WQ0020239_Residual Annual Report 2014_20150306

cFW
MAR 0 6 2015
TOWN OF HERTFORD
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
CLASS B PROGRAM
WQ0020239
Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858
February 9, 2015
a�

February 9, 2015
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Town of Hertford "Class B" Program
NC Permit No.: WQ0020239
Soil Plus Project No. 200802.A10
Information Processing Unit:
Soil Plus,. LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Hertford on behalf of Atlantic
Sewage Control. Soil Plus compiled this report using data gathered during the compliance
year. This data includes (1) certification form, (2) residual sampling, (3) field loading
calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil
fertility nutrient analysis.
The Town of Hertford conducted application events on permitted fields in Perquimans
County during 2014. A total of 30.09 Dry Tons or 220,000 gallons of permitted residual
bio-solids were land applied to permitted fields.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Town of Hertford (252-426-8182) for further
assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
Charles Jones, Town of Hertford
J. Bryan Smith, Granville Farms
208 Williams St.
Greenville, NC 27858
t [phone]
f [phone]
www.soilplus.net

Town of Hertford
2014 Annual Land
Application of
Residual Bio-Solids
Report
WQ0020239
Hertford, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Loading Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Nutrient Analysis
503 Metal Analysis
TCLP
FIELD LOADING
SUMMARY FORM
Nixon Farm
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
SOIL SAMPLES

APPENDIX -I
CERTIFICATION FORM
SUMMARY FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0020239 Town of Hertford Atlantic Sewage Control Perquimans [phone]
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 12
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied. during the -year for all application sites: 30.09
Total number of acres utilizes for land application during the year: 27.6
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑d ❑❑
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
?. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
t. Annual TCLP analysis '(if required) was performed and three (3) copies of certified laboratory results are attached
i. All other monitoring was performed in accordance with the pen -nit and reported during the year as required and three (3) copies of
zertified laboratory results are attached
S.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit
3. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilitie
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
-nclude appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
?art C - Certification:
'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
:omplete. I am'aware that there are significant penalties for submitting false information, including the possibility of fines and
mprisonment for knowing violations."
3randon Shoaf
Pe Name�nd 1. tie (type or print):
(�/t 1 2-27 , 15-
>i ature of Preparer* Date
if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
" Monday, February 9, 2015
Signature of Permittee
February 9, 2015
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
WW I P, 4olurneApplied. Total Dry Toris-
r -
l`, Town of Hertford WWTP 220,000 30.09
Total 220,000 30.09
Monday, February 9, 2015 Page 1 of 1

Site# 2
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 27.6 220,000 30.09 32.99 Common 220 15.0% Annual Ryegrass -
Bermudagrass Pasture
Total 220,000 30.09
50
Monday, February 9, 2015 Page 1 of 1

