sample. The analytical data and
qualitative results are provided herein. Please note this sample was collected as water
permeated through the riprap allowing contact with the underlying sediment along the
drainage ditch. Additionally, in response to the.best management practice suggestions
conveyed during the NCDENR site inspection and Compliance Inspection Report, Sims has
1.) Placed hay bales along the northern property boundary to impede surface water flow
and control sediment runoff and 2.) Redesigned the low lying native soil areas on the
property via grading and finishing with concrete at the surface. Furthermore, a drainage
ditch with #hand #2 stone has been completed along the northern property border. The
drainage'ditch'.has been designed to accept, transport and discharge stormwater into an
onsite retention pond (pond currently under construction). All efforts to date have/are
being completed'to effectively manage stormwater onsite and considered best
management practices (BMPs) for the facility.
As implied above, Sims intends to continue its proactive approach in the mitigation of
metals in the surface water during construction of onsite BMPs; however, maintains that
Cutfall 001 remains sealed due to Sims inability to collect a representative sample (Semi
Page I of 2

Annual Discharge Monitoring Report August 8, 2014) and that the sample collection point as
directed by the NCDENR (August 29, 2014) does not lend itself to an accurate portrayal of
the properties surface water. Subsequently Sims is continuing on the path of managing
stormwater onsite and will update the NCDENR accordingly.
A copy of the Semi -Annual Discharge Monitoring Report, Qualitative Monitoring Report and
Pace Analytical Laboratory Report are attached. Please contact Bobby Glenn or me at (252)
633-0892 should you have any questions or concerns.
Sincerely,
eeey Tyree
Manager
Enclosures
l
Semi -Annual Stormwater Monitoring Report
Qualitative Monitoring Report
Pace Analytical Laboratory Report
Page 2 of 2

Fryt
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling Out thisform, please visit: h-q]2;1112QEtal,ncdenr-rg/web/wq/ws/stltnr)desw#ta
Permit No.: N/C41-0131 O/ d/ 0/ !J'/ or Certificate of Coverage No.: jy/C���0�3
Facility Name: S M M to idhee01tC- ill u �c�w iLcC pr ('r <i
County: C r ey eai Phone No. } 5 G 33 OS� j--
Inspector: _T e .^ e rtv 7" T 4,,-
Date of Inspection:_( ^a — ao
Time of Inspection: /57 : D C
Total Event Precipitation (inches): I I I
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below,)
21�yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureahle storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "nleasureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office:
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
Permitty r Designee)
Paget of 2
SWU-242, Last modified 10/2S/2012

1. Outfall Dc
Outfall No. OD
Receiving Stream:
Describe the indus
(pipe, ditch,
activities that occur
the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: S N O
3. Odor: Describe any disti ct o rs that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): _
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 l/ 4 5
5. Floating Solids: Choose the number which best describes the amount of Floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
1 2 lam' 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
11
9. Is there evidence of erosion or depositioti,at the outfall?
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Yes No
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, last mudified 10/25/2012

(�55?eAnalyfijfoca
wxwpxNabs.com
June 17, 2015
Pace Analytical services, Inc.
9800 Kincey Ave. Suite 100
• Huntersville, NC 28078
[phone]
Eli Holland
One Environmental Group, LLC
223 S. Wilmington St.
Unit 200-D
Raleigh, NC 27601
RE: Project: STORMWATER
Pace Project No.: 92252847
Dear Eli Holland:
Enclosed are the analytical results for sample(s) received by the laboratory on June 04, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
kevin.godwin@pa elal
Project Manager
Enclosures
0
o
e
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Pagel or 27
11 i

aceAnalytical e
a 'pscelebs:com
Project: STORMWATER
Pace Project No.: 92252847
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
F
'4
I
al
C.
1'
y
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the w6ften consent of Pace Analytical Services, Inc..
a °
Pace Analytiyal services, Inc.
A 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone] •'
CERTIFICATIONS °
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
° r
FloridalNELAP Certification #: E87627 '
Kentucky UST Certification #: 84 '
West Virginia Certification #: 357
VifginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
4
e
Page 2 of 27 ' r

1;
11
4�1
N

IaceAnalyticale
wwwpecek6s:com -
SAMPLE SUMMARY
Project: STORMWATER
Pace Project No.: 92252847
Lab ID Sample ID Matrix Date Collected Date Received
92252847001 OUTFALL 001 Water 06102/15 19:15 06/04/15 10:00
e
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
1. Huntersville, NC 28078
[phone]
Q
Page 3 of 27 .I
1�

aceAnalytical
w pecelabs.cem
11
Pace Analytical Services, Ina I'
9800 Ki ncey Ave. Suite 100
-ti
Hunlersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER
92252847
SAMPLE ANALYTE COUNT
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
t {
92252847001
OUTFALL 001
EPA 16646
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA625
BPJ
60
PASI-C
EPA624
GAW
37
PASI-C
SM 2540D
RC
1
PASI-R
SM 4500-H+B
JW1
1
PASI-R
I
1
1
'
,1
'j
t.
o..
-q
p .
rv'
REPORT OF LABORATORY ANALYSIS
1
This report shall not be reproduced, except in full,
t
without the written consent of Pace Analytical Services, Inc..
Page 4 of 27
'
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pp/�p pp r� •
GceAn lyfical
axw.pscelabs.cam
Project:,. STORMWATER
Pace Project No.: 92252847
..
ANALYTICAL RESULTS
i.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 106
Huntersville, NC 28078
[phone]
' Sample: OUTFALL 001
Lab ID: 92252847001 Collected: 06/02/15 19:15
Received: 06/04/15 10:00 Matrix: Water '
a Parameters
Results
Units
• Report Limit OF
Prepared
Analyzed
CAS No. Oual
µ
1664 SGT-HEM, TPH
C
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
NO
mg/L
5.0 1
06/16/15 10:57
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation
Method: EPA 3510
Aldrin
NO
ug/L
0.050 1
06/08/15 10:30
06108/1518:27
309-00-2
alpha-BHC
NO
ug/L
0.050 1
06/08/15 10:30
06/08/15 18:27
319-84-6
beta-BHC
NO
ug/L
0.050 1
06/08M510:30
06/0811518*27
319-85-7 '
delta-BHC -�
NO
ug/L
0.050 1
0610811510:30
06/08/15 18:27
319-86-8 -
gamma-BHC (Llddane)
NO
ug/L
0.050 1
06/08/15 10:30
06/08/15 18:27
58-89-9
Chlordane (Techpical)
NO
ug/L
0.50' 1
06/08/15 10:30
06/08/15 18:27
57-74-9
4;4'-DDD 'I,
NO
ug/L
0.050 1
06/08/15 10:30
06/08/15 18:27
72-54-8
4,4'-DDE ^ii
NO
ug/L
0,050 1
06/08/15 10:30
06/08/15 18:27
72-55-9
4;4'-DDT ; ,1)'i:
NO
ug/L
0,050 1
06/08/15 10:30
06/08/15 18:27
50-29-3
Dieldrin !,^',�
ND
ug/L
0.050 1
06/08/15 10:30
06/08/15 18:27
60-57-1
Endosulfanl �,%+:j�,
NO
ug/L
0.050 1
06/08/15 10:30
06108/1518:27
959-98-8
Ehdosulfan II4,,
NO
ug/L
0.050 1
06108/1510:30
06/08/15 18:27
33213-65-9
Endosulfan suffete.'
NO
ug/L
0.050 1
06/08/15 10:30
06/08/15 18:27
1031-07-8 .
Endrim
NO
ug/L
0.050 1
06/0811510:30
06/08/15 18:27
72-20-8
End rin aldehyde:!
NO
ug/L
0.050 1
06/08/15 10:30
06/08/1518:27
7421-93-4
Heptachlor i'%'
NO
ug/L
0.050 1
06108/1510:30
06/08/15 18:27
7644-8
Heptachlor epoxide
NO
ug/L
0.050 1
06/08/15 10:30
06/0811518:27
1024-57-3
PC9. 1016 (Arocli�.1016)
NO
ug/L
0.50 1
06/08/15 10:30
06/08/15 18:27
12674-11-2
PCB,,-1221 (Aropl6r. 1221)
NO
ug/L
0.50 1
06/0811510:30
06/0811518:27
11104-28-2
PCB'.'.-1232 (Arocior 1232)
NO
ug/L
0.50 1
06/08/15 10:30
06/08/1518:27
11141-16-5
PCB-1242 (Arodlor 1242)
NO
ug/L
0.50 1
06/08/15 10:30
06/08/15 18:27
53469-21-9
PCB-1248(AroG8r7248)
NO
ug/L
0.50 1
06/08/15 10:30
06/08/15 18:27
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0,50 % 1
06/08/15 10:30
06/08/15 18:27
11097-69-1
PCB-1260(Aroc1or. 1260)
NO
ug/L
0.50, 1
06108/1510:30
0610811518:27
11096-82-5
Toxaphene
NO
ug/L
0.50 1
06108/1510:30
06/081151827
8001-35-2
{Surrogates
Tetrachloro-m- 18ne (S)
50
%
20-110 1
06/08/15 10:30
06/08/15 18:27
877-09-8
Decachlorobipl erlyh (S)
60
%
20-138 1
06/08/15 10:30
06/08/15 18:27
2051-24-3
'200.7 MET ICP;
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
Copper' 'r;;r
40.8
ug/L
5.0 1
06/08/1517:10
06/09/1523:52
7440-50-8
Lead ,�,��.
31.2
ug/L
5.0 1
06/08/1517:10
06109/1523:52
7439-92-1
Zinc ;'r `
118
ug/L
10.6 1
06108/1517:10
06/09/1523:52
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparalll), Method: EPA
625
r
Acenaphthene`:'' ,
NO
ug/L
5.0 1
06109/1513:00
06/10/1504:26
83-32-9
. Acenaphthylen2; ,.
NO
ug/L
5.0 1
06M9/1513:00
06/10/1504:26
208-96-8
Anthraoene
NO
ug/L
5.0 1
06109/1513:00
06/10/1504:26
120-12-7
Benzitline
NO
ug/L
50.0 1
06/09/15 13:00
06/10/15 04:26
92-87-5 ,
Benzo(a)anthracene
NO
ug/L
5.0 1
06/09/15 13:00
06/10/15 04:26
56-55-3
Benzo(a)pyren,6 4_
NO
ug/L
5.0 1
06/09/15 13:00
06/10/15 0426
50-32-8
Benzo(b)Fluoranthene
NO
ug/L
5.0 1
06/09/1513:00
06110/150426
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0 1
06/0911513:00
06/10/1504:26
191-24-2
REPORT OF'LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 06117/2015,11:52 AM
i
without the written consent
of Pace Analytical Services, Inc..
Page 5 of 27
cl

N
A
A
N
4
ID

aceAnalytical
wwwpecelabs tom
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92252847
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Sample: OUTFALL 001 Lab ID: 92262847001 Collected: 06/02/15 19:15 Received: 06/04/15 10:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Oual
Pyrene.,'.
. 1,2,44 Trichlorobenzene
2,4,e-Trichlorophenol
I. t.
l i i
. Date 06/17/2015 11:52 AM
Analytical Method: EPA 625 Preparation Method: EPA 625
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04.26
207-08-9
ND
ug/L;
5.0
1
06/09/15 13:00
06/10/15 04:26
101-55-3
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
85-68-7
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
59-50-7
ND
ug/L
10.0
1
06/09115 13:00
06/10/15 04:26
111-91-1
ND
ug/L :
5.0
1
06/09/15 13:00
06/10/15 04:26
111-44-4
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
108-60-1
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
91-58-7
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
95-57-8
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
7005-72-3
ND
ug/L
5.0
1
06/09115 13:00
06/10/15 04:26
218-01-9
ND
ug/L 1
5.0
1
06/09/15 13:00
06/10/15 04:26
53-70-3
ND
ug/L
25.0
1
06/09/15 13:00
06/10/15 04:26
91-94-1
ND
ug/L 1
5.0
1
06109/1513:00
06/1011504:26
120-83-2
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
84-66-2
ND
ug/L
10.0
1
06109/1513:00
06110/1504:26
105-67-9
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
131-11-3
ND
ug/L
5.0
1
06/09/15 13:00
06/1011504:26
84-74-2
ND
ug/L
20.0
1
06/09/15 13:00
06/10/15 04:26
534-52-1
ND
ug/L
50.0
1
06/09/15 13:00
06/10/15 04:26
51-28-5
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
121-14-2
ND
ug/L
5.0 r
1
06/09/15 13:00
06/10/15 04:26
606-20-2
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
117-84-0
ND
ug/L :
5.0
1
06/09/15 13:00
06/10115 04:26
122-66-7
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
117-81-7
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
206-44-0
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
86-73-7
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
87-68-3
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
118-74-1
ND
ug/L
10.0
1
06/09/15 13:00
06/10/15 04:26
77-474
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
67-72-1
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
193-39-5
ND
ug/L
10.0
1
06/09115 13:00
06/10/15 04:26
78-59-1
ND
ug/L
5.0
1
06109115 13:00
06/10/15 04:26
91-20-3
ND
ug/L
5.0
1
06/09115 13:00
06/10/15 04:26
98-95-3
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
88-75-5
ND
ug/L I
50.0
1
06/09/15 13:00
06/1011504:26
100-02-7
ND
ug/L , -
5.0
1
06/09/15 13:00
06/10/15 04:26
62-75-9
ND
ug/L,
5.0
1
06/09/15 13:00
06/10/15 04:26
621-64-7
ND
ug/L
10.0
1
06/09/15 13:00
06/10/15 04:26
86-30-6
ND
ug/L
10.0
1
06/09115 13:00
06/10/15 04:26
87-86-5
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
85-01-8
ND
ug/L
5.0
1
06/09/15 13:00
06/1011504:26
108-95-2
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
129-00-0
ND
ug/L
5.0
1
06/09/15 13:00
06/10/15 04:26
120-82-1
ND
ug/L
10.0
1
06/09/15 13:00
06/10/15 04:26
88-06-2
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
without
the written consent
of Pace Analytical Services, Inc..
K
I
,
.1
t .
.•r
Page 6 of 27

aceAnalytical
a oacelebs.cort
, • 1
ANALYTICAL RESULTS
1 � ,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100'
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92252847
Sample: OUTFALL 001
Lab ID: 92252847001
Collected: 06/02/15 19:15
Received: 06/04/15 10:00 Matrix:
Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Oual
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA
625
Surrogates
Nitrobenzene-d5 (S)
29
%
10-120
1
06/09/15 13:00
06/10/15 04:26
4165-60-0
2-Fluorobiphenyl (S)
25
%
,15-120
1
06/09/15 13:00
06/10/15 04:26
321-60-8
Terphenyl-d14(S)
76
%
'11-131
1
06/09/15 13:00
06/10/15 04:26
1718-51-0
Phenol-d6(S)
11
%
•1,.16-120
1
06/09/15 13:00
06/1011504:26
13127-88-3
2-Fluorophenol(S)
15
%
10-120
:_ 1
06/09/15 13:00
06/10/15 04:26
367-12-4
2 4 6-Tribromophenol (S)
63
%
10-137
1
06/09/15 13:00
06/10/15 04:26
118-79-6
624 Volatile Organics
.Acrolein
Acrylonitrile
Benzene
Bromodichloromelhane
Bromoform
Bromomethane
Carbon tetrachloride
,Chlorobenzene
,Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromoch loro methane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-1)ichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
'cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
. Methylene Chloride
1,1,2,2-Tetrachloroelhane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chl orofl u orometh a ne
Vinyl chloride
- Surrogates
4-Bromofluorobenzene (S)
. Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
Date: 06/17/2015 11:52 AM
Analytical Method: EPA 624
NO
ug/L
5.0
1
06/09/15 21:29
107-02-8
ND
ug/L
50.0
1
06109/15 21:29
107-13-1
NO
"Jug/L
2.0
1
06/09/15 21:29
71-43-2
NO
ug/L
2.0
1
06/0911521:29
75-27-4
NO
fug/L
2.0
1
06/09/15 21:29
75-25-2
ND
!ug/L
2.0
1
06/09/15 21:29
74-83-9
NO
;ug/L
2.0
1
06/09/15 21:29
56-23-5
NO
.ug/L
2.0
1
06/09/15 21:29
108-90-7
ND
(fig/L
2.0
1
06/09/15 21:29
75-00-3
NO
•': ug/L
5.0
1
06/09/15 21:29
110-75-8
NO
',:ug/L
2.0
1
06/09/15 21:29
67-66-3
NO
ug/L
2.0
1
06/09015 21:29
74-87-3
NO
'.;'69/L
2.0
1
06/09/15 21:29
124-48-1
NO
; 46/1-
2.0
1
06109/1521:29
95-50-1
ND
'�:ltg/L
2.0
1
06/09/l 5 21:29
541-73-1
NO
,;u91L
2.0
1
'06/09115 21:29
106-46-7
ND,'Lg/L
2.0
1
-06/09/15 21:29
75-34-3
NO
Ug/L
2.0
-1
i 06/09/15 21:29
107-06-2
ND
•, ipgll_ •,
2.0
1
+• 06/0911521:29
75-35-4
ND
-- ug/L
2.0
-1
06/09/15 21:29
156-59-2
NO
6g/L
2.0
1
06/09/15 21:29
156-60-5
NO
:Ng/L'
2.0
1
06/09/15 21:29
78-87-5
ND
!,u6/L
2.0
1
06/09/15 21:29
10061-01-5
NO
ug/L
2.0
1 -
06/09/15 21:29
10061-02-6
NO
'; ug/lL
2.0
1
06109/1521:29
100-41-4
NO
: ,'ug/L
2.0
1
06109/1521:29
71-09-2
ND
; 66/L
° 2.0
1
.' 06/09/15 21:29
79-34-5
ND
,Gug/L
2.0
1
06/09/15 21:29
127-18-4
NO
, ug/L
2.0
1
06/09/15 21:29
108-88-3
NO
"'-ug/L
2.0
1
06/09/15 21:29
71-55-6
NO
ug/L
2.0
1
06/09115 21 *29
79-00-5
ND
' ug/L
2.0
1
06/09/15 21:29
79-01-6
NO
ug/L
2.0
1
06/09/15 21:29
75-69-4
NO
ug/L
2.0
1
06/09/15 21:29
75-01-4
91 %' 70-130 1
109 %' 70-130 1
120 t.% 70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. .; 1
06/09/15 21:29 460-00-4
06/09/15 21:29 2037-26-5
06/09/15 21:29 17060-07-0
i
Page 7 of 27

