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Home My WebLink AboutNCS000101_DMR_2019 wta INTERNATIONAL(49 PAPER RIEGELW00D MILL JOHN L.RIEGEL.ROAD RIEGELWOOD NC 28456 January 22,2020 RECEIVED Attention: Central Files JAN 3 O 2020 Division of Energy,Minerals, and Land Resources 1612 Mail Service Center DENR-LAND QUALITY Raleigh,NC 27699-1612 STORMWATER PERMITTING Subject: Fall,2019 Semi-annual Monitoring Report,NPDES Permit NCS000101 Dear Stormwater Section: Enclosed are two copies of the Fall, 2019 semi-annual analytical monitoring report for.NPDES Permit No. NCS000101,issued December 1,2014 to International Paper's Riegelwood Mill. Lab results are included,as well as a mill stonnwater basin map. Analytical samples were collected on July 3,•November 12,and December 23,2019. Analytical results appear in the attached data table. During the Fall semester of 2019, weather conditions during work hours allowed collection of three Tier 2 samples for Basin T. Analytical.Results and Corrective Actions: Since the Spring 2019sampling events, housekeeping has.continued in an aggressive manner in an effort to meet benchmarks in Basin.T,a Tier 2 outfall. Basins B,E,.and I: Sample.results for Basin B were within all benchmark values. Basins E and I had COD results just above the benchmark of 120 mg/L: 135 and 136 mg/L,respectively. Basin E, adjacent to the wood chip pile, last had an elevated COD result_in:2017; housekeeping will be re-emphasized in this area. It is unusual for Basin I COD to exceed the limit, and no immediate cause was found. Basin I TSS was also above the benchmark of l0Omg/L at 277mg/L. Semi-annual cleanouts of the two catch. basins in Basin I will be scheduled earlier than usual. Basin T: Basin T remains a.Tier 2 outfall during this semester. Rainfall allowed three representative sampling events during the semester. The July3.,2019 sample exceeded the benchmarks for COD (120 mg/L) and TSS (100 mg/L); results were 168 and 33.6, respectively. On a 1/12119, Basin T was sampled, and again the COD result was 168; however, all other parameters..were within the benchmarks. The. 12/23/19 sample was within benchmarks for all parameters. Since that time,the roadsides in Basin T have been cleared of wood debris,and drainage.patterns have been re-shaped in an effort to eliminate S/Groups/Environmental/Stormwater/Reportst2017,I8, 19:rpts/falI2019/Anal Qv!'Lir contamination from the roadway and from the adjacent driveway,which is more heavily traveled since traffic was rerouted for safety reasons. Iousekeeping efforts remain stringent in Basin T. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,accurate, and complete. I. am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. If you have questions or need additional information,please call me at(910) 362-4753 or Wallace Coverdale of my staff at(910) 362-4590.. Sincere y, Kimberly W. ail,P.B.,Environmental Compliance Manager cc: Brian Lambe, Wilmington Regional Office S/Groups/Environmental/Stormwater/Reports/2017,18, 19:rpts/fall 20 19/Anal Cyr Ltr STORM WATER DISCHARGE OUTFALL(SDO) MONITORING REPORT Permit Number NCS_000101 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME_International Paper COUNTY Columbus PERSON COLLECTING SAMPLE(S) Wallace Coverdale PHONE NO.(_910)362-4590 CERTIFIED LABORATORY(S)_International Paper Lab# 140_ Environmental Chemists, Inc. Lab# 94_ SIGNATURE OF PERMITTEE OR DESIGNEE REQI IRED ON PAGE 2. Part A: Specific Monitoring Requirements Outfall Date 50050 No. Sample Total Total Collected Flow(if app.) Rainfall mo/dd/yr MMG inches B 11/12/2019 0.09 0.48 E 7/3/2019 0.66 0.5 7/3/2019 0.31 0.5 T 7/3/2019 0.31 0.5 T 11/12/2019 0.15 0.48 T 12/23/2019 0.34 1.09 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes x no not in runoff areas (if yes, complete Part B)' Part B: Vehicle Maintenance Activity Monitoring Requirements N/A Outfall Date 50050 00556 00530 00400 No. Sample Total Flow Total Oil&Grease Non-polar Total pH New Motor Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage (Method 1664 Solids SGT-HEM),if appl. mo/dd/yr MG inches mg/I mg/I unit gal/mo Form SWU-247, last revised 2/2/2012 �� 1 of 2 STORM EVENT CHARACTERISTICS: 2 events: ; Mail Original and one copy to: Division of Water Quality Date: _07/03/1.9 Attn: Central Files Total Event Precipitation(inches): 0.50_ 1617 Mail Service Center Event Duration(hours):,N/A_(only if applcable—see permit;) Raleigh,North Carolina 27699-16I7 (if more than one storm event was sampled) y �l. Date_11/12/19 Total Event Precipitation(inches): 0.48 Event Duration(hours):N/A (only if applicable—see permit.) Date 12/23/2019 l€ Total Event Precipitation(Inches): 1.09 . Event Duration(hours):N/A (only ifapp icable—see permit.) "I certify,under penalty of law,that this docun4ent and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the. best of my knowledge and belief,true,accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonnfent for knowing violations." 