WQ0021577_Residual Annual Report 2014_20150227

177
KAPSTONE .
KRAFT PAPER. CORPORATION
A Division of KAPSTONE PAPER AND PACKAGING CORPORATION
100 Gaston Road Roanoke Rapids, NC 27870 -
kapstonepaper.corn .
rcuruary ��, /.ula
V
OED
FEB 2 7 2015
NCDENR-DWQ DVVR SECTION "
Attention Information Processing Unit . INFORMATION PROCESSING UNIT
1617 Mail Service Center
Raleigh, North Carolina 27699-01617
To Whom It May Concern:
Permit No. WQ0021577 requires that KapStone Kraft Paper Corporation, Roanoke Rapids Mill,
submit an'annual Distribution of Residuals Solids report. Included in the yearly report are the
Toxicity Characteristics Leaching Procedure analysis, nutrient analysis, pathogen .reduction, and
distribution of residuals report for 2014
Flyash residuals generated in 2014 were sent to the KapStone Surface Disposal Unit, Permit #
WQ000436 for disposal or sold to Scotts Hyponex in Lawrenceville, Va. To use as a potting soil
amendment: KapStone sent 982.7 scaled tons to Scott Hyponex.
No beneficial use -of the Primary Clarifier Residuals for the year 2014 was found. All Primary
Clarifier residuals generated in 2014 were sent to the KapStone Surface Disposal Unit, Permit #
WQ000436 for -disposal..,
If there are any questions or concerns please contactme at 252-533-6295:
'Sincerely,. ..
Ne 1 Davis
Environmental Engineer
Enclosures
xc:
Bill Kessinger
Ben White
Mike Knudson.
Steven Walker

ANNUAL DISTRIBUTION OF RESIDUAL PERMIT REPORT 2014
PERMIT #WQ0021577
KAPSTONE KRAFT PAPER CORPORATION
RoANoKE RAPIDS, NC
TABLE OF CONTENTS
Page
Distribution of Residuals Summary Table 2014............................................................ 1— 2
Form DMSDF — Primary Clarifier Residuals Annuals Certification 2014 .................. 3-4
Form RSSF — Primary Clarifier Residuals Sampling Summary....................................5-6
Form RSSF-B — Primary Clarifier Residuals Sampling Summary B ............................7-8
Sample Analysis Primary Clarifier Residuals..............................................................9 — 34
TCLP — Sampling Analysis Primary Clarifier Residuals ......................................... 35 — 39
Form PVRF' 02T — Primary Clarifier Residuals Annual Pathogen Reduction ........ 40 — 69
Form DMSDF — Flyash Residuals Annuals Certification 2014 .............................. 70 — 71
Form RSSF — Flyash Residuals Sampling Summary .............................................. 72 — 73
Form RSSF-B — Flyash Residuals Sampling Summary B........................................ 74 — 75
Sample Analysis Flyash Residuals........................................................................ 76 —100
TCLP — Flyash Residuals...................................................................................... 101-105
Form PVRF 02T — Flyash Residuals Annual Pathogen Reduction Form ........... 106 —135

DISTRIBUTION OF RESIDUALS
SUMMARY TABLE
2014

2014 Kapstone Surface Disposal Unit Inputs
Permit # WQ0021577
�� AltJmts are In As is (Scaled T'00W pus
Prunar2
an
-TdA
Wit
January
February
466.0
466.0
March
516.7
516.7
April
May
June
July
August
September
October
November
December

FORM DMSDF
PRIMARY CLARIFIER RESIDUALS
ANNUAL CERTIFICATION
2014

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0021577
PHONE: [phone]
FACILITY NAME: KAPSTONE KRAFT PAPER CORP. ROANOKE RAPIDS, NC
COUNTY: HALIFAX OPERATOR:
NEAL DAVIS
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
21 Distribution and Marketing (complete Parts A, B, and C)
Was the facilitv in operation during the Dast calendar vear? Yes R1 No --* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
. Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
PRIMARY CLARIFIER RESIDUALS
910.8
MONOFIL WQ 0000436
910.8
February
PRIMARY CLARIFIER RESIDUALS
725.2
MONOFIL WQ 0000436
725.2
March
PRIMARY CLARIFIER RESIDUALS
914.8
MONOFIL WQ 0000436
914.8
April
PRIMARY CLARIFIER RESIDUALS
891.1
MONOFIL WQ 0000436
891.1
May
PRIMARY CLARIFIER RESIDUALS
758.4
MONOFIL WQ 0000436
758.4
June
PRIMARY CLARIFIER RESIDUALS
843.7
MONOFIL WQ 0000436
843.7
July
PRIMARY CLARIFIER RESIDUALS
1142.3
MONOFIL WQ 0000436
1,142.3
August
PRIMARY CLARIFIER RESIDUALS
943.3
MONOFIL WQ 0000436
943.3_
September
PRIMARY CLARIFIER RESIDUALS
1085.5
MONOFIL WQ 0000436
1085.5
October
PRIMARY CLARIFIER RESIDUALS
910.1
MONOFIL WQ 0000436
910.1
November
PRIMARY CLARIFIER RESIDUALS
981.2
MONOFIL WQ 0000436
981.2
December
PRIMARY CLARIFIER RESIDUALS
1365.1
MONOFIL WQ 0000436
1,365.1
Total from FORM DMS DF ( P su
0 .
x: W
4:
„
Totals:
Annual (dry tons):
n�.0�,���-
1. 11��4,�tk,5X
71:5
i1�.
i T`.. e
1`1' 4115 , ;
Amendment(s) used: 0
* If more space is required, attach additional information sheets (FORM DMSDF
Bulking Agents used: 0
(supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the Distribution of Residuals 21 Yes
permit (including but not limited to items 1-3 below) issued by the Division of Water Quality: 13 No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
f �/ �I
1 I
Signature of PenLtee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Sign,gture of Preparer**
(if different from Permittee)
"11-5-
Date
DENR FORM DMSDF (12/2006) 4

Form RSSF
Primary Clarifier Residuals Sampling Summary

I -
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
w
.WQ Permit Number: WQ 0021577 Laboratory: 1) Meritech, Inc. Reidsville NC
Facility Name: KapStone Kraft Paper Corporation 2)
Residual Source
WQ # or NPDES NC0000752 4)
#:
)
WWTP Name: KapStone Kraft Paper Corporation 5) Primary Clarifier Residuals
Parameter
(mg/kg)
Conc.
Limit
m
Sample or Composite Date
1/7/14
2/4/14
3/4/14
4/2/14
5/7/14
6/10/14
7/8/14
8/5/14
9/2/14
10/14/14
11/4/14
12/9/14
Percent Solids (%)
NA
39.7
46.2
48.6
49.4
45.7
43.9
44.7
42.6
45.8
50.3
44.1
37.3
Arsenic
75
5.63
-18.4
13.2
11.7
4.27
9.93
1.12
1.17
13.2
0.994
2.95
6.94
Cadmium
85
2.5
0.539
1.72
1.53
2.09
0394
1.8
1.25
2.18
3.22
1.47
1.39
Copper
4,300
96.3
55.4
58.4
46.4
84.9
30.3
65.8
200
62.7
21.7
1.21
63.5
Chromium
NA
18
14.4
14.4
11.7
18.9
8.11
13.4
13.9
16.8
20.3
0.254
27.1
Lead
840
10.8
19.2
12.1
10.8
10.8
9.64
10.9
7.8
11
8.39
11.6
15.1
Mercury
57
0.05
0.17
0.134
0.071
0.28
0.068
0.078
0.07
0.066
0.02
0.045
0.04
Molybdenum
75
0.625
0.543
0.51
0.506
0.547
0.569
0.559
0.587
0.546
0.497
0.567
0.67
Nickel
420
18.6
17.8
15.7
13.5
18.8
10.9
13
64.6
16.4
16.7
15.1
24.1
Selenium
100
1.25
1.09
1.02
1.01
1:09
1.16
0.224
1.17
2.53
0.994
1.13
2.92
Zinc
7,500
323
37.8
153
142
234
19.1
208
149
189
100
183
158
Total Phosphorus
NA
1480
543
706
844
1,324
269
1,010
770
1,120
1,130
916
1,340
TKN
NA
107
43.3
170
40.5
330
101
120
198
47.7
288
150
456
Ammonia -Nitrogen
NA
25.2
21.6
20.6
20.2
21.9
22.8
22.4
23.5
21.8
19.9
22.7
26.8
Nitrate and Nitrite
NA
25.2
21.6
20.6
20.2
21.9
22.8
22.4
1 23.5
21.8
1 19.9
1 22.7
1 515
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitten false info mation, including the possibility of fines and imprisonment for knowing violations."
a z� A5
Signature of Pr arer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) 6

Form RSSF-B
Primary Clarifier Residuals Sampling
Summary B

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
WQ 0021577
KAPSTONE KRAFT PAPER CORP
NPDES # NC0000752
KAPSTONE KRAFT PAPER CORP
Laboratory: 1) Meritech, Inc. Reidsville NC
2)
3)
4)
5) Primary Clarifier Residuals
1\qv.;a UR1 Al1LLl ala 1 -..w
Parameter
(mg g)
_
Sample or Composite Date
1/7/14
2/4/14
3/4/14
4/2/14
5/7/14
6/10/14
7/8/14
8/5/14
9/2/14
10/14/14
11/4/14
12/9/14
Aluminum
7,980
21,600
12,410
2,145
7,614
8,861
7,520
5,210
7,270
2700
7,800
9,840
Magnesium
6,380
2,040
4,350
858
4,748
1,473
3,620
2,790
3,930
2,270
4,130
3,080
Sodium
Potassium
CCE
6,050
2,040
43.80%
4,540
7,540
33.30%
3,530
3,350
27.20%
2,085
1,767
20.00%
5,185
1,630
26.90%
4,784
2,802
24.00%
5,190
1,910
21.30%
5,400
1,070
21.1%
2,790
1,690
28.60%
2,470
513
42.5%
4,970
1,260
30.40%
3,380
2,820
25.10%
SAR
PAN
6.3
70.5
12.5
41.1
4.83
1 90.7
5.64
38.4
5.91
156.1
17.4
65.5
6.77
72.6
19.9
105.1
8.8
43.1
2.59
137.1
6.19
85
4.62
700.1
pH
8.4
8.5
8.7
7.8
7.8
9.4
7.6
7.4
8.7
-8.7
7.4
7.5
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly
gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment .
for knowing violations."
Signature of Pre/arer *
*Preparer is defined in 40-CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
a /x
Date
DENR FORM RSSF - B (12/2006) 8

Sampling Analysis Primary Clarifier Residuals

� 1S
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
•.A �."fX,
Contact: Neal Davis Report Date: 1/20/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Project: Send Even Months
Date Sample Rcvd: 1/7/2014
Meritech Work Order #
01071470 San,plE: Primary Clarif er Grab
1/7/14
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
39.7 %
1/8/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 25.2 mg/kg
1/9/14
25.2 mg/kg
EPA 350.1
TKN
107.0 mg/kg
1/10/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 25.2 mg/kg
1/10/14
25.2 mg/kg
EPA 353.2
Nitrogen, total
107 mg/kg
1/16/14
20 mg/kg
EPA 353.2
Aluminum, total
7,980 mg/kg
1/16/14
5.00 mg/kg
EPA 200.7
Arsenic, total
5.63 mg/kg
1/16/14
1.00 mg/kg
EPA 200.7
Barium, total
388 mg/kg
1/16/14
0.500 _mg/kg
EPA 200.7
Cadmium, total
2.50 mg/kg
1/16/14
0.200 mg/kg
EPA 200.7
Calcium, total
129,000 mg/kg
1/16/14
10.0 mg/kg
EPA 200.7
Chromium, total
18.0 mg/kg
1/16/14
1.00 mg/kg
EPA 200.7
Copper, total
96.3 mg/kg
1/16/14
1.00 mg/kg
EPA 200.7
Lead, total
10.8 mg/kg
1/16/14
1.00 mg/kg
EPA 200.7
Magnesium, total
6,380 mg/kg
1/16/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.05 mg/kg
1/8/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.625 mg/kg
1/16/14
0.625 mg/kg
EPA 200.7
Nickel, total
18.6 mg/kg
1/16/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
1,480 mg/kg
1/16/14
2.00 mg/kg
EPA 200.7
Potassium, total
2,040 mg/kg
1/16/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 1.25 mg/kg
1/16/14
1.25 mg/kg
EPA 200.7
Sodium, total
6,050 mg/kg
1/16/14
20.0 mg/kg
EPA 200.7
Zinc, total
323 mg/kg
1/16/14
1.0 mg/kg
EPA 200.7
SAR
6.30
1/16/14
-
-
pH
8.4 S.U.
1/8/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
43.8 %
1/10/14
1 %
AOAC 955.01
I hereby certify that / have reviewed and approve these data. P!, -w4r
Laboratory Representative
10
642 Tamco Road, Reidsville, North Carolina 27320
tnlfW2KV2A7 A'9A0C-!77L%7A� � r I -

%-UbLU ay mecord (COC)
,
ERIT ECH INC
,:
Client: Kapstone Paper `.�
`
Environmental Labor^torie�c
Phone:
:..
A Division of Water Technology and Control, inc.
Address: 100 Gaston Rd
642 Tamco Rd
Phone
Email: ;�-7�•� ./):�•::�( ���:�1:�s-'.....�,,�
Roanoke Rapids, NC
,
Reidsville, NC
1-336-342-4748
Project: Send Even Months
27870
Fax: [phone]
Po #:
27320
-- ---- ----------
Email: wtclab(a-bellsouth net_
---- ---- - ---
Turn Around Time*
---Attention:--Neal-Davis
Web Site: www.meritech-labs.com
- ----- ---8fii-(1;O:daysj --3 = 5 Day 24 - 48 Hr
Sample
p
Sampling Dates 8� Times
r—
Location/ID #
START
, : rl .'
Person Taking Sample (Signature): �:;, ; : Lab Use Only
END
Date Time Date Time
Comp? # of s
Grab? Conts. Tests,Required On pH OK?
'rimary Clarifier
I _:.,�
ice? C12 OK?
-;
/o Total Solids, pH ()
1 Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn
1 NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Comments:
?thod of Shipment:
UPS
Will these resultsibe'used for regulatory
Fed Ex
purposes?
Yes �- No
*RUSH work must roved prior to submitting samples.
1Hand Delivery
Relinquished'. 7`
Daje:
Tin e: R i Date:
pis
Othe,
Reli
Date: �/
C % —7 /
(�/�
Time: Received by:
/6 , /Q Date; Time:
7
Relinquished by:
Date:
(
Time: Received at la b y'
Date: Time:
1.
11

Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
2/19/2014
NPDES#:
WQ0021577
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
2/4/2014
Meritech Work Order # 020414121 Sample: Primary Clarifier Grab 2/4/14
% Total Solids
Ammonia, Nitrogen
46.2 %
< 21.6 mg/kg
2/5/14
2/14/14
0-100 %
21.6
SM2540B
TKN
Nitrate/Nitrite Nitrogen
< 43.3 mg/kg
< 21.6 m lc
2/7/14
2/6/14
mg/kg
43.3 m k
g/ g
EPA 350.1
EPA 351.1
Nitrogen, total
Aluminum, total
< 43.3 mg/kg
2/10/14
21.6 mg/kg
43.3 mg/kg
EPA 353.2
EPA 353.2
Arsenic, total _
2143.3 mg/kg
18.4 mg/kg
2/9/14
2/9/14
5.00 mg/kg
1.00
EPA 200.7
Barium, total
Cadmium, total
934 mg/kg
g/ g
2/9/14
mg/kg
0.500 mg/kg
EPA 200.7'
EPA 200.7
Calcium, total
0.539 m k
16,700 mg/kg
,700
2/9/14
2/9/14
0.200 mg/kg
10.0
EPA 200.7
Chromium, total
Copper, total
mg/kg
g/ g
2/9/14
mg/kg
1.00 mg/kg
EPA 200.7
EPA 200.7
Lead, total
55.4 mg/kg
.2
19.2 m k
2/9/14
2/9/14
1.00 mg/kg
1.00
EPA 200.7
Magnesium, total
Mercury, total
mg/kg
,040
2,0
2/9/14
mg/kg
10.0 mg/kg
EPA 200..7
EPA 200.7
Molybdenum, total -
mg/kg
< 0.543 mg/kg
g/ g
2/7/14
2/9/14
0.02 mg/kg
0.543 mg/kg
EPA 245.1
EPA 200.7
Nickel, total
Phosphorous, total
17.8 mg/kg
543 m
2%9/14
2/9/14
1.00 mg/kg
EPA 200.7
Potassium, total.
7,540 mg/kg
2/9/14
2.00 mg/kg
20.0 mg/kg
EPA 200.7
EPA
Selenium, tutal
Sodium, total
g/kkk g
< 1.09 mg/kg
2/9/14
1.09 mg/kg
200.7
EPA 200.7
Zinc, total
4,540 mg/kg
37.8 mg/ k g
2/9/14
2/9/14
20.0 mg/kg
EPA 200.7
SAR
12.5
2/9/14
- 1.0 mg/kg
_
EPA 200.7
pH
CCE
8.5 S.U.
33.3 %
2/5/14
2/10/14
1.0 - 14.0 S.U. _
SM 45- H B
1
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
- U 1, P.
Laboratory Representative
12
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

ain of Custody Record (COC)
MERI'T'ECH INC.
Environmental Laboratories
iw
A Division of Water Technology and Control, Inc.
642 Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
27320
Email: wtcla b(cb-bells outh. net
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START END
Date Tlme Date =Time
I
Primary Clarifier
n �: /.., /1
0-2 ,%A
Comments:
Aethod of Shipment:
❑ UPS
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
Person Taking Sample (Sign
Comp? # of
//Grryab? Conts.
( rl 1 % Total S
1 Metals -,A
Ni,Ptot.Se
1
re):
Tests Required
ds, pH
T
NPDES #:
Phone: d, ja -.33 "6 -5
Fax: a _ Jw
A
Email: 1I016 �AU,csC lii�� LYlIG6' f�
Project: Send Even Months
PO #:
Turn Around Time*
Std 10 ays) 3 - 5-Day 24 - 48 Hr
O
Lab Use Only
On pH OK?
Ice? �,°j C12 OK?
la,
Mo
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation
] Fed Ex
Will these results be u for regulatory purposes?
Yes No
`RUSH work
Hand Delivery
Reil d by: D Dat . Time:
t z %f� U�3
Recei
]Other
Re q sh d Date: Time:
!$fS'
Received by:
C
Relinquished by: Date: Time;
Received at lab by:
approved prior to submitting samples.
Date:
Date: Time:
n Date: -Tlme:
15 1 13