Pace Analytical Services, Inc.
• 9800 Kincey Ave. Suite 100
aceq /I Analytical Huntemville, NC 28078
mrwpsrole6s.can [phone]
�i
ANALYTICAL RESULTS
Project:. STORMWATER
Pace Project No.: 92252847
'
Sample: OUTFALL 001
Lab ID: 92252847001,' Collected: 06/02/15 19:15
Received: 06104/15 10:00 Matrix: Water
Parameters
Results Units Report Limit; DF
Prepared, Analyzed CAS No. Oual
SM 2540D
2540D Total Suspended Solids
Analytical Method:
I.
Total Suspended Solids'
36.4 mg/L '10.0 ' 1
06/05/15 10:52
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+0
pH at 25 Degrees C
6.8 Std. Units 1.0 1
06/05/15 14:30 H6
I
I •
REPORT OF LABORATORY ANALYSIS
This repor(,shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc..
a
C
Page 8 of 27
m

fli
ka
114
n
u
r1l

aceAnalytical
1/ wrrw.peceless.mm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
STORMWATER
Pace Project No.:
92252847
QC Batch:
GCSV/21659 Analysis Method: EPA 1664B
QC Batch Method:
EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples:
92252947001
METHOD BLANK: 1485451
Matrix:
Water
,
Associated Lab Samples: 92252847001
Blank
Reporting
,
Parameter
Units
Result.
Limit
Analyzed
.Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO
5.0
; 06/16/15 10:56 „
LABORATORY CONTROL SAMPLE:
1485452
'
Spike
'. LCS
1-CS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20
16.0
80
64-132
MATRIX SPIKE SAMPLE:
1485453
92253652001
Spike
MS
MS % Rec
Parameter
Units
Result
Conc.
Result
%Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
,ND
20
18.3
91 64-132 ,
b
a
Results prevented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the reaua.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2015 11:52 AM without the written consent of Pace Analytical Services, Inc_
I
Page 9 of 27

Pace Analytical Services, Inc.
•
Analytical
9800
Kincey Ave. Suite 100
Hunlersville, NC 28078
wawpeceieba.cam
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
1 ,'
Pace Project No.: 92252847
QC Balch: MPRP/18647
Analysis Method: EPA200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92252847001
METHOD BLANK: 1478723
Matrix: Water
Associated Lab Samples: 92252847001
1,
'!
Blank Reporting)
tl
Parameter
Units Result ILimit Analyzed •Qualifiers
Copper
ug/L ND 5.0 06/09/1523:18 j
r
Leah;
ug/L ND.. 5.0 06/09/1523:18
Zinc,
ug/L NO 10.0 06/09/15 23:18
s
r
LABORATORY CONTROL SAMPLE: 1478724
�•;
,1
Spike LCS LCS % Rae
' 1
Parameter
Units Cone. Result % Rae Limits Qualifiers
'.I1i
1
Copper
ug/L 500 . 455 91 85-115
-•
Lead . i
ug/L 500 456 91 85-115
"I
Zinc
ug/L 500 450 90 85-115
I
I"
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478725 1478726
MS MSD
92252759003 Spike Spike MS MSD MS MSD
%Rec
!:Max:1
., Parameter Units
Result Cone. Cone. Result Result %Rec %Rec
Limits
RPD RPDQual
Copper ug/L
ND 500 500 458 458 91 91
70-130
0! 20
Lead. ug/L
ND 500 500 426 426 85 85
70-130
0 20
Zinc - ug/L
ND 500 500 463 462 92 91
70-130
0 20' 1i
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479001 1479002
MS MSD
'
92253118001 Spike Spike MS MSD MS MSD
% Rae
I,
Max',
•Quai
.' Parameter Units
Result Cone. Cone.- Result Result %Rec %Rec
Limits
RPD RPD
Copper ug/L
7.8 50Q . 500 474 516 i93 102
70-130
8 2b
Lead ug/L
5.8 500: " 500 449 492 89 97
70-130
9 20
Zinc ug/L
42.2 500' 500 500 542 92 100
70-130
8 20. -
h
1 a
t
I
Results presented on this page are in the units Indicated by the "Units" column except w mre an attemate unit Is presented lathe fight of the result.
REPORT OF LABORATORY ANALYSIS
Rt
This report shall not be reproduced, except in full,
Date: 06/17/2015 11:52AIN
without the wnden consent of Pace Analytical Services, Inc..
Page 10 of 27
1
ace

.
Pace Analytical services, Inc.
®
Analytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
w Pscelabs.tnrn -
1
[phone]
QUALITY CONTROL DATA
1
t I
Project: STORMWATER'
Pace Project No.: 92252847
1_
QC Batch: MSV/32059
Analysis Method: EPA624 I
QC Batch Method* EPA 624
Analysis Description: 624 MSV
'
Associated Lab Samples: 9225284'7001
ace
METHOD BLANK: 1480084
: <'1
Matrix: Water
Associated Lab Samples: 92252847.001
-
i�'•
Blank
Repotting
1
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
NO
2.0
06/09/15 15:26
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
06/09/15 15:26 II
1,1,2-Trichloroethane
ug/L
ND
2.0
06/09/15 15:26 '
1,1-Dichloroethane
ug/L
ND
2.0
06/09/15 15:26
1, 1 -Di chloroethene
ug/L
ND
2.0
06/09/15 15:26
1,2-Dichlorobenzene
f'
ug/L
ND
2.0
06/09/15 15:26
1,2-Dichloroethane
ug/L
NO
2.0
06/09/15 15:26
1,2-Dichloropropane
ug/L
ND
2.0
06/09/15 15:26
1,3-Dichlorobenzene
ug/L
ND
2.0
06109/1515:26
.-
1,4-Dichlorobenzene
ug/L
ND
2.0
0610911515:26 ,
2-Chloroethylvinyl ether
ug/L
NO
5.0
06109/15 15:26
Acrolein
ug/L
ND
5.0
06/09/15 15:26
Acrylonitrile
ug/L
NO
50.0
06/09/15 15:26
Benzene
ug/L
NO
2.0
06/09/15 15:26
Bromodichloromethane
ug/L
NO
2.0
06/09/15 15:26
Bromoform
ug/L
NO
2.0
06109/1515:26
Bromomelhane
ug/L
ND
2.0
06/0911515:26 .
Carbon tetrachloride
ug/L
NO
2.0
06/09/15 15:26
Chlorobenzene
ug/L
NO
2.0
06109/1515:26
Chloroethane
ug/L
NO
2.0
06/09/15 15:26
'
Chloroform
ug/L
NO
2.0
06/09/15 15:26
Chloromethane
ug/L
NO
, 2.0
06/09/15 15:26
.
cis-1,2-Dichloroethene
ug/L
NO
2.0
06/09/15 15:26
cis-1,3-Dichloropropene
ug/L
NO
' 2.0
06/09/15 15:26
Dibromochloromethane
/
ug/L
ND;
2.0
06/0911515:26
,
Ethylbenzene
+ �
ug/L
ND�
a 2.0
06/09/15 15:26 ,.
Methylene Chloride
ug/L
3.2°
2.0
06/09/15 15:26 C9', I`
'
Tetrachloroethene
ug/L
ND
2.0
06/09/15 15:26 1
Toluene
ug/L
NO'.
,2.0
06/09/15 15:26
trans-1,2-Dichloroethene
'
ug/L
NO
2.0
06/09/15 15:26
trans-1,3-Dichloropropene
ug/L
NO
2.0
-06/09/15 15:26
Trichloroelhene
ug/L
ND •
2.0
06/09/15 15:26
•yh
Trichlorofluoromethane
ug/L
NO
2.0
06/09/15 15:26
)�
Vinyl chloride
,
ug/L
NO
2.0
06/09/15 15:26
1,2-Dichloroethane-d4 (S)
%
114
70-130
06/09/15 15:26
4-Bromofluorobenzene (S)
%
90
70-130
06/09/15 15:26
Toluene-d8 (S)
%
103
70-130
06/09/15 15:26
Results presented on this page
are In the
units Indicated by the "Units"
I
column except where an alternate unit Is presented to the night of the result.
"
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2015 11:52 AM
without the written consent
of Pace Analytical
Services, Inc,.
Page 11 of 27

+Cv
I 'y
4�
4'
i

aceAnalytical
wewpecela6a.com '
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATBR
Pace Project No.: 92252847
LABORATORY CONTROL SAMPLE:
1480085
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
52.3
105
52-162
1,1,2,2-Tetrachloroethane
ug/L
50
54.2
108
46-157
1,1,2-Trichloroethane
uglL
50
54.5
109
52-150
1,1-Dichloroethane
ug/L
50
51.4
103
59-155
1,1-Dichloroethene
ug/L
50
50.5
101
1-234
1,2-Dichlorobenzene
ug/L
50
56.3
113
18-190
1,2-Dichloroethane
ug/L
50
52.0
104
49-155
1,2-Dichloropropane
ug/L
50
53.8
108
1-210
1,3-Dichlorobenzene
ug/L
50
56.1
112
59-156
1,4-Dichlorobenzene
ug/L
50
52.6
105
18-190
2-Chloroethylvinyl ether
ug/L
100
101
101
1-305
Acrolem
ug/L
250
102
41
15-152
Acrylonitrile
ug/L
250
264
106
75-132
Benzene
ug/L
50
55.6
111
37-151
Bromodichloromethane
ug/L
50
51.3
103
35-155
Bromoform
ug/L
50
56.2
112
45-169
Bromomethane
ug/L
50
43.9
88
1-242
Carbon tetrachloride
ug/L
50
57.5
115
70-140
Chlorobenzene
ug/L
50
54.1
108
3Z-160
Chloroethane
ug/L
50
37.3
75
14-230'
Chloroform
ug/L
50
50.9
102
51-138
Chloromethane
ug/L
50
46.0
92
1-273
cis-1,2-Dichloroethene
ug/L
50
54.9
110
68-146
cis-1,3-Dichloropropene
ug/L
50
54.7
109
1-227
Dibromochloromethane
ug/L
50
52.2
104
53-149
Ethylbenzene
ug/L
50
52.1
104
37-162
Methylene Chloride
ug/L
50
57.0
114
1-221
Telrachloroethane
ug/L
50
54.6
109
64-148
Toluene
ug/L
50
52.2
104
47-150
trans-1,2-Dichloroethene
ug/L
50
52.8
106
54-156
trans-1,3-Dichloropropene
ug/L
'50
- 55.1
110
17-183
Trichloroethane
ug/L
:50
52.8
• 106
71-157
Trichlorofluoromethane
ug/L
50 ,,,
.41.7
83
17,-181
Vinyl chloride
ug/L
'50 .";
48.3
97
1-251
1,2-Dichloroethane-d4 (S)
%
'
_
98
70-130 „
4-Bromofluorobenzene (S)
%
100
70-130'"
Toluene-d8 (S)
%
t,
a
99
70-130
E
MATRIX SPIKE SAMPLE: 1480088
92252724003 Spike MS MS %Rec
Parameter Units Result Conc. Result e/ Rec Limits Qualifiers
1,1,1-Trichloroethane.
ug/L
ND 20 20.0
100
46-171
11,2,2-Tetrachloroetlane
ug/L
ND 20 23.6
118
73-159
1,1,2-Trichloroethane'
u /L
ND 20 19.8
99
64-152
1,1-Dichloroethane
u�i-
NO 20 24.6
123
43-172
Results pmented on this page are In the
units Indicated by the "units" column except where an alternate unit Is
presented to the right
of the mutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2015 11:52 AM
.'
without the written consent of Pace Analytical Services, Inc..
'
Page 12 of 27
. •,I

(�5?ceAnalyficalo
wwwpealeAecom
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92252847
e
Pace Analytical Services, Inc
n
9800 Kincey Ave. -Suite 100
Hunhumville. NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1480088
Units
92252724003
Result
Spike
Conc.
MS
Result
MS •.
%Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
NO
•, 20
25.5
128
48-189
1,2-Dichlorobenzene
ug/L
NO
20
19.4
97
54-154
1,2-Dichloroethane
ug/L
NO
20
23.7
118
42-171
1,2-Dichloropropane
ug/L
ND
20
23.9
119
55-157
1,3-Dichlorobenzene
ug/L
NO
20
19.9
99
57-148 1
1,4-Dichlorobenzene
ug/L
NO
20
21.4
107
58-149
2-Chloroethylvinyl ether
ug/L
NO
40
NO
0
70-130 MI
Acrolein
ug/L
NO
100
101
101
70-130
Acrylonitnle
ug/L
NO
too
125
125
70-130
Benzene
ug/L
NO
20
25.1
126
54-163
Bromodichloromelhane
ug/L
NO
20
19.7
99
56-152
Bromoform
ug/L
NO
20
17.4
87
53-151
Bromomethane
ug/L
NO
20
19.4
97
10-200
Carbon tetrachloride
ug/L
NO
20
20.7
103
41-175
Chlorobenzene
ug/L
NO
20
23.2
116
67-152
Chloroethane
ug/L
NO
20
32.7
163
23-200
Chloroform
ug/L
NO
20
20.0
100
51-166
Chloromethane
ug/L
NO
20
23.2
116
40-175
cis-1,2-Dichloroethene
ug/L
NO
20
24.3
122
45-174
cis-1,3-Dichloropropene
ug/L
NO
20
21.5
107
38-146
Dibromochloromethane
ug/L
NO
., 20
16.1
81
65-144
Ethylbenzene
ug/L
NO
20 -
24.6
123
57-152
Methylene Chloride
ug/L
ND
20
'27.0
135
40-167
Tetrachloroelhene
ug/L
NO
20
119.3
96
59-155
Toluene
ug/L
NO
20
23.4
117
47-162 •'
trans-1,2-Dichloroethene
ug/L
NO
20
23.7
118
47-178
trans-1,3-Dichloropropene
ug/L
NO
20
22.1
111
39-148
Trichloroethene
ug/L
NO
20
20.6
103
60-153
Trichlorofluoromethane
ug/L
NO
20
27.2
136
42-199
Vinyl chloride
ug/L
NO
20
26.3
131
46-176
1,2-Dichloroethane-d4 (S)
%
'''
121
70-130
4-BromoFluorobenzene (S)
%
95
�70-130
Toluene-d8 (S)
%
'ja
104
i 0-130
SAMPLE DUPLICATE: 1480087
Parameter
Units
92252724002 bup
Result Result RPb
Max-"
°RPO
Olallfiers
1i:
1,1,1-Trichloroethane
ug/L
NO NO
l 30
it
1,1,2,2-Tetrachloroethane
ug/L
NO NO
30!'.
<.
1,1,2-Trichloroethane
ug/L
NO NO
30
�h
1,1-Dichloroethane
ug/L
NO NO
30
1,1-Dichloroethene
ug/L
NO NO
30
(a
1,2-Dichlorobenzene
ug/L
NO NO �
• 30
1,2-Dichloroethane
ug/L
NO NO
30
' t•`
1,2-Dichloropropane
ug/L
NO NO
30
II
i Results presented on this page are In the
units Indicated by the "Units" column except where an ahemate unit
is presented to the right of the result.
j
REPORT OF LABORATORY ANALYSIS
'r
This report shall not be reproduced, except in full,
;
Date: 06/17/201511:52 AM
without theiwritten consent of Pace Analytical Services, Inc..
,P. f
li
Ill•li
Page 13 of 27