1,1.1 , i z y 2 4 l (Signature of Permittee) l (Date) Form SWU-247,last revised 2/2/2012 ge2of2 STORMWATER DISCHARGE OUTFALL (SDO) SEMI-ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year_ 2019 , Individual NPDES Permit No. NCS000101 Certificate of Coverage (COC) No. NCG This monitoring report summary of the calendar year should be kept on file on-site with the facility SPPP. Facility Name: _International Paper County: _Columbus Phone Number: (910)_362-4590 Total no. of SDOs monitored 4 Outfall No. B, E, I Is this outfall currently in Tier 2 (monitored monthly)? Yes n No x Was this outfall ever in Tier 2 (monitored monthly) during the past year? Outfalls B, I Yes x ❑No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? N/A Enough consecutive samples below benchmarks to decrease frequency x Received approval from DWQ to reduce monitoring frequency xl I Other (_] Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No x Parameter, (units) Total Rainfall, inches Benchmark N/A COD BOD TSS pH Date Sample 120 mg/L 3O In04 100 A 6-9 so Collected, mm/dd/yy B 11/12/2019 35 4 4 6.7 E 7/3/2019 135* 20 7 6.7 I 7/3/2019 136* 14 227* 8.2 SWU-264-Generic-1lnec2012 STORMWATER DISCHARGE OUTFALL (SDO) SEMI-ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2019 Individual NPDES Permit No. NCS000101 Certificate of Coverage (COC) No. NCG I This monitoring report summary of the calendar year should be kept on file on-site with the facility SPPP. Facility Name: _International Paper County: _Columbus Phone Number: (910)_362-4590 Total no. of SDOs monitored 4 Outfall No. B, E, I Is this outfall currently in Tier 2 (monitored monthly)? Yes (l No x Was this outfall ever in Tier 2 (monitored monthly) during the past year? Outfalls B, I Yes x ❑No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? N/A Enough consecutive samples below benchmarks to decrease frequency xl j Received approval from DWQ to reduce monitoring frequency xn Other Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No x Parameter, (units) Total Rainfall, inches Benchmark N/A COD BOO T;';; pH Date Sample '120 mglL 30 mglL '100rrro/I y-.6-9 -. su Collected, mm/dd/yy B 11/12/2019 35 4 4 6.7 E 7/3/2019 135* 20 7 6.7 I 7/3/2019 136* 14 227* 8.2 SWU-264-Generic-13Dec2012 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate. and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." • Signature L� Date I/�� z� For questions, contact your local Regional Office: DWQ Regional Office Contact Information: 41) .y II e 71 Fayothwitlo • WW1 ngton ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville,NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704)663-1699 (910)433-3300 RALEIGH REGIONAL OFFICE WASHINGTON REGIONAL OFFICE WILMINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington, NC 27889 Wilmington,NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTON-SALEM REGIONAL OFFICE CENTRAL OFFICE 585 Waughtown Street 1617 Mail Service Center "To preserve.protect Winston-Salem, NC 27107 Raleigh, NC 27699-16171 and enhance (336) 771-5000 (919) 807-6300 North Carolina's water..." SWU-264-Generic-13f)ec2012 STORMWATER DISCHARGE CALCULATION WORKSHEET Fall 2019 Total Impervious Unpaved Area Total Gallons Gallons from Gallons from Discharge Outfall Total Acres Area (Ac) (Ac) Rainfall (in)* Rainfall Impervious Area Unpaved Area (MG) Basin B 11/12/19 0.57 0.34 0.23 0.48 89147 53175 35971 0.09 Basin E 7/3/19 4.04 1.01 3.03 0.5 658174 164544 493631 0.66 Basin 17/3/19 1.88 1.78 0.1 0.5 306279 289988 16291 0.31 Basin 17/3/19 1 88 1.78 0.1 0.5 306279 289988 16291 0.31 Basin T 7/3/19 1.88 1.78 0.1 0.5 306279 289988 16291 0.31 Basin T 11/12/19 0.95 0.9 0.05 0.48 148578 140758 7820 0.15 Basin T 12/23/19 0.95 0.9 0.05 1.09 337396 319638 17758 0.34 _ * Rainfall measured by onsite rain gauge. Sample information (sampling must begin within 30 minutes of runoff flow) Time Time event Time sample Time event Time sample Time event sample Outfall began collected Outfall began collected Outfall began collected Basin B 11/12/19 approx. 17:45 Basin E 7/3/19 approx. 14:20 Basin 17/3/19 approx. 14:07 Basin T 7/3/19 approx. 1:57pm Basin T 11/12/19 4:20 PM Basin T 12/23/19 3:10:00 pm* 15:20 Sample Collection Date: 7/3/2019 11/12/2019 12/23/2019 Approx. Duration of Event: n/a Previous Repr. Event and Amount: 6/7/19, 0.36" 11/7/19, 0.86" 12/13/19, .083" sq.ft/acre=43,560 *The 12/23/19 Basin T rain event started on 12/22, with a very light, constant drizzle. 0.3" fell overnight and all day,just keeping the ground wet but no flow. Late in the day rain increased enough to allow light runoff for a sample. Overnight on 12/23, rain increased to 1.09"for the total, 2-day rain event. Prepared by: i„tj :- t ;. '. `‘•. • ...ALI certify that this information is true and accurate to the best of my knowledge. Signature and date: .t) .C 91_e I .2Q9, y() \C1 SET UP '*.