Meritech, Inc.
Y° Environmental Laboratory
Laboratory Certification No.165
F
Report Date: 3/20/2014
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Send Even Months
Roanoke Rapids, NC 27870 Date Sample Rcvd: 3/4/2014
Meritech Work Order #
Parameters
03041437 Sample: Primary Clarifier Residuals Grab
ResultResult Analysis Date
3/4/14
% Total Solids
48.6 %
3/5/14
Reporting Limit
0-100 %
Method
SM2540B
Ammonia, Nitrogen
20.6 mg/kg
3/6/14
20 mg/kg
EPA 350.1
TKN
170 mg/kg
3/14/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 20.6 mg/kg
3/13/14
20.6 mg/kg
EPA 353.2
Nitrogen, total
170 mg/kg
3/18/14
20 mg/kg
EPA 353.2
Aluminum, total
12,410 mg/kg
3/11/14
5.00 mg/kg
EPA 200.7
Arsenic, total
13.2 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Barium, total
500 mg/kg
3/11/14
0.500 mg/kg
EPA 200.7
Cadmium, total
1.72 mg/kg
3/12/14
0.200 mg/kg
EPA 200.7
Calcium, total
73,470 mg/kg
3/11/14
10.0 mg/kg
EPA 200.7
Chromium, total
14.4 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Copper, total
58.4 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Lead, total
12.1 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Magnesium, total
4,350 mg/kg
3/11/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.134 mg/kg
3/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.510 mg/kg
3/12/14
0.510 mg/kg
EPA 200.7
Nickel, total
Phosphorous, total
15.7 mg/kg
706 mg/kg
3/12/14
3/12/14
1.00 mg/kg
2.00 mg/kg
EPA 200.7
EPA 200.7
Potassium, total
3,350 mg/kg
3/11/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 1.02 mg/kg
3/12/14
1.02 mg/kg
EPA 200.7
Sodium, total
3,530 mg/kg
3/11/14
20.0 mg/kg
EPA 200.7
Zinc, total
153 mg/kg
3/12/14
1.0 mg/kg
EPA 200.7
SAR
4.83
3/19/14
-
-
pH
CCE
8.7 S.U.
3/5/14
1.0 - 14.0 S.U.
SM 4500 H B
27.2 %
3/19/14
1 %
AOAC 955.01
! hereby certify that I have reviewed and approve these data. !(/0"
Laboratory Rep re entative
14
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
MERITECH INC.
Environmental Laboratories
A Division of Water Technology and Control, Inc.
642 Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
27320
Email: wtcfab(�lfsouth net
Web Site: www-meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START END
Date Time Date Time
'rimary Clarifier
-------------
Comments:
lethod of Shipment:
UPS
] Fed Ex
Will these results be used for regulatory purposes?
Yes No
] Hand Delivery
Relinquished b
]Other
Relinquishe /
� �_ `. Date:J lJ1/ ,41
Relinquished by: Date:
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
'erson Taking Satnpie (Signature):
Comp? # of
Grab? Conts. Tests/Required
1 % Total Solids, pH
1 Metals - AI,Ar,Cd,Ca,CU,K,Pb,i
Ni,Ptot,Se,Na,Zn,
1 NH3, TKN,NO2,NO3.
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio
NPDES #: / S
Phone: j S
Fax:
Email: /✓G'�JL, c71�G.5 ,v�iv�1
Project: Send Even Months
PO #:
Tyrn Around Time*
Std (10 ys) 3 - 5 Day 24 - 48 Hr
Lab Use Only
On pH OK?
Ice? C12 OK?
Calcu
*RUSH work must be approved prior to submitting samples.
Time: Received b
7 LI v /Date' Time:
ac V11 �/,-/
Time: Received by:
1--•� Date: Time:
Time: Received a b Da /I
Time:
15

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis Report Date: 4/15/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd: WQ00436
Roanoke Rapids, NC 27870 Project: Send Even Months
Date Sample Rcvd': 4/2/2014
Meritech Work Order #
040214120 Sample: Primary Clarifier Grab
4/2/14
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
49.4 %
4/3/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 20.2 mg/kg
4/3/14
20.2 mg/kg
EPA 350.1
TKN
< 40.5 mg/kg
4/7/14
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 20.2 mg/kg
4/4/14
20.2 mg/kg
EPA 353.2
Nitrogen, total
< 40.5 mg/kg
4/10/14
40.5 mg/kg
EPA 353.2
Aluminum, total
2,145 mg/kg
4/14/14
5.00 mg/kg
EPA 200.7
Arsenic, total
11.7 mg/kg
4/14/14
1.00 mg/kg
EPA 2.00.7
Barium, total
103 mg/kg
4/14/14
0.500 mg/kg
EPA 200.7
Cadmium, total,
1.53 mg/kg
4/14/14
0.200 mg/kg
EPA 200.7
Calcium, total
19,251 mg/kg
4/14/14
10.0 mg/kg
EPA 200.7
Chromium, total
11.7 mg/kg
4/14/14
1.00 mg/kg
EPA 200.7
Copper, total
46.4 mg/kg
4/14/14
1.00 mg/kg
EPA 200.7
Lead, total
10.8 mg/kg
4/14/14
1.00 mg/kg
EPA 200.7
Magnesium, total
858 mg/kg
4/14/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.071 mg/kg
4/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.506 mg/kg
4/14/14
0.506 mg/kg
EPA 200.7
Nickel, total
13.5 mg/kg
4/14/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
844 mg/kg
4/14/14
2.00 mg/kg
EPA 200.7
Potassium, total
1,767 mg/kg
4/14/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 1.01 mg/kg
4/14/14
1.01 mg/kg
EPA 200.7
Sodium, total
2,085 mg/kg
4/14/14
20.0 mg/kg
EPA 200.7
Zinc, total
142 mg/kg
4/14/14
1.0 mg/kg
EPA 200.7
SAR
5.64
pH
CCE
7.8 S.U.
4/4/14
1.0 - 14.0 S.U.
SM 4500 H B
20.0 %
4/7/14
3.60 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.(336]3424522

Chain of Custody Record (COC)
NPDES#:
-
ERY1ECH INC.
Client:
CCJrle ac -f�ci�e,
Environmental Laboratories
Ka stone Paper
Phone:
So?�3
A Division of Water Technology and control, Inc.
Address:
100 Gaston Rd
Fax: cj��
-
642 Tamco Rd
Phone, 1-336-342-4748
Roanoke Rapids, NC
Email: /)/c��.!)�ns
Project:
��%
Send Even Months
Reidsville, NC
Fax: [phone]
27870
Po #:
27320
Email: wtclabo)bellsouth.net
Attention:
Neal Davis �
Turn Around Time*
Web Site: www.meritech-labs.com
std (1 d
3 - 5 Day 24 - 48 Hr
Sample
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
Location/ID #
START END
Comp? #of
Date Time Date Time
Grab? Conts.
Tests Required
pH OK?
Primary Clarifier
Ice? ,) C120K?
Ice?.)
% Total Solids, pH
}
i
1
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,'
Ni,Ptot,Se,Na,Zn-
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation
Comments:
Method of Shipment:
UPS
Fed Ex
Will these results be use or regulatory purposes?
*RUSH
Yes o
work must be approved prior to submitting samples.
r
and Delivery
Relinquished by: Date: /) Time:
- Y� // k
A I
�-I Rec ' d
Date: Time,
❑Other
Relin i e ate:
I7� % IL 2#
Time:
�ssv
Received by:
Date: Time:
Relinquished by; Date:
Time:
Received at labs y:
Date: Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date: 6/5/2014
NPDES#: WQ0021577
WQ0000436.
Project: Send Even Months
Date Sample Rcvd: 5/7/2014
Meritech Work Order tt
050714109 Sample: Primary Clarifier Grab
5/7/14
Parameters
ResResul
Analysis Date
Reporting Limit
Method
% Total Solids
45.7 %
5/7/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 21.9 mg/kg
5/7/14
21.9 mg/kg
EPA 350.1
TKN
330 mg/kg
5/13/14
20 mg/kg
EPA 3$1.1
Nitrate/Nitrite Nitrogen
< 21.9 mg/kg
5/9/14 -
21.9 mg/kg
EPA 353.2
Nitrogen, total
330 mg/kg
5/15/14
20 mg/kg
EPA 353.2
Aluminum, total
7,614 mg/kg
5/9/14
5.00 mg/kg
EPA 200.7
Arsenic, total
4.27 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Barium, total
409 mg/kg
5/9/14
0.500 mg/kg
EPA 200.7
Cadmium, total
2.09 mg/kg
5/9/14
0.200 mg/kg
EPA 200.7
Calcium, total
108,533 mg/kg
5/9/14
10.0 mg/kg
EPA 200.7
Chromium, total
18.9 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Copper, total
84.9 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Lead, total
10.8 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Magnesium, total
4,748 mg/kg
5/9/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.28 mg/kg
5/12/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.547 mg/kg
5/9/14
0.547 mg/kg
EPA 200.7
Nickel, total
18.8 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
1,324 mg/kg
5/9/14
2.00 mg/kg
EPA 200.7
Potassium, total
1,630 mg/kg
5/9/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 1.09 mg/kg
5/9/14
1.09 mg/kg
EPA 200.7
Sodium, total
5,185 mg/kg
5/9/14
20.0 mg/kg.
EPA 200.7
Zinc, total
234 ing/kg
5/9/14
1.0 mg/kg
EPA 200.7
SAR
5.91
6/5/14
-
-
pH
7.8 S.U.
5/15/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
26.9 %
5/13/14
3.60 %
AOAC 955.01
hereby certify that ! have reviewed and approve these data.
6.ke_�'
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Client:
Address:
NPDES #: 7 -
�) �� ` r
!.v 4�
Kapstone Paper Phone: 3r
Fax: ,
100 Gaston Rd Email:
Roanoke Rapids, NC Project: Send Even Months
27870 Po #:
Chain of Custody Record (COC)
ECH INC.
'`tom Environmental Laboratories
t>• ...h
:r A Division of Water Technology and Control, Inc.
•
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320
Email: wtclab(&bellsouth.net
Web Site: www.meritech-labs.com
Attention:
Tu Around Time*
Neal Davis Std (Io ys) 3 - 5 Day 24 - 48 Hr
Sample
Location/ID #
Sampling Dates & Times
START END
Date Time Date Time
o
Person Taking Sample
Comp? #of
Grab? Conts.
(Signature):
Test Required
% Total Solids, pH
Lab Use only
pH OK?
Ice?
Ice? I , Ip C12 OK?
Primary Clarifier
1
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation
C-C-E (by titration)
Comments:
Sodium Adsorption Ratio by Calculation
Oethod of Shipment:
❑ UPS
❑ 7Hand
Will these results bepsCd for regulatory purposes?
Yes No
*RUSH work must be approved prior to submitting samples.
Delivery
❑Other
Relinquished D
Relinquished Date:
te
Time:
33
Jlme:
Received Date: Time:
Received by: Date: Time:
Relinquished by: Date:
Time:
Received hklab by: � Date: Time:
ISM

Meritech, Inc.
Environmental Laboratory
Laboratory Certification 1110.165
e P
Contact: Neal Davis Report Date: 6/23/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ00436
Roanoke Rapids, NC 27870 Project: Send Even Months
Date Sample Rcvd: 6/10/2014
Meritech Work Order # 06101486 Sample: Primary Clarifier Grab 6/10/14
Parameters Resu t Analysis Date Reporting Limit Method
% Total Solids
43.9 %
6/11/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 22.8 mg/kg
6/13/14
22.8 mg/kg
EPA 350.1
TKN
101 mg/kg
6/12/14
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 22.8 mg/kg
6/11/14
22.8 mg/kg
EPA 353.2
Nitrogen, total
101 mg/kg
6/13/14
40.5 mg/kg
EPA 353.2
Aluminum, total
8,861 'mg/kg
6/16/14
5.00 mg/kg
EPA 200.7 ,
Arsenic, total
- 9`.93 mg/kg-.-
6/12/14
` 1.00 mg/kg
EPA 200.7
Barium, total
435 mg/kg
6/16/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.394 mg/kg
6/12/14
0.200 mg/kg
EPA 200.7
Calcium, total
9,066 mg/kg
6/16/14
10.0 mg/kg
EPA 200.7
Chromium', total
8.11 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Copper, total
30.3 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Lead, total
9.64 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Magnesium, total
1,473 mg/kg
6/16/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.068 mg/kg
6/14/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.569 mg/kg
6/12/14
0.569 mg/kg
EPA 200.7
Nickel, total
10.9 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
269 mg/kg
6/12/14
2.00 mg/kg
EPA 200.7
Potassium, total
2,802 mg/kg
6/16/14
20.0. mg/kg
EPA 200.7
Selenium, total
1.16 mg/kg
6/16/14
1.01 mg/kg
EPA 200.7
Sodium, total
4,784 mg/kg
6/16/14
20.0 mg/kg
EPA 200.7
Zinc, total
19.1 mg/kg
6/12/14
1.0 mg/kg -
EPA 200.7
SAR
17.4
6/16/14
-
-
pH
9.4 S.U.
6/11/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
24.0 %
6/13/14
3.60 %
AOAC 955.01
1 hereby certify that 1 have reviewed and approve these data.
Laboratory Repres tative
21
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

L.nain OT L;ustocly Record (COC)
NPDES #: �S `
TEC
MERI H INC
„......z»' .,..•.
'
.
Environmental Laborato
Client:
Kapstone Paper
Phone:
av� - 3 3 —1 S
ries
A Division of Water Technology and Control Inc.
®
Address:
100 Gaston Rd
Fax:
+
Email:
//�� ,,��
NEi�L . zit7ai L.-IY�i�L10EXl�/` ee
642 Tamco Rd
Phone [phone]
Roanoke Ra ids, NC
Project:
Send Even Months
Reidsville, NC
Fax: [phone]
27870
Po #:
Attention:
Neal Davis
Turn Around Time*
27320 Email: [e-mail]
Web Site: www.meritech-labs.com
std
days)
3 - 5 Day
24 - 48 Hr
Sample
Sampling Dates & Times
C�__
Person Taking Sample
(Signature):+
Lab Use Only
Y
Location/ID #
START END
Date Time Date Time
Comp?
Grab?
#of
Conts.
Test Required
on
IceT
pH OK?
C12 OK?
Primary Clarifier
? ��d
bl"
1
% Total Solids, pH
G�
1 Metals -A IAACd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn C C
1 NH3, TKN,NO2,NO3, `
P-A-N by Calculation)
C-C-E (by titration
Sodium Adsorption Ratio (by Calculation)
Aethod of Shipment:
Comments:
] UPS
-]Fed Ex
Hand Delivery
]/�
Other
Will these results
Yes
wused for regulatory purposes?
No
Relinquish , Dat :
7G1W
Ti ;
( O
Relin shed h r( �• _ L
r , �Ti
!
Relinquished by:
Date:
Time:
*RUSH work must be approved prior to submitting samples.
d b � Date: T1 /0 54
red by: Date: Time:
77-
22

Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date:
7/22/2014
NPDES#:
WQ0021577
WQ00436
Project:
Send Even Months
Date Sample Rcvd:
7/8/2014
Meritech Work Order #
07081480 Sample: Primary Clarifier Grab
7/8/14
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
Ammonia, Nitrogen
44.7 %
< 22.4 mg/kg
7/9/14
7/10/14
0-100 %
22.4
SM2540B
TKN
Nitrate/Nitrite Nitrogen
120 m k
g/
< 22.4 mg/kg
7/21/14
7/9/14
m k
g/ g
40.5 mg/kg
EPA 350.1
EPA 351.1
Nitrogen, total
120 mg/kg
g/ g
7/21/14
22.4 mg/kg
40.5 mg/kg
EPA 353.2
EPA
Aluminum, total
7,520 mg/kg
7/16/14
5.00 mg/kg
353.2
EPA 200.7
Arsenic, total
Barium, total
< 1.12 mg/kg
7/16/14
1.12 m
mg/kg g
EPA 200.7
Cadmium, total
436 mg/kg
1.80 mg/kg
7/16/14
7/16/14
0.500 mg/kg
EPA 200.7
Calcium, total
82,800 mg/kg
7/16/14
0.200 m
mg/kg g
10.0 mg/kg
EPA 200.7
EPA
Chromium, total
13.4 mg/kg
7/16/14
1.00 m k
g/ g
200.7
EPA 200.7
Copper, total
Lead, total
65.8 m k
7/16/14
1.00 mg/kg
EPA 200.7
Magnesium, total
10.9 mg/kg
3,620.9 mg/kg
7/16/14
7/16/14
1.00 mg/kg
EPA 200.7
Mercury, total
0.078 mg/kg
7/14/14
10.0 mg/kg
0.02 mg/kg
EPA 200.7
Molybdenum, total
Nickel, total
< 0.078S59 mg/kg
7/16/14
0.559 mg/kg
EPA 245.1
EPA 200.7
Phosphorous, total
13.0 mg/kg
1010 mg/kg
7/16/14
7/16/14
1.00 mg/kg
2.00
EPA 200.7
Potassium, total
Selenium, total
1,91U mg/kg
7/16/14
mg/kg
20.0 mg/kg
EPA 200.7
EPA 200.7
Sodium, total
0.224 mg/kg
5,190 m mg/kg
7/16/14
7/16/14
1.01 mg/kg
20.0
EPA 200.7
Zinc, total
SAR
208 mg/kg
g/ g
7/16/14
mg/kg
1.0 mg/kg
EPA 200.7
EPA 200.7
6.77
7/16/14
_
CC
CC
7.6 S.U.
21.3 %
7/10/14
7/17/14
1.0 - 14.0 S.U.
SM 4500 H B
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data. (,--
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
23

Chain of Custody Record (COC)
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
NPDES.#: 13-7
Phone: d �- _ ��'
+
Fax: 07 -533 ..
Email: n/�,,y,4U►/5���Ty1�
Project: Send Even Months
PO #:
rRIECH INC.
...,.
Environmental Laboratories
\t;tv;
/. ..nP�ti.:.A.y,
A Division of Water Technology and Control Inc.
"n
6.42 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclaWED-bellsouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
Std (lo ays)
3 - 5 Day
o
24 - 48 Hr
0
Sample
Location/ID #
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
START
END
Comp?
Grab?
#ot
Conts,
Tests equired
On
ice?
pH OK?
C12 OK?
Date
Time
Date
Time
Primary Clarifier
'Z[,
1
% Total Solida, pH O1
r
V 1.0
1 I
Metals - AI ,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
c�
Ni,Ptot,Se,Na,Zn yXPM
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Method of Shipment:
Comments:
❑ UPS
❑ Fed E
and Delivery
Other
Will these results be used gulatory purposes?
Yes No
*RUSH work must be approved prior to submitting samples.
Relinquished by- Date: Time:
_ /�� ...
Receive y: Date: Time:
'2.
Relin uis 6y: Date: Time:
f o-n%, e II y�•a,
Received by: Date: Time:
Relinquished by: Date: Time:
ceived a b Date.,Ti * A(
i ` 24

Meritech, Inc.
A� Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:'
NPDES#:
Project:
Date Sample Rcvd:
8/27/2014
WQ0021577
WQ00436
Send Even Months
8/5/2014
Meritech Work Order #
08051485 Sample: Primary Clarifier Grab
8/5/14
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
42.6 %
8/6/14
0-100 %
SM2540B
Ammonia, Nitrogen,
< 23.5 mg/'kg
8/12/14
23.5. mg/kg
EPA 350.1
TKN
198 mg/kg
8/20/14
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 23.5 mg/kg
8/6/14
23.5 mg/kg
EPA 353.2
Nitrogen, total
198 mg/kg
8/20/14
40.5 mg/kg
EPA 353.2
Aluminum, total
5,210 mg/kg
8/18/14
5.00. mg/kg
EPA 200.7
Arsenic, total
< 1.17 mg/kg
8/18/14
1.17 mg/kg
EPA.200.7
Barium, total
413 mg/kg
8/18/14
0.500 mg/kg
EPA 200.7
Cadmium, total
1.25 mg/kg
8/18/14
0.200 mg/kg
EPA 200.7
Calcium, total
6,550 mg/kg
8/18/14
10.0 mg/kg
EPA 200.7
Chromium, total
13.9 mg/kg
8/18/14
1.00 mg/kg
EPA 200.7
Copper, total
200 mg/kg
8/18/14,
1.00 mg/kg
EPA 200.7
Lead, total
7.80 mg/kg
8/18/14
1.00 mg/kg
EPA 200.7
Magnesium, total
2,790 mg/kg
8/18/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.070 mg/kg
8/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.587 mg/kg
8/18/14
0.587 mg/kg
EPA 200.7
Nickel, total
64.6 mg/kg '
8/18/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
770 mg/kg
8/18/14
2.00. mg/kg
EPA 200.7
Potassium, total
1,070 mg/lcg
8/18/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 1.17 mg/kg
8/18/14
1.17 mg/kg
EPA 200.7
Sodium, total
5,400 mg/kg
8/18/14
20.0 mg/kg
EPA 200.7
Zinc, total
149 mg/kg -
8/18/14
1.0 mg/kg ,
EPA 200.7
SARI
19.9
8/18/14
-
-
pH
7.4 S.U.
8/6/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE.
21.1 %
8/7/14
1 %
AOAC 955.01
1 hereby certify that 1 have reviewed and approve these data. t}
94--
Laboratory Representative
25
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone] - -

