HomeMy WebLinkAboutWQ0021826_Residual Annual Report 2014_20150302CITY OF ROXBORO, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0021826
2014 ANNUAL REPORT
City of Roxboro, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00021826 County Person Year 2014
Facility Name (as shown on permit) City of Roxboro W WTP & WTP NPDES No. NCO021024
Land. Application Operator Synapro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 22
Total number of fields utilized for land application during the year: 12
Total amount of dry tons applied during the year for all application sites: 431.76
Total number of acres utilized for land application during the year: 81.2
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water. Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
it. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Thomas S. Warren. Assistant City Manager
Permittee Name and Tii//M1�lle (type or print)
Signature of Preparer* Date
(if different from Permittee)
re e i ee i!ate
��B ! IJ2 2015 ,
Signa re of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
ROXBORO,NC
. tOXBORO, NC WWTP AEROB. DIGESTED CAKE
October 2014
November 2014
December 2014
YEARLY TOTAL
AMOUNT UNIT
400.00
Y
841.00
Y
525.00
Y
1,766.00
Y
DRY TONS
UNIT
97.80
D
205.61
D
128.35
D
431.76
D
DRY METRIC
TONS
88.71
186.50
116.42
391.63
1/30/2015
2014 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
Town of Roxboro
Roxboro, NC
Roxboro WWTP
902 Cavel-Chub Lake Rd.
Roxboro, NC 27573
336-599-8232
NC0021024
Thomas S. Warren, Jr
Manager
P.O. Box 128
Roxboro, NC 27573
336-542-4621 ext.22
, Assistant City
Derek Clayton, WWTP Superintendent
902 Cavel-Chub Lake Rd.
Roxboro, NC 27573
336-599-8232
Synagro Central, LLC
Contact: Marshall Puryear
(336) 998-7150 ext. 17
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: "WQ0021826
Laboratory
Facility Name: ROXBORO, NC
A&L Eastern Laboratories Inc.
NPDES# : NCO021024
or WQ# (residual only)
WWTP Name: ROXBORO WWTP
Residuals Analysis Data .
Product Type AEDCAK
MIX
MIX
AEDCAK
Date Sampled (grab) or 09/03/14
09/03/14
11/04/14
11/04/14
Date Composited
Percent Solids 29.03
77.76
34.93
23.33
PARAMETERS (mg/kg dry weight)
-
Arsenic 5
6
7
5
Cadmium 2
2
<2
2
Mercury 1.4
0.5
2.4
1.3
Chromium 92
73
77
75
Copper 580
269
362
592
Lead 40
28
28
40
Molybdenum 8
<5
<5
6
Nickel 43
32
34
38
Selenium 6
<5
<5
6
Zinc 1160
489
656
1130
Total Phosphorus 21500
9570
12600
19100
TKN 41700
19900
20800
37900
Ammonia -Nitrogen 3690
849
3520
4710
Nitrate and Nitrite 772
264
91
1090
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X_S
(SIGN]
OF PREP
Date a - to -/
DENR FORM RSSF (5/2003) Printed: Friday - January 30 2015 at 16:59.53 for: 2102 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0021826 Laboratory
Facility Name: ROXBORO, NC A&L Eastern Laboratories Inc.
NPDES# : NCO021024
or WQ# (residual only)
WWTP Name: ROXBORO ,WWTP
Residuals Analysis Data
Product Type
AEDCAK
MIX
MIX
AEDCAK
Date Sampled (grab) or
09/03/14
09/03/14
11/04/14
11/04/14
Date Composited
Percent Solids
29.03
77.76
34.93
23.33
PARAMETERS (mg/kg
dry weight)
Aluminum
29000
38700
39700
30200
Calcium
16700
6980
10500
15000
Magnesium
3910
3410
3340
3700
pH
5.91
5_, 81
7.65
5.79
Potassium
2420
2970
2630
2310
Sodium
1030
498
553
817
"I certify, under penalty ,of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that,qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIG
R)
NR - Data Not Reported or Data Not Required
Date 2-/e, /?—
DENR FORM RSSF-B (7/2002) Printed: Friday - January 30 2015 at 17:00:12 for: 2102 01
Page: 1 of 2
Report Number: 14-248-0202 �u,�J( A&L Eastern Laboratories, lhc._
Account Number: 46487 7.621 Whitepine Road Riehmond,'Virginia 23237 '(804)'743.9401 Fax (804) 271-6446'
Submitted By: MARSHALL PURYEAR wwiwaleastern.com.
Send To, SYNAGRO'CENTRAL LLC/ROXBORO Project: ROXBORO CAKE
Mary Brewer NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS Date Sampled: 9/3/2014 09:00:00
Lab Number: 57429 Date Received: 09/05/2014 00:00
Sample Id : ROXBORO CAKE Date Reported: 09/11/2014
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Total Phosphorus
Total Potassium
Total Sulfur
Total Calcium
Total Magnesium
Total Sodium
Total Iron
Total Aluminum
Total Manganese
Total Copper
Total Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
29.03
70.97
4.17
2.15
0.24
0.85
1.67
0.39
0.10
0.37
3.80
Q1*01
MVV
MW
JM
KM
KM
KM
KM
KM
KM
KM
KM
KM
KM
KM
JM
JM
Total Cadmium 2.0 2.0 KM
All values are on a dryweight eight basis except as noted by asterisk. Detection limit on all N series is on a wet basic
41700
21500
2420
8540
16700
3910
1030
24800
29000
1080
580
1160
3690
38010
772
100.0
100.0
10.0
100
100
100
100
100
100
100
100
5
5
5
10.0
10.0
2.00
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
UU/Ud/LU"14 UO:US
09/08/2014 08:05
09/08/2014 08:44
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/10/2014 12:48
09/08/2014 08:44
09/08/2014 08:44
09/08/2014 08:45
09/10/2014 12:48
01V1-L04UV
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NI3C
CALCULATION
SM-450ONO3F
SW 6010C
Debbie Holt
Page: 2 of 2
Report Number: 14-248-0202
Account Number: 46487
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
@P A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
www.aleastem.com
Project: ROXBORO CAKE
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/3/2014 09:00:00
Lab Number: 57429 Date Received: 09/05/2014 00:00
Sample Id : ROXBORO CAKE Date Reported: 09/11/2014
Total Chromium
92
b
NIVI
UZI/ IU/GV I4 14.Y0
Ovv vv ivv
Total Nickel
43
5
KM
09/10/2014 12:48
SW 6010C
Total Lead
40
5
KM
09/10/2014 12:48
SW 6010C
Total Arsenic
5.0
3.0
KM
09/10/2014 12:48
SW 6010C
Total Mercury
1.4
0.4
KM
09/08/2014 09:00
SW-7471 B
Total Selenium
6.0
5.0
KM
09/10/2014 12:48
SW 6010C
pH (Standard Units) *
5.91
2.00
JM
09/08/2014 07:30
SW-9045D
Total Molybdenum
8
5
KM
09/10/2014 12:48
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMTIS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
J
Debbie Holt
SAMPLING LOG # o� imc' CHAIN OF CUSTODY
111'IuI�I��IIIII�IIIII�III�B��Ig1�II�IINI'N�Ilill,RECORRECORD ANALYSIS
CUSTOMER: SYNAGRO SOUTHEAST SYNAGROCENTRALLLCrROXBORO 13.3046
.w 'f
ROXBORO CAK6'NC CERT#257 r the proper field sampling procedures
PROJECT MANAGER: r' during the collection of these samples.
i
Phone: SAM Ll=Ft Y
A & L CUSTOMER
SAMPLING
SAMPLE
TYPE
# OF
CONTAINERS
SAMPLING
DATE TIMEn
METHOD METHOD
PRESERVED SHIPPED
LAB # SAMPLE I.D.
LOCATION
ts7l(. f
I r
/!k 3 I
Relinquished by Sampler:
Timb
Recieved by.
REMARKS.
/Datyer
Relinquished by:
Date Time
Recieved by:
fec�i
`� �3FSf,�S5z15'
0 ! �7;
3
Relinquished by: Da e Time Recieved by:
SPECIAL INSTRUCTIONS:
For monitoring purposes. PO#:
ANALYSIS REQUEST
SAMPLE CaCO3 Volatile
I.D. SL1 SL2 NH, N NO3 N Organic Cd Cr NI Pb As H Se M Mo CI NO2 N
9 p equiv. Solids
r
10 POO k0o"' J009 k0or k0 Poo, loot 10 100 iO kooIr POO 10"
SL1: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
White — A & L Canary — MANAGER COPY
kL
Sodium Absorption Ratio calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2102-01-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 9/3/2014 1011/2014-12/31/2014 1.0015
CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (1030 x 29.0300) =100 = 299.009
Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (16700 x 29.0300) + 100 = 4848.01
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3910 x 29.0300) _ 100 = 1135.07
Na meq = Na mg/I _ Molec.Wgt.Na = 299.009 = 23 = 13.0004
Ca meq = Ca mg/1 = Molec.Wgt.Ca = 4848.01 _ 20 = 242.401
Mg meq = Mg mg/1.= Molec.Wgt.Mg = 1135.07 = 12 = 94.5894
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 13.0004 = SgrRoot[0.5(242.401+94.5894)] = 1.00153
Printed: 1 /30/2015
Page 1 17:01
1
Page: 1 of 2
Report Number: 14-248-0201
Account Number: 46487
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028.
Y�
L A&L Eastern Laboratories, Inc.__
7621 Whitepine Road Richmond, Virginia 23237 (804)'743-9401 Fax (804) 271-6446
wwwaleastem.com
Project: ROXBORO DB
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/3/2014 08:30:00
Lab Number: 57428 Date Received: 09/05/2014 00:00
Sample Id : ROXBORO DB Date Reported: 09/11/2014
Total Solids *
77.76
777600
100.0
MW
09/08/2014 08:05
SM-2540G
Moisture *
22.24
100.0
MW
09/08/2014 08:05
SM-2540G
Total Kjeldahl Nitrogen
1.99
19900
10.0
JM
09/08/2014 08:44
SM-4500-NH3C-TKN
Total Phosphorus
0.96
9570
100
KM
09/10/2014 12:48
SW 6010C
Total Potassium
0.30
2970
100.
