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HomeMy WebLinkAboutWQ0019960_Residual Annual Report 2014_20150213RECEIVED FEB 13 2015 DVVR SECTION INFORMATION PROCESSING UNIT City ®f Marion 2. 0 1 City of Marion, NC Waste Water Treatment Plant 2014 Annual Report Land Application Program NC Permit No. WQ0019960 arNi'm VAl. LAlVU AYYLiLt_aI IVA Ut nIIVJ 1 AIIVlr V'VK1Vl WQ Permit#r WQ0019960 County: McDowell Year; 2p14 Facility Name (as shown on permit): City of Ma' don Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909 Land application of residuals as allowed by the permit occurred during the past calendar year? Lf Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on'how the residuals were handled. Part A;- Residuals; Application Summary: Total number of application fields in the ermit: 8 Total number of fields utilized for land application during the year: ' 6 Total amount of dry tons applied during the year for all -application sites: 117.23 Total number of acres utilizes for land application during the year: 113.7 i ui L IP rIL..nuuI Cumuiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. [( 'Yes ® No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soi] pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the, limit specified in the permit. 3) Annual soils an were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All, other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6), The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T :l 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) Alt general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All' monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All; operations and maintenance requirements in the permit were complied with or, in the case of a deviation,; ,prior authorization was received from the Division of Water Resources. 10) No'contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals; as specified in the permit. 12) No:runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there aresignificant penalties for submitting false information; including -the possibility ,of fines and imprisonment for knowing violations." �'-I Permittee Name and Title (type or print) Si'Patureof Pe " ` ee Date of Preparer* Date Sign tune of Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006) e ANNUAL RESIDUAL SAMPLING SUMMARYFORM x Please note that your permit may contain additional -parameters to be.analyzed. The parameters can 'be reported in FORM RSSF - B WQ Permit Number: WQ0019960 Laboratory 1) ETS Facility Name: City- of Marion 2) Residual Source WQ # or NCO031879 3) NPDES #: 4) WWTP Name: Corpening Creek WWTP 5) Residual Analvsis Data Parameter (mg/kg) Cone. Limit m a Sarrlple or Co Yoslte Date 4-7-14 'Percent Solids (%) NA 2.5 Arsenic 75 19.9 Cadmium 85 7.95 Copper 4M0 343 Chromium NA NA Lead 840 49.8 Mercury 57 0.8 Molybdenum 75 19.9 Nickel 420 14.2 Selenium 100 19.9 zinc 7,500 912 Total, Phosphorus NA 274.00 TKN NA 55800 Ammonia -Nitrogen NA 2000 Nitrate and Nitrite NA 9449.97 ..L -Aar v, uiayvaaa ,a%.uuio, um ueuu g cuuceHU-d1lon emirs llstea m t111s corm are not applicable. Reference the individual.permit for metals limits. "I certify, under penalty of law; that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaltipc for submitting falea lnfnrm.ofinr_ i„n1.��7i��r 4-1. •l.•1•a� r r_ a a f-_ t ■ -�biu2 pvSSiivialay ku xmua anu ituvllSviliiuCii� for t�iOwiliig viOlatlOIIS.�� S'ig6atifre of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) Eilr1\UALMir, IALoVJJVLAlLVA.V11V1=3U1V11VjLPKI rVnmL• • Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): Permit #: WQ 0019960 