Chain of Custody Record (COC)
NPDES #:
Environmental Laboratories
A Division of Water Technology and Control, Inc.
642- Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
27320
Email: wtclab(a)bellsouth.net
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START
END
Date
Time
Date
Time
mary Clarifier
Comments:
Viethod of Shipment:
El UPS
Will these results be
❑ Fed Ex Yes (/
Relinquis
and Delivery ,'-/,
Reli UT d b
❑Other
Relinquished by:
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
Person Taking Sample (Signature): ? ,.
Comp? T sts Required
Grab? Contonts,
1 % Total Solids, p
1 _ Metals - AI,Ar,Cd,Ca,Cu,K,Pb,I
Ni,Ptot.Se Na_Zn / 2"", a
1 ' INH3, TKN,NO2.NO3
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio
Phone:
Fax:
Email:
Project:
PO #:
Std (1 Si
MID
Send Even Months
Turn Around Time*
ays) 3 - 5 Day 24 - 48 Hr
Lab Use Only
On pH OK?
Ice? C12 OK?
Calculation
for regulatory purposes?
No *RUSH work must be approved prior to submitting samples.
ce
Dat Time: Reiv by:
I / / " / j� / Date: Time: p
vf� 6� .. �• Vic+ Z✓
ate: Time: Received by:
v., (5 `� �. -�Date: Time:,
Date: Time: R�ee ved at I y: � te;
M1 j t_/ Tl�e: &
I

Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
9/12/2014
NPDES#:
WQ0021577
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
9/2/2014
Meritech Work Order #
09021441
Sample: Primary Clarifier Grab
9/2/14
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
45.8 %
9/3/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 21.8 mg/kg
9/4/14
21.8 mg/kg
EPA 350.1
TKN
47.7 mg/kg
9/5/14
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 21.8 mg/kg
9/3/14
21.8 mg/kg
EPA 353.2
Nitrogen, total
47.7 mg/kg
9/10/14
20 mg/kg
EPA 353.2
Aluminum, total
7,270 mg/kg
9/8/14
5.00 mg/kg
EPA 200.7
Arsenic, total
13.2 mg/kg
9/8/14
1.17 mg/kg
EPA 200.7
Barium, total
439 mg/kg
9/8/14
0.500 mg/kg
EPA 200.7
Cadmium, total
2.18 mg/kg
9/8/14
0.200 mg/kg
EPA 200.7
Calcium, total
8,730 mg/kg
9/8/14
10.0 mg/kg
EPA 200.7
Chromium, total
16.8 mg/kg
9/8/14
1.00 mg/kg
EPA 200.7
Copper, total
62.7 mg/kg
9/8/14
1.00 mg/kg
EPA 200.7
Lead, total
11.0 mg/kg
9/8/14
1.00 mg/kg
EPA 200.7
Magnesium, total
3,930 mg/kg
9/8/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.066 mg/kg
9/4/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.546 mg/kg
9/8/14
0.546 mg/kg
EPA 200.7
Nickel, total
16.4 mg/kg
9/8/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
1,120 mg/kg
9/8/14
2.00 mg/kg
EPA 200.7
Potassium, total
1,690 mg/kg
9/8/14
20.0 mg/kg
EPA 200.7
Selenium, total
2.53 mg/kg
9/8/14
1.17 mg/kg
EPA 200.7
Sodium, total
2,790 mg/kg
9/8/14
20.0 mg/kg
EPA 200.7
Zinc, total
189 mg/kg
9/8/14
1.0 mg/kg
EPA 200.7
SAR
8.80
9/8/14
-
-
pH
8.7 S.U.
9/3/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
28.6 %
9/8/14
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data. A(. c
Laboratory Representative
27
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
:
ERITECH INC.
.:
Environmental Laboratories
A Division of Water Technology and Control, Inc.
642 Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
27320
Email: wtclab(a-)bellsouth.net
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START END
Date
Time
Date
Time
mart' Clarifier
0 /� /V
4 ram^
Comments_ :
Method of Shipment:
El UPS
Will these results be
0 Fed Ex Yes
Relinqui d by:
and Delivery
Reli lshed by:
nOti.,er �ti
by:
for
Date:
E
Date:
Date:
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
Person Taking Sample (Signature):
Comp? # of Tests
Grab? Conts.
1 % Total Solids, pH
1 Metals - Al, ;C�C
N ,Ptot St Na.2
1 JNH3, TKN,NO2,N
I Ime•
Time:
NPDES #: el
074 77
Phone: as S3 9S
Fax:
Email: 1)rbK.,�.4llls � ��s22-
Project: Send Even Months
PO #:
Turn Around Time*
Std (10 days) 3 - 5 Day 24 - 48 Hr
Lab Use Only
wired on pH OK?
Ice? C12 OK?
�11 1:G
P-A-N (by Calculation)
C-C-E�(by titration)
Sodium Adsorption Ratio (bv Calc
*RUSH work must be approved prior to submitting samples
6d by: f/ Dat : Time:
ed by: Date: Time:
D5te: lrge�

Meritech, Inc.
Environmental Laboratory
' Laboratory Certification No. 165
P
i!
Contact: Neal Davis
Client: l<apstone Paper &Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Revised Date:
Report Date:
NPDES#:
Project:
Date Sample Rcvd:
1012912014
10/27/2014
WQ0021577
WQ0000436
Monthly
10/14/2014
Meritech Work Order #
101414138 Sample: Primary Clarifier Residuals Grab
10/14/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
50.3 %
10/15/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 19.9 mg/kg
10/21/14
19.9 mg/kg
EPA 350.1
TKN
288 mg/kg
10/20/14
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 19.9 mg/kg
10/16/14
19.9 mg/kg
EPA 353.2
Nitrogen, total
288 mg/kg
10/23/14
20 mg/kg
EPA 353.2
Aluminum, total
2,700 mg/kg
10/21/14
5.00 mg/kg
EPA 200.7
Arsenic, total
< 0.994 mg/kg
10/21/14
0.994 mg/kg
EPA 200.7
Barium, total
233 mg/kg
10/21/14
0.500 mg/kg
EPA 200.7
Cadmium, total
3.22 mg/kg
10/21/14
0.200 mg/kg
EPA 200.7
Calcium, total
134,000 mg/kg
10/21/14
10.0 mg/kg
EPA 200.7
Chromium, total
20.3 mg/kg
10/21/14
1.00 mg/kg
EPA 200.7
Copper, total
21.7 mg/kg
10/21/14
1.00 mg/kg
EPA 200.7
Lead, total
8.39 mg/kg
10/21/14
1.00 mg/kg
EPA 200.7
Magnesium, total
2,270 mg/kg
10/21/14
10.0 mg/kg
EPA 200.7
Mercury, total
< 0.020 mg/kg
10117114
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.497 mg/kg
10/21/14
0.497 mg/kg
EPA 200.7
Nickel, total
16.7 mg/kg
10/21/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
1,130 mg/kg
10/21/14
2.00 mg/kg
EPA 200.7
Potassium, total
513 mg/kg
10/21/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 0.994 mg/kg
10/21/14
0.994 mg/kg
EPA 200.7
Sodium, total
2,470 mg/kg
10/21/14
20.0 mg/kg
EPA 200.7
Zinc, total
100 mg/kg
10/21/14
1.0 mg/kg
EPA 200.7
SAR
2.59
10/21/14
-
-
PH
8.7 S.U.
10/15/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
42.5 %
10/20/14
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data. 6 &4�2
Laboratory Representative
29
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-21)-p13 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577'
5 f�I���, INC, Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
u 4 ' V/ 1 '' Road Addre 100 Gaston R
_ Fax: [phone] • I
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC. Email:_ Neal. Davis(@ Kapstonepaper. c,
d 642 Tamco Rd. Phone: [phone] , 27870
Project:_ Monthly I
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
www.meritech-labs.com' $id 1 .3-5 DJ z4.48►,�=
Circle all that apply: Email (preferred) , Fax, ail
Person Taking Sample (Sign/Print):` Sampling Dates &Times Lab USE
Sample Location and/or ID # Start ✓
End Comp?
Date Time Date Time Grab? #of Cont. est(s) Required on Ice? pH OK?
e No Cl OK?
PRIMARY CL�A:RIF�IERRES�JDUALS /cf q.a p �,� %TOT SOLIDS Ph
Method Of *** Dechlorination <
Comments: ��1C� Woo
1V o
9
C UPS
Fed Ex Are these results for
Hand Delivery Relinquishediby:
Other Relinquished
Relinquished
Metals: A , , Ca, C'u, , M ;, o, i, 3e, Na
Chromiu3n, Barium, um, P _ot, NHS, TK , NOZ, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
m) of Ammonia, Cyanide, Phenol and TKN Sam les must be done in the field prior to reservation. *** G R
I- Lr c VN Odds I ��Z�� Compositor #
latory purposes? Ye Jug #
Report results in: g/� �: mg/ ug/L [
Date: Time:N
Rc11 e' by:i — (0 Da TimIOZ 5—
Time:�� :�G Received by: ate:Time:
Date: Time:R ed by .
[o - I T1el `f 141rntf T`
30

Meritech, Inc.
Environmental Laboratory
Jam' Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper
& Packaging
Report Date:
11/18/2014
100 Gaston Rd.
NPDES#:
WQ0021577
Roanoke Rapids,
NC 27870
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
11/4/2014
Meritech Work Order #
110414103 Sample:
Primary Clarifier Residuals Grab
11/4/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
Ammonia, Nitrogen
44.1 %
22.7
11/5/14
0-100 %
SM2540B
< mg/kg
11/10/14
22.7 mg/kg
EPA 350.1
Nitrate/Nitrite Nitrogen
150 mg/kg
< 22.7 mg/kg
11/17/14
11/5/14
40.5 mg/kg
22.7
EPA 351.1
Nitrogen, total
150 mg/kg
11/17/14
mg/kg
20 mg/kg
EPA 353.2
EPA 353.2
Aluminum, total
7,800 mg/kg
11/12/14
5.00 mg/kg
EPA 200.7
-Arsenic, total
Barium, total
2.95 mg/kg
11/12/14
0.994 m k
g/ g
EPA 200.7
Cadmium, total
376 mg/kg
1.47 mg/kg
11/12/14
11/12/14
0.500' mg/kg
EPA 200.7
Calcium, total �
90,700 mg/kg
11/12/14
0.200 m
mg/kg g
10.0 mg/kg
EPA 200.7
EPA
Chromium, total
0.254 mg/kg
11/12/14
0.100 m k
g/ g
200.7
EPA 200.7
Copper, total
Lead, total
1.21 mg/kg
11/12/14
1.00 mg/kg
EPA 200.7
Magnesium, total
11.6 mg/kg
4130 m k
g/ g
11/12/14
11/12/14
1.00 m k
g/ g
10.0
EPA 200.7
Mercury, total
0.045 mg/kg
11/11/14
mg/kg
0.02 mg/kg
EPA 200.7
EPA 245.1
Molybdenum, total
Nickel, total
< 0.567 mg/kg
11/12/14
0.567 m k
g/ g
EPA 200.7
Phosphorous, total
15.1 mg/kg
916 mg/kg
11/12/14
11/12/14
1.00 mg/kg
2.00
EPA 200.7
Potassium, total
1,260 mg/kg
11/12/14
m k
g/ g
20.0 mg/kg
EPA 200.7
EPA 200.7
Selenium, total
Sodium, total
< 1.13 mg/kg
11/12/14
1.13 m k
g/ g
EPA 200.7
Zinc, total
4,970 mg/kg
11/12/14
20.0 mg/kg
EPA 200.7
SAR
183 mg/kg
11/12/14
1.0 m k
g/ g
EPA 200.7
6.19
11/12/14
-
pH
CCE
7.4 S.U.
11/10/14
1.0 - 14.0 S.U.
SM 4500 H B
30.4 %
11/17/14
1 %
AOAC 955.01
I hereby certify that ! have reviewed and approve these data.
Laboratory Represeritative
31
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES #:
..°` ERITE CH
INC.
-,
Client: Kapstone Pa erEnvironmental Laboratories Phone:d,ld-533 -G ,a�y_�
TS.`. A Division of Water Technology Fax:
gy and Control, Inc. Address: 100 Gaston Rd
Email: /I��`-.�1,1�4G%sue✓ �k�.7r��?��L:2
Roanoke Ra ids, NC Project: Send Even Months
642 Tamco Rd Phone [phone] Reidsville, NC Fax: [phone] 27870 PO #:
27320 Email: wtclab(a)bellsouth net Turn Around Time*
Attention: Neal Davis Std (Q days) 3 - 5 Day 24 - 48 Hr
Web Site: www:meritech-labs.com
O
Sample Sampling Dates & Times l
Person Taking Sample (Signature): ; Lab Use Only
Location/ID # START END Comp? #of
Date Tlme Date Time Grab? Conts. Tests Required On .� pH OK?
Wmo
C12 OK?
Primary Clarifier /� f •
,/� rt 1 % Total olids, ply1 Metals - AiI,rG*aC%I,K�PN ;Pto�Se;AiaZn
1 NH3, TKN,Ng2,N0",
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio by Calculation)
Comments:
Method of Shipment:
❑ UPS
Will these results sed for regulatory purposes?
❑ Fed Ex Yes No *RUSH work must be approved prior to submitting samples.
RelingLf�fletl y: Dat Time; Rec ed b ���tttDat Time:
Hand Delivery v,/� _
Reliti 7 /
Date: , /� a Received by: Date: Time:
❑(ether � Y /� - •
Rellnquished by: Date: Time: Received at lab I
:
y Date: Time:
t "k m i �J 132

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
v._
Contact: Neal Davis
Client: Kapstone Paper
& Packaging
Report Date:
12/23/2014
100 Gaston Rd.
NPDES#:
WQ0021577
Roanoke Rapids,
NC 27870
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
12/9/2014
Meritech Work Order #
12091495 Sample: Primary Clarifier Residuals Grab
Parameters
12/9/14
Results
Analysis Date
Reporting Limit
Method
Total Solids
Ammonia, Nitrogen
37.3
< 26.8 m k
mg/kg
12/15/14
12
0-100 %
SM2540B
TKN
456 mg/kg
/15/14
/14
26.8 mg/kg
EPA 350.1
Nitrate/Nitrite Nitrogen
Nitrogen,
515 mg/kg
12/1114
40.5 mg/kg
EPA 351.1
total
1
97mg/kg
12/16/14
/ /
22.7 mg/kg
EPA 353.2
Aluminum, total
9,84m
mg/kg g
12/11/14
20 mg/kg
EPA 353.2
Arsenic, total
6.9.9
. 4 m
12/11/14
5.00 mg/kg
EPA 200.7
Barium, total
678 mg/kg
12/11/14
0.994 mg/kg
EPA 200.7
Cadmium, total
.39 mg/kg
12/11/14
0.500 mg/kg
EPA 200.7
Calcium, total
75,900 g/kg
mg/kg
12/11/14
0.200 mg/kg
EPA 200.7
Chromium, total
m 27.1 k
12/11/14
10.0 mg/kg
EPA 200.7
Copper, total
63.mg/kg
g/ g
12/11/14
0.100 mg/kg
EPA 200.7
Lead, total
15.1 mg/kg
12/11/14
1.00 mg/kg
EPA 200.7
Magnesium, total
3,080 m
mg/kg 1;
12/11/14
1.00 m k
g/ g .
EPA 200.7
Mercury, total �
0.040 mg/kg
12/12/14
10.0 mg/kg
EPA 200.7
Molybdenum, total
< 0.670 m k
g/ g
12/11/14
0.02 m k
g/ g
EPA 245.1
Nickel, total
24.1 m
mg/kg g
12/11/14
0.670 mg/kg
EPA 200.7
Phosphorous, total
1,340 mg/kg
12/11/14
1.00 mg/kg
EPA 200.7
Potassium, total
2,820 m k
g/ g
12/11/14
2.00 m k
g/ g
EPA 200.7
Selenium, total
2.92 mg/kg
12/11/14
20.0 mg/kg
EPA 200.7
Sodium, total
3,380 m
mg/kg
g
12/11/14
113 k
g/ g
.m20.0
EPA 200.7
Zinc, total
158 m lc
g/ g
12/11/14
mg/kg
EPA 200.7
SAR
�
4.62
12/11/14
1.0 mg/kg
EPA 200.7
p H
CCE
7.5 S.U.
25.1 %
12/15/14
1.0 - 14.0 S.U.
_
SM 4500 H B
12/16/14
1 % AOAC 955.01
' hereby certify that ! have reviewed and approve these data.
-O-Z& - � ��7
Laboratory Representative
33
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC
MEHITECH INC>ti
m?..
Environmental Laboratories
<';���`'w •
A Division of Water Technology
gy and Control, Inc.
642 Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
27320
Email: wtclab(cilbellsouth net
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START END
Date Time Date Time
'rimary Clarifier
Comments:
�thod of Shipment:
J UPS
WZK
y purposes?
Fed Ex Date:Hand DeliveryDate:
Other.
Z r lei
Relinquished by: Date:
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
Comp? # or
Grab? conts_ Tests Required
1 % Total Solids, H
1 Metals -Al. Cd,Ca,Cu,K,I?b,f
r�
J3
Ni;Ptot;Se,Na,Zn
1 loll-r3, TKN.1\1 2,NO3,
P-A-N •(by Calculai
C-C-E (by titration
Sodium Aasorptio
Phone: ) r, S .
Fax: Asa? -33
Email:
Project: Send Even Months
Po #:
Turn Around Time*
Std (10 da ) 3 - 5 Day 24 - 48 Hr
C7
Lab Use only
On pH OK?
Ice? C12 OK?
1,Hg,Mo;
Ratio (by Calculati
*RUSH work must be approved prior to submitting samples.
Time: Recei y:
Date: Time:
Tim ' Received by:
Date: Time:
Time: J R eived ab
' te: Time,
34