��t SET UP END(5-DAY) Met II setup time: U -Composite date: READ Bii:-•. C(i k''° DAY: v r._, DAY: '`'ue Metter-.,al read: ..l•fS/56-SS I _ Grab date: 1 ` -lc\ CALC BY:** TIME el--`-) TIME: SSO (•Clmg1L) Buffered water temp (•C): ;IQ,,c\ CHECKED BY:** DATE: -1-y_1a DATE: -.1_Cy_1c1 •All samples are incubated immediately after initial U.O.and read immediately upon removal from incubator. bop i 6� SAMPLE ID GM BOTTLE ID lAi.E SAMPLE INITIAL D.O. 5-DAY D.O. OXYGEN l MLS SEED IN ROD j (mgR) (mg/Il LEFT(moil) NUTRIENT PILLOWS: 11 LITERS WATER: BOTTLES: CCn,,,tr• jM1I �1(p t Avg.Uesue lim .. ._..._._. DILUTION H2O 300 7 , •, •,, •x ,. I E DILUTION H2O 300 s ,,, 75 1 S -(a[/ „ 11 tD mg+L SEED CORR. AVERAGE org pH f adi pH SAMPLE POLYSEED y,S 25 .6-z)a 3 .4C 4•s-ej SOD(moil) g L (mgfL) BOD(man) (s.u.) ! (s.u.) TEMP('cl -POLYSEED Ir\ 20 4/.,1,4 ''Z 9 4 C5 POLYSEED r 15 -i:,?1'1, 5. 3�1 2. et 4- i — nga. GGA �,\ B ? 4 /0 ! h.' ,20±3*C GGA "l,• 6 . 1. ( is /‘) -1, GGA 6 ;�`� �1`# f( l L 11111111E— SEEDED BLANK •),r 7 5 3\ 4•3Z 0-1 1.0 mg/L #1 CLARIFIER C _...-4 i t -t-t - • n j .J.- 7 - (-. -1 .1 - a 1 L 1 EH.Duplicates must agree within 30% #1 CLARIFIER C z ry - �' - -' -( /x / #2 CLARIFIER C s 1 •.t 15,2'- 2.'S' C. 9-G ,f 4 `k.1 \O d-1 5 EFFLUENT #2 CLARIFIER C 1 I 0 0 3 -3,`-j 3.24 5, // /y, SAMPLE TIME:Gam-6am ASB C �ti �'� , _1 i %,' •r ,, r,`.. PRESERVATION CC): 1,1� ASB C , 1 -1.-I 3 , n(., .', NEW BAY C 411 `O,r�` .l Co S C 5 ?il z, 1-DAY BOD(unseeded)&51 NEW BAY C I.') a('i $.I'1"-/s S.i 4 ' . it Volume Eff.Used(mL) ..lej SOUTH BAYp G ' - r i-- _ i'.. 7. '' i 4- 'L.' / ; l • ..1.4..) IN y-1. RESULTS SOUTH BAY G -,;�`� t \( , `t.0 ,. :s. , • -- -4 = - / r MP1 ," " �S.L\ EFFLUENT C -.5k . '15 `3.4o 4• CI 3. SS s // -(c\ - \et-1 2 1•a-1 . EFFLUENT C 1) SO Is,4y 5.54 Z-y'C 12 3 1 ?<5 EFFLUENT C •3y'1 4 0 ¶5.L1a S 8 5 2.-o 4 / 4 4../¢ ,- t. EFFLUENT DUP C -,Lej`e2 c-,, `t 44 5.5 t0 2. /( Eff dup%DIFFERENCE 5 ' ; i AVG FOR EFF 1 MI f, ( Nitrate/Nitrite Test Strips Nitrate(NO3) Nitrite(NO2) Effluent S.Bay ""f gptr WISMR D 0 Baron. D.O.Atter DRIFT CHECK , -0.= - (mg;y (mg'L) New Bay Standard Method 52108.2011(5-Day BOO Test). G=GRAB C=COMPOSITE -" NOTES: :1 0 CurF..1 I certify \by this signature that this document is true,accurate,and complete /to the best of my knowledge . 4(0 I� r) e to / C1 tv( (c— \ ^_ I C&J X 1_\AA(\ lI-c\-kcA �c.;c mot'' �> C;�:� .f�tl'� ANALYST PRII` SAME ANALYST SIGNATURE G . rri, SET UP B 1 �l SET UP END (5-DAY) Mt ;.al setup: Composite date: 1- S" READ BY: ** C W l;,j DAY: - v„„„,,j f-3 DAY: `\ ,,c -, Meter cal read: -_ Grab date: "1 ..`1 1 c1 CALC BY: ** TIME: -175 TIME: 5-4 4-- Buffered water temp: CHECKED BY: ** DATE: n_V_\r\ DATE: - 1.c\ \' .All samples are incubated immediately after initial D.O.and read immediately upon removal from incubator. bugs ij,�l ,) r ,C, J. SAMPLE ID GJC BOTTLE ID MC8 SAMPLE INITIAL D.O. 5-DAY D.O. OXYGEN MLb seen IN mg/I mgn USED mgn NUTRIENT PILLOWS: LITERS WATER: SAMPLES:-) Avg. DILUTION H2O 300 1 II 11 s e to t Unseeded dilution water,_<0.2 mg/L QUALITY ASSURANCE DILUTION H2O 300 Seed Controls,0.6-1.0 mg/L. Unseeded dilution water,5.0.20 mgll SEED CORR. SOD mgn AVERAGE org pH ad)pH I SAMPLESeed Controls,0.6-1.0 m L POLYSEED 25 SOD NO TEMP ~POLYSEED 20 Dilution H2O DO,7.5-9.0 mg/L — POLYSEED 15 All Other Bottles DO,7-9 mg/L GGA 6 Dii.H2O 8 Sample Temperature,20±3'C GGA 6 Adj.pH,7.0-7.2 s.u. GGA 6 I Y GGA Std.,198*/-30.5 mg1L • "pc 51 v"‘41 DO,Deplete 2.0 mgll 8 Residual 1.0 mgJL _ G .6 -l�-f,\ , _ l;A..1 — 6-Z4 ;L-s'c J .—' `o _—Eff.Duplicates must agroe within 31W._ G `-1 r1r, - i�- 2,0 r0 �.“0 II' EFFLUENT G ', _, f .1- 'CI ? i SAMPLE TIME: G c� '}r PRESERVATION: G 7 tc c ,of ar 3, ? 541 _ C 3 -1 .;. G 9 o rlc) `it 4.!S 4.' , / 1-DAY BOO (unseeded) G c ,-- I,L6 '-).?tit i c i 1 III Volume Eff. Used: G 'SS.yZ '� `34 -' .-f• I ' (4. IN RESULTS G i r C C,rc) 3.51 �.� 7 1 \ t — - t1 } �.4I 5-oC, Z`t- 2 G ". 3 �- . _ -• ` • 7>.LC--) -I. i I / 2 2 a _ ,>r ti 4 `_ 5 - — G DILUTION WATER CHECK ' CHECK Standard Method 5210E-2011(5-Day BOO Test). G=GRAB C=COMPOSITE NOTES: I certify by this signature that this document is true,accurate,and complete to the best of my knowledge \} I,,, �C\_4.5 I C LJ l e;t.y. ` .- '� --, - I C. CJ IIY,,�/, -0-1-lc\ 1 fl-C\-AI ANALYST PRINTED NAME At iT SIGNATURE j� DATE SET UP '*CL'thra SET UP END(5-DAY) Mel aI setup time: -- ci I Composite date: )(-12_ 1 CI) READ BY:-** c '..uKro,y DAY: v`e t.. DAY: nr(.1n Metei cal read: 22`1 (c' Grab date:_ I 1- (3 - 1 61 CALC BY: ** TIME: (? TIME: sad C/mg/L) Buffered water temp(•C): 1 L CHECKED BY: •* DATE: 1,\-\3.\,cal DATE: 11- I '- 1 'All samples are incubated immediately after initial D.O.and read immediately upon removal from incubator. begs e"j-1 Vr h t�.n'1.