KM
09/10/2014 12:48
SW 6010C
Total Sulfur
0.35
3470
100
KM
09/10/2014 12:48
SW 6010C
Total Calcium
0.70
6980
100
KM
09/10/2014 12:48
SW 6010C
Total Magnesium
0.34
3410
100
KM
09/10/2014 12:48
SW 6010C
Total Sodium
0.05
498
100
KM
09/10/2014 12:48
SW 6010C
Total Iron
40500
100
KM
09/10/2014 12:48
SW 6010C
Total Aluminum
38700
100
KM
09/10/2014 12:48
SW 6010C
Total Manganese
865
5
KM
09/10/2014 12:48
SW 6010C
Total Copper
269
5
KM
09/10/2014 12:48
SW 6010C
Total Zinc
489
5
KM
09/10/2014 12:48
SW 6010C
Ammonia Nitrogen
0.08
849
10.0
JM
09/08/2014 08:44
SM-4500-NH3C
Organic N
1.91
19051
10.0
09/08/2014 08:44
CALCULATION
Nitrate+Nitrite-N
264
2.00
JM
09/08/2014 08:45
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
09/10/2014 12:48
SW 6010C
All values are on a dry weight basis except as noted' by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-248-0201
Account Number: 46487
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57428
Sample Id: ROXBORO DB
99,A&L EasternLaboratories, Inc.
7621 Whltepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446
www.aleastern.com
Project: ROXBORO DB
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/3/2014 08:30:00
Date Received: 09/05/2014 00:00
Date Reported: 09/11/2014
Total Chromium
73
5
KM
09/10/2014 12:48
SW 6010C
Total Nickel
32
5
KM
09/10/2014 12:48
SW 6010C
Total Lead
28
5
KM
09/10/2014 12:48
SW 6010C
Total Arsenic
6.0
3.0
KM
09/10/2014 12:48
SW 6010C
Total Mercury
0.5
0.4
KM
09/08/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
09/10/2014 12:48
SW 6010C
pH (Standard Units) *
5.81
2.00
JM
09/08/2014 07:30
SW-9045D
Total Molybdenum
<5
5
KM
09/10/2014 12:48
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMTIS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SAMPLING LOG #
r#ii
CUSTOMER: SYNAGRO SOUTHEAST
PROJECT MANAGER:
Phone: )n 16,
t4-248-
us 11111111 44O
01
14SYNAGRO CENTRAL
CHAIN OF CUSTODY
RECORD & ANALYSIS
RECORD
ROXBORO [)WNC CERT#n7 14, �
1per neld sampling P10-ar —
were used during the collection of these samples.
SAMPLER,
A & L CUSTOMER SAMPLING
SAMPLE #OF
CONTAINERS
SAMPLING METHOD METHOD
DATE TIME PRESERVED SHIPPED
LAB # SAMPLE I.D. LOCATION
TYPE
Date
Time Recieved by:
REMARKS:
Relinquished by Sampler,
Time Recieved by:
Date
Relinquished by:
1305LIT
Relinquished by:
Dale
Time Recieved by:
SPECIAL INSTRUCTIONS:
monitoring purposes.
For STATE)
ANALYSIS REQUEST
SAMPLEOrganic
Se
I.D. SL1 I SL2 N Cd Cr Ni Pb As Hg
PO#:
PH CaCO Volatile Mo
I eawV31 Solids I
10#0 loo k#00 1400 k0or k0or 10#0 tow k000 ( k000 1000 1.000
01
SLII: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SI-2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
White-A&L Canary - MANAGER COPY
100"'
C1 NO2NI __j
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name' Sample Date Report Range Ratio
2102-01-MIX-NC ROXBORO, NC WWTP/WTP MIX 9/3/2014 10/112014-12/31/2014 1.0731
Na mg/1= (Na mg/kg x % Solids) _ 100 = (498 x 77.7600) = 100 = 387.245
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6980 x 77.7600) _ 100 = 5427.65
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3410 x 77.7600) = 100 = 2651.62
Na meq = Na mg/I + Molec.Wgt.Na = 387.245 _ 23 = 16.8367
Ca meq = Ca mg/1= Molec.Wgt.Ca = 5427.65 _ 20 = 271.382
Mg meq = Mg mg/I = Molec.Wgt.Mg = 2651.62 = 12 = 220.968
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 16.8367 = SgrRoot[0.5(271.382+220.968)] = 1.07309
Printed: 1/30/2015
Page 1 17:09
Page: 1 of 2
Report Number: 14-309-0206
Account Number: 46487
Submitted By: NATE ROTH
Send To: SYNAGRO CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 58525
Sample Id : ROXBORO WWTP MIX
A&L Eastern Laboratories, Inc.
7621,Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446
www.aleastem.com
Project: ROXBORO WWTP MIX
. NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:30:00
Date Received: 11/05/2014 00:00
Date Reported: 11/11/2014
Total Solids *
34.93
349300
100.0
BW
11/05/2014 14:30
SM-254OG
Moisture
65.07
100.0
BW
11/05/201414:30
SM-254OG
Total Kjeldahl.Nitrogen:
2.08
20800
10.0
JM
11/06/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
1.26
12600
100
KM
11/06/2014 11:19
SW 6010C
Total Potassium
0.26
2630
100
KM
11/06/2014 11:19
SW 6010C
Total Sulfur
0.53
5330
100
KM
11/06/2014 11:19
SW 6010C
Total Calcium
1.05
10500
100
KM
11/06/2014 11:19
SW 6010C
Total Magnesium
0.33
3340
100
KM
11/06/2014 11:19
SW 6010C
Total Sodium,
0.06
553
100
KM
11/06/2014 11:19
SW 6010C
Total Iron
34600
100
KM
11/06/2014 11:19
SW 6010C
Total Aluminum
39700
100
KM
11/06/2014 11:19
SW 6010C
Total Manganese
1050
5
KM
11/06/2014 11:19
SW 6010C
Total Copper
362
5
KM
11/06/2014 11:19
SW 6010C
Total Zinc
656
5
KM
11/06/2014 11:19
SW 6010C
Ammonia Nitrogen
0.35
3520
10.0
JM
11/06/2014 08:19
SM-4500-NH3C
Organic N
1.73
17280
10.0
11/06/2014 08:19
CALCULATION
Nitrate+Nitrite-N
91.0
2.00
JM
11/06/2014 08:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
11/06/2014 11:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. \ //
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made , (`�%�.
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-309-0206
Account Number: 46487
Submitted By: NATE ROTH
Send To:. SYNAGRO CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58525
Sample Id: ROXBORO WWTP MIX
AFL Eastern. Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446
www,aleastern.com
Project: ROXBORO WWTP MIX
NC CERT#257
REPORT OFANALYS/S Date Sampled: 11/4/2014 10:30:00
Date Received: 11/05/2014 00:00
Date Reported: 11/11/2014
Total Chromium
77
5
KM
11/06/2014 11:19
SW 6010C
Total Nickel
34
5
KM
11/06/2014 11:19
SW 6010C
Total Lead
28
5
KM
11/06/2014 11:19
SW 6010C
Total Arsenic
7.0
3.0
KM
11/06/2014 11:19
SW 6010C
Total Mercury
2.4
0.4
KM
11/06/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
11/06/2014 11:19
SW 6010C
pH (Standard Units) *
7.65
2.00
JM
11/06/2014 08:19
SW-9045D
Total Volatile Solids
34.06 340600
100.0
BW
11/05/2014 14:30
SM-2540G
Total Molybdenum
<5
5
KM
11/06/2014 11:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "K" AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2102-01-MIX-NC. ROXBORO, NC WWTP/WTP MIX 11/4/2014 / / - / / 0.7090
Na mg/I = (Na mg/kg x % Solids) _ 100 = (553 x 34.9300) _ 100 = 193.163
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (10500 x 34.9300) t- 100 = 3667.65
Mg mg/1 = (mg mg/kg x % Solids) = 100 = (3340 x 34.9300) _ 100 = 1166.66
Na meq = Na mg/I = Molec.Wgt.Na = 193.163 + 23 = 8.39839
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 3667.65 = 20 = 183.382
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 1166.66 + 12 = 97.2218
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.39839 = SgrRoot[0.5(183.382+97.2218)] = 0.709028
Printed: 1 /30/2015
Page 1 17:09
Page: 1 of 2
Report Number: 14-309-0205
Account Number: 46487
Submitted By: NATE ROTH
Send To: SYNAGRO,CENTRAL LLC/ROXBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58524;
Sample Id: ROXBORO WWTP CENTRIFUGE MAT
y3° A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 FaX (804) 271.6446
wwwaleastemxom
Project: ROXBORO WWTP CENTRIFUGE MAT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:00:00
Date Received: 11/05/2014 00:00
Date Reported: 11/11/2014
Total Solids
23.33
233300
100.0
BW
11/05/2014 14:30
SM-2540G
Moisture "
76.67
100.0
BW
11/05/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
3.79
37900
10.0
JM
11/06/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
1.91
19100
100
KM
11/06/2014 11:19
SW 6010C
Total Potassium
0.23
2310
100
KM
11/06/2014 11:19
SW 6010C
Total Sulfur
0.90
8950
100
KM
11/06/2014 11:19
SW 6010C
Total Calcium
1.50
15000
100
KM
11/06/2014 11:19
SW 6010C
Total Magnesium
0.37
3700
100
KM
11/06/2014 11:19
SW 6010C
Total Sodium
0.08
817
100
KM
11/06/2014 11:19
SW 6010C
Total Iron
25200
100
KM
11/06/2014 11:19
SW 6010C
Total Aluminum
30200
100
KM
11/06/2014 11:19
SW 6010C
Total Manganese
1100
5
KM
11/06/2014 11:19
SW 6010C
Total Copper
592
5
KM
11/06/2014 11:19
SW 6010C
Total Zinc
1130
5
KM
11/06/2014 11:19
SW 6010C
Ammonia Nitrogen
0.47
4710
10.0
JM
11/06/2014 08:19
SM-4500-NH3C
Organic N
3.32
33190
10.0
11/06/2014 08:19
CALCULATION
Nitrate+Nitrite-N
1090
2.00
JM
11/06/2014 08:20
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
11/06/2014 11:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made9,&U,LNK.t✓
�%
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14309-0205 n4J( /`► &L Eastern Laboratories, Inc.
