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HomeMy WebLinkAboutNCG030466_MONITORING INFO_20181108STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V DOC TYPE p HISTORICAL FILE f� MONITORING REPORTS DOC DATE ❑ YYYYMMDD Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03'o`'i ,G 16 SAMPLE COLLECTION YEAR 9-0,$ FACILITY NAME F_eton C,_orpof e; hotn SAMPLE PERIOD ❑ Jan -June [Z July -Dec COUNTY "nCo mlo-e or ❑ Monthly' (month) PERSON COLLECTING SAMPLES Mark $udg _ RECEIVEDIIsCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water Supply [:]SA LABORATORYYAC.�_ AAgk1j -� c--,l Lab Cert. #! 19z d- Lio NOV 0 8 zole ❑Other Comments on sample collection or analysis: CENTRAL Fil_e5 7VVR SEECT1Qn PLEASE REMEMBER TO SIGN ON PAGES ZAND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, IncheS3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L DOS 1ar'to 18 3. a1" G. Q m 7. 3 .00C,9 M L 4.005 m L o6W4 rK 1L 45.0 on,51L NIP, 00;L to to l% 3.1 m L T'i c.coc, fm)IL c-,005 (%11L oaa.q rVIL 45-0 M L O03 to t0 $ 3,-A1" a.q MI/1— T3 c.005 L �.005 L .ctioo .r9.0 rh A 00{-1 t0 Lo 8 3.�\'' 4,'-1 a c.005 n+ L c,aofs L o55'i cS.4 rn L NIP, ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'For sampling periods with no discharge at any single outfali, you must still submit this discharge monitoring report `with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes.. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample I(for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics MO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." U2 r[/[ (fit Z x— Name (Prin ame) Title (Print tit e to 2 r� (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,,<PQL, Non -detect, ND, or.other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit,'etc. in mg/L. ' Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period:2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail on original and one copy of this DMR, including all ;;No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there ar_q--,igpificant pena,/es for s/mitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 e P (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalytical wwwpwelab&c= October 24, 2018 Mark Buda Eaton 221 Heywood Rd. Arden, NC 28704 RE: Project: Stormwater 10102018 Pace Project No.: 92402892 Dear Mark Buda: Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7178 Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 acmnalj6cal wm.p8celabs.mm Project: Stormwater 10102018 Pace Project No.: 92402892 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Charlotte Certification Ms 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NEL.AP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certiflcation #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 UrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAna4 tical www.pacefabswrn SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: Stormwater 10102018 92402892 Analytes Lab lD Sample ID Method Analysts Reported Laboratory 92402892001 OUTFALL 001 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 MVC 1 PASI-A EPA 9040C RLO 1 PASI-A 92402892002 OUTFALL 002 EPA 1664E JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 MVC 1 PASI-A EPA 9040C RLO 1 PASI-A 92402892003 OUTFALL 003 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 MVC 1 PASI-A EPA 9040C RLO 1 PASI-A 92402892004 OUTFALL 004 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 MVC 1 PASI-A EPA 9040C RLO 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical wyvw.pecefabs.c�rrt ANALYTICAL RESULTS Project: Stormwater 10102018 Pace Project No.: 92402892 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 288114 (828)254-7176 Sample: OUTFALL 001 LabID: 92402892001 Collected: 10/10/18 06:30 Received: 10/10/18 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Oil and Grease 200.7 MET IC Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 9040 pH pH at 25 Degrees C Analytical Method: EPA 1664B ND mg1L 5.0 1 10/24/18 01:13 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 6.9 ug/L 5.0 1 10/11/18 04A0 10/14/18 22:10 7440-50-8 ND ug/L 5.0 1 10/11/18 04:10 10/14/18 22:10 7439-92-1 56.6 ug/L 10.0 1 10/11/18 04:10 10/14/18 22:10 7440-66-6 Analytical Method: SM 254OD-2011 6.2 mg1L 2.8 1 10112/1816:49 Analytical Method: EPA 9040C 6.9 Sid. Units 0.10 1 10/12/18 07:04 Q Sample: OUTFALL 002 Lab ID: 92402892002 Collected: 10/10/18 06:30 Received: 10/10/18 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 9040 pH pH at 25 Degrees C Analytical Method: EPA 1664B ND mg1L 5.0 1 10/24/18 01:14 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 ND ug/L 5.0 1 10/11/18 04:10 10/14/18 22:13 7440-50-8 ND ug/L 5.0 1 10/11/18 04:10 10/14/18 22A3 7439-92-1 22.7 ug/L 10.0 1 10/11/18 04:10 10/14/18 22:13 7440-66-6 Analytical Method: SM 2540D-2011 3.9 ' mg/L 2.9 1 10/12/1816:50 Analytical Method: EPA 9040C 6.0 Std. Units 0,10 1 10/12/18 07:23 Q Sample: OUTFALL 003 Lab ID: 92402892003 Collected: 10/10/18 06:30 Received: 10/10/18 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Oil and Grease 200.7 MET IC Copper Lead Zinc Date: 10/24/2018 05:27 PM Analytical Method: EPA 1664B ND mg1L 5.0 1 10/24/18 01:15 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 ND ug/L 5.0 1 10/11/18 04:10 10/14/18 22:16 7440-50-8 ND ug1L 5.0 1 10/11/18 04:10 10/14/18 22:16 7439-92-1 40.0 ug/L 10.0 1 10/11/18 04:10 10/14/18 22:16 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 lacieAnalj4icale Kww.pacelabs.com ANALYTICAL RESULTS Project: Stormwater 10102018 Pace Project No.: 92402892 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 003 Lab ID: 92402892003 Collected: 10/10/18 06:30 Received: 10110118 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND n1g1L 2.9 1 10/12/18 16:50 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 5.6 Std. Units 0.10 1 10/12/18 07:37 Q Sample: OUTFALL 004 Parameters Lab ID: 92402892004 Collected: 1011Oil 8 06:30 Results Units Report Limit DF Received: 1011 Oil 15:15 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mglL 5.0 1 10/24/18 01:15 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper ND ug1L 5.0 1 10/11/18 04:10 10/14/18 22:19 7440-50-8 Lead ND uglL 5.0 1 10111/18 04:10 10/14/18 22:19 7439-92-1 Zinc 55.4 uglL 10.0 1 10/11/18 04:10 10/14/18 22:19 7440-65-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 6.4 mg1L 5.6 i 10/12/18 16:50 J(D6) 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 5.8 Sid. Units 0.10 1 10/12/18 07:48 Q REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2018 05:27 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalyticar tnrw.pecelabs.corm QUALITY CONTROL DATA Project: Stormwater 10102018 Pace Project No.: 92402892 QC Batch: 437929 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples. 92402892001, 92402892002, 92402892003, 92402892004 METHOD BLANK: 2407907 Matrix: Water Associated Lab Samples: 924028920D1, 92402892002, 92402892003, 92402892004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 4.8 10/24/18 01:12 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2407908 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 38.5 35.8 93 78-114 MATRIX SPIKE SAMPLE: 2407909 35423719002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 13.5 40 51.3 94 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2018 05:27 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 acmnalytical. wwwpacalabs.com QUALITY CONTROL DATA Project: Stormwater 10102018 Pace Project No.: 92402892 QC Batch: 435624 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92402892001, 92402892002, 92402892003, 92402892004 METHOD BLANK: 2397556 Matrix: Water Associated Lab Samples: 92402892001, 92402892002, 92402892003, 92402892004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper uglL ND 5.0 10/14/18 20:23 Lead uglL ND 5.0 10/14/18 20:23 Zinc uglL ND 10.0 10/14/18 20:23 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2397557 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 504 101 85-115 Lead uglL 500 482 96 85-115 Zinc ug1L 500 490 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2397558 2397559 MS MSD 92402598002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 500 500 508 515 101 103 70-130 1 Lead uglL ND 500 500 485 492 97 98 70-130 1 Zinc ug1L 3,51 500 500 504 510 100 101 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2397560 2397561 MS MSD 92402936001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % ReC % Rec Limits RPD Qua] Copper uglL 36.0 500 500 580 580 109 109 70.130 0 Lead ug1L ND 500 500 484 482 97 96 70-130 0 Zinc uglL 60.0 500 500 629 631 114 114 70-130 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2018 05:27 PM without the written consent of Pace Analytical Services, LLG. Page 7 of 14 acmnalXical. tanrw.pacele6s.mm QUALITY CONTROL DATA Project: Stormwater 10102018 Pace Project No.: 92402892 QC Batch: 436046 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92402892001, 92402892002, 92402892003, 92402892004 METHOD BLANK: 2399591 Matrix: Water Associated Lab Samples: 92402892001, 92402892002, 92402892003, 92402892004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/12/18 16:47 LABORATORY CONTROL SAMPLE: Parameter 2399592 Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2399593 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2399594 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28a04 (828)254-7176 Spike LCS LCS % ReC Cone. Result % Rec Limits Qualifiers 250 234 94 90-110 92403211001 Dup Result Result RPD Qualifiers 172 166 4 92402892004 Dup Result Result RPD Qualifiers 6.4 12.0 61 J(D6) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2018 06:27 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 lacieAnalyticala trwwpaselabs.corrr QUALITY CONTROL DATA Project: Stormwater 10102018 Pace Project No.: 92402892 QC Batch: 435877 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92402892001, 92402892002, 92402892003, 92402892004 SAMPLE DUPLICATE: 2398807 92402801001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.3 7.3 0 Q Pace Analytical Services, LLC 2225 Riverside pr. Asheville, NO 28804 (82B)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an attemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2018 05:27 PM without the written consent of Pace Analytical Services, LLC. Page 9of14 Pace Analytical Services, LLC 2225 Riverside Dr. aceAnalytical Asheville, NC 28804 www.pwolabs.com (828)254-7176 QUALIFIERS Project: Stormwater 10102018 Pace Project No.: 92402892 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SVV846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Q Sample held beyond the accepted holding time. Sample was received outside EPA method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/2412018 05:27 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 14 aceAnalytical . W"4acelaacom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 10102018 Pace Project No.: 92402892 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample fD QC Batch Method QC Batch Analytical Method Analytical Batch 92402892001 OUTFALL 001 EPA1664B 437929 92402892002 OUTFALL 002 EPA1664B 437929 92402892003 OUTFALL 003 EPA 1664B 437929 92402892004 OUTFALL 004 EPA 1664B 