APPENDIX II
RESIDUAL SAMPLING SUMMARY FORM
FIELD LOADING CALCULATIONS
ANALYTICAL

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0020239 Facility Name Town of Hertford Source Permit No. NCO021849
Laboratory 1 A&L Eastem
Labs, Inc.
Laboratory 2
Sample or CompositeDate 4/24/2014
Parameter (mg/Yg) Class A Clas B
Aluminum
N/A
N/A
12,600
Ammonia Nitrogen
N/A
N/A
2,440
Arsenic
41
75
9
Cadmium
39
85
3
Calcium
N/A
N/A
26,600
Copper
1,500
4,300
366
Lead
300
840
36
Magnesium
N/A
N/A
2,430
Mercury
17
57
0.7
Molybdenum
N/A
75
5
Nickel
420
420
25
Nitrate -Nitrite Nitrogen
N/A
N/A
543
Percent Solids
N/A
N/A
3.28
pH (no units)
N/A
N/A
7.14
Phosphorus
N/A
N/A
20,500
Potassium
N/A
N/A
2,060
PAN (Inj./Inc.)
N/A
N/A
16,351
PAN (Surface)
N/A
N/A
15,131
Selenium
100
100
7
Sodium
N/A
N/A
2,570
SAR
N/A
N/A
0.73
Total Nitrogen
N/A
N/A
47,000
Zinc
2,800
7,500
1180
Source Name Town of Hertford W WTP
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitt' se information, including the possibility of fines and imprisonment for knowing violations."
nature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ADMAN
Facility Town of Hertford WWI?
Sampling Date 4/24/2014
% Solids 3.28
Mineralization Rate 0.30
FIELD LOADING ESTIMATES
Gallons per DT 7,311.22
PH 7.14
Sodium Absorpotion 0.73 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 47,000 lbs./1,000 gal 12.86 Potassium lbs./1,000 gal 0.56
Ammonia Nitrogen (mg/Kg) 2,440.00 lbs./1,000 gal 0.67 Phosphorus lbs./1,000 gal 5.61
Nitrate -Nitrite (mg/Kg) 543.00 lbs./1,000 gal 0.15 Calcium lbs./1,000 gal 7.28
PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.66
PAN (mg/Kg) 15,131 lbs./1,000 gal 4.14 Manganese lbs./1,000 gal 0.51
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal 2.30
PAN (mg/Kg) 16,351 lbs./1,000 gal 4.47 _ Molybdenum lbs./1,000 gal 0.00
Volatization Rate= 0.5 Surface Application -
1.0 Injection/Incorporation
EPA METAL LIMITS
1st Yeat
2nd Year
3rd Year
4th Year
y '5th Year
i
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
9.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
3.00
Cadmium lbs./1,000 gal
0.06
Copper (mg/Kg)
366.00
Copper lbs./1,000 gal
0.10
Lead (mg/Kg)
36.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.70
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
25.00
Nickel lbs./1,000 gal,
0.01
Selenium (mg/Kg)
7.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1180.00
Zinc lbs./1,000 gal
0.32
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TEN
PAN PAN
Nitrogen
TKN
PAN
PAN
Nitrogen
(mg/kg) (lbs/D'I)
(mg/Kg)
(mg/kg) (lbs/DT)
(mg/Kg)
47,000
15,131 30.26
31,869
47,000
16,351
32.70
30,649
31,869
4,780 9.56
27,089
30,649
4,597
9.19
26,052
27,089
2,032 4.06
25,057
26,052
1,954
3.91
24,098
25,057
940 1.88
24,117
24,098
904
1.81
23,194
24,117
452 0.90
23,665
23,194
435
0.87
22,759
Total 23,335 46.67
Total 24,241 48.48
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/K& 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

Page: 1 of 2
Report Number: 14-118-0204
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 55052
Sample Id : TH042414
IROM A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: 200802.A10-TOWN OF HERTFORD WWTP
NC CERT#257
REPORT OF ANALYSIS
Total Solids
3.28
32800
100.0
JM
Moisture *
96.72
100.0
JM
Total Kjeldahl Nitrogen
4.70
47000
10.0
JM
Total Phosphorus
2.05
20500
100
KM
Total Potassium
0.21
2060
100
KM
Total Sulfur
0.84
8410
100
KM
Total Calcium
2.66
26600
100
KM
Total Magnesium
0.24
2430
100
KM
Total Sodium
0.26
2570
100
KM
Total Iron
51000
100
KM
Total Aluminum
12600
100
KM
Total Manganese
1880
5
KM
Total Copper
366
5
KM
Total Zinc
1180
5
KM
Ammonia Nitrogen
0.24
2440
10.0
JM
Organic N
4.46
44560
10.0
Nitrate+Nitrite-N
543
2.00
JM
Total Cadmium
3.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Date Sampled: 4/24/2014 11:00:00
Date Received: 04/28/2014 00:00
Date Reported: 04/30/2014
04/28/2014 13:59
04/28/2014 13:59
04/29/2014 08:44
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 13:20
04/29/2014 08:44
04/29/2014 08:44
04/29/2014 08:45
04/29/2014 13:20
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C

Page: 2 of 2
Report Number: 14-118-0204
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 55052
Sample Id : TH042414
AL A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Project: 200802.A10-TOWN OF HERTFORD-WWTP
NC CERT#257
REPORT OF ANALYSIS
Total Chromium
48
5
Total Nickel
25
5
Total Lead
36
5
Total Arsenic
9.0
3.0
Total Mercury
0.7
0.4
Total Selenium
7.0
5.0
pH (Standard Units) "
7.14
2.00
Total Molybdenum
5
5
Soluble Phosphorus
0.02 200
100
Comments:
WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. J
Date Sampled: 4/24/2014 11:00:00
Date Received: 04/28/2014 00:00
Date Reported: 04/30/2014
KM
04/29/2014 13:20
SW 6010C
KM
04/29/2014 13:20
SW 6010C
KM
04/29/2014 13:20
SW 6010C
KM
04/29/2014 13:20
SW 6010C
KM
04/29/2014 09:00
SW-7471 B
KM
04/29/2014 13:20
SW 6010C
JM
04/29/2014 08:44
SW-9045D
KM
04/29/2014 13:20
SW 6010C
JM
04/29/2014 10:39
SOLUBLE P IN MANURE
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