Account Number: 46487 M ii1 7621 Whitepine Road Richmond; Virginia 23237 (804)-743-9401 Fax (804) 271.6446
Submitted By: NATE ROTH www.aleastern.com -
Send To: SYNAGRO'CENTRAL LLC/ROXBORO Project: ROXBORO WWTP CENTRIFUGE MAT
Mary Brewer NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:00:00
Lab Number: 58524 Date Received: 11/05/2014 00:00
Sample Id': ROXBORO WWTP CENTRIFUGE MAT Date Reported: 11/11/2014
Total Chromium
75
5
KM
11/06/2014 11:19
SW 6010C
Total Nickel
38
5
KM
11/06/2014 11:19
SW 6010C
Total Lead
40
5
KM
11/06/2014 11:19
SW 6010C
Total Arsenic
5.0
3.0
KM
11/06/2014 11:19
SW 6010C
Total Mercury
1.3
0.4
KM
11/06/2014 09:00
SW-7471B
Total Selenium
6.0
5.0
KM
11/06/2014 11:19
SW 6010C
pH (Standard Units) "
5.79
2.00
JM
11/06/2014 08:19
SW-9045D
Total Volatile Solids
55.67 556700
100.0
BW
11/05/2014 14:30
SM-254OG
Total Molybdenum
6
5
KM
11/06/2014 11:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "K" AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2102-01-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 11/4/2014 / / - / / 0.7459
CAKE
Na mg/1= (Na mg/kg x % Solids) _ 100 = (817 x 23.3300) =100 190.606
Ca mg/1= (Ca mg/kg x % Solids) = 100 = (15000 x 23.3300) + 100 = 3499.5
Mg mg/[ = (mg mg/kg x % Solids) _ 100 = (3700 x 23.3300) + 100 = 863.21
Na meq = Na mg/I = Molec.Wgt.Na=.190.606 + 23 = 8.28722
Ca meq = Ca mg/1= Molec.Wgt.Ca = 3499.5 + 20 = 174.975
Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 863.21 + 12 = 71.9342
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.28722 _ SgrRoot[0.5(174.975+71.9342)] = 0.745857
Page 1
Printed: 1/30/2015
17:01
FACILITY NAME: ROXBORO, NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 86.06
OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/30/14
224.00 (CY)
14.933
29.03
3.651
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
10/31/14
128.00 (CY)
8.533
29.03
2.086
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Oct-14
352.00 (CY)
23.466
Total Cubic Yds/Ac: 23.47
TOTALS:
Annual lbs/acre
Cumulative lbs/acre
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
161
0.057
0.023
1.056
6.656
0.459
0.016
0.092
0.493
0.069
13.311
246.72
0.966
0.180
8.057
40.665
4.176
0.124
0.764
4.821
0.516
69.784
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
...
_
-
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
c Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 3.91
OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 0.70 ACRES PERMITTED: 0.70
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/31/14
16.00 (CY)
22.857
29.03
5.589
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
TT7.3,690.00
p
1 772.00 p
14020
FESCUE
Oct-14
16.00 (CY)
22.857
Total Cubic YdstAc: 22.86
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.056
0.022
1.028
6.483
0.447
0.016
0.089
0.481
0.067
12.965
24031
157
Cumulative lbs/acre
0.665
I
1 0.108
1 5.845
1 29.939
-
1 3.036
0.083
0.538
I
1 3.865
0.315
49.878
F
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
""
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L�
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X ✓ /S�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 7.82
OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60
Page
Lime Applied ***
Date
Lb./A.
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
TPer Acre
Solids
10/31/14
32.00 (CY)
20.000
29.03
4.890
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Oct-14
32.00 (CY)
20.000
rota[ uub[C YOSIAc: 20.U0
As
Cd
Cr
Cu
Pb
I-Ig
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.049
0.020
0.900
5.672
0.391
0.014
0.078
0.421
0.059
11.345
210.27
137
Cumulative lbs/acre
0.729
0.110
6.119
1 30.033
2.968
0.086
0.551
1 3.832
0.299
49.112
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
. �kvlZf�— o�oy/,r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0001 A
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0021826 ANNUAL DRY TONS APPLIED: 97.80
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.50 ACRES PERMITTED: 17.50
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/4/14
400.00 (CY)
22.857
29.03
5.589
ROAEDC
DRY ,
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Nov-14
400.00 (CY)
22.857
Total Cubic Yds/Ac: 22.86
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:.
157
Annual lbs/acre
0.056
0.022
1.028
6.483
0.447
0.016
0.089
0.481
0.067
12.965
240.31
Cumulative lbs/acre
1.406
0.231
10.491
49.195
5.731
0.142
1.071
1 6.700
0.566
81.232
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
12
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0001 B
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 12.23
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 2.50 ACRES PERMITTED: 2.50
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/5/14
50.00 (CY)
20.000
29.03
4.890
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Nov-14
50.00 (CY)
1 20.000
Total Cubic Yds/Ac: 20.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
137
Annual lbs/acre
0.049
0.020
0.900
5.672
0.391
0.014
0.078
0.421
0.059
11.345
210.27
Cumulative lbs/acre
0.825
0.150
6.992
36.079
3.658
0.112
0.650
4.114
0.451
62.327
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop-
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X (fit 210
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/hicorporation 1.0
e Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields'where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0021826 ANNUAL DRY TONS APPLIED: 30.56
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/5/14
125.00 (CY)
20.161
29.03
4.929
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
1 772.00 p
14120
1 FESCUE
Nov-14
125.00 (CY)
20.161
Total Cubic Yds/Ac: 20.16
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.049
0.020
0.907
5.718
0.394
0.014
0.079
0.424
0.059
11.436 211.97
138
Cumulative lbs/acre
0.478
0.076
4.206
22.335
1 1.904
0.051
0.384
2.757
0.273
37.391
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X ,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0003
RESIDUAL SOURCE(S):*. See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 30.56
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.10 ACRES PERMITTED: 6.10
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/5/14
50.00 (CY)
8.197
29.03
2.004
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
I FESCUE
11/6/14
75.00 (CY)
12.295
29.03
3.006
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Nov-14
1 125.00 (CY)
20.492
Total Cubic Yds/Ac: 20.49
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
140
Annual lbs/acre
0.050
0.020
0.922
5.812
0.401
0.014
0.080
0.431
0.060
11.624 215.44
Cumulative lbs/acre
0.953
0.151
6.335
27.914
3.766
0.087
0.709
3.785
0.294
47.874
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 30.56
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20
Page: 1
Lime Applied ***
Date I Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppni)
Crop
MONTH
Total
Per Acre
Solids
11/5/14
125.00 (CY)
20.161
29.03
4.929
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
TT7.3,690.00
p
1 772.00 p
14020
FESCUE
Nov-14
125.00 (CY)
20.161
i otal uublc Y USIAC: 2U.16
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.049
0.020
0.907
5.718
0.394
0.014
0.079
0.424
0.059
11.436 211.97
138
Cumulative Ibs/acre
1.083
0.172
7.335
31.895
4.385
0.097
0.815
4.685
0.320
53.199
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
(
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X ,G� Dz��
(SIGNAT&E OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 3.91
OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 0.90 ACRES PERMITTED: 0.90
Page: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
I1/5/14
16.00 (CY)
17.778
29.03
4.347
ROAEDC
DRY
0-<I/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
1 772.00 p
14020
FESCUE
Nov-14
16.00 (CY)
17.778
Total Cubic Yds/Ac: 17.78
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
122
Annual Ibs/acre
0.043
0.017
0.800
5.042
0.348
0.012
0.070
0.374
0.052
10.084
186.91
Cumulative lbs/acre
0.981
1 0.168
6.510
27.451
1 3.973
0.076
0.763
1 4.437
0.306
45.038I
F
"
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
212
FD Cumulative I Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
`
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
XS-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: HENRY MARTIN
SITE #: NC PS 00026 FIELD# : PS 00026 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 12.23
OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.20 ACRES PERMITTED: 3.20
Page : 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pptll)
Crop
MONTH
Total
Per Acre
Solids
12/15/14
50.00 (CY)
15.625
29.03
3.820
ROAEDC
MOIST
0-11/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Dec-14
50.00 (CY)
15.625
Total Cubic Yds/Ac: 15.63
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
107
Annual lbs/acre
0.038
0.015
0.703
4.432
0.306
0.011
0.061
0.329
0.046
8.863
164.27
Cumulative lbs/acre
1.417
0.223
9.566
44900
5.730
0.122
1.075
6.210
0.554
77.190
2 11
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
""
'" "`
--
. •
-.
4
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X �\ p O ; e/
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation " 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page
FACILITY NAME: ROXBORO, NC PREDOMINANT SOIL SERIES: HERNDON Lime Applied ***
OWNER: HENRY MARTIN PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 24.45 Date Lbs/Ae
SITE #: NC PS 00026 FIELD# : PS 00026 0002 OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70
Total Cubic YdstAc: 17.54
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
120
Annual lbs/acre
0.043
0.017
0.789
4.976
0.343
0.012
0.069
0.369
0.051
9.952
184.45
Cumulative lbs/acre
1.574
1 0.251
10.859
49.373
1 6.550
0.135
1.211
1 7.279
1 0.548
82.998
Pennit PAN Limit (lbs/acre) 1st Crop/2nd Crop
2 11
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
W,
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X /1 �f� 'T/ / ✓
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be.applied in 2015
FACILITY NAME: ROXBORO, NC
OWNER: HENRY MARTIN
SITE #: NC PS 00026 FIELD# : PS 00026 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 91.69
OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.60 ACRES PERMITTED: 15.60
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
12/5/14
250.00 (CY)
16.026
29.03
3.918
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
0
F140220
I FESCUE
12/6/14
25.00 (CY)
1.603
29.03
0.392
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
I FESCUE
12/15/14
100.00 (CY)
6.410
29.03
1.567
ROAEDC
MOIST
0-<1/2"
SUR
0.5
0.30
41,700. p
3,690.00 p
772.00 p
14020
FESCUE
Dec-14
375.00 (CY)l
24.039
Total Cubic YastAc: 24.U4
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
165
Annual lbs/acre
0.059
0.024
1.081
6.818
0.470
0.016
0.094
0.505
0.071
13.636
252.73
Cumulative lbs/acre
1.584
0.268
10.925
50.029
6.642
0.147
1.225
6.915
0.594
85.668
11
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
.