437929 92402892001 OUTFALL 001 EPA 200.7 Rev 4.4 1994 435624 EPA 200.7 Rev 4.4 1994 435649 92402892002 OUTFALL 002 EPA 200.7 Rev 4.4 1994 435624 EPA 200.7 Rev 4.4 1994 435649 92402892003 OUTFALL 003 EPA 200.7 Rev 4A 1994 435624 EPA 200.7 Rev 4.4 1994 435649 92402892004 OUTFALL 004 EPA 200.7 Rev. 4.4 1994 435624 EPA 200.7 Rev 4.4 1994 435649 92402892001 OUTFALL 001 SM 254OD-2011 436046 92402892002 OUTFALL 002 SM 254OD-2011 436046 92402892003 OUTFALL 003 SM 254OD-2011 436046 92402892004 OUTFALL 004 SM 254OD-2011 436046 92402892001 OUTFALL 001 EPA 9040C 435877 92402892002 OUTFALL 002 EPA 9040C 435877 92402892003 OUTFALL 003 EPA 9040C 435877 92402892004 OUTFALL 004 EPA 9040C 435877 Date: 10/24/2018 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Document Name: Document Revised: February 7, 2018 e � aeek7alyfieal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: 1 F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving s rrtples: Ashevi9, Eden[:] Greenwood ❑ Huntersvi(le ❑ Raleigh❑ Mechanicsville[] Ci�gnt Name: Project #: Courier: ❑Fed Ex []UPS CUSPS 26ient ❑ Commercial ❑Pace ❑Other: Custody Seal Present? ❑Yes Intact? ❑Yes �f 0 Packing Material. ❑Bubble Wrap 12 ub8 bie Bags ❑None ❑ Other Thermometer: ❑IRGunType of Ice: �❑ et Blue �ljp: � Cooler Temp (°C): (i it 1 Correction Factor: Add/Subtract (°C) �^ Cooler Temp Corrected (°C): �— USDA Regulated Soil (p A, watersample) Did samples originate in quarantine zone within the United States: CA, NY, or SC (check maps)? nYes nNo Wa#:92402892 111111111111111 IN III 92402692 Date/Initials Person Exaln nAOCMents:Or- Biological Tissue From? [-]Yes []No [DNIA ❑None Temp should be above freezing to VC ❑Samples out of temp Criteria. Samples on Ice, Cooling process has begun Did samples originate from a foreign source (internationally, inrIndino Hawaii and Puerto RicoV MYes MNo Comments/Discrepancy: Chain of Custody Present? Ye ❑No ❑N/A 1. Samples Arrived within Hold Time? ❑Yes No [I N/A 2. Short Hold Time Analysis (<72 hr.)? (-]Yes -NNoq H/A 3. Rush Turn Around Time Requested? ❑Yes Na ❑N/A 4. Sufficient Volume? es ❑No [I N/A 5. Correct Contalnem Used? -Pace Containers Used? res es ❑No (:]No ❑N/A []N/A 6. Containers Intact? Yes ON. ❑N/A 7. Dissolved analysis: Samples Field filtered? ❑Yes 211. ONJA S. Sample Labels Match COC? -Includes Date/Tim Date/Time/ID/Analysis Matrix: +❑YYees 4,� f�/ V V "tl ,jTNo ❑N/A 9. o o C 5�1 I'J I �`!s O V) CO j�toolVt �tJ fist :J Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No ,,.}},.,j [N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []Yes [-]No ❑No N/A TN/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: M Date/Time: Project Manager SRF Review:' Field Data Required? ❑Yes ❑No Date: i(a IC Date: ! ! } Page 12 of 14 Document Name: Document Revised: February 7, 2018 aeeAnaly 6l Sam le Condition Upon Receipt(SCUR) Page I of 2 Document No.: Issuing Authority: + F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project ft verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC. LLHg "Bottom half of box is to list number of bottle Igo#:92402892 PM: CD1 Due Date: 10/24/18 CLIENT: 93-CutlerH E d — V �U 4 tir Z c, a) m a a J J E E ,n a .-1 N 7 0. 0. m m ICI 2 u m a E ❑ Yl 7 a m ? d a @ a .y a Q. CC!m V 2 a a E �n en 0. N 2 a O2 a J E o N z 6 m A W 1a Q a J E N a cc ~ 2 n Z n• J E ui ,Ny V a ccd a m Y o E Q1 v a� Z s E Q w - w ..-1 7 l7 N E Q `J - rl Y [7 Q U c, Q E o N 7 0 Q N v 2 N b E Q m H ve 0 Q V 2 v E Q J E a N C� 0 Q V U 2 z E o n ¢ m Q ID Q x ¢ O 7 E VO i 2 W O Q x Q O �. J E p p F l�7 2 7 a 0 i E 0 Y 7 0 7 a Rl a ¢ O > -' E O a 11' \ z oN M x m a N m y `p Y > Z Y ra � w x a rs .S m' te ? 4 m ?' E .-/ a to m i Z a C! m vi J E N A. h CP C; v O Z [J m a J E o Vl N C IYl Z N E d E o P •--I Q z 0 f0 N J E O N 7 d v ac c Q E O Q 1 ` � 1 1\N l i I T 1 11 I 3 y i ) 4 S 6 7 S 9 1D NN III I 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 9 Note: Whenever there Is a discrepancy affecting North Caraiina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 CHAIN -OF -CUSTODY Analytical Request Document ,PaceAna1Xica1' Chain -of -Custody is a LEGAL DOCUMENT - CompleIe all relevent fields LAB USE ONLY -Affix Workorder/Login Label Here or List Pace Workorder Number or MTJL Login Number Here r 0 ALL SHADED AREAS are for LAB USE ONLY m Company: Eatai't Billing Information: Address: all ale wood mad Container Preservative Type " Lab Project Managers Report To Q� 3 R r.n Ne a87064 �9L7L Email To: rnRf k bLAd � -if" " Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hy'roxIde, (5) zinc acetate, (6) methanol, (7) sodium bisulfate, a sodium thiasulrate, 91 hexane, (A) ascorbic acid, (B ammonium sulfate, (C) ammonium hydroxide, (0)TSP, (VI Unprescrvcd, (01 Other Copy To: Site. Collection Info/Address: Analyses Lab'Profile/Une: Customer Project Name/Number. �t 5t✓�mvgA.#ec Soto V�++i� State: County/City: Time Zane Collected: NG/ A('d-en [ ]PT] JMT[ ]CT [.'JET - Lab Sample Receipt, Checklist: Custody.Seals Present/Intact Y N NA Custody Signatures Present, Y N NA :Collector- Signature Present Y N NA Bottles Intact Y N NA `Coirect Bottles Y N NA Sufficient volume Y N NA Samples Received on Ice Y N NA -`vOA -. Headspace Acceptable, YN. NA , USDA' Requluted-Soila Y,N NA Samples in Holding Time' Y N NA Residual -Chlorine Present 'Y' N.NA Cl. Strips: ' sample pH Acceptable Y N NA pH. Strips: Sulfide Present Y N UA Lead Acetate Strips: LAB USE ONLY: Lab Sample # / Comments V�P • �` Phone:(83$) Cob-1-i`;a7 Email: Site/Facility ED 9: Compliance Monitoring? [ ]Yes [ ] No Collected By [print : M4+11- Purchase Order 4: Quote $11: DW PWS ID 0: DW Location Code: Colleqto By Isigna a}; Turnaround Date Required: Immediately Pace on Ice: (/4Yes 1 )No Sample Disposal: J-h Pisposeasappropriate [ ] Return J J Archive: ( ) Hold: Rush: [ I Same Day [ ] Next Day ( ] 2 Day [ ] 3 Day [ ] 4 Day [ [5 Day (Expedite Charges Apply) FitldTiltered (if applicable): [ ] Yes ( ] No Analysis: ' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (Si.), Oil (OLJ, Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix" Camp/ 1 Grab Collected (or Composite Start) Composite End Res CI p of Ctns Date Time Date Time Owt oo\ brie la to 0b30 3 -c9D 0,'r ao 3 Cn lb to to Sc o1.349 3 OD 6' — ooA Gr.b to 0' 4 0(030 3 .bp Customer Remarks / Special Conditions / Possible Hazards: 0tA001 ?LA, 7.3 0-to" Pli_ 7.K 0,4003 PH' -7.3 0L%t-0OW R', 72. Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (c72 hours): 'Y N -N/A tab Sample Temperature Info: Temp Blank Rem[ T /�Y N 1/01 L" Therm Ibis: . `[ z.I Cooler l Temp Upan Receipt: oC Cooler 1-Therm Corr, Factor: -i�oC -Cooler l Corrected Temp: oC �Ctimments:. Packing Material Used: Lab Tracking k: 2 3 3.13 51 Radchem sample(s) screened (<5O0 cpm]; Y.,� N NA Samples received via:- ' FEDEX UPS Client, Courier Pace Courier Relinquished /Com an(Signature)! Y CG`FC`!GL.f/ lane/Tp a:a Z: +v R eittveetdllby/Company: (Signature) {yi0h DIa}te/Tijm/e: log I� [�V MTJL LAB USE ONLY' Actlnum: Template; Prelogin: PM: PB: Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date%Time: Trip Blank Received: Y N NA HCL McOH TSP Other Relinquished by/ (Signature) Date/Time: Received by/Company: (Signature) Date/Time: Non Conformance(s): YES / NO Page: of: Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 O 'A (o- Co SAMPLE COLLECTION YEAR 020t 8 FACILITY NAME E O,t" N__ CQ! R9(-,Z '►0rN `;- t / SAMPLE PERIOD [oJan-June ❑ July -Dec COUNTY ZxyNcOmbe E li ED or El Monthly' (month) PERSON COLLECTING SAMPLES 1UN 13 zQ18 DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA LABORATORY ?^C,E Ar\-Ay-1'cAk Lab Cert. # I e2 t 40 ❑Zero -flow [:]Water Supply ❑SA Comments on sample collection or analysis: t'iwl�J I RAL FILES Other GVVJR SECTION Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> No discharge this period ?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks =__> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 05 0211S .3 a" `13.5 r+n [_ (D.9 .Otsy a► c.005 •rift. .00 1 J/L z5.0 m L. N A 00a o5 0$ is .3a" , % 4 Co .$ ,00(07 art L 4.006cn /t .oT5ZZ r4j IL c.J;.0 rn,3 IL. N A 003 05 0S (S .32" 25.E L G.c1 .005(a MA e-.005rn L .0c05 a+ /t. c5.0 rjIL N J'+ 00%4 05 O8 I S .311)" `AOM rn L �a. ,00(a& 4.Ooy L .13c. rn► L 45.0 in ZL N A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Nam (Print name) [ �. J �(tU T' t title �( Q U U (Sign (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, IUD, or.other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware hat thane significant p alties f r submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 � � 1 � - ) /4 /u (Signature o er i (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 r aceAnalj cal. WWW.Pecelabs.com May 21, 2018 Mark Buda Eaton 221 Heywood Rd. Arden, NC 28704 RE: Project: Stormwater 05082018 Pace Project No.: 92383992 Dear Mark Buda: Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (826)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on May 09, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincereiy, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 laneAnalXical' wwwpecaiabs com Project: Stormwater 05082018 Pace Project No,: 132383992 Pace Analytical Services, LLC 2225 Riverside Dr. t Asheville, NC 28804 (828)254-7178 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisia na/N ELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #� 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #; 37712 CERTIFICATIONS South Carolina Certification #; 99006001 Florida/NELAP Certification #; E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 r laceAnalytical" www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: Stunnwater 05082018 92383992 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92383992001 OUTFALL 1 EPA 166413 JMS 1 PASI-C EPA200.7 SH1 3 -PASI-A SM 2540D MVC 1 PASI-A EPA 9040 RLO 1 PASI-A 92383992002 OUTFALL 2 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D MVC 1 PASI-A EPA 9040 RLO 1 PASI-A 92383992003 OUTFALL 3 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D MVC 1 PASI-A EPA 9040 RLO 1 PASI-A 92383992004 OUTFALL 4 EPA 1664B JMS 1 PASI-C EPA 200.7 SH1 3 PASI-A SM 2540D MVC 1 PAS] -A EPA 9040 RLO 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 14 aceAnalytical WW..pecelahsmm ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 05082018 Pace Project No.: 92383992 Sample: OUTFALL 1 Lad ID: 92383992001 Collected: 05/08/18 17:30 Received: 05/09/18 13:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 5.0 1 05/21/18 05:44 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 18.4 uglL 5.0 1 05/16/18 04:55 05/19/18 00:33 7440-50-8 Lead ND uglL 5.0 1 05/16/18 04:55 05/19/18 0033 7439-92-1 Zinc 100 uglL 10.0 1 05/16/18 04:55 05/19/18 00:33 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 43.5 mglL 12.5 1 05/14/18 23:36 9040 pH Analytical Method: EPA 9040 pH 6.8 Std. Units 0.10 1 05/10/18 01:09 Q Sample: OUTFALL 2 Lab ID: 92383992002 Collected: 05/08/18 17:30 Received: 05/09/18 13:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 05/21/18 05A4 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 6.7 uglL 5.0 1 05/16/18 04:55 05/19/18 00:43 7440-50-8 Lead ND uglL 5.0 1 05/16/18 04:55 05/19/18 00:43 7439-92-1 