S£
slanpIsay aaif!aaI3 Aavuqad srsApau y 5qi1dwDs
d7.71

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging Report Date: 12/29/2014
100 Gaston Rd NPDES#: WQ0000436
Roanoke Rapids, NC 27870 WQ0021577
Date Sample Rcvd: 12/9/2014
Meritech Work Order # 12091498 Sample: Primary Clarifier Residuals Mollection Date: 12/9/14
13 11 - TCLP Metals
Parameter
Results
Analysis
Det. Limit Reg. Limit Metho
Arsenic
Barium
< 0.100 mg/L
12/17/14
0.100 5.0
EPA 200.7
Cadmium
1.95 m L
g/
< 0.020 mg/L
12/17/14
12/17/14
0.050 100.0
0.020
EPA 200.7
Chromium
Lead
< 0.050 m L
g/
12/17/14
1.0
0.050 5.0
EPA 200.7
EPA 200.7
Mercury
0.145 mg/L
< 0.02 mg/L
12/17/14
12/16/14
0.100 5.0
0.02
EPA 200.7
Selenium �
Silver
< 0.100 m g/ L
12/17/14
0•2
0.100 1.0
EPA 245.1
EPA 200.7
< 0.050 mg/L
12/17/14
0.050 5.0
EPA 200.7
TCLP Organics
Parameter
R 9 LU-1 s
Anal, sis
-
M ttho
Volatiles 8260
Attached
12/12/14
Semi Vol. 8270
Attached
12/15/14
8260
Ignitability
> 140 °F
12/10/14
8270
pH
8.5 S.U.
12/10/14
-
1.0 - 14.0 S.U.
EPA 1030
SM 4500 HB
Other Tests
Parameter
R—u1t
Ana is
Deporting Limit
Method
Sulfide, total
Cyanide, total
< 10 mg/kg
< O.S m k
g/
12/1.0/14
10 m k
g/ g
SM 4500 SD
g
12/15/14
0.5 mg/kg
EPA 335.4
36
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Neal Davis
Client: Kapstone Paper& Packaging
100 Gaston Rd
Roanoke Rapids, NC 27870
Meritech Work Order # 12091497
Meritech, Inc..
Environmental Laboratory
'Laboratory Certification No. 165
Sample: Fly Ash
Report Date: 12/29/2014
NPDES#: WQ0000436
WQ0021577
Date Sample Rcvd: 12/9/2014
Collection Date: 12/9/14
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8O81A
Analyst: Summit
Analysis Date: 12/19/14
Parameter
Results
Det. Limit
Reg. Limit
Dilution Factor
Heptachlor Epoxide
< 0.002 mg/L
0.002
0.008
1
Endrin
< 0.002 mg/L
0.002
0.02 .
1
Chlordane
< 0.01 mg/L
-0.01
0.03
1
Toxaphene
< 0.1 mg/L
0.1
0.5
1
'Methoxychlor
< 0.002 mg/L
0.002
10.0
1
Heptachlor
< 0.002 mg/L
0.002
0.008
1
Lindane Gamma - BHC
< 0.002 mg/L
0.002
0.4
1
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Analyst: Summit
Results Det. Limit
Analysis Date: 12/18/14
Reg. LimitDilution Factor
5.0 mg/L 5.0 10.0
< 0.5 mg/L 0.5 1.0
1
1
I hereby certify that I have reviewed and approve these data. (�
Laboratory Representative
37
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone] -

MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
Client: Kapstone Kraft Paper Corp.
Project: TCLP
Client Sample ID: Primary Clarifier Residuals
Sample Collection: 12/09/14
Meritech Sample DD: 12091498
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 12/12/14 Extracted: 12/10/14
Analyst: VWV
Parameter Result Units Det. Limit Ree. Limit Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
I00
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1, 1 -Diehl oroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
<0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Extraction: 12/15/14
Analysis: 12/20/14 Analyst: PM
Parameter
Result
Units
Det. Limit
Ree. Limit Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5 10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13 10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5 10
Hexachloroethane
<0.100
mg/L
0.100
3.00 10
o-cresol
<0.100
mg/L
0.100
200 10
m&p-cresol
<0.200
mg/L
0.200
200 10
Total cresols
<0.300
mg/L
0.300
200 10
Nitrobenzene
<0.100
mg/L
0.100
2.00 10
Pentachlorophenol
<0.500
mg/L
0.500
100 10
Pyridine
<0.100
mg/L
0.100
5.0 10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400 10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2:00 10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13 10
I hereby certify that Iltave
reviewed and approve these
data.
Laboratory Representative
38
642 Tamco Road " Reidsville, NC 27320
[phone]
Ph *
[phone] Fax

PD `3
Chain of Custody Record (COC)
Client:'- IMF'MERITECH,
INC.
Address:�o ����R�^
FE
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
�,
Reidsville NC 270320 Fax: [phone]
P.O.#:
Turn Around Time*
Email: [e-mail]
Attention: .cr,o��
�
S •RUSH work needs prior approval.
How would you like your report sent?
3 S Oa s
www
y�
-I a b s . c O I 1 1
Circle all that apply:
Std lad -
Email (preferred), Fax, ail
.meritech
PersonTakin S pie(Sig rin
Lab UsSampling
R
Dates & TimesSample
Location and/or.lD # Start End
Comp? Hof Tests) Required
On ice?
/ No
Date Time Date Time
Grab? Cont.
0
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroed=e (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1, l-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5) Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (imd its hydroxide) (0.008)
Toxaphene (0.5)
Chloroform (6.0)
7iexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5 Trichlorophenol (400.0
m-Cresol (200.0)
Lead (5.0)
2,4,6-Tri-chlorophenol (2.0)
o-Cresol (200.0),
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-13 (10.0)
Methyl ethyl ketone (200.0)
Method of
Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Ph
--
Compositor #
Comments:
Shipment:
Jug #
❑.. UPS
ed Ex
Are these results for regulatory purposes? Yes
No
'Report results in: mg/L
mg/kg ug/L
L
Relinquished by: Date:
Time: r; ��f Re y:
Iv
Date �' / Time: d ° a
7
W Hand Delivery
C1 Other
Date Ti e: Received by:
"qu /Z-/�' /6l
Date: Time:
Relinquished�by-
Time: ceiv
39Date:

Form PVRF 02T
Primary Clarifier Residuals
Annual Pathogen Reduction Form
LUO

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
4
Facility Name: Kapstone Kraft Paper Corporation
WWTP Name: Roanoke Rapids Mill
Monitoring Period: From 1/1/2014 To
WQ Permit Number:
NPDES Number:
12/31/2014
WQ 0021577
NC 0000752
Pathogen Reduction (15A NCAC 02T :1106) - Please indicate level achieved and alternative performed:
Class A.
Alt. A (time/temp) Q
Alt B (Alk Treatment)Q
Alt. C (Prior Testing) v...........
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost El
Heat Drying El
Heat Treatment 0
Thermophilic
Beta Ray
Gamma RayPasteurization
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization L3
Air Drying 13
Composting 0 jAerobic
Digestion
bic Di i n
Anaero Digestion
g
.................................................. ........
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
18.9
294
mpn/g
0
Annual
Fecal
sm9221ce
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) E3
Alt. 2 (40-day bench) L3
Alt. 3 (30-day bench)
Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) L3
Alt. 6 (Alk. Stabilization L3
Alt 7 (Drying - Stable) E3
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 21
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Neal R. Davis Environmental Engineer None Applied
Preparer Name and Ti e ( e rint) Land Applier Name and Title (if applicable)(type or print)
Signature o Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
41
DENR FORM PVRF 02T (12/2006)

r- yt ..,
aceAnalytical-"
- xwW.pecoleba�
November 24, 2014
Neal Davis
Kapstone Kraft Paper Corp.
100 Gaston Road
Roanoke Rapids, NC 27870
RE: Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Dear Neal Davis:
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2014.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�t cam•.-- Cc� � ��-
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
42

r �
acmnalytical o
W"..pacelabs.cam
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification M 67
CERTIFICATIONS
North Carolina Bloassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Pace Analytical Services, Inc.
6101 Conference Drive
Raleigh, NC 27607
(919)8344984
Charlotte Certificatlon IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
Fiodda/NELAP Certification #: E87627
North Carolina Field Services Certification M 5342
Kentucky LIST Certification #: 84
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
EW

aceAnalytical
' wwwpocelebacw
I
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Lab ID Sample ID
92226108001 PCR-1-14
92226108002 PCR-2-14
92226108003 PCR-3-14
92226108004 PCR-4-14
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
'3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.. 44

aceAnalytical'
wawwpecelabs.core
PROJECT NARRATIVE
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Method: SM9221C E (MPN) 503
Description: 92210E Fecal Coliform, MPN RAL
Client: Kapstone Kraft Paper Corp.
Date: November 24, 2014
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
General Information:
4 samples were analyzed for SM9221C E (MPN) 503. All samples were received in acceptable condition with any exceptions noted
below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit In the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
- - - 45

aceAnalyfical
wwwpacWabs.cm
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Sample: PCR-1-14
Lab ID: 92226108001 Collected: 11/18/14 08:00
Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM 02974-87
Percent Moisture
59.1 % 0.10 1
11/21/14 13:27
92210E Fecal Coliform, MPN RAIL
Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN
98.3 MPN/g 0.018 1
11/18/14 16:42
Date: 11/24/2014 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
46

aceAnalytical
www.pacslaf)soom
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: PCR-2-14 Lab ID: 92226108002 Collected: 11/18/14 08:10 Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 57.8 % 0.10 1 11/21/14 13:27
92210E Fecal Conform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 178 MPN/g 0.018 1 11/18/14 16:42
Date: 11/24/2014 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
47

i''
aceAnalytical
wwvw.pec�absoom
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: PCR-3-14 Lab ID: 92226108003 Collected: 11/18/14 08:20 Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS'No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 59.9 % 0.10 1 11/21/14 13:27
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 294 MPN/g 0.018 1 11/18/14 16:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/24/2014 04:51 PM without the written consent of Pace Analytical Services, Inc.. 48

acmnalytical
www.pacelaucom
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: PCR-4-14 Lab ID: 92226108004 Collected: 11/18/14 08:30 Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry-welght" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 59.4 % 0.10 1 11/21/14 13:27
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 186 MPN/g 0.018 1 11/18/14 16:42
Date: 11/24/2014 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
49

aceAnalytical
wwwpacelaucam
QUALITY CONTROL DATA
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
QC Batch: PMST/7259 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92226108001, 92226108002, 92226108003, 92226108004
SAMPLE DUPLICATE: 1334662
92226286001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.0 16.0 0
SAMPLE DUPLICATE: 1334663
92226299002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.2 15.7 3
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/24/2014 04:51 PM without the written consent of Pace Analytical Services, Inc..
50

a
aceAnalytical
agvlrpatxleba.com
QUALITY CONTROL DATA
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
QC Batch: RBIO/4578 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92226108001, 92226108002, 92226108003, 92226108004
METHOD BLANK: 1335600 Matrix: Solid
Associated Lab Samples: 92226108001, 92226108002, 92226108003, 92226108004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND - 0.018 11/18/14 16:42
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE DUPLICATE: 1335601
922261,08002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 178 178 0
Results presented on this page are In the unite Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/24/2014 04:51 'PM without the written consent of Pace Analytical Services, Inc..
---- 54

.j
r' Pace Analytical Services, Inc.
acmnalytical a 6701 Conference Drive
wwwpacele6,tcom
Raleigh, NC 27607
(919)834A984
QUALIFIERS
Project: CLARIFIER SFEC_ AL
Pace Project No.: 92226108
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/24/2014 04:51 PM without the written consent of Pace Analytical Services, Inc..
- -- - 52

P
Y
aceAnalytical'
ww»:pacelaDacom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CLARIFIER SFECAL
Pace Project No.: 92226108
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92226108001
PCR-1-14
ASTM D2974-87
PMST/7259
92226108002
PCR-2-14
ASTM D2974-87
PMST/7259
92226108003
PCR-3-14
ASTM D2974-87
PMST/7259
92226108004
PCR-4-14
ASTM D2974-87
PMST/7259
92226108001
PCR-1-14
SM9221C E (MPN) 503
R610/4578
92226108002
PCR-2-14
SM9221C E (MPN) 503
R1310/4578
92226108003
PCR-3-14
SM9221C E (MPN) 503
R1310/4578
92226108004
PCR-4-14
SM9221C E (MPN) 503
R1310/4578
Date: 11/24/2014 04:51 PM
REPORT OF .LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..

Document Name: Sample Condition Upon
Document Revised: April 04, 2013
f aCeAnal�t;Cal
Rocel t SCUR
Pa a 'l of 2
Document No,:
Issuing Authorities:.
...r
f
F-RAL CS-001.rev,02
`Pace Asheville Quality Office
Client Name: 17 ,t �
Where Received: [] Hunters011e Asheville Eden Raleigh -
Courier (Circle): • Fad Ex UPS USPS Client Commercial Pa Other
Custody Seal on Cooler/Box Present: yes 3 no Seals Inject:Z you [] no
Packing Material: Ej Bubble Wrap 1?hli�,a�s 0 None Other
ip
Circle 'thermometer Used: iR Gun S �12208638 of ice: et etua None �] Samples on ice, ocoling process has begun
to nun Rack r Ins 2066374
Tom Correction Raotori Add Subtract
Date and InVals of person examining
Corrected Cool01'Tomp,: C
Biological Tissue Is Frozen: Yes N/A
o nt a Pros rv�ti t
sh
Temp should be above freezing to 664
Comments:
Chain of Custody Present:
OYes ON, • OWA
t -
Chain of Custod •Filled Out:
Eives ON*
OwA
2. '
Chain of Custod • Relinquished,'
vcs ON,
Owa•
3.
Sam ler Name $ Signature on COC:
e6wo ON.
OwA
4,
Samples les Arrived within Hold Time:
16yes I ONo
OwA
ti, -
Short Hold Time Anal sis' 42hr ;
Yes ONo
17wA
Rush Turn Around Time Requested.
OYee Nb
ONIA
7:
Sufficient volume:
Aft 17No
ON/A
8.
Correct Containers Used:
Yw ONo
MA
9.
•Pace "Containers Used:
Yea ONo
OWA
Containers. Intact
OYes dNo
ONIA
10, '
Filtered volume • received for Dissolved testa
Oyes ONo
ONIA
11.
Sample Labels match COO:
[ Yes quo
OWA
12.
-Includes date/ilme/ID/Anal sis Matfhc
AI containers neadbtp•preservatlon have been checked,
i]7Yo5 ONo
CINlA
13.
All contalners needing preservation are found to be In
(p�Yes ONo
OwA
compllanw. with EPA recommendation..
r
;�
exception: VON Qd1form, M 03G, wbDRO tar .
Yee ONo
r
Samples checked fordechlodnatlon:
byes ONo
MA
14,
Heads ace In VOA Vials >6mm :
OYes ONo
OQWA
16,
Trip Blank Present:
OYe's ONo
WA
18,
Trip Blank Custody Seats Present
Oyes ONo
wA
Pace Trip Blank Lot # If urchased :
Client Notlflcationli Resolution: Meld Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF /SRF Da
L
ta:
Review:: t. C 1-
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Caroline DEHNR
CertiHcadon Office (i,a out of hold, incorrect preservative, out of temp,
Incorreot containers)
�z�r9.22261 Q8
1111
II I�I..". i•A.. - .

Chain of Cust
Report Results to: Bill Results to:
KaPstone Paper
100 Gaston Rd
Roanoke Rapids. NC
ATTN: Neal Davis Ate:
Phone: [phone]
[a Standard Report Delivery
❑ Rush Report Delivery (w/ surcharge)
Requested Due Date:
Project Reference: Clarifier fecW AnaWm-Nov. 2014
Purchase Order lt:
Sampled By:
�ampleDescription
Composite
orGrab
Start date
Stop Date
ww.ow.
Sw.Gw.etc
aof t
conp;nns
r
- ;, 11poyslsRequested,
SYartTime
Stopiitne
2
_fecal
2
/f
feral sludge. %.moisttire
- 3 - %
/�
C]
yy zo
/ - A!
2
/i fecal sludge �� e.?f
fecal sludge, 9�fi u p'
2
2Jea4zkWse. %vmesaure
Z
Zetaq�islied M siQnaWre)
Daft rme
A �re- For Lab Use Only
nQed pt {rd
iA 1�� n•Z� Temperature at receipt:
dr awl Date mn
�.
Temp: G_ C
v
0
ca
IL
55

G �
aceAnalytical
wwwpacelaDscam
November 26, 2014
Neal Davis
Kapstone Kraft Paper Corp.
100 Gaston Road
Roanoke Rapids, NC 27870
RE: Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Dear Neal Davis:
Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2014.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
`Sincerely,
yak CA� �—
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. _ _ _ L_ S 6

aceAnalytical
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i
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
57

�aceAnalytical
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i
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Clarifier Fecal - Nov 2014
Pace Project No.:
92226604
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92226604001
PCR-5-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226604002
PCR-6-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226604003
PCR-7-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226604004
PCR-8-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical'
www.pecelabs.com
PROJECT NARRATIVE
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Method: SM9221C E (MPN) 503
Description: 92210E Fecal Coliform, MPN RAL
Client: Kapstone Kraft Paper Corp.
Date: November 26, 2014
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
General Information:
4 samples were analyzed for SM9221C E (MPN) 503. All samples were received in acceptable condition with any exceptions noted
below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
- 59

aceAnalytical
wmo:pacelatu.WM
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834A984
Sample: PCR-5-14 Lab ID: 92226604001 Collected: 11/20/14 09:35 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 58.7 % 0.10 1 11/25/14 13:19
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 43.6 MPN/g 0.018 1 11/21/14 08:43
Dale: 11 /26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
- 60

aceAnalytical
wwwpacelab&c=
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: PCR-6-14 Lab ID: 92226604002 Collected: 11/20/14 09:45 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 60.4 % 0.10 1 11/25/14 13:19
92210E Fecal Collform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 35.1 MPN/g 0.018 1 11/21/14 08:43
Date: 11/26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
61

aceAnalytical
wwwpacelabs com
I
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
sample: FUR-7-14 Lab ID: 92226604003 Collected: 11/20/14 09:55 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 59.3 % 0.10 1 11/25/14 13:20
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 73.7 MPN/g 0.018 1 11/21/14 08:43
Date: 11/26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
62

�aneAnalyfical0
wwwpacelatu.cwn
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: PCR-8.14 Lab ID: 92226604004 Collected: 11/20/14 10:05 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 57.2 % 0.10 1 11/25/14 13:20
92210E Fecal Collform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 18.9 MPN/g 0.018 1 11/21/14 08:43
Date: 11/26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
63

aceAnalytical'
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QUALITY CONTROL DATA
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
QC Batch: PMST/7272 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92226604001, 92226604002, 92226604003, 92226604004
SAMPLE DUPLICATE: 1336870
92226473001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 14.0 11.7 18
SAMPLE DUPLICATE: 1336871
92226677002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 17.1 16.5 3
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2014 10:50 AM without the written consent of Pace Analytical Services, Inc..
64

aceAnalytical
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QUALITY CONTROL DATA
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
QC Batch: RBIO/4588 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92226604001, 92226604002, 92226604003, 92226604004
METHOD BLANK: 1336835 Matrix: Solid
Associated Lab Samples: 92226604001, 92226604002, 92226604003, 92226604004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 11/21/14 08:43
SAMPLE DUPLICATE: 1336836
92226604002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 35.1 17.5 87
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /26/2014 10:50 AM without the written consent of Pace Analytical Services, Inc..
65

y ,
acmnalytical.
ww oc6sbicom
QUALIFIERS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
DEFINITIONS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
Date: 11 /26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Z•