-c 'C') I UFZ SAMPLE tD k...... BOTTLE ID MLS SAMPLE r INITIAL O.O. 5-DAY D.O. OXYGEN ,�y MLS SEED IN SOD (mgn) (mg/II LEFT(malt) NUTRIENT PILLOWS:6/,L(�.1 (r^✓ LITERS WATER: 12 BOTTLES: 4 DILUTION H2O �300 • Avg.Unneeded {{ DILUTION H2O 300 i 1- 'is 20 mglL ti5 2 S 2. �Sorg p SEED CORR. AVERAGE R ad)pH SAMPLE 1/� POLYSEED 3 3 3 25 - (mg1L) BOO(mgn) BOD m tl (s.o.) Is.u.t TEMP ci GI• )`o g� POLYSEED 33 5 20 s;-L f- ;.-75 q Q- eig1L POLYSEED 3 3\0 15 `• — — mgrL 1 n-23 G3 3 f t tto . `j�5� GGA i 6 i •• i l (1'(•-� 4. 7O :, sot3c GGA ,ayK 6 ) , GGA 6 ,1 1 . - SEEDED BLANK 3(r,0 4 c1 20 4. ,c-- O.h-IL ,1 1.0 mg/L #1 CLARIFIER C I 5 i l / - i i I Eff.Duplicates must agree within 30% #1 CLARIFIER C _3c) #2 CLARIFIER C 12 C. 3 S.1 2 3.' O 4•22 3 "y'5 IQ•L 1 C, 20 u EFFLUENT #2 CLARIFIER C /43 Z_ 5S. 14 4�.b- 3-z C� 3 5i• -jt, SAMPLE TIME:6am-6am ASB C = — I d`. -1 PRESERVATION (•C): 0, ASB C ,l, N NEW BAY C ‘, I 7)0 -C 3 'iO 4. is 2.5 :7- 1 — ?To 1-DAY BOD(unseeded) )cs- NEW BAY C (3 2.0 q•12. ; - 2 2.‘t6 2 4 Volume Eft Used(mL) , SOUTH BAY G -)Cl 1 • IN S$•Z c"j RESULTS CW(c;\ SOUTH BAY G 11 -,• 1 C) -t EFFLUENT C �-3 - SC' g 24 q.U 4 `f-Z3 746 -c, l i 2 C q C, EFFLUENT C 3 4c �•z--3 - 3.4C l 3 G Cu _ EFFLUENT C C•4 30 +"-2s `s 4�� 2 1-4- /5 — 1 4 1 EFFLUENT DUP C i 4 C <-z4 4- '4 .3•)L / el Eff dup%DIFFERENCE 5 AVG FOR EFF 1 ." I- r _ 4 Z ,3 Nitrate/Nitrite Test Strips r.- Nitrate(NO3)Nitrite(NO2) Effluent i MINS same within S. Bay 0.0 Before D After DRIFT CHECK G.2 m9lL /L) CZ -Ci rn �- A New Bay Standard Method 5210E-2011(S-Day BOO Test). 6-GRAB C=COMPOSITE NOTES: I certify by this signature that this document is true,accurate,and complete to the best of my knowledge C 1 e,nh .� Ct,,,i<,w•- / C w"<<�e - CL_1 /C0-y /( t,-.i ,,-, !HH, iG 111-ih -rc, F7 S 4 ANALYST PRIN. AME ANALYST SIGNATURE DI SET UP B' [1_l,,j 640)c SET UP END(5-DAY) Mt cal setup: _ Composite date:_ A( '} __- READ BY: ** C.t,„/K,.,o,f DAY: W e` DAY: th diA Meter cal read: Grab date: I(- 12 -I cr1 CALC BY: ** TIME: TIME: Buffered water temp:_ CHECKED BY: ** DATE: i t_i 3-la DATE: /I-{ir_%0\ *All samples are incubated immediately after initial D.O.and read immediately upon removal from incubator. bugs 1v1 Li et 1 ei f�• 2 R INITIAL D.O. S-0AY D.O. OXYGEN ) mt-'�_=�um SAMPLE ID OIC BOTTLE ID MLS SAMPLE ( mg/I mgA USED mgA NUTRIENT PILLOWS:G I,S 4.b ) LITERS WATER: (-2-- SAMPLES: 4-. 0 DILUTION H2O 300 Avg. Unseeded dilution water,=c 0.2 mg/L Unseeded QUALITY ASSURANCE DILUTION H2O 300 Seed Controls,0.6.1.0 mg1L Unsoodod dilution wator,5 0.20 mg/L AVERAGE SAMPLE POLYSEED 25 SEED CORR. BOO mgll BOD mg/ org pH adj pH TEMP Seed Controls,0.6-1.0 mg/L POLYSEED 20 I} Dilution H2O DO,7.5.9.0 mglL POLYSEED 15 I — — All Other Bottles DO,7-9 mg/L GGA 6 — Dif.H2O&Sample Temperature,20 t 3'C GGA i 6 (I Adj.pH,7.0-7.2 s.u. GGA 6 ( GGA Std.,198+l-30.5 mg/L DO,Deplete 2.0 mg/L&Residual 1.0 mg/L 'f y /A, G I(0 _ f-4-5 �-3-L .4 elf- 3. $ - ?> - L It I 1...1 . , Eff.Duplicates must agree within 30% 1‘ G 1'3 (e, 150 SS•3-? I-3- S(o 2. 7-1- .I- —. EFFLUENT t\ G 1 C%'i /f':' `n 1 t•.i 2 i -, SAMPLE TIME: r' 'f 0 t i `i ii- 1 b Cr- '. 4- - — PRESERVATION: -'.-1 i G 1( 2_ /cv Ss c icl S,,45 3. s - `f Ti { --- 14, 7- l Z_+ S 'F -�-3. (,,. 23 1- S4 7- 1-DAY BOD (unseeded) i , G f { ,tl , it - (4. ..'6 / < l`�� = Volume Eff. Used: t: G 'L. ,c( I� ' * �-�' * IN RESULTS G r 1 2 -G 3 4 G 5 G G ' DILUTION WATER CHECK CHECK Standard Method 5210E-2011(5-Day BOB Test). G=GRAB C=COMPOSITE NOTES: I certify by this signature that this document is true,accurate, and complete to the best of my knowledge e 4tl<iz(C))12 /C t..J '/-!0'7 -• C IA-,K.--ele I C Li/l ,-- _ II-CI-ICI I //-i i--(ei ANALYST PRINTED NAME A ST SIGNATURE DATE mu SET UP **r f,,S SET UP END (5-DAY) Me( al setup time: `A Composite date: 1.1-;.)-�`\c1 READ BY: ** C(ij DAY:"1 ki P-) DAY: `w N. Meter cal read: 3"1 I .51 Grab date: 1 1-a-\-\QI CALC BY: ** TIME:U 5 TIME: 5 04- ('Clmg/L) Buffered water temp('C): a\ CHECKED BY:** DATE: \a_may_0 DATE: 1 a-.- t_ \C) .All samples are incubated immediately after initial D.O.and read immediately upon removal from incubator. bugs �) O �- SAMPLE ID WC BOTTLE ID MLS SAMPLE INITIAL D.O. 5.DAY O.O. OXYGEN MLS SEED IN BOD (mg/I) IIIMA LEFT(mg11) NUTRIENT PILLOWS: (.0 rr\_kLI,,,1 LITERS WATER: \'. ....... BOTTLES: 4 DILUTION H2O 300 Avg.Unsaeded ' l.\t� SS. C.' mglL QUALITY ASSURANCE DILUTION H2O 300 'e ,to 4S Unseeded dilution water,<_0.20 mg!L POLYSEED 25 5 (C( 1 SEED /LI BOO(mg/I) AVERAGE 1 erg pH ad)pH SAMPLE Seed Controls,0.6-CO mglL �� L{ (mglL) BOD lmga) (so.) (s.u.) TEMP CO POLYSEED `a(r. 20 c0-0-\ .?C 4.24 ?'•y Dilution H2O DO,7.5-9.0 mgiL POLYSEED --�\C\ 15 �,\.\3 rj_`I 5S 2•ci rj c All Other Bottles DO,7-9 mg/L GGA 1' + 6 Ljr� ) Dil.H2O&Sample Temperature,20 2 3'C GGA \-, 6 lam- l,.. ; •1 • + Ad).pH,7.0-7.2 s.u. GGA t,.` 6 `?. 3 +- , I • , i r GGA Std.,198 st.30.5 mg/L SEEDED BLANK L11 4 lit 4 L-k -.. S r 0.c` j DO,Deplete 2.0 mg(L&Residual 1.0 mg/L #1 CLARIFIER C •- Lk ` - . . Eff.Duplicates must agree within 30% #1 CLARIFIER C } ,. ti - ';,y„- #2 CLARIFIER C -15 ">j , L)\ Gl 34 SS Uq _ °i I, -'. 