A
I
I
9

I
laceAnalyficalo
wwxpecala0.ccan
i Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100 ..
Huntersville, NC 26078
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92252847
�•
SAMPLE DUPLICATE: 1480087
92252724002 Dup Max
Parameter
Units
Result Result RPD RPD
Qualifiers
1,3-Dichlorobenzene
ug/L
ND ND
30
1,4-Dichlorobenzene
ug/L
ND ND -
30
2-Chloroethylvinyl ether
ug/L
NO -ND
30
Acrolein
ug/L
NO NO
30
Acrylonilrile
ug/L
ND NO ' ,
30
Benzene
ug/L
NO ND
30 '
Bromodichloromethane
ug/L
ND NO
30
Bromoform
ug/L
NO NO
30
,.
6Tomomethane
ug/L
NO NO
30
Carbon tetrachloride
ug/L
I ND r ND -
30
Chlorobenzene
ug/L
;ND NO
30
Chloroethane
ug/L
NO NO
30
Chloroform
ug/L
NO NO
30
rJ,
Chloromethane
ug/L
ND ND
30
cis-1,2-Dichlorcethene
ug/L
NO ND
30
cis-1,3-Dichloropropene
ug/L
NO NO
30
. Dibromochloromethane
ug/L
NO NO
30
0
Ethylbenzene
ug/L
ND NO
30
i" •"
Methylene Chloride
ug/L
ND ND
30
':Tetrachloroethene
ug/L
NO NO
30
Toluene
ug/L
NO NO ., a
30i'
trans-1,2-Dichloroethene
ug/L
NO NO
30
trans-1,3-Dichloropropene
ug/L
ND ND
30
t
Trichloroethene
ug/L
NO ND
30
,'lt;
Trichlorofluoromethane
ug/L
a. NO NO
30
it. .I
Vinyl chloride
ug/L
NO NO
30
r
1,2-Dichloroethane-d4 (S)
%
123 122 1
4-Bromofluorobenzene (S)
%
'91 t 91
Toluene -dB (S)
%
106 106 1
+
y n
•
+' Results presented on this page are In the units indicated by the "Unite" column except where an ahemate unit Is presented to the right of the resWl.
p
,
,Y
•
REPORT OF LABORATORY ANALYSIS
f
'
This report shall not be reproduced, except in full, 1
Date: 06117/2015 11:52 AM
without the written consent of PaceAnalytical Services, Inc..
Page 14 of 27
,`j I'

I�
lace Analytical
wwwpecMaW.cdm
Y•.
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
,
Pace Project No.: 92252847
QC Batch: OEXT/35597
Analysis Method: EPA 608
OC Batch Method: EPA 3510
Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92252847001.';;,
i tr�
METHODBLANK: 1478498
Matrix: Water -
Associated Lab Samples: 92252847001
,:,`,,.
• �':. ,
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
",'
4,4'-DDD
ug/L
ND 0.050
06108/1513:47
(1F
4,4'-DOE
ug/L
•'
NO .0.050
06108/1513:47
4,4'-DDT
ug/L
NO 0.050
06/08/15 13:47
Aldrin
ug/L
F: ND 0.050.
06/08/15 13:47
alpha-BHC
ug/L
ND 0.050
06/08/15 13:47
beta-BHC
uglL
ND 0.050
06/08/15 13:47
Chlordane (Technical)
ug/L
ND 0.50
06/08/1513:47
delta-BHC
uglL
ND n 0,050
06/08115 13:47
Dieldrin
ug/L
ND 0.050
06/08/15 13:47
Endosulfan I
ug/L
ND 0.050
•
06/08/15 13:47
�
Entlosulfan ll
ug/L
ND 0,050
06/08/15 13:47.
Entlosulfan sulfate
uglL
ND r, 0.050
06108/1513:47
�'•;' •-
Endrin
ug/L
ND 0,050
06/08/15 13:47
Endrin aldehyde
ug/L
-ND , 0.050
06/08115 13:47
•`.' `�
gamma-BHC (Lindane)
ug/L
'ND,. 0,050
06108/1513:47
Heptachlor
uglL
ND 0.050
06/08/15 13:47
Heptachlor epoxide
ug/L
ND 0.050
06/08/15 13:47
PCB-1016 (AfOC10F 1016)
ug/L
ND 0.50
06/08/15 13:47
PCB-1221 (Aroclor 1221)
ug/L
ND 0.50
06/08115 13:47
r:(a
PCB-1232 (Aroclor 1232)
ug/L
NO 0.50
06/08/15 13:47
PCB-1242 (Aroclor 1242)
ug/L
ND 0.50
06/08/15 13:47
'(,'
PCB-1248 (Aroclor 1248)
ug/L
ND 0!50
06/08115 13:47
'I If
PCB-1254(Aroclor 1254)
ug/L
ND, 0.50
06/08/15 13:47
PCB-1 260 (Aroclor 1260)
ug/L
ND 0.50
06/08/15 13:47
',x.. ii •,r
Toxaphene
ug/L
ND 0.50
06/08/15 13:47
Decachlorobiphenyl(S)
%
70 20-138
06/08115 13:47
Tetrachloro-m-xylene (S)
%
84 20-110
06/08/15 13:47
(` ,
n.
LABORATORY CONTROL SAMPLE: 1478499
Spike LCS
-CS %Rec
••I•
Parameter
Units
Conic. Result
%Rec Limits Qualifiers'
_ !'
4,4'-DDD
ug/L
.25 0.21
86
31-141
.;''I•�
4,4'-DDE
ug/L
.25 0.20
80
30-145
1
4,4'-DDT
ug/L
.25 0.21
86
25-160
'• t
Aldrin
ug/L
.2� 0.17
67
42-122
�!
alpha-BHC
ug/L
.25 0.22
89
37-134
,
beta-BHC
ug/L
.25 0.22
90
17-147
delta-BHC
ug/L
.25 0.24
95
19-140
,
Dieldrin
ug/L
.25 0.22
89
36-146
,
Endosulfan I
ug/L
.25 0.22
88
45-153
-
i
Results presented on this page
are In the
units Indicated by the "Units" column except where
an attemate unit is presented to the fight of the
mutt.'.
1,
REPORT OF LABORATORY ANALYSIS
Z(h
This report shall not be reproduced, except in full,
Date: 06/17/2016'11:52 AM
without the written consent of Pace Analytical Services, Inc..
Page 15 of 27
i. 11
i

®
Analytical
owwpecalabs.con,
Project: STORMWATER
Pace Project No.: 92252847
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
I 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
�r
•r-
LABORATORY CONTROL SAMPLE:
1478499
Spike LCS� 1-CS
%Rec
Parameter
Units
Conic. Result %Rec
Limits
Qualifiers
-
Endosulfan II
ug/L
.25 0.23 91
1-202
Endosulfan sulfate
ug/L
.25 1, 0.23 91
26-144
Endrin
ug/L
.25 0.23 95
30-147
Endrin aldehyde't
ug/L
.25 0.19 76
50-150
gamma-BHC (Llnifane)
ug/L
.25 0.22 89
32-127
Heptachlor 'R't
ug/L
.25 0.18 74
34-111
Heptachlor epoxide
ug/L
.25 '0.21 87
41-126
Decachlorobiplienyl(S)
%
84
20-138
-
Tetrachloro-m-aylene (S)
%
95
20-110
1,
I
r
-I
IP
:
I
I
i
j
14
i
Results presented on this
page are In the units Indicated by the "Unite" column except wTere an ehemate unit
is Presented to the right or IM1e result.
- '
e
,
REPORT OF LABORATORY ANALYSIS
L t'
1'
This report shall not be reproduced, except in full,
Date: 06117/2015,11:52 AM
without the written consent of Pace Analytical Services, Inc..
Page 16 of 27. f -
n

0
I

1�5ace*'alytical
wwwpacelabscom
QUALITY CONTROL DATA
i
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone] -
Project:
STORMWATER
Pace Project No.:
92252847
QC Batch:
OEXT/35626 . Analysis Method: EPA 625
QC Batch Method:
EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92252847001
METHOD BLANK: 1479591 Matrix: Water
Associated Lab Samples: 92252847001
Parameter
1,2,4-Trichlorobenzene
1,2-Diphenylhydrazine
2,4,6-Tnchlorophenol
2,4-Dichlorophenel
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dihitrololuene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,3'-Dich forobe nzidi ne
4,6-Dinitro-2-methyl phenol
4-13romophenylphenyl ether
4-C h to ro,3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphtnylene
Anthrac66e
Benzidine
Benzo(a)anthracene
Benzo(ajpyrene
Benzo(b)fluoranthene
Benzo(g;hJ)perylene
Benzo(k)fluoranlhene
bis(2-Chloroethoxy) methane
bis(2-Chlor9elhyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
B utyl benzylphtha late
Chrysene '
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Diethyl phtha late
Dimelhylphthalate
Fluoran(hene'
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Results presented on this page are In the units Indicated by the "Unlis" column except where an ahemate unit Is presented to the right of the result.
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
ND �
10.0
06/10/15 08:03 1
ug/L
ND,
5.0
06/10/15 08:03
1
ug/L
NO,
10.0
06/10/15 08:03
ug/L
ND;
50.0
06110/1508:03
ug/L
ND,
5.0
06/10115 08:03
ug/L
NO
5.0 .
06/10/15 08:03 '
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
25.0
06/10/15 08:03
ug/L
NO
20.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03 E
ug/L
ND',
50.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03 1
ug/L
ND'
5.0
06/10115 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
ND
50.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/1508:03
ug/L
;ND
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03 i
ug/L
ND
10.0
06/10115 08:03
ug/L
ND
5.0
06/10/15 08:03
ug/L
ND '•;
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
ND
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
ND
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
NO
5.0
06/10/15 08:03
ug/L
ND
5.0
06/10/15 08:03
E
:.t
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/17/2015 11:52 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of-27

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OeAnalytical"
mvwpeale0.v.mn
"Pace Analytical Services, Inc.
'r
'` • 9800 Kincey Ave. Suite 100
I'
Huntersville, NC 28078
I. [phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92252847
_
METHOD BLANK: 1479591
Matrix: Water
Associated Lab Samples: 92252947001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
'
Hexachlorocyclopentadiene
uglL
ND 10.0
06/10/15 08:03
Hexachloroethane
ug/L
ND 5.0
06/1011508:03
Indeno(1,2,3-cd)pyrene
ug/L
NO 5.0
06/10/15 08:03
.
Isophorone
ug1L
ND 10.0
06/10/15 08:03
N-Nitroso-di-n-propylamine
ug/L
ND 5.0
06/10/15 08:03
_
N-Nitrosodimethylamine
ug/L
NO 5.0
06/10/15 08:03
1
N-Nitrosodiphenylamine
ug/L
ND 10.0
06/10/15 08:03
Naphthalene
ug/L
ND 5.0
06/10/15 08:03
Nitrobenzene
ug/L
NO 5.0
06/10/15 08:03
Pentachlorophenol
ug/L
NO 10.0
06/10/15 08:03
Phenanthrene
ug/L
NO 5.0
06110/1508:03
Phenol
uglL
ND 5.0
06/10/15 08:03
Pyrene
ug/L
ND 5.0
06/10/15 08:03
2,4,6-Tribromophenol(S)
%
95 10-137
06/10/15 08:03
2-Fluorobiphenyl (S)
%
78 15-120
06/10/15 08:03
2-Fluomphenol (S)
%
42 10-120
06/10/15 08:03
Nitrobenzene-d5 (S)
%
95 10-120
06/10/15 08:03
`
Phenol-d6 (S)
e/
28 10-120
06/10/15 08:03
Terphenyl-dl4(S)
%
109 11-131
06/10/15 08:03
i'
LABORATORY CONTROL SAMPLE:
1479592
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
%Rec Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
33.2
66
44-142'
1,2-Diphenylhydrazine
ug/L
50
46.4
93
25-150,
2,4,6-Trichlorophenol
ug/L
50
43.3
87
37-144.
2,4-Dichlorophenol
ug/L
50
39.3
79
1-191
2,4-Dimethylphenol
ug/L
50
36.2
72
�32-1191
,•
2,4-Dinitrophenol
ug/L
250
,' 244
98
1-181
,
2,4-Dinitrotoluene
ug/L
50
45.6
91
39-139
IN ,
2,6-Dinitrotoluene
ug/L
50
45.7
91
50-1581,.
2-Chloronaphlhalene
ug/L
50
•38.4
77
60-118','
j '
2-Chlorophenol
ug/L
SO
37.7
75
23-134
2-Nitrophenol
ug/L
50
41.0
82
29-182-.•,
3,3'-Dichlorobenzidine
ug/L,
100
89.9
- 90
1-262
4,6-Dinitro-2-methylphenol
ug/L(c
100
99.8
100
1-181
,'ll
4-Bromophenylphenyl ether
ug/L `if•,
50
46.7
93
.53-127
4-Chloro-3-methylphenol
ug/L ','j.
100
79.5
79
22-147
4-Chlorophenylphenyl ether
uglL'y
50
43.8
88
25-158
4-Nitrophenol
ug/C•�I;,'
250
84.2
34
1-132�
Acena hthene
u /L';%,'.
50
39.6
79
47-145.
i••'
Acenaphthylene
uglll', j,•.
50
41.4
83
33-145
Anthracene
ug/L;'iii
50
46.8
94
1-166
Benzidine
ug/L`�;'S!',_
100
30.7J
31
25-150
Results presented on iM1ls page am In ttie bolts
lntllcetetl by the
"Unita"column except xTere an alternate unit is
preuntetl to the right of the
revutt. ;,v
REPORT OF
`�
LABORATORY ANALYSISot
. ) •I
q
This report shall not be reproduced, except in full,
,k.
Date: 06/17/2015 11:52 AM
without the written consent of Pace Analytical Services, Inc..
", Page 18 01r27