Zinc 75.2 uglL 10.0 1 05/16/18 04:55 05/19/18 00:43 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 38.8 mg1L 10.0 1 05/14/18 23:36 9040 pH Analytical Method: EPA 9040 pH 6.3 Sid. Units 0.10 1 05/10/18 01:09 N Sample: OUTFALL 3 Parameters Lab ID: 92383992003 Collected: 05/08/18 17:30 Results Units Report Limit OF Received: 05/09/18 13:02 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 05/21/18 05:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA200.7 Copper 5.6 ug1L 5.0 1 05/16/18 04:55 05119/18 00:46 7440-50-8 Lead ND uglL 5.0 1 05/16/18 04:55 05/19/18 00:46 7439-92-1 Zinc 65.0 uglL 10.0 1 05/16/18 04:55 05/19/18 00:46 7440-66-6 Date: 0512112018 04:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 4 1 aceAnalytical a www.pacelabs.00m ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 05082018 Pace Project No.: 92383992 Sample: OUTFALL 3 Lab ID: 92383992003 Collected: 05108118 17:30 Received: 05/09/18 13:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 25.2 mg1L 10.0 1 05/14/18 23:37 9040 pH Analytical Method: EPA 9040 PH 5.8 Std. Units 0.10 1 05/10118 01:09 Q Sample: OUTFALL 4 Parameters Lab lD: 92383992004 Collected: 05/08/18 17:30 Results Units Report Limit DF Received: 05109118 13:02 Matrix: Water Prepared Analyzed CAS No. Qual HEM, oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 05/21/18 05:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 6.8 uglL 5.0 1 05/16/18 04:55 05/19/18 00:49 7440-50-8 Lead ND uglL 5.0 1 05/16/18 04:55 05/19/18 00:49 7439-92-1 Zinc 136 ug1L 10.0 1 05/16/18 04:55 05/19/18 00:49 7440-66-6 '540D Total Suspended Solids Analytical Method: SM 2540D .otal Suspended Solids 40.4 mglL 10.0 1 05/14/18 23:37 J(D6) 9040 pH Analytical Method: EPA 9040 pH 5.5 Std. Units 0.10 1 05/10/18 01:09 Q REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2018 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aoAnalXical "W..pacelabs.corn QUALITY CONTROL DATA Project: Stormwater 05082018 Pace Project No.: 92383992 QC Batch: 411537 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92363992004 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 METHOD BLANK: 2283247 Matrix: Water Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg]L ND 5.0 05/21/18 05:43 LABORATORY CONTROL SAMPLE: 2283248 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 38.5 37.6 98 78-114 MATRIX SPIKE SAMPLE: 2283249 35392422001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 1 A U 38.5 38.6 99 78-114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0512112018 04'.31 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 r aceAnalj cal www,eacehib&com QUALITY CONTROL DATA Project: Stormwater 05082018 Pace Project No.: 92383992 QC Batch: 410867 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 2003 MET Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 METHOD BLANK: 2279340 Matrix: Water Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 Biank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 05/19/18 00:12 Lead ug/L ND 5.0 05/19/18 00:12 Zinc ug1L ND 10.0 05/19/18 00:12 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7178 LABORATORY CONTROL. SAMPLE: 2279341 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 504 101 85-115 Lead ug1L 500 460 92 85-115 Zinc ug1L 500 458 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2279342 2279343 MS MSD 92383974001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Quat Copper ug/L 0.10 500 500 606 607 101 101 70-130 0 mg/L Lead ug/L ND 500 500 456 459 90 91 70-130 1 Zinc ug/L 0.24 500 500 686 686 88 88 70-130 0 mg1L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2279344 2279345 MS MSD 92384063001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0,023 500 500 539 539 103 103 70-130 0 mg1L Lead ug1L ND 500 500 457 464 91 93 70-130 1 Zinc ug1L 0.35 500 500 800 814 90 93 70-130 2 mg1L Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2018 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 a acmnalytica! trwwwpacak'r &o= QUALITY CONTROL DATA Project: Stormwater 05082018 Pace Project No.: 92383992 Pace Analytical Services, LLC 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 QC Batch: 410678 Analysis Method: SM 2540D QC Hatch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 METHOD BLANK: 2278289 Matrix: Water Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L NO 2.5 05/14/18 23:34 LABORATORY CONTROL SAMPLE: 2278290 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 254 102 90-110 SAMPLE DUPLICATE: 2278291 92383874001 Dup Parameter Units Result Result RFD Qualifiers Total Suspended Solids mglL 14.2 14.6 3 SAMPLE DUPLICATE: 2278292 92383992004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 40.4 47.6 16 J(D6) Results presented on this page are In the units indicated by the "units" column except where an alterrtale unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in foil. Date: 05/21/2018 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 r aceAnalytircal Nnvwpecelabscarr QUALITY CONTROL DATA Project: 5tormwater 05082018 Pace Project No.: 92383992 QC Batch: 410064 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92383992001, 92383992002, 92383992003, 92383992004 SAMPLE DUPLICATE: 2275050 92384122002 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 7.0 7.0 0 Q Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2018 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 acmnalXical wwwpacwiabs.com QUALIFIERS Project: Stormwater 05082018 Pace Project No.: 92383992 DEFINITIONS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count MDL -Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydra7ine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylon4rile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NE LAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Q Sample held beyond the accepted holding time. Q Sample held beyond the accepted holding time. Analysis initiated more than 15 minutes after sample collection. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2018 0431 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 ' s aceAnalWical www.pec9Jab&cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLG 2225 Riverside Dr. Asheville, NC 28804 (828)254-7175 Project: Pace Project No.: Stormwater 05082018 92383992 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92383992001 OUTFALL 1 EPA 1664B 411537 92383992002 OUTFALL 2 EPA 1664B 411537 92383992003 OUTFALL 3 EPA 1664B 411537 92383992004 OUTFALL 4 EPA 1664B 411537 92383992001 OUTFALL 1 EPA 200.7 410867 EPA 200.7 411246 92383992002 OUTFALL 2 EPA 200.7 410867 EPA 200.7 411246 92383992003 OUTFALL 3 EPA 200.7 410867 EPA 200.7 411246 92383992004 OUTFALL 4 EPA 200.7 410867 EPA 200.7 411246 92383992001 OUTFALL 1 SM 2540D 410678 92383992002 OUTFALL 2 SM 2540D 41 DB78 92383992003 OUTFALL 3 SM 2540D 410678 92383992004 OUTFALL4 SM 2540D 410678 92333992001 OUTFALL 1 EPA 9040 410064 92383992002 OUTFALL 2 EPA 9040 410064 92383992003 OUTFALL 3 EPA 9040 410064 92383992004 OUTFALL 4 EPA 9040 410064 Date: 05/21/2018 04:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Document Name: Document Revised: February 7, 2018 �6011nalyucal' Sample condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-05-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving Sam S: Asheville2Eden❑ Greenwood ❑ Huntersville❑ Raleigh❑ Mechanicsville[] Client Name: Project f#: WO# . 92383992 Courier: ❑Fed Ex ❑UPS ❑USPS ❑ Commercial ❑Pace ❑Other. 92383992 Custody Seal Present? ❑Yes 'Pilo Seats Intact? ❑Yes l"' O L �lil I Date/initials Person xa ml g ntents: Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ Other Biological Tissue Fro n? Thermometer: ❑Yes ❑No N/A ❑IR Gun ID:ff�_ Type of Ice: Wet ❑Blue ❑None Cooler Temp (°C); Correction Factor: Add/Subtract (°C) ^ � Temp should be above freezing to 6°C Cooler Temp Corrected (° C' : I Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Sail N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes FIND Includins!Hawahand Puerto Rico)?❑Yes DN. Comments/Discrepancy: Chain of Custody Present? Q<LE1N0 ❑N/A 1. Samples Arrived within Hold Time? es No ❑NIA 2. Short Hold Time Analysis (c72 hr.)? []Yes ❑N/A 3. Rush Turn Around Time Requested? []Yes No ❑N/A A. Sufficient Volume? 2<s ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? es es ❑No ❑N/A El No El N/A 6. Containers Intact? es ❑No [_]N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes No El N/A 8. Sample Labels Match COC? includes Date/Time/ID/Analysis Matrix: i, J��� 1 Yes �d`� Nn ❑NIA 9•� �Q-� �;Sj3 �Yl C Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes _ -[--].Yes ❑No �]N/A ❑Na UN/A 11. COMMENTS/SAMPLE DISCREPANCY i CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? ❑Yes []No Lot ID of split containers: Date: /iel ` Date: 5 "O Page 12 of 14 w 0 41 b A O D ry o_ R 2 m m z C A �n C- w +� rt g w � m m rt r � o 7 � m a O C -S N A a � Ln to � C 3 ro f° O. a v in M � d � o' fD A 3 w o a -0 D. -0 N 6 xt N F+ O c0 W til dl � A W N N Itemff SP4U-125 mL Plastic Unpreserved (N/A) (CI-) BP3U-25D mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) J" BP1U•1 liter Plastic Unpreserved (N/A) I BP45-125 mL Plastic H2504 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 21 OP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (Cl-) WGPU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) AGSH-1liter Amber HCl (pH <2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AGSS-1 Iiter Amber H2SO4 (pH < 2) AG35.250 mL Amber H2504 (p H < 2) AG3A(DG3A)-250 mLAmber NH4Ci (N/A)(CI-) DG9H-4D mL VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U- G mL VOA Unp (NIA) DGSP-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A - lab) SP2T-250 ml. Sterile Plastic (N/A -lab) zz BP3A-250 mL Plastic (NH2)2SO4 (93-9.7) AGOU-100 mL Amber Unpreserved vials (N/A) VSGU-20 mL Scintillation vials (N/A) D69U-40 mL Amber Unpreserved vials (N/A) -t7 a rfl 2t H m 0 1 O to . . CA) 1 (L/ / �! C C 2 m \�� W m a N w t 00 CHAIN-OF-CUSTC 1 Analytical Request Document w PaceAnalyhr al The Chain -of -Custody is a LEGAL DOCUMENT. All relevant Gelds must be completed accumtely. T www.pacele6s.roni a Section A Section B Section C Page; N of Required Client Information: Company: Required Project lnformalion Invoice Information: 196 2361 Te: Attention: E.4 to ex"" M ask.. �udLq Address:2z y U 4� Copy To: Company Namei REGULATORY AGENCY Aram mL ,t ill) y OW L Address: r NPDES F- GROUNDWATER (— DRINKING WATER Email TA1�CI� Purchase Order No,; Paco Ouow f usr I-cRA f OTHER bud4 �g.CoM R ramncc, Fax: Project Name: SL-.�.mW q�� tv c Q �J Q 8 a� P''ra Protect PM Slt© Location nagar: l I Requested Duo DatorrAT: Project Number: P,acc Psofilo 0; Requested Analysis Filtered (YIN) Section D Matrix Codas z Rnqulrvd Client Inlorrnmion MATRIX f CODE —' COLLECTED Preservatives > Orinkinp Water DW o }+, O U n O WasBp water WW U COMPOSITE CaytvPOC.rSvw w z Product P i Qq- 1 10 r SAMPLE ID SoiUSotitl Oil SL OL . ! 0 n v a —0j a, (A-Z, 0.9 f : } Wipe Air WP AR w 0 — w ¢ c tu 411 F- c a Sampio IDs MUST BE UNI-QUE Tissue TS O U cy- W # other OT X F a- F a.� Q U U. m 2O � o m 2,{. � JS � � � 4 2 Ct O 0 0 � � _ f � C� f z N DATE TIME DATE TIME rn � a:S S Z Z Z O . 