(5)MI ' Microbac Laboratories, Inc. - Wilson Division
3809 Airport Drive NW
Wilson, NC 27896
Tel: [phone]
CERTIFICATE OF ANALYSIS Report Date: 2014/05/15
C.:
SIDN Client Marks
AA47537
Town of Hertford
AA47537
Town of Hertford
AA47537
Town of Hertford
AA47537
Town of Hertford
AA47537
Town of Hertford
Comments:
Quote: 23-20140328-14
Work Order: 2014-04-25-007
Matrix: Sludge
Collection Date: 2014/04/25
Sample Submission Date: 2014/04/25
Analysis Name Method
Flash Point - LiquidsSubcontracted
pH (Corrosivity) Subcontracted
Reactive Cyanide Subcontracted
Reactive Sulfide Subcontracted
TCLP Full Metals V(Subcontracted
Approved by:
Kim Hesse
`.
Result Unit
*See Attached
*See Attached
*See Attached
*See Attached
*See Attached
For any feedback concerning our services, please contact James Nokes, Senior Vice President, at [e-mail]
. ' or Trevor Boyce at [e-mail]
C Environmental • Agrochemical 9 Food • 'P.harmaceuticals Page 1 of 1

° Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 i Nashville; TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY - FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1407445 Project: Soil Sampling
Date Reported: 5/15/2014
Date Received: 4/30/2014
Cust #: R9024
Po#:
Analyte Result Units Dil Qualifier ReportingLimit Analyst Analyzed Method
AA47537 Sampled: 04/29/2014 00:00
1407445-01 (Solid)
Wet Chemistry
Analyzed By: Microbac Knoxville Division
pH (Corrosivity) 7.3 pH Units 1 H4 SLN 65/05/2014 16:15 SW846 9045D
General Chemistry
Analyzed By: Microbac Knoxville Division
TCLP Extraction Fluid 1 1 JNB 05/02/2014 10:41 SW846 1311
TCLP Metals by 6000/7000 Series Methods
Analvzed Bv: Microbac Knoxville Division
Arsenic
0.0157
mg/L
1
0.0150
JNB
05/02/2014 18:30
SW846 6010E
Cadmium
ND
mg/L
1
0.00750
JNB
05/02/2014 18:30
SW846 6010B
Chromium
ND
mg/L
1
0.00750
JNB
05/02/2014 18:30
SW846601oB
Mercury
ND
mg/L
1
0.000200
JNB
05/05/2014 15:00
SW846 7470A
Selenium
ND
mg/L
1
0.0200
JNB
05/02/2014 18:30
SW846 6010B
Silver
0.00170
mg/L
1 B
0.00100
JNB
05/02/2014 18:30
SW846 6010B
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
4,4'-DDD
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
4,4'-DDE
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
4,4'-DDT
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Aldrin
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
alpha-BHC
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
beta-BHC
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Chlordane
ND
ug/L
1
U
10.0
ECL
05/09/2014 18:17
SW8081A
delta-BHC
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Dieldrin
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Endosulfan I
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
' Endosulfan II
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Endosulfan sulfate
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Endrin
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
Endrin aldehyde
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
gamma-BHC (Lindane)
ND
ug/L
1
U
0.500
ECL
05/d9/2014.18:17
SW8081A
Heptachlor
ND
ug/L
1
U
0.500
ECL
05/09/2014 18:17
SW8081A
The data and information on this,
and other accompanying documents,
represent only the sample(s)
analyzed and is rendered upon
condition
MEMBER
' that it is not to be reproduced wholly or in part for advertising
or other purposes without approval from the laboratory.
USDA-EPA-NIOSH
Testing Food Sanitation Consulting
Chemical and Microbiological Analyses and Research
Page 1 of 6
www.microbac.com
[e-mail]
i"