212
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
!
1339.0
267.9
15.0 375.0
89.0
2500.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
X v �G���
(SIGNAT RE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
F-.HVIAON1QE'td�AL.��13C7f3hlRG7�� lrtr~
.�rrai�+tit;allw�;�Eaar'�Ye�I'1�� -
September 22, 2014
Marshall Puryear
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Roxboro WWTP
Dear Marshall Puryear:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX. (330) 253-4489
Website: hIIDAvtviv.settek.com
Order No.: 14090554
Summit Environmental Technologies, Inc. received 1 sample(s) on 9/5/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
N �-
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho 01-100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3,
Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940,
Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8
8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vennont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and
9957C and E87688, Wisconsin 399013010
Page 1 of 6
Summit Environmental Technologies, Inc. Workorder
v g 3310 Win St.
P° Afli OONfilEAJTAL"TEC:8' OLOC)'c5r im- ,, Cuyahoga Falls, Ohio 44223 Sample .Summary
�krrae rcal iai a to '1Q TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14090554
Website: htto:llivivw.settek.coin 22-Sep-14
CLIENT: Synagro
Project: Roxboro WWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
14090554-001 Roxboro WWTP 9/3/2014 9:00:00 AM 9/5/2014 10:15:00 AM Solid
Page 2 of 6
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX- (330) 253-4489
Website: httQ.1Aviviv.settek.cont
CLIENT: Synagro
Project: Roxboro WWTP
Case Narrative
WO#: 14090554
Date: 9/22/2014
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ)
but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with
these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any con-iments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 6
SununitEnvironniental Technologies, Inc. WO#: 14090554
MINI
SuffiAAA115 3310 Win St.
FNVIRONME'N'r l-7 CHUCiLQGM5, 9P=G Cuyahoga Falls, Ohio 44223 Date Reported 9/22/2014
Ia'raiytital CesEzai 3t0,,9es TEL: (330) 253-8211 FAX (330) 253-4489 Company: Synagro
Website: hQ:1Anvw.settek.com
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 9/5/2014
Project#: Roxboro WWTP
TCLP Metals Analysis (6010)
Client IN
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Roxboro WWTP
001
9/3/2014 TCLP Arsenic(As)
0.50 ND mg/L
Solid
EPA 6010 C
1
5.0
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Badum(Ba)
5.0 ND mg/L
Solid
EPA 6010 C
1
100
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Cadmium(Cd)
0.10 ND mg/L
Solid
EPA 6010 C
1
1.0
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Chromium(Cr)
0.20 ND mg/L
Solid
EPA 6010 C
1
5.0
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Lead(Pb)
0.50 ND mg/L
Solid
EPA 6010 C
1
5.0
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Selenium(Se)
0.50 ND mg/L
Solid
EPA 6010 C
1
1.0
9/11/2014
VVK
Roxboro WWTP
001
9/3/2014 TCLP Silver(Ag)
0.50 ND mg/L
Solid
EPA 6010 C
1
5.0
9/11/2014
VVK
TCLP Mercury Analysis (1311/7470)
Client ID#
Lab IN Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Roxboro WWTP
001
9/3/2014 TCLP Mercury
0.0020 ND mg/L
Solid
EPA 7470 A
1
0.20
9/10/2014
ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Roxboro WWTP
001
9/3/2014 Chlordane, total
0.010 ND mg/L
Solid
EPA 8081 B
1
0.030
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 Toxaphene
0.10 ND mg/L
Solid
EPA 8081 B
1
0.50
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 Endrin
0.0020 ND mg/L
Solid
EPA 8081 B
1
0.020
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 gamma-BHC
0.0020 ND mg/L
Solid
EPA 8081 B
1
0.40
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 Heptachlor
0.0020 ND mg/L
Solid
EPA 8081 B
1
0.0080
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 Heptachlor epoxide
0.0020 ND mg/L
Solid
EPA 8081 B
1
0.0080
9/12/2014
JBN
Roxboro WWTP
001
9/3/2014 Methoxychlor
0.0020 ND mg/L
Solid
EPA 8081 B
1
10
9/12/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Roxboro WWTP
001
9/3/2014
1,1-Dichloroethene
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
1,2-Dichloroethane
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Benzene
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Carbon tetrachloride
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Chlorobenzene
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Chloroform
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Tetrachloroethene
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Trichloroethene
0.10
ND mg/L
Roxboro WWTP
001
9/3/2014
Vinyl chloride
0.20
ND mg/L
Roxboro WWTP
001
9/3/2014
MEK
2.0
ND mg/L
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
Solid
EPA 8260 B 1
0.70
9/10/2014
MES
0.50
9/10/2014
MES
0.50
9/10/2014
MES
0.50
9/10/2014
MES
100
9/10/2014
MES
6.0
9/10/2014
MES
0.70
9/10/2014
MES
0.50
9/10/2014
MES
0.20
9/10/2014
MES
200
9/10/2014
MES
Page 4 of 6
f
�'
let
SzznunitEnvironmental Technologies, Inc.
3310 Win St.
W04:
14090554
EO'VI}3tly MENTALTPCHNOL.d ]8$�J G
Cuyahoga Falls, Ohio 44223
Date Reported
9/22/2014
>natyfvc ni'!_,�ii�rr?te7i3er
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro
Website: ham:1Avivw.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
9/5/2014
Project#:
Roxboro WWTP
SVOC 8270 TCLP BNA List
Client II)# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Roxboro WWTP
001
9/3/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
2,4,6-Trich lorophenol
0.25
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Cresols, Total
5.0
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Hexachloro-1,3-
0.10
ND mg/L
Solid
EPA 8270 C 1
butadiene
Roxboro WWTP
001
9/3/2014
Hexachlorobenzene
0.10
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Hexachloroethane
0.10
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Nitrobenzene
0.10
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Pentachlorophenol
0.25
ND mg/L
Solid
EPA 8270 C 1
Roxboro WWTP
001
9/3/2014
Pyridine
0.25
ND mg/L
Solid
EPA 8270 C 1
SVOC SW-846: 8321 Herbicides-TCLP
7.5
9/17/2014
JRT
400
9/17/2014
JRT
2.0
9/17/2014
JRT
0.13
9/17/2014
JRT
200
9/17/2014
JRT
0.50
9/17/2614
JRT
0.13
9/17/2014
JRT
3.0
9/17/2014
JRT
2.0
9/17/2014
JRT
100
9/17/2014
JRT
5.0
9/17/2014
JRT
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Roxboro WWTP 001 9/3/2014 2,4-D 5.0 ND mg/L Solid EPA 8321 A 1 10 9/15/2014 AMZ
Roxboro WWTP 001 9/3/2014 2,4,5-TP 0.50 ND mg/L Solid EPA 8321 A 1 1.0 9/15/2014 AMZ
Page 5 of 6
Summit Environmental Technologies, Inc.
3310 Win St.
WO#: 14090554
EHVIRt 14MENTAL;3`£CH6'+•"OL,=
Si INC
Cuyahoga Falls, Ohio 44223
Date Reported 9/22/2014
LT f.r m'Wi6al
TEL: (330)
253-8211 FAX.- (330) 253-4489
Company: Synagro
Website: hLW:Ilmvw.settek.con:
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 9/5/2014
Project#: Roxboro WWTP
Client ID# Lab ID# Collected Analyte
Result Units
Matrix Method DF RL
Run Analyst
Roxboro WWTP 001 9/3/2014
Flashpoint (140°F)
>140 °F
Solid EPA 1010 1
9/9/2014 TAH
Roxboro WWTP 001 9/3/2014
Cyanide, Reactive
ND ppm
Solid EPA 9014 1 0.50
9/9/2014 TIR
Roxboro WWTP 001 9/3/2014
pH
6.9 s.u.
Solid EPA 9045 D 1
9/8/2014 AYS
Roxboro WWTP 001 9/3/2014
Sulfide, Reactive
ND ppm
Solid EPA 9034 1 25
9/9/2014 TIR
Page 6 of 6
l' .
DC-7
Rev 13
08/21/14
Summit Environmental Technologies, Inc.
Cooler Receipt Form
Initials of person inspecting cooler and samples �7c
Client: c �11r KaUfi _ _.._ ,� Order Number:
Date Received: Tote Received1 yr5_ Date/Time coolers) opened and samples inspectedgL:j±L�jjt�
Number of Coolers/Boxes- _ _ _I_ _ NIA
Shipper: QE20 UPS DHL Airborne US Postal Walk-in Pickup Other
Packaging Peanuts Bubble Wrap Paper
Foam None
Tape on cooterlbox
N WA
sc ti•r,ti
Custody Seats intact
YATAT
C-O-C in plastic
N
NIA
Sc ty-5-ry
lee Blue ice I/
present
I absent I melted NIA
Sample Temperature IR Gun #16020459 CF_D.°C
+-7 °C-y
N/A
Radiological Testing Instrument serial * 1 7
Y
Z
NIA
(see page 2 for scan results)
"Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified
Immediately.
C-O-C fitted out property
l /
N
NIA
Samples in separate bags
Y
N
Q;I
Sample containers intact'
01
N
N/A
'If no, Fist broken sample(s)
Sample labels) complete (ID, date, etc.)
Label(s) agree with C-O-C
Correct containers used
Sufficient sample received
Bubbles absent from 40 mL vials"
Y
— Samples with bubbles <6mm are acceptable
Indicate bubble size d >6mm.
Was client contacted about samples
Y N
Will client send new samples
Y N
Client contact:
DatelTime:
Logged in by:
Comments:
N
N
N
N
K
NIA
NIA
NIA
NIA
NIA
G:1QC SHAREMDocument Control Templates - TrackinglCooler reeetpt form Rev. 13 08-28-14.doc Page 1 of 2
F---� Summit Environmental Iechnolt)gies, h1c.