0 r�li3.0 EFFLUENT #2 CLARIFIER C ��j 14� 51 S 3.Z 3C . ..1_ SAMPLE TIME: 6am-6am ASB C i 1 '7 , (4, I 1 • . PRESERVATION ('C): 1,(,', ASB C --1,,, : . ) Z J NEW BAY C -T.\ LA 0 ac,\ .3 S' 4-..7( -' \ R,\ --1 fs t,,-a_ 1-DAY SOD(unseeded)' NEW BAY C 1e\ _)L ')(F `i.( 1-(.C 't7 1 Volume EN.Used(mL) cs(,, SOUTH BAY G +;.V(.. + IN 6,y9 RESULTS SOUTH BAY G `?-L\C- _ . n t- 1 -7,�a- EFFLUENT C %,(r, -]L� �,Sp -5 2S 3-2-S I'_., 1 - EFFLUENT C ckcj \--\C; ci.,y..') C -1O 2, 71- 15 3 C-- �Lr EFFLUENT C 31(, 2 (-- _ .___ i EFFLUENT DUP C " 1 y C, c-(7,,L1 i ;. ( Z., e )4 Elf dup%DIFFERENCE 5 > -1— AVG FOR EFF f f3 C,,5 Nitrate/Nitrite Test Strips Nitrate(NO3)Nitrite(NO2) Effluent S.Bay ^` limier.within P.O B.fora D.O.Attar DRIFT CHECK :o 2 mg L ( ) Cb,t.\a (mgt.) 1 , ' . New Bay Standard Method 52108-2011,k5-Day BOO Tont). O•GRAB C•COMPOSITE NOTES: :- 5 �Q- I certify by this signature that this document is true,accurate,and complete to the best of my knowledge . SG ---.,n� '>b\v5 / C .tl<, < .._ �`_-,c; ') / ('k,K,(h y7-' \o.-a�1-19 11.- f(- ANALYST PRINT^"'AME ANALYST SIGNATURE ' D1"' SET UP B', c-c- SET UP END (5-DAY) Mt cal setup: Composite date: READ BY: ** (' tt;ilc/iie DAY: T„,, DAY:S",., Meter cal read: Grab date: 1 .)-•'J-\° CALC BY: ** TIME: \v5 TIME: Buffered water temp: CHECKED BY: ** DATE: _a„..k_to\ DATE: , _D,Q\ \C1 'All samples are incubated immediately after initial(� D.O.and read immediately upon removal from incubator. bugs �� (""-C- — —7S t ML)...1)10 MLS SAMPLE A a- - SAMPLE ID WC 60TTLti INITIAL D.O. 5-DAY D.O. OXYGEN �'L7 JCCV IIY mg?' mgil USED mg/I NUTRIENT PILLOWS: LITERS WATER: SAMPLES: y DILUTION H2O 300 Any. Unseeded dilution water,_<0.2 mg/L QUALITY ASSURANCE Unseeded DILUTION H2O 300 Seed Controls,0.6-1.0 mg/L Unseeded dilution water,5 0.20 mg/L —+ — -- -t AVERAGE SAMPLE POLYSEED 25 SEED CORR. BOD mg/I erg pH adj pH Seed Controls,0.6-1.0 mg/L BOO mgll TEMP POLYSEED 20 Dilution H2O DO,7.5-9.0 mg/L POLYSEED 15 Ali Other Bottles DO,7-9 mg/L GGA 6 Dil.H2O 8 Sample Temperature,20±3'C GGA 6 Adj.pH,7.0-7.2 s.u. GGA 6 GGA Std.,198+1-30,5 mg/L DO,Deplete 2.0 mg/L 8 Residual 1.0 mg/L ,.3\ I1/4.1 ` G , 1 CQ \ -3 %l 0 2.l I ,.U 7- ( ',y - a1 y EN.Duplicates must agree within 30% G4 ��L1 \C S� 3. �� I / .- EFFLUENT G r. \` , :e'.r. H ' '1•( , SAMPLE TIME: G . < �L� _ ., •? PRESERVATION: G G 1-DAY BOD (unseeded) G Volume Eff. Used: -- -- IN RESULTS G 1 _ G 2 G 3 1 Th 4 _ G 5 G G r - DILUTION WATERL I CHECK - CHECK Standard Method 5210E-2011(5-Day ROD Test). G-GRAS C..COMPOSITE NOTES: I certify by this signature that this document is true,accurate,and complete to the best of my knowledge \'i_r<DT\e`j I C tA.‘l rC ( .)4ah- `� ,,^) / C G:(l s...,,,z 1 D-�`.‘-19 I 1;--3.(\-VI ANALYST PRINTED NAME ANALYST SIGNATURE DATE DAILY TOTAL SUSPENDED SOLIDS FORM • •SAMPLE INDENTIFIGATION t4,Kj k�S . FILTERING START TIME`1 5 SAMPLE INDENTIFIGATION y 05'l CZS\�� FILTERING 1 DATE COLLECTED \• -,-\ FILTERING STOP TIME DATE COLLECTED —1-3"1cl FILTERING STOP TIME402— DATEANALTZED —`A—Al DATE ANALYZED ---1-4.- �n-\-l. FILTERING TIME MUST BE FILTERING TIME MUST BE -SAMPLEVOLUME USED c.\l��O mis e10MINUTES •SAMPLE VOLUME USED p,.'1 � mis o10M9t'UTES- TIME 1NIOUT OF OVI�F'1o7 1 tt 'Time In oven must be greaterthan or equal to drying TIME IN/OUT OF OVEN 01 5I C 'Time In ovon must ha grater than sr man to driing ,,� umaot most rodent erIt1L sl drying study time of most recent annual diying Addy TIME WEIGHED ,l 7G.,_\q TIME WEIGHED - ,, �� 'T' r DRY SAMPLE VIT.+PAPER WT.+4O+�� a DRY SAMPLEWT+PAPERWE::�( y 1c B DRIED RESIDUE MUST BE DRY FILTER PAPERWF A14Vile It DRIED RESIDUE MUST DRYFILTER PAPER WT ey1 t'. g BETWEEN 0.0025 g.and BE-BETWEEN 0.002E g 0.2000 g DR/Y.samPPLEIwr a On -5 o End 0.200D g ^DRY SAMPLE WT c c. k- - g FACTOR(F) 1000 I \�-.%�L. R N FACTOR In 1000 1 p` C' = du_of ranlpie mL of sample CALCULATIONS: CALCULATIONS: r G TOTAL SUSPENDED SOLIDS.- 1000.' ` C;Cr), '-2? = TOTAL SUSPENDED SOURS= 1000' - .....,1-. " dOt'I J`,1 =-dg,- 7 F wLgrams mgll F wtgrams 041 SAMPLE INDENT1FICATON \+.?N'S i'1%4 \ FILTERNG STARTTIMEC'Ib3 SAMPLE MNDENTIF-CATION FILTERING START TIME. • ........,___,.., C Qtc._. -._...,....�� _...._..__ .._ _...... ...._.,..,_..-._..._.D47E COLLECTED...."."."'"1��T,'�'.."'. fIL7ERINGSTOP TIME-t�'.' .� .._...'�_.,DATS'COli:ECTED � FILTERING STOP TIME'.... DATE ANALYZED "LI-I°'T FILTERING-TIME MUST BE DATE ANALYZED FILTERING TIME MUST BE SAMPLE VOLUME USEDL A.� ntis <1 D MINUTES SAMPLE VOLUME USED egg r10 MINUTES TIME WIDUT OF OVE1 D1 I - • eM Oreirinuit beeleoier than or equal to drying TIME IN/OUT OF OVEN 1 'The In oven most be groetcr than or equal to drying time of most rowin annual drying study time of most recent annual drying surly LIME WEIGHED I3� TIME WEIGHED "$y2. DRY SAMPLE WY 4 PAPER W7 i Lk%S;,.. g DRY SAMPLE TNT+PAPER PIT g . DRIED.RESIDUE MUST BE DRY TILTER PAPER WT sti -l1 g DRIED RESIDUE MUST DRY FILTER PAPER WT g BETWEEN 0.0025 g-and BE BETWEEN 0.0025 g 0:2000 g DRY SAMPLE WT e V l:,—1 1.