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226604
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92226604001
PCR-5-14
ASTM D2974-87
PMST/7272
92226604002
PCR-6-14
ASTM D2974-87
PMST/7272
92226604003
PCR-7-14
ASTM D2974-87
PMST/7272
92226604004
PCR-8-14
ASTM D2974-87
PMST/7272
92226604001
PCR-5-14
SM9221C E (MPN) 503
RBIO/4588
92226604002
PCR-6-14
SM9221C E (MPN) 503
RBIO/4588
92226604003
PCR-7-14
SM9221C E (MPN) 503
RBIO/4588
92226604004
PCR-8-14
SM9221C E (MPN) 503
RB10/4588
Date: 11 /26/2014 10:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
M

a
Document Name: Sample Condition Upon
Document Revised: April 04, 2013
; .PaCOAna lCal'
Receipt SCUR
Page 1 of 2
Document No,:
Issuing Authorities:
"°""
F•RAL-CS-001-rev.02
Pace Asheville Qualit Office
Client Name: Y-- ����
Where Received: Huntersville Asheville [] Eden Raleigh
Courier (Circle): • Fed Ex UPS USPS Client • Commercial Paco Other
Custody Seal on Cooler/sox Present: [] yes Vno Seals Intact' /6 yes [] no
Packing Material: Bubble Wrap Bubble Baps 0 None Other
Circle Thermometer Used: IR Gun S 2206538 a of lco. Wet Blue None ij Somples on Ice, cooling process has begun
IR Gun Baer-11:12208537S
Tomp Corrootlon Factor: A / tract , p C
Corrected Cooler TomI.Lj�ep.: Biological Tissue Is Frozen: Yee NJINt/A
Temp should be above frevyng to VC� Comments:
Date and Initials of person examining
o t / plto
chook
Chain ofCustody Present:
4yes, r3No
ONrA
1•.
Custody Filled out
Yc. 13%
OWA
2. '
stod Relin uished:
es ONo
MA
3.
rof0ustody
me 8, 51tue on COC:
Yee ONo
OwA
4,
ived within Hold Time:
Yes qNo
❑wA
6,
Ttme Anal sls' <72hr :
Yes ❑No
❑wAround
Time Requested:
C]Yos 0,
ON1A
T.
Sufficient Volume:
Yee ONo
13WA
8.
Correct Containers Used:•
-Paco Containers Used:
Ye, ONo
AyAs ONo
OwA
❑wA
0,
Containers Intact:
eYos ONo
❑wA
10.
Filtered volume -received for Dissolved tests
Ova Mo
VfNIA
11.
Sample Labels match COC:
-Includes date/tlmellD/Anal to Matrix:
Yea quo
❑wA
12.
All contalnore needing preservation have been chocked.
'
All conlslnwa needing preservation are found to be In
compliance with EPA recommendation,
exceptions; yoA, gollform,Too, 0AG, WwRo (water
�a []No
Yes ONo
f'[/
[J ee 13No
OwA
❑NIA
13.
Sam les checked for dechlodnatlon:
6Y, ON.
13WA
14.
Heads aoe In VOA Vials >6mm :
OYaa ON.
MA
15,
Trip Blank Present
Trip Blank Custody Seals Present
Pace Trip Blank Lot # If purchased):
Olfos ONo P8A
OYas ONo YwA
16.
Client Notlllcation/ Resofutlon: Field Data Required? Y / N
Person Contacted, Date/Time:
Commenis/ Resolution:
SCURF /SRF Dato:VIt' _. ,QQ
Review:: �) �t� I`®.' a�'222V
so4::
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR IIIIIIIIIIIIIII F , -
CertlBcetlon Office (Le out of hold, Incorrect eservallve out of tamp,
Pr
incorrect containers)
68

r
O
� - e
m
Chain of Custody
a
Report Results to: Bill Results to: Standard Report Delivery
Kapstane Paper r� Rush "Re �r< Delivery 100 Gaston Rd ❑ P very lw/ surcharge)
Roanoke Rapids, NC _
Requested Due Date:
Project Reference: Clarifier Feat AnalysI%44,v. 2D14
ATTN: Neal�Davis ATM:-
Phone: 2S2-533-6295 Purchase order
Sampled By.
M
0(Z
MM

FORM DMSDF
FLYASH RESIDUALS
ANNUAL CERTIFICATION
2014
70

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0021577 FACILITY NAME: KAPSTONE KRAFT PAPER CORP. ROANOKE RAPIDS, NC
PHONE: [phone] COUNTY: HALIFAX OPERATOR: I NEAL DAVIS
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
21 Distribution' and Marketing (complete Parts A, B, and C)
Was the facility in operation durinn the nast calendar year? Yes No 0 —* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources s (include NPDES # if
(
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (As Is
Tons)
Intended use(s)
January
FLYASH
1,131.8
February
FLYASH
672.2
Scotts Hyponex,
466
Potting Soil
March
FLYASH
679.6
Lawerenceville, Va
516.7
Amendment
April
FLYASH
747
May
FLYASH
797
June
FLYASH
745.7
July
FLYASH
693
August
FLYASH
614.5
September
FLYASH
1,201
October
FLYASH
936.7
November
FLYASH
821.6
December
FLYASH
510.6
Total from FORM DMSDF su
( P)
, �; -�..0 ; :,: _, -,�-
�. r..
,Q:.<'> .,,.
Totals.
Annual (dry tons).
,.m,;,:"_._,-:0•.... ��.� ...-
..,_.,_9,55,0,7�,,;;:.,
:.,�..�,, ,.
Amendment(s) used: 0 Bulking Agent(s) used: 0
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the Distribution of Residuals 21 Yes
permit (including but not limited to items 1-3 below) issued by the Division of Water Quality: 13 No —, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. '
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date
Si ature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
llell�
Date
DENR FORM DMSDF (12/2006)
71

Form RSSF
Flyash Residuals Sampling► Summary
72

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0021577 Laboratory: 1)
Facility Name: KapStone Kraft Paper Corporation 2)
Residual Source WQ # or WQ000436 3)
NPDES #: 4)
WWTP Name: KapStone Kraft Paper Corporation 5)
Meritech, Inc. Reidsville, NC
FLYASH
1\6iJ1K6l N1 1
Parameter
(mg/kg)m
Percent Solids (%)
Conc.
Limit
NA
Sample or Composite Date
1/7/14
47
2/4/14
45.5
3/4/14
53
4/2/14
55.3
5/7/14
55.4
6/10/14
58.2
7/8/14
58.7
8/5/14
59
9/2/14
57
10/14/14
58.4
11/4/14
56.4
12/9/14
56.1
Arsenic
75
16.1
16.6
12.7
15.4
16
6.96
0.85
0.847
11
7.47
14.6
15.1
Cadmium
85
0.426
0.448
0.394
0.476
0.477
0.296
0.457
0.358
0.342
0.42
0.36
0.41
Copper
4,300
43.6
45.4
39.8
39.1
53.6
23.4
44
39.3
42.1
41.4
38.3
40.3
Chromium
NA
12.8
13
12.5
12.1
11.7
6.25
12.2
11.5
11.8
12.8
12.4
11.9
Lead
840
14
16.7
12.4
11.8
12.6
7.54
11.6
10.1
11.9
12
11.8
10.8
Mercury
57
0.15
0.16
0.132
0.09
0.15
0.112
0.187
0.144
0.148
0.128
0.133
0.152
Molybdenum
75
0.532
0.543
0.472
0.452
0.451
0.43
0.629
0.424
0.439
0.443
0.443
0.619
Nickel
420
14.7
15.8
13.7
15.1
16.8
8.45
14.9
14.5
14.1
14
12.2
13.3
Selenium
100
1.06
1.09
0.943
0.904
1.58
1.16
0.596
0.847
0.877
0.856
0.887
0.891
Zinc
7,500
30.5
34.8
22.3
26.2
27.3
14.6
18.9
63.6
18.1
17.5
17.7
22.5
Total Phosphorus
TKN
NA
NA
398
552
457
44
411
68.1
392
633
410
1190
208
2,060
276
634
239
627
254
226
312
34
294
486
320
636
Ammonia -Nitrogen
NA
42
22
18.9
18.1
18.1
17.2
21.5
16.9
27.5
17.1
17.7
17.8
Nitrate and Nitrite
NA
21.3
22
5.85
18.1
18.1
17.2
17
16.9
17.5
17.1
17.7
17.8
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for sub mi g false ' formation, including the possibility of fines and imprisonment for knowing violations."
-.-4,A:C
Signature o Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) '73
DENR FORM RSSF (12I2006)

Form RSSF-8
Flyash Residuals Sampling Summary
74

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
WQ 0021577
KAPSTONE KRAFT PAPER CORP
WQ0000436
KAPSTONE KRAFT PAPER CORP
Laboratory: 1) Meritech, Inc. Reidsville, NC
2)
3)
4)
5) Flyash
1\r J10161M1 �
Parameter
(mg)
Sample or Composite Date
1/7/14
2/4/14
3/4/14
4/2/14
5/7/14
6/10/14
7/8/14
8/5/14
9/2/14
10/14/14
11/4/14
12/9/14
Aluminum
16,300
15,800
12,620
14,629
12,382
6,586
11,800
10,700
11,400
12,100
13,600
11,500
Magnesium
1,850
2,390
2,150
1,641
1,931
1,131
1,210
11.3
1,280
1,200
1,300
1,255
Sodium
2,890
3,610
4,340
3,002
2,960
3,745
2,250
3,390
3,860
2,890
1,990
3,080
Potassium
5,320
5,240
4,230
4,213
3,592
2,165
3,220
2,320
2,950
3,070
3,560
3,420
CCE
12.50%
36.30%
2.10%
2.70%
1.80%
3.00%
1.00%
2.98%
2.08
0.65%
1.00%
4.69%
SAR
PAN
8.93
246.3
10.6
41.8
13.1
35
9.54
276.1
9.15
495.9
15.6
842.9
8.02
272.8
12.6
269.4
13
110.7
9.54
32.4
6.44
213.9
11
274
pH
9.4
8.5
9.7
8.1
9.2
10
6.6
9.1
9.4
9.3
8.8
8.9
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including t
possibility of fines and imprisonment for knowing violations."
Signaturefreparer
*Prep ers defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
O
7 ZI
Date
DENR FORM RSSF - B (12/2006) 75

Sampling Analysis Flyash Residuals
76

Meritech, Inc.
,F
a Environmental Laboratory
4. Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging Report Date: 1/17/2014
100 Gaston Rd. NPDES#: WQ0021577
Roanoke Rapids, NC 27870 WQ0000436
Project: Send Even Months
Date Sample Rcvd: 1/7/2014
Meritech Work Order # 01071469
Sample: 1•ly Ash Grab
Para_ mars 1/7/14
Result Analysis
R-eporting Limit Method
% Total Solids
Ammonia, Nitrogen < 47.0 %
42.0 mg/kg 1/8/14
0-100 % SM2540B
TKN 552 m k / / 42 mg/kg EPA 350.1
Nitrate/Nitrite Nitrogen < 21.3 mg/kg 1/10/14 20 m k
Nitrogen, total g/ g 1/10/14 g/ g EPA 351.1
552 mg/kg 1/10/14 21.3 mg/kg EPA 353.2
Aluminum, total 16,300 mg/kg 1/16/14 20 mg/kg EPA 353.2
Arsenic, total5.00 mg/kg EPA 200.7
Barium, total 16.1 mg/kg 1/16/14
647 rng/kg 1/16/14 1.00 mg/kg EPA 200.7
Cadmium, total 0.500 mg/kg EPA 200.7
Calcium, total 0.406 mg/kg 1/16/14
12,800 mg/kg 1/16/14 0.200 mg/kg EPA 200.7
Chromium, total 10.0 mg/kg EPA 200.7
Copper, total 12.8 mg/kg 1/16/14
Lead, total
43.6 mg/kg 1/16/14 1.00 mg/kg EPA 200.7
14.0 m k 1.00 mg/kg EPA 200.7
Magnesium, total g/ g 1/16/14 Mercury, total 1.00 m 1< 1,850 mg/kg 1/16/14 g/ g EPA 200.7
Molybdenum, total mg/kg 1/8/14 0.15 m k 10.0 mg/kg EPA 200.7 Nickel, total 1/16/14 0.02 mg/kg < 0.532 mg/kg EPA 245.1
Phosphorous, total 14.7 mg/kg 1/16/14 0.532 Mg/kg EPA 200.7
Potassium, total
398 mg/kg 1/16/14 1.00 mg/kg EPA 200.7
2.00 mg/kg
Selenium, total 5,320 m�/kg 1/16/14 EPA 200.7
Sodium, total 1/16/14
< 1.06 mg/kg U.0 `mg111`g EPA 200.7
Zinc, total 2,890 mg/kg 1/16/14 1.06 mg/kg EPA 200.7
SAR
30.5 mg/kg 1/16/14 20.0 mg/kg EPA 200.7
pH 1/16/14 _ 8.93 1.0 mg/kg EPA 200.7
CCE 9.4 S.U. 1/8/14 -
12.5 % 1.0 - 14.0 S.U. SM 4500 H B
1/10/14 3.60 % AOAC 955.01
-------------
' hereby certify that I have reviewed and approve these data.
lC_
Laborator-4y Representative
77
642 Tamco Road, Reidsville, North Carolina 27320
teL(336)34?-a7a.Q ,-- - -

chain of Custody Record (COC)
L. MERITECH INC.
�:.'.
A Division of Water Technology and Control, Inc.
642 Tamco Rd
Phone [phone]
Reidsville, NC
Fax: [phone]
--- --—2.7-320--
Email: wtclab(abellsouth.net
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
Location/ID #
START
IEND
=k, A. -I -
Comments:
lethod of Shipment:
UPS
] Fed Ex
�' Hand Delivery
]Other
ill these results be used for regulatory purposes?
Yes No r--�
mquished qy:,? Date
Date:
inquished by: Date:
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
Person Taking Sample (Signature):
Comp? Ci! of
Grab? onts. Test:
L '' 1 % Total Solids, �h
1 Metals - AI,Ar,Cd,(
Ni,Ptot,Se,Na,Zn
1 NH3, TKN,NO2,N0
/'- i
wired
11
(Phone:
1---
ax: -
-------------
Email: /- ,, / -�
,,.
Project: Send Even Months
PO #:
Turn Around Time*
days) 3 - 5 Day 24 - 48 Hr
Lab Use Only
On pH OK?
Ice? �� C12 OK?
Cu,K,Pb,Mg,Hg,Mo,
I
P-A-N (by Calculation)
C-C E (by titration)
Sodium Adsorption Ratio (by Calculation
*RUSH work be approved prior to submitting samples.
Time:, R eiv Date: Time:
Time: Received by: Date: Time:
"i ime: ReceiveA at lab iS
} Date: Time:
i

Meritech, Inc.
Environmental Laboratory
w z Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 020414122
Parameters Result
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE
Sample: Fly Ash Grab
45.5 %
< 22.0 mg/kg
< 44.0 mg/kg
< 22.0 mg/kg
< 44.0 mg/kg
15,800 mg/kg
16.6 mg/kg
765 mg/kg
0.448 mg/kg
13,500 mg/kg
13.0 mg/kg
45.4 mg/kg
16.7 mg/kg
2,390 mg/kg
0.16 mg/kg
< 0.543 mg/kg
15.8 mg/kg
457 mg/kg
5,240 mg/kg
< 1.09 mg/kg
3,610 mg/kg
34.8 mg/kg
10.6
8.5 S.U.
36.3 %
Aiialy7$iS 11atl
2/5/14
2/14/14
2/7/14
2/6/14
2/10/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/7/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/9/14
2/5/14
2/10/14
Report Date:
2/19/2014
NPDES#:
WQ0021577
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
2/4/2014
0-100 %
22.0 mg/kg
44.0 mg/kg
22.0 mg/kg
44.0 mg/kg
5.00 mg/kg
1.00 mg/kg
0.500 mg/kg
0.200 mg/kg
10.0 mg/kg
1.00 mg/kg
1.00 mg/kg
1.00 mg/kg
10.0 mg/kg
0.02 mg/kg
0.543 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
1.09 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 -14.0 S.U.
3.60 %
2/4/14
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200:7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
I hereby certify that I have reviewed and approve these data. G .
Laboratory Representative
79
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
Client: Ka stone Paper
Addr@SS: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal 'Davis
NPDES #:
Phone:
Fax: dSd -53 ! �� S -
Email: n/�L. �r'}iJ/S f,�i��5'ittc/�4
Project: Send Even Months
PO #:
MERITEC H ITC.
Environmental Laboratories
A Division of Watar Technology and Control, Inc.
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclab@_bellsouth.net
Web Site: www.meritech-labs.com
Turn
Around Time*
Std ( o days)
3 - 5 Day
24 - 48 Hr
Sample
Location/ID #
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
START
END
Comp?
Grab?
#or
conts,
Tests Required
q
On
Ice?
pH OK?
C12OK?
Date
Time
Date
Time
Fly Ash
/
1
1
% Total Solids, pH a
.Metals-AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn /111-yi)
1 INH3,
TKN,NO2,NO3,
IP-A-N
(by Calculation
IC-C-E
(by titration)
..
Sodium Adsorption Ratio by Calculation)
Method of Shipment:
Comments:
UPS
❑ Fed Ex
I .11 Hand Delivery
7C
Other
Will these results be used t regulatory purposes?
Yes No
*RUSH work must be roved prior to submitting samples.
Relin d by: Da : / Time: 1
t�J
Re ed b Date:�l T o� Time: / , /y
/(%r
Relln s ed: Date: Time:
/�
Relinquished by Date: Time:
Received by: Date: Time:
Received at b byc Date: Time:E5==
_

�A
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 3/20/2014
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Send Even Months
Roanoke Rapids, NC 27870 Date Sample Rcvd: 3/4/2014
Meritech Work Order # 03041 38 Sample: Fly Ash Grab 3/4/14
Parameters Result Analysis Date Reporting Limit, Method
% Total Solids
'53.0 %
3/5/14
0400 %
SM2540B
Ammonia, Nitrogen
18.9 mg/kg
3/6/14
10 mg/kg
EPA 350.1
TKN
68.1 mg/kg
3/14/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
5.85 mg/kg
3/13/14
5.0 mg/kg
EPA 353.2
Nitrogen, total
74.0 mg/kg
3/18/14
20 mg/kg
EPA 353.2
Aluminum, total
12,620 mg/kg
3/11/14
5.00 mg/kg
EPA 200.7
Arsenic, total
12.7 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Barium, total
880 mg/kg
3/11/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.394 mg/kg
3/12/14
0.200 mg/kg
EPA 200.7
Calcium, total
13,150 mg/kg
3/11/14
10.0 mg/kg
EPA 200.7
Chromium, total
12.5 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Copper, total
39.8 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Lead, total
12.4 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7'
Magnesium, total
2,150 mg/kg
3/11/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.132 mg/kg
3/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.472 mg/kg
3/12/14
0.472 mg/kg
EPA 200.7
Nickel, total
13.7 mg/kg
3/12/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
411 mg/kg
3/12/14
2.00 mg/kg
EPA 200.7
Potassium, total
4,230 mg/kg
3/11/14
20.0 mg/kg
EPA 200.7
Selenium, total
0.943 mg/kg
3/12/14
0.5 mg/kg
EPA 200.7
Sodium, total
4,340 mg/kg
3/11/14
20.0 mg/kg
EPA 200.7
Zinc, total
22.3 mg/kg
3/12/14
1.0 mg/kg
EPA 200.7
SAR
13.1
3/19/14
-
-
pH
9.7 S.U.
3/5/14
1.0 - 14.0 S.U.
-SM 4500 H B
CCE
2.1 %
3/19/14
1 %
AOAC 955.01
hereby certify that! have reviewed and approve these data. �. 14�'J
Laboratory Repr sentative
81
642 Tamco Road, Reidsville, North Carolina 27320
tel.f3361342-474R fax-f-VIA1142-1 S2?