Microbac Laboratories, Inc.
Knoxville Division
• . 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY: CONSUMER PRODUCTS -WATER -AIR • WASTES - FOOD - PHARMACEUTICALS • NUTRACEUTICALS
\ y
i. CERTIFICATE OF ANALYSIS
r Kimberly Hesse Date Reported: 5/15/2014
- Microbac Laboratories, Inc. - Wilson Date Received: 4/30/2014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 Po#:
Workorder: 1407445 Project: Soil Sampling
Analyte Result Units Dil Qualifier ReportingLimit Analyst Analyzed Method
AA47537 Sampled: 04/29/2014 00:00
1407445-01 (Solid)
Heptachlor epoxide ND ug/L 1 U 0.500 ECL 05/09/2014 18:17 SW8081A
Methoxychlor ND ug/L 1 U 0.500 ECL 05/091201418:17 SW8081A
Toxaphene ND ug/L 1 U 10.0 ECL 05/09/2014 18:17 SW8081A
Surrogate: 2,4,5,6-7etrach1oro-m-xy1ene
20-180
44.9 %
05/09/2014 18:17
SW8081A
Surrogate: Decachlorobiphenyl
25-140
35.7 %
05/09/2014 18:17
SW8081A
8270 TC
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
1,4-Dichlorobenzene
ND
ug/L
1
U
50.0
CAA
05/091201415:52
SW8270C
2,4,5-Trichlorophenol
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
2,4,6-Trichlorophenol
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
2,4-Dinitrotoluene
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
o-Cresol
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
m-,p-Cresol
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
Hexachlorobenzene
ND
ug/L
1
U
50.0
CAA
05109/201415:52
SW8270C
Hexachlorobutadiene
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
` Hexachloroethane
ND
ug/L
1
U
50.0
CAA
05/09/2014 15:52
SW8270C
Nitrobenzene
ND
ug/L
1
U
50.0
CAA
o5/09/2ol415:52
SW8270C
Pentachlorophenol
ND
ug/L
1
U
250
CAA
06/09/201415:52
SW8270C
Pyridine
ND
ug/L
1
U
250
CAA
05/09/2014 15:52
SW8270C
Surrogate: 2-Fluorophenol
21-100
39.3 %
05/09/2014 15:52
SW8270C
Surrogate: Phenol-d5
10-94
26.9 %
05/09/2014 15:52
SW8270C
Surrogate: Nitrobenzene-d5
35-114
79.1 %
05/09/2014 15:52
SW8270C
Surrogate: 2-Fluorobiphenyl
- 43-116
80.5 %
05/09/2014 15:52
SW8270C
Surrogate: 2,4,6-Tribromophenol
10-123
52.0 %
05/09/2014 15:52
SW8270C
l Surrogate: p-Terphenyl-d14
33-141
46.6 %
05/09/2014 15:52
SW8270C
- The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition MEMBER
(rY� that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
`-. USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research iii:d>r�
r4 �
Page 2 of 6
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
tenness ee@microbac. com