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' Pace Analytical Services, Inc. .
a�/�QQ /I /� /� ®,�
QIie Analytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wew.pecelahs.00m
,
(704)8759042
QUALITY CONTROL DATA
2• '
Project: STORMWATER
Pace Project No.: 92252847
LABORATORY CONTROL SAMPLE:
1479592
Spike
LCS
LCS
,%Rec
Parameter
Units
Cone.
•Result %Rec
.Limits Qualifiers
Benzo(a)anthracene
ug/L
50
50.4
101
33-143
Benzo(a)pyrene
ug/L
50
53.9
108
17-163 „
Benzo(b)fluoranthene
ug/L
50
51.9
104
24-159 ,.
Benzo(g,h,i)perylene
ug/L
50
53.8
108
1-219
Benzo(k)fluoranthene
ug/L
- 50
52.6
105
11-162 ,
bis(2-Chloroethoxy)methane
ug/L
50
41.8
84
33-184
bis(2-Chloroethyl) ether
ug/L
50
43.9
88
12-158 '
bis(2-Chloroisopropyl) ether
ug/L
50
46.9
94
36-166 '
bis(2-Ethylhexyl)phthalate
ug/L
50
52.7
105
8-158
Butylbenzylphthalate
ug/L
50
51.9
104
1-152
Chrysene
ug/L
50
52.2
104
17-168.
Di-n-butylphthalate
ug/L
50
47.5
95
1-118
Di-n-octylphthalate
ug/L
50
53.6
107
4-146 '
Dibenz(a,h)anthracene
ug/L
50
54.0
108
1-227 ,
Diethylphthalate
ug/L
50
43.6
87
1-114
Dimethylphihalate
ug/L
50
41.7
83
1-112
Fluoranthene
ug/L
50
45.8
92
26-137
Fluorene
ug/L
50
43.4
87
59-121
Hexachloro-1,3-butadiene
ug/L
50
31.2
62
24-116
Hexachlorobenzene
ug/L
' 50,
46.9
94
1-152
Hexachlorocyclopentadiene
ug/L
50
4` 31.0
62
25-150
Hexachloroethane
ug/L
50
�• 32.1
64
40-113
Indeno(1,2,3-cd)pyrene,
ug/L
50
53.8
108
1-171
Isophorone
ug/L
50
39.7
79
21-196
N-Nitroso-di-n-propylamine
ug/L
50
46.4
93
1-230
N-Nitrosodimethylamine
ug/L
50
24.9
50
25-150
N-Nitrosodiphenylamine
ug/L
50
45.9
92
25-150
Naphthalene
ug/L
50
35.4
71
21-133
Nitrobenzene
ug/L
50
36.1
72
35-180
Pentachlorophenol
ug/L
100
98.1
_ 98
14-176 -.
Phenanthrene
ug/L
50
43.9
88
54-120
Phenol
ug/L
50
, - 20.0
40
5-112
Pyrene
ug/L
50
�+ 49.2
98
52-115
2,4,6-Tribromophenol(S)
°k
n
100
10-137
2-Fluorobiphenyl(S)
-%
74
15-120
2-Fluorophenol(S)
%+'
45
10-120
Nitrobenzene-d5(S)
%
1=
75
10-120'
Phenol-d6 (S)
%
33
10-120 +
Terphenyl-d14 (S)
%
107
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1479593
1479594
•MIS
MSD
- +
92252724002�' Spike
Spike MS
MSD
MS MSD %Rec Max
Parameter
Units Result Cone,
Cone. (Result'
Result
%Rec %Rec Limits RPD RPD Dual
1,2,4-Trichlorobenzene
ug/L
ND'� 100
100 80.7
86.5
81 87 44-142 7 30
Results Presented on
this page am in the
units indicated by the
"Units" column except where an altemate
unit is presented to the right of the result.
REPORT,OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
Date: 06/17/2015 11:52 AM
without the written consent of Pace Analytical Services, Inc_
,I
Page 19 of 27
,

ace Analytical
® www.pecelabs.cdm
Project: STORMWATER
Pace Project No., 92252847
P
QUALITY CONTROL DATA
Pace Analytical SeMces, Inc.
9800 Kincey Ave. S1�1�e, 10o
Huntersville, NCI 8078
(704)ft�9092
m
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1479593
1479594
^.. ).p,.
- .
r.'
MS
MSD
92252724002
Spike
Spike �
MS
MSD
MS
MSD
%Rec
Maxi '. Max. ,{
,,,
Parameter
Units
Result
Conc.
conc. ,
Result
Result °A Rec
%Rec
Limits
RPD RPR;:;;Qual
.I
1,2-Diphenylhhrazine
uglL
NO
100
100
100
99.2
100
1 99
25-150
1
2,4,6-Trichlorophenol
ug/L
ND
100
100
98.2
88.3
98
•. 88
37-144
11
30 ./,V �
!
2,4-Dichlorophenol
ug/L
NO
100
•100
88.2
89.7
88
90
1-191
2
30 �.; +
',
2,4-Dimethylphenol�
ug/L
NO
100
100
84.4
85.8
84
86
32-119
2
30');'..'�tV;
'
2,4-Dinitrophenol
ug/L
NO
500
500
486
253
97
51
1-181
63
30 R.1
1
2,4-Dinitrotoluene ;'S'
uglL
NO
100
100
94.9
91.6
95
92
39-139
3
30,iy4
l
2,6-Dinitrotoluene .J'
ug/L
NO
100
100
94.4
93.8
94
94
50-158
1
30'i
I
2-Chloronaphthalen0'
ug/L
ND
100
'100
90.9
93.1
91
93
60-118
2
30''y'.'
��•�
2-Chlorophenol ,r'"',
ug/L
NO
100
100
89.2
89.7
89
90
23-134
1
30)il:i,'
2-Nitrophencl
ug/L
NO
100
100
93.5
94.8
93
95
29-182
i
30, �.l;i� ••
3,3'-Dich1orobenzldm4I'
ug/L
NO
200
200
162
173
81
86
11-262
6
30
4,6-Dinitro-2-methylphf
ug/L
NO
! 200
200
208
146
104
73
11-181
35
30
4-13romophenylphenyj.gther
ug/L
NO
100
100
99.3
99.2
99
99
53-127
0
30`h''!
,
4-Chloro-3-methyll;hpr;Dl
ug/L
NO
200
200
175
171
88
85
22-147
3
.30 •,
4-ChlorophenylphenyV ether
ug/L
NO
100
100
93.9
92.8
94
93
25-158
1
30+: !, <
4-Nitrophenol"1!ri{i
ug/L
ND
500
500
241
206
48
41
1-132
16
301 `(.'��
,
Acenaphthene �.I'
ug/L
NO
100
100
88.5
88.8
89
89
47-145
0
3011
Acenaphthylene .',f�-`I'r.
ug/L
NO
100
100
94.0
92.7
94
93
33-145
1
30b','.i
Anthracene - ,°"
ug/L
NO
100
100
98.5
97.0
99
97
1-166
2
30':.';r
Benzidine , •"-�:;
ug/L
NO
200
200
38.4J
82.3J
19
41
25-150
30'Mi.
Benzo(a)anthracene}�
ug/L
ND
100
100
103
103
103
103
33-143
0
' 3017 {'
Benzo(a)pyrene 'I
ug/L
NO
100
100
110
110
110
110
17-163
0.
30"",..
Benzo(b)fluoranthene,';.
ug/L
NO
tis 100
100
111
109
111
109
24-159
2
30%1
Benzo(g,hJ)perylene,,:;j
ug/L
NO
100
100
118
115
118
115
1-219
2
Benzo(k)fluoranthehe{II,
uglL
NO
100
100
106
107
106
107
, 11-162
0
30'o. f•
bis(2-Chloroethoxy)me(hane
ug/L
NO
100
100
91.91
92.9
92
93
33-184
1
30
bis(2-Chloroethyl),eJhen
ug/L
ND
100
100
97.4
98.6
97
99
12-158
1
30
bis(2-Chloroisopropyl)�,ether
ug/L
NO
100
100
103
102
103
102
36-166
'1
30f
bis(2-Ethy1hexy1)phthatate..
ug/L
NO
- 100
100
- 110
106
110
106
8-158
4
30 `
Butylbenzylphthalate J'
ug/L
NO
100
100
109
107
109
107
1-152
2
30 ,
Chrysene ' t.'
ug/L
NO
100
100
107
107
107
107
17-168
0
30
,.
Di-n-butylphthalate `.. ,rl
ug/L
ND
100
100
101
97.6
101
98
1-118
3
30..
Di-n-octylphthalate �)
ug/L
ND
100
100
114
109
114
109
4-146
430
Dibenz(a,h)anthracenrr.ef
ug/L
ND
100
100
117
115
117
115
,1-227
2
30 j
i
Diethylphlhalate ' �) �'•, �
ug/L
ND
100
100
91.4
88.6
91
89
1-114
3
30
Dimethylphthslate r r
ug/L
NO
100
100
88.7
86.6
89
87
.1-112
2
30
Fluoranthenei
uglL
NO
100
100
95.1
93.7
95
94
26-137
2
30 p '
Fluorene �..6' -
ug/L
AND
'100
100
93.2
91.9
° 93
92
59-121
1
36 1•
'
Hexachloro-1,3-butadiene
ug/L
NO
•100
100
80.0
86.9
80
87
24-116
8
30 ,..
.
Hexachlorobenzene' r.
ug/L
ND
100
100
99.8
100
100
100
1-152
0
30
Hexachlorocyclopentsiliene,
ug/L
ND
100
100
83.8
89.4
84
89
25-150
7
30
Hexachloroethane
ug/L
ND
100
100
79.8
84.7
80'
85
.40-113
6
.30
•„
Indeno(1,2,3-cd)pyrene
uglL
NO
100
100
114
111
114
111
1-171
3
30
Isophorone - ,�.1'-
ug/L
NO
100
100
85.4
85.6
85
86
21-196
0
30 i
N-Nitroso-di-n-propylamine
ug/L
NO
100
100:
98.9
93.0
99
93
1-230
6
!36:
N-Nitrosodimethylamine
ug/L
NO
100
100
76.8
80.8
77
81
25-150
5.
30".
.
Results, presented on this page are In the units indicated
by the "Unite" ionnan except where an alternate unit Is presentee to the fight of the result.
REPORT OF
LABORATORY ANALYSIS
This
report shall not be reproduced, except in full,
Date: 06117/2015 11:52 AM
without
the written consent of Pace Analytical
Services, Inc..
Page'20 of 27

o9800Kincey
�111a�
IG'�C�I
owwpecelahs.Wm
r
Project: STdRMWATER
Pace Project No.: 922!52847
u
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
Ave. Su ile100I"II
Huntersville, NC 28078
[phone], •�"
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1479593-1479594
,.
�V
r?
MS MSD
.
-
92252724002 Spike Spike = ' MS MSD
MS
MSD
% Rec
Max
Parameter
Units
Result Cone. ' Cone. Result Result %Rec
%Rec
Limits RPD
RPD Qual
N-Nitrosodiphenylamir1 r;,
ug/L
IND 100 ''100 97.7 97.8
98
98
25-150 0
30
Naphthalene j'":
ug/L
IND 100 100 83.2 87.2
-83
87
21-133 5
30
Nitrobenzene*.
ug/L
ND 100 100 82.1 84.9
82
85
35-180 3
30
Pentachlorophenol . ' ..
ug/L
ND 200 200, E 191 128
-95
64
14-176 40
. 30 R1
Phenanthrene "! +'
ug/L
ND 100 109: 93.3 92.1
93
92
54-120 1
30
Phenol I, .?•: ;,I�
ug/L
ND 100 100' 57.4 61.5
57
62
5-112 7
30
Pyrene ;;::�j �•.,
ug/L
ND 100 100 101 101
101
101
52-115 0
30
2,4,6-Tribromophen6l,($)';.
%
103
94
10-137
2-Fluorobiphenyl (S) •;%!� •
°/
83
86
15-120
2-Fluorophenol(S) `.'Sl.?;
%
60
64
10-120
t: ,,
Nitrobenzene-d5 (S) � �;,'l-
°h
81,
84
10-120
Phenol-d6 (S)r; rj(
%
47:
51
10-120
Terphenyl-d14 (S) '�a�c, `
%
107
106
11-131
It
I 1,
It
I I
`p Results'presentod on this page are
in the units Indicated by the "Waits" column except where an ahemate unit
Is presented to the right of the resun.
ti .I
, I.l
r.
i:..
REPORT OF LABORATORY ANALYSIS
;
This report shall,not be reproduced, except in full,
Dale: 06/17/2015 �11:52 AM
a,
without the written consent of Pace Analytical services, Inc..
•
Page 21 of 27

/55'ceAnalyfical"
w ..pacelabs.cwn
Project: STORMWATER
Pace Project No.: 92252847
' I
QUALITY CONTROL DATA
QC Batch: RWET/8383 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspend ed Solids -
Associated Lab Samples: 92252847001
METHOD BLANK: 1477579 Matrix: Water;!
Associated Lab Samples: 92252847001
Blank 'Reporting ,
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND' " 2.5 06/05/15 10:43
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1477580
-
. ' ,
Spike LCS' LCS ..
% Rec '
Parameter
Units
,. Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 i, �,:,, .272 109
90-110
SAMPLE DUPLICATE: 1477581
,
aw
92252755001 Cup -
Max
Parameter
Units
Result • Result RPD
RPD. Qualifiers
Total Suspende68olids
mg/L
353 342
3 5
SAMPLE DUPLICATE: 1477582
92252758001 Dup
Max
Parameter
Units
., Result Result RPD
RPD' Qualifiers
Total Suspended Solids
mg/L
180, <, I', 195
8 I. 5 D6
tI t
Ret:uhs presented on this page are In the
I
units Indicated by the "Units column except where an alternate unit
is presented to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06117/2015 11:6�;AM
l:
without the written consent of Pace Analytical Services, Inc..
I
I
Page'22 of 27

1�5?ceAnalytica'le
eww.pscelaba. con,
Project: STORMWATER
Pace Project No.: 92252847
QC Batch: RWET/8382
OC Batch Method: SM 4500-H+B
Associated Lab Samples: 92252847001
SAMPLE DUPLICATE: 1476920
Parameter Units
pH at 25 Degrees C Std. Units
Q=111
i
QUALITY CONTROL DATA
Analysis Method: SM 4500-H+B
Analysis Description: 4500H+B pH Raleigh
92252409002 Cup
Result Result RPD
6.8 6.9 0
R
Max
RPD
Pace Analytical Services, Inc.
9800 Ki may Ave. Suite 100
Huntersville, NC 28678
[phone]
Qualifiers
10 H6
i
��I r i
t
• I,
• I -
I I.
t I
ij •
Results presented on this page are in the units Indicated by the "Units" column except xhere an alternate unit Is presented to the right of the result.
)REPORT OF LABORATORY ANALYSIS
' This report shall not be reproduced, except in full, .I
Date: 06/17/2015 11:52 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 27
I

Pace Analytical Services, Inc.
aceAnalytical ® I 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
~..pacelebs.mm [phone]
QUALIFIERS
Project: STORMWATER
. Pace Project No.: 92252847
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. 4 '
ND - Not Detected at or above adjusted reporting limit. l� n
sand
J - Estimated concentration above the adjusted method detection limit below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit
PQL - Practical Quantitation Limit.
RL- Reporting Limit. '
S - Surrogate
1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration. I
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
i
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
'
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
y
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles.
TNI - The NELAC Institute.
1
LABORATORIES r,
i
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh ,
1'
ANALYTE QUALIFIERS.'
C9 Common Laboratory Contaminant.
'
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
•
P•
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
,
'
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.�y
'N
tijt �
REPORT OF LABORATORY ANALYSIS
t
?6 I
This report shall not be reproduced, except in full,�i;'
Dale: 06117/2015 11:52 AM without the written consent of Pace Analytical Services, Inc_
Qa 24 of 27
t

1�55?e Analytical
s escelabs.ccm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
STORMWATER
92252847
Lab ID
Sample ID
QC Batch Method
92252847001
OUTFALL 001
EPA 1664B
92252847001
OUTFALL 001
I
EPA3510
92252847001
OUTFALL 001
EPA200.7
92252847001
OUTFALL 001
EPA 625�
92252847001
OUTFALL 001
EPA624
92252847001
OUTFALL 001
SM 2540D
92252847001
OUTFALL 001
SM 4500-H+B
.'Date: 06/17/2015 11:52 AM
Pace Analytical Services, Inc. ,
9800 Kincey Ave. Suite 100 J
Huntersville, NC 28078
[phone],
Analytical ;
QC Batch
Analytical Method I
Batch
GCSV/21659
1,
OEXT/35597
EPA608
GCSV/21595
MPRP/18647
EPA 200.7
ICP/16721
0EXT/35626
EPA625
MSSV/10786
MSV/32059
RWET/8383
RWET/8382
s
I
i
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 25 of 27 ,l
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7
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.,, aceNrarical
°"`°'" `
Document Name: Sample'ConditlonUpon
Receipt SCUR
Document Revised: May 15, 2015
Page 1 of 2'
Document No.:
F•RAL-CS•OOPreviO3
Issuing Authorities:
Pace Raleigh Qualit Office
'Page 2 of Is for Internal Use Only
Client Name: 'SUM'S WA-(at\!� �'N\D C �w� VViQan
Courlor (Circle): Fed Ex UPS LISPS ' Client I Commerclal I Pace Other
Custody Seal on CoolerlBox Presonl:. 0 yes 0 - no Seals Intact: Oyes no
Packing Materl?i: l] Bubble Wrap l None Other
Circle Thermoi eter Used: IR Gun S 122086387T of lee• et,Blue None Samples on Ice. cooling process has begun
lRoua .fxenasnit
Temp Correctlon Factor: Addbtract 1 �k0
C
Date and Initials ofing
"Corrected Cogler Temp.:. ._C
BlologlcdLTIssue
is Frozen:, Yea No A
chock:to ! r se co ip
J
Temp should be dbove frwzing to WC
Comments:
Chain OfCustody PfBae111:
Yn'ONO'
MIA
1.
Chain of Custody Filled Out:
Y6 ONO
ONIA
2.
Chain of Custody Relinquished:
ea ONO
ONIA
3.
.i
Sam IerNameit'Sl natureomCOC:
YvesONO
OWA
4.
Samples Arrived W th!n Hold Time:
.Coves ON.
OWA
5.
Short Hold Time Analysis <72hr :
Oves No
OWA
6.
Rush Turn Around Timu Re uested:
OYea No
OWA
7.
1.
Sufficient Volume:
CW.. ONO
Oran
8.
Correct Containers Used:
Yea -ONO
OWA
9.
' f=Pace Containers Used:
Yn ONo
ONIA
'
Containers Intact::
Yes .ONO
13WA
10.
Filtered volume received for Dissolved tests
0ye$ ONO
Wa
11.
Sample Labels match CDC:
Ye ONo
❑Nln
12.
i-Include9detehime/10/Anal sla Matrix:
All containers needing preservetlm have Won checked.
�.
,_,/
?ONo
ONIA
13.
'
All containers needing proservoaon are round to to in
``—/
liYea' ONo
!'
OWA
compliance vdih EPA recommendation.
(((
1
_
exceptions: VOA, OolifOirn TOC, OaG, W}DRO (w 1.)
VYoe ONO
Samples checked for dechlodnalion:.
es ONo
LXA
14.
i
1
Heads ace in VOA Vials >6mm'
Dye, ONO
NIA
15.
Trip Blank Present: :
OYee ONo
NIA
16.
Trip Blank Custody Seals Present
Yea ONO
W/WA
Pace ' Trip Blank Lot N (L`� urchosed;:
Cllenl NotiBcationl ResoluNsin
Person Contacted. ju• Date/flmet
Comments/ Resolutlei:: '
-- „
S66RF,ISRFLData:
Review:: h'
Note: Whenever i1vOre Is a dlccropaecy effacing North Carollm comp!tenee
zam0los, a copy of thin form will be .'ent to the North Carolina DEHNR
C r0caeon O'lce (I.; out of hold, :nwrrect preservative, out of temp,
nctco italmrs )
�r l
r i
I
Field Data Required? Y I N
WO#:92252847
.i II�II1�II ��II III II �II
92252847
r
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1
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(19
Page 26 of 27
1

a
6
3

-
Chain of Custody
Report Results to: Bill Resulfs•to:' Erstandard ReportDelivery
SIMS Metals/One Environment $10-ph, $15-TSS, $50-oil & grease - Q RushReport Delivery(w/ surcharge)
a 10_ n itvU; f31 v
$30-Copper, Lead, Zinc _ Requested Due Date: ..
New Bern, NC - $4o0-TTO (624-625-608)
/�%r Ko�irrl>I Project Reference:. Stormwater
ATTN: Screw j/ �' riVr/mod ATTN: - - -- Purchase order
Phone: a �di 7i a -yO`I ( / /y 1%D�-95fI - Sampled By:. J' P e ye•G y r
Grp b . 19: 0C
Outfall bbl pH, TSS, SGT-HEM, 200.7-(Cu, Pb, Zn), TTO-(624, 625, 608)
by
by (signature)
For Lab Use Only
Temperature at receipt:
Temp: O-� 6s-•::�.v -:::