\ g, and 0.2000 g DRY SAMPLE WI g FACTOR IF) 1000 I UI.j = G3 FACTOR IF) -1d0d 1 = mL ot.sample m L of sample CALCULATIONS; I CALCULATIONS: TOTAL SUSPENDED SOLIDS= 1000" \1 + 'O 1I 1 = 33(. TOTAL SUSPENDED SOLIDS= 1001) ` rs 1 F wtgrains mon F wtgrams. mgH SAMPLE INDENTIFICATION FILTERING START TIME SAMPLE-INDENTIFIGATION FILTERING START TIME- PATE COLLECTED FILTERING STOP TIME DATE COLLECTED FILTERING STOP TIME- DATE ANALYZED DATE ANALYZED FILTERING TIME MUST BE FILTERING TIME MUST BE SAMPLE VOLUME USED runs <TO MINUTES SAMPLE VOLUME USED mis <YD MINUTES TIME INIOUT OF OMEN I 71mo In oven must be.gtmoter than oregaai to drying TIME INIOUT OF OVEN. i Tine in oven must bo greaterthan nregdaI to drying Alm of MOO recant annual drying study — time ci most recent 0nm+at drying study TIME WEIGHED. TIME WEIGHED DRY SAMPLE WI+PAPER WT 9 DRY SAMPLE WT*PAPER WY t1 DRIED RESIDUE MUST B£ DRY FILTER PAPER WY g DRIED RESIDUE.M UST- PRY-FILTER PAPER WT g BETWEEN 0.0025 g and SE BETWEEN 0,0025 g 0.2000 g ORY SAMPLE WT g and 0,2000 g DRY SAMPLE INT g FACTOR(F) 1000. 1 = FACTOR(F) 1000 I -- mL ote mple mL or sempIO CALCULATIONS: CALCULATIONS: TOTAL-SUSPENDED SOLIDS= 1000.' ` u TOTAL SUSPENDED SOUDS0 1000-' ' F wtgranls men -F wtg/arns mgH Classy caiibratlon Wetght g Balanca.YYt g Effluent Duplicates Must Be Run Each-Tuesday %DIFFERENCEs,12(Absoluta{EFF -EFFDUP I()F(EFP *EFFDUP. 1100s EFFLUENT DUPLICATES MUST AGREE WITHIN 2595 DIFFERENCE I certify by thfs signature that this document is trun,:acourate,and tornplete to tho best of • my knowledge. PRINTED NAME OF ANALYST SIGNATURE Of"ANALYST Standard Mot/rods,2510O.2077IAndeuua) DAILY TOTAL SUSPENDED SOLIDS !FORM .\ SAMPLE ENDENTIFtCATION i](a S•l.t\i �. Ff4TER!NG START TTME�A' SAMPLE INDENTIFICATIOE �:QS\. ..J FILTERING START TIMI D 1s. DATE COLLECTED• 1V`1.rt'1 FILTERING STOP TINE '‘.1.-. DATE COLLECTED .1 l .I►:—.`-I[j FRIERING STOP TIME '4. DATE ANALYZED 11-13—1°1 DATE ANALYZED 1 II'�1 -'1 FILTERING TIME MUST BE FILTERING TIME MUST BE SAMPLE VOLUME USED 40 0 rots c 1a MINUTES SAMPLE VOLUME USED p atb c 10 MINUTES TIME W10Ur OF OVF3u' �4'� ! • t /f� / "Time In oven must be greater than°rental to dying TIME IN7O11T OF OVEN 'C'T .1 U.5a•Ttme In oven must be gm-ate:1110n or equal to dryIrm lL tlmp atmest record-annual drying study time of most mattannual dryingstudy • TIME WEIGHED (1- I TIME WEIGHED. IZ3 A. DRY SAMPLE WT+PAPER WT t 2--q3: a DRY SAMPLE WT+PAPER NR P O 4 DRIED RESIDUE MUST BE DRY FILTER PAPER WT +-1.1'_'wl-g DRIED RESIDUE MUST DRY KILTER PAPER WT - g BETWEEN 0.0025 g and 3Y% DE DETWEEN 0.0325 g ��31_ 0.2000 g DRY SANPtd Wt • �Z 1 a and 0.2000 g DRY SAMPLE WT +c6Z.1 e p FACTORIPI 1000 f 4.4-)C, _. 14011 FACTORIFT toga I 5cc> = a, ml of sampio mL of sample CALCULATIONS: `(-t,. k CALCULATIONS: - TOTALSUJPENDED SOLIDS= 1000' t,.(e1 • = TOTAL SUSF1RUEEDSDUDS= 1aRo" • .02Cco _ of3 , F wt.grams mqn F yrtgrams mail SAMPLE iNDEldiiFICAT1ON FILMING START TIME SAMPLEINDENTW7CATION FILTERING START TIME ...DATE COLLF�C'CEb..-,.•<..••...•.r.�.-....,r--r,-r-e:r--e•s-..v-FILTPfOpSG STOP'fT10��._,,._.. . __ �IEC FILTERING STOP TIME DATE ANALYZED FILTERING TiME MUST BE DATE ANALYZED FILTERING TIME MUST SE SAMPLE VOLUME USED mis G 10 MINUTES SAMPLE VOLUME USED into <10 MINUTES TIME INIOUTOF OVEN / limo In oven must be greater then or aqua/to drying Tim INccUT OF OVEN f 'lima In even mast be graaierthan or equal to drying amo of rem-1 recent annual drying study time et most recant annual drying study TIME Wk1GHE0 TIME WEIGHED CRY SAMPLE WT r PAPER WT g DRY SAMPLE 011+PAPER WT g DRIED RESIDUE MUST BE DRY FILTER PAPER(VT g DRIED RESIDUE MUST DRY FILTER PAPER WT BETWEEN 0.0025 g and BE BETWEEN 0.0025 9 0 0.2000 g DRY SAMPLE WT 0 and 0.2000 g DRY SAMPLE WT g t FACTOR(P) lass / _ FACTOR(FI 1000 / = mL of sompta mL o[sample CALCUL;TOMS: CALCULATIONSI. TOTAL SUSPENDS]SOUDSv 1000' - TOTAL SUSPENDED SOLIDS= 10u0' F WLgrams mgf p _ wLgrams man SAMPLE INCENTIFICA7fON FILTERING START TINE SAMPLE INDENTIFICATION FILTERING START TIME ___.i • DATE COLLECTED FILTERING STOP TIME DATE COLLECTED FILTERING STOP TIME. , DATE ANALYZED DATE ANALYZED t • FILTERING TIME MUST BE FILTERING TIME MUST BE I SAMPLE VOLUME.USED Ws <10 MINUTES SAMPLE VOLUME USED rots <10 MINUTES TIME IN/OUT OF.OVEN / "Time In a von must be greater than aregmd to drying .Tttne In oven must ba water than or I toQ 1 1 time at most recant sbuuai drying strey TIME t1111D11T OF OVEN ! 