[-1 1 . r.1 r, Y
Chain of Custody Record (COC)
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: 'Neal Davis
NPOES #: 44 ox, (In l.5 7
Phone: �_cre-`/: �z .�
Fax:
Email: /I%j�, ���Jj.'�'�:,��1,o yoti[:�if�
Project: Send Even Months
PO #:
ER1 1 CH INC.
<> S environmental Laboratories
aA;::::.
A Division of Water Technology and Control, Inc.
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclabp_bellsouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
Sid (10s)
3 - 5 Day
24 - 48 Hr
Sample
Location/ID #
Sampling Dates & Times
Person Takingam e(Si nature :
-
Lab Use Only
START
END
Comp?
Grab?
#of
Conts.
Tests q a uired
On
Ice?
pH OK?
C12OK?
Date
Time
Date
Time
Fly Ash
�� /5i %T
L4
iy
1
1
% Total Solids, pH
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn &4'11�11dm,�/cwyt
1
NH3, TKN,NO2,NO3,
1P-A-N
(by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Method of Shipment:
Comments:
El UPS
�edx
Hand Delivery
Other
Will these results be u-5edfor regulatory purposes?
Yes No
*RUSH work must be approved prior to submitting samples.
Dat,/ �/� Time:
RelinquishZ11
a� L , ) 1 /,/ c
Received 4�4:— Date: Time:
�— 3 �-/ �� /Z G
Relinquished D te: Time:
3�
Received by: Date: Time:
Relinquished by: Date: Time:
Recei�vedbby;�

Meritech, Inc.
N. Environmental Laboratory
Laboratory Certification No.165
i.
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 040214119
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total ,
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, tbtal
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE
Result
Sample: Fly Ash Grab
55.3 %
< 18.1 mg/kg
633 mg/kg
< 18.1 mg/kg
633 mg/kg
14,629 mg/kg
15.4 mg/kg
738 mg/kg
0.476 mg/kg
12,278 mg/kg
12.1 mg/kg
39.1 mg/kg
11.8 mg/kg
1,641 mg/kg
0.090 mg/kg
< 0.452 mg/kg
15.1 mg/kg
392 mg/kg
4,213 me/kg
0.904 mg/kg
3,002 mg/kg
26.2 mg/kg
9.54
8.1 S.U.
2.7 %
Analysis Date
4/3/14
4/3/14
4/7/14.
4/4/14
4/10/14
4/14/14
4/14/14
4/14/14
4/14/14
4/14/14
4/14,/14
4/14/14
4/14/14
4/14/14
4/7/14
4/14/14
4/14/14
4/14/14
4/141/14
4/14/14
4/14/14
4/14/14
4/14/14
4/4/14
4/7/14
Report Date:
4/15/2014
NPDES#:
WQ0000436
WQ0021577
Project:
Send Even Months
Date Sample Rcvd:
4/2/2014
,•fL�l4
Reporting Limit - M-ethod
0-100 %
SM2540B
18.1 mg/kg
EPA 350.1
20 mg/kg
EPA 351.1
18.1 mg/kg
EPA 353.2
20 mg/kg
EPA 353.2
5.00 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
0.500 mg/kg
EPA 200.7
0.200 mg/kg
EPA 200.7
10.0 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7....
10.0 mg/kg
EPA 200.7
0.02 mg/kg
EPA 245.1
0.452 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
2.00 mg/kg
EPA 200.7
20.0 mg/kg
EPA 200.7
0.5 mg/kg
EPA 200.7
20.0 mg/kg
EPA 200.7
1.0 mg/kg
EPA 200.7
1.0-- 14.0 S.U.
SM 4500 H B
3.60 %
AOAC 955.01
hereby certify that I have reviewed and approve these data.
Laboratory Repres ntative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
NPDES
Phone:c�
-�.. -�..
Fax:
Email: �
Project: Send Even Months
PO #:
" ERI 1 ECH INC.
Environmental Laboratories
A Division of Water Technology and Control Inc.
`-�
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclab(&bellsouth.net
Web Sate: www.meritech-labs.com
Turn Around Time*
Std 1 days)
3 - 5 Day I
o
24 - 48 Hr
t�
Sample
Location/tD #
Sampling Dates & Times
Person Taking Sample (Signature): �, J
Lab Use Only
START
END
Comp?
Grab?
#of
Conts.
Tests equired7
On
Ice? "1 (,,
pH OK?
C12 OK?
Date
Time
Date
Time
Fly Ash
_ %
-7, v�
ra
�
1
% Total Solids, pH
1
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn � A/!/aw"
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Method of Shipment:
Comments:
UPS
Fed Ex
Band Delivery
Other
Will these results bemused for regulatory purposes?
Yes I No
*RUSH work must be approved prior to submitting samples.
Relinquished %at Time:
' X Y' 1��
Re a Date:: Time:
( �
Relinqui rDate, c% T�ne:
Received by: Date: Time:
Relinquished by: Date: Time:
Received' I b by: Date: Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Project:
Date Sample Rcvd:
6/5/2014
WQ0021577
WQ0000436
Send Even Months
5/7/2014
Meritech Work Order #
050714110 Sample: Fly Ash Grab
5/7/14
Parameters
Resul
Analysis Date
Reporting Limit
Method
% Total Solids
55.4 %
5/7/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 18.1 mg/kg
5/7/14
18.1 mg/kg
EPA 350.1
TICN
1,190 mg/kg
5/13/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 18.1 mg/kg
5/9/14
18.1 mg/kg
EPA 353.2
Nitrogen, total
1,190 mg/kg
5/15/14
20 mg/kg
EPA 353.2
Aluminum, total
12,382 mg/kg
5/9/14
5.00 mg/kg
EPA 200.7
Arsenic, total
16.0 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Barium, total
653 mg/kg
5/21/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.477 mg/kg
5/9/14
0.200 mg/kg
EPA 200.7
Calcium, total
12,653 mg/kg
5/21/14
10.0 mg/kg
EPA 200.7
Chromium, total
11.7 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Copper, total
53.6 mg/kg
5/21/14
1.00 mg/kg
EPA 200.7
Lead, total
12.6 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Magnesium, total
1,931 mg/kg
5/21/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.15 mg/kg
5/12/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
0.451 mg/kg
5/9/14
0.452 mg/kg
EPA 200.7
Nickel, total
16.8 mg/kg
5/9/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
410 mg/kg
5/9/14
2.00 mg/kg
EPA 200.7
Potassium, total
3,592 mg/kg
5/9/14
20.0 mg/kg
EPA 200.7
Selenium, total
1.58 mg/kg
6/5/14
0.5 mg/kg
EPA 200.7
Sodium, total
2.960 mg/kg
5/9/14
20.0 mg/kg
EPA 200.7
Zinc, total
27.3 mg/kg
5/9/14
1.0 mg/kg
EPA 200.7
SAR
9.15
6/5/14
-
-
pH
9.2 S.U.
5/15/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
1.8 %
5/13/14
3.60 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
,. P'(� -, -
Laboratory Representi7tive
RR
642 Tamco Road, Reidsville, North Carolina 27320
tel.f3361342-4748 fax.f3361342-1.1;22

Iv
Chain of Custody Record (COC)
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
NPDES #: li
(D0a 3�
Phone: _ 3 -
Fax: a 3
/�
Email: .�✓E�L�$ /!�L �AiQSO,�E=�
Project: Send Even Months,
MERITECH INC.
Environmental Laboratories
a ;�
`..... .. A Division of Water Technology and Control, Inc.
a
642 Tamco Rd
Reidsville, NC
27320
Phone [phone]
Fax: [phone]
Email: wtclab(c_bellsouth.net
27870
Attention: Neal Davis
PO #:
Turn Around Time*
Std (10 d s)
33-555DDay
24 -
Web Site: www.meritech-labs.com
Person Taking Sample (Signature:
Z�L
Lab Use Only
Sample
Location/ID #
Sampling Dates & Times
p 9
START END
Date Time Date Time
Comp? # of
Grab? Conts.
Tests equired
On
ice?
pH OK?
C12OK?
Ash
.'�3om
1
% Total Solids, H
, �U
Fly
1
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation
C-C=E (by titration)
Sodium Adsorption Ratio (by Calculation
Comments:
Method of Shipment:
UPS
Will these results be
ed for regulatory purposes?
*RUSH work must be approved prior to submitting samples.
Yes
No
�edx
Relin 's by: /1
ate: /�
Time:
3 3
Received Date: me:
-- 7 / 3 3
Delivery
!///
Hand
Date:
Time:
Received by: Date: Time:
Relinquish
- -7
/
/,6
Other
Date
Time:
Received by: Date: Time:
at i
Relinquished by:
-
86

Meritech, Inc.
w.. Environmental Laboratory
a Laboratory Certification No. 165
G
Contact: Neal Davis
Report Date:
6/24/2014
Client: Kapstone Paper
& Packaging
NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870
Project:
Send Even Months
Date Sample Rcvd:
6/10/2014
Meritech Work Order #
06101485 Sample: Fly Ash Grab
6/10/14
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
58.2 %
6/11/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 17.2 mg/kg
6/13/14
17.2 mg/kg
EPA 350.1
TKN
2,060 mg/kg
6/12/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 17.2 mg/kg
6/11/14
17.2 mg/kg
EPA 353.2
Nitrogen, total
2,060 mg/kg
6/16/14
20 mg/kg
EPA 353.2
Aluminum, total
6,586 mg/kg
6/16/14
5.00 mg/kg
EPA 200.7
Arsenic, total
6.96 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Barium, total
364 mg/kg
6/16/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.296 mg/kg
6/12/14
0.200 mg/kg
EPA 200.7
Calcium, total
6,890 mg/kg
6/1/14
10.0 mg/kg
EPA 200.7
Chromium, total
6.25 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Copper, total
23.4 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Lead, total
7.54 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Magnesium, total
1,131 mg/kg
6/16/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.112 mg/kg
6/14/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
< 0.430 mg/kg
6/12/14
0.430 mg/kg
EPA 200.7
Nickel, total --
8.45 mg/kg
6/12/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
208 mg/kg
6/12/14
2.00 mg/kg
EPA 200.7
Potassium, total
2,165 mg/kg
6/16/14
20.0 mg/kg
EPA 200.7
Selenium, total
1.16 mg/kg
6/16/14
0.5 mg/kg
EPA 200.7
Sodium, total
3,745 mg/kg
6/16/14
20.0 mg/kg
EPA 200.7
Zinc, total
14.6 mg/kg
6/12/14
1.0 mg/ kg
EPA 200.7
SAR
15.6
6/16/14
-
-
pH
10 S.U.
6/11/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
3.0 %
6/13/14
3.60 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
EIMA
642 Tamco Road, Reidsville, North Carolina 27320
te1.VT1A1'A47-474R fatic_fggA1q47-1 ri77

■ v
Chain of Custody Record (COC)
NPDES #:
1
w
MERITECH INC.
Client:
Kapstone Paper
Phone: ��
,;3_ a9s
Environmental Laboratories
Fax: 0?5'
's G
A Division of Water Technology anP. d Control, Inc.
Address:
100 Gaston Rd
Email: L
�.....
Roanoke Rapids, NC
Project: Send Even Months
642 Tamco Rd
Phone [phone]
27870
Po #:
Reidsville, NC
Fax: [phone]
Turn Around Time''
27320
Email: wtclab(&bellsouth.net
Attention:
Neal Davis
std 45ays)
3 - 5 Day
24 - 48 Hr
Web Site: www.meritech-labs.com
t�
Sample
Sampling Dates & Times
p 9
Person Taking Sample (Signature)- y
Lab Use Only
Location/lD #
START
END
Comp?
Grab?
#of
Conts.
Tes s Required
q
On
ice??
pH OK?
C12OK?
Date
Time
Date
Time
Fly Ash
p /
Jr'
i�
1
% Total Solids, pH
G "1
1
Metals - AI,Ar,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Comments:
Method of Shipment:
❑ UPS
Will these results be
❑ Fed Ex Yes
Relinquishe
land Delivery
R�ulshed
❑Other
Relinquished by:
1 INH3, TKN,NO2,NO3
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (bv Calculation
regulatory purposes? *RUSH work must be approved prior to submitting samples.
No
Date• t7ime Recei d by: Date / Time: r—�j
�0 /`� I 2f a j d
Dat / 3jiriw� Receiv by: Date: Time:
Date: Time: Recei at la by: Date: Time:
••

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Report Date:
7/22/2014
Client: Kapstone Paper & Packaging
NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids,
NC 27870
Project:
Send Even Months
Date Sample Rcvd:
7/8/2014
Meritech Work Order #
07081479 Sample: Fly Ash Grab
7/8/14
Parameters
Resul
Analysis Date
Reporting rting Limit
Method
% Total Solids
58.7 %
7/9/14
0-100 %
SM2540B
Ammonia, Nitrogen
21.5 mg/kg
7/10/14
17.2 mg/kg
EPA 350.1
TKN
634 mg/kg
7/21/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 17.0 mg/kg
7/9/14
17.0 mg/kg
EPA 353.2
Nitrogen, total
634 mg/kg
7/21/14
20 mg/kg
EPA 353.2
Aluminum, total
11,800 mg/kg
7/16/14
5.00 mg/kg
EPA 200.7
Arsenic, total
< 0.850 mg/kg
7/16/14
0.85 mg/kg
EPA 200.7
Barium, total
658 mg/kg
7/16/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.457 mg/kg
7/16/14
0.200 mg/kg
EPA 200.7
Calcium, total
9,900 mg/kg
1 7/16/14
10.0 mg/kg
EPA 200.7
Chromium, total
12.2 mg/kg
7/16/14
1.00 mg/kg
EPA 200.7
Copper, total
44.0 mg/kg
7/16/14
1.00 mg/kg
EPA 200.7
Lead, total
11.6 mg/kg
7/16/14
1.00 mg/kg
EPA 200.7
Magnesium, total
1,210 mg/kg
7/16/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.187 mg/kg
7/14/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
0.629 mg/kg
7/16/14
0.430 mg/kg
EPA 200.7
Nickel, total
14.9 mg/kg
7/16/14
1.00 mg/kg
EPA 200.7
Phosphorous, total
276 mg/kg
7/16/14
2.00 mg/kg
EPA 200.7
Potassium, total
3,220 mg/kg
7/16/14
20.0 mg/kg
EPA 200.7
Selenium, total
0.596 mg/kg
7/17/14
0.5 mg/kg
EPA 200.7
Sodium, total
2,250 mg/kg
7/16/14
20.0 mg/kg
EPA 200.7
Zinc, total
18.9 mg/kg
7/16/14
1.0 n.g/kg
EPA 200.7
SAR
8.02
7/16/14
-
-
pH
6.6 S.U.
7/10/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
< 1 %
7/17/14
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
%. ff)av
Laboratory Representative 89
642 Tamco Road, Reidsville, North Carolina 27320
teLf3361342-4748 fax.f3361342-1522

Chain of Custody Record (COC)
Client: Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
NPDES #:
Phone:
Fax: Sa -,S3 - ,
(�
Email: /I/LrL�9L(!$ii�J���p<y
Project: Send Even Months
PO #:
MERITECH INC.
Environmental Laboratories
` A Division of Water Technology and Control, Inc.
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclabObellsouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
Std days)
3 - 5 Day
o
24 - 48 Hr
Sample
Location/ID #
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
START
END
Comp?
Grab?
# of
Conts.
Tests quired
On
Ice?
pH OK?
C12OK?
Date
Time
Date
Time
Fly Ash
/
Y"/Q
1
% Total S ids, pH
U
1
Metals - AI ,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn • �y/TlYf/LrY s}tJ�yn
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation
Method of Shipment:
Comments:
❑ UPS
❑ Fed
Hand Delivery
❑Other
Will these results be for regulatory purposes?
Yes No
*RUSH work must be approved prior to submitting samples.
Relinquished b Date' Time:
/Z/ ✓l%,�tS'2
Receive �f 6-7Date: Time:
_ e 1/i�v. / • -%/ Illf.'J``L
Relin i.p by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
R ved at la a ime�

Meritech, Inc.
F
Environmental Laboratory
Laboratory Certification No.165
s _
Report Date:
8/26/2014
Contact: Neal Davis
NPDES#:
WQ0021577
Client: Kapstone Paper & Packaging
WQ0000436
100 Gaston Rd.
Project:
Send Even Months
Roanoke Rapids,
NC 27870
Date Sample Rcvd:
8/5/2014
Meritech Work Order #
08051486 Sample: Fly Ash Grab
8/5/14
Parameters
Resul
Analysis Date
Reporting Limit
Method
%Total Solids
a
59.0 /0
8/6/ 14
8/12/14
0-100 %
16.9 mg/kg
SM2540B
EPA 350.1
Ammonia, Nitrogen
< 16.9 mg/kg
627 mg/kg
8/20/14
20 mg/kg
EPA 351,1
TKN
Nitrate/Nitrite Nitrogen
< 16.9 mg/kg
8/6/14
16.9 mg/kg
20 mg/kg
EPA 353.2
EPA 353.2
Nitrogen, total
627 mg/ kg
10,700 mg/kg
8/20/14
8/18/14
5.00 mg/kg
EPA 200.7
Aluminum, total
Arsenic, total
847 m k
< 0.14
8/18/14
0.847 mg/kg
0.500 mg/kg
EPA 200.7
EPA 200.7
Barium, total
588 mg/kgg/g
0.358 mg/kg
8/18/
8/18/14
0.200 mg/kg
EPA 200.7
Cadmium, total
Calcium, total
9,150 mg/kg
8/18/14
10.0 mg/kg
EPA 200.7
EPA 200.7
Chromium, total
11.5 mg/kg
39.3 mg/kg
8/18/14
8/18/14
1.00 mg/kg
1.00 mg/kg
EPA 200.7
Copper, total
Pp
Lead, total
.
101 mg/kg
8/18/14
1.00 mg/kg
10.0 mg/kg
EPA 200.7
EPA 200.7
Magnesium, total
11.30 mg/kg
0.144 mg/kg
8/18/14
8/7/14
0.02 mg/kg
EPA 245.1
Mercury, total
Molybdenum, total
< 0.424 mg/ g k
8/18/14
0.424 mg/kg
1.00 mg/kg
EPA 200.7
EPA 200.7
Nickel, total
Phosphorous, total
14.5 mg/kg
239 m k
g/ g
8/18/14
8/18/14
2.00 mg/kg
EPA 200.7
EPA 200.7
Potassium, total
2,320 mg/kg
< 0.847 mg/kg
8/18/14
8/18/14
20.0 mg/kg
0.847 mg/kg
EPA 200.7
Selenium, total
Sodium, total
3,390 m k
g/ g
8/18/14
20.0 mg/kg
1.0 m 1.
g/ g
EPA 200.7
EPA 200.7
Zinc, total
63.6 mg/kg
8/18/14
SAR
12.6
9.1 S.U.
8/18/14
8/6/14
-
1.0 - 14.0 S.U.
SM 4500 H B
PH
CCE
2.98 %
8/ 7/ 14
3.60 %
AOAC 955.01
hereby certify that I have reviewed and approve these data. u'
Laboratory Represen ative
91
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

r I I . e-,-"r'k
Chain of Custody Record (COC)
Kapstone Paper
Address: 100 Gaston Rd
Roanoke Rapids, NC
27870
Attention: Neal Davis
NPDES #: /S % '7
Phone: s
Fax: 3
Email:
Project: Send Even Months
Po #:
.g, 1'1fIERITECH ITC
`' .INC.Client:
Environmental Laboratories
3hyt��< A Division of Water Technology and Control, Inc.
642 Tamco Rd Phone [phone]
Reidsville, NC Fax: [phone]
27320 Email: wtclab(a)bellsouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
Std (10 ays)
3-5 Day
24 - 48 Hr
o
Sample
Location/ID #
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
START
END
Comp?
Grab?
#of
Conts.
Tests�equired
On
Ice?
pH OK?
C12 OK?
Date
Time
Date
Time
Fly Ash
/
r.35
1
% Total Solids, pH
I
-1
Metals - AI,Ar,Cd,Ca,Cu;K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn 44
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Method of Shipment:
Comments:
El UPS
Fed Ex
���and Delivery
❑Other
Will these results be ed for regulatory purposes?
Yes No
RUSH work must be approved prior to submitting samples.
Reling a by:
•Y
at/ / Time:
> f� ,/ 5'
Rec ive��y: Date: / T me:
_ _� //I !� cp• �' . f= J 2; .� ,f
ed by: Date: Time:
ZX'."'�-c+-I,�, Cj L j Ls-, 'S-d
Received by: j Date: Time:
Relinquished by: Date: Time:
Rprc ved at by:
U
92
o" I%-