A
wa
ri

/SIMS
METAL
MANAGEMENT
january27, 2015.
Division of Water Quality
Attn: DWQ Central Files RECEIVE®
North Carolina Department of Environment and Natural Resources
1617 Mail Service Center FEB 0 2 2015
Raleigh, North Carolina 27699-1617
CENTRAL FILES
DWR SECTION
RE: Semi -Annual Discharge Monitoring Report - Year 2 Period 2
General Permit NCG030000
Certificate of Coverage No. NCG030333
To NCDENR Division of Water Quality,
SMM Southeast LLC (d.b.a., Sims Metal Management - New Bern Facility) herein provides
the Year 2 Period 2 Semi -Annual Discharge Monitoring Report and Qualitative Monitoring
Report for the facility located at 2912 Neuse Boulevard in New Bern, North Carolina.
Its Sims understanding that although outfall 001 is technically sealed preventing a
concentrated discharge of stormwater runoff to the adjoining drainage ditch, the NCDENR
has requested a representative sample be collected from the overflow that intermittently
permeates though the riprap at the northwestern corner of the property. This request was
verbally communicated during a site inspection by the NCDENR (Mr. Vernon Riggs) and
subsequent Compliance Inspection Report dated August 29, 2014.
In response, Sims has collected a representative sample. The analytical data and
qualitative results are provided herein. Please note this sample was collected as water
permeated through the riprap allowing contact with the underlying sediment along the
drainage ditch. Additionally, in response to the NCDENR site inspection and Compliance
Inspection Report best management practice suggestions, Sims has placed hay bales along
the northern property boundary to impede surface water Flow and control sediment
runoff. Furthermore, the conceptual design of a stormwater pond(s) and associated
drainage ditch network has been completed for the property with construction execution
planned for February 2015.
A copy of the Semi -Annual Discharge Monitoring Report, Qualitative Monitoring Report and
Pace Analytical Laboratory Report are attached. Please contact Bobby Glenn or me at (252)
633-0892 should you have any questions or concerns.
Page l (�%2

�4
Sincerely,
Jeremy Tyree
Manager
Enclosures
Semi -Annual Stormwater Monitoring Report
Qualitative Monitoring Report
Pace Analytical Laboratory Report
Page 2 of 2

N
NCD-ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: bUI2;//portal.ncdenr.or2/"web/wq/ws/­su/updessw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: -5Mh Sovtkces+L L A/ rc! germ, Ke, c vc,l;rt�
County: L r eL if e- 0— Phone No.
Inspector: Sere ,,Vv Tvee- -e, C vis VJ
Date of Inspection: —La /d % //t%.
Time of Inspection: - � : (5 6, e in ,
Total Event Precipitation (inches): a a ✓7)/
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
U Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Pet'mittee or
7.
Page 1 of 2
SWU-242, Last modified 10/25/2012

I'
Outfall Description: n
{(� Outfall No. Dp [ Structure (pipe, ditch, etc.) P P 5 c- �e r
Receiving Stream: Un d- �y�_P;.l r1, l nl
Describe the industrial activities that occur within the outfall drainage area: S r La .� fl e4-ed Lck, Ilr J
2. Color: Describe the color of the discharge using basi colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: � rn & 4 M e-I" d d
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): Al Z 6
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 40 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 6) 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
M solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 V 4 5
7. Is there any foam in the stormwater discharge? Yes 1
8. Is there an oil sheen in the stormwater discharge? Yes �d
9. Is there evidence of erosion or deposition at the outfall? Yes (No/
10. Other Obvious Indicators of Stormwater Pollution: lam/
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

for North
Ina Mston ofWaiir atiility General Pe
Datesubmitted -,)715
—
3 3 p SAMPLE COL
SAMPLE PER
Al,.w6e.-6,
fyr�-e-
DISCHARGIP
ABORATORY Lab Cert. if QOther.
orrim en ts on ia nipl e colledi o n o r an a iysys:
I a . e - v a0l 6' Of �6 d Cc lec f FVB 0 � 2015 PLEASE RE MENWER TO SIGN ON PAGES 2 A.)C)YOR 3
V, K,, p p iAFilfrattoa 4s F' r w( u r v N r, 1 15 `5'�'CENTRAL FILES
.Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION disihor e, isp ici
eiiod?? "i bev
I
1 N110n,1wPolar,O&G/
Tc6LTox1c
WWINo
Date siipid
' "
24-hb�riainfall
-
Total Suspend
PH
Siaid r untsCPP
�F
Load
zinc
Total Pettoieum
Collected,Hydrocarbons
�6;0
0.007 njuv
OJ033 mak,
0.
Of I i a L—T-
�Ia
rho
.1
he 6nie outfill.
itl
rria6uficturetise the definition as fo
tube manufacture use the definition
Permit Date: 11/112012-10(31!2017
in
amar k hem
%iiverrof the rain gauge requirement.
etienchniark applies.
ire Se M:itohducifors, man ufactu re
Is that d'effnition.contained in the EPA
40rCf R 433.11: for sernictin r ductor
ii4&R469.226 � and for cathode ray
I
SWU-245, $a%t rcl�,Wd 101251201
P;t)!c 1 of 3

n,
FaCdities that incctwq!�W a solvent management plan into the St or mwater Pollution Preven lion Plan and the requirLment.for ng.monitorin'g
. - ,., __ - organic
_ listed in lh(- � 6 FI
66yhi�waived, the solvent managemeni:plan shall include a list 6f the total toxic or-ganic compounds used IntYl lie other elements ii-st Cc e -1
Permit:. For those fac1hiles electing to .2moloV the TTO monitoring waiver, the discharger shall sig-o The following certification statement:
'Based upon my itiouiry of tho person Gi persons ditccuir retpuniiiiN for rriahasiiig Ine Permit rrioniioriirip requ;rehemfor cotattcAic orgy nits
6el-.el no intoo-the icirmwater o - - area rhicn'are'.posed to nwnf ill or
storm%v.11r.r junolfhas actuired since filing the last itpom: iu'6er ce'r,ify. that. tW facility is ihipinmentingthe all the provisronr. 0.
--tl,ent enuynt plom included JA the.5%armwater oNution OreverrtrcuvPIan.-,
T e,
Ill a Ine (Print 'ria rise) 71�
f
Tit[6 (Pfiriftitle)
other similar,
time­11, 1 .., I ­.. .
rical,value (if the detection
Note If.ydii,pejo.dit ir sample voluit in,excen 6f, the benchmark, you Muit eiriplement,,rlei . jor2,ortir.3responses. See:Generol Permit text.
Put B:�, Vihicle.ftfl ritterva nce Area Monitoring Restults: dri ly for facili ties: wiieragi i 8 >, 551, alotnew'bil'permorith.
2A4_ Ri` "
o aikfia rgeirhis period?
Date sample
Collected
-'241hour rainfall -
3111110uhl,
Inches
Non-ool�r.O 1&5�
EPAAW (SITT--NEFA)
total suspended Solids
PH
AS riii/L
100 MBA or 50 ziidll.-
6.ti �q.osiv
01 1134i T
Fobtrioles frairn Piirt A alib,jpply to this Plaft R
See deneral Perrvritj(?At; Table 5. idLi-itifying the especially sensitive receiving water ctassirications where the room protective benchmark applies.
Permit Dart: till 12 012- t(J/31/2017 SWU-245. last revised 1012512012
Page 2 of 3

n,.
Note: if you report sornple value is caceas of the benchmark, you must implemeri! VerI, Fier2, or FieO responses. See Gen eml Permit text.
Permit Date: 111112012-1013117017
PART II S[C11 Y. D.
YES, C ti0 j,
SWU•7..45, 1,4�t revised IQ/ZS12012
Pagr.3 b1 3

(52ceAnalyticale
xww.paoeleDs.arn
January 27, 2015
Eli Holland
One Environmental Group, LLC
304 Glenwood Ave
Unit 9
Raleigh, NC 27603
RE: Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Dear Eli Holland:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
--zi---k---1
Kevin Godwin
[e-mail]
Project Manager
Enclosures
/pC
oar
2fttelVYPY/ \PO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Wwithout the written consent of Pace Analytical Services, Inc.. Page 1 of 27
BSI

IeAnalytical e
xww.pacalaas.mn
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Raleigh Certification IDS
6701 Conference Drive, Raleigh, INC 27607
North Carolina Wastewater Certifcation #: 67
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Dunking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Flonda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Flonda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 27

laceAnalytical'
...pace/abs can
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Lab ID Sample ID Matrix Date Collected Date Received
92233194001 Outfall 001 Water 01/12/15 07:45 01/1311510:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 27

IeAnalytical e
epncalaes.m
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9500 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SIMs Metals Stormwater
92233194
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92233194001
Outfall 001
EPA 16646
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA625
Bpi
60
PASI-C
EPA 624
GAW
37
PASI-C
SM 2540D
RC
1
PASI-R
SM 4500-H+B
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc.. Page 4 of 27

laceAnalyficale
~paroboscam
ANALYTICAL RESULTS
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall 001 Lab ID: 92233194001 Collected: 01/12/15 07:45 Received:. 01/13/15 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
01/16/15 09:47
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
ND ug/L
0.050
1
01/15/15 18:15
01/2111502:58
309-00-2
alpha-BHC
ND ug/1-
0.050
1
01/15/1518:15
01/2111502:58
319-84-6
beta-BHC
ND ug/L
0.050
1
01115/1518:15
01/21/1502:58
319-85-7
delta-BHC
ND ugIL
0.050
1
01/15/1518:15
01121/1502:58
319-86-8
gamma-BHC(Lindane)
ND ug/L
0,050
1
01115/1518:15
01121/1502:58
58-89-9
Chlordane( Technical)
ND ug/L
0.50
1
01/15/1518:15
01/2111502:58
57-74-9
4,4'-DDD
ND ug/L
0.050
1
01/15/1518:15
01/2111502:58
72-54-8
4,4'-DDE
ND ug/L
0.050
1
01/15/15 18:15
01121/1502:58
72-55-9
4,4'-DDT
ND ug/L
0.050
1
01115/1518:15
01/21/1502:58
50-29-3
Dieldrin
ND ug/L
0.050
1
01/1511518:15
01/21/1502:58
60-57-1
Endosulfan I
ND ug/L
0.050
1
01/15115 18:15
01/21/15 02:58
959-98-8
Endosulfan II
ND ug/L
0.050
1
01/15/15 18:15
01/21/15 02:58
33213-65-9
Endosulfan sulfate
ND ug/L
0,050
1
01/15/1518:15
0112111502:58
1031-07-8
Endrin
ND ugIL
0.050
1
01/15/1518:15
01/2111502:58
72-20-8
Endrin aldehyde
ND ugIL
0.050
1
01/15/1518:15
01/21/1502:58
7421-93-4
Heptachlor
ND ug/L
0.050
1
01/1511518:15
01/2111502:58
76-44-8
Heptachlor epoxide
ND ug/L
0.050
1
01/1511518:15
01121/1502:58
1024-57-3
PCB-1016 (Aroclor 1016)
ND ug/L
0.50
1
01115/15 18:15
01/21/15 02:58
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/L
0.50
1
01/1511518:15
01/21/1502:58
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/L
0.50
1
01/15/15 18:15
01/21/15 02:58
11141-16-5
PCB-1242 (Aroclor 1242)
ND ugIL
0.50
1
01/15/15 18:15
01/21/15 02:58
53469-21-9
PCB-1248(Aroclor 1248)
ND ugIL
0.50
1
01/15/15 18:15
01121/1502:58
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
0.50
1
01/15/15 18:15
01/21/15 02,58
11097-69-1
PCB-1260(Aroclor 1260)
ND ug/L
0.50
1
01/15/1518:15
01/21/1502:58
11096-82-5
Toxaphene
ND ugIL
0.50
1
01/1511518:15
0112111502:58
8001-35-2
Surrogates
Tetrachloro-m-xylene(S)
48 a/
20-110
1
01/15/1518:15
01121/1502:58
877-09-8
Decachlorobiphenyl(S)
58%
20-138
1
01/15/1518:15
01/2111502:58
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Copper
26.0 ug/L
5.0
1
01/15/1515:10
01/16/1502:41
7440-50-8
Lead
18.9 ugIL
5.0
1
01/15/1515:10
01116/1502*41
7439-92-1
Zinc
127 ug/L
10.0
1
01/15/1515:10
0111611502:41
7440-66-6
626 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND ug/L
5.0
1
01/1511509*30
01116/1507:44
83-32-9
Acenaphthylene
ND ug/L
5.0
1
01/15/1509:30
01/16/1507:44
208-96-8
Anthracene
ND ug/L
5.0
1
01/15/1509:30
01/16/1507:44
120-12-7
Benzidine
ND ug/L
50.0
1
01/15/1509:30
01/1611507:44
92-87-5
Senzo(a)anthracene
ND ugIL
5.0
1
01/15/15 09:30
01/16/15 07:44
56-55-3
Benzo(a)pyrene
ND ug/L
5.0
1
0111511509:30
01/16/1507:44
50-32-8
Benzo(b)Buoranthene
ND ug/L
5.0
1
01/1511509:30
01116115 07 44
205-99-2
Benzo(g,hj)perylene
ND ug/L
5.0
1
01/15/1509:30
01/16/1507:44
191-24-2
REPORT OF LABORATORY ANALYSIS
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Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27