0 K ace Project No./ Lab I.O. OK� 11 & 5f S 18 t 3a 3 1 t t l O 2 Qu \i a G 58tTf 1730 3 a dL. tit LA er 518112 t-"0 3 t I I —ooul ADDITIONAL COMMENTS RELINQUISHED BY / AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS dt�ttl 1 H co.8 9 r� 3'�a 5 130� Z IJ Okt4�Ll 2 N� : (a. 8 0" ill 3 K : 6. 9 O Utz a N I-t: &.44 ORIGINAL SAMPLER NAME AND SIGNATURE u `o F a o PRINT Name of SAMPLER: M QS k �9 a 0 3 m z SIGNATURE of SAMPLER: DATE Signed 0� O ~ o: rn h [MMIDDIYY}: 'important Nolo: By signi?ig this form you are amep" Pace's NET 30 day payment lorms and ogreemg to fate charges of 1.5% per month for any irrvoices not paid ws hin 3D days. F-ALL-0-020rev.07, 15-May-2007 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 " Date submitted CERTIFICATE OF COVERAGE NO. NCG03 0 .4. (o (o FACILITY NAME Eakt`0r% COC-Poratlon COUNTY 13ur\r_or+n61e PERSON COLLECTING SAMPLES M�►c4c �udG► LABORATORY ?,, e. A \0Ay;C,1kV Lab"Cert. # 12 + 40 Comments onAample collection or analysis: R4►��11 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD 0 Jan -June '2 July -Dec or ❑ Monthlyi_ (month) ISC�AAG TO CLASS ❑ORW. ❑HQW ❑Trout ❑PNA RECD OCT 0 ��11 ❑Zero -flow ❑Water Supply [:]SA ❑Other CENTRAL FILES DWR SCCTiOi`10LEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period:' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks =__> _ - 100 mg/L or 50 mg/L .6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L . 1 mg/L t 08%31 a I,.o�' (0.0 m 1L T.3 c.005 MS IL e-.006 r� L. 1-_a1 r.L <5.0 M5 IL K/P. .7 05131111 �.02'' �0�.8 rL (Q.4{ 4.p06 MIL4.006 M31L .013toc% e- M rt%3 IL N/A 3 os 31 tT 10 �' c 23 ns /4 6 .? c .005 <:oo s, L . a 2H m 1a. a m L N P ' Monthly sampling (instead of semi-annual). must begin with .the second consecutive benchmark ekceedance for the sarn.e parameter at the same outfall. Z For sampling periods with no discharge at any single outfall,.youymust still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Uhattende4sites may'be.eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water..classifications'where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to'sample (for, metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469,22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the T70 monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no clumping of concentrated toxic organics into the stormwater or areas.which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." - Name (Print name) Title (Print kit (5i re) (Date Note: Results must be reporfed in numerical format:' Do not report Below Detection Limif, BDL, <PQL, Non -detect, ND, or"other similar norm -numerical format.'.When results are below the applicable limits, -they must be reported in the format: "<XX rWA/L'; where XX is the6Um6ical value of the detection limit, reporting limit, etc. d mg/L. - Note: If you report a sample value in excess of the. benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new'oil per month.' .0 No discharge this period?z outfall No. Date.Sample ' . ' 1 Collected -.(mo/dd/yr) - - 24-hour rainfall _ amount, 3 inches w. 'Non -polar O&G/TPH by EPA .1664'(S.GT-HEM] ;7. _ . "Total Suspended,5olids -pH- Benchmarks 15 mg/L :,= - '100.mg/L or 50 mg/L*. 6.'0 =9.0 su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must impleme,., Tier 1, Tier2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE -SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES RN07 IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this_DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage.the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware t here are significant penalties for submitting false information, including the possibility,of fines and imprisonment for knowing violations. !� 4 re of Permitteej Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalXical wwwpaeelabs.cnm September 18, 2017 Mark Buda Eaton 221 Heywood Rd. Arden,.NC 28704 RE: Project: Stormwater 0831,2017 Pace Project No.: 92353850 . Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Mark Buda: Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2.017. The'results relate only to the samples included.in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report: If you have any questions concerning this report, please feel free to contact me. Sincerely, - Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 (�5a'neAnalyticale www.pecelabs.cnm CERTIFICATIONS Project: Stormwater 08312017 Pace Project No.: 92353850 Charlotte Certification Ids 9800 KinceyAve. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianaINELAP Certification # LA170028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification Ids 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (82B)254-7176 Page 2 of 12 Pace Analytical Services, LLC aceMalXical 2225 Riverside Dr. Ashoville, NC 26804 W*WPetelada.cam (828)254-7176 SAMPLE ANALYTE COUNT Project: Stormwater 08312017 Pace Project No.: 92353850 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92353850001 Outfall 001 EPA 1664B JMS 1 PASI-C EPA 200.7 IDES 3 PASI-A SM 2540D SLB 1 PASI-A 92353850002 Outfall 002 EPA 1664B JMS 1 PASI-C EPA 200.7 DS 3 PASI-A SM 2540D SLB 1 PASI-A 92353850003 Outfall 003 EPA 1664B JMS 1 PASI-C EPA 2007 SER 3 PASI-A SM 2540D SLB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalj cal" Hww.peCOW&MM ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Slormwater 08312017 Pace. Project No.: 92353850 Sample: Outfall 001 Lab ID: 92353850001 Collected: 08/31/17 14:40 Received: 09/01/17 15:11 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 166413 Oil and Grease ND mg1L 5.0 1 09/15/17 05:44 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 50.0 10 09/13/17 21:20 09/16/17 1715 7440-50-B Lead ND ug1L 50.0 10 09/13/17 21:20 09/16/17 17:15 7439-92-1 Zinc ND uglL too 10 09/13/17 21:20 09/16/17 17:15 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids, 6.0 mg1L 2,8 1 09/06/17 10:46 Sample: Outfall 002 Lab ID: 92353850002 Collected: 08/31/17 14:40 Received: 09101117 15:11 Matrix: Water Parameters . Results Units Report Limit DF 'Prepared Analyzed CAS No. Qual HEM, Oil and.Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 09/15/17 05:44 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper. ND ug/L 5.0 1 09/13/17 21:20. 09/16117 1718 7440-50-8 Lead ND ug1L 5.0 1- 09/13/17 21:20 09/16/17 17:18 7439-92-1 Zinc 13.6 ug1L 10.0 1 09/13/17 21:20 09/16/17 17:18 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540❑ Total Suspended Solids ND mg/L 2.8 1 09/06/17 10:46 Sample: Outfall 003. Lab ID: 92353850003 Collected: 08/31117 14:40 Received: 09101117 15:11 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Analytical Method: EPA 1664E Oil -and Grease 12.2 mglL 5.0 1 09/15/17 05:44 200.7 MET ICP Analytical Method: EPA204.7 Preparation Method: EPA 200.7 Copper ND uglL 5.0 1 09/13/17 21:20 09/18/17 11:32 7440-50-8 Lead ND ug1L 5.0 1 09/13/17 21:20 09/18/17 11:32 7439-92-1 Zinc 24.0 ug1L 10.0 1 09/13/17 21:20 09/18/17 11:32 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 2.7 1 09/06/17 10:46 LI:It�illi�lY��ilfi�b3[+ic11,1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 (�Iaoftlj&i mm.Aacalabs com QUALITY CONTROL DATA Project: Stormwater 08312017 Pace Project No.: 92353850 QC Batch: 377847 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples.: 92353850001, 92353850002, 92353850003 METHOD BLANK: 2093523 Matrix: Water Associated Lab Samples: 92353850001, 92353850002. 92353850003 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, 128804 (828)254-7176 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 09/15/17 05:43' LABORATORY CONTROL SAMPLE: 2093524 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers. Oil and Grease mglL 40 37.3 . 93 78-114 MATRIX SPIKE SAMPLE: 2093525 92353910001 Spike MS MS % Rec Parameter Units Result Conc. Result %'Rec Limits Qualifiers Oil and Grease mglL ND 40 39.8 97 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 06:53 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 laneAnalyticale www.pacelahs.cbm QUALITY CONTROL DATA Project: Stormwater 08312017 Pace Project No.: 92353850 QC Batch: 377598 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92353850001, 92353850002, 92353850003 METHOD BLANK: 2092273 Matrix: Water Associated Lab Samples: 92353850001, 92353850002, 92353850003 Blank Reporting , Parameter Units Result Limit Analyzed Qualifiers Copper ug1L ND 5.0 09/16/17.16:17 Lead ug1L ND 5.0 09/16/1716:17 Zinc ug/L ND 10.0 09/161171617 LABORATORY CONTROL SAMPLE: 2092274 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 489 98 85 115 Lead ug/L 500 481 96 85-115 Zinc ug1L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2092275 2092276 MS MSD 92353725016 Spike Spike MS i MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec .% Rec Limits RPD Qua] Copper uglL 8.6 500 500 510 506 ' 100 99 70-130 1 Lead ug/L ND 500 500 453 446 •.90 89 70-130 2 Zinc ug1L ND 500 500 492 484 97 95 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2092277 2092278 MS MSD 92353850003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 433 430 86. 86 70-130 1 Lead ugIL. ND 500 500 432 ' 420 86 84 70-130 3 Zinc uglL 24.0 500 500 457 446 '87 84 70-130 3 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 05:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 (�15'cie Anafytical wwww.peoWabs.com QUALITY CONTROL DATA Project: Stormwater 08312017 Pace Project No.: 92353850 QC Batch: 376439 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92353850001, 92353850002, 92353850003 METHOD BLANK: 2085382 Matrix: Water Associated Lab Samples: 92353850001, 92353850002, 92353850003 ..Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Total Suspended Solids mg1L ND 2.5 09/06/17 10:45 LABORATORY CONTROL SAMPLE: 2085383 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE: 2085384 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2085385 Parameter Total Suspended Solids 92353841001 Dup Units Result Result mg1L 25.6 23.2 92353717001 Dup Units Result Result mg/L 12,3 11.0 RPD Qualifiers 10 J_(D6) RPD Qualifiers 11 J(D6) Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 09/18/2017 05:53 PM without the wntten consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalytical" »ww.pacefabs.oam QUALIFIERS Project: Stormwater 08312017 Pace Project No.: 92353850 DEFINITIONS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC -Too Numerous To Count MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit.. S -Surrogate 1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and -have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate . RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up' U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SVV846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-N itrosodi phenyl a mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration: Pace Analytical is TNI accredited. Contact your Pace.PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 05:53 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 laneAnalyfical tnv Mcefabs Cora QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 08312017 Pace Project No.: 92353850 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7178 Lab ID Sample ID QC Batch Method GC Batch Analytical Method 92353850001 Outfall 001 EPA 1664B 377847 92353850002 Outfall 002 EPA 1664B 377847 92353850003 Outfall 003 EPA 1664B 377847 92353850001 Outfall 001 EPA 200.7 377598 EPA 200.7 92353850002 Outfall 002 EPA 200.7 377598 EPA 200.7 92353850003 Outfall 003 EPA 200.7 377598 EPA 200.7 92353850001 Outfall 001 SM 2540D 376439 92353850002 Outfall 002 SM 2540D 376439 92353850003 Outfall 003 SiA 2540D 376439 Date: 09/18/2017 05:53 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 377676 377676 377676 Page 9 of 12 Document Name: Document Revised: July 25, 2017 aceAnalXiCal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev-03 Pace Quality Office Laboratory receiving samples Asheville []/ Eden❑ Greenwood ❑ Huntersville❑ Raleigh[] Mechanicsville[] Client Name: Project WO# : 92353350 Courier: ❑Fed Ex ❑UP5 ❑ Client Commercial Pace other: ElCommercial []Other:— jl +I 1{ jt ll +32333850 ^_✓/ Custody Seal Present? []Yes Seals intact?