=rdol!] Analysis Request/Chain of Custody
3,310 Win Street h(,r Summit Envirtmilicnial Ted,11010gic'- 111' USC 001%
n]
Cuphop Falls. Ohio 44223 Tel: 330,253.9211 Fax: 330,253.4-IS" Z� Pit ,,e
CoinvanvNanw FW(—)jmk Name Analytical ha tarn and jMethods
C0116—anvy" 'Ad, S Project AddressC, X,
/ t 70:2
Oc j l
Client Phone No, Report lo
C Isent hux No, E] P0#
Client Email -Quoic No. it
C1511factfPerNolk It
J,
Ufleck if (,)Ili' A
Sim)P19d b)
# Sample Identirication nllecteJ erte7.
,IT—tv rune Vcvi%ccIts: iatv 'tints
F;`i ,c�. linents,
Date Fillic
Rush Retlueste
the pt
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: . City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number: NC 0021024
Monitoring Period: From 01/01/14 To 03/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if ., ..1;..., l.lo +., .,14o n4:. .-f nrl id"Inve A nv !lace M rmmnla4n fhn fnllnwina mnni+nrina data[
Parameter
Allowable Level in Sludge
Pathogen . Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'h
CFU
CFU/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MP NO LAND APPLICATION THIS PERIOD
total solids
3 MPN per
Salmonella
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer Name nd Titl ( type or print)
1 ��, a_lors
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
ROXBORC /TP LAB
DIGESTER
"COOLER"
SLUDGE
DGE
% TOTAL RESIDUE .- .OLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Jason Wilson Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
RPD"S
ANALYST
INITIALS
1/7/14
1/7/2014
6
35
70.9170
106.3440
35.4270
70.9173
.0003
Blank
70.917
.0003
Blank
JW
8:30 AM
1/6/2014
4
35
70.4084
105.6505
35.2421
70.7578
.3494
0.99
70.5310
.2268
65
JW
1/6/2014
9
35
73.4440
107.8052
34.3612
73.7858
.3418
0.99
73.5650
.2208
65
JW
1/14/2014
1/14/2014
4
35
70.4090
105.3732
34.9642
70.4090
.0000
Blank
70.4090
.0000
Blank
JW
8:00 AM
1/13/2014
6
35
70.9179
105.5233
34.6054
71.2106
.2927
0.85
71.0187
.1919
66
JW
1/13/2014
9
35
73.4453
108.2050
34.7597
73.7395
.2942
0.85
73.5475
.1920
65
JW
1/21/2014
1/21/2014
4
35
70.4087
105.3128
34.9041
70.4086
-.0001
Blank
70.4085
.0001
Blank
Jw
8:30 AM
1/20/2014
9b
35
72.5505
107.3402
34.7897
72.8240
.2735
0.79
72.6461
.1779
65
JW
1/20/2014
6
35
70.9182
105.3116
34.3934
71.1898
.2716
0.79
71.0126
.1772
65
JW
1/29/14
1/29/2014
4
35
70.9177
105.8467
34.9290
70.9177
.0000
Blank
70.9174
.0003
Blank
JW
9:20 AM
1/27/2014
6
35
70.4083
105.7995
35.3912
70.6852
.2769
0.78
70.5067
.1785
64
JW
1/27/2014
9b
35
72.5502
107.7595
35.2093
72.8258
.2756
0.78
72.6477
.1781
65
JW
2/4/14
2/4/2014
6
35
70.9177
105.3976
34.4799
70.9178
.0001
Blank
70.9179
-.0001
Blank
CS
8:17 AM
2/3/2014
9
35
72.5504
105.9153
33.3649
72.8050
.2546
0.76
72.6420
.1630
64
CS
2/3/2014
4
35
70.4089
104.5435
34.1346
70.6692
.2603
0.76
70.5022
.1670
64
CS
2/10/14
2/10/2014
6
35
70.9171
105.0344
34.1173
70.9173
.0002
Blank
70.9173
.0000
Blank
CS
10:10 AM
2/10/2014
4
35
70.4093
104.2807
33.8714
70.6489
.2396
0.71
70.4939
.1550
65
CS
2/10/2014
9
35
73.4447
107.5212
34.0765
73.6860
.2413
0.71
73.5302
.1558
65
CS
VSR
0%
PASS
DC
x - Blank
2014 (First Quarter) VECTOR ATTRACTION CALCULATIONS
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxboro WWTP
WWTP Name: Roxboro WWTP NPDES Number:
Monitoring Period: From 4/01/14 To 6/30/14
WQ Permit Number:
WQ 0021826
NC 0021024
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class li complete the followin2 monitoring aata:
Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo. Mean Maximum Units dences Analysis
Fecal 2x10 to the 6 1h CFU CFU/g
Coliform power per gram
of total solids
CFU CFU/g
1000 MPN pei NO LAND APPLICATION THIS PERIOD
total solids (d
Salmonella I 3 MPN per 4
bacteria (in solids (dry
lieu of fecal
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
—Pix�arer Name d Title (type or print) Land Applier Name and Title (if applicable) (type or print)
rDA
Signature of Preparer late Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date
ROXBORO 'TP LAB
DIGESTER
"COOLER"
SLUDGE
% TOTAL RESIDUE L- _ JLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Jason Wilson Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
I
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
RPD"S
ANALYST
INITIALS
4/15/14
4/15/2014
1
35
78.2040
113.2590
35.0550
78.2040
.0000
Blank
78.204
.0000
Blank
JW
10:30am
4/14/2014
2
35
80.1507
115.8932
35.7425
80.4756
.3249
0.91
80.2558
.2198
68
JW
4/14/2014
9
35
72.5513
107.2444
34.6931
72.8696
.3183
0.92
72.6543
.2153
68
JW
4/21/2014
4/21/2014
1
35
78.2025
113.0606
34.8581
78.2028
.0003
Blank
78.2025
.0003
Blank
JW
9:00am
4/21/2014
2
35
80.1495
115.2770
35.1275
80.4285
.2790
0.79
80.2428
.1857
67
JW
4/21/2014
9
35
72.5499
107.7420
35.1921
72.8296
.2797
0.79
72.6428
.1868
67
JW
4/28/2014
4/28/2014
4
35
70.4076
105.4820
35.0744
70.4076
.0000
Blank
70.4076
.0000
Blank
JW
8:00am
4/28/2014
6
35
70.9163
105.9360
35.0197
71.2069
.2906
0.83
71.0092
.1977
68
JW
4/28/2014
9
35
73.4416
108.4340
34.9924
73.7075
.2659
0.76
73.5290
.1785
67
JW
5/5/14
5/5/2014
4
35
70.4073
105.7320
35.3247
70.4073
.0000
Blank
70.4073
.0000
Blank
JW
10:00am
5/5/2014
6
35
70.9162
106.0290
35.1128
71.1546
.2384
0.68
70.9990
.1556
65
JW
5/5/2014
9
35
72.5490
107.6712
35.1222
72.7894
.2404
0.68
72.6324
.1570
65
JW
5/13/14
5/12/2014
4
j 35
70.4071
105.8623
35.4552
70.4071
.0000
Blank
70.4071
.0000
Blank
JW
5/12/2014
6
35
70.9170
105.7935
34.8765
71.1188
.2018
0.58
70.9879
.1309
65
JW
5/12/2014
9
35
72.5499
107.5158
34.9659
72.7524
.2025
0.58
72.6211
.1313
65
JW
5/20/14
5/20/2014
1
35
78.2028
113.2232
35.0204
78.2025
-.0003
Blank
78.2027
-.0002
Blank
JW
5/19/2014
6
35
70.9168
105.9402
35.0234
71.1305
.2137
0.61
70.9943
.1362
64
JW
5/19/2014
9
35
72.5498
107.4247
34.8749
72.7624
.2126
0.61
72.6261
.1363
64
JW
VSR
16.7%
411�
DC
x - Blank
2014 ( Second Quarter) VECTOR ATTRACTION CALCULATIONS
ROXBORO WWTP LAB
% TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
DIGESTER Analyst: Jason Wilson, Crystal Shotwell
"COOLER"
si 1 inr.F
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
RPD"S
ANALYST
INITIALS
5/27/14
5/27/2014
1
35
78.2025
113.6370
35.4345
78.2023
-.0002 1
Blank
78.2025
-.0002
Blank
JW
9:45 AM
5/27/2014
6
35
70.9170
106.6385
35.7215
71.2038
.2868
0.80
71.0221
.1817
63
JW
5/27/2014
9
35
73.4409
108.9046
35,4637
73.7250
.2841
0.80
73.5447
.1803
63
JW
6/3/2014
6/3/2014
1
35
78.2024
113.2160
35.0136
78,2023
-.0001
Blank
78.2022
.0001
Blank
JW
8:20AM
6/3/2014
6
35
70.9168
105.9188
35.0020
71,1709
.2541
0.73
71.0091
.1618
64
JW
6/3/2014
9
35
72.5497
107.5970
35.0473
72.8014
.2517
0.72
72.6418
.1596
63
JW
6/10/2014
6/10/2014
1
35
78.2025
113.3531
35.1506
78.2025
.0000
Blank
78.2023
.0002
Blank
JW/CLS
8:00 AM
6/10/2014
6
35
70.9170
106.2242
35.3072
71.1563
.2393
0.68
71.0050
.1513
63
JW/CLS
6/10/2014
9
35
72.5484
107.9188
35.3704
72.7884
.2400
0.68
72.6379
.1505
63
JW/CLS
6/18/14
6/18/2014
1
35
78.2023
113.8240
j 35.6217
78.2025
.0002
Blank
78.2023
.0002
Blank
JW
8:00 AM
6/17/2014
6
35
70.9164
106.1305
35.2141
71.1424
.2260
0.64
71.0020
.1404
62
JW
6/17/2014
9
35
72.5489
107.8722
35.3233
72.7765
.2276
0.64
72.6349
.1416
62
JW
6/24/14
6/24/2014
1
35
78.2021
113.5701
35.3680
78.2022
.0001
Blank
78.2021
.0001
Blank
JW
8:20 AM
6/24/2014
6
35
70.9166
106.3015
35,3849
71.1383
.2217
0.63
71.0021
.1362
61
JW
6/24/2014
9
35
72.5492
107.6919
35.1427
72.7701
.2209
0.63
72.6345
.1356
61
JW
7/1/2014
7/1/2014
2
35
80.1492
115.8632
35.7140
80.1493
.0001
Blank
80,1491
.0002
Blank
JW
8:00 AM
7/1/2014
6
35
70.9168
106.1922
35.2754
71,1174
.2006
0.57
70.9940
1 .1234
62
JW
7/1/2014
9
35
73.4390
109.0218
1 35.5828
73.6424
.2034
0.57
73.5170
.1254
62
JW
VSR
4%
PASS
DC
x - Blank
West Lagoon 2014 (Second Quarter Re -do) VECTOR ATTRACTION CALCULATIONS
a.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number:- NC O021024
Monitoring Period: From 07/01/14 To 09/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class
A or Class 13 complete the following momtorm
data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
CFU
CFU/g
0
4/yr
Grab
9222D
Coliform .
power per gram
of total solids
CFU/g
CFU
1000 MPN pe NO LAND APPLICATION THIS PERIOD
total solids (d
Salmonella 3 MPN per 4
bacteria (in solids (dryl
lieu of fecal
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
, Option/Mt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why.you have not met one or both of the requirements.).
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer name And Title(print or type) Land Applier Name and Title (if applicable) (type or print)
a -,a
Signature of Preparer*f Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date
Meritech, Inc.
Environmental Laboratory
.« Laboratory Certiflcation No.165
Page 1
Contact: Marshall Puryear Report Date .. 9/8/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014
Meritech Work Order # 09031424 Sample: Roxboro WWTP Cake 1 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 26.14 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,530 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D Bl
Meritech Work Order #. 09031425 Sample: Roxboro WWTP Cake 2 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 26.16 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,780 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D 131
Meritech Work Order # 09031426 Sample: Roxboro WWTP Cake 3 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method ualifier
% Total Solids 3128 % 9/3/14 0-100 % - SM 2540B
Fecal Coliform (Sludge) < 27 col/g dry wt 9/3/14 27 col/g dry-wt SM 9222D B2
Meritech Work Order # 09031427 Sample: Roxboro WWTP Cake 4 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Metbod Qualifier
%Total Solids 25.99 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 35 col/g dry wt 9/3/14 35 col/g dry wt SM 9222D B2
Meritech Work Order # 09031428 Sample: Roxboro WWTP Cake 5 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
%Total Solids 31.45 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 29 col/g dry wt 9/3/14 29 col/g dry wt SM 9222D B2
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 nil.
B2 Counts from all filters were zero. The value reported is based on the number of colonies per 100 nil that
would have been reported if there had -been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
642 Tamco Road; Reidsville, Nortlr Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
X Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Marshall Puryear Report Date 9/8/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028. Date Sample Rcvd: 9/3/2014
Meritech Work Order # 09031429 Sample: Roxboro WWTP Cake 6 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method ualifier
Total Solids 24.7 % 9/3/14 0-100 % SM 2540E
Fecal Coliform (Sludge) 1,579 col/g cry wt 9/3/14 45 col/g dry wt SM 9222D
Meritech Work Order # 09031430 Sample: Roxboro WWTP Cake 7 Grab 9/3/14
Parameters Results Analysis Date Reporting Lim! Method Qualifier
% Total Solids 24.79 % 9/3/14 0-100,0/0 SM 2540B
Fecal Coliform (Sludge) 1,815 col/g dry wt _ 9/3/14 45 col/g dry wt SM 9222D
131 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 in].
132 Counts From all filters were zero. The value reported is based on the number of colonies per 100 nil that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
I hereby certify that I have reviewedand approve these data. [;{.
Laboratory Representative
642 Tatnco Road, Reidsville, North Carolfrra 27320
tel.(336)342-4748 fax.(336)342-1522
3.70-2033
Chain of Custody Record (COC)
NPDES#:
Client: AV Phone:
i -
MERI"wN Le
Address• !>Q i'Lf sk Fax:
ENVIRONMENTAL LABORATORIES
M oG�Ple— 7Z7o2? Email:
+
642 TamcoRd. Phone: 336-342-4748
Project:
Reidsville NC 27320 Fax: 336-342-1522
P.O.#:
Email: info@meritech-labs.com
Attention: AIAA%
Turn Around Time*
How would you like your report sent?
*RUSH work needs prior approval.
www.merl'Tech-I(D��-�is.com
=
StdllOdays)
Circle all that apply: Email (preferred) , Fax, Mail
3-5 Da s 24-48Hrs
.Sampling Dates & Times
Person Taking Sample (sign/Print):
Lab Use ®iniy
Sample Location and/or lD #
Start
End
Comp?
of
lest(s) Required
On Ice?.
Yes
pH OK?
Date
Time .
Date
Time
Grab?
Cont.
/ No
Cl OK?
c>sLa i�✓�v %' Grr(�
O ` D
r 4f0
L
'
Temperature.Upon
.Receipt
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN
samples must be done in the field prior to preservation. ***
Comments:
]Jug
Compositor#
Shipment:
[: UPS
#
Q: Fed Ex
Arethese esultsfor regulatory purposes? Yes
No
Report results in: mg/L [ :
mg/kg } ug/L (.
Q-Hand Delivery
Relinquis' ate �
,� 1 t��f�GD _
T m
'Z
Received by:
Date:
Time:
Other
Relinquis try: Date:
Time:
Received by.
Date:
Time:
Relinquished by: Date:
Time:
R ed by La _ •
Datk:..
Time,
l
Meritech, Inc®
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Marshall Puryear Report Date 9/8/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014
Meritechi Work Order # 09031431 Sample: Roxboro WWTP PB 1 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 36.52 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 25 col/g dry wt 9/3/14 25 col/g dry wt SM 9222D B2
Meritech Work Order # 09031432 Sample: Roxboro WWTP PB 2 Grab
Parameters Results Analysis Date Reporting Unit
9/3/14
Method Qualifier
%Total Solids 39.73 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 340 col/g drywt 9/3/14 45 col/g dry wt SM 9222D B1
Meritech Work Order # 09031433 Sample: Roxboro WWTP PB 3 Grab 9/3/14
Parameters Results Analysis Date ReportingUnrit Method ualifer
% Total Solids 43.44 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 187 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D B1
Meritech Work Order # 09031434 Sample: Roxboro WWTP PB 4 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 68.21 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 13 col/g dry wt 9/3/14 13 col/g dry wt SM 9222D B2
Meritech Work Order # 09031435 Sample: Roxboro WWTP PB 5 Grab 9/3/14
Parameters Results Aialysis Date Reporting Limit Method Qualifier
%Total Solids 60.19 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 15 col/g dry wt 9/3/14 15 col/g dry wt SM 9222D B2
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 ml.
B2 Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342.4748 fax.(336)342-1522
Meritech, Inc®
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Marshall Puryear Report- Date 9/8/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014
Meritech Work Order## 09031436 Sample: Roxboro WWTP PB 6 Grab 9/3/14
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 39.45 % 9/3/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 461 col/g dry wt 9/3/14 45 col/g dry w( SM 9222D B1
Meritech Worlc Order # 09031437 Sample: Roxboro WWTP PB 7 Grab 9/3/14
Parameters Results Analysis Date Reportiva Limit Method Qualifier
% Total Solids
47.62 %
9/3/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
777 col/g dry wt
9/3/14
45 col/g dry wt
SM 9222D
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the colons on
all filters reported per 100 till.
B2 Counts from all filters were zero. The valuereported is based on the number of colonies per 100 till that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than 'V' value).
D/J
I hereby certify that I have reviewed and appr®ve these data.
laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
2-26-:0:3 Chain of Custody Record (COC)
NPDES#:
Client: �9 v Phone:
Address:-2 63 o - & L,/f Fax:
Lr� If a2P Email:
Project:
P.Q.#:
Attention: j �L Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Std 10 days) 3- 5 Da s 24-48 Hrs
Circle all that apply: Email (preferred), Fax, Mail
� j p
l 137 �J 1 °
e ENVIRONMENTALLABORATORIES9�OG1�S
642 Tamco.Rd. Phone: 336-342-4748
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs.com
a a a�
�E•� p�� . med I ec —� s _ co
Sample Location and/or ID #
SaE'i'ipg[Ing Dates &Times
Person Taking Sample (Sign/Print):
Lab Use Only
Start
EndComp?
Grab?
Cont.