(�52ceAnalyfical'
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ANALYTICAL RESULTS
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall 001 Lab ID: 92233194001 Collected: 01/12/1507:45 Received: 01/1311510:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Dual
626 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(k)fluoranthene
NO ug/L
5.0
1
01/15/15 09:30
01/16115 07:44
207-08-9
4-Bromophenylphenyl ether
NO ug/L
5.0
1
01/15/15 09:30
01/16115 07:44
101-55-3
Butylbenzylphthalate
NO ug/L
5.0
1
01/15/1509:30
01/16115 07:44
85-68-7
4-Chloro-3-methylphenol
NO ug/L
5.0
1
01/15/1509:30
01/16/1507:44
59-50-7
bis(2-Chloroethoxy)methane
NO ug/L
10.0
1
01/15/15 09:30
0111611507:44
111-91-1
bis(2-Chloroethyl) ether
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
111-44-4
bis(2-Chloroisopropyl) ether
NO ug/L
5.0
1
01115/15 09:30
01/16115 07:44
108-60-1
2-Chloronaphthalene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
91-58-7
2-Chlorophenol
NO ug/L
5.0
1
01/15/15 09:30
01/16/1507:44
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
7005-72-3
Chrysene
NO ug/L
5.0
1
01/15/15 09:30
01/16/1507:44
218-01-9
Dibenz(a,h)anthracene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
53-70-3
3,3'-Dichlorobenzidine
NO ug/L
25.0
1
01/15/15 09:30
0111611507:44
91-94-1
2,4-Dichlorophenol
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
120-83-2
Diethylphthalate
NO ug/L
5.0
1
01/15/1509:30
0111611507:44
84-66-2
2,4-Dimethylphenol
ND uglL
10.0
1
01115M509:30
01/16115 07:44
105-67-9
Dimethylphthalate
NO ug/L
5.0
1
01/15/15 09:30
01116115 07:44
131-11-3
Di-n-butylphthalate
NO ug/L
5.0
1
01/15/1509:30
01/16/1507:44
84-74-2
4,6-Dinitro-2-methylphenol
NO ug/L
20.0
1
01/15/15 09:30
01/16/15 07:44
534-52-1
2,4-Dinitrophenol
NO ug/L
50.0
1
01/15/1509:30
0111611507*44
51-28-5
2,4-Dinitrotoluene
NO ug/L
5.0
1
01/15/1509:30
01/16115 07:44
121-14-2
2,6-Dinitrotoluene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
606-20-2
Di-n-octylphthalate
NO ug/L
5.0
1
01/15M5 09:30
01/16/15 07:44
117-84-0
1,2-Diphenylhydrazine
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
122-66-7
bis(2-Ethylhexyl)phthalate
NO ug/L
5.0
1
01/15/1509:30
01/1611507:44
117-81-7
Fluoranthene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
206-44-0
Fluorene
ND ug/L
5.0
1
01/15/15 09:30
01/16115 07:44
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
01/15/15 09:30
01116/15 07:44
87-68-3
Hexachlorobenzene
NO ug/L
5.0
1
01/1511509:30
01/16115 07:44
118-74-1
Hexachlorocyclopentadiene
NO ug/L
10.0
1
01/15/1509:30
01/1611507:44
77-47-4
Hexachloroethane
NO ug/L
5.0
1
01/15/1509:30
01/1611507:44
67-72-1
Indeno(1,2,3-cd)pyrene
NO ug/L
5.0
1
01/15/15 09:30
01/16115 07:44
193-39-5
Isophorone
NO ug/L
10.0
1
01/15/1509:30
01/16/1507:44
78-59-1
Naphthalene
ND ug/L
5.0
1
01/15/15 09:30
01116/1507:44
91-20-3
Nitrobenzene
NO ug/L
5.0
1
01115/1509:30
01/16/1507:44
98-95-3
2-Nitrophenol
NO ug/L
5.0
1
01/1511509:30
01/16/1507:44
BB-75-5
4-Nitrophenol
NO ug/L
50.0
1
01/1511509:30
01/16/1507:44
100-02-7
N-Nnrosodimethylamine
NO ug/L
5.0
1
01/15/1509:30
01/16/15 07:44
62-75-9
N-Nitroso-di-n-propylamine
NO ug/L
5.0
1
01115/1509:30
01h6/1507:44
621-64-7
N-Nitrosodiphenylamine
NO ug/L
10.0
1
01/15/1509:30
0111611507:44
86-30-6
Pentachlorophenol
NO ug/L
10.0
1
01/15/1509:30
01116/1507:44
87-86-5
Phenanthrene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
85-01-8
Phenol
NO ug/L
5.0
1
01/15/15 09:30
01/16115 07:44
108-95-2
Pyrene
NO ug/L
5.0
1
01/15/15 09:30
01/16/15 07:44
129-00-0
1,2,4-Trichlorobenzene
NO ug/L
5.0
1
01/15/15 09:30
01116/15 07:44
120-82-1
2,4,6-Tdchlorophenol
NO ug/L
10.0
1
01/15/15 09:30
01/16/15 07:44
88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc., Page 6 of 27

Pace Analytical Services, Inc.
laceMalytiol"
9800 Ki ncey Ave. Suite 100
Huntersville, NC 28078
aww.peule0s.mn [phone]
ANALYTICAL RESULTS
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
Sample: Outfall 001 Lab ID: 92233194001 Collected: 01/1211507:45 Received: 01113/1510:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
626 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Nitrobenzene-d5(S)
39 %
10-120
1
01/15M509:30
01/16/1507:44
4165-60-0
2-Fluorobiphenyl (S)
39 %
15-120
1
01/15/15 09:30
01/16/15 07:44
321-60-8
Terphenyl-d14(S)
60 a/
11-131
1
01/15/1509:30
0111611507:44
1718-51-0
Phenol-d6(S)
14 %
10-120
1
01/15/1509:30
01/1611507:44
13127-88-3
2-Fluorophenol(S)
21 %
10-120
1
01/15/15 09:30
01/16/15 07:44
367-12-4
2,4,6-Tribromophenol(S)
55 %
10-137
1
01/15/15 09:30
01/16115 07:44
118-79-6
624 Volatile Organics Analytical Method: EPA 624
Acrolein
NO ug/L
5.0
1
01/1711511:03
107-02-8
Acrylonitdle
NO ug/L
50.0
1
01/17/1511:03
107-13-1
Benzene
NO uglL
2.0
1
01/17/15 11:03
71-43-2
Bromodichloromethane
NO uglL
2.0
1
01/17/1511:03
75-27-4
Bromoform
NO ug/L
2.0
1
01117/1511:03
75-25-2
Bromomethane
ND ug/L
2.0
1
01/17/1511:03
74-83-9
Carbon tetrachloride
NO ug/L
2.0
1
01/17/15 11:03
56-23-5
Chlorobenzene
ND ug/L
2.0
1
01/17/1511:03
108-90-7
Chloroethane
NO ug/L
2.0
1
01117/15 11:03
75-00-3
2-Chloroethylvinyl ether
NO ug/L
5.0
1
01/17/15 11:03
110-75-8
Chloroform
NO ug/L
2.0
1
01/17/1511:03
67-66-3
Chloromethane
ND ug/L
2.0
1
01117/1511:03
74-87-3
Dibromochloromethane
NO ug/L
2.0
1
01/17/1511:03
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
01/17/15 11:03
95-50-1
1,3-Dichlorobenzene
ND ug/L
2.0
1
01/17/15 11:03
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
01/17/15 11:03
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
01117/15 11:03
75-34-3
1,2-Dichloroethane
NO ug/L
2.0
1
01/17/15 11:03
107-06-2
1,1-Dichloroethene
NO ug/L
2.0
1
01/17/1511:03
75-35-4
cis-1,2-Dichloroethene
NO ug/L
2.0
1
01117/1511:03
156-59-2
trans-1,2-Dichloroethene
NO uglL
2-0
1
01/17/15 11:03
156-60-5
1,2-Dichloropropane
NO uglL
2.0
1
01/17115 11:03
78-87-5
cis-1,3-Dichloropropene
NO ug/L
2.0
1
01/17115 11:03
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
2.0
1
01/17/15 11:03
10061-02-6
Ethylbenzene
NO ug/L
2.0
1
01/17115 11:03
100-41-4
Methylene Chloride
NO ug/L
2.0
1
01/1711511:03
75-09-2
1,1,2,2-Tetrachloroethane
NO ug/L
2.0
1
01117/15 11:03
79-34-5
Tetrachloroethene
NO uglL
2.0
1
01117/15 11:03
127-18-4
Toluene
NO ug/L
2.0
1
01117/1511:03
108-88-3
1,11-Trichloroethane
ND ug/L
2.0
1
01/17/1511:03
71-55-6
1,1,2-Trichloroethane
NO ug/L
2.0
1
01/17/1511:03
79-00-5
Tnchloroethene
ND ug/L
2.0
1
01/17/15 11:03
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
01/17/15 11:03
75-69-4
Vinyl chloride
ND ug/L
2.0
1
01/17/15 11:03
75-01-4
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
01/17/15 11:03
460-00-4
Toluene-d8 (S)
93 %
70-130
1
01/17/15 11:03
2037-26-5
1,2-Dichloroethane-d4 (S)
92 %
70-130
1
01/17115 11:03
17060-07-0
REPORT OF
LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM
wihout the written consent of Pace Analytical Services, Inc -
Page 7 of 27

(�55'ceAnalyficalo
ew+ePaceWDemn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Sample: Outlall 001 Lab ID: 92233194001 Collected: 01/12/15 07:45 Received O1/13/151020 Matrix : Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 22.4 mg/L 10.0 1 01/20/15 12:48 H1
4600H+ pH, Electrometric Analytical Method: SM 4500-H+B
pH at 25 Degrees C 7.1 Std. Units 1_0 1 01/15/15 14:01 H6
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 27

laceAnalyfical'
wwwpanalabs.com
QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
OC Batch: GCSV/20094 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92233194001
METHOD BLANK: 1371727
Associated Lab Samples: 92233194001
Parameter Units
Total Petroleum Hydrocarbons mg/L
LABORATORY CONTROL SAMPLE: 1371728
Parameter Units
Total Petroleum Hydrocarbons mglL
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01116/1509:33
Spike LCS LCS %Rec
Conic. Result %Rec Limits Qualifiers
20 17.2 86 64-132
MATRIX SPIKE SAMPLE: 1371729
92233150001 Spike MS MS %Rec
Parameter Units Result Conic. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 20 16.4 82 64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Dale: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 27

laceAnalyfical'
wwwpacetaeecom
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SIMs Metals Stormwater
Pace Project No.:
92233194
OC Batch:
MPRP/17724 Analysis Method: EPA 200.7
QC Batch Method:
EPA 2007 Analysis Description: 200.7 MET
Associated Lab Samples:
92233194001
METHOD BLANK: 1371116
Associated Lab Samples: 92233194001
Parameter
Copper
Lead
Zinc
ug/L
ug/L
ug/L
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
NO 5.0 01/16/1502:16
NO 5.0 01/16/15 02:16
NO 10.0 01/16/15 02:16
LABORATORY CONTROL SAMPLE:
1371117
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result %Rec Limits Qualifiers
Copper
ug/L
500
470 94 85-115
Lead
ug/L
500
474 95 85-115
Zinc
ug/L
500
463 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1371118 1371119
MS MSD
92233290005 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Copper ug/L 5.3 Soo 500 491 484 97 96 70-130 1 20
Lead ug/L NO 500 500 474 472 95 94 70-130 0 20
Zinc ug/L ND 500 500 471 472 92 93 70-130 0 20
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 1371120
1371121
MS
MSD
92233283002
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Copper
ug/L
ND
500
500
480
471
96
94
70-130
2
20
Lead
ug/L
ND
500
500
471
458
94
92
70-130
3
20
Zinc
ug/L
4.9J
500
500
463
454
92
90
70-130
2
20
Results presented on this page are in the units Indlcmed by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc..
Page 10 of 27

(�52ceAnalyfical'
w,vepaoela6s.can
QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
OC Batch: MSV/30026 Analysis Method: EPA 624
QC Batch Method. EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92233194001
METHOD BLANK: 1372627
Associated Lab Samples: 92233194001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Tdchloroethane
ug/L
NO
2.0
01/16/1523:18
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
01/16/1523:18
1,1,2-Tricheroethane
ug/L
NO
2.0
01/16/15 23:18
1,1-Dichloroethane
ug/L
ND
2.0
01/16/15 23:18
1,1-Dichloroethene
ug/L
NO
2.0
01/16115 23:18
1,2-Dichlorobenzene
ug/L
NO
2.0
01116/1523:18
1,2-Dichloroethane
ug/L
NO
2.0
01/16/1523:18
1,2-Dichloropropane
ug/L
NO
2.0
01/16/15 23:18
1,3-Dichlorobenzene
ug/L
NO
2.0
01/16/15 23:18
1 4-Dichlorobenzene
ug/L
ND
2.0
01/16/15 23:18
2-Chloroethylvinyl ether
ug/L
ND
5.0
01/16/15 23:18
Acrolein
ug/L
NO
5.0
01/16/15 23:18
Acrylonitme
ug/L
NO
50.0
01/16/1523:18
Benzene
ug/L
ND
2.0
01/1611523:18
Bromodichloromethane
ug/L
NO
2.0
01/16/1523*18
Bromoform
ug/L
NO
2.0
01116/1523:18
Bromomethane
ug/L
NO
2.0
01/1611523:18
Carbon tetrachloride
ug/L
NO
2.0
01/1611523:18
Chlorobenzene
ug/L
NO
2.0
01/16/15 23:18
Chloroethane
ug/L
NO
2.0
01/16/15 23:18
Chloroform
ug/L
NO
2.0
01/16115 23:18
Chloromethane
ug/L
NO
2.0
01/16/15 23:18
cis-1,2-Dichloroethene
ug/L
ND
2.0
01/16/15 23:18
cis-1,3-Dichloropropene
ug/L
NO
2.0
01/16/15 23:18
Dibromochloromethane
ug/L
NO
2.0
01/16/1523:18
Ethylbenzene
ug/L
NO
2.0
01/16/1523:18
Methylene Chloride
ug/L
NO
2.0
01/16/15 23:18
Tetrachloroethene
ug/L
ND
2.0
01/16/15 23:18
Toluene
ug/L
NO
2.0
01/16/15 23:18
trans-1 2-Dichloroethene
ug/L
NO
2.0
01/16/15 23:18
trans-1,3-Dichloropropene
ug/L
NO
2.0
01/16/1523:18
Trichloroethene
ug/L
NO
2.0
01/16/1523:18
Trichlorofluoromethane
ug/L
NO
2.0
01/16/1523:18
Vinyl chloride
ug/L
ND
2.0
01/16/15 23:18
1,2-Dichloroethane-d4 (S)
%
93
70-130
01/16/15 23:18
4-Bromofluorobenzene (S)
%
106
70-130
01/16/15 23:18
Toluene-d8 (S)
%
93
70-130
01/16/15 23:18
Qualifiers
pace Analytical Sarvices, Inc.
9800 Kii Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presentee on this page are In the units Indicated by the "Unt s" column except where an alternate unit Is press Mod to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
LABORATORY CONTROL SAMPLE:
Parameter
1372628
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Rec
Limits
1,1,1-Trichloroethane
ug/L
20
18.7
94
52-162
1,1,2,2-Tetrachloroethane
ug/L
20
19.2
96
46-157
1,1,2-Trichloroethane
ug/L
20
20.0
100
52-150
1,1-Dichloroethane
ug/L
20
18.5
92
59-155
1,1-Dichloroethene
ug/L
20
17.5
88
1-234
1,2-Dichlorobenzene
ug/L
20
20.6
103
18-190
1,2-Dichloroethane
ug/L
20
17.5
87
49-155
1,2-Dichloropropane
ug1
20
19.2
96
1-210
1,3-Dichlorobenzene
ug/L
20
20.3
101
59-156
1,4-Dichlorobenzene
ug/L
20
20.2
101
18-190
2-Chloroethylvinyl ether
ug/L
40
39.4
99
1-305
Acrolein
ug/L
100
98.9
99
15-152
Acfylonitdle
ug/L
100
105
105
75-132
Benzene
ug/L
20
20A
100
37-151
Bromodichloromethane
ug/L
20
17.4
87
35-155
Bromoform
ug/L
20
18.6
93
45-169
Bromomethane
ug/L
20
11.9
59
1-242
Carbon tetrachloride
ug/L
20
19.6
98
70-140
Chlorobenzene
ug/L
20
19.9
100
37-160
Chloroethane
ug/L
20
14.2
71
14-230
Chloroform
ug/L
20
17.3
86
51-138
Chloromethane
ug/L
20
13.8
69
1-273
cis-1,2-Dichloroethene
ug/L
20
19.3
97
68-146
cis-1,3-Dichloropropene
ug/L
20
18.8
94
1-227
Dibromochloromelhane
ug/L
20
18.6
93
53-149
Ethylbenzene
ug/L
20
19.6
98
37-162
Methylene Chloride
ug/L
20
18.2
91
1-221
Tetrachlorcethene
ug/L
20
19.7
99
64-148
Toluene
ug/L
20
19.5
98
47-150
trans-12-Dichloroethene
ug/L
20
19.7
99
54-156
trans-1,3-Dichloropropene
ug/L
20
19.4
97
17-183
Trichloroethene
ug/L
20
20.2
101
71-157
Trichlorofluoromethane
UgIL
20
18.5
93
17-181
Vinyl chloride
ug/L
20
15.5
77
1-251
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene(S)
%
103
70-130
Toluene-d8(S)
%
97
70-130
Pace Analytical Services, Inc.
9800 Kinwy Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
1372633
92232777002
Spike
MS
MS
%Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
NO
20
19.6
98
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
18.3
92
73-159
1, 1,2-Trichl oroethane
ug/L
ND
20
2Q2
101
64-152
1,1-Dichloroethane
ug/L
ND
20
19Y
99
43-172
Resubs presentee on this page ant In the ..Its indlcated by the "Units" column except where an anernate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducer, except in full,
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Silvis Metals Slormwaler
Pace Project No.: 92233194
MATRIX SPIKE SAMPLE:
1372633
92232777002
Spike
MS
MS
%Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
ND
20
19.3
97
48-189
1,2-Dichlorobenzene
ug/L
ND
20
16.0
80
54-154
1,2-Dichloroethane
ug/L
ND
20
17.0
85
42-171
1,2-Dichloropropane
ug/L
ND
20
20.0
100
55-157
1,3-Dichlorobenzene
ug/L
ND
20
15.9
79
57-148
1,4-Dichlorobenzene
ug/L
ND
20
16.2
81
58-149
2-Chloroethylvinyl ether
ug/L
ND
40
ND
0
70-130 P5
Acrolein
ug/L
ND
100
30.6
31
70-130 MO
AcrylorhOle
ug/L
ND
100
108
105
70-130
Benzene
ug/L
ND
20
22.2
111
54-163
Bromodichloromelhane
ug/L
ND
20
18.7
93
56-152
Bromoform
ug/L
ND
20
19.4
97
53-151
Bromomethane
ug/L
ND
20
7.9
39
10-200
Carbon tetrachloride
ug/L
ND
20
20.4
102
41-175
Chlorobenzene
ug/L
ND
20
19.4
97
67-152
Chloroethane
ug/L
ND
20
19.0
95
23-200
Chloroform
ug/L
24.2
20
38.5
71
51-166
Chloromethane
ug/L
ND
20
13.9
70
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
19.8
99
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
18.6
93
38-146
Dibromochloromethane
ug/L
ND
20
19.3
96
65-144
Ethylbenzene
ug/L
ND
20
17.7
88
57-152
Methylene Chloride
ug/L
ND
20
16.3
78
40-167
Telrachloroethene
ug/L
ND
20
18.5
93
59-155
Toluene
uglL
ND
20
21.3
101
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
19.8
99
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
18.7
93
39-148
Trichloroelhene
ug/L
ND
20
22.3
112
60-153
Trichlorofluoromethane
ug/L
ND
20
20.9
105
42-199
Vinyl chloride
ug/L
ND
20
18.5
92
46-176
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene(S)
IN
95
70-130
Toluene-d8 (S)
e/
95
70-130
SAMPLE DUPLICATE: 1372632
92232710001
Cup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1-Tdchloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
Results presented on this page are In the units indicated by the "Un IN" column except whom an alternate unit is presented to the dgM or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the wntten consent of Pace Analytical Services, Inc.. Page 13 of 27