0 qua drying Unto of most regent annual drylOg stady TIME WEIGHED TIME WEIGHED I DRY SAMPLE WT+PAPERWI g DRY SAMPLE WI,PAPER WT a DRIED RESIDUE MUST BE DRY FILTER PAPER WT g DRIED RESIDUE MUST PRY FILTER PAPER WT BETWEEN 00025 g and SE BETWEEN 0.0025 g 0 0.2000g DRY SAMPLE WT g and 0.2000g DRYSAMPLEWT E FACTOR(F) IC00 / = FACTOR(F) 1000 I mL et samptn rnL of sample CALCULATIONS: CALCULATIONS: TOTAL SUSPENDED SOLDS= 1000• " = TOTAL SUSPENDED SOLIDS• 1000• • - F wtgrams me ` F r vn.praits mgI Classy C.iitbr lec Weight g 9alanee Wt g Effluent Duplicates Must BD Run Each Tuesday %DIFFERENCE n 12(Abseiute(EFF -5FF DUP }}f(EPF +EFF DUP I.100 e EFFLUENT DUPLICATES MUST AGREE WITHIN 25%DIFFERENCE I certify by this slgoature that this docimient Is true,accurate,and complete to the best of my knowledge. PRINTED NAME OF ANALYST SIGNATURE OF ANALYST Srmtdard Mono*,25d01i.Zot1(Agu000s) nr DAILY TOTAL SUSPENDED SOLIDS FORM JSAMPLE 1NDENTIFICA1IDN -\\ !�S t N T FILTERING START TIME 901 SAMPLE INDENT1FICATION FILTERING START TIME DATE COLLECTED I O.•A.)—VA FILTERING STOP TIME CI 3 DATE COLLECTED FILTERING STOP TIME DATE ANALYZED ,a.a.Lk',g DATE ANALYZED FILTERING TIME MUST BE FILTERING TIME MUST SE SAMPLE VOLUME USED C70 tom <10 MINUTES SAMPLE VOLUME USED cols <10 MINUTES TIME INIOUT OF OVEN sL,'-", 1`tt'LC) •Time In oven must be grouter than or aqua;to drying TIME INIOUT OF OVEN I •Tlma In boon must be greater then or equal to drying time of most moors annual drying study �av �j y time of most mount annual drying study n Irv, TIME WEIGHED \\ 1 TIME WEIGHED DRY SAMPLE VJT+PAPER WT •lAy 1(.0 g DRY SAMPLE WT+PAPERWr g DRIED RESIDUE MUST BE DRY FILTER PAPER WT .LI�S g DRIED RESIDUE MUST BETWEEN 0.0025 g and (e U 1' BE BETWEEN 0.0025 g DRY FILTER PAPER WT g 0.2000 g DRY SAMPLE WT •0, g and 0.2000 g DRY SAMPLE WT g FACTOR(F) 1000 I '7)0 O = a FACTOR(F) 1000/ _ mL of sample OIL of sample CALCULATIONS: 11 Q CALCULATIONS: TOTAL SUSPENDED SOLIDS= 1000• • •L\(.0,,"V — J� TOTAL SUSPENDED SOLIDS. 1000' • _ F wt.granls mg0 F vtgrams mg0 SAMPLE Il.DENTIFlCATION FILTERING START TIME SAMPLE INOENTIFICATION FILTERING START TIME DATE COLLECTED FILTERING STOP TIME DATE COLLECTED FILTERING STOP TIME DATE ANALYZED DATE ANALYZED FILTERING TIME MUST BE FILTERING TIME MUST BE SAMPLE VOLUME USED min <10 MINUTES SAMPLE VOLUME USED mis <10 MINUTES TIME INIOUT OF OVEN I •Time In oven must be grantor than or equal to drying TIME INIOUT OF OVEN I 'Time In oven must tut greater than or equal to drying timo of most meets annual drying study time of mast recent annual drying study OTIS WEIGHED TIME WEIGHED DRY SAMPLE WT+PAPER MT g DRY SAMPLE WI+PAPER WT g DRIED RESIDUE MUST BE DRY FILTER PAPER WT g DRIED RESIDUE MUST DRY FILTER PAPER WT BETWEEN 0.0025 g and BE BETWEEN 0.0025 g g 0.2000 g DRY SAMPLE WT a and 0.2000 g DRY SAMPLE WT g FACTOR IF/ 1000 I = FACTOR IF) 1000 I — mL orrampto mL of sample CALCULATIONS: CALCULATIONS: TOTAL SUSPENDED sOUDS' logo• — TOTAL SUSPENDED SOLIDS= 1000• • = F wtgratrr mg/I F vrtgromo mga SAMPLE INDENTIFICATION FILTERING START TIME SAMPLE INDENTTFICATION FILTERING START TIME DATE COLLECTED FILTERING STOP TIME DATE COLLECTED FILTERING STOP TIME DATE ANALYZED DATE ANALYZED FILTERING TIME MUST SE FILTERING TIME MUST BE SAMPLE VOLUME USED reds <10 MINUTES SAMPLE VOLUME USED mis <10 MINUTES , TIME IN/OUT OF OVEN I "Ttmn In oven mist bo greater than or equal to drying TIME IN/OUT OF OVEN I `Time In oven must bo greater than or equal to drying time of most recent annul drying study Umo of most recent annual dryIng study j TIME WEIGHED TIME WEIGHED DRY SAMPLE WT+PAPER WT g DRY SAMPLE WT+PAPER WT g DRIED RESIDUE MUST BE D BETWEEN 0.0025 g and RY FILTER PAPER WT g DRIED RESIDUE MUST DRY FILTER PAPER WT g BE BETWEEN 0.0025 g 0.2000g DRY SAMPLE WT g and 0.2000g DRY SAMPLE INT g FACTOR(F) 1000 / = FACTOR(F) 1000 I = mL of sample mL of smote CALCULATIONS: CALCULATIONS: TOTAL SUSPENDED SOLIDS. 1000' ' = TOTAL SUSPENDED SOUDs• 1000• • = i F wt.gmms mgll F wtgrams mg0 + Close S Calibration Weight 1,00 Ulu g nuance w ,00 t , 06 g Effluent Duplicates Must Be Run Each Tuesday %DIFFERENCE•(2(Absohne(EFF .EFF DUP )I)t(EPP +OFF OUP ___I 1g0 o EFFLUENT DUPLICATES MUST AGREE WITHIN 25%DIFFERENCE t I certify by this signature that this document Is true,accurate,and complete to the best of my knowlodge. PRINTED NAME OF ANALYST (P' Cam, _ SIGNATURE OF ANALYST�,....__ � _ Standard Method.;25400-201!(Aqueous) Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 l3owsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info(ienvironmentalchemists.com International Paper-Riegelwood Date of Report: Jul 18, 2019 865 John L. Riegel Road Customer PO#: Riegelwood NC 28456 Customer ID: 09010017 Attention: Report#: 2019-11052 Project ID: Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-28412 Site: Basin E 7/3/2019 2:20 PM Water KCB/KWF Test Method Results Date Analyzed COD SM 5220D 135 mg/L 07/12/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-28413 Site: Basin I 7/3/2019 2:07 PM Water KCB/KWF Test Method Results Date Analyzed COD SM 5220D 136 mg/L 07/12/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-28414 Site: Basin T 7/3/2019 1:57 PM Water KCB/KWF Test Method Results Date Analyzed COD SM 5220D 168 mg/L 07/12/2019 Comment: n, 1 Reviewed by: RakkA, V),j , E-MAILED JUL 19 2019 Report#:: 2019-11052 Page 1 of 1 ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way envirochem Wilmington,NC 28405 Sample Collection and Chain of Custody Phone: (910)392-0223 .x-�`�ice Cove z o��` w�\\°& •Q-`)' 0.