-, , ❑Yes ._ ❑No Date/Initials Person Examining Contents: Packing Material: _ []Bubble Wrap ❑Bubble Sags ffN'�.na ❑ Other Biological Tissue Fr Zen? Thermometer: let ❑glue ❑hone ❑Yes ❑No N/A ❑ Gun ID: Type of ice: Correction Factor: Cooler,Temp Corrected ('C): 1 • ti Temp should be above freezing to 6°C ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil ( N/A, water sample) Did In '. samples originate a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intern" nally, FlYes ❑No inrtedine Hawaii and Puerto Rim)? r1Yes IAO Comments/Discrepancy: Chain of Custody Present? s-' ❑No N/A 1. Samples Arrived within Hold Time? Yes ❑Na ❑N/A 2. Short Hold Time Analysis (0I hr.)? ❑Yes ❑N/A 3. Rush Turn Around Time Requested? ❑Yes ffN. ❑N/A 4. Sufficient Volume? es []No' ❑N/A 5: Correct Containers Used? -Pace Containers Used? es ❑No []No ❑N/A ❑N/A 6. Containers Intact? es ❑Na ❑N A 7. Dissolved analysis: Samples Field Filtered? ❑Ye ❑Nn NIA 8, Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: 04, 1MJ ❑No ❑N/A 9, Headspace in VOA Vials (>5-6mml? ❑Yes ❑No A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No. ❑No N/A N/A 11, CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Date/Time; Date: Date: Field Data Required? l_JYes YJNo Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers) Page 10 of 12 O rp a M a 3 A 0 v 0 ry 2 x 0 n a ro � � n a � rt � R M A m � ' 3 a �n c � D a to lD _! C 3 M m a D CL n m vy 2 � � 2 .a fD I o a 0— CL M CL N 2 a c P ar to CO v :M In A W ~ - Item# zzzxzzzz/zizz BP4U-125 mL Plastic Unpreserved (N/A) (CI-( BP3U-250 mL Plastic Unpreserved (N/A) BPZU-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP45-125 mL Plastic H2SO4 (pH <-2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2j BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) BP3C-250 mL Plastic N20H (pH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved i AG1U-1 liter Amber Unpreserved (N/A) (CI-) AG1H•1 liter Amber HCl (pH < 21 f AG3U-250 mLAmber Unpreserved (N/A) ICI-) AG15-1 liter Amber H2SO4 (pH < 21 AG35-250 mL Amber H2504 (pH < 2) AG3A(DG3A)-2SO mL Amber NH4CI (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) _ VG9T-40 mL VOA Na2S203 (N/A)} VG91J-40 mL VOA Unp (NIA) , OG9P-40 mL VOA H3PO4 (N/A) I VOAK (6 vials per kit)-5035 kit (N/A) I V/GK (3 vials per kit)-VPH/Gas kit (N/A( SPST-125 mL Sterile Plastic (N/A- lab) SP2T-250 mL Sterile Plastic (N/A— lab) 8P3A-250 mL Plastic (NH2)2504 (9.3-9.7) Cubitainer V5GU-20 mL Scintillation vials (N/A) GN' O w OD w J p(D � V W W ;P •FaceAnalXical " CHAIN -OF -CUSTODY ! Analytical Request'Docurnent The Chtl.in•ot•Custody is a LEGAL DOCUMENT. All relevant fields must be completed accuralely. 0 www.pacuiabs.mam Section A Section B Section C Page: of m rn Required Client Intarmali= Required Project information: Invoice Information: - !L Company: E Rt at1 Report TO: �/I an� u� Attention: i 1. 181 7981 Address: ry ,-y 1 W4D O� 3 ' Ci Copy To: Company Name: REGULATORY AGENCY deli t4G Z? 8lc)'A f Address: F- NPDES F GROUND WATER i— DRINKING WATER r usr r RCRA r orrlER Email To: k6u�dq�eq Purchase Order No.: Pam Q-le mac aT" Relemnw: P$onaeS rp7-340"Fax: } Projact Name:Cj,•�rmwaye�, o53ka'�}T Site Location 1 -P"o,y STATE: Requested DOuee Dail lTAT: Project Number. Paco Pi M: Requested Analysis Filtered (YIN) Section D Matrix Coded — z Required Client lnremwtion MATRIX I COnE i COLLECTED Preservalives `r Dnnking Water DW O Water 4VT Waste Water WIAI Product iP Ry a U m COMPOSITE START COMPOSITE ruDrC:RAn W Z SolUSolid 51- SAMPLE ID WIPe WP w (A-Z, 0 91:) Air AIR ..uj LU a Z Sample IDS MUST BE UNDUE Tissue TS 0 G a h Z a�i Ir) t at: Other OT � a a0� _� � m N� w ¢ 4 a LL 0 2 Oz Ua 46 yi Q�r' y rn DATE TIME GATE 'TIME (A • �: D T 7- Z O y i7 C7C Pace Project No.l Lab LD- 1 pmt-L-i Dot lq:40 C) 1 3. �S 2 o,.A+r ooa U B ti �,: `10 .3 t 1 t I crr` 3 O+il OQ3 Gr 91NO 14140 1 :i % s r Gti 4 6 7 I 8 9 1p 11 I 1z ADD1TfONAL COMMENTS RELINQUISHED BY / AFFILIATION DATE TIME ACCEPTED BY r AFFILIATION DATE TIME SAMPLE CONDITIONS OL%t�lk ool : 7.3 led ©tatf+kk OOP : &,,4 ` SAMPLER NAME_ AND SIGNATURE -- ORIGINAL PRINT Name of SAMPLER:M�C� r+K DATE Signed / SIGNATURE of SAMPLER: a9 0 E u = m U E {MMlDDIYY): f k�to -lmparlenl Noto: By Srpnmg INS term you are amopling Paw's NET 30 day paymant tomvS and agreeing to We charpos or 1.5% per inohtll for any invoices not paid rnthin 30 days. F-ALL-0-020rBu.07. 15-MDY-2007 Semi-annual Stormwater Dia'charge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted - CERTIFICATE OF COVERAGE NO. NCG03 0 ll G G FACILITY NAME �c�tav_�C.p o✓\ COUNTY 1Q k_ PERSON COLLECTING SAMPLES�Sc,v LABORATORYpo,Gt- A�nal+,k,�: l Lab Cert. # i a. It b Comments on sample collection or analysis: Part A: Stormwater Benchmarks and.Monitoring Results SAMPLE COLLECTION YEAR oZ 0 0- SAMPLE PERIOD � Jan -June ❑ July -Dec or Monthly' (month) DISC GfNG TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �% ❑Zero -flow ❑Water Supply ❑SA 9 J�V []Other SUN C��TRp& -PLEASE REMEMBER TO SIGN ON.PAGES 2 AND/OR 3 4 flWR SEC ❑ No discharge this period?z Outfall No. Date`Sample CoUect`edl (mo/dd/yr) 24-Hour rainfall amount, inches:' Total Suspended Solids pH, 'Standard units Copper Lead Zinc Non -Polar o&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> _ 100 mg/L or 50 mg/L 6,0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L < 0.005, [ v,aas1 0 .01'SM "k M L a 3 o a. 5 L $ c 0 .oasm ,a o . aoll- a.a� < S .0 9 <0.0 < o <T.0" >I 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on-site.rain gauge, Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found it 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40.CFR 469.31). Permit Dr, ,/1/2012-10/31/2017 SWU-245, last reviser'-"? 5/2012 a3 Page 1 of 3 �r r 'I Facilk._, that incorporate a solvent management plan into the Stormwater Pu'..jtion Prevention Plan may so certify, and the requirement for TTO mormoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." 0 Name (Print name) Title (Print title) (Si ure) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar 0&G/TPH by EPA .1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Note. , you report a sample value in excess of the benchmark, you must imp -meat Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 1F YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 da ►ems of receipt of the lab results (or at end of monitoring period in the case o "No Dischar e" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submittling false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) (Datef Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 ,Facet- ralytical' arvm.pacelabs.com Section A Required Client information: CHAIN-OF-M-70DY I Analytical Request Document The Chain -of -Custody is a, hL DOCUMENT. All relevant fields must be completed accurately. Section B Section C i. 1 Required Project Information: Invoico Information: Page: of Company: f . Report To: ' �/ j Attention: Z U C) t) 1 4 '7 L ` Address: f < r{ Copy To: J Company Name: REGULATORY AGENCY �+ f`J �, ``{�fn�t.� Address: NPDES F GROUNDWATER F DRINKING WATER F, V r UST r RCRA �� OTHER Email To: B : , 1-t rC p Y, ly j 711A 1, A Purchase Order No.: Pace Quota Reference: Phone: Fax: --- Project Name; Pace PmJod Site Location .. ,'�.{ manager: STATE: Requested Due DatefrAT: Project Number Pace Profile N: Requested Analysis Filtered (YIN) , Section D +• ' Matrix Codes x z Required Client Information _ "`j" mATRIx r CODE " 9 g COLLECTED Preservatives 'Y Drinking Water OW 0 O Water WT Waste Water WW SStt v U ITE oaTART COMPOSITE.a EIiI w Z Product P� - SoilfSclid St, SAMPLE ID iilpe op �; F W N 03 (A-z, D-s r: j Air AR o w Sample IDs MUST BE UNIQUE Tissue TS O a w e' S U Other OT U X ill W Z O Q C j., -" V t 5 W Q y 11 � O Q {n M L L to ^v �- N ~ DATE TIME DATE TIME Z) _ _ = Z Z g Q y J.3 IY Pace Project No.I Lab I.D. c::;.�`` CJCtir r,, iJ'•x I �� i I I. I t 4 5 6 7 8 A., 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION - DATE TIME SAMPLE CONDITIONS C~tC�f SAMPLER NAME AND SIGNATURE U o ^ d T� U C PRINT Name of SAMPLER;1'Sa n m SIGNATURE of SAMPLER: ,f/A DATE Signed E N - (MMfDDiYY); r.� S�f 7 cn 'Important N c W By signing this farm you are accepting Pace's NET 30 day payment terms and agreeing to late charges of I.5% per month1o6-ny invoicaa not paid within4days r F-ALL-Q-020rev.07, 15-May-2007 aceAnalXical www.pacelabs cram June 05, 2017 Michael Hickey Eaton 221 Heywood Rd Arden, NC 28704 RE: Project: Stormwater Q5212017 Pace Project No.: 92341423 Dear Michael Hickey: Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on May 22, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalj cal ww .pacelabs.rom Project: Stormwater 05212017 Pace Project No.: 92341423 Pace Analytical Services, LLC 2225 Riverside Dr. AshevNe, NC 28804 (828)254-7176 Charlotte Certification Ms 9800 KinceyAve. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florid alNFLAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virg inialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalj cal wwwpacelabs corn 1 Project: Stonnwater Q5212017 Pace Project No.: 92341423 Lab ID Sample ID 9 2341423 001 O utfa 11001 92341423002 Outfall002 92341423003 Outfall003 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7175 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D NAL 1 PASI-A EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D NAL 1 PASI-A EPA 16646 JMS 1 PASI-C EPA 200.7 SH1 3 PASI-A SM 2540D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical W"Pacelabs.com l ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater Q5212017 Pace Project No.: 92341423 Sample: Outfall 001 Lab ID: 92341423001 Collected: 05/21/17 17:00 Received: 05/22/17 15A5 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Collected Date Collected Time Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Capper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 1f Sample: Outfall002 ` Parameters Field Data Collected By Collected Date Collected Time Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Sample: Outfall 003 Parameters Field Data Collected By l Date: 06/05/2017 11:05 AM Analytical Method: Jason M 1 05/21/17 17:00 5/21117 1 05/21/17 17:00 17:00 1 05121 /17 17:00 7.0 Std. Units 0.10 1 05/21/17 17:00 Analytical Method: EPA 1664B ND mg/L 5.0 1 06/01/17 06A6 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug/L 5.0 1 05/26/17 1520 06/03/17 22:29 7440-50-8 NO uglL 5.0 1 05/26/17 15:20 06/01/17 05:32 7439-92-1 13.0 ug/L 10.0 1 05/26/17 15:20 06/01117 05:32 7440-66-6 Analytical Method: SM 2540D 5.7 mg1L 3.3 1 05/24/17 22:32 Lab ID: 92341423002 Collected: 05/21/17 17:10 Received: 05/22/17 15:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: Jason M 1 05/21/17 17:10 5/21117 1 05/21/17 17:10 17.10 1 05/21/17 17:10 6.8 Std. Units 0.10 1 05/21/17 17:10 Analytical Method: EPA 1664E ND mg1L 5.0 1 06/01/17 06:17 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 NO ug1L 5.0 1 05/26/17 1520 06/03/17 22:33 7440-50-8 NO ug/L 5.0 1 05/26/17 15:20 06/01/17 05:35 7439-92-1 ND ug/L 10.0 1 05/26/17 15:20 06/01/17 05:35 7440-66-6 Analytical Method: SM 2540D NO mg1L 5.0 1 05/24/17 22:32 Lab ID: 92341423003 Collected: 05/21/17 17:15 Received: 05/22/17 15:45 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Qua] Analytical Method: Jason M I REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05121117 17:15 Page 4 of 13 aceAnaIX cal www.pacelebs.com 1 Project: Stormwater Q5212017 Pace Project No.: 92341423 ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28604 (828)254-7176 Sample: Outfall 003 Lab lD: 92341423003 Collected: 05/21117 17:15 Received: 05/22/17 15:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Field Data Collected Date Collected Time Field pH HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Date: 06/05/2017 11:05 AM Analytical Method: 5121117 1 05/21/17 17A5 17:15 1 05/21/17 47:15 6.9 Std. Units 0.10 1 05/21/17 17:15 Analytical Method: EPA 1664B ND mg/L 5.0 1 06/01/17 06:17 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug/L 5.0 1 05/26/17 15:20 06/03/17 22:36 7440-50-8 ND ug/L 5.0 1 05/26/17 15:20 06/01/17 05:38 7439-92-1 NO ug1L 10.0 1 05/26/17 15:20 06/01/17 05:38 7440-66-6 Analytical Method: SM 2540D ND mg1L 5.0 1 05/24/17 22:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytrcal wvwpacelabs.com fF QUALITY CONTROL DATA Project: Stormwater 05212017 Pace Project No.: 92341423 QC Batch: 362952 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Descliption: 1664 HEM, Oil and Grease Associated Lab Samples: 92341423001, 92341423002, 92341423003 METHOD BLANK: 2012102 Matrix: Water Associated Lab Samples: 92341423001, 92341423002, 92341423003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 06/01/17 06:14 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE & LCSD: 2012103 2012104 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Oil and Grease mg1L 40 38.8 38.5 97 96 78-114 1 30 Results presented on this page arc in the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/05/2017 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytical wwwpamlahs.00m QUALITY CONTROL DATA Project: Stormwater Q5212017 Pace Project No.: 92341423 QC Batch: 362417 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92341423001, 92341423002, 92341423003 METHOD BLANK: 2009485 Matrix: Water Associated Lab Samples: 92341423001, 92341423002, 92341423003 Blank Reporting Parameter Units Result Limit Analyzed Copper ug1L ND 5.0 06/03/17 22:22 Lead ug1L ND 5.0 06/01/17 04:11 Zinc uglL ND 10.0 06/01/17 04:11 Qualifiers Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28604 (828)254-7176 LABORATORY CONTROL SAMPLE; 2009486 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 500 527 105 85-115 Lead ug/L 500 490 98 85-115 Zinc ug1L 500 507 101 85-115 ,• MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2009487 2009488 (o MS MSD 92341629002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Copper ug1L ND 500 500 499 497 100 99 70-130 D Lead ug1L NO 500 500 482 481 96 96 70-130 0 Zinc ug/L 3.5J 500 500 505 507 100 101 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2009489 2009490 MS MSD 92341629012 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Copper uglL 21.3 500 500 532 522 102 100 70-130 2 Lead ug/L NO 500 500 485 479 97 96 70-130 1 Zinc uglL 19.4 500 500 527 523 102 101 70-130 1 Results presented on this page are In the units indicated by the "Units" column except where an aRemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/05/2017 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytcal wwwpacefahscom QUALITY CONTROL DATA Project: Stormwater 05212017 Pace Project No.: 92341423 QC Batch: 362096 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92341423001, 92341423002, 92341423003 METHOD BLANK: 2008066 Matrix: Water Associated Lab Samples: 92341423001, 92341423002, 92341423003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/24/17 22:29 Pace Analytical Services, LLC 2225 Riverside Or, Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2008067 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 230 92 90-110 SAMPLE DUPLICATE: 2008068 Parameter / Total Suspended Solids 1 SAMPLE DUPLICATE: 2008069 Parameter Total Suspended Solids 92341347003 Dup Units Result Result RPD Qualifiers mg/L 5.8 6.0 3 92341423003 Dup Units Result Result RPD Qualifiers mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 06/05/2017 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 Pace Analytical Services, LLC aceMaOcal 2225 Riverside for. Asheville, NC 28804 www.pacelabs.cam (82$)254-7176 1' QUALIFIERS Project: Stormwater Q5212017 Pace Project No.: 92341423 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method ❑etection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each anatyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/05/2017 11:05 AM without the written consent of Pace Analytical Services, LLC, Page 9 of 13 aceAnalytical wmvpacelabstw QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 05212017 Pace Project No.: 92341423 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92341423001 Outfall 001 92341423002 Outfall 002 92341423003 Ouffall003 92341423001 Outfall 001 EPA 1664B 362952 92341423002 Outfall 002 EPA 16648 362952 92341423003 Outfall 003 EPA 1664E 362952 92341423001 Outfall 001 EPA 200.7 362417 EPA 200.7 362550 92341423002 Outfall 002 EPA 200.7 362417 EPA200.7 362550 92341423003 Ouffall 003 EPA 200.7 362417 EPA 200.7 362550 92341423001 Outfall 001 SM 2540D 362096 92341423002 Outfall 002 SM 2540D 362096 92341423003 Outfall 003 SM 2540D 362096 Date: 06/05/2017 11:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 DRarsxnt Name: DOLUrne111 Revtea: Sept RS, 291fi �,..�An Sam Mfall®fonU RnRgl I$CyR Pa 1p12 � �"""/'�• Dpam.nl No.: laply MrtMltty: F{ARti-017-Ravel Pxe QwR D7R! l2herMerlf feC¢ivj{tg camAl M: -,A C-41e �' .Edens . Greenwood[] .-Huntetsellle ❑ RRlelghD Mechanl—ille❑ . NERM Oi.ntN me: WO#: 92341423 Project C..der: Fed U UUPS Inpl - ©corpmer[W OP."other;_ ll111111111111111 g23A1823 CsstodT Sexl Pre[ent7 RYae 2<- Se.111n1a.17 ❑Yea ❑N. D+rtMlaab perran d.mY;tlR t'anun P•e>tlry M.teH.l; ❑Buhhk Wrep I--I�� ❑3ubble bap [)Ndp ❑ether:_ Thertnpmeter:' Jy,- ! Qtyrc F"i s>n,pW y,ke,moln{porn har blo [orcealnn Fuaur. Cpdef Temp Cnnc[ted l'[}l� 61do{kal these Froren? Cl.. ❑N. POIA T—p[IUNdbeaEvrc eernRt CC t1SDA Re{ulatea Sn{{�Rfgw[lerGnplll Nd` - - - - w[ArineXrve{antlFiw[bW[elT ljX. Gmmml.lh+pmp Chain or[Sas Prenenti Yea n'A ]. Sam [A..iued wS:hN Meld Tlmrt • y �Shov Noy o.. ana h<71 llr.t r3pu. 3- R=hCumA.v..rdT-0. tedT rb suff .Vdvrv:t ONJA 5. - —eu emanr[uKdt z Cmr+tl+•f weds �' da pX1A G vmde[F vrtlreel Ell, •. s. Narrr+l[wRbkklA•m[rd+w evm.ta Sample fabrL RutdrmCt aSrwe..',;axgrrnNfJ Ant. Japk: r ..JJn L'Irn Ona ^_ Neaapr. Rr 1'dI VIW 56mm1 • ]6 TM B4nF Frnen:? err[ 6[e C'GW It — np ipldtVllVALfIXy—MtalMii.rr Ljy. IU- pawn Connoted: CpmmemtjSRmple Qaaeyrcy: D.[enf : —q- Mana{er scuRF i.vkw: /] Date: PrRje[t Mana{rr SRF Review: / Oxe: J2 r� i r. W heiw.m tM2 h a dhuepan[y+ravW No[pr Cereluv raep{arcr v.Wn [ a.A+•f W I[ forma a [em so rr NeM GrpM.a mRrtR Cer4fi�14n wee fie. Out of btl, NSxrev prtfem We, out d IemR lam+fert [entAn ml Pape X t of 13 13—.name: I PeCwrMtAeWM. SeyL 71, 701fi SCV0. Pee 7 d 7 dGC %V$�J a Opcenm, nOMAethohry: Ff4ei]43i-Bee.01 n Pace WiG)/0—. �] •[heck mark top half of 6ax it pH end/or dechlodnatlon Project C LJO# ; 92341 A 23 Is MiHed and within the acceptance range for, . _, of J preservation samples. PA 01 are Bate: ogjogll, ••Bottom half of hox is to list numher of bottles LLFEB7: 93-Cutlpr14 HOME RON1100.0 MONO MERSOM ■ mokimenso ONE an ON MEMOS 0 Osman a ��NOON 0 pH Adjustment Log for Presemed Samples Saeglpp type oftnpeltauv pll upon nnabt WM wnp�whon Mk�na lima piwemcbn aqulaN amemtdh�er.Wr! deed 1pp Pap 1] Ct 3 U ' CHAIN•OF•CUSTODY I Analytical Request Document 4ceAna&lIca!" (�5a'cieAnalyfical wwwpacelabs.cam SAMPLE ACKNOWLEDGMENT Samples Submitted By: Eaton Corporation Client Project ID: Stormwater Q5212017 Client PO#: Acquire PO # Pace Project Manager: Pace Analytical Project ID Samples Received: Estimated Completion: 9800 KinceyAve., Suite 100 Huntersville, NC 28078 (704)875-9092 Chris Derouen Phone(704)875-9092 christopher.derouen@pacelabs.com 92341423 May 22, 2017 03:45 PM June 06, 2017 CC: Ben Hale,Lee Bishop,Michael Hickey Pace Analytical Date/Time Customer Sample ID Lab ID Matrix Collected Method Outfall 001 92341423001 Water 05/21/17 17:00 200.7 ICP Metals Copper, Lead, Zinc 2540D Total Suspended Solids Field Data HEM, Oil and Grease Outfali 002 92341423002 Water 05/21/17 17: l0 200.7 ICP Metals Copper, Lead, Zinc 2540D Total Suspended Solids Field Data HEM, Oil and Grease Outfall 003 92341423003 Water OSY21117 17: l5 200.7 ICP Metals Copper, Lead, Zinc 2540D Total Suspended Solids Field Data HEM, Oil and Grease Please contact your project manager if you recognize any discrepancy in this form or have any questions about your project. Thank you for choosing Pace Analytical Services, LLC. 05/22/2017 04:41 PM Page 1 of 1 Bxumepl NiMq po[Umen! nexe.d: LpL 21, 2016 Sam Cavdlrlr.au 0..w1 SN P lOF2 • llanwmr No.: Nv,ir�AurbrAY l-tM-6-033-ae.Al Pare lau 01Boe la6onialy reYxivinC samples: ,. _ •--AsiteWllB �. Edeno ... Greenwood ❑ .-RuntenviNe 0 RalelghQ Mechanicsville❑ . 111-1N ., Wp#:92341423 Pra,ea ,, ❑P.. OZ341Q111llllllllll111 BZ3413 eu,t,NS,,l P,esentl ��,,// Ely. IQ^v seal, Inr.rtl D] . ❑Nv as W Ixnl.x nrwn tr..d.A+S Ccnoen��� P.&M M.r.N4 E)Bubble Wrap 03-1, Gies ( M6, 13oftr.— Th.. —; RsTtt O¢ One.. ,nA>- C—pion Farts. CurlerTempim..xaed Ccl ewud3T71—Fre,ertl ❑Yo []W [�lalA TemP.Aedd h abweS`�, nYK lv e"C tISBA A..ei..�.,....l.5ai(L.i Nlti� t+?�}},.n.. _... e........ ..._v,.`._Y... ,...,_�....�.... ...., _..�.r a. No' NddnaN.+a. xM Pwrt. Rim a Ov.s [rmm.nl,Poir lTaln vlCwtvtl vroenli ry No 1. Lm ArNved wltN, NrAtl fYn.7 x/i L Saxxr Nid Me a.,. .T] Fw. P a ;_ urn Nea Around T.n.R rtll . A. nl Vdurcl WA i -n [onsYer Vu o i [e111i.1IM N,edl ge. cl- OWA r7N. G hers lrttaglrl.. MA 1. Sur. neM FileredTr7, A B. Ndai(aelin,enrN Nnbl.ln rh. duseNed wnUuar San.Pte label. Marti uBCl AST. 0. OWa R nfW arVMVIW aS4nnl 16 Te. 61anY PrneMl TdpelanYGatvdxS kk,.nsl 01.a I Qtn Ox. 041A m.A IL wn, xaniiGYlaxiRF56ulr,ax iNY a.r. uquFedl L11. Ljxa Person cawrted: OOmrYMrTI/SampN DDueYR'l D.tnlnme: P.°J'rt avaaier SCtlaP R..I.rr: lz W.: Z .7 P,n,tn Man.l.r SRF ReNaw; � oa a; , 7 wn.n.x., m.2 �. dl.r.rymry.mcma wnR c.,nlx. camoe,,...amPin. mPrnr 16h ra.. w e. kxr ro m. xnrrn e.