Ttest(s) �������
on Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
i1me
oXbp2- 4vv7/-" ��
o
_ Dc
(�
d
��7iQL Sa
5
j
r
' -7
1'/7
I `
N
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #;
UPS
Jug#
Fed Ex
i Are these results for regulatory purposes? Yes No }
Report results in: mg/t [ mg/kg E ugJL <'
��Hand Delivery
jRelinquished e: Time:
, 0%g
Received by: Date: Time:
Other
Relinquished y: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
me:
Receive b Lab �, D e:j 'rime:
Y
R0XB01 'WTP LAB
DIGESTER
"COOLER"
% TOTAL RESIDU- a..J VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Jason Wilson Crystal Shotwell
DATE / TIME
OF
TEST
OL-UuuG
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
RPD"S
ANALYST
INITIALS
7/8/14
7/8/2014
1
35
78,2025
114.5390
36.3365
78.2022
-.0003
Blank
78.2022
.0000
Blank
JW
8:30 AM
7/8/2014
6
35
70.9173
106.0916
35.1743
71.1989
.2816
0.80
71.0275
.1714
61
JW
7/8/2014
9
35
72.5492
107.7043
35.1551
72.8292
.2800
0.80
72.6592
.1700
61
JW
7/15/2014
7/15/2014
1
35
78.2027
112.2038
34.0011
78.2028
.0001
Blank 1
78.2024
.0004
Blank
CS
8:00 AM
7/15/2014
7/15/2014
2
9
35
35
80.1493
73.4395
114.2340
107.1488
34.0847
33.7093
80.3957
73.6802
.2464
.2407
0.72
0.71
80.2439
73.5319
.1518
.1483
62
62
CS
CS
7/22/2014
7/22/2014
1
35
78.2024
113.3050
35.1026
78.2020
-.0004
Blank
78.2020
.0000
Blank
JW
8:00 AM
7/22/2014
6
35
70.9166
106.1274
35.2108
71.1645
.2479
0.70
71.0107
.1538
62
JW
7/22/2014
9
35
1 72.5490
107.6555
35.1065
72.7961
.2471
0.70
72.6429
.1532
62
JW
7/29/14
7/29/2014
1
35
78.2022
113.2345
35.0323
78.2022
.0000
Blank
78.2022
.0000
Blank
JW
8:00 AM
7/29/2014
6
35
70.9168
106.2140
35.2972
71.1337
.2169
0.61
70.9987
.1350
62
JW
7/29/2014
9
35
72.5487
107.7702
35.2215
72.7641
.2154
0.61
72.6307
.1334
62
JW
8/5/14
8/5/2014
2
35
80.1488
115.1521
35.0033
80.1494
.0006
Blank
80.1490
.0004
Blank
JW
8:00 AM
8/5/2014
6
35
70.9180
106.2083
35.2903
71.1255
.2075
0.59
70.9965
.1290
62
JW
8/5/2014
9
35
73.4389
108.9099
35.4710
73.6487
.2098
0.59
73.5188
.1299
62
JW
8/12/14
8/12/2014
2
35
80.1495
115.1959
35.0464
80.1493
-.0002
Blank
80.1493
.0000
Blank
JW
8:00 AM
8/12/2014
6
35
70.9174
106.0212
35.1038
71.1147
.1973
0.56
70.9935
.1212
61
JW
8/12/2014
9
35
73.4394
108.4972
35.0578
73.6369
.1975
0.56
73.5155
.1214
61
JW
VSR
0%
PASS
WW
x - Blank
2014 (Third Quarter) VECTOR ATTRACTION CALCULATIONS
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP
Monitoring Period: From 10/01/14 To 12/31/14
NPDES Number: NC 0021024
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Composting Aerobic Digestion
Anaerobic Digestion
If annlicable to alternative nerformed (Class A or Class B) comalete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6 th
CFU
27
35
39
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
17
26
33
CFU/g
0
4/yr
Grab
9222D
CFU
2x10to the 6 th
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. l
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly Qather and evaluate the information used to determine that the ppathogen and
vector attraclion reduction requirements Piave been met. I am aware that there are significant penalties or false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
Pxc arer Name and Title Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Marshall Puryear
Report Date
11/6/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Date Sample Rcvd:
11/4/2014
Meritech Work Order #
11041409 Sample: Roxboro WWTP Centrifuge Material
11/4/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
29.13 % 11/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 34 col/g dry wt 11/4/14 34 col/g dry wt
SM 9222D
Meritech Work Order #
11041410 Sample: Roxboro WWTP Centrifuge Material
11/4/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
27.40 % 11/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 37 col/g dry wt 11/4/14 37 col/g dry wt
SM 9222D
Meritech Work Order #
11041411 Sample: Roxboro WWTP Centrifuge Material
11/4/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
25.44 % 11/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 39 col/g dry wt 11/4/14 39 col/g dry wt
SM 9222D
Meritech Work Order #'
11041412 Sample: Roxboro WWTP Centrifuge Material
11/4/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
27.61 % 11/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 36 col/g dry wt 11/4/14 36 col/g dry wt
SM 9222D
Meritech Work Order #
11041413 Sample: Roxboro WWTP Centrifuge Material
11/4/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
28.91 % 11/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 35 col/g dry wt 11/4/14 35 coI/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Marshall Puryear
Client: Synagro
284 Boger Road
Page 2
Report Date 11/6/2014
Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014
Meritech Work Order # 11041414 Sample: Roxboro WWTP Centrifuge Material 11/4/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 36.8 % 11/4/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 27 col/g drywt 11/4/14 27 col/g dry wt SM 9222D
Meritech Work Order # 11041415 Sample: Roxboro WWTP Centrifuge Material 11/4/14
Parameters Results Analy�iE Date Reporting Limit Method
% Total , Solids
26.18 %
1114/14
0-100 %
SM2540E
y Fecal Coliform (Sludge)
< 38 col/g dry wt
11/4/14
38 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data.
,Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
34a-2013: Chain of Custody Record (COC)
NPDESit-.
Client: Phone:
MERFECH
Address: Fax:
ENVIRONMENTAL LABORATORIES
Email:
642 Tamcb.Rd. Phone: 336-342-4748
Project:
Reidsville NC 27320 Fax: 336-342-1522
P.OX:
Email: info@meritech-labs.com
Attention: Turn Around Tirne*
-
How would you like your report sent? *RUSH work needs prior approval.
,www.meri techdabs,CorM
(
Circle all that apply: Email (preferred), Fax, Mail -Std io days) 3 5 Da s 24-481-irs
.Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use 0 n . IV'
Samplelocatibri and./or ID-#
'7-0)'�L#62
Start
Enid
comp?
It of
Test(s) Required
I S)94ce?
H OK?
Date
Time
Date
Time
Grab?
Cont.
-Yes No
Yes
CI: OK?
11/1"ho
/0-.00
ALL] 557/44. e_
NA
J5
4V
Terbperature Upon
Recs'pt:
(—
Dechlorinatioh of Ammonia, Cyanide, Phen-ol.and TKN
be done field
Method of
(-c0.5 p0m)
samples must in the prior to preservation:
"5
Comments;
IJug
Compositor It
Shipment:
ET UPS
Fed Ex
Are these results for regulatory purposes? 'Yes Et No Or
Report results in: nig/L [I,' mg/kg Q- ug/L Q;
qHand Delivery
Relinquished by%// Date�/,, Time:
Received by: Date: Time:,
Other
Relinquished by:. Date:f Time.:
Received by: Date: Time:
- I
Relinquished by: Date: Time:
e: im
Y PT IT -D � %6
Meritech, Inc.
Environmental Laboratory
x. ._ .
Laboratot• Certification No 165
Page 1
Contact: Marshall Puryear Report Date 1.1/13/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014
Meritech Work Order # 11041416 Sample: Roxboro WWTP Mix Gram 11/4/14
Parameters Results Analysis Date Reporting_Limit Method
% Total Solids 35.09 % 11/4/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 29 col/g dry wt 11/4/14 29 col/g dry wt SM 9222D
Meritech Work Order # 11041417 Sample: Roxboro WWTP Mix Grab 11/4/14
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 36.43 % 11/4/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 27 col/g dry wt 11/4/14 27 col/g dry wt SM 9222D
Meritech Work Order # 11041418 Sample: Roxboro WWTP Mix Grab 11/4/14
Parameter s Results Analysis Date Reporting Limit Method
%Total Solids 36.40 % 11/4/14 0-.100 % SM 2540B
Fecal Coliform (Sludge) .... < 27 col/g dry wt .11/4/14 27 col/g dry wt SM 9222D
Meritech Work Order # 11041419 . Sample: Roxboro WWTP Mix Grab
Parameters Results Analysis Date Reporting Limit Method
%'Total Solids 41.74 % 11/4/14 0-100 % SM 254OB
Fecal Coliform (Sludge) < 24 col/g dry wt 11/4/14 24 col/g drywt . SM 9222D
Meritech Work Order # 11041420 Sample: Roxboro WWTP Mix Grab 11/4/14
Parameters Results Analysis Date Reporting Lhnit Method
% Total Solids
30.65 % -
11/4/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 33 col/g dry wt
11/4/14
33 col/g dry wt
SM 9222D
642 Tatttco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
erl"tech, Inc,,
:. Environmental Laboratory
Laboratory Certification No.165
Page 2
Cozitact: Marshall Puryear Report Date 1.1/13/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014
Meritech Work Order # 11041421 Sample: Roxboro W WTP Mix Grab 11/4/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 57.32 % 11/4/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 17 col/g dry wt . 11/4/14 17 col/g dry wt SM 9222D
Meritech Work Order # 11041422 Sample: Roxboro WWTP Mix Grab 11/4/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
33.37 %
11/4/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 30 col/g dry wt
11/4/14
30 col/g dry wt
SM 9222D
bi
1 hereby certify that I have reviewed and approve these data. G
Laboratory Represent tive
642 Tamco Road, Reidsville, North Carolina. 27320
tel,(336)342-4748 fax.(336)342-1522
3�o-zo�a
Chain of Custody Record (COC)
NPDES#:
Client:_ Sal Phone:
11-INC.
.
Address: Fax:
'�� `
y J X
ENVIRONMENTAL L BORATO.R6ES
Email:
642 Tam coRd. Phone: 336-342-4748
Project:
M�L
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs.com
Attention:
Turn Around Time*
How would you like your report sent?
*RUSH work needs prior approval.
vvvi.mentech—labso(®m
Circle all that apply: Email (preferred), Fax, Mail
Std 20da s)
3-S Davs, 24-48Hrs
= 0:
.Sc"31iY'dpfrog Dates six Times
Person Taking Sample (Sign/Print):
Lab We Only
Sample Location, and/or ID #
Start
End
,
Comp.
r
#o,
Test(s)Required
Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yes / No
7
CI OK.
C1
€
Temperature Upon
cp�t
" L
*** Dechlorination (<0.5 Ammonia, Cyanide, Phenol TKN be done in the field ***
Method o''�
ppm) of
and samples must prior to preservation.
Compositor: #
Comments:
Shipment:
�
❑' UPS
j
Jug #
Fed Ex
Are these results for regulatory purposes? Yes Q
No Q ! Report results in: mg/L
Q mg/kg 0 ug/L :
JRelinquished by: Date: Time:
Hand Delivery
)Received by:
�� 30
Date:
Time:
z/ ¢ /9-
Other
iRelinquished by: Date.. Time: Received by:
Date:
Time:
_
r
IIRelinquished by: Date: Time:
f.'