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS WATER AIR WASTES FOOD • PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Date Reported: 5/15/2014
Microbac Laboratories, Inc. - Wilson
Date Received: 4/30/2014
3809 Airport Drive
cust M R9024
Wilson, NC 27896
Po#:
Workorder: 1407445 Project: Soil Sampling
Reporting
Analyte Result Units Dil Qualifier Limit Analyst Analyzed Method
AA47537 Sampled: 04/29/2014 00:00
1407445-01 (Solid)
herbicides
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
2,4,5-T
ND
ug/L
1
U
2.00
ECL
05/12/2014 13:20
SW8151A
2,4,5-TP (Silvex)
ND
ug/L
1
U
2.00
ECL
05/12/2014 13:20
SW8151A
2,4-D
ND
ug/L
1
U
20.0
ECL
05/12/2014 13:20
SW8151A
2,4-DB
ND
ug/L
1
U
20.0
ECL
05/12/2014 13:20
SW8151A
Dinoseb
ND
ug/L
1
U
10.0
ECL
05/12/2014 13:20
SW8151A
Dalapon
ND
ug/L
1
U
50.0
ECL
05112/201413:20
SW8151A
Dicamba
ND
ug/L
1
U
2.00
ECL
05/12/2014 13:20
SW8151A
Dichloroprop
ND
ug/L
1
U
20.0
ECL
05/12/2014 13:20
SW8151A
MCPA
ND
ug/L
1
U
2500
ECL
05/12/2014 13:20
SW8151A
MCPP
ND
ug/L
1
U
2500
ECL
05/12/2014 13:20
SW8151A
Pentachlorophenol
ND
ug/L
1
U
2.00
ECL
05/12/2014 13:20
SW8151A
Surrogate: 2,4-Dichlorophenylacetic acid
20-144
66.9 %
05/12/2014 13:20
SW8151A
/
GCMS Volatiles
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
1,1-Dichloroethene
ND
mg/L
10
0.050
jln
05/13/201413:38
1311/8260B
1,2-Dichloroethane
ND
mg/L
10
0.050
jln
05/13/2014 13:38
1311/8260B
2-Butanone
ND
mg/L
10
0.10
jln
05/13/2014 13:38
1311/8260B
Benzene.
ND
mg/L
10
0.050
jln
05/13/2014 13:38
1311/8260B
Carbon tetrachloride
ND
mg/L
10
0.050
jln
05/13/2014 13:38
1311/8260B
Chlorobenzene
ND
mg/L
10
0.050
jln
05113/201413:38
1311/8260B
Chloroform
ND
mg/L
10
0.050
jln
05/13/2014 13:38
1311/8260B
I' Tetrachloroethene
ND
mg/L
10
0.050
jln
05/13/2014 13:38
1311/8260B
Trichloroethene
ND
mg/L
10.
0.050
jln
05/13/2014 13:38
1311/8260B
Vinyl chloride
ND
mg/L
10
0.020
jin
05/13/2014 13:38
1311/8260B
1,4-Dichlorobenzene
ND
mg/L
10
0.10
jln
05/13/2014 13:38
1311/8260B
Surrogate: 1,2-Dichloroethane-d4
74.5-132
97.5 %
05/13/2014 13:38
131118260B
Surrogate: 4-Bromofluorobenzene
80-120
92.1 %
05/13/2014 13:38
131118260E
Surrogate: Dibromofluoromethane
80-120
100 %
05/13/2014 13:38
131118260E
Surrogate: Toluene -dB
80-120
95.9 %
05/13/2014 13:38
131118260E
The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition
that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research
www.microbac.com [e-mail]
MEMBER
Page 3 of 6

° Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
tennessee@microbac. com
CHEMISTRY • MICROBIOLOGY - FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 5/15/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/30/2014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 PO#:
Workorder: 1407445 Project: Soil Sampling
Reporting
Analyte Result Units Dil Qualifier Limit Analyst Analyzed Method
AA47537 Sampled: 04/29/2014 00:00
1407445-01 (Solid)
Wet Chemistry
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
Ignitability > °F 1 30 EB 05/08/2014 10:10 ASTM D92-90
MOD
Reactive Sulfide ND mg/Kg 1 2.0 EB 05/05/2014 10:20 Chapter 7/9034
AA47537 Sampled: 04/29/2014 00:00
1407445-01 RE1 (Solid)
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Barium 0.173 mg/L 1
0.00400 JNB 05/05/2014 16:09 SW846 6010B
Lead 0.0212 mg/L 1
0.0200 JNB 05/05/2014 16:09 SW846 601OB
Wet Chemistry
Analyzed By: Microbac Laboratories, Inc. - Chicagoland
Reactive Cyanide ND mg/Kg 10
20 AGRIE 05/06/2014 13:24 Chapter 7/9014
Ii
The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition MEMBER
that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research Li1:1.i�
www.microbac.com [e-mail]
Page 4 of 6

r
Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
tennessee@microbac. corn
CHEMISTRY • MICROBIOLOGY - FOOD SAFETY - CONSUMER PRODUCTS -WATER • AIR - WASTES - FOOD • PHARMACEUTICALS - NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1407445 Project: Soil Sampling
Certifications
Date Reported: 5/15/2014
Date Received: 4/30/2014
oust #: R9024
PO#:
Code
Description
Number
Expires
A2LA
A2LA ISO/IEC 17025 Env. DoD Testing
3045.02
09/30/2014
A2LA_
A2LA ISO/IEC 17025 Biological Testing
3045.01
09/30/2014
A2LAB-KNX
ISO 17025 KNX food
3131.01
05/31/2015
A2LAB-NSH
ISO 17025 NSH food
3131.02
06/30/2014
FL
State of Florida NELAC
E87966
06/30/2014
GA
Georgia Dept Natural Resources
980
04/13/2014
ILDPH
Illinois DOPH Micro analysis of drinking water
1755266
12/31/2016
ILEPA
Illinois EPA wastewater and solid waste analysis
200064
04/01/2015
INDEM
Indiana DEM support lab wastewater and solid waste
A305-9-292
12/31/2013
INDH
Indiana SDH Micro analysis of drinking water
M-45-8
12/31/2016
INSDH
Indiana SDH chemical analysis of drinking water
C-45-03
08/14/2016
KSDOH
Kansas Dept Health & Env. NELAP
E-10397
01/31/2015
KYEPP
Kentucky EPPC analysis Underground Storage Tanks
75
01/31/2015
NCENV
NC Environmental
678
12/31/2014
NYDOH
New York State Department of Health Wadsworth
49179
04/01/2015
NYDOH-1
New York State Department of Health Wadsworth
49386
04/01/2015
PADEP
Pennsylvania Department of Environmental Protect
68-04863
07/31/2014
PEDEP
Pennsylvania DEP Registration for Air analysis
68-04863
TN_DW
North Carolina DENR NPDES effluent, surface water
TNNC597
12/31/2014
TN_DW
State of Tennessee
TN02017
04/30/2017
USDA
US Department of Agriculture
12/31/2014
USDAS
USDA Permit To Receive Soil
P330-12-00174
06/20/2015
WADOE
Washington State Department of Ecology
C992
10/22/2014
WSDNR
Wisconsin DRN chemical analysis wastewater, solids
998036710
08/31/2014
The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition MEMBER
that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research Li'►r�.l�
Page 5 of 6
i
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 . I Nashville, TN 615.242.1480
www.microbac.com
tennessee@microbac. com
CHEMISTRY - MICROBIOLOGY - FOOD SAFETY - CONSUMER PRODUCTS -WATER • AIR - WASTES - FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson„ NC 27896
Workorder: 1407445 Project: Soil Sampling
Notes and Definitions
U Not detected at or above adjusted sample detection limit
R1 Duplicate RPD is outside of acceptance limits.
M2 Matrix spike recovery is outside of acceptance limits, biased low.
M1 Matrix spike recovery is outside of acceptance limits, biased high.
Date Reported: 5/15/2014
Date Received: 4/30/2014
Cust #: R9024
PO#:
J [Undefined]'
H4 The test was performed outside of the EPA recommended holding time of 15 minutes.
B Target analyte is detected in the method blank at or above method criteria. Sample result is greater than 10 times amount
found in blanks. Blank hit is insignificant to reported result.
1
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
RPD Relative Percent Difference
Microbac Laboratories, Inc. - Knoxville
cvm�LY}r'��
Maraea Branner, Project Manager
Thank you for your business. For any feedback, please contact Ashley Morris, at [e-mail]. You may also contact Trevor Boyce,
I President, at [e-mail].
As regulatory limits change frequently, Microbac advises the recipient of this report'to confirm such limits with the appropriate Federal, state, or local
authorities before acting in reliance on the regulatory limits provided.
The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition
that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research
www.microbac.com [e-mail]
MEMBER
Page 6 of 6

1407445-01
Sampled: 04/29/2014 00:00
r"
Microbac Laboratories,
Inc. -Wilson
--
Illllllllllllllllllllll�llllll�llldllllllllllll�lllllllllllll
i
Yr
COOLER INSPECTIOP
-'
Client Name: tryr)[',� c- �e. v)
Date/Time Received:
-4 /�o 11-f
����Work
•
Order:
No. of Samples:
f
Received By: ( /;/1 1
Checklist Completed By:j /
Carrier: FedEx(_) UPS Client(_) Field
Services(_) Other(:
After -Hours Receipt?
Yes ❑
No ,2'
Shipping container in good condition?
Yes 0'-`
No ❑ Not Present ❑
_
Custody seals intact on cooler?
Yes ❑
No ❑ Not Present-P-
Custody seals intact on samples?
Yes ❑
No ❑ Not Present CQ'-
Chain of custody present?
Yes ❑
N6-J21
Chain of custody includes proper client information?
Yes ❑
No 2
Chain of custody includes proper collection information and signatures? Yes ❑
No .E
Chain of custody includes dates and times of sample collection?
Yes ❑
No 0'
Chain of custody includes proper sample descriptions?
Yes ❑
No 41--
Chain of custody agrees with sample labels?
Yes ❑
No ,2-
Chain of custody identifies proper sample matrix?
Yes ❑
No ,,9
Chain of custody identifies proper number of samples?
Yes ❑
No .E'
Chain of custody includes required analysis?
Yes ❑
No 13-
Chain of custody signed when relinquished and received?
Yes ❑
No -ET
Samples are in proper containers/bottles?
Yes 21
No ❑
Sample containers are intact?
Yes J
No ❑
Sufficient sample volume collected for requested analysis?
Yes ,12'
No ❑
VOA vials for aqueous samples have zero headspace?
Yes ❑
No ❑ Not Presen�
Samples received within holding times?
Yes ' ❑
No ❑
Samples received on ice?
Yes A'
No ❑
Sample properly preserved?
Yes -0�-
No ❑
If No, adjusted by?
Date/Time:
Remarks:
ANY "NO" EVALUATION REQUIRES CLIENT NOTIFICATION (excluding After -Hours Receipt).
Comments:
Effective Date: 05/05/11 F:\shared files\Forms\Cooler Inspection Form #10001.1.pdf Page 1 of 1

APPENDIX III
FIELD LOADING SUMMARY FORM

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0020239
Site# 2 County Pcryuimans
Crop 1 Common Bermudagrass Pasture
Facility Name Town of Iertford
Field Name 1 Soilseries
Crop 1 Pan 220
Landowner John Hobbs, Sr.
Acres Permited 27.60 Soil Abbrevation:
Crop 2 Annual Ryegrass - Pasture
Operator Johns Hobbs, Jr.
Crop 2 Pan 50
Volume
Acres Dn Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied
%Solids Used DT/Ac. Tons Source Condition Precip
Method
P
Volatilization Mineralization TKN Ammonia Nitrite PAN
PAN Crop
05/23/2014 Gallons 135,000
3.28 27.60 0.67 18.46 Town of Hertford WWTP Dry 0
Surface
27.43
0.50 0.30 47,000 2,440.00 543.(X) 20.25
Crop 1
05/26/2014 Gallons 85,0(N)
3.28 27.60 0.42 11.63 Town of Hertford WWTP Dry 0
Surface
17.27
0.50 030 47,000 2,440.00 543.(X) 12.75
Crop 1
Total Volume Applied 220,(H)0 Total Dry Tons 30-09
Sum Total P 44.70
Total 32.99
Total
Reported in Gallons Arsenic
Cadmium Copper Chromium
Lead Mercun Mokbdenum Nickel Selenium Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.020
0.007 0.798 0.105
0.078 0.002 0.011 0.055 0.015 2.573
(Ibs./Ac.)
Lime (T/Ac.) Date
(Ibs./Ac.)
Prior Year 0.103
0.036 3.544 0.218
0.402 0.007 0.070 0.189 0.047 10.478
Cumulative Total 0.123
0.043 4.342 0.322
0.481 0.008 0.081 0.243 0.062 13.051
Permitted CPLR 36
34 1338
267 15 374 89 2498
"I certify, under penalty of law, that
this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibilitv of fines and imprisonment for (mowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Ao-�-
Februa 9, 2015
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier
Date
****C.P.L.R.: Cumulative Pollutant Loading Rate