�l:,, Down c.min.P.n mna u.. v,A.,>•u.A NCR n..,....a,a.r<x,rmr. �.ra..r...wx,hw Gsrumlrr xr.r4- ponment RrNrld SlpC 2��rb eerrnn�ee ism lCaMrtirn Brce Sale Pa ids r-G1a{SO3]�Ir.�Ai eat 'Check mart top half of boa If pH and/or dechlerinadon Project (,ja# • 92341423 ' Is verified and within the acceptance range for, .. , _, _ _ pnrservatfon samples. Pry` MI. Bw Bate. OS/B6/t7 •Bottom ha€i of box is to list number of bottles CLIENT: 93-0ut I erH No mass Mii' �i u INS 00,111MEM ON 0 011610 MEN on son M ME WEIN ■ pH Adjustment Log for Preserved Samples saMrio zrae ofrrue..ae.. Rx aan naaor orta w•+r+.'+eor+dtke zxu elrm.rien rAaua �mn�w®..u.. .aa.a taa G,' CHAIN•OF-CUSTODY I Analytical Request Document rkann�r -ch—C yb.I � *mnth- Semi-annual_Stormwater L:scharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted P.1 d d 0 I G CERTIFICATE OF COVERAGE NO. NCG03-0 56.E SAMPLE COLLECTION YEAR d 01 (a FACILITY NAME Eato_v) Goroorg_*70�- SAMPLE PERIOD ❑Jan -June aJuly-Dec COUNTY pR - - or ❑ Monthly' (month2 PERSON COLLECTING SAMPLES i 0) t✓l F k i G�2 r-` DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY PCG lab Cert. # �� y REC�1 V ED ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: ❑Other NOV a 9 2016 CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results No discharge this period: Date Sample p 24-hour rainfall pH, Non -Polar O&G/ c Total Toxic Outfall No. Collected' amount, Total Suspended Solids Standard units Copper lead Zinc Total Petroleum Organics sr (mo/dd/yr) lnches3 Hydrocarbons Benchmarks ==> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L �olaoi(, 0.60 /o.(P to L 9 0,0 4.017 . /3A 4,005- tJ A tt aoic 0 .50 31 M ±,o 1 0.00&0 < .00s" 032a <, 009- IJ A 3 oio 0.60 C a.b L -. 3 1 0.00SCIO c . 006 . or, T5 < . 005, N ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceeciance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Fabli.—, that incorporate a solvent management plan into the Stormwater Pt'_jtion Prevention Plan may so certify, and the requirement for TTO mor,.toring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Pa: mit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." ,7;�50 19 if e� Name (Print name) Title (Print title) /gnature) (Date) Note: (Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be reported in the format, "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664-(SGT-HEM) Total'Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note. , you report a sample value in excess of the benchmark, you must imp _ment Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case o "No Discharge" re orts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." G'.ry ature of Permittee) Permit Date:11/1/2012-10/31/2017 /r 7 Zml (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 � - r aceAnalytical VMW,pacelabs.c= October 19, 2016 Michael Hickey Eaton 221 Heywood Rd Arden, NC 28704 RE: Project: Stormwater 10072016 Pace Project No.: 92315459 picc- 030�46,� RECEIVED Nov o 9 2016 CENTRAL FILES DWR SECTION Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NG 28804 (828)254-7176 Dear Michael Hickey: Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Rhonda Gray, Eaton Corporation Kathleen Rasmussen. Eaton REPORT OF LABORATORY ANALYSIS ' TNI This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 9g0 A�� aceAnalytical www.pacefa6s.cam CERTIFICATIONS Project: Stormwater 10072016 Pace Project No.: 92315459 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #. 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 r ;aceAnalXieal Pace Analytical Services, LLC ® 2225 Riverside Dr. Asheville, NC 28804 www.pacelabs.com (628)254-7176 SAMPLE ANALYTE COUNT Project: Stormwater 10072016 Pace Project No.: 92315459 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92315459001 OUTFALL 001 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D MLS 1 PASI-A 92315459002 OUTFALL 002 EPA 1664B JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D MLS 1 PASI-A 92315459003 OUTFALL 003 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PAS1-A SM 2540D MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 laneAnayical" wwwpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 10072016 Pace Project No.: 92315459 Sample: OUTFALL 001 Lab ID: 92315459001 Collected: 10/07/16 17:20 Received: 10/10/16 13:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By Michael 1 10/07/16 17:20 Hickey Collected Date 1017116 1 10/07/16 17:20 Collected Time 17:20 1 10/07/16 17:20 Field pH 6.9 Std. Units 0.10 1 10/07/16 17:20 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 10/19/16 09:00 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 21.2 ug1L 5.0 1 10/13/16 01:30 10/18/16 00:42 7440-50-8 Lead N❑ uglL 5.0 1 10/13/16 01:30 10/18/16 00:42 7439-92-1 Zinc 132 ug1L 10.0 1 10/13/16 01:30 10/18/16 00:42 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 25401) Total Suspended Solids 10.6 mg1L 2.9 1 10/13/16 13:36 Sample: OUTFALL 002 Lab 1D: 92315459002 Collected: 10/07/16 17:20 Received: 10110116 13:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] Field Data Analytical Method: Collected By Michael 1 10/07/16 17:20 Hickey Collected Date 1017116 1 10/07/16 1 T.20 Collected Time 17:20 1 10/07/16 17:20 Field pH 7.07 Std. Units 0.10 1 10/07/16 17:20 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 5.0 1 10/19/16 09:00 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA 200.7 Copper 6.0 ug1L 5.0 1 10/13/16 01:30 10/18/16 00:45 7440-50-8 Lead ND ug1L 5.0 1 10/13/16 01:30 10/18/16 00:45 7439-92-1 Zinc 32.2 ug1L 10.0 1 10/13/16 01:30 10/18/16 00:45 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.8 mglL 2.8 1 10/13/16 13:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2016 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 lacieAnalyfical"' www.pacelabs ow ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 26804 (828)254-7176 Project: Stormwater 10072016 Pace Project No.: 92315459 Sample: OUTFALL 003 Lab ID: 92315459003 Collected: 10/07/16 17:20 Received: 10/10/16 13:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By Michael 1 10/07/16 17:20 Hickey Collected Date 1017116 1 10/07/16 17:20 Collected Time 17:20 1 10/07/16 17:20 Field pH 6.31 Std. Units 0,10 1 10/07/16 17:20 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 10/19/16 09:00 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Copper 5.6 ug1L 5.0 1 10/13/16 01:30 10/18/16 00:58 7440-50-8 Lead ND ug1L 5.0 1 10/13/16 01:30 10/18/16 00:58 7439-92-1 Zinc 68.3 uglL 10.0 1 10/13/16 01:30 10/18/16 00:58 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 2.5 1 10/13/16 13:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2016 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 5of12 (:�;a'cieAnaVical wwwpacelabs cam QUALITY CONTROL DATA Project: Stormwater 10072016 Pace Project No.: 92315459 QC Batch: 333690 Analysis Method: EPA 1664B QC Batch Method: EPA 16648 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples. 92315459001, 92315459002, 92315459003 METHOD BLANK: 1849198 Matrix: Water Associated Lab Samples: 92315459001, 92315459002, 92315459003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 10/19/16 09:00 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: Parameter 1840199 Units Spike LCS Conc. Result LCS % Rec % Rec Limits Qualifiers Oil and Grease mg1L 40 35.3 88 78-114 MATRIX SPIKE SAMPLE: 1849200 92315526001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 34.5 86 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2016 03:36 PM without the written consent of Pace Analytical Services, LLC- Page 6 of 12 aceAnalytical wwwpaoelabs-corn QUALITY CONTROL DATA Project: Stormwater 10072016 Pace Project No.: 92315459 QC Batch: 332777 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92315459001, 92315459002, 92315459003 METHOD BLANK: 1844053 Matrix: Water Associated Lab Samples: 92315459001, 92315459002, 92315459003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 10/18/16 00:05 Lead ug1L ND 5.0 10/18/16 00:05 Zinc ug/L ND 10.0 10/18/16 00:05 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1844054 Spike LCS LGS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 520 104 85-115 Lead ug/L 500 503 101 85-115 Zinc ug/L 500 502 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1844055 MS 92315432002 Spike Parameter Units Result Conc. Copper ug/L 7.0 500 Lead ug1L 9.3 500 Zinc ug1L 190 500 1844056 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 538 535 106 106 70-130 0 500 516 514 101 101 70-130 0 500 687 688 99 100 70-130 0 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1844057 1844058 MS MSD 9231WO003 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0.10 500 500 624 603 104 100 70-130 3 mg/L Lead ug/L NO 500 500 501 482 100 96 70-130 4 Zinc ug/L ND 500 500 504 486 100 96 70-130 4 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1011912016 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalXical wwwpacelabs-Conn QUALITY CONTROL DATA Project: Stormwater 10072016 Pace Project No.: 92315459 OC Batch: 332948 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92315459001, 92315459002, 92315459003 METHOD BLANK: 1845096 Matrix: Water Associated Lab Samples: 92315459001, 92315459002, 92315459003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Total Suspended Solids mg/L ND 2.5 10/13/16 13:32 LABORATORY CONTROL SAMPLE: 1845097 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 1845098 92315452002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 15.6 16.8 7 D6 SAMPLE DUPLICATE: 1845099 92315605001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 53.0 52.0 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 10/19/2016 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 acmnalytical ww .pacelabs.c m QUALIFIERS Project Stormwater 10072016 Pace Project No.: 92315459 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated fromAzobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2016 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 aceAnalytical mm..pacelahs com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Starmwater 10072016 Pace Project No.: 92315459 Lab ID 92315459001 92315459002 92315459003 92315459001 92315459002 92315459003 92315459001 92315459002 92315459003 92315459001 92315459002 92315459003 Sample ID OUTFALL 001 OUTFALL 002 OUTFALL 003 OUTFALL 001 OUTFALL 002 OUTFALL 003 OUTFALL 001 OUTFALL 002 OUTFALL 003 OUTFALL 001 OUTFALL 002 OUTFALL 003 Date: 10119/2016 03:36 PM QC Batch Method EPA 16648 EPA 1664B EPA 1664B EPA 200.7 EPA 200.7 EPA 200.7 SM 2540D SM 2540D SM 2540D Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch Analytical Method 333690 333690 333690 332777 332777 332777 332948 332948 332948 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. EPA 200.7 EPA 200.7 EPA 2003 Analytical Batch 333058 333058 333058 Page 10 of 12 Document Name: Document Revised: Sept. 21, 2016 /! ?eAt7a1j4ica1' Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: j F-CAR-CS-033-Rev.00 Pace Quality Office Page 2 of 2 for Internal Use ONLY .. .. Client Name: WO# : 9231 459 Project #: I +j Courier: ❑Fed Ex UP5 ❑USPS Commercial ❑Pace ❑0ther-1 111912311154159 11 iilli Custody Seal Present? ❑Yes Seals Intact? ❑Yes []No Date/initials Person Examining Contents: Packing Material: ❑Bubble Wrap �21ubble Bags ❑None ❑Other: Thermometer: R Gun 10: Type of ice: f"`- I�et ❑❑ Blue None ❑Samples on ice, cooling process has begun �I� Correction Factor: tj Cooler Temp Corrected ('Q: 3 , n Biological Tissue Frozen? ❑Ye []No ❑N/A Temp should be above freezing to 6'C USDA Regulated Soil (ON/A, water sample) Did samples originate ih a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, FlYes F-]No includine Hawaii and Puerto Rico)? nYes 11No Comments/Discrepancy: Chain of Custody Present? CYes ❑No ❑N/A 1. Samples Arrived within Hold Time? P<es ❑Na [—I N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes o ❑NIA B. Rush Turn Around Time Requested? ❑Yes P6 ❑N/A 4. Sufficient Volume? Yes ❑No ❑N/A 5. Correct Containers used? -Pace Containers Used? Yes Yes ❑NO ❑NO ❑N/A ❑N/A 6. Containers Intact? Yes [:]No []NIA 7.. Samples Field Filtered? ❑Yes ❑No . NIA. S, Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Yes [:]No ❑N/A 9. All containers needing acid/base preservation have been checked and documented on page two of SCURF? Exceptions: VOA, Coliform, TOC, Dil and Greas DRO/8015 (water) DOC, LLHg Samples checked for dechlorination? [les Des ❑No ❑No ❑N/A N/A 10 11: Headspace in VOA Vials (>5-6mm)? ❑Yes [-]NO'ON/A' 12. Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot N (if purchased): ❑Yes ❑Yes ❑No ❑No gN/A gN/A 13. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Date/Time: Comments/Sample Discrepancy: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Note: whenever there is a.discreparrcy affecting North Carolina compliance samples, a copy of this form will be sent to the North Out of hold, incorrect preservative, out of temp, incorrect containers) Laboratory receiving samples: Ashevillex Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ EHNR Certification Office (Le, Mechanicsville[] Page 11 of 12 -PaceAnalvtical ' CHAIN -OF -CUSTODY / Analytical Request Document The.Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 6 www.patelahs.eom Section A Section B Section C Page: of ar Required Client lnformalion: Required Project Information: Invoice Inlormalion: Ali4 yi 'ry q C- r 1 Company: Report To: k 1 Address: CopyTo: :1 Company Name: REGULATORY AGENCY d Address: r Ni IF GROUND WATER r DRINKING WATER � UST i— RCRA [ OTHER Email To: �/ �% Purchase Order NiPam Quote Ruk:rr�aco: Phone: Fax " �iT�:�'j.�f� Project Name: ..r Y", �M r, } /n•� --pp � �ai� 4"✓!i. Racy Projrrct Site L ocation 4.i D w✓ •� ! 2�f[J Mnnagcr: S7ATE: Requested Due DateFrAT: Project Number: Pace Rmnte rt Requested Analysis Filtered (YIN) Section D ,Matrix Codes — .z Roquirod Client lnforrnatinn MATRIX'! CODE, o CL COLLECTED Preservatives 'r onnkinq Water DW o 0 Water WT Waste Water WWa m e0MPOSITE START COMPOSnE EHo�cane U w Z_ Product p SoiVSolid St. r d q r,. d -� .�► } SAMPLE ID Oil UP W w°O= {A-Z,.C-9l,-) Air AR u3 Sari IDS MUST BE UNIQUE Tissue TS O IL Other OT x w lu M r EL It - 1 U LL o Ed 3 = N DATE TIME DArE TIME a z" = i i z Pace Project Nod Lab I.D. t io i c t `v , C-V,� bJ% 4 l: ,2. '-x 1 k I 3 4 5 6 7 8 9 1a 11 yi ADDITIONAL COMMENTS RELINQUISHED BY / AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION- DATE TIME SAMPLE CONDfTtONS �. ORIGINAL SAMPLER NAME AND SIGNATURE c PRINT Name of SAMPLER: r M L E o } a cr U E �"'�' Si RE of SAMPLE - Signed DATE Si9 %/ -u>gzwmno Nam: by m.1-9Ina Corm you srru noa:{wag Pxc's NET 30 day payment terms and 1!pwi 1C laic dmrlles of 1,5')8 p,;r r,mnw for any inwir:cs riot paid vhthin 3n days. F-ALL-4-020rev.07. 15-1 Semi-annual Stormwater Discharge MonitorinlZ Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 71S/16 CERTIFICATE OF COVERAGE NO. NCG03 0- FACILITYNAME roJon Co*lcvla�lch COUNTY 5anc-or+bc_ PERSON COLLECTING SAMPLES 0n 11 orq 0M LABORATORY Fo,ct_ Lab Cert. # 12k- + 40 Comments on sample collection or analysis: R Avk l i Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �y16 SAMPLE PERIOD 0 Jan -June ❑ July -Dec or ❑ Monthly' (mont n(I'--m DISCHARGING TO CLASS ❑ORW ❑HOW ❑Trout ❑Zero -flow ❑Water Supply A7 RECEIVED ❑Other JQL 13 2RiASE REMEMBER TO SIGN ON PAGES 2 AND%OR 3 CENT14AL FILES 7WR SECTION ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks =__> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L a S/31/zo,1, .31 17.Sn �, a. �,ocs,-31t <.009It/z ,C%gEZ 14 T•sA /C N/A 3 -,/3► aQ14 .3)1) 2 3.7 M . � 1. o s-'Mek C oo s & . o s rq,* A- /V A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring "'may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ij A 5vh yylo jy,� Name (Print name) 115_ Title (Print title) ^— . C,� ^-�� (Si ure) (Da(e) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note, If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this periad?Z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NOX IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one coav of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permitteej Permit Date:11/1/2012-10/31/2017 Z�� (Date] SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted b l l7 1 (o CERTIFICATE OF COVERAGE NO. NCG03 4 L (� FACILITY NA�AE �a cJn ��rf�Oc]r� i ► COUNTY PERSON COLLECTING SAMPLES 1Cr.S0,n ,AA0L$cXr\ LABORATORY_ygck_►Q1_�r,_,/ Lab Cert. # I L rJ- 4,L7 Comments on sample ction or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR A 01(4 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or RMonthly1 /ul D_ month DISCHARGING TO CLASS ❑ORW [:]HQ ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other RECE IVE4LEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 JUN 21. 2016 CENTRAL FILES ❑ No dischorge this period?' Date Sample 24-hour rainfall pH, Non -Polar 0&G/ Total Toxic Outfall No. Collected k amount, Total Suspended Solids Standard units Copper Lead Zinc Total Petroleum , 5 Organics (mo/dd/yr) Inches3 Hydrocarbons /X Benchmarks =__> _ 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L ►� 16 1 C R-6_v•L/L <.ao IL 0 1 if < 6-for,' Lz tr -Na l( 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same pik"rametern-at the,sam outfali} ZForsampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained'in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring maybe waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report, I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) ,� —/7'/G (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * see General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOREPART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEE DANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FORTHE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." o% of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted con CERTIFICATE OF COVERAGE NO. NCG03 O LJ_ L( SAMPLE COLLECTION YEAR FACILITY NAnMEq~n_�,pDr�- i on �— SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY !{lMf�aM�� or E94Aonthlyl r' month PERSON COLLECTING SAMPLES Z30A DISCHARGING TO CLASS ORW HQW DTrout [:]PNA LABORATORY P" 4,\ .tyi-,G Lab Cert. # I cl t-{ Q RE "" E` " ED ❑Zero -flow [:]WaterSupply ❑SA Co ments on sample collection or analysis: ft ,p /ps ❑Other OU.. 11 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results No discharge this period?z Date Sample 24-hour rainfall pH, Non -Polar O&G/ Total Toxic Outfall No. Collected' amount, Total Suspended Solids Standard units Copper Lead Zinc Total Petroleum Organics5 (mo/dd/yr) Inches3 Hydrocarbons Benchmarks =__> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L '! . 72 L Q ..' a- •it LA: L o. L e- o,o 4 5 L rV A �✓E..I V I MAY 2 3 Pitts I DW ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." 1Gt Son N1.o ro,an Name (Print name) F G Title (Print title) (5i ture) (Date) r Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format,. "<XX mg/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 3.0 SU Footnotes from Part A also apply to this Part B * see General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO pa" IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware .I t there are significant pMalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (O re of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 D Date submitted L{11-11Z ! 1 CERTIFICATE OF COVERAGE No. NC903 0 .�1~�—b- FACILITY NAME Ee.a01 LbrDa a-Jru-+ COUNTY &unro.,--�R- PERSON COLLECTING SAMPLES — _3630A JMaroAC.✓, LABORATORY Pcq_ Lab Cert. # 19, d- `1 0 Cments on sample collection or analysis: C n & 1 I< Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 0 to SAMPLE PERIOD ❑Jan -June ❑Jul -Dec E/ or [9"Monthly' Mc.rC_k (month) DISCHARGING TO CLASS ❑ORW ❑HOW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfa[I amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===n _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L d Ao 1 to 1 S < 5rM ( L 7, to < U • 2QJA45 / 'Ca,1Z T t 1 G S l c_ Z ilk" I,., t:I v t U AP 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring reportwith A eppma ^kchere. 3al The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver ofthe-rainigauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ]Lason MoLOOn Name (Print name) FFFS Mr.y-�a,q(2 C" Title nt title) T ignature) Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX miz/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period:2 Qutfall No. Date Sample Collected, (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO [jj' IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the fob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST•SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Of 46W / r e- re of Permittee]r Permit Date: 11/1/2012-10/31/2017 S� G (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG03000 t9' e. Date submitted 3 /k k J CERTIFICATE OF COVERAGE NO. NCG030 C1 & (, FACILITYNAME �rl C oipar�iio� COUNTY i3 ✓� c o�.� b t' PERSON COLLECTING SAMPLES J"i ccie i G �i'S LABORATORY_�,xc_,L A,,�, J i coN I Lab Cert. # I k --W o Comments on sample collection or analysis: r Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �` 0 16 1: �_Wk SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or 0 onthly' (month' DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [—]Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Totak Total Petroleum Hydrocarbons Toxic Organicss Benchmarks 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L ! mg/L eS-l" S gr? L 7$ -oo7t,-, /V>J ,os n /� JUD NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." .Tasnn Mo Name (Print name) Mc�n� r Title int title) i e�J "'. 3 -� , 6 ignature) K (Dat ) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the. format. "<XX mgZU', where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' OutfalhNo. Date Sample Collected' (mo/dd/yr) 24-hour, rainfall amount, lnches3 Non -polar 0&G/TPH,by EPA 1664'{SGT-HEM}` Total Suspended. Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50'mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANC£ TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case o f "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i am aware^at there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) 3 bzz /G (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3