Meritech, Inc.
Environmental Laboratory
�. Laboratory Certification No.165
a' y.
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 09021442
parame M
Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
PH
CCE
Resul
Sample: Fly Ash Grab
57.0 %
27.5 mg/kg
226 mg/kg
< 17.5 mg/kg
226 mg/kg
11,400 mg/kg
11.0 mg/kg
846 mg/kg
0.342 mg/kg
11,200 mg/kg
11.8 mg/kg
42.1 mg/kg
11.9 mg/kg
1,280 mg/lcg
0.148 mg/kg
< 0.439 mg/kg
14.1 mg/kg
254 mg/kg
2,950 mg/kg
< 0.877 mg/kg
3,860 mg/kg
18.1 mg/kg
13.0
9.4 S.U.
2.08 %
Analysis Date
9/3/11
9/4/14
9/5/14
9/3/14
9/10/14
9/8/14
9/8/14
9/8/14
9/8/14
9/8/14
9/8/14
9/8/14
9/8/14
9/8/14
9/4/14
9/8/14
9/8/14
9/8/14
9/8/11
9/8/14
9/8/14
9/8/14
9/8/14
9/3/14
9/8/14
I hereby certify that 1 have reviewed and approve these data.
Report Date:
9/12/2014
NPDES#:
WQ0021577
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
9/2/2014
Reporting Limit
0-100 %
16.9 mg/kg
20 mg/kg
17.5 mg/kg
20 mg/kg
5.00 mg/kg
0.847 mg/kg
0.500 mg/kg
0,200 mg/kg
10.0 mg/kg
1.00 mg/kg
1.00 mg/kg
1.00 mg/kg
10.0 mg/kg
0.02 mg/kg
0.439 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.877 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 - 14.0 S.U.
3.60 %
a Q 114
Metho
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 2003
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
Laboratory Representative
�3
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

rli . '--,fik
Chain of Custody Record (COC)
Kapstone Paper
NPDES #: 0 crm J1
Phone: �z/57�
a9S
1 �1z INC.Client:
Environmental Laboratories
oZZ?S33
Fax:
{Z
z?• A Division of Water Technology and Control Inc.
Address: 100 Gaston Rd
Email: ^/�}�/, ✓�Al�is(�i;A.Qr1F,-
Roanoke Rapids, NC
Project: Send Even Months A* �V
642 Tamco Rd Phone [phone]
27870
PO #:
Reidsville, NC Fax: [phone]
Turn Around Time*
Std 1 ays)
3 - 5 Day
24 - 48 Hr
27320 Email: wtclabpbelisouth.net
Attention: Neal Davis
Web Site: wvvw.meritech-labs.com
A
r--=
Sample
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
START
END
Comp?
Grab?
#of
Conts.
Tests equired
ce
Ice?
pH OK?
C12 OK?
Location/ID #
Date
Time
Date
Time
Fly Ash
'30
I
1
% Total S lids,. pH 1`
•G
M
1
Metals - Af, fCd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Pt6t,Se
Ni Na,Zn
1
NH3, TKN,NO2,NO3,
IP-A-N
(by Calculation)
C-CGE (by titration)
Sodium Adsorption Ratio (by Calculation
Comments:
Method of Shipment:
❑ UPS
Will these results be qs6d for regulatory purposes?
*RUSH work must be approved prior to submitting samples.
❑ Fed Ex
Yes I I No r-
Relinqu' b //J
Da Tim
Recei d by: Date: line: / 0 1 C
_�r( ( o
Hand Delivery
ReH uish by: Date: 2T
�
Received by: Date: Time:
❑Other
Relinq fished by: Date: Time:
a Dater, Time:
)4

f Meritech, Inc@
r. .
Environmental Laboratory
Laboratory Certification No.16
,f
Revised Date: 10/29/2014
Contact: Neal Davis Report Date: 10/27/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
WQ0000577
100 Gaston Rd.
436
Roanoke Rapids, NC 27870 Project: Monthly
Date Sample Rcvd: 10/14/2014
Meritech Work Order # 101414137
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE
Result
Sample: Fly Ash Grab
58.4 %
< 17.1 mg/kg
< 34.2 mg/kg
< 17.1 mg/kg
< 34.2 mg/kg
12,100 mg/kg
7.47 mg/kg
731 mg/kg
0.420 mg/kg
11,900 mg/kg
12.8 mg/kg
41.4 mg/kg
12.0 mg/kg
1,200 mg/kg
0.128 mg/kg
0.443 mg/kg
14.0 mg/kg
312 mg/kg
3,070 mg/kg
o � �i
< 0.��5, � irg� •cg
2,890 mg/kg
17.5 mg/kg
9.54
9.3 S.U.
0.65 %
Analysis Date
10/16/14
10/21/14
10/20/14
10/16/14
10/23/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10117114
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/21/14
10/15/14
10/20/14
Reporting Limit
0-100 %
17.1 mg/kg
34.2 mg/kg
17.1 mg/kg
34.2 mg/kg
5.00 mg/kg
0.847 mg/kg
0.500 mg/kg
0.200 mg/kg
10.0 mg/kg
1.00 mg/kg
1.00 mg/kg
1.00 mg/kg
10.0 mg/kg
0.02 mglkg
0.424 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.856 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 - 14.0 S.U.
3.60 %
10/14/14
Method
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
I hereby certify that I have reviewed and approve these data. k . �&L
Laboratory Representative
95
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

1-20-20B
Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
100 Gaston Road Fax: [phone]
� � �
�� � � � INC'
MERAddre
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC. Email:_ Neal.Davis(@Kapstonepaper.c
. �
642 Tamco Rd. Phone: [phone]
27870 Project:_ Monthly I
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
WWW . m e ri t e c h -I a b s . C I 1 YY1 I
Attention: Neal Davis Turn Around Time'
'RU,S rk needs prior approval.
How would you like your report sent?
Circle all that apply: Email (preferred) , Fax Mail Std (10 - s Des 2�5
I
Sampling Dates & Times
P g
Person Taking Sample Sign/Print):
n�cx}� ��- chi S
C[.,-
Lab Use
Sample Location
and/or ID #
Start
End
Comp.
Grab?
# of Cont.
t(s) Required
on Ice?
Yes No
pH OK?
Cl OK?
Date
Time
Date
Time
FLYASH
%Q / /'
Lt—
_
%TOTA SOLIDS, Ph,
Metals: M, , Pb, M , Ni,
a/
Z hro lum, Barfum, P t, N , T , NO�N&3
, C
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
Method Of
Shipment:
UPS
Fed Ex
and Delivery
Other
R� -
QT
Dechlorination (<0.5 m of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation.'
Comments: l�-�`?jCompositor #
c'1�.h �0�1� IiK��r� added
� Jug #
g
Are these results for regulatory`� purposes? Y Report results in: mg/ u /kg ug/L U
Relinquished by: D te: ,/J/, Time: Z Rec ed by: �1 Dajg:� / Time: Q ��
` f//72 = = z
Relinq hed by: L0 D yti Time: tl C~ Receiv by: Date: Time:
✓ L /7 T J
Relinquis ed by: Date: Time:
ra
W

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 110414102
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE
Resul
Sample: Fly Ash Grab
56.4 %
< 17.7 mg/kg
486 mg/kg
< 17.7 mg/kg
486 mg/kg
13,600 mg/kg
14.6 mg/kg
851 mg/kg
0.360 mg/kg
12,300 mg/kg
12.4 mg/kg
38.3 mg/kg
11.8 mg/kg
1,300 mg/kg
0.133 mg/kg
< 0.443 mg/kg
12:2 mg/kg
294 mg/kg
3,560 mg/kg
< 0.887 mg/kg
1,990 mg/kg
17.7 mg/kg
6.44
8.8 S.U.
<1 0/0
Analysis Date
11/5/14
11/10/14
11/17/14
11/5/14
11/17/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/11/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/12/14
11/10/14
11/17/14
Report Date:
11/18/2014
NPDES#:
WQ0021577
WQ0000436
Project:
Send Even Months
Date Sample Rcvd:
11/4/2014
Reporting Limit
0-100 %
17.7 mg/kg
20 mg/kg
17.7 mg/kg
20 mg/kg
5.00 mg/kg
0.847 mg/kg
0.500 mg/kg
0.200 mg/kg
10.0- mg/kg
1.00 mg/kg
1.00 mg/kg
1.00 mg/kg
10.0 mg/kg
0.02 mg/kg
0.443 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.887 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 - 14.0 S.U.
3.60 %
11/4/14
Method
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
7
I hereby certify that 1 have reviewed and approve these data. L
Laboratory Represe tative
97
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (CCC)
NPDES #: j , r,
Client: Kapstone Paper
Phone:
MERITECH INC.
Environmental Laboratories
i Fax:
A Division of Water Technology and Control, Inc.
Address: 100 Gaston Rd
Email: M- Alt
Roanoke Rapids, NC
Project: Send Even Months
642 Tamco Rd Phone [phone]
27870
PO #:
Reidsville, NC Fax: [phone]
Turn Around Time*
Std (1 lclays)
3 - 5 Day
24 - 48 Hr
27320 Email: wtclabpbelisouth.net
Attention: Neal Davis
Web Site: www.meritech-labs.com
Sample
Sampling Dates & Times
person Taking Sample (Signature): i / n
Lab Use Only '
LocationllD #
START
END
Comp?
#of
Tests effttuired
`'
On
Ice?
pHOK?I
C12 OK?
Date
Time
Date
Time
Grab?
Conts.
,..
-
Fly Ash
1
/
% Total Solids, pH,'
1 :
Metals - I,q r,Cd, a,CU�, ,1P g,Hg,Mo,
L:A 67
' /
I�li,Pt6t,Se,Na - ilte
1
NH3, TKN,NO2,NO3,
P-A-N (by Calculation)
C-C-E (by titration)
Sodium Adsorption Ratio (by Calculation)
Comments:
Method of Shipment:
UPS
Will these results be- ysed for regulatory purposes?
*RUSH work must be approved prior to submitting samples.
Fed Ex
Yes No
Reliryqut;hed by: Da,/ TI ��
Rec Date Time:
Hand Delivery
•�
Relin a Date: Time:
II ����� 5
Received by: Date: Time:
Other
-7
Relinquished by: Date: Time:
Received at lab Date: Time:
�
:'

` Meritech, Inc.
Environmental Laboratory
F Laboratory Certification No. 165
Contact: Neal Davis Report Date: 12/23/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Project: Send Even Months
Date Sample Rcvd: 12/9/2014
Meritech Work Order # 12091494 Sample: Fly Ash Grab 12/9/14
Parameters Resu t Analysis Date Reporting Limit Method
% Total Solids
56.1 %
12/10/14
0-100 %
SM2540B
Ammonia, Nitrogen
< 17.8 mg/kg
12/15/14
17.8 mg/kg .
EPA 350.1
TKN
636 mg/kg
12/16/14
- 20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
< 17.8 mg/kg
12/11/14
17.8 mg/kg
EPA 353.2
Nitrogen, total
636 mg/kg
12/16/14
20 mg/kg
EPA 353.2
Aluminum, total
11,500 mg/kg
12/11/14
5.00 mg/kg
EPA 200.7
Arsenic, total
15.1 mg/kg
12/11-/14
0.847 mg/kg
EPA 200.7
Barium, total
709 mg/kg
12/11/14
0.500 mg/kg
EPA 200.7
Cadmium, total
0.410 mg/kg
12/11/14
0.200 mg/kg
EPA 200.7
Calcium, total
9,750 mg/kg
12/11/14
10.0 mg/kg
EPA 200.7
Chromium, total
11.9 mg/kg
12/11/14
1.00 mg/kg .
EPA 200.7
Copper, total
40.3 mg/kg
12/11/14
1.00 mg/kg
EPA 200.7
Lead, total
10.8 mg/kg
12/11/14
1.00 mg/kg
EPA 200.7
Magnesium, total
1,255 mg/kg
12/11/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.1.52 mg/kg
12/12/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
0.619 mg/kg
12/11/14
0.443 mg/kg
EPA 200.7
Nickel, total
13.3 mg/kg
12J11/14 .
1.00 mg/kg
EPA 200.7
Phosphorous, total
320 mg/kg
12/11/14
2.00 mg/kg
EPA 200.7
Potassium, total
3,420 mg/kg
12/11/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 0.891 mg/kg
12/11/14
0.891. mg/kg
EPA 200.7
Sodium, total
3,080 mg,/kg
12/11/14
20.0 mg/kg
EPA 200.7
Zinc, total
22.5 mg/kg
12/11/14
1.0 mg/kg
EPA 200.7
SAR
11.0
12/11/14
pH
8.9 S.U.
12/15/14
1.0 - 14.0 S.U.
SM 4500 H B
CCE
4.69 %
12/16/14
3.60 %
AOAC 955.01
! hereby certify that / have reviewed and approve these data,
Laboratory Representative 99
642 Tamco Road, Reidsville, North Carolina 27320
tel.f3361342-4748 fax.f3361342-1572

Chain of Custody Record (COC)
NPDES #:
s
/I
Y.
MERITECH INC.
Client:
Kapstone Paper.
Phone:
..
Environmental Laboratories
Fax:
A Division of Water Technology and Control, Inc.
Address:
100 Gaston Rd
Email: avl/ n
E/`%L.1)Al/!s' l"�i%rQS7lfitt~ %J
Z
::.�.
Roanoke Rapids,_ NC
Project: Send Even Months
642 Tamco Rd
Phone [phone]
27870
PO #:
Reidsville, NC
Fax: [phone]
Turn Around Time*
27320
Email: wtclab(a�bellsouth.net
Attention:
Neal Davis
Std (10 days
-3 - 5 Day
24 - 48 Hr
Web Site: www.meritech-labs.com
o
Sample
Sampling Dates & Times
Person Taking Sample (Signature):
Lab Use Only
Location/ID #
START
END
Comp?
Grab?
# of
Conts.
Test Required
_
On
Ice?
pH OK?
C12OK?
Date
Time
Date
Time
-ly
'`
Z �r
'
1
% Total -Solids, H'
b �Vc-
`
Ash'
Y
1
Metals -AI,A ,Cd,Ca,Cu,K,Pb,Mg,Hg,Mo,
Ni,Ptot,Se,Na,Zn `lOf
.045-e
IrIJ
1
NH3, TKN,NO2,NO3,
Comments:
Method of Shipment:
Q UPS
Will these results be
Fed Ex Yes
Relinquish
and Delivery
e inqui by:
Other
nqulshed
for regulatory purposes?
No
Date: j Time:
Date: Timms
/a-'
Date: Time:
P-A-N (by Calculation)
C-GE (by titration)
Sodium Adsorption Ratio (by Calculation
*RUSH work must be approved prior to submitting samples -
by: Date: Time:
ived by: Date: Time:
ived a ` Date. _ , �_( Time: r p t
100

TCLP
Flyash Residuals
1.01

Meritech, Inc.
Environmental Laboratory
µtp.
F" Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
12/29/2014
WQ0000436
WQ0021577
12/9/2014
Meritech Work Order #
12091497 Sample: Fly Ash
Collection Date:
12/9/14,
1311-
TCLP Metals
Parameter
Results
Analysis
Det. Limit
Reg. Limi
Method
Arsenic
< 0.100 mg/L
12/17/14
0.100
5.0
EPA 200.7
Barium
0.512 mg/L
12/17/14
0.050
100.0
EPA 200.7
Cadmium
< 0.020 mg/L
12/17/14
0.020
1.0
EPA 200.7
Chromium
< 0.050 mg/L
12/17/14
0.050
5.0
EPA 200.7
Lead
< 0.100 mg/L
12/17/14
- 0.100
5.0
EPA 2.00.7
Mercury
. < 0.02 mg/L
12/16/14
0.02
0.2
EPA 245:1
Selenium
< 0.100 mg/L
12/17/14
0.100
1.0
EPA 200.7
Silver
< 0.050 mg/L
12/17/14
0.050
5.0
EPA 200.7
TCLP Organics
Parameter Results Analysis Method
Volatiles 8260
Attached
12/12/14
8260
Semi Vol. 8270
Attached
12/20/14
8270 .
Ignitability
> 140 °F
12/10/14
- EPA 1030
pH
9.3 S.U.
12/10/14
1.0 - 14.0 S.U. SM 4500 HB
Other Tests
Parameter
Results
Analysis
Reporting Limit Method
Sulfide, total
< 10 mg/kg
12/10/14
10 mg/kg SM 4500 SD
Cyanide, total
< 0.5 mg/kg
12/15/14
0.5 mg/kg EPA 335.4.
102
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]-

Meritech, Inc.
Environmental Laboratory
,5a Laboratory Certification No. 165
Contact: Neal Davis Report Date: 12/29/2014
Client: Kapstone Paper & Packaging NPDES#: WQ0000436
100 Gaston Rd WQ0021577
Roanoke Rapids, NC 27870 Date Sample Rcvd: 12/9/2014
Meritech Work Order # 12091497 Sample: Fly Ash Collection Date: 12/9/14
13 11 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Analyst: Summit Analysis Date: 12/19/14
Parameter Results Det. Limit Reg. Limit Dilution Factor
Heptachlor Epoxide
< 0.002 mg/L
0.002
0.008 1
Endrin
< 0.002 mg/L
0.002
0.02 1
Chlordane
< 0.01 mg/L
0.01
0.03 1
Toxaphene
< 0.1 mg/L
0.1
0.5 1
Methoxychlor
< 0.002 mg/L
0.002
10.0 1
Heptachlor
< 0.002 mg/L
0.002
0.008 1
Lindane Gamma - BHC
< 0.002 mg/L
0.002
0.4 1
Herbicides - SW-846 8151A
Analyst: Summit Analysis Date: 12/18/14
Parameter Results Det. Limit Reg. Limit Dilution Factor
2,4-D < 5.0 mg/L 5.0 10.0 1
2,4,5-TP (Silvex) < 0.5 mg/L 0.5 1.0 1
I hereby certify that I have reviewed and approve these data. � . a
Laboratory Representative
103
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Client:
Project:
Client Sample ID:
Sample Collection:
Meritech Sample ID:
MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
Kapstone Kraft Paper Corp.
TCLP
Fly Ash
12/09/14
12091497
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 12/12/14
Extracted:
12/10/14
Analyst: VWV
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloro ethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Extraction: 12/15/14
Analysis: 12/20/14 Analyst: PM
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. (� I
Laboratory Representative
104
642 Tamco Road * Reidsville, NC 27320
(3361 342-4748 Ph * (3361 342-1522 Fax

NPDES#: '�.71e" ` 3 1 Chain-
' of Custody Record (CCQ
�a Phone: � 0� -7r7�-G�
Client: �� -,��r��,,;�Avrr a2
MCI� 'NC. DQ�V� A Fax:-
ERITE � Address: /o �
s' iC10S, f✓�Email: '�- t7d� C
ENVIRONMENTAL LABORATORIES
r Project:
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone] Turn Around Time*
Email: [e-mail] Attention: *RUSH work needs prior approval.
How would you like your report sent? sid (io d a -s Da s )a-aR "n
m I Email (preferred), Fax, ail
WW�W.meritech-Iabs.co I t Circle all thatappy: '
Person-rakin s pie (sigq/ rin Lab Use Only
Sampling Dates & Times // ,L !-Y
On ice? pH OK?
Sample Location and/or ID # Start End comp? #of Test(s) Required es No Cl OK?
Date Time . Date Time Grab? Cont. 'r. 1 C
Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0)
Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0)
Benzene (0.5) 1;1-Dichloroethylene (0.7) Pyridine (5.0)
Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0)
Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0)
Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7)
Chlorobenzene (100.0) Heptachlor (and in hydroxide) (0.008) Toxaphene (0.5)
Chloroform (6.0) -Hexachloro-1,3 butadiene (0.5) Trichloroethylene (0.5)
Chromium (5.0) Hexachloroethane (3.0) 2,4,5 Trichlorophenol (400.0
m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2)
Cresol (200.0) Methoxychlor (10.0)
2,4-D (10.0) Methyl ethyl ketone (200.0)
Method of '** Dechlorinat!on (<0.5 ppm) of Ammonia, Cyanide, Ph _. _ - ..._. - Compositor
Comments:
Shipment: Jug #
Q UPS
ed Ex Are these resu for regulatory purposes? Yes No <� Report results' mg/t mg/kg ug/L
Date: Time- r
Relinqu Da e• Time: / E Ya Rec r- Z - `( 16110
Hand Delivery
Received by: Date: Time:
Reli � Date: Tme• .�
Other 2_ y ��/ �615
Date: Time: Re • ed by 1,� ^�' 11 11 er
Relinquished by: I I 6
105