\ - : fie' .c"'� Fax (910) 392.4424 Client: IP Riegelwood c\‘0- tc \ C j ccN..... waAA,,e,ct c,<- ccecY:\- ec,.�c� Collected By: \'\c(; I `-ter Report No: e'i - 1 l • Sample Type: I= Influent, E=Effluent, W=Well, ST=Stream,, SO =Soil, SL= Sludge Other:' \ i -'---,'-'cc- ,�`„��pr A Collection = „ •h n PRESERVATION az Sample Identification 9 E 0. a L •� 'L .a E.. o ° o ct. .c E o c c o w ANALYSIS REQUESTED z DATE TIME TEMP u (5 v u z m x m z �. c \)),�,,N __ ass X ins. N \ .S-y "Ie Transfer Relinquished By: Date/Time Received By: Date/Time 1. �� \`� ,-- �' / `� �/41(� a` ' ' -3-' ? -- — 2. V Temperature when Received: '3- L- Accepted: Z jec d: Resample Reque eO: Delivered By: - (/� Received By:!' , C Date: --7 y l t 5 Time: 1 : 3 : /1-- Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.57(12 Lab/Fax 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info(kienvironmentalchemists.com International Paper-Riegelwood Date of Report: Nov 29, 2019 865 John L. Riegel Road Customer PO#: Riegelwood NC 28456 Customer ID: 09010017 Attention. Wallace Coverdale Report#: 2019-19489 Project ID: Stormwater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-49474 Site: Basin 8 11/15/2019 5:45 PM Water W. Coverdale Test Method Results Date Analyzed COD SM 5220D 35 mg/L 11/25/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-49475 Site: Basin T 11/15/2019 4:20 PM Water W Coverdale Test Method Results Date Analyzed COD SM 5220D 168 mg/L 11/25/2019 Comment: Reviewed by: Va,pW, aLtaul)' E-MAILED DEC 02 2019 Report*: 2019.19489 Page 1 of 1 6602 ill Way ENVIRONMENTAL CHEMISTS, I N C OFFICE 9r10 392-0223 F'Ax 910-392 4424 Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY is iaL iNiiLL-it S ''1=O t'k rll T ; .3k H 5)(IC __A__--,-)CLIENT: `'1; n\�iY,c, . \ ��oc PROJECT NAME: cvv�\ t�TtZ / e REPORT NO: (q- C9M ADDRESS: `gins j„,,.,, ,Q.ct\ Zc�,c-� _, CONTACT NAME: tack.\\per._ C�v e.� Q PO NO: \ J �\Q Q.•.Jocxi \Q yc'S(3 REPORT TO: V 0c1/4.\\c,.c�. �_ov€c-o\E_ PHONE/FAX:c\\L -'Yca-- '3 k(.2 COPY TO:j.i -dlit- .(4,;(,ci)AL'i l 4';tr .CC;::i email:\v0.\\o.t;2_.Q.`oEs o�E ‘)c.�cLc .Cc-N•r, Sampled By: , - ( o i ;c l.a l,� SAMPLE TYPE: I=Influent, E = Effluent, W=Well, ST=Stream, SO=Soil, SL=Sludge, Other: Collection ;, c�_ c PRESERVATION n = J ow Sample Identification E ,. 0 22 o f i o 0 o w ANALYSIS REQUESTED N ° 0 a u 'J z z = i x z o Date Time Temp v F� i1) A fttl �; w �G_ G GZ CO C tifitlA TK I I-1•iq ` :zbjr/{ L S .0l C (P' / C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G I Transfer Relinquished By: Date/Time e By: Date/Time / 1. C \A-' `,c-`: //- 11 tci [ V/4/ %/2C 2. _1 r _ Temperature when Received: I�5 Accepted: YY Re' Resample Requested:/ .3t5.79 Delivered By: Received By: Date: `l�-C°t-Zel Time: Comments: TURNAROUND: Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com International Paper-Riegelwood Date of Report: Dec 31, 2019 865 John L. Riegel Road Customer PO#: Riegelwood NC 28456 Customer ID: 09010017 Attention: Wallace Coverdale Report#: 2019-21672 Project ID: Stormwater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-54905 Site: Basin T 12/23/2019 3:20 PM Water Wallace Coverdale Test Method Results Date Analyzed COD SM 5220D 68 mg/L 12/27/2019 Comment: Vatik Reviewed by: 014DA E-MAILED DEC 31 2019 Report#• 2019.21672 Page 1 of 1 c '` 6602 Windmill Way Wilmington,NC 28405 . .:.i:; w :) ENVIRONMENTAL ENTALCHEMpSTSINC .4„: 4,� ti OFFICE:910-392-0223 FAX 910-392-4424 Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCOHHS:OLS CERTIFICATION#37729 Infe@envlronmentalchemists.com COLLECTION AND CHAIN OF CUSTODY C /c}LL. i0P c,i.fi UT C b , f'£f,7? 1 CLIENT: -.7 .e,zs:\ PROJECT NAME: tsrrt\wt C?-- REPORT NO: (7 - al 6, 7 a— ADDRESS: `z(oS Join \--, ,Q*_ ~Z„e,� CONTACT NAME:Wit\oc_._Cc�vQiic Q PO NO: �'.p_ \.,-ac-scs + \C ayc"sto REPORT TO: W��,\c Q Csecrc�-\� PHONE/FAX:ct\u-'3Coa-'�5 COPY TO: email:wa.1. QCWZA \ \ c c C�� Sampled By: (///)Pi L(! C�C.( ` 1 L SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil, SL=Sludge, Other: STO RAY Collection _ _ c PRESERVATION Sample Identification 1 P, a a 0 `o o a m CA w a M x n E o a E o i °a o u, ANALYSIS REQUESTED Time Temp y " z x Stekl- C g SSN j 1 -?3iv r?op _,-m.B031 _W,612. c9G ;Cot L, —p-J-- P t G G C P 1 _ G G { C P G G C P G G C P _ G G C P G G C P G G 1 C P G G C P G G Transfer _ ��dd , (,�Rellin�quished By: ' y� Date/Time Received By: / Date/Time I. lb Cl (.��V� txL� ' ?,sue 1 p` ( /r - /4(2 3/q !1:/O.4"- 2. Temperature when Received: 114, j' C.., Accepted: Rejected: Resample Rested: )elivered By: 11--, << 7fReceived By: i - Date:_ /d-frL S'r r' Time: /02 7U7' comments: TURNAROUND: