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HomeMy WebLinkAboutWQ0021826_Residual Annual Report 2014_20150302CITY OF ROXBORO, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0021826 2014 ANNUAL REPORT City of Roxboro, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00021826 County Person Year 2014 Facility Name (as shown on permit) City of Roxboro W WTP & WTP NPDES No. NCO021024 Land. Application Operator Synapro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 22 Total number of fields utilized for land application during the year: 12 Total amount of dry tons applied during the year for all application sites: 431.76 Total number of acres utilized for land application during the year: 81.2 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water. Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. it. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Thomas S. Warren. Assistant City Manager Permittee Name and Tii//M1�lle (type or print) Signature of Preparer* Date (if different from Permittee) re e i ee i!ate ��B ! IJ2 2015 , Signa re of Land Applier Date (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION ROXBORO,NC . tOXBORO, NC WWTP AEROB. DIGESTED CAKE October 2014 November 2014 December 2014 YEARLY TOTAL AMOUNT UNIT 400.00 Y 841.00 Y 525.00 Y 1,766.00 Y DRY TONS UNIT 97.80 D 205.61 D 128.35 D 431.76 D DRY METRIC TONS 88.71 186.50 116.42 391.63 1/30/2015 2014 ANNUAL REPORT PROJECT: FACILITY: NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: Town of Roxboro Roxboro, NC Roxboro WWTP 902 Cavel-Chub Lake Rd. Roxboro, NC 27573 336-599-8232 NC0021024 Thomas S. Warren, Jr Manager P.O. Box 128 Roxboro, NC 27573 336-542-4621 ext.22 , Assistant City Derek Clayton, WWTP Superintendent 902 Cavel-Chub Lake Rd. Roxboro, NC 27573 336-599-8232 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: "WQ0021826 Laboratory Facility Name: ROXBORO, NC A&L Eastern Laboratories Inc. NPDES# : NCO021024 or WQ# (residual only) WWTP Name: ROXBORO WWTP Residuals Analysis Data . Product Type AEDCAK MIX MIX AEDCAK Date Sampled (grab) or 09/03/14 09/03/14 11/04/14 11/04/14 Date Composited Percent Solids 29.03 77.76 34.93 23.33 PARAMETERS (mg/kg dry weight) - Arsenic 5 6 7 5 Cadmium 2 2 <2 2 Mercury 1.4 0.5 2.4 1.3 Chromium 92 73 77 75 Copper 580 269 362 592 Lead 40 28 28 40 Molybdenum 8 <5 <5 6 Nickel 43 32 34 38 Selenium 6 <5 <5 6 Zinc 1160 489 656 1130 Total Phosphorus 21500 9570 12600 19100 TKN 41700 19900 20800 37900 Ammonia -Nitrogen 3690 849 3520 4710 Nitrate and Nitrite 772 264 91 1090 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X_S (SIGN] OF PREP Date a - to -/ DENR FORM RSSF (5/2003) Printed: Friday - January 30 2015 at 16:59.53 for: 2102 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0021826 Laboratory Facility Name: ROXBORO, NC A&L Eastern Laboratories Inc. NPDES# : NCO021024 or WQ# (residual only) WWTP Name: ROXBORO ,WWTP Residuals Analysis Data Product Type AEDCAK MIX MIX AEDCAK Date Sampled (grab) or 09/03/14 09/03/14 11/04/14 11/04/14 Date Composited Percent Solids 29.03 77.76 34.93 23.33 PARAMETERS (mg/kg dry weight) Aluminum 29000 38700 39700 30200 Calcium 16700 6980 10500 15000 Magnesium 3910 3410 3340 3700 pH 5.91 5_, 81 7.65 5.79 Potassium 2420 2970 2630 2310 Sodium 1030 498 553 817 "I certify, under penalty ,of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that,qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X (SIG R) NR - Data Not Reported or Data Not Required Date 2-/e, /?— DENR FORM RSSF-B (7/2002) Printed: Friday - January 30 2015 at 17:00:12 for: 2102 01 Page: 1 of 2 Report Number: 14-248-0202 �u,�J( A&L Eastern Laboratories, lhc._ Account Number: 46487 7.621 Whitepine Road Riehmond,'Virginia 23237 '(804)'743.9401 Fax (804) 271-6446' Submitted By: MARSHALL PURYEAR wwiwaleastern.com. Send To, SYNAGRO'CENTRAL LLC/ROXBORO Project: ROXBORO CAKE Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 9/3/2014 09:00:00 Lab Number: 57429 Date Received: 09/05/2014 00:00 Sample Id : ROXBORO CAKE Date Reported: 09/11/2014 Total Solids Moisture * Total Kjeldahl Nitrogen Total Phosphorus Total Potassium Total Sulfur Total Calcium Total Magnesium Total Sodium Total Iron Total Aluminum Total Manganese Total Copper Total Zinc Ammonia Nitrogen Organic N Nitrate+Nitrite-N 29.03 70.97 4.17 2.15 0.24 0.85 1.67 0.39 0.10 0.37 3.80 Q1*01 MVV MW JM KM KM KM KM KM KM KM KM KM KM KM JM JM Total Cadmium 2.0 2.0 KM All values are on a dryweight eight basis except as noted by asterisk. Detection limit on all N series is on a wet basic 41700 21500 2420 8540 16700 3910 1030 24800 29000 1080 580 1160 3690 38010 772 100.0 100.0 10.0 100 100 100 100 100 100 100 100 5 5 5 10.0 10.0 2.00 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. UU/Ud/LU"14 UO:US 09/08/2014 08:05 09/08/2014 08:44 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/10/2014 12:48 09/08/2014 08:44 09/08/2014 08:44 09/08/2014 08:45 09/10/2014 12:48 01V1-L04UV SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NI3C CALCULATION SM-450ONO3F SW 6010C Debbie Holt Page: 2 of 2 Report Number: 14-248-0202 Account Number: 46487 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 @P A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastem.com Project: ROXBORO CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 9/3/2014 09:00:00 Lab Number: 57429 Date Received: 09/05/2014 00:00 Sample Id : ROXBORO CAKE Date Reported: 09/11/2014 Total Chromium 92 b NIVI UZI/ IU/GV I4 14.Y0 Ovv vv ivv Total Nickel 43 5 KM 09/10/2014 12:48 SW 6010C Total Lead 40 5 KM 09/10/2014 12:48 SW 6010C Total Arsenic 5.0 3.0 KM 09/10/2014 12:48 SW 6010C Total Mercury 1.4 0.4 KM 09/08/2014 09:00 SW-7471 B Total Selenium 6.0 5.0 KM 09/10/2014 12:48 SW 6010C pH (Standard Units) * 5.91 2.00 JM 09/08/2014 07:30 SW-9045D Total Molybdenum 8 5 KM 09/10/2014 12:48 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMTIS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. J Debbie Holt SAMPLING LOG # o� imc' CHAIN OF CUSTODY 111'IuI�I��IIIII�IIIII�III�B��Ig1�II�IINI'N�Ilill,RECORRECORD ANALYSIS CUSTOMER: SYNAGRO SOUTHEAST SYNAGROCENTRALLLCrROXBORO 13.3046 .w 'f ROXBORO CAK6'NC CERT#257 r the proper field sampling procedures PROJECT MANAGER: r' during the collection of these samples. i Phone: SAM Ll=Ft Y A & L CUSTOMER SAMPLING SAMPLE TYPE # OF CONTAINERS SAMPLING DATE TIMEn METHOD METHOD PRESERVED SHIPPED LAB # SAMPLE I.D. LOCATION ts7l(. f I r /!k 3 I Relinquished by Sampler: Timb Recieved by. REMARKS. /Datyer Relinquished by: Date Time Recieved by: fec�i `� �3FSf,�S5z15' 0 ! �7; 3 Relinquished by: Da e Time Recieved by: SPECIAL INSTRUCTIONS: For monitoring purposes. PO#: ANALYSIS REQUEST SAMPLE CaCO3 Volatile I.D. SL1 SL2 NH, N NO3 N Organic Cd Cr NI Pb As H Se M Mo CI NO2 N 9 p equiv. Solids r 10 POO k0o"' J009 k0or k0 Poo, loot 10 100 iO kooIr POO 10" SL1: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc White — A & L Canary — MANAGER COPY kL Sodium Absorption Ratio calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2102-01-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 9/3/2014 1011/2014-12/31/2014 1.0015 CAKE Na mg/I = (Na mg/kg x % Solids) = 100 = (1030 x 29.0300) =100 = 299.009 Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (16700 x 29.0300) + 100 = 4848.01 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3910 x 29.0300) _ 100 = 1135.07 Na meq = Na mg/I _ Molec.Wgt.Na = 299.009 = 23 = 13.0004 Ca meq = Ca mg/1 = Molec.Wgt.Ca = 4848.01 _ 20 = 242.401 Mg meq = Mg mg/1.= Molec.Wgt.Mg = 1135.07 = 12 = 94.5894 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 13.0004 = SgrRoot[0.5(242.401+94.5894)] = 1.00153 Printed: 1 /30/2015 Page 1 17:01 1 Page: 1 of 2 Report Number: 14-248-0201 Account Number: 46487 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028. Y� L A&L Eastern Laboratories, Inc.__ 7621 Whitepine Road Richmond, Virginia 23237 (804)'743-9401 Fax (804) 271-6446 wwwaleastem.com Project: ROXBORO DB NC CERT#257 REPORT OF ANALYSIS Date Sampled: 9/3/2014 08:30:00 Lab Number: 57428 Date Received: 09/05/2014 00:00 Sample Id : ROXBORO DB Date Reported: 09/11/2014 Total Solids * 77.76 777600 100.0 MW 09/08/2014 08:05 SM-2540G Moisture * 22.24 100.0 MW 09/08/2014 08:05 SM-2540G Total Kjeldahl Nitrogen 1.99 19900 10.0 JM 09/08/2014 08:44 SM-4500-NH3C-TKN Total Phosphorus 0.96 9570 100 KM 09/10/2014 12:48 SW 6010C Total Potassium 0.30 2970 100. KM 09/10/2014 12:48 SW 6010C Total Sulfur 0.35 3470 100 KM 09/10/2014 12:48 SW 6010C Total Calcium 0.70 6980 100 KM 09/10/2014 12:48 SW 6010C Total Magnesium 0.34 3410 100 KM 09/10/2014 12:48 SW 6010C Total Sodium 0.05 498 100 KM 09/10/2014 12:48 SW 6010C Total Iron 40500 100 KM 09/10/2014 12:48 SW 6010C Total Aluminum 38700 100 KM 09/10/2014 12:48 SW 6010C Total Manganese 865 5 KM 09/10/2014 12:48 SW 6010C Total Copper 269 5 KM 09/10/2014 12:48 SW 6010C Total Zinc 489 5 KM 09/10/2014 12:48 SW 6010C Ammonia Nitrogen 0.08 849 10.0 JM 09/08/2014 08:44 SM-4500-NH3C Organic N 1.91 19051 10.0 09/08/2014 08:44 CALCULATION Nitrate+Nitrite-N 264 2.00 JM 09/08/2014 08:45 SM-450ONO3F Total Cadmium 2.0 2.0 KM 09/10/2014 12:48 SW 6010C All values are on a dry weight basis except as noted' by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-248-0201 Account Number: 46487 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 57428 Sample Id: ROXBORO DB 99,A&L EasternLaboratories, Inc. 7621 Whltepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: ROXBORO DB NC CERT#257 REPORT OF ANALYSIS Date Sampled: 9/3/2014 08:30:00 Date Received: 09/05/2014 00:00 Date Reported: 09/11/2014 Total Chromium 73 5 KM 09/10/2014 12:48 SW 6010C Total Nickel 32 5 KM 09/10/2014 12:48 SW 6010C Total Lead 28 5 KM 09/10/2014 12:48 SW 6010C Total Arsenic 6.0 3.0 KM 09/10/2014 12:48 SW 6010C Total Mercury 0.5 0.4 KM 09/08/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 09/10/2014 12:48 SW 6010C pH (Standard Units) * 5.81 2.00 JM 09/08/2014 07:30 SW-9045D Total Molybdenum <5 5 KM 09/10/2014 12:48 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMTIS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLING LOG # r#ii CUSTOMER: SYNAGRO SOUTHEAST PROJECT MANAGER: Phone: )n 16, t4-248- us 11111111 44O 01 14SYNAGRO CENTRAL CHAIN OF CUSTODY RECORD & ANALYSIS RECORD ROXBORO [)WNC CERT#n7 14, � 1per neld sampling P10-ar — were used during the collection of these samples. SAMPLER, A & L CUSTOMER SAMPLING SAMPLE #OF CONTAINERS SAMPLING METHOD METHOD DATE TIME PRESERVED SHIPPED LAB # SAMPLE I.D. LOCATION TYPE Date Time Recieved by: REMARKS: Relinquished by Sampler, Time Recieved by: Date Relinquished by: 1305LIT Relinquished by: Dale Time Recieved by: SPECIAL INSTRUCTIONS: monitoring purposes. For STATE) ANALYSIS REQUEST SAMPLEOrganic Se I.D. SL1 I SL2 N Cd Cr Ni Pb As Hg PO#: PH CaCO Volatile Mo I eawV31 Solids I 10#0 loo k#00 1400 k0or k0or 10#0 tow k000 ( k000 1000 1.000 01 SLII: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SI-2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc White-A&L Canary - MANAGER COPY 100"' C1 NO2NI __j Sodium Absorption Ratio Calculation (SAR) Product Code Product Name' Sample Date Report Range Ratio 2102-01-MIX-NC ROXBORO, NC WWTP/WTP MIX 9/3/2014 10/112014-12/31/2014 1.0731 Na mg/1= (Na mg/kg x % Solids) _ 100 = (498 x 77.7600) = 100 = 387.245 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6980 x 77.7600) _ 100 = 5427.65 Mg mg/I = (mg mg/kg x % Solids) = 100 = (3410 x 77.7600) = 100 = 2651.62 Na meq = Na mg/I + Molec.Wgt.Na = 387.245 _ 23 = 16.8367 Ca meq = Ca mg/1= Molec.Wgt.Ca = 5427.65 _ 20 = 271.382 Mg meq = Mg mg/I = Molec.Wgt.Mg = 2651.62 = 12 = 220.968 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 16.8367 = SgrRoot[0.5(271.382+220.968)] = 1.07309 Printed: 1/30/2015 Page 1 17:09 Page: 1 of 2 Report Number: 14-309-0206 Account Number: 46487 Submitted By: NATE ROTH Send To: SYNAGRO CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 58525 Sample Id : ROXBORO WWTP MIX A&L Eastern Laboratories, Inc. 7621,Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 www.aleastem.com Project: ROXBORO WWTP MIX . NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:30:00 Date Received: 11/05/2014 00:00 Date Reported: 11/11/2014 Total Solids * 34.93 349300 100.0 BW 11/05/2014 14:30 SM-254OG Moisture 65.07 100.0 BW 11/05/201414:30 SM-254OG Total Kjeldahl.Nitrogen: 2.08 20800 10.0 JM 11/06/2014 08:19 SM-4500-NH3C-TKN Total Phosphorus 1.26 12600 100 KM 11/06/2014 11:19 SW 6010C Total Potassium 0.26 2630 100 KM 11/06/2014 11:19 SW 6010C Total Sulfur 0.53 5330 100 KM 11/06/2014 11:19 SW 6010C Total Calcium 1.05 10500 100 KM 11/06/2014 11:19 SW 6010C Total Magnesium 0.33 3340 100 KM 11/06/2014 11:19 SW 6010C Total Sodium, 0.06 553 100 KM 11/06/2014 11:19 SW 6010C Total Iron 34600 100 KM 11/06/2014 11:19 SW 6010C Total Aluminum 39700 100 KM 11/06/2014 11:19 SW 6010C Total Manganese 1050 5 KM 11/06/2014 11:19 SW 6010C Total Copper 362 5 KM 11/06/2014 11:19 SW 6010C Total Zinc 656 5 KM 11/06/2014 11:19 SW 6010C Ammonia Nitrogen 0.35 3520 10.0 JM 11/06/2014 08:19 SM-4500-NH3C Organic N 1.73 17280 10.0 11/06/2014 08:19 CALCULATION Nitrate+Nitrite-N 91.0 2.00 JM 11/06/2014 08:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 11/06/2014 11:19 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. \ // Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made , (`�%�. to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-309-0206 Account Number: 46487 Submitted By: NATE ROTH Send To:. SYNAGRO CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 58525 Sample Id: ROXBORO WWTP MIX AFL Eastern. Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 www,aleastern.com Project: ROXBORO WWTP MIX NC CERT#257 REPORT OFANALYS/S Date Sampled: 11/4/2014 10:30:00 Date Received: 11/05/2014 00:00 Date Reported: 11/11/2014 Total Chromium 77 5 KM 11/06/2014 11:19 SW 6010C Total Nickel 34 5 KM 11/06/2014 11:19 SW 6010C Total Lead 28 5 KM 11/06/2014 11:19 SW 6010C Total Arsenic 7.0 3.0 KM 11/06/2014 11:19 SW 6010C Total Mercury 2.4 0.4 KM 11/06/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 11/06/2014 11:19 SW 6010C pH (Standard Units) * 7.65 2.00 JM 11/06/2014 08:19 SW-9045D Total Volatile Solids 34.06 340600 100.0 BW 11/05/2014 14:30 SM-2540G Total Molybdenum <5 5 KM 11/06/2014 11:19 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "K" AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2102-01-MIX-NC. ROXBORO, NC WWTP/WTP MIX 11/4/2014 / / - / / 0.7090 Na mg/I = (Na mg/kg x % Solids) _ 100 = (553 x 34.9300) _ 100 = 193.163 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (10500 x 34.9300) t- 100 = 3667.65 Mg mg/1 = (mg mg/kg x % Solids) = 100 = (3340 x 34.9300) _ 100 = 1166.66 Na meq = Na mg/I = Molec.Wgt.Na = 193.163 + 23 = 8.39839 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 3667.65 = 20 = 183.382 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 1166.66 + 12 = 97.2218 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.39839 = SgrRoot[0.5(183.382+97.2218)] = 0.709028 Printed: 1 /30/2015 Page 1 17:09 Page: 1 of 2 Report Number: 14-309-0205 Account Number: 46487 Submitted By: NATE ROTH Send To: SYNAGRO,CENTRAL LLC/ROXBORO Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 58524; Sample Id: ROXBORO WWTP CENTRIFUGE MAT y3° A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 FaX (804) 271.6446 wwwaleastemxom Project: ROXBORO WWTP CENTRIFUGE MAT NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:00:00 Date Received: 11/05/2014 00:00 Date Reported: 11/11/2014 Total Solids 23.33 233300 100.0 BW 11/05/2014 14:30 SM-2540G Moisture " 76.67 100.0 BW 11/05/2014 14:30 SM-2540G Total Kjeldahl Nitrogen 3.79 37900 10.0 JM 11/06/2014 08:19 SM-4500-NH3C-TKN Total Phosphorus 1.91 19100 100 KM 11/06/2014 11:19 SW 6010C Total Potassium 0.23 2310 100 KM 11/06/2014 11:19 SW 6010C Total Sulfur 0.90 8950 100 KM 11/06/2014 11:19 SW 6010C Total Calcium 1.50 15000 100 KM 11/06/2014 11:19 SW 6010C Total Magnesium 0.37 3700 100 KM 11/06/2014 11:19 SW 6010C Total Sodium 0.08 817 100 KM 11/06/2014 11:19 SW 6010C Total Iron 25200 100 KM 11/06/2014 11:19 SW 6010C Total Aluminum 30200 100 KM 11/06/2014 11:19 SW 6010C Total Manganese 1100 5 KM 11/06/2014 11:19 SW 6010C Total Copper 592 5 KM 11/06/2014 11:19 SW 6010C Total Zinc 1130 5 KM 11/06/2014 11:19 SW 6010C Ammonia Nitrogen 0.47 4710 10.0 JM 11/06/2014 08:19 SM-4500-NH3C Organic N 3.32 33190 10.0 11/06/2014 08:19 CALCULATION Nitrate+Nitrite-N 1090 2.00 JM 11/06/2014 08:20 SM-450ONO3F Total Cadmium 2.0 2.0 KM 11/06/2014 11:19 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made9,&U,LNK.t✓ �% to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14309-0205 n4J( /`► &L Eastern Laboratories, Inc. Account Number: 46487 M ii1 7621 Whitepine Road Richmond; Virginia 23237 (804)-743-9401 Fax (804) 271.6446 Submitted By: NATE ROTH www.aleastern.com - Send To: SYNAGRO'CENTRAL LLC/ROXBORO Project: ROXBORO WWTP CENTRIFUGE MAT Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 11/4/2014 10:00:00 Lab Number: 58524 Date Received: 11/05/2014 00:00 Sample Id': ROXBORO WWTP CENTRIFUGE MAT Date Reported: 11/11/2014 Total Chromium 75 5 KM 11/06/2014 11:19 SW 6010C Total Nickel 38 5 KM 11/06/2014 11:19 SW 6010C Total Lead 40 5 KM 11/06/2014 11:19 SW 6010C Total Arsenic 5.0 3.0 KM 11/06/2014 11:19 SW 6010C Total Mercury 1.3 0.4 KM 11/06/2014 09:00 SW-7471B Total Selenium 6.0 5.0 KM 11/06/2014 11:19 SW 6010C pH (Standard Units) " 5.79 2.00 JM 11/06/2014 08:19 SW-9045D Total Volatile Solids 55.67 556700 100.0 BW 11/05/2014 14:30 SM-254OG Total Molybdenum 6 5 KM 11/06/2014 11:19 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "K" AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2102-01-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 11/4/2014 / / - / / 0.7459 CAKE Na mg/1= (Na mg/kg x % Solids) _ 100 = (817 x 23.3300) =100 190.606 Ca mg/1= (Ca mg/kg x % Solids) = 100 = (15000 x 23.3300) + 100 = 3499.5 Mg mg/[ = (mg mg/kg x % Solids) _ 100 = (3700 x 23.3300) + 100 = 863.21 Na meq = Na mg/I = Molec.Wgt.Na=.190.606 + 23 = 8.28722 Ca meq = Ca mg/1= Molec.Wgt.Ca = 3499.5 + 20 = 174.975 Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 863.21 + 12 = 71.9342 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.28722 _ SgrRoot[0.5(174.975+71.9342)] = 0.745857 Page 1 Printed: 1/30/2015 17:01 FACILITY NAME: ROXBORO, NC OWNER: RONALD CARVER SITE #: NC PS 00024 FIELD# : PS 00024 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 86.06 OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip, cation tili- ali- Ammonia Nitrate PAN DATE or % per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/30/14 224.00 (CY) 14.933 29.03 3.651 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE 10/31/14 128.00 (CY) 8.533 29.03 2.086 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Oct-14 352.00 (CY) 23.466 Total Cubic Yds/Ac: 23.47 TOTALS: Annual lbs/acre Cumulative lbs/acre As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 161 0.057 0.023 1.056 6.656 0.459 0.016 0.092 0.493 0.069 13.311 246.72 0.966 0.180 8.057 40.665 4.176 0.124 0.764 4.821 0.516 69.784 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ... _ - 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 c Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: RONALD CARVER SITE #: NC PS 00024 FIELD# : PS 00024 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 3.91 OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 0.70 ACRES PERMITTED: 0.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/31/14 16.00 (CY) 22.857 29.03 5.589 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 TT7.3,690.00 p 1 772.00 p 14020 FESCUE Oct-14 16.00 (CY) 22.857 Total Cubic YdstAc: 22.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.056 0.022 1.028 6.483 0.447 0.016 0.089 0.481 0.067 12.965 24031 157 Cumulative lbs/acre 0.665 I 1 0.108 1 5.845 1 29.939 - 1 3.036 0.083 0.538 I 1 3.865 0.315 49.878 F Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop "" 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 L� 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X ✓ /S� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: RONALD CARVER SITE #: NC PS 00024 FIELD# : PS 00024 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 7.82 OPERATOR: RONALD CARVER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60 Page Lime Applied *** Date Lb./A. allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total TPer Acre Solids 10/31/14 32.00 (CY) 20.000 29.03 4.890 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Oct-14 32.00 (CY) 20.000 rota[ uub[C YOSIAc: 20.U0 As Cd Cr Cu Pb I-Ig Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.049 0.020 0.900 5.672 0.391 0.014 0.078 0.421 0.059 11.345 210.27 137 Cumulative lbs/acre 0.729 0.110 6.119 1 30.033 2.968 0.086 0.551 1 3.832 0.299 49.112 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE . �kvlZf�— o�oy/,r (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0001 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: WQ0021826 ANNUAL DRY TONS APPLIED: 97.80 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 17.50 ACRES PERMITTED: 17.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/4/14 400.00 (CY) 22.857 29.03 5.589 ROAEDC DRY , 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Nov-14 400.00 (CY) 22.857 Total Cubic Yds/Ac: 22.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS:. 157 Annual lbs/acre 0.056 0.022 1.028 6.483 0.447 0.016 0.089 0.481 0.067 12.965 240.31 Cumulative lbs/acre 1.406 0.231 10.491 49.195 5.731 0.142 1.071 1 6.700 0.566 81.232 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 12 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0001 B RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 12.23 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 2.50 ACRES PERMITTED: 2.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/5/14 50.00 (CY) 20.000 29.03 4.890 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Nov-14 50.00 (CY) 1 20.000 Total Cubic Yds/Ac: 20.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 137 Annual lbs/acre 0.049 0.020 0.900 5.672 0.391 0.014 0.078 0.421 0.059 11.345 210.27 Cumulative lbs/acre 0.825 0.150 6.992 36.079 3.658 0.112 0.650 4.114 0.451 62.327 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop- 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X (fit 210 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/hicorporation 1.0 e Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields'where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: WQ0021826 ANNUAL DRY TONS APPLIED: 30.56 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/5/14 125.00 (CY) 20.161 29.03 4.929 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 1 772.00 p 14120 1 FESCUE Nov-14 125.00 (CY) 20.161 Total Cubic Yds/Ac: 20.16 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.049 0.020 0.907 5.718 0.394 0.014 0.079 0.424 0.059 11.436 211.97 138 Cumulative lbs/acre 0.478 0.076 4.206 22.335 1 1.904 0.051 0.384 2.757 0.273 37.391 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X , (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0003 RESIDUAL SOURCE(S):*. See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 30.56 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.10 ACRES PERMITTED: 6.10 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/5/14 50.00 (CY) 8.197 29.03 2.004 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 I FESCUE 11/6/14 75.00 (CY) 12.295 29.03 3.006 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Nov-14 1 125.00 (CY) 20.492 Total Cubic Yds/Ac: 20.49 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 140 Annual lbs/acre 0.050 0.020 0.922 5.812 0.401 0.014 0.080 0.431 0.060 11.624 215.44 Cumulative lbs/acre 0.953 0.151 6.335 27.914 3.766 0.087 0.709 3.785 0.294 47.874 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: HERNDON PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 30.56 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20 Page: 1 Lime Applied *** Date I Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation till- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppni) Crop MONTH Total Per Acre Solids 11/5/14 125.00 (CY) 20.161 29.03 4.929 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 TT7.3,690.00 p 1 772.00 p 14020 FESCUE Nov-14 125.00 (CY) 20.161 i otal uublc Y USIAC: 2U.16 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.049 0.020 0.907 5.718 0.394 0.014 0.079 0.424 0.059 11.436 211.97 138 Cumulative Ibs/acre 1.083 0.172 7.335 31.895 4.385 0.097 0.815 4.685 0.320 53.199 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ( 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X ,G� Dz�� (SIGNAT&E OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: PAUL BAILEY SITE #: NC PS 00025 FIELD# : PS 00025 0005 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 3.91 OPERATOR: PAUL BAILEY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 0.90 ACRES PERMITTED: 0.90 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids I1/5/14 16.00 (CY) 17.778 29.03 4.347 ROAEDC DRY 0-<I/2" SUR 0.5 0.30 41,700. p 3,690.00 p 1 772.00 p 14020 FESCUE Nov-14 16.00 (CY) 17.778 Total Cubic Yds/Ac: 17.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 122 Annual Ibs/acre 0.043 0.017 0.800 5.042 0.348 0.012 0.070 0.374 0.052 10.084 186.91 Cumulative lbs/acre 0.981 1 0.168 6.510 27.451 1 3.973 0.076 0.763 1 4.437 0.306 45.038I F " Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 212 FD Cumulative I Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ` 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE XS- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: HENRY MARTIN SITE #: NC PS 00026 FIELD# : PS 00026 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 12.23 OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3.20 ACRES PERMITTED: 3.20 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptll) Crop MONTH Total Per Acre Solids 12/15/14 50.00 (CY) 15.625 29.03 3.820 ROAEDC MOIST 0-11/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Dec-14 50.00 (CY) 15.625 Total Cubic Yds/Ac: 15.63 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 107 Annual lbs/acre 0.038 0.015 0.703 4.432 0.306 0.011 0.061 0.329 0.046 8.863 164.27 Cumulative lbs/acre 1.417 0.223 9.566 44900 5.730 0.122 1.075 6.210 0.554 77.190 2 11 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop "" '" "` -- . • -. 4 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X �\ p O ; e/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation " 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page FACILITY NAME: ROXBORO, NC PREDOMINANT SOIL SERIES: HERNDON Lime Applied *** OWNER: HENRY MARTIN PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 24.45 Date Lbs/Ae SITE #: NC PS 00026 FIELD# : PS 00026 0002 OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70 Total Cubic YdstAc: 17.54 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 120 Annual lbs/acre 0.043 0.017 0.789 4.976 0.343 0.012 0.069 0.369 0.051 9.952 184.45 Cumulative lbs/acre 1.574 1 0.251 10.859 49.373 1 6.550 0.135 1.211 1 7.279 1 0.548 82.998 Pennit PAN Limit (lbs/acre) 1st Crop/2nd Crop 2 11 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 W, ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X /1 �f� 'T/ / ✓ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be.applied in 2015 FACILITY NAME: ROXBORO, NC OWNER: HENRY MARTIN SITE #: NC PS 00026 FIELD# : PS 00026 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GEORGEVILLE PERMIT #: W00021826 ANNUAL DRY TONS APPLIED: 91.69 OPERATOR: HENRY MARTIN CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 15.60 ACRES PERMITTED: 15.60 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 12/5/14 250.00 (CY) 16.026 29.03 3.918 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 0 F140220 I FESCUE 12/6/14 25.00 (CY) 1.603 29.03 0.392 ROAEDC DRY 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p I FESCUE 12/15/14 100.00 (CY) 6.410 29.03 1.567 ROAEDC MOIST 0-<1/2" SUR 0.5 0.30 41,700. p 3,690.00 p 772.00 p 14020 FESCUE Dec-14 375.00 (CY)l 24.039 Total Cubic YastAc: 24.U4 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 165 Annual lbs/acre 0.059 0.024 1.081 6.818 0.470 0.016 0.094 0.505 0.071 13.636 252.73 Cumulative lbs/acre 1.584 0.268 10.925 50.029 6.642 0.147 1.225 6.915 0.594 85.668 11 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop . 212 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ! 1339.0 267.9 15.0 375.0 89.0 2500.0 ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE X v �G��� (SIGNAT RE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 F-.HVIAON1QE'td�AL.��13C7f3hlRG7�� lrtr~ .�rrai�+tit;allw�;�Eaar'�Ye�I'1�� - September 22, 2014 Marshall Puryear Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Roxboro WWTP Dear Marshall Puryear: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hIIDAvtviv.settek.com Order No.: 14090554 Summit Environmental Technologies, Inc. received 1 sample(s) on 9/5/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, N �- Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho 01-100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vennont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 6 Summit Environmental Technologies, Inc. Workorder v g 3310 Win St. P° Afli OONfilEAJTAL"TEC:8' OLOC)'c5r im- ,, Cuyahoga Falls, Ohio 44223 Sample .Summary �krrae rcal iai a to '1Q TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14090554 Website: htto:llivivw.settek.coin 22-Sep-14 CLIENT: Synagro Project: Roxboro WWTP Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix 14090554-001 Roxboro WWTP 9/3/2014 9:00:00 AM 9/5/2014 10:15:00 AM Solid Page 2 of 6 Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX- (330) 253-4489 Website: httQ.1Aviviv.settek.cont CLIENT: Synagro Project: Roxboro WWTP Case Narrative WO#: 14090554 Date: 9/22/2014 This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any con-iments or problems with the analytical events associated with this report are noted below. Original Page 3 of 6 SununitEnvironniental Technologies, Inc. WO#: 14090554 MINI SuffiAAA115 3310 Win St. FNVIRONME'N'r l-7 CHUCiLQGM5, 9P=G Cuyahoga Falls, Ohio 44223 Date Reported 9/22/2014 Ia'raiytital CesEzai 3t0,,9es TEL: (330) 253-8211 FAX (330) 253-4489 Company: Synagro Website: hQ:1Anvw.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 9/5/2014 Project#: Roxboro WWTP TCLP Metals Analysis (6010) Client IN Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 TCLP Arsenic(As) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Badum(Ba) 5.0 ND mg/L Solid EPA 6010 C 1 100 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Solid EPA 6010 C 1 1.0 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Chromium(Cr) 0.20 ND mg/L Solid EPA 6010 C 1 5.0 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Lead(Pb) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Selenium(Se) 0.50 ND mg/L Solid EPA 6010 C 1 1.0 9/11/2014 VVK Roxboro WWTP 001 9/3/2014 TCLP Silver(Ag) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 9/11/2014 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab IN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 TCLP Mercury 0.0020 ND mg/L Solid EPA 7470 A 1 0.20 9/10/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 Chlordane, total 0.010 ND mg/L Solid EPA 8081 B 1 0.030 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 Toxaphene 0.10 ND mg/L Solid EPA 8081 B 1 0.50 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 Endrin 0.0020 ND mg/L Solid EPA 8081 B 1 0.020 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 gamma-BHC 0.0020 ND mg/L Solid EPA 8081 B 1 0.40 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 Heptachlor 0.0020 ND mg/L Solid EPA 8081 B 1 0.0080 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 Heptachlor epoxide 0.0020 ND mg/L Solid EPA 8081 B 1 0.0080 9/12/2014 JBN Roxboro WWTP 001 9/3/2014 Methoxychlor 0.0020 ND mg/L Solid EPA 8081 B 1 10 9/12/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 1,1-Dichloroethene 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 1,2-Dichloroethane 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Benzene 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Carbon tetrachloride 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Chlorobenzene 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Chloroform 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Tetrachloroethene 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Trichloroethene 0.10 ND mg/L Roxboro WWTP 001 9/3/2014 Vinyl chloride 0.20 ND mg/L Roxboro WWTP 001 9/3/2014 MEK 2.0 ND mg/L Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 Solid EPA 8260 B 1 0.70 9/10/2014 MES 0.50 9/10/2014 MES 0.50 9/10/2014 MES 0.50 9/10/2014 MES 100 9/10/2014 MES 6.0 9/10/2014 MES 0.70 9/10/2014 MES 0.50 9/10/2014 MES 0.20 9/10/2014 MES 200 9/10/2014 MES Page 4 of 6 f �' let SzznunitEnvironmental Technologies, Inc. 3310 Win St. W04: 14090554 EO'VI}3tly MENTALTPCHNOL.d ]8$�J G Cuyahoga Falls, Ohio 44223 Date Reported 9/22/2014 >natyfvc ni'!_,�ii�rr?te7i3er TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: ham:1Avivw.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 9/5/2014 Project#: Roxboro WWTP SVOC 8270 TCLP BNA List Client II)# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 1,4-Dichlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 2,4,6-Trich lorophenol 0.25 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 2,4-Dinitrotoluene 0.10 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Cresols, Total 5.0 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Hexachloro-1,3- 0.10 ND mg/L Solid EPA 8270 C 1 butadiene Roxboro WWTP 001 9/3/2014 Hexachlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Hexachloroethane 0.10 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Nitrobenzene 0.10 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Pentachlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 Roxboro WWTP 001 9/3/2014 Pyridine 0.25 ND mg/L Solid EPA 8270 C 1 SVOC SW-846: 8321 Herbicides-TCLP 7.5 9/17/2014 JRT 400 9/17/2014 JRT 2.0 9/17/2014 JRT 0.13 9/17/2014 JRT 200 9/17/2014 JRT 0.50 9/17/2614 JRT 0.13 9/17/2014 JRT 3.0 9/17/2014 JRT 2.0 9/17/2014 JRT 100 9/17/2014 JRT 5.0 9/17/2014 JRT Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Roxboro WWTP 001 9/3/2014 2,4-D 5.0 ND mg/L Solid EPA 8321 A 1 10 9/15/2014 AMZ Roxboro WWTP 001 9/3/2014 2,4,5-TP 0.50 ND mg/L Solid EPA 8321 A 1 1.0 9/15/2014 AMZ Page 5 of 6 Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14090554 EHVIRt 14MENTAL;3`£CH6'+•"OL,= Si INC Cuyahoga Falls, Ohio 44223 Date Reported 9/22/2014 LT f.r m'Wi6al TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: hLW:Ilmvw.settek.con: Address: 284 Boger Rd. Mocksville NC 27028 Received: 9/5/2014 Project#: Roxboro WWTP Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Roxboro WWTP 001 9/3/2014 Flashpoint (140°F) >140 °F Solid EPA 1010 1 9/9/2014 TAH Roxboro WWTP 001 9/3/2014 Cyanide, Reactive ND ppm Solid EPA 9014 1 0.50 9/9/2014 TIR Roxboro WWTP 001 9/3/2014 pH 6.9 s.u. Solid EPA 9045 D 1 9/8/2014 AYS Roxboro WWTP 001 9/3/2014 Sulfide, Reactive ND ppm Solid EPA 9034 1 25 9/9/2014 TIR Page 6 of 6 l' . DC-7 Rev 13 08/21/14 Summit Environmental Technologies, Inc. Cooler Receipt Form Initials of person inspecting cooler and samples �7c Client: c �11r KaUfi _ _.._ ,� Order Number: Date Received: Tote Received1 yr5_ Date/Time coolers) opened and samples inspectedgL:j±L�jjt� Number of Coolers/Boxes- _ _ _I_ _ NIA Shipper: QE20 UPS DHL Airborne US Postal Walk-in Pickup Other Packaging Peanuts Bubble Wrap Paper Foam None Tape on cooterlbox N WA sc ti•r,ti Custody Seats intact YATAT C-O-C in plastic N NIA Sc ty-5-ry lee Blue ice I/ present I absent I melted NIA Sample Temperature IR Gun #16020459 CF_D.°C +-7 °C-y N/A Radiological Testing Instrument serial * 1 7 Y Z NIA (see page 2 for scan results) "Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified Immediately. C-O-C fitted out property l / N NIA Samples in separate bags Y N Q;I Sample containers intact' 01 N N/A 'If no, Fist broken sample(s) Sample labels) complete (ID, date, etc.) Label(s) agree with C-O-C Correct containers used Sufficient sample received Bubbles absent from 40 mL vials" Y — Samples with bubbles <6mm are acceptable Indicate bubble size d >6mm. Was client contacted about samples Y N Will client send new samples Y N Client contact: DatelTime: Logged in by: Comments: N N N N K NIA NIA NIA NIA NIA G:1QC SHAREMDocument Control Templates - TrackinglCooler reeetpt form Rev. 13 08-28-14.doc Page 1 of 2 F---� Summit Environmental Iechnolt)gies, h1c. =rdol!] Analysis Request/Chain of Custody 3,310 Win Street h(,r Summit Envirtmilicnial Ted,11010gic'- 111' USC 001% n] Cuphop Falls. Ohio 44223 Tel: 330,253.9211 Fax: 330,253.4-IS" Z� Pit ,,e CoinvanvNanw FW(—)jmk Name Analytical ha tarn and jMethods C0116—anvy" 'Ad, S Project AddressC, X, / t 70:2 Oc j l Client Phone No, Report lo C Isent hux No, E] P0# Client Email -Quoic No. it C1511factfPerNolk It J, Ufleck if (,)Ili' A Sim)P19d b) # Sample Identirication nllecteJ erte7. ,IT—tv rune Vcvi%ccIts: iatv 'tints F;`i ,c�. linents, Date Fillic Rush Retlueste the pt ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: . City of Roxboro WWTP WQ Permit Number: WQ 0021826 WWTP Name: Roxboro WWTP NPDES Number: NC 0021024 Monitoring Period: From 01/01/14 To 03/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion if ., ..1;..., l.lo +., .,14o n4:. .-f nrl id"Inve A nv !lace M rmmnla4n fhn fnllnwina mnni+nrina data[ Parameter Allowable Level in Sludge Pathogen . Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6'h CFU CFU/g Coliform power per gram of total solids CFU/g CFU 1000 MP NO LAND APPLICATION THIS PERIOD total solids 3 MPN per Salmonella bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Derek Clayton WWTP Superintendent Preparer Name nd Titl ( type or print) 1 ��, a_lors Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) ROXBORC /TP LAB DIGESTER "COOLER" SLUDGE DGE % TOTAL RESIDUE .- .OLATILE SOLIDS STANDARD METHODS 18TH ED. 2540B and 2540E Analyst: Jason Wilson Crystal Shotwell DATE / TIME OF TEST SAMPLE DATE DISH # VOL. ML INITIAL DISH WEIGHT (grams) WEIGHT DISH + WET SOLIDS (grams) WEIGHT WET SOLIDS (grams) WEIGHT DISH + DRY SOLIDS (grams) WEIGHT DRY SOLIDS (grams) % TOTAL SOLIDS IGNITED WEIGHT (grams) WEIGHT VOLATILE SOLIDS (grams) % VOLATILE SOLIDS RPD"S ANALYST INITIALS 1/7/14 1/7/2014 6 35 70.9170 106.3440 35.4270 70.9173 .0003 Blank 70.917 .0003 Blank JW 8:30 AM 1/6/2014 4 35 70.4084 105.6505 35.2421 70.7578 .3494 0.99 70.5310 .2268 65 JW 1/6/2014 9 35 73.4440 107.8052 34.3612 73.7858 .3418 0.99 73.5650 .2208 65 JW 1/14/2014 1/14/2014 4 35 70.4090 105.3732 34.9642 70.4090 .0000 Blank 70.4090 .0000 Blank JW 8:00 AM 1/13/2014 6 35 70.9179 105.5233 34.6054 71.2106 .2927 0.85 71.0187 .1919 66 JW 1/13/2014 9 35 73.4453 108.2050 34.7597 73.7395 .2942 0.85 73.5475 .1920 65 JW 1/21/2014 1/21/2014 4 35 70.4087 105.3128 34.9041 70.4086 -.0001 Blank 70.4085 .0001 Blank Jw 8:30 AM 1/20/2014 9b 35 72.5505 107.3402 34.7897 72.8240 .2735 0.79 72.6461 .1779 65 JW 1/20/2014 6 35 70.9182 105.3116 34.3934 71.1898 .2716 0.79 71.0126 .1772 65 JW 1/29/14 1/29/2014 4 35 70.9177 105.8467 34.9290 70.9177 .0000 Blank 70.9174 .0003 Blank JW 9:20 AM 1/27/2014 6 35 70.4083 105.7995 35.3912 70.6852 .2769 0.78 70.5067 .1785 64 JW 1/27/2014 9b 35 72.5502 107.7595 35.2093 72.8258 .2756 0.78 72.6477 .1781 65 JW 2/4/14 2/4/2014 6 35 70.9177 105.3976 34.4799 70.9178 .0001 Blank 70.9179 -.0001 Blank CS 8:17 AM 2/3/2014 9 35 72.5504 105.9153 33.3649 72.8050 .2546 0.76 72.6420 .1630 64 CS 2/3/2014 4 35 70.4089 104.5435 34.1346 70.6692 .2603 0.76 70.5022 .1670 64 CS 2/10/14 2/10/2014 6 35 70.9171 105.0344 34.1173 70.9173 .0002 Blank 70.9173 .0000 Blank CS 10:10 AM 2/10/2014 4 35 70.4093 104.2807 33.8714 70.6489 .2396 0.71 70.4939 .1550 65 CS 2/10/2014 9 35 73.4447 107.5212 34.0765 73.6860 .2413 0.71 73.5302 .1558 65 CS VSR 0% PASS DC x - Blank 2014 (First Quarter) VECTOR ATTRACTION CALCULATIONS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Roxboro WWTP WWTP Name: Roxboro WWTP NPDES Number: Monitoring Period: From 4/01/14 To 6/30/14 WQ Permit Number: WQ 0021826 NC 0021024 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class li complete the followin2 monitoring aata: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 1h CFU CFU/g Coliform power per gram of total solids CFU CFU/g 1000 MPN pei NO LAND APPLICATION THIS PERIOD total solids (d Salmonella I 3 MPN per 4 bacteria (in solids (dry lieu of fecal Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Derek Clayton, WWTP Superintendent —Pix�arer Name d Title (type or print) Land Applier Name and Title (if applicable) (type or print) rDA Signature of Preparer late Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date ROXBORO 'TP LAB DIGESTER "COOLER" SLUDGE % TOTAL RESIDUE L- _ JLATILE SOLIDS STANDARD METHODS 18TH ED. 2540B and 2540E Analyst: Jason Wilson Crystal Shotwell DATE / TIME OF TEST SAMPLE DATE DISH # I VOL. ML INITIAL DISH WEIGHT (grams) WEIGHT DISH + WET SOLIDS (grams) WEIGHT WET SOLIDS (grams) WEIGHT DISH + DRY SOLIDS (grams) WEIGHT DRY SOLIDS (grams) % TOTAL SOLIDS IGNITED WEIGHT (grams) WEIGHT VOLATILE SOLIDS (grams) % VOLATILE SOLIDS RPD"S ANALYST INITIALS 4/15/14 4/15/2014 1 35 78.2040 113.2590 35.0550 78.2040 .0000 Blank 78.204 .0000 Blank JW 10:30am 4/14/2014 2 35 80.1507 115.8932 35.7425 80.4756 .3249 0.91 80.2558 .2198 68 JW 4/14/2014 9 35 72.5513 107.2444 34.6931 72.8696 .3183 0.92 72.6543 .2153 68 JW 4/21/2014 4/21/2014 1 35 78.2025 113.0606 34.8581 78.2028 .0003 Blank 78.2025 .0003 Blank JW 9:00am 4/21/2014 2 35 80.1495 115.2770 35.1275 80.4285 .2790 0.79 80.2428 .1857 67 JW 4/21/2014 9 35 72.5499 107.7420 35.1921 72.8296 .2797 0.79 72.6428 .1868 67 JW 4/28/2014 4/28/2014 4 35 70.4076 105.4820 35.0744 70.4076 .0000 Blank 70.4076 .0000 Blank JW 8:00am 4/28/2014 6 35 70.9163 105.9360 35.0197 71.2069 .2906 0.83 71.0092 .1977 68 JW 4/28/2014 9 35 73.4416 108.4340 34.9924 73.7075 .2659 0.76 73.5290 .1785 67 JW 5/5/14 5/5/2014 4 35 70.4073 105.7320 35.3247 70.4073 .0000 Blank 70.4073 .0000 Blank JW 10:00am 5/5/2014 6 35 70.9162 106.0290 35.1128 71.1546 .2384 0.68 70.9990 .1556 65 JW 5/5/2014 9 35 72.5490 107.6712 35.1222 72.7894 .2404 0.68 72.6324 .1570 65 JW 5/13/14 5/12/2014 4 j 35 70.4071 105.8623 35.4552 70.4071 .0000 Blank 70.4071 .0000 Blank JW 5/12/2014 6 35 70.9170 105.7935 34.8765 71.1188 .2018 0.58 70.9879 .1309 65 JW 5/12/2014 9 35 72.5499 107.5158 34.9659 72.7524 .2025 0.58 72.6211 .1313 65 JW 5/20/14 5/20/2014 1 35 78.2028 113.2232 35.0204 78.2025 -.0003 Blank 78.2027 -.0002 Blank JW 5/19/2014 6 35 70.9168 105.9402 35.0234 71.1305 .2137 0.61 70.9943 .1362 64 JW 5/19/2014 9 35 72.5498 107.4247 34.8749 72.7624 .2126 0.61 72.6261 .1363 64 JW VSR 16.7% 411� DC x - Blank 2014 ( Second Quarter) VECTOR ATTRACTION CALCULATIONS ROXBORO WWTP LAB % TOTAL RESIDUE and VOLATILE SOLIDS STANDARD METHODS 18TH ED. 2540B and 2540E DIGESTER Analyst: Jason Wilson, Crystal Shotwell "COOLER" si 1 inr.F DATE / TIME OF TEST SAMPLE DATE DISH # VOL. ML INITIAL DISH WEIGHT (grams) WEIGHT DISH + WET SOLIDS (grams) WEIGHT WET SOLIDS (grams) WEIGHT DISH + DRY SOLIDS (grams) WEIGHT DRY SOLIDS (grams) % TOTAL SOLIDS IGNITED WEIGHT (grams) WEIGHT VOLATILE SOLIDS (grams) % VOLATILE SOLIDS RPD"S ANALYST INITIALS 5/27/14 5/27/2014 1 35 78.2025 113.6370 35.4345 78.2023 -.0002 1 Blank 78.2025 -.0002 Blank JW 9:45 AM 5/27/2014 6 35 70.9170 106.6385 35.7215 71.2038 .2868 0.80 71.0221 .1817 63 JW 5/27/2014 9 35 73.4409 108.9046 35,4637 73.7250 .2841 0.80 73.5447 .1803 63 JW 6/3/2014 6/3/2014 1 35 78.2024 113.2160 35.0136 78,2023 -.0001 Blank 78.2022 .0001 Blank JW 8:20AM 6/3/2014 6 35 70.9168 105.9188 35.0020 71,1709 .2541 0.73 71.0091 .1618 64 JW 6/3/2014 9 35 72.5497 107.5970 35.0473 72.8014 .2517 0.72 72.6418 .1596 63 JW 6/10/2014 6/10/2014 1 35 78.2025 113.3531 35.1506 78.2025 .0000 Blank 78.2023 .0002 Blank JW/CLS 8:00 AM 6/10/2014 6 35 70.9170 106.2242 35.3072 71.1563 .2393 0.68 71.0050 .1513 63 JW/CLS 6/10/2014 9 35 72.5484 107.9188 35.3704 72.7884 .2400 0.68 72.6379 .1505 63 JW/CLS 6/18/14 6/18/2014 1 35 78.2023 113.8240 j 35.6217 78.2025 .0002 Blank 78.2023 .0002 Blank JW 8:00 AM 6/17/2014 6 35 70.9164 106.1305 35.2141 71.1424 .2260 0.64 71.0020 .1404 62 JW 6/17/2014 9 35 72.5489 107.8722 35.3233 72.7765 .2276 0.64 72.6349 .1416 62 JW 6/24/14 6/24/2014 1 35 78.2021 113.5701 35.3680 78.2022 .0001 Blank 78.2021 .0001 Blank JW 8:20 AM 6/24/2014 6 35 70.9166 106.3015 35,3849 71.1383 .2217 0.63 71.0021 .1362 61 JW 6/24/2014 9 35 72.5492 107.6919 35.1427 72.7701 .2209 0.63 72.6345 .1356 61 JW 7/1/2014 7/1/2014 2 35 80.1492 115.8632 35.7140 80.1493 .0001 Blank 80,1491 .0002 Blank JW 8:00 AM 7/1/2014 6 35 70.9168 106.1922 35.2754 71,1174 .2006 0.57 70.9940 1 .1234 62 JW 7/1/2014 9 35 73.4390 109.0218 1 35.5828 73.6424 .2034 0.57 73.5170 .1254 62 JW VSR 4% PASS DC x - Blank West Lagoon 2014 (Second Quarter Re -do) VECTOR ATTRACTION CALCULATIONS a. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826 WWTP Name: Roxboro WWTP NPDES Number:- NC O021024 Monitoring Period: From 07/01/14 To 09/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class 13 complete the following momtorm data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 th CFU CFU/g 0 4/yr Grab 9222D Coliform . power per gram of total solids CFU/g CFU 1000 MPN pe NO LAND APPLICATION THIS PERIOD total solids (d Salmonella 3 MPN per 4 bacteria (in solids (dryl lieu of fecal Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 , Option/Mt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why.you have not met one or both of the requirements.). "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Derek Clayton WWTP Superintendent Preparer name And Title(print or type) Land Applier Name and Title (if applicable) (type or print) a -,a Signature of Preparer*f Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date Meritech, Inc. Environmental Laboratory .« Laboratory Certiflcation No.165 Page 1 Contact: Marshall Puryear Report Date .. 9/8/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014 Meritech Work Order # 09031424 Sample: Roxboro WWTP Cake 1 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 26.14 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,530 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D Bl Meritech Work Order #. 09031425 Sample: Roxboro WWTP Cake 2 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 26.16 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 2,780 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D 131 Meritech Work Order # 09031426 Sample: Roxboro WWTP Cake 3 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method ualifier % Total Solids 3128 % 9/3/14 0-100 % - SM 2540B Fecal Coliform (Sludge) < 27 col/g dry wt 9/3/14 27 col/g dry-wt SM 9222D B2 Meritech Work Order # 09031427 Sample: Roxboro WWTP Cake 4 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Metbod Qualifier %Total Solids 25.99 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 35 col/g dry wt 9/3/14 35 col/g dry wt SM 9222D B2 Meritech Work Order # 09031428 Sample: Roxboro WWTP Cake 5 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier %Total Solids 31.45 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 29 col/g dry wt 9/3/14 29 col/g dry wt SM 9222D B2 B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 nil. B2 Counts from all filters were zero. The value reported is based on the number of colonies per 100 nil that would have been reported if there had -been one colony on the filter representing the largest filtration volume (reported as a less than "<" value). 642 Tamco Road; Reidsville, Nortlr Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. X Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Marshall Puryear Report Date 9/8/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028. Date Sample Rcvd: 9/3/2014 Meritech Work Order # 09031429 Sample: Roxboro WWTP Cake 6 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method ualifier Total Solids 24.7 % 9/3/14 0-100 % SM 2540E Fecal Coliform (Sludge) 1,579 col/g cry wt 9/3/14 45 col/g dry wt SM 9222D Meritech Work Order # 09031430 Sample: Roxboro WWTP Cake 7 Grab 9/3/14 Parameters Results Analysis Date Reporting Lim! Method Qualifier % Total Solids 24.79 % 9/3/14 0-100,0/0 SM 2540B Fecal Coliform (Sludge) 1,815 col/g dry wt _ 9/3/14 45 col/g dry wt SM 9222D 131 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 in]. 132 Counts From all filters were zero. The value reported is based on the number of colonies per 100 nil that would have been reported if there had been one colony on the filter representing the largest filtration volume (reported as a less than "<" value). I hereby certify that I have reviewedand approve these data. [;{. Laboratory Representative 642 Tatnco Road, Reidsville, North Carolfrra 27320 tel.(336)342-4748 fax.(336)342-1522 3.70-2033 Chain of Custody Record (COC) NPDES#: Client: AV Phone: i - MERI"wN Le Address• !>Q i'Lf sk Fax: ENVIRONMENTAL LABORATORIES M oG�Ple— 7Z7o2? Email: + 642 TamcoRd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritech-labs.com Attention: AIAA% Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. www.merl'Tech-I(D��-�is.com = StdllOdays) Circle all that apply: Email (preferred) , Fax, Mail 3-5 Da s 24-48Hrs .Sampling Dates & Times Person Taking Sample (sign/Print): Lab Use ®iniy Sample Location and/or lD # Start End Comp? of lest(s) Required On Ice?. Yes pH OK? Date Time . Date Time Grab? Cont. / No Cl OK? c>sLa i�✓�v %' Grr(� O ` D r 4f0 L ' Temperature.Upon .Receipt Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: ]Jug Compositor# Shipment: [: UPS # Q: Fed Ex Arethese esultsfor regulatory purposes? Yes No Report results in: mg/L [ : mg/kg } ug/L (. Q-Hand Delivery Relinquis' ate � ,� 1 t��f�GD _ T m 'Z Received by: Date: Time: Other Relinquis try: Date: Time: Received by. Date: Time: Relinquished by: Date: Time: R ed by La _ • Datk:.. Time, l Meritech, Inc® Environmental Laboratory Laboratory Certification No.165 Page 1 Contact: Marshall Puryear Report Date 9/8/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014 Meritechi Work Order # 09031431 Sample: Roxboro WWTP PB 1 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 36.52 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 25 col/g dry wt 9/3/14 25 col/g dry wt SM 9222D B2 Meritech Work Order # 09031432 Sample: Roxboro WWTP PB 2 Grab Parameters Results Analysis Date Reporting Unit 9/3/14 Method Qualifier %Total Solids 39.73 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 340 col/g drywt 9/3/14 45 col/g dry wt SM 9222D B1 Meritech Work Order # 09031433 Sample: Roxboro WWTP PB 3 Grab 9/3/14 Parameters Results Analysis Date ReportingUnrit Method ualifer % Total Solids 43.44 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 187 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D B1 Meritech Work Order # 09031434 Sample: Roxboro WWTP PB 4 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 68.21 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 13 col/g dry wt 9/3/14 13 col/g dry wt SM 9222D B2 Meritech Work Order # 09031435 Sample: Roxboro WWTP PB 5 Grab 9/3/14 Parameters Results Aialysis Date Reporting Limit Method Qualifier %Total Solids 60.19 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 15 col/g dry wt 9/3/14 15 col/g dry wt SM 9222D B2 B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 ml. B2 Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been reported if there had been one colony on the filter representing the largest filtration volume (reported as a less than "<" value). 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342.4748 fax.(336)342-1522 Meritech, Inc® Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Marshall Puryear Report- Date 9/8/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 9/3/2014 Meritech Work Order## 09031436 Sample: Roxboro WWTP PB 6 Grab 9/3/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 39.45 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 461 col/g dry wt 9/3/14 45 col/g dry w( SM 9222D B1 Meritech Worlc Order # 09031437 Sample: Roxboro WWTP PB 7 Grab 9/3/14 Parameters Results Analysis Date Reportiva Limit Method Qualifier % Total Solids 47.62 % 9/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 777 col/g dry wt 9/3/14 45 col/g dry wt SM 9222D B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the colons on all filters reported per 100 till. B2 Counts from all filters were zero. The valuereported is based on the number of colonies per 100 till that would have been reported if there had been one colony on the filter representing the largest filtration volume (reported as a less than 'V' value). D/J I hereby certify that I have reviewed and appr®ve these data. laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 2-26-:0:3 Chain of Custody Record (COC) NPDES#: Client: �9 v Phone: Address:-2 63 o - & L,/f Fax: Lr� If a2P Email: Project: P.Q.#: Attention: j �L Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Std 10 days) 3- 5 Da s 24-48 Hrs Circle all that apply: Email (preferred), Fax, Mail � j p l 137 �J 1 ° e ENVIRONMENTALLABORATORIES9�OG1�S 642 Tamco.Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs.com a a a� �E•� p�� . med I ec —� s _ co Sample Location and/or ID # SaE'i'ipg[Ing Dates &Times Person Taking Sample (Sign/Print): Lab Use Only Start EndComp? Grab? Cont. Ttest(s) ������� on Ice? Yes / No pH OK? Cl OK? Date Time Date i1me oXbp2- 4vv7/-" �� o _ Dc (� d ��7iQL Sa 5 j r ' -7 1'/7 I ` N Temperature Upon Receipt: Method of Shipment: *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: Compositor #; UPS Jug# Fed Ex i Are these results for regulatory purposes? Yes No } Report results in: mg/t [ mg/kg E ugJL <' ��Hand Delivery jRelinquished e: Time: , 0%g Received by: Date: Time: Other Relinquished y: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: me: Receive b Lab �, D e:j 'rime: Y R0XB01 'WTP LAB DIGESTER "COOLER" % TOTAL RESIDU- a..J VOLATILE SOLIDS STANDARD METHODS 18TH ED. 2540B and 2540E Analyst: Jason Wilson Crystal Shotwell DATE / TIME OF TEST OL-UuuG SAMPLE DATE DISH # VOL. ML INITIAL DISH WEIGHT (grams) WEIGHT DISH + WET SOLIDS (grams) WEIGHT WET SOLIDS (grams) WEIGHT DISH + DRY SOLIDS (grams) WEIGHT DRY SOLIDS (grams) % TOTAL SOLIDS IGNITED WEIGHT (grams) WEIGHT VOLATILE SOLIDS (grams) % VOLATILE SOLIDS RPD"S ANALYST INITIALS 7/8/14 7/8/2014 1 35 78,2025 114.5390 36.3365 78.2022 -.0003 Blank 78.2022 .0000 Blank JW 8:30 AM 7/8/2014 6 35 70.9173 106.0916 35.1743 71.1989 .2816 0.80 71.0275 .1714 61 JW 7/8/2014 9 35 72.5492 107.7043 35.1551 72.8292 .2800 0.80 72.6592 .1700 61 JW 7/15/2014 7/15/2014 1 35 78.2027 112.2038 34.0011 78.2028 .0001 Blank 1 78.2024 .0004 Blank CS 8:00 AM 7/15/2014 7/15/2014 2 9 35 35 80.1493 73.4395 114.2340 107.1488 34.0847 33.7093 80.3957 73.6802 .2464 .2407 0.72 0.71 80.2439 73.5319 .1518 .1483 62 62 CS CS 7/22/2014 7/22/2014 1 35 78.2024 113.3050 35.1026 78.2020 -.0004 Blank 78.2020 .0000 Blank JW 8:00 AM 7/22/2014 6 35 70.9166 106.1274 35.2108 71.1645 .2479 0.70 71.0107 .1538 62 JW 7/22/2014 9 35 1 72.5490 107.6555 35.1065 72.7961 .2471 0.70 72.6429 .1532 62 JW 7/29/14 7/29/2014 1 35 78.2022 113.2345 35.0323 78.2022 .0000 Blank 78.2022 .0000 Blank JW 8:00 AM 7/29/2014 6 35 70.9168 106.2140 35.2972 71.1337 .2169 0.61 70.9987 .1350 62 JW 7/29/2014 9 35 72.5487 107.7702 35.2215 72.7641 .2154 0.61 72.6307 .1334 62 JW 8/5/14 8/5/2014 2 35 80.1488 115.1521 35.0033 80.1494 .0006 Blank 80.1490 .0004 Blank JW 8:00 AM 8/5/2014 6 35 70.9180 106.2083 35.2903 71.1255 .2075 0.59 70.9965 .1290 62 JW 8/5/2014 9 35 73.4389 108.9099 35.4710 73.6487 .2098 0.59 73.5188 .1299 62 JW 8/12/14 8/12/2014 2 35 80.1495 115.1959 35.0464 80.1493 -.0002 Blank 80.1493 .0000 Blank JW 8:00 AM 8/12/2014 6 35 70.9174 106.0212 35.1038 71.1147 .1973 0.56 70.9935 .1212 61 JW 8/12/2014 9 35 73.4394 108.4972 35.0578 73.6369 .1975 0.56 73.5155 .1214 61 JW VSR 0% PASS WW x - Blank 2014 (Third Quarter) VECTOR ATTRACTION CALCULATIONS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826 WWTP Name: Roxboro WWTP Monitoring Period: From 10/01/14 To 12/31/14 NPDES Number: NC 0021024 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlicable to alternative nerformed (Class A or Class B) comalete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 th CFU 27 35 39 CFU/g 0 4/yr Grab 9222D Coliform power per gram of total solids 17 26 33 CFU/g 0 4/yr Grab 9222D CFU 2x10to the 6 th CFU CFU/g power per gram of total solids 1 solids Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. l Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly Qather and evaluate the information used to determine that the ppathogen and vector attraclion reduction requirements Piave been met. I am aware that there are significant penalties or false certification including fine and imprisonment." Derek Clayton, WWTP Superintendent Pxc arer Name and Title Land Applier Name and Title (if applicable) (type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 1 Contact: Marshall Puryear Report Date 11/6/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014 Meritech Work Order # 11041409 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 29.13 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 34 col/g dry wt 11/4/14 34 col/g dry wt SM 9222D Meritech Work Order # 11041410 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 27.40 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 37 col/g dry wt 11/4/14 37 col/g dry wt SM 9222D Meritech Work Order # 11041411 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 25.44 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 39 col/g dry wt 11/4/14 39 col/g dry wt SM 9222D Meritech Work Order #' 11041412 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 27.61 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 36 col/g dry wt 11/4/14 36 col/g dry wt SM 9222D Meritech Work Order # 11041413 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 28.91 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 35 col/g dry wt 11/4/14 35 coI/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Marshall Puryear Client: Synagro 284 Boger Road Page 2 Report Date 11/6/2014 Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014 Meritech Work Order # 11041414 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 36.8 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 27 col/g drywt 11/4/14 27 col/g dry wt SM 9222D Meritech Work Order # 11041415 Sample: Roxboro WWTP Centrifuge Material 11/4/14 Parameters Results Analy�iE Date Reporting Limit Method % Total , Solids 26.18 % 1114/14 0-100 % SM2540E y Fecal Coliform (Sludge) < 38 col/g dry wt 11/4/14 38 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. ,Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 34a-2013: Chain of Custody Record (COC) NPDESit-. Client: Phone: MERFECH Address: Fax: ENVIRONMENTAL LABORATORIES Email: 642 Tamcb.Rd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.OX: Email: info@meritech-labs.com Attention: Turn Around Tirne* - How would you like your report sent? *RUSH work needs prior approval. ,www.meri techdabs,CorM ( Circle all that apply: Email (preferred), Fax, Mail -Std io days) 3 5 Da s 24-481-irs .Sampling Dates & Times Person Taking Sample (Sign/Print): Lab Use 0 n . IV' Samplelocatibri and./or ID-# '7-0)'�L#62 Start Enid comp? It of Test(s) Required I S)94ce? H OK? Date Time Date Time Grab? Cont. -Yes No Yes CI: OK? 11/1"ho /0-.00 ALL] 557/44. e_ NA J5 4V Terbperature Upon Recs'pt: (— Dechlorinatioh of Ammonia, Cyanide, Phen-ol.and TKN be done field Method of (-c0.5 p0m) samples must in the prior to preservation: "5 Comments; IJug Compositor It Shipment: ET UPS Fed Ex Are these results for regulatory purposes? 'Yes Et No Or Report results in: nig/L [I,' mg/kg Q- ug/L Q; qHand Delivery Relinquished by%// Date�/,, Time: Received by: Date: Time:, Other Relinquished by:. Date:f Time.: Received by: Date: Time: - I Relinquished by: Date: Time: e: im Y PT IT -D � %6 Meritech, Inc. Environmental Laboratory x. ._ . Laboratot• Certification No 165 Page 1 Contact: Marshall Puryear Report Date 1.1/13/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014 Meritech Work Order # 11041416 Sample: Roxboro WWTP Mix Gram 11/4/14 Parameters Results Analysis Date Reporting_Limit Method % Total Solids 35.09 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 29 col/g dry wt 11/4/14 29 col/g dry wt SM 9222D Meritech Work Order # 11041417 Sample: Roxboro WWTP Mix Grab 11/4/14 Parameters Results Analysis Date Reporting Limit Method %Total Solids 36.43 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 27 col/g dry wt 11/4/14 27 col/g dry wt SM 9222D Meritech Work Order # 11041418 Sample: Roxboro WWTP Mix Grab 11/4/14 Parameter s Results Analysis Date Reporting Limit Method %Total Solids 36.40 % 11/4/14 0-.100 % SM 2540B Fecal Coliform (Sludge) .... < 27 col/g dry wt .11/4/14 27 col/g dry wt SM 9222D Meritech Work Order # 11041419 . Sample: Roxboro WWTP Mix Grab Parameters Results Analysis Date Reporting Limit Method %'Total Solids 41.74 % 11/4/14 0-100 % SM 254OB Fecal Coliform (Sludge) < 24 col/g dry wt 11/4/14 24 col/g drywt . SM 9222D Meritech Work Order # 11041420 Sample: Roxboro WWTP Mix Grab 11/4/14 Parameters Results Analysis Date Reporting Lhnit Method % Total Solids 30.65 % - 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 33 col/g dry wt 11/4/14 33 col/g dry wt SM 9222D 642 Tatttco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 erl"tech, Inc,, :. Environmental Laboratory Laboratory Certification No.165 Page 2 Cozitact: Marshall Puryear Report Date 1.1/13/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 11/4/2014 Meritech Work Order # 11041421 Sample: Roxboro W WTP Mix Grab 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 57.32 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 17 col/g dry wt . 11/4/14 17 col/g dry wt SM 9222D Meritech Work Order # 11041422 Sample: Roxboro WWTP Mix Grab 11/4/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 33.37 % 11/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 30 col/g dry wt 11/4/14 30 col/g dry wt SM 9222D bi 1 hereby certify that I have reviewed and approve these data. G Laboratory Represent tive 642 Tamco Road, Reidsville, North Carolina. 27320 tel,(336)342-4748 fax.(336)342-1522 3�o-zo�a Chain of Custody Record (COC) NPDES#: Client:_ Sal Phone: 11-INC. . Address: Fax: '�� ` y J X ENVIRONMENTAL L BORATO.R6ES Email: 642 Tam coRd. Phone: 336-342-4748 Project: M�L Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs.com Attention: Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. vvvi.mentech—labso(®m Circle all that apply: Email (preferred), Fax, Mail Std 20da s) 3-S Davs, 24-48Hrs = 0: .Sc"31iY'dpfrog Dates six Times Person Taking Sample (Sign/Print): Lab We Only Sample Location, and/or ID # Start End , Comp. r #o, Test(s)Required Ice? pH OK? Date Time Date Time Grab? Cont. Yes / No 7 CI OK. C1 € Temperature Upon cp�t " L *** Dechlorination (<0.5 Ammonia, Cyanide, Phenol TKN be done in the field *** Method o''� ppm) of and samples must prior to preservation. Compositor: # Comments: Shipment: � ❑' UPS j Jug # Fed Ex Are these results for regulatory purposes? Yes Q No Q ! Report results in: mg/L Q mg/kg 0 ug/L : JRelinquished by: Date: Time: Hand Delivery )Received by: �� 30 Date: Time: z/ ¢ /9- Other iRelinquished by: Date.. Time: Received by: Date: Time: _ r IIRelinquished by: Date: Time: f.' DIGESTER "COOLER" ROXBORC '/TP LAB % TOTAL RESIDUE OLATILE SOLIDS STANDARD METHODS 18TH ED. 2540B and 2540E Analyst: Jason Wilson Crystal Shotwell DATE / TIME OF TEST SAMPLE DATE DISH # VOL. ML INITIAL DISH WEIGHT (grams) WEIGHT DISH + WET SOLIDS (grams) WEIGHT WET SOLIDS (grams) WEIGHT DISH + DRY SOLIDS (grams) WEIGHT DRY SOLIDS (grams) % TOTAL SOLIDS IGNITED WEIGHT (grams) WEIGHT VOLATILE SOLIDS (grams) % VOLATILE SOLIDS RPD"S ANALYST INITIALS 10/7/14 10/7/2014 1 35 78.2020 114.0271 35.8251 78.2020 .0000 Blank 78.2021 -.0001 Blank JW 8:15 AM 10/6/2014 2 35 80.1495 115.3586 35.2091 80.5052 .3557 1.01 80.2842 .2210 62 JW 10/6/2014 6 35 70.9171 106.1904 35.2733 71.2745 .3574 1.01 71.0515 .2230 62 JW 10/14/2014 10/14/2014 1 35 78.2022 113.8495 35.6473 78.2022 .0000 Blank 