Form PVRF 02T
Fl yash Residuals
Annual Pathogen Reduction Form
�61

. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Kapstone Kraft Paper Corporation
WWTP Name: Roanoke Rapids Mill
Monitoring Period: From 1/1/2014 To
WQ Permit Number: WQ 0021577
NPDES Number: NC 0000752 FA
12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)®
AIt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 13
Heat Drying 0
Heat Treatment ❑
Thermophilic 04
Beta Ray E3
Gamma R❑
Pasteurization [3aY
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑
Composting
Aerobic Digestion El
Anaerobic Di estion
g
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
n; ue
inimurr
Geo. Mean
Maximurr
Unitsd
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
3.2
12.2
0
Annual
Fecal
sm9221 ce
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
E
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench)
Alt. 4 (Spec. OZ uptake)
Alt. 5 (14-Day Aerobic) L3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable)
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed 21
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment." .
Neal R. Davis Environmental Engineer None Applied
Preparer Name a Title (t or print) Land Applier Name and Title (if applicable)(type or print)
v
Signa a of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
107
DENR FORM PVRF 02T (12/2006)

laneAnalytical'
www.pacewacom
November 24, 2014
Neal Davis
Kapstone Kraft Paper Corp.
100 Gaston Road
Roanoke Rapids, NC 27870
RE: Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Dear Neal Davis:
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2014.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. - 108

aceAnalytical
wrnrpacefatucam
I
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Charlotte Certiflcatlon IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. 109

laceAnalytical s
wwwpecefabacom
SAMPLE ANALYTE COUNT
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226/09
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92226109001
FA-1-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226109002
FA-2-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226109003
FA-3-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226109004
FA-4-14
ASTM D2974-87
ACS.
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

laoeAnalytica!®
wwwpaMaba.00m
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
PROJECT NARRATIVE
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Method: SM9221C E (MPN) 503
Description: 92210E Fecal Coliform, MPN RAL
Client: Kapstone Kraft Paper Corp.
Date: November 24, 2014
General Information:
4 samples were analyzed for SM9221C E (MPN) 503. All samples were received in acceptable condition with any exceptions noted
below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: R610/4578
1 g: This is a less than value.
• FA-1-14 (Lab ID: 92226109001)
• Fecal Coliforms, MPN
• FA-2-14 (Lab ID: 92226109002)
• Fecal Coliforms, MPN
• FA-3-14 (Lab ID: 92226109003)
• Fecal Coliforms, MPN
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
111

4
(1-1aneAnalytical e
wwwpacelebsoom
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-1-14 Lab ID: 92226109001 Collected: 11/18/14 08:35 Received: 11/18/1413:25 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results, Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 42.9 % 0.10 1 11/21/14 13:27
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.5 MPN/g 0.018 1 11/18/1416:42 1g
Date: 11/24/2014 04:47 PM'
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
t� I

b
(0-;5neAna1ydca1'
www.pacebUmm
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-2-14 Lab ID: 92226109002 Collected: 11/18/14 08:45 Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Molsture Analytical Method: ASTM D2974-87
Percent Moisture 37.5 % 0.10 1 11/21/14 13:28
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.2 MPN/g 0.018 1 11118/1.4 16:42
Date: 11 /24/2014 04:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1g
- --- -- -113

ti.
aceAnalyiical
www.pocelabl.cort►
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-3-14 Lab ID: 92226109003 Collected: 11/18/14 08:55 Received: 11/18/14 13:20 Marnx: bona
Results reported an a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 44.0 % 0.10 1 11/21/14 13:28
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.6 MPN/g 0.018 1 11/18/14 16:42 lg
Date: 11/24/2014 04:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
114

a
aceAnalytkal'
wwwpecelabs.com
ANALYTICAL RESULTS
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-4-14 Lab ID: 92226109004 Collected: 11/18/14 09:05 Received: 11/18/14 13:25 Matrix: Solid
Results reported on a "dry -weight" bas/s
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 43.3 % 0.10 1 11/21/14 13:28
92210E Fecal Collform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 12.2 MPN/g 0.018 1 11/18/1416:42
Date: 11/24/2014 04:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
115

_,,aceAnalyiical
www.pacelebs.00r0
i
QUALITY CONTROL DATA
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
QC Batch: PMST17259 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92226109001, 92226109002, 92226109003, 92226109004
SAMPLE DUPLICATE: 1334662
92226286001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.0 16.0 0
SAMPLE DUPLICATE: 1334663
92226299002 Cup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.2 15.7 3
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the unite Indicated by tho "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full, 116
Date: 11/24/2014 04:47 PM without the written consent of Pace Analytical Services, Inc..

l�
aceAnalytical
wwwPacelabscom
QUALITY CONTROL DATA
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
QC Batch: RBI0/4578 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92226109001, 92226109002, 92226109003, 92226109004
METHOD BLANK: 1335600 Matrix: Solid
Associated Lab Samples: 92226109001, 92226109002, 92226109003, 92226109004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 11/18/14 16:42
SAMPLE DUPLICATE: 1335601
92226108002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 178 178 0
Paco Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the units indicated by the "Units" column except whore an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, - - 117
Date: 11/24/2014 04:47 PM without the written consent of Pace Analytical Services, Inc..

L-
("
aceAnalytical
"mpaceiabsaom
QUALIFIERS
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
DEFINITIONS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the -reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodlphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroelhylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PAST-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
Date: 11/24/2014 04:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
MC]

b'
aceAnalytical
www.pacelaUmn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CLARIFIER SFECAL 2014
Pace Project No.: 92226109
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92226109001
FA-1-14
ASTM D2974-87
PMSTr7259
92226109002
FA-2-14
ASTM D2974-87
PMST/7259
92226109003
FA-3-14
ASTM D2974-87
PMST/7259
92226109004
FA-4-14
ASTM D2974-87
PMST/7259
92226109001
FA-1-14
SM9221C E (MPN) 503
R1310/4578
92226109002
FA-2-14
SM9221C E (MPN) 503
RB10/4578
92226109003
FA-3-14
SM9221C E (MPN) 503
RB10/4578
92226109004
FA-4-14
SM9221C E (MPN) 503
R1310/4578
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11 /24/2014 04:47 PM without the written consent of Pace Analytical Services, Inc..
119

5,61 Ana�,�lCal
Document Name: Sample Condition Uport
Receipt (SCUM
Document Revised: April 04, 2013
Page I of 2
im"119�:00M
I
Document No..,
P-RAL-C9-001-rev.02
Issuing Authorities:
Pace Asheville Qu4ifty Office
Client Name: 1C�0,
Where Received: [] Huntersville (] Asheville [] Eden Raleigh
Courier (Circle): • Fed Ex UPS USPS Client Commercial . Y�ace Other
Custody Seal on CooledBox Present: ❑ yes ja no Seals intact: 21 yes ❑ no
Packing Material: Bubble Wrap _q—Dab1*AQ9S 6 None Other
Circle Thermometers Used: (R Gun St�+12.2Q86387T o lco: Wet Blue None 0 8110e0 on Ice; cooling process has begun
Temp Correction Factor: Add Subtract", "`V� `
Date and (nitlais o person o amfning
Corrected Cooler Temp.: C
Biological Tissue to Frozen: Yet No A
check n lereat t t
Temp. should be above freezing to WO
Comments:
Chain of Custody Present:.
Yea Me •
OwA
t.
Chain of Custody Filled Out;'
es Me
OM,
2. '
Chain of Custody Relinquished:
ONo.
ONrA
3.
Sampler Name & Si nature on COC.'
Yea CINo,
1314
4,.
Samples Arrived within Hold 11me:
Yee CINo
13MA
6.
Short Hold The Anal Is' <72hr i
es [it o.
OM
Rush Turn Around Time R uested:
Oyes JeNo
OwA
7,
Suff1clont Volume;
j6yot ❑ i,
OwA
8.
Correct Containers Used:
Yew ONo
OWA
9. '
-Pace Containers Used;
Yea. Oft
dwh
Containers Intact:
bYos. ONo
E30JA
10. '
Flltared volume�recelved for Dissolved tests:
Met ONo
�fWA
11.
Sample Labels match COC:
Yea No
❑wA
12.
-includes datoAlmeAD/Analyals; Matrix:.
Aitcontalnore needing preservatlan have heen checked.
Jf iYes ONo
Own
13.
All contelners needing preservatfon are found to be In
VYea ONo
EIN1A
compliance with EPA' recommendation.
f'
oxce done: VOA, 0Ywm.T0C.6M W1-OR0 atar
4ee ONO;
r
Sam les cheoked for dechlorination:
Yes OIVo
MA
14.
Heads ace In VOAAAals. 56rrtrrt :
❑Yea 13No
WA
16.
Trip Blank Present:
clYei E1No
5WA
16,
Trip Blank Custody Seals Present
C1yae ONO
41A
Pace Trip Blank Lot # 11 urchased .
Client Notification/ Resolution: Plow Data Required? Y ! N
Person Contacted; Datamme:
Commen{sl Resolutlont:
SCURF l9RF Date: tt- t�3-►�1 eN•!v 'Iuu
�,
-1 tl`�lU �l • - •.im'.+�, 5.: .•a31„q,?zriis-.I�'re:fx."
Nate: Whenever there is a discrepancy affeoUng North C&dlnacomplianco IIII�IIII�1111111 II 'rt'L ssw'f {s ° Y`l 4. `t x=s s = ?r <<
p y f Il.:.• �:f . y..yx �•.•�.:r.
samples, a copy of this form will be sent to the North Carolina DEHNR 9222610�3'
ortif eation•Office • I.a out of hoid incorrect proaervative, out Of (emp,
C t inoorr6d oontatriere) t

ro.
Chain of Custody
a
a
Report Results to:
Bill Results ta:
�tandard
Kapsione Paper
100 Gaston Rd
Report Delivery
0 Rush Report Devery (w%surcharge)
Roanoke Rapids, Nc •
ReQuest6d Dde Datw.
AT7N: Neal Davis
A7TN:
Project Ref@mnce: Oaaifier Fecal Analysis Nov. 2014
Phone: 2S2-533-6295
Purchase Order#:'
Sampled By:
I
121

aceAnalydcal'
WW'PaceraUmv
November 26, 2014
Neal Davis
Kapstone Kraft Paper Corp.
100 Gaston Road
Roanoke Rapids, NC 27870
RE: Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Dear Neal Davis:
Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2014.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
V�t cll . C-P4, - J L-,b--
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
_ 122

aceAnalytical
w�aropecele(uoorn
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Charlotte Certiflcatton IDs
9800 Kincey Ave. Ste 100, Nuntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, 123
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.
6701 Conference Drive
aceAnalytical Raleigh, NC 27607
wwc (919)834-49e4
SAMPLE ANALYTE COUNT
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Lab ID
Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92226602001
FA-5-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226602002
FA-6-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226602003
FA-7-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92226602004
FA-8-14
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
124

laneiAnalytical
wwwpecetatum"
PROJECT NARRATIVE
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Method: SM9221C E (MPN) 503
Description: 92210E Fecal Coliform, MPN RAL
Client: Kapstone Kraft Paper Corp.
Date: November 26, 2014
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
General Information:
4 samples were analyzed for SM9221C E (MPN) 503. All samples were received in acceptable condition with any exceptions noted
below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the. report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: RBI0/4588
1g: This is a less than value.
• FA-5-14 (Lab ID: 92226602001)
• Fecal Coliforms, MPN
• FA-7-14 (Lab ID: 92226602003)
• Fecal Coliforms, MPN
• FA-8-14 (Lab ID: 92226602004)
• Fecal Coliforms, MPN
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. 125

laceAnalyfical'
wwwpawabacm
ANALYTICAL RESULTS
Project Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-5-14 Lab ID: 92226602001 Collected: 11/20/14 10:10 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry-welght" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 42.1 % 0.10 1 11/25/1413:18
92210E Fecal Collform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.5 MPN/g 0.018 1 11/21/14 08:43 1g
Date: 11/26/2014 10:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
- -126

aceAnalytical'
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Sample: FA-6-14 Lab ID: 92226602002 Collected: 11/20/14 10:20 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 42.3 % 0.10 1 11/25/14 13:19
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.5 MPN/g 0.018 1 11/21/14 08:43
Date: 11/26/2014 10:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
-127

aceAnalytical
www.pamlaba.com
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: FA-7-14 Lab ID: 92226602003 Collected: 11/20/14 10:30 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 53.2 % 0.10 1 11/25/14 13:19
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 4.3 MPN/g 0.018 1 11/21/14 08:43
Date: 11/26/2014 10:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1g
Qual
_128

GIUMnalytical
ffimpacehftcom
ANALYTICAL RESULTS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Sample: FA-8-14 Lab ID: 92226602004 Collected: 11/20/14 10:40 Received: 11/20/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 47.0 % 0.10 1 11/25/14 13:19
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.8 MPN/g 0.018 1 11/21/14 08:43 1g
Date: 11/26/2014 10:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
- - 129

aceAnalyt¢ical e
wwwpacelaDstxun
QUALITY CONTROL DATA
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
QC Batch: PMST/7272 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92226602001, 92226602002, 92226602003, 92226602004
SAMPLE DUPLICATE: 1336870
92226473001 Dup
Parameter Units Result Result - RPD Qualifiers
Percent Moisture % 14.0 11.7 18
SAMPLE DUPLICATE: 1336871
Parameter Units
Percent Moisture %
92226677002 Dup
Result Result
17.1 16.5
RPD Qualifers
3
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this pogo are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /26/2014 10:56 AM without the written consent of Pace Analytical Services, Inc..
130

r � x
NeAnalytical
wwwpacela0scom
QUALITY CONTROL DATA
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
QC Batch: RBIO/4588 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92226602001, 92226602002, 92226602003, 92226602004
METHOD BLANK: 1336835 Matrix: Solid
Associated Lab Samples: 92226602001, 92226602002, 92226602003, 92226602004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifers
Fecal Coliforms, MPN MPN/g ND 0.018 11/21/14 08:43
SAMPLE DUPLICATE: 1336836
92226604002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 35.1 17.5 67
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to tho right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /26/2014 10:56 AM without the written consent of Pace Analytical Services, Inc..
--- - - 131

t
Pace Analytical Services, Inc.
aceAnalytical ® 6701 Conference Drive
Raleigh, NC 27607
++rpac®IaDscam
[phone]
QUALIFIERS
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitatlon Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full, 132
Date: 11/28/2014 10:58 AM without the written consent of Pace Analytical Services, Inc..

4 w
i
aceAnalytical
H+rntpa wftcarrr
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Clarifier Fecal - Nov 2014
Pace Project No.: 92226602
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92226602001
FA-5-14
ASTM D2974-87
PMST/7272
92226602002
FA-6-14
ASTM D2974-87
PMST/7272
92226602003
FA-7-14
ASTM D2974-87
PMST/7272
92226602004
FA-8-14
ASTM D2974-87
PMST/7272
92226602001
FA-5-14
SM9221C E (MPN) 503
RB10/4588
92226602002
FA-6-14
SM9221C E (MPN) 503
RBIO/4588
92226602003
FA-7-14
SM9221C E (MPN) 503
RBIO/4588
92226602004
FA-8-14
SM9221C E (MPN) 503
RB10/4588
Date: 11/26/2014 10:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
133

Document Name: Sample Condition Upon
Document Revised: April 04, 2013
r „ aCBAnalytlCat'
Rece(t (SCUR)
Page 1 of t
Document No.:
Issuing Authorities:
'
F•RAL-CS-001-rev,02
Pace Asheville Quality Oface
►lent Name: Y.a. p11ni
Whore Recelvod: 0 Huntersville [] Asheville [( Eden Raleigh
Courler(Circlo): • Fed Ex UPS- USPS Client • Commercial Pow Other
Custody Seal on Coolor/Box Present: yes 12f no Seals Intact ,6 yes [] no
Packing Material: Bubble Wrap Bubb a Bags � None Other
Circle Thermometer Used. iR Gun 1 208B38 pe of Ice: Wot Blue None [� Samples on ioe, 000ling process has begun
IR Gun Back U�12200e3it
Temp Correction Factor. Add ! uhtrac �'
Corrected Cooler Temp.; C
Temp should be above freezing to WC
D C
Biological Tissue is Frozen: Yes No WA
Comments:
Date and Initials of parson oxamint g
CO L `Isla r U
Chock:
1
Chdin of Custody Presentr
CWes I7No • 17WA
1,
Chain of Custod Filled Out:
Yps ONo
ptUA
2.
Chain of Custod • Relinquished:
Yoe ONo
❑N/A
3.
Sampler Name& Signature on CO C:
vos ON.
❑WA
4..
Samples Arrived within Hold Time:
R(vw ON.
❑NIA
S..
Short Hold Time Analysts {72hr :
Y, LIN.
❑WA
6.
Rush Turn Around Time Requested:
OYea o
❑NIA
7.
Sufficient Volume:
W., ON,
QNA
8.
Correct Containers Used:
-pace Containers Used:
Yea [IN*
th, ON,
DIVA
C1NrA
g,
Containers Intact:
Yea ON'&
E71,11A
10.
Filtered volume•recelved for Dissolved tests
❑yes ONO
wA
it,
Sample t.abole match COC:
-Includes datoltime/ID/Anal sis Matrix
f%JYos. Qo
❑WA
12.
All containera needing preservation have been checked.
All contalners needing preservation are found to be in
compliance with EPA recommendation.
oXceptionst VOA, @ollform, Too, 03Q; MORO (water)
, w� []No
Yee ONo
Yw ❑NO
L7WA
TWA
13.
Samples checked for dechlotlnatlon:
6Yes ❑No
❑WA
14;
Hoads arcs In VOA Vials 4mrn :
13Yoe' ONO
&A
15;
Trip Blank Present:
Trip Blank Custody Seals Present
Pace TripBlank Loot (I purchased):
IYoe ❑IVo
❑Yos t7No
WA
f�WA
`
10,
Client Notification/ Resolution: F1eid Data Required? Y I N
Person Contacted: DYatoMme:
Comments/ Resolution:
SCURF•/SRF `u Date:
Review:: (� 1• .
Note: Whenever there is a discrepancy affecting North Carolina rompllanco
samples, a copy of, this form vAll be sent to the North Carolina ❑EHNR
Certiticauon office( 1.9 out of hold, incorrect preeebvedve, out of temp,
incorrect containers)
��922z66o�
v�,ev
I II IIIIII II
�r
134

Report Results to:
Kapstone Paper
100 Gaston Rd
Roanoke Rapids, NC
ATTN: Neal Davis
Phone: [phone]
o.
Q
Chain of Custody
NOT Results to:
vj Standard Report Delivery
Rush Report Delivery (w/ surcharge)
Requested Due Date:
Project,Referenm Clarifier fecal Anatysis-Nov. 2014
Purchase order fi:
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