APPENDIX IV
PATHOGEN AND VECTOR VERIFICATION

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Hertford WQ Permit Number: WQ0020239
WWTP Name: Town of Hertford WWTP NPEDS Number: NCO021849
r
Monitoring Period: 01/01/2014 to 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class. B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform_ Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 39,026 41,646 47,394 0 1 Grab Samples
Weight)
(Analytical Technique SM 9221 E
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
0 requirement in 40 CFR 503.33 have been met."
`-`I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Charles A. Jones, ORC
Preparer Name and Title (type or print)
ee �-Zl4z, Z• 2?- IS
S gnature of Preparer* Date
J. Bryan Smith Operator
Land Applier Name and Title (if applicable) (type or print)
February 9; 2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 9, 2015

pLk
PROMPT•ACCU RATE- RELIABLE
LABORATORI:,S, INC
WWNN;.PARLABS.CO1
REPORT OF ANALYSES
Attn: SCOTT CARPENTER
SOIL PLUS PROJECT NAME: APR 14
208- WILLIAMS STREET DATE: 05/29/14
GREENVILLE, NC 27858-
SAMPLE NUMBER- 113630 SAMPLE ID- TH0042414 SAMPLE MATRIX- SO
DATE SAMPLED- 04/24/14 TIME SAMPLED- 1100
DATE RECEIVED- 04/25/14 SAMPLER- SC RECEIVED BY- DJ
TIME RECEIVED- 1025 DELIVERED BY- UPS TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 04/26/14 RE ATTACHED
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 04/25/14 1300 RE 41,646 MPN/g
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]

AOL
RV X F;Z
PR13MPT•ACOU RATE -RE LIABLE
LASORATORIES, INC
WWW.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SOIL PLUS
® TH0042414
b` 113630
' 04/26/14
®' 05/24/14
Start- Fnd-
TS
0.2262
0.2314
TS%
1.77%
1.77%
VS
0.1460
0.1458
VS%
64.54%
63.01 %
yIN
0.004805
yOUT
0.00466068
FSVR (Mass Balance)
3.00%
FSVR (Van Kleeck)
6.44%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O- Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] * Fax: [phone]

'PAF;Z
PROMPT•ACCURATE• PELGoa3LE
1- A.bh 0 R, A7JC U P,I1✓ S j. i lam' C
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
r
SOIL PLUS
TH0042414
04/24/14
AN '
®®
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
113630
1
1,082
2.66%
40,686.13
2
1,019
2.61%
39,026.41
3
1,043
2.67%
39,048.60
4
1,168
2.69%
43,434.05
5
1,148
2.66%
43,151.25
6
1,022
2.59%
39,451.67
7
1 1,265
1 2.67%
1 47,394.09
Fecal' Coliform
Geotnetcic Mean= ,

APPENDIX V
SOIL SAMPLES

NC:DA&L;8 Agronomic Division phone: (91U) 733-2655
Website: www.ncagr.goV/agronomi/
Report No. FY14-SL013292
c, rruu,.
Client: Granville Farms Inc.
Advisor: Scott Carpenter
Predictive
3717 Edwards Mill Rd
252-903-0390
Soil Plus LLC
208 Williams St.
.;."}
Soil Re oft
p
Mehlich-3
Extraction
Raleigh, NC 27612
Greenville, NC 27858
Sampled County: Perquimans
Sampled: 10/14/2013 Received:
10/29/2013
Completed: 11/08/2013
Farm: NIXON
Links to Helpful Information
Sample ID: 1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Soybean
0.0
0 0
0 0 0
$pH
0
0 0
Note: 3 Note: -
2 - Corn, grain
0.0
120 - 160 0
0 0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca%. Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NOS-N
3.28 0.97
24.7 100 0.0 7.3
192 107
81 17
41
31 9 16
55
55
90 0.1 0
Sample ID: 2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.0
0 0
0 0 0
$pH
0
0 0
Note: 3 Note:
2- Corn, grain
0.0
120 - 160 0
0 0 0-
$pH
0
0 0
Note: 3 Note: II
Test Results [units - W/V in g/cri4i; CEC and Na in meq/100 cm3; NO3-N in mg/dO]-.
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
3.28 0.93
24.8 100 0.0 7.3
198 109
81 17
46
32 9 16
57
57
89 0.1 0
Sample ID: 3
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Soybean
0.0
0 0
0 0 0
$pH
0
0 0
Note: 3 Note:
2- Corn, grain
0.0
120 - 160 0
0 0 0
0
0 0
Note: 3
Test Results [units - WN in g/cO; CEC and Na in meq/100
cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral -Organic
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
3.67 0:93
20.7 97 0.6 6.8
140 85
77 18
72
37 20 27
73
91
85 0.1 0
North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded
`. through a grant from the North Carolina Tobacco Trust Fund Commission.
jr �N( Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture
Tolxicco Trust Fuial CwnmissiGo11