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QUALITY CONTROL DATA
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
SAMPLE DUPLICATE: 1372632
Parameter
Units
92232710001
Result
Dup
Result
1,3-Dichlorobenzene
ug/L
NO
NO
1,4-Dichlorobenzene
ug/L
NO
ND
2-Chloroethylvinyl ether
ugll-
NO
ND
Acrolein
uglL
ND
NO
Acrylonitdle
ug/L
NO
ND
Benzene
ug/L
NO
NO
Bromodichloromethane
ug/L
NO
NO
Bromoform
ug/L
NO
NO
Bromomethane
ug/L
NO
NO
Carbon tetrachloride
uglL
NO
NO
Chlorobenzene
ug/L
NO
NO
Chloroethane
ug/L
NO
ND
Chloroform
ug/L
6.2
6.2
Chloromethane
ug/L
ND
NO
cis-1,2-Dichloroethene
ug/L
NO
NO
cis-1,3-Dichloropropene
ug/L
NO
NO
Dibromochloromethane
ug/L
NO
NO
Ethylbenzene
ug/L
NO
NO
Methylene Chloride
ug/L
NO
NO
Tetrachlorcethene
ug/L
NO
NO
Toluene
uglL
NO
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
NO
Trichloroethene
ug/L
NO
NO
Tnchlorofluoromethane
ug/L
NO
NO
Vinyl chloride
ug/L
NO
NO
1,2-Dichloroelhane-d4 (S)
%
99
97
4-Bromofluorobenzene (S)
e/
96
96
Toluene-d8(S)
%
94
94
Max
RPD RPD
i7
2
1
0
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical SGI VICea, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SIMs Metals Stormwater
Pace Project No.:
92233194
QC Batch:
OEXT/32333 Analysis Method: EPA 608
QC Batch Method:
EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples:
92233194001
METHOD BLANK: 1371575
Associated Lab Samples: 92233194001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
4,4'-DDD
uglL
NO
0.050
01/20/15 19:56
4,4'-DDE
uglL
NO
0.050
01/20/15 19:56
4,4'-DDT
ug/L
NO
0.050
01/2011519:56
Aldrin
ug/L
NO
0.050
01/2011519:56
alpha-BHC
ug/L
NO
0.050
01/20/1519:56
beta-BHC
ug/L
NO
0,050
01/20/15 19:56
Chlordane (Technical)
ug/L
NO
0.50
01/20/15 19:56
delta-BHC
ug/L
NO
0.050
01/2011519*56
Dieldrin
uglL
NO
0.050
01/2011519:56
Endosulfan I
uglL
NO
0,050
01/20/15 1956
Endosulfan II
ug/L
NO
0.050
01120/1519:56
Endosulfan sulfate
ug/L
NO
0,050
01/20/15 1956
Endrn
ug/L
NO
0.050
01120/1519:56
Endrin aldehyde
ug/L
NO
0.050
01/20/15 19:56
gamma-BHC (Lindane)
ug/L
NO
0.050
01/20/15 1956
Heptachlor
ug/L
NO
0.050
01/20/1519:56
Heptachlor epoxide
ug/L
NO
0.050
01/20/1519:56
PCB-1016 (Aroclor 1016)
ug/L
NO
0.50
01/20/15 19:56
PCB-1221(Aroclor 1221)
ug/L
NO
0.50
01/20/1519:56
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
01/20/15 19:56
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
01/20/15 19:56
PCB-1248 (Aroclor 1248)
ug/L
NO
0,50
01/20/15 19:56
PCB-1254 (Aroclor 1254)
uglL
NO
0.50
01/20/15 19:56
PCB-1260 (Aroclor 1260)
uglL
NO
0,50
01/20/15 1956
Toxaphene
ug/L
NO
0.50
01/2011519:56
Decachlorobiphenyl (S)
%
76
20-138
01/20/15 19:56
Telrachloro-m-xylene (S)
%
82
20-110
01/20/15 19:56
Qualifiers
LABORATORY CONTROL SAMPLE:
1371576
Spike
LCS
LCS
% Rec
Parameter
Units
Conic.
Result
%Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.22
89
31-141
4,4'-DOE
ug/L
.25
0.21
85
30-145
4,4'-DDT
ug/L
.25
0.21
85
25-160
Aldrin
ug/L
.25
0.18
72
42-122
alpha-BHC
uglL
.25
0.24
98
37-134
beta-BHC
uglL
.25
0.26
104
17-147
delta-BHC
uglL
.25
0.26
103
19-140
Dieldrin
ug/L
.25
0.22
90
36-146
Endosulfan I
ug/L
.25
0.23
93
45-153
Results presented on this page are in the units Indicated by the' Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
LABORATORY CONTROL SAMPLE:
1371576
Spike
Parameter
Units
Conc.
Endosulfan II
ug/L
.25
Endosulfan sulfate
ug/L
.25
Endrin
ug/L
.25
Enddn aldehyde
ug/L
.25
gamma-BHC (Lindane)
ug/L
.25
Heptachlor
ug/L
.25
Heptachlor epoxide
ug/L
.25
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
LCS
Result
LCS
%Rec
% Rec
Limits
0.24
96
1-202
0.23
94
26-144
0.23
92
30-147
0.19
76
50-150
0.24
98
32-127
OAS
73
34-111
0.22
90
41-126
86
20-138
96
20-110
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1371577
MS
92233037001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1371578
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
Max
RPD RPD Qual
4,4'-DDD
ug/L
NO
.5
.5 041
0.41
84
82
31-141
2
30
4,4'-DDE
ug/L
NO
.5
.5 0.38
0.39
77
78
30-145
1
30
4,4'-DDT
ug/L
NO
.5
.5 0.36
0.39
73
79
25-160
8
30
Aldrin
ug/L
NO
.5
.5 0.39
0.40
78
81
42-122
4
30
alpha-BHC
ug/L
NO
.5
.5 0.42
0A0
84
81
37-134
4
30
beta-BHC
ug/L
NO
.5
.5 0.55
0.54
110
109
17-147
2
30
delta-BHC
ug/L
NO
.5
.5 0.47
0.45
94
90
19-140
5
30
Dieldrin
ug/L
NO
.5
.5 0.39
0.40
80
80
36-146
0
30
Endosulfan)
uglL
NO
.5
.5 0.42
042
85
84
45-153
1
30
Endosulfan II
ug/L
NO
.5
.5 0.41
0.40
83
81
1-202
3
30
Endosulfan sulfate
ug/L
NO
.5
.5 0.43
0.41
87
83
26-144
4
30
Endrin
ug/L
NO
.5
.5 0.44
0.44
89
89
30-147
0
30
Endrm aldehyde
ug/L
NO
.5
.5 0.34
0.35
69
71
50-150
3
30
gamma-BHC (Lindane)
ug/L
NO
.5
.5 0.41
0.41
84
82
32-127
2
30
Heptachlor
ug/L
NO
.5
.5 0.38
0.39
77
80
34-111
3
30
Heptachlor epoxide
ug/L
NO
.5
.5 0.39
0.38
79
78
41-126
2
30
Decachlorobiphenyl (S)
%
58
28
20-138
Tetrachloro-m-xylene (S)
e/
84
84
20-110
Results presented on this page are In the units indicated by the "Units" column except yMere an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 16 of 27

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QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
QC Batch: OEXT/32298 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92233194001
METHOD BLANK: 1370688
Associated Lab Samples: 92233194001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
01/15/15 23:12
1,2-Diphenylhydrazine
ug/L
NO
5.0
01/15/15 23:12
2,4,6-Trichlorophenol
ug/L
NO
10.0
01/15/15 23:12
2,4-Dichlorophenol
ug/L
NO
5.0
01115/1523:12
2,4-Dimelhylphenol
ug/L
NO
10.0
01/1511523:12
2,4-Dinitrophenol
ug/L
NO
50.0
01/1511523:12
24-Dinitrotoluene
ug/L
NO
5.0
01/1511523:12
2,6-Dinitrotoluene
ug/L
NO
5.0
01/15/1523:12
2-Chloronaphthalene
ug/L
NO
5.0
01/15/15 23:12
2-Chlorophenol
uglL
NO
5.0
01/15/1523:12
2-Nitrophenol
ug/L
NO
5.0
01/1511523*12
3,3'-Dichlorobenzidine
ug/L
NO
25.0
01/1511523:12
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
01/1511523:12
4-Bromophenylphenyl ether
ug/L
NO
5.0
01115/1523:12
4-Chloro-3-methylphenol
ug/L
NO
5.0
01115/1523:12
4-Chlorophenylphenyl ether
ug/L
NO
5.0
01/15/1523:12
4-Nitrophenol
ug/L
ND
50.0
01/15/15 23:12
Acenaphthene
ug/L
NO
5.0
01/15/1523:12
Acenaphthylene
ug/L
NO
5.0
01/15/1523: 12
Anthracene
ug/L
NO
5.0
01/15/15 23:12
Benzidine
ug/L
NO
50.0
01/15/15 23:12
Benzo(a)anthracene
ug/L
NO
5.0
01115/1523:12
Benzo(a)pyrene
ug/L
NO
5.0
01/15/1523:12
Benzo(b)0uoranthene
ug/L
ND
5.0
01/15/15 23:12
Benzo(g,h,i)perylene
ug/L
NO
5.0
01/15/15 23:12
Benzo(k)fluoranthene
ug/L
NO
5.0
0111511523:12
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
01/15/15 23:12
bis(2-Chloroethyl) ether
ug/L
NO
5.0
01/15115 23:12
bis(2-Chloroisopropyl) ether
ug/L
NO
5.0
01/15/15 23:12
bis(2-Ethylhexyl)phthalate
ug/L
NO
5-0
01/15/15 23:12
Butylbenzylphthalate
ug/L
NO
5.0
01/15/15 23:12
Chrysene
ug/L
NO
5.0
01/1511523:12
Di-n-butylphthalate
ug/L
NO
5.0
Ot/15/1523:12
Di-n-octylphthalate
ug/L
NO
5.0
01/15/1523:12
Dibenz(a,h)anthracene
ug/L
NO
5.0
01/15/15 23:12
Diethylphthalate
ug/L
NO
5.0
01/15/1523:12
Dimethylphthalate
ug/L
NO
5.0
01/15/1523:12
Fluoranlhene
ug/L
NO
5.0
01/15/15 23:12
Fluorene
ug/L
NO
5.0
01/1511523:12
Hexachloro-1,3-butadiene
ug/L
NO
5.0
01/15/15 23:12
Hexachlorobenzene
ug/L
NO
5.0
01115/1523:12
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2BC78
[phone]
Results presented on this page are In the units Indicated by the "Units" column except whore an alternate unit Is pmsemeE to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 27

(�Ia?eAnalytiml
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Project: SIMS
Pace Project No.: 92233
METHOD BLANK: 13706
Associated Lab Samples:
Parameter
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propyla mi ne
N-Nitrosodi met hyl ami ne
N-N itrosod i phenylami ne
Naphthalene
Nitrobenzene
Penlachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tnbromophenol (S)
2-Fluorobiphenyl(S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
LABORATORY CONTROL
Parameter
1,2,4-Trichlorobenzene
1, 2-Diphenylhydrazin e
2, 4, 6-Trich loro phen of
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3, 3'-Dich lorobenzidi ne
4, 6-Di nitro-2-methyl phenol
4-Bromophenylphenyl ethe
4-C hl oro-3-methyl p henol
4-Chlorophenylphenyl ethe
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Results pre
Date: 01/27/2015 10:42 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28075
[phone]
QUALITY CONTROL
DATA
Metals Stormwater
194
88
Matrix:
Water
92233194001
Blank
Reporting
Units
Result
Limit
Analyzed
Qualifiers
ug/L
NO
10.0
01/15/15 23:12
ug/L
NO
5.0
01/15/1523:12
ug/L
NO
5.0
0111511523:12
ug/L
NO
10.0
01/15/15 23:12
ug/L
NO
5.0
01/15/15 23:12
ug/L
NO
5.0
01/15/1523:12
ug/L
NO
10.0
01115/15 23:12
ug/L
NO
5.0
01/15/15 23:12
ug/L
NO
5.0
01/15/15 23:12
ug/L
NO
10.0
01/15/1523:12
ug/L
NO
5.0
01/15115 23:12
ug/L
NO
5.0
01/15/15 23:12
ug/L
NO
5.0
01/15/15 23:12
%
48
10-137
01115/1523:12
%
45
15-120
01/15/15 23:12
%
24
10-120
01/15/1523:12
%
42
10-120
01/15115 23:12
%
16
10-120
01/15/1523:12
%
76
11-131
01/15/15 23:12
SAMPLE:
1370689
Spike
LCS
-CS %
Rec
Units
Conc.
Result
%Rec Limits
Qualifiers
ug/L
50
24.8
50
44-142
ug/L
50
36.2
72
25-150
ug/L
50
29.3
59
37-144
ug/L
50
28.2
56
1-191
ug/L
50
26.2
52
32-119
ug/L
250
192
77
1-181
ug/L
50
42.9
86
39-139
ug/L
50
41.2
82
50-158
ug/L
50
27.8
56
60-118 L2
ug/L
50
24.5
49
23-134
ug/L
50
29.2
58
29-182
ug/L
100
82A
82
1-262
ug/L
100
86.0
86
1-181
r
ug/L
50
39.8
80
53-127
ug/L
100
58.8
59
22-147
r
ug/L
50
36.2
72
25-158
ug/L
250
81.9
33
1-132
ug/L
50
32.6
65
47-145
ug/L
50
32.7
65
33-145
ug/L
50
43.1
86
1-166
ug/L
100
NO
2
25-150 L2
s<rned on this page are In the units Indicated by the "Units"
column except where an altemote unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc..
Page 18 of 27