DIGESTER
"COOLER"
ROXBORC '/TP LAB
% TOTAL RESIDUE OLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Jason Wilson Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
RPD"S
ANALYST
INITIALS
10/7/14
10/7/2014
1
35
78.2020
114.0271
35.8251
78.2020
.0000
Blank
78.2021
-.0001
Blank
JW
8:15 AM
10/6/2014
2
35
80.1495
115.3586
35.2091
80.5052
.3557
1.01
80.2842
.2210
62
JW
10/6/2014
6
35
70.9171
106.1904
35.2733
71.2745
.3574
1.01
71.0515
.2230
62
JW
10/14/2014
10/14/2014
1
35
78.2022
113.8495
35.6473
78.2022
.0000
Blank
78.2022
.0000
Blank
JW
10/13/2014
2
35
80.1492
115.3514
35.2022
80.4660
.3168
0.90
80.2652
.2008
63
JW
10/13/2014
9
35
72.5483
107.6409
35.0926
72.8622
.3139
0.89
72.6624
.1998
64
JW
10/20/2014
10/20/2014
1
35
78.2018
113.5582
35.3564
78.2018
.0000
Blank
78.2018
.0000
Blank
JW
8:30 AM
10/20/2014
2
35
80.1488
115.4020
35.2532
80.4455
.2967
0.84
80.2586
.1869
63
JW
10/20/2014
9
35
72.5480
107.9370
35.3890
72.8454
.2974
0.84
72.6576
.1878
63
JW
10/27/14
10/27/2014
1
35
78.2016
113.8252
35.6236
78.2018
.0002
Blank
78.2016
.0002
Blank
JW
10/27/2014
2
35
80.1490
115.2628
35.1138
80.4202
.2712
0.77
80.2483
.1719
63
JW
10/27/2014
9
35
72.5479
107.9455
35.3976
72.8207
.2728
0.77
72.6482
.1725
63
JW
11/3/14
11/3/2014
1
35
78.2013
113.6320
35.4307
78.2015
.0002
Blank
78.2013
.0002
Blank
JW
9:15 AM
11/3/2014
2
35
80.1488
115.4568
35.3080
80.4094
.2606
0.74
80.2443
.1651
63
JW
11/3/2014
9
35
72.5479
108.3052
35.7573
72.8124
.2645
0.74
72.6449
.1675
63
JW
11/11/11
11/11/2014
1
35
78.2013
113.4001
35.1988
78.2014
.0001
Blank
78.2014
.0000
Blank
JW
8:15AM
11/10/2014
2
35
80.1491
115.2948
35.1457
80.4115
.2624
0.75
80.2462
.1653
63
JW
11/10/2014
9
35
72.5479
107.7833
35.2354
72.8124
.2645
0.75
72.6459
.1665
63
JW
VSR
-4%
PASS
WW
x - Blank
2014 (Fourth Quarter) VECTOR ATTRACTION CALCULATIONS
2014
603 VECTOR ATTRACTION
This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction %
Formula Reduction
In - Out n .65,65 .65 n .00 n .00 n
In - (In x Out) .65 - (.65 x .65) .65 - .42 .23 .000 x 100 0 .0 First Quarter 2014
In - Out .68 - .64 n .040 n 040 n
In - (In x Out) . .68 - (.68 x .64) .68 - .44 .24 .167 x 100 16.7 Second Quarter 2014
In - Out n
.63 - .62 rl
.010
n
.01
n
In - (In x Out)
63 - (.63 x .62)
.63 - .39
.24
0.042 x 100 4 Second Quarter 2014
In - Out
0.61 - 0:61 n
.00 n
.00
n
In - (In x Out)
61 (.61 x .61)
0.61 - .37
24
0 x 100 Q 0.0 Third Quarter. 2014
In - Out n 0.62 - 0.63 n -.01 n -.01 n
In - (In x Out) .62- (.62 x .63) 0.62- .39 23 -0.043 x 100 0 -4.3 Fourth Quarter 2014
Agricultural Lime Application Log
Year: 2014
Project:
Roxboro
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-PS-24-01 Ronald Carver
6.0 O:OT/Ac.
NC-PS-24-02 Ronald Carver
5.8
OAT/Ac.
NC-PS-24-03 Ronald Carver
6.0
O.OT/Ac.
NC-PS-25-1A Paul Bailey
6.5
O.OT/Ac.
NC-PS-25-1 B Paul Bailey
6.6
O.OT/Ac.
NC-PS-25-02 Paul Bailey
5.6
0.8T/Ac.
NC-PS-25-03 Paul Bailey
5.9
O.OT/Ac.
NC-PS-25-04 Paul Bailey
6.3
O.OT/Ac.
NC-PS-25-05 Paul Bailey
6.5
O.OT/Ac.
NC-PS-26-01 Henry Martin
6.3
O.OT/Ac.
NC-PS-26-02 Henry Martin
6.2
O.OT/Ac.
NC-PS-26-03 Henry Martin
5.9
O.OT/Ac.
Lime will be applied when field conditions
permit.
NCDA&CS, iomic Division Phone: (919) 733-2665
Website: www.r__,`
I gov/agronomi/
Report No. FY111 )16359
Predictive
Client: Ronald Carver
105 Carver Farm Rd.
Advisor:
Nate Roth
Synagro
.
Mehlich-3 Extraction
Roxboro, NC 27573
284 Boger Rd
Mocksville, NC 27028
A
Soil Report
Sampled County: Perquimans
r
Sampled: Received: 11/14/2014
Completed: 12109/2014
Farm: NC-PS-24
Links to Helpful Information
Sample ID: 24-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
100 0 0
0
0
0
0
Note: 12
2-
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drrP]:
Soil Class:
Mineral,
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1 Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.41 0.88 11.5 86 1.6 6.0 171 22
61 24
38
536 339
274
274
490
0.1 1
Sample ID: 24-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.4
120-200 0
20 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in g/crrP; CEC and Na in meq/1 00 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.36 . 0.86' 12.5 86 1.7 5.8 244 68
54 30
64
232 156
368
368
433
0.1 1
Sample ID: 24-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
20 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WIV in g/cd; CEC and Na in meq/100 crrP; NO3-N in mgldd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1 Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 0.92 10.7 89 1.2 6.0 112 63
54 31
44
301 197
170
170
218
0.1 1
Y,-North'Carolina
fobaccoTiu!,; 1�uml Cwilads%loti
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox1er, Commissioner of Agriculture
NCDA&CS ".. ;%iomic Division Phone: (919) 733-2655 Website: www.nw ..goy/agronomil
Ronald Carver
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to .micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note• Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncagr.aov/agronomi/oboart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.goy/agronorni/uyrst.htm
for more information.
Report No. FY1,__1016359
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index
NCDA&CS .,_ comic Division Phone: (919) 733-2656
Website: www.f,,
_„gov/agronomi/
Report No. FYI- `)16358
Client: Paul Bailey
Advisor:
Nate Roth
Predictive
2260 Haywood Bailey Rd.
Synagro
,_ .
Roxboro, NC 27573
284 Boger Rd
Mocksville, NC 27028
Soil Report Mehlich-3 Extraction
Sampled County: Perquimans
Sampled: Received: 11/14/2014
Completed: 12/09/2014
Farm: NC-PS-25
Links to Helpful Information
Sample ID: 25-1a
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.0
120-200 0
90 0 0 pH$
0
0
0
Note: 12 Note:
2-
Test Results [units - W/V in g/crrt3; CEC and Na in meg1100 cd; NO3-N in mg/drrr`t]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.22 0.93 12.3 94 0.7 6.5 195 24
72 21
52
717 439 430
430
616
0.1 1
Sample ID: 25-1b
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.0
120-200 0
70 0 0 pH$
0
0
0
Note: 12 Note:
2-
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/dd]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.22 0.88 13.9 96 0.6 6.6 247 36
73 22
53
191 122 408
408
570
0.1 1
Sample ID: 25-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.8
120-200 0
40 0 0 0
0
0
0
Note: 12
2-
Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 cm3; NO3-N in mg/drrt3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 0.91 12.2 84 1.9 5.6 202 51
55 27
49
198 136 420
420
537
0.1 1
North Carolina
Tobacco 7n15s fwid camni6ssicre
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
. - Steve Troxler, Commissioner of Agriculture
NCDA&CS .-_._.__comic Division Phone: (919) 733-2655
Website: www.r:__.__gov/agronomi/
Report No.
FYI_-_316358
Paul Bailey
Page 2 of 3
Sample ID: 25-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0
0
0
0
0 0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.84 10.3 87 1.4 5.9 114 80
58 25
50
265
.176
342
342
271 0.1
1
Sample ID: 25-04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim,1 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
2-
Test Results [units - W/V in g/cd; CEC and Na in meq/100 crrr3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.27 0.84 11.6 92 1.0 6.3 197 40
61 29
44
208
138
346
346
467 0.1
1
Sample ID: 25-05
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.0
120-200 0
80
0
0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cmR; NO3-N in mgldd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.22 0.94 10.3 93 0.7 6.5 97 31
64 28
36
235
150
148
148
277 0.1
1
NCDA&CS,., ,.:;,comic Division Phone: (919) 733-2665 Website: www.rl___�_gov/agronomi/ Report No. FY16_6016358
Paul Bailey Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uyrsthtm
for more information.
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20.
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-Ail
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-Al
zinc availability index
Zn-I
zinc index
NCDA&CS, _w__lomic Division Phone: (919) 733-2655 Website: w4vw.r1.,
_,,govlagronomi/
Report No. FY1 )16366
Predictive
Client: Henry Martin
183 Martin Estate Rd
Advisor:
Nate Roth
Synagro
Mehlich-3 Extraction
.►¢ �x� Soil. „rt
Roxboro, NC 27573
Boger Rd
284 Bo 9
Mocksville, NC 27028
rx,{ 1`�N
Sampled County:
�a�: �t'Ylilt�fi
5y
Sampled: Received: 11/14/2014 completed: 12/09/2014
Farm: NC-PS-26
Links to Helpful Information
Sample ID: 26-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., M 0.0 180-220 0
0 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meg1100 cnY3; NO3-N in mgldd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 0.85 11.8 92 1.0 6.3 268 138 57 29
62
250 163
463
463
587
0.1 1
Sample ID: 26-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., M 0.0 180-220 0
0 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in glcrn3; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.83 12.2 91 1.0 6.2 354 120 58 28
66
199 134
644
644
719
0.1 1
Sample ID: 26-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P206
K20 Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0 120-200 0
10 0 0
0
0
0
0
Note: 12
2-
Test Results [units - W/V in g/crrti3; CEC and Na in meq/100 cnr3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-1 Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.85 10.8 86 1.6 5.9 244 78 55 27
49
233 157
541
541
664
0.1 1
North Carolina
Tobacco Trust rund Com1M%%13u
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture
NCDA&CS ). 4 _i�-iomic Division Phone: (919) 733-2655 Website: www.r:�_-&.tgov/agronomi/
Report No. FY1 . D16366
Henry Martin
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer .
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown,' not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-.0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.Htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncaar.pov/agronomi/oboart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
Mn-All
Mn-Al2
Mn-I
M-O
N
Na
NO3-N
ORG
pH
P-1
P205
S-1
SS-1
W/V
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
Zn-I
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacrr.gov/aaronomi/uvrst.htm
for more information.
manganese
Mn-availability index for crop 1
Mn-availability index for crop 2
manganese index ,
mineral -organic soil class
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index