78.2022 .0000 Blank JW 10/13/2014 2 35 80.1492 115.3514 35.2022 80.4660 .3168 0.90 80.2652 .2008 63 JW 10/13/2014 9 35 72.5483 107.6409 35.0926 72.8622 .3139 0.89 72.6624 .1998 64 JW 10/20/2014 10/20/2014 1 35 78.2018 113.5582 35.3564 78.2018 .0000 Blank 78.2018 .0000 Blank JW 8:30 AM 10/20/2014 2 35 80.1488 115.4020 35.2532 80.4455 .2967 0.84 80.2586 .1869 63 JW 10/20/2014 9 35 72.5480 107.9370 35.3890 72.8454 .2974 0.84 72.6576 .1878 63 JW 10/27/14 10/27/2014 1 35 78.2016 113.8252 35.6236 78.2018 .0002 Blank 78.2016 .0002 Blank JW 10/27/2014 2 35 80.1490 115.2628 35.1138 80.4202 .2712 0.77 80.2483 .1719 63 JW 10/27/2014 9 35 72.5479 107.9455 35.3976 72.8207 .2728 0.77 72.6482 .1725 63 JW 11/3/14 11/3/2014 1 35 78.2013 113.6320 35.4307 78.2015 .0002 Blank 78.2013 .0002 Blank JW 9:15 AM 11/3/2014 2 35 80.1488 115.4568 35.3080 80.4094 .2606 0.74 80.2443 .1651 63 JW 11/3/2014 9 35 72.5479 108.3052 35.7573 72.8124 .2645 0.74 72.6449 .1675 63 JW 11/11/11 11/11/2014 1 35 78.2013 113.4001 35.1988 78.2014 .0001 Blank 78.2014 .0000 Blank JW 8:15AM 11/10/2014 2 35 80.1491 115.2948 35.1457 80.4115 .2624 0.75 80.2462 .1653 63 JW 11/10/2014 9 35 72.5479 107.7833 35.2354 72.8124 .2645 0.75 72.6459 .1665 63 JW VSR -4% PASS WW x - Blank 2014 (Fourth Quarter) VECTOR ATTRACTION CALCULATIONS 2014 603 VECTOR ATTRACTION This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15% Reduction % Formula Reduction In - Out n .65,65 .65 n .00 n .00 n In - (In x Out) .65 - (.65 x .65) .65 - .42 .23 .000 x 100 0 .0 First Quarter 2014 In - Out .68 - .64 n .040 n 040 n In - (In x Out) . .68 - (.68 x .64) .68 - .44 .24 .167 x 100 16.7 Second Quarter 2014 In - Out n .63 - .62 rl .010 n .01 n In - (In x Out) 63 - (.63 x .62) .63 - .39 .24 0.042 x 100 4 Second Quarter 2014 In - Out 0.61 - 0:61 n .00 n .00 n In - (In x Out) 61 (.61 x .61) 0.61 - .37 24 0 x 100 Q 0.0 Third Quarter. 2014 In - Out n 0.62 - 0.63 n -.01 n -.01 n In - (In x Out) .62- (.62 x .63) 0.62- .39 23 -0.043 x 100 0 -4.3 Fourth Quarter 2014 Agricultural Lime Application Log Year: 2014 Project: Roxboro Field (state -county -site -field) Soil pH Lime Requirement (from soil analysis) Tons/Acre Applied Date Applied NC-PS-24-01 Ronald Carver 6.0 O:OT/Ac. NC-PS-24-02 Ronald Carver 5.8 OAT/Ac. NC-PS-24-03 Ronald Carver 6.0 O.OT/Ac. NC-PS-25-1A Paul Bailey 6.5 O.OT/Ac. NC-PS-25-1 B Paul Bailey 6.6 O.OT/Ac. NC-PS-25-02 Paul Bailey 5.6 0.8T/Ac. NC-PS-25-03 Paul Bailey 5.9 O.OT/Ac. NC-PS-25-04 Paul Bailey 6.3 O.OT/Ac. NC-PS-25-05 Paul Bailey 6.5 O.OT/Ac. NC-PS-26-01 Henry Martin 6.3 O.OT/Ac. NC-PS-26-02 Henry Martin 6.2 O.OT/Ac. NC-PS-26-03 Henry Martin 5.9 O.OT/Ac. Lime will be applied when field conditions permit. NCDA&CS, iomic Division Phone: (919) 733-2665 Website: www.r__,` I gov/agronomi/ Report No. FY111 )16359 Predictive Client: Ronald Carver 105 Carver Farm Rd. Advisor: Nate Roth Synagro . Mehlich-3 Extraction Roxboro, NC 27573 284 Boger Rd Mocksville, NC 27028 A Soil Report Sampled County: Perquimans r Sampled: Received: 11/14/2014 Completed: 12109/2014 Farm: NC-PS-24 Links to Helpful Information Sample ID: 24-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 100 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drrP]: Soil Class: Mineral, HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.41 0.88 11.5 86 1.6 6.0 171 22 61 24 38 536 339 274 274 490 0.1 1 Sample ID: 24-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.4 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crrP; CEC and Na in meq/1 00 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.36 . 0.86' 12.5 86 1.7 5.8 244 68 54 30 64 232 156 368 368 433 0.1 1 Sample ID: 24-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cd; CEC and Na in meq/100 crrP; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.32 0.92 10.7 89 1.2 6.0 112 63 54 31 44 301 197 170 170 218 0.1 1 Y,-North'Carolina fobaccoTiu!,; 1�uml Cwilads%loti Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox1er, Commissioner of Agriculture NCDA&CS ".. ;%iomic Division Phone: (919) 733-2655 Website: www.nw ..goy/agronomil Ronald Carver Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to .micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note• Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.aov/agronomi/oboart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.goy/agronorni/uyrst.htm for more information. Report No. FY1,__1016359 Page 2 of 2 Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-AI1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P206 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS .,_ comic Division Phone: (919) 733-2656 Website: www.f,, _„gov/agronomi/ Report No. FYI- `)16358 Client: Paul Bailey Advisor: Nate Roth Predictive 2260 Haywood Bailey Rd. Synagro ,_ . Roxboro, NC 27573 284 Boger Rd Mocksville, NC 27028 Soil Report Mehlich-3 Extraction Sampled County: Perquimans Sampled: Received: 11/14/2014 Completed: 12/09/2014 Farm: NC-PS-25 Links to Helpful Information Sample ID: 25-1a Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 0 90 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - W/V in g/crrt3; CEC and Na in meg1100 cd; NO3-N in mg/drrr`t]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.22 0.93 12.3 94 0.7 6.5 195 24 72 21 52 717 439 430 430 616 0.1 1 Sample ID: 25-1b Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 0 70 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - W/V in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 0.88 13.9 96 0.6 6.6 247 36 73 22 53 191 122 408 408 570 0.1 1 Sample ID: 25-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.8 120-200 0 40 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 cm3; NO3-N in mg/drrt3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.32 0.91 12.2 84 1.9 5.6 202 51 55 27 49 198 136 420 420 537 0.1 1 North Carolina Tobacco 7n15s fwid camni6ssicre Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. . - Steve Troxler, Commissioner of Agriculture NCDA&CS .-_._.__comic Division Phone: (919) 733-2655 Website: www.r:__.__gov/agronomi/ Report No. FYI_-_316358 Paul Bailey Page 2 of 3 Sample ID: 25-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.84 10.3 87 1.4 5.9 114 80 58 25 50 265 .176 342 342 271 0.1 1 Sample ID: 25-04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim,1 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cd; CEC and Na in meq/100 crrr3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.27 0.84 11.6 92 1.0 6.3 197 40 61 29 44 208 138 346 346 467 0.1 1 Sample ID: 25-05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 0 80 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cmR; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 0.94 10.3 93 0.7 6.5 97 31 64 28 36 235 150 148 148 277 0.1 1 NCDA&CS,., ,.:;,comic Division Phone: (919) 733-2665 Website: www.rl___�_gov/agronomi/ Report No. FY16_6016358 Paul Bailey Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uyrsthtm for more information. Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-I potassium index K20. potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-Ail Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-Al zinc availability index Zn-I zinc index NCDA&CS, _w__lomic Division Phone: (919) 733-2655 Website: w4vw.r1., _,,govlagronomi/ Report No. FY1 )16366 Predictive Client: Henry Martin 183 Martin Estate Rd Advisor: Nate Roth Synagro Mehlich-3 Extraction .►¢ �x� Soil. „rt Roxboro, NC 27573 Boger Rd 284 Bo 9 Mocksville, NC 27028 rx,{ 1`�N Sampled County: �a�: �t'Ylilt�fi 5y Sampled: Received: 11/14/2014 completed: 12/09/2014 Farm: NC-PS-26 Links to Helpful Information Sample ID: 26-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cd; CEC and Na in meg1100 cnY3; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 0.85 11.8 92 1.0 6.3 268 138 57 29 62 250 163 463 463 587 0.1 1 Sample ID: 26-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in glcrn3; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.83 12.2 91 1.0 6.2 354 120 58 28 66 199 134 644 644 719 0.1 1 Sample ID: 26-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/crrti3; CEC and Na in meq/100 cnr3; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.85 10.8 86 1.6 5.9 244 78 55 27 49 233 157 541 541 664 0.1 1 North Carolina Tobacco Trust rund Com1M%%13u Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS ). 4 _i�-iomic Division Phone: (919) 733-2655 Website: www.r:�_-&.tgov/agronomi/ Report No. FY1 . D16366 Henry Martin Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer . Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown,' not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-.0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.Htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncaar.pov/agronomi/oboart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results Page 2 of 2 Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn Mn-All Mn-Al2 Mn-I M-O N Na NO3-N ORG pH P-1 P205 S-1 SS-1 W/V The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacrr.gov/aaronomi/uvrst.htm for more information. manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index , mineral -organic soil class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index