(�IaceAnalyfical'
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QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
LABORATORY CONTROL SAMPLE:
1370689
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Benzo(a)anthracene
ug/L
50
44.9
90
33-143
Benzo(a)pyrene
uglL
50
49.1
98
17-163
Benzo(b)fluoranthene
ug/L
50
47.1
94
24-159
Benzo(g,h,i)perylene
ug/L
50
45.1
90
1-219
Benzo(k)fluoranthene
ug/L
50
42.4
85
11-162
bis(2-Chloroethoxy)methane
ug/L
50
26.9
54
33-184
bis(2-Chloroethyp ether
ug/L
50
26.5
53
12-158
bis(2-Chloroisopropyl) ether
ug/L
50
22.0
44
36-166
bis(2-Ethylhexyl)phthalate
ug/L
50
49.3
99
8-158
Butylbenzylphthalate
uglL
50
49.1
98
1-152
Chrysene
ug/L
50
45.5
91
17-168
Di-n-butylphthalate
ug/L
50
46.7
93
1-118
Di-n-octylphthalate
uglL
50
59.0
118
4-146
Dibenz(a,h)anthracene
ug/L
50
47.0
94
1-227
Diethylphthalate
ug/L
50
43.8
88
1-114
Dimethylphthalate
ug/L
50
40.5
81
1-112
Fluoranthene
ug/L
50
46.5
93
26-137
Fluorene
ug/L
50
38.8
78
59-121
Hexachloro-1,3-butadiene
ug/L
50
24.3
49
24-116
Hexachlorobenzene
uglL
50
40.6
81
1-152
Hexachlorocyclopentadiene
ug/L
50
24.7
49
25-150
Hexachloroethane
ug/L
50
21A
42
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
49.8
100
1-171
Isophorone
ug/L
50
27.4
55
21-196
N-Nitroso-di-n-propylamine
uglL
50
25.3
51
1-230
N-Nitrosodimethylamine
ug/L
50
16.6
33
25-150
N-Nitrosodiphenylamine
ug/L
50
41.0
82
25-150
Naphthalene
ug/L
50
26.8
54
21-133
Nitrobenzene
ug/L
50
26.5
53
35-180
Pentachlorophenol
ug/L
100
81.1
81
14-176
Phenanthrene
ug/L
50
41.0
82
54-120
Phenol
uglL
50
11.3
23
5-112
Pyrene
ug/L
50
43.6
87
52-115
24,6-Tnbromophenol(S)
%
83
10-137
2-Fluorobiphenyl (S)
%
56
15-120
2-Fluorophenol(S)
%
29
10-120
Nitrobenzene-d5 (S)
%
51
10-120
Pher l-d6(S)
%
20
10-120
Terpher l-d14 (S)
%
86
11-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370690
1370691
MS
MSD
92233032001 Spike
Spike
MS
MSD
MS MSD %Rec Max
Parameter Units Result Conic,
Conc.
Result
Result
%Rec %Rec Limits RPD RPD Qual
1,2,4-Trichlorobenzene ug/L ND 100
100
45.3
44.5
45 44 44-142 2 30
Results presented on this page are in the units indicated by the
"Units" column
except where
an ahernate unit is presented to the right of no result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 27

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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1370690
1370691
MS
MSD
92233032001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc,
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qua[
1,2-Diphenylhydrazine
ug]L
NO
100
100
65.7
72.4
66
72
25-150
10
30
2,4,6-Tdchlorophenol
ug/L
NO
100
100
49.8
50.6
50
51
37-144
2
30
2,4-Dichlorophenol
ug/L
NO
100
100
48.0
46.1
48
46
1-191
4
30
2,4-Dimethylphenol
ug/L
NO
100
100
47.2
46.8
47
47
32-119
1
30
2,4-Dinitrophenol
uglL
NO
500
500
357
366
71
73
1-181
3
30
2,4-Dinitrotoluene
uglL
NO
100
100
85.4
86.4
85
86
39-139
1
30
2,6-Dinitrotoluene
ug/L
NO
100
100
77.8
78.7
78
79
50-158
1
30
2-Chloronaphthalene
ug/L
NO
100
100
47.0
47.0
47
47
60-118
0
30 MO
2-Chlorophenol
ug/L
NO
100
100
43.8
44.4
44
44
23-134
1
30
2-Nitrophenol
ug/L
ND
100
100
49.7
48.0
50
48
29-182
3
30
3,3'-Dichlorobenzidine
ug/L
NO
200
200
159
161
80
80
1-262
1
30
4,6-Dinitro-2-methylphenol
ug/L
NO
200
200
165
172
83
86
1-181
4
30
4-Bromophenylphenyl ether
ug/L
NO
100
100
73.5
77.9
73
78
53-127
6
30
4-Chloro-3-methylphenol
ug/L
NO
200
200
112
109
56
55
22-147
3
30
4-Chlorophenylphenyl ether
ug/L
NO
100
100
63.9
66.0
64
66
25-158
3
30
4-Nitrophenol
ug/L
NO
500
500
237
249
47
50
1-132
5
30
Acenaphthene
ug/L
NO
100
100
55.6
55.5
56
56
47-145
0
30
Acenaphthylene
ug/L
NO
100
100
56.0
56.0
56
56
33-145
0
30
Anthracene
uglL
NO
100
100
81.7
84.9
82
85
1-166
4
30
Benzidine
ug/L
NO
200
200
17.5J
NO
9
2
25-150
30 MO
Benzo(a)anthracene
ug/L
ND
100
100
87.2
92.0
87
92
33-143
5
30
Benzo(a)pyrene
ug/L
NO
100
100
91.1
95.0
91
95
17-163
4
30
Benzo(b)Fluoranthene
ug/L
NO
100
100
89-8
96.9
90
97
24-159
8
30
Benzo(g,h,i)perylene
ug/L
NO
100
100
87.5
87.6
87
88
1-219
0
30
Benzo(k)fluoranthene
ug/L
NO
100
100
81.0
84.2
81
84
11-162
4
30
bis(2-Chloroethoxy)methane
ug/L
NO
100
100
44.4
44.7
44
45
33-184
1
30
bis(2-Chloroethyl) ether
ug/L
NO
100
100
45.1
45.9
45
46
12-158
2
30
bis(2-Chloroisopropyl) ether
ug/L
NO
100
100
37.2
38.2
37
38
36-166
3
30
bis(2-Ethylhexyl)phthalate
ug/L
NO
100
100
93.4
99.9
93
100
8-158
7
30
Butylbenzylphthalate
uglL
NO
100
100
94.7
101
95
101
1-152
7
30
Chrysene
ug/L
NO
100
100
87.0
92.4
87
92
17-168
6
30
Di-n-butylphthalate
uglL
NO
100
100
89.8
94.8
90
95
1-118
5
30
Di-n-octylphthalate
ug/L
ND
100
100
111
114
111
114
4-146
3
30
Dibenz(a,h)anthracene
ug/L
NO
100
100
93.2
92.6
93
93
1-227
1
30
Diethylphthalate
ug/L
NO
100
100
e4.6
87.6
85
88
1-114
4
30
Dimethylphthalate
ug/L
NO
100
100
77.1
81.1
77
81
1-112
5
30
Fluoranthene
ug/L
NO
100
100
90.2
93.1
90
93
26-137
3
30
Fluorene
ug/L
NO
100
100
70.1
71.7
70
72
59-121
2
30
Hexachloro-1,3-butadiene
ug/L
NO
100
100
45A
42.9
45
43
24-116
5
30
Hexachlorobenzene
ug/L
NO
100
100
77.0
79.6
77
80
1-152
3
30
Hexachlorocyclopentadiene
ug/L
NO
100
100
41.1
40.6
41
41
25-150
1
30
Hexachloroethane
ug/L
NO
100
100
39.4
39.9
39
40
40-113
1
30 MI
Indeno(1,2,3-cd)pyrene
ug/L
NO
100
100
95.4
97.6
95
98
1-171
2
30
Isophorone
ug/L
ND
100
100
45.8
46.3
46
46
21-196
1
30
N-Nitroso-di-n-propylamine
ug/L
NO
100
100
43.2
42.0
43
42
1-230
3
30
N-Nitrosodimethylamine
ug/L
ND
100
100
34.9
377
35
38
25-150
8
30
Results presentee on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc.. Page 20 Of 27

aceAnalytical"
~..paceraes.can
QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX
Parameter
SPIKE DUPLICATE: 1370690
MS
92233032001 Spike
Units Result Conc.
MSD
Spike
Conc,
1370691
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD Qual
N-Nitrosodiphenylamine
ug/L
ND
100
100
76.9
82.2
77
82
25-150
7
30
Naphthalene
ug/L
ND
100
100
47.5
46.8
47
47
21-133
2
30
Nitrobenzene
ug/L
ND
100
100
44.6
45.1
45
45
35-180
1
30
Pentachlorophenol
ug/L
ND
200
200
150
151
75
76
14-176
1
30
Phenanthrene
ug/L
ND
100
100
79.7
82.6
80
83
54-120
4
30
Phenol
ug/L
ND
100
100
27.2
27.7
27
28
5-112
2
30
Pyrene
ug/L
ND
100
100
84.0
90.6
84
91
52-115
8
30
2,4,6-Tribromophenol IS)
%
77
82
10-137
2-Fluorobiphenyl (S)
e/
46
46
15-120
2-Fluorophenol (S)
%
30
32
10-120
Nitrobenzene-d5(S)
%
43
44
10-120
Phenol-d6(S)
%
24
25
10-120
Terphenyl-d14 (S)
%
79
86
11-131
Results presented on this pare are In the units indicated by the"Units" column except where an alternate unit Is press Mod to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/27/2015 10:42 AM without the whiten consent of Pace Analytical Services, Inc..
Page 21 of 27

laceAnalyticala
wwwpaceleee.com
QUALITY CONTROL DATA
Project: SIMs Metals Stormwater
Pace Project No.: 92233194
OC Batch: RWET/7907 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92233194001
METHOD BLANK: 1373215 Matrix: Water
Associated Lab Samples: 92233194001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 01/20/15 12:47
Pace Analytical services, Inc.
9800KinceyAve. Suite100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1373216
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 210 84 90-110 LO
SAMPLE DUPLICATE: 1373217
92233071001
Dup
Max
Parameter Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids mg/L
226
216
5 10
SAMPLE DUPLICATE: 1373218
92233187005
Dup
Max
Parameter Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids mglL
75.0
91.0
19 10 D6
Results presented on this page are in the units Indicated by the "Unds" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc..
Page 22 of 27

aceAnalytical"
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SIMs Metals Stormwater
Pace Project No.:
92233194
QC Batch:
RWET/7891 Analysis Method: SM 4500-H+B
QC Batch Method:
SM 4500-H+B Analysis Description. 4500H+B pH Raleigh
Associated Lab Samples:
92233194001
SAMPLE DUPLICATE: 1371061
92232751002 Cup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 7.5 7.5 0 10 H6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent or Pace Analytical Services, Inc.. Page 23 of 27

(�55OAnalyficale
' xxw.peaelehxmn
QUALIFIERS
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
DEFINITIONS
Pace Analytical SO"ICe5, Inc.
9800 Kincey Ave. Suite 100
Huntersville, 128078
(7D4)875-9092
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Dipheny1hydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside OC limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below OC limits. Results for this analyze in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded CC limits. Balch accepted based on laboratory control sample (LCS) recovery.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2015 10:42 AM without the written consent of Pace Analytical Services, Inc- Page 24 of 27

aceAnalytical e
e .pacelabs.carn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SIMS Metals Stormwater
Pace Project No.: 92233194
Pace Analytical Sen/IcaS, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92233194001
Outfall 001
EPA 1664B
GCSV/20094
92233194001
Outfall 001
EPA 3510
0EXT/32333
EPA 608
92233194001
Outfall 001
EPA 200.7
MPRP/17724
EPA 200.7
92233194001
Outfall 001
EPA 625
OEXT/32298
EPA 625
92233194001
Outfall 001
EPA 624
MSV/30026
92233194001
Outfall 001
SM 2540D
RWET/7907
92233194001
Outfall 001
SM 4500-H+B
RWET/7891
Date: 01/27/2015 10:42 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
GCSV/20120
ICP/15955
MSSV/10198
Page 25 of 27

i,08?/i Document Name:.Sampls Condition Upon Dobumant Revised: April 04,.2013
0 a141Ca(A Receipt SCUR - Pagee t of 2
,......nne.m cam
' Document No.: Issuing Authorities:
F-RAL-CS-001-tev.02 Pace Asheville QualitY Office
Client Name: /
Where Received: F1 Huntersville C] Asheville Eden Raleigh
Courfcr.(Clrclo): F ij.F.n UPS USPS Client Commercial Fare .Other
Custody Seal on Coole'Box Present: C] yes R1 no Seals Intact: 0 yes [] no
Packing Material: ❑ Bubble Wrap; C) Bubble Bags V. Nano Other
Circle Thermometer Usod: IR Gun S 2065387T of V. Wet Blue None Samples on Ica, cooling process has begun
IR Grn Raek l n.�i J.1
Temp Correction Add 1 btract
Corrected Cooler Temp.: �' C
Temp should be above freezing to 8'10
- C -
Blolo ical Tissue Frozen: Yea 110 con
9
Comments:
-0ata and Initials of p@ on examining
c t P7 a o
ct,ecNj��
Chain of Custody Present:
j6Yos ONO
OWA
1.Chain
of Custody Filled Out,
v s ON.
OwA
2.
Chain of Custody Relinquished'.
fdY.. ON1o.
L7wA
3.
Sam ter Name &Signature onCOC:
YasON.
OwA
4..
Samples Arrived'vANin Hold Time:
16Y, ONO*
❑wA
5..
'
Short Hold. Time Analysis (<Mr):
OYae
OwA
6.
Rush Turn Around Time Requested:
OY% No
ONIA
7.
Surmar.
ea o
OwA
6.
Correct Containers Used'
-Pace Containers Used:
n ONO
vas ONO.
OWA
OwA
9.
Containers Intact:
Ye..WE
OwA
16.
rillered volume -received for Dissolved toils
O4as Quo
A
11..
Semple Labols match CDC:
-Includes dateltime/lDlAnalysis Matrix:
Yes ONO.
❑NA,
12.
Nl containers needing peservaton have been chocked.
All containers nooding preservation are found to be in
compliance With EPA reoommsndation.
axcopaone: VOA, conform. TOC, O&G. WM0 water
1lIrry%Jr,µhhhA'�rYee ONO
ILL Yee ONO
Yse ONO
OMA
Owp
13
.
'.
Samples chocked fordechlodnallon:
- Yos ONO
OwA
14.
Heeds aca In VOA Vials >6mm :
OY.a ON.
wA
15.
Trip Blank Present;
Trip Blank Custody Seals Present
Pace Tri Blank Lot d Ifpurchased),,
Dye's ONO
OY.s ONO
/,WA
IDwA
/
16.
Client Notification! Resolution: Field Data Required? Y / N
Person Contactedo:XP(( br,.— - D
t- aterfime:
Comments/ResolullwL(- ai c Kll of L ire Gyt u lej),�I"wef (-ki �A rr/ ov'ei
SCURF view:: K sI � pate:I „J'
Review:: Lc)
Note: Whenever there is a discrepancy affecting North Caroline compliance
Samples, a copy of this form YAII be sent to the North Carolina DEHNR
Cerll6ca0on Olfice.(i.o out of hold, Incoroct preservative, out of lamp,
incorrect containers)

4
Report Results to:
Sims Metal S/One Environn)ental
dfl? $1 , Vf(,,
New-sem, NC
ATTN:
Phone: ZS-d,— 77,? — lf'Olf
Chain of Custody
gill Results to: 19 Standard Report Delivery
$ I 10-ph, $15-TSS, $50-oil & grease EyRush Report Delivery (w/ surcharge)
$30-Copper, Lead, Zinc Requested Due Date:
S40G-TTO (624-625-608)
Project Reference: Stormwater
ATTN: Purchase Order #:
Sampled By: T,
4
COMP65 W
Q _Qrab
6
rt M m e,
spo Ime:
d "
Outfali 001
—VIVIT
5 —W
pH, TSS, SGT-HEM, 200.7-(Cu, Pb, Zn), TTO-(624, 625, 608)
Rel =Ish.ed
b��
Date
Ir JFor
Lab Use Only
Temperature at receipt:
I Temp: —A �Z-C.
R ned
a I L J.
J❑K )
ReJINL"hed by (slgr.awre)
5netedby(I,v.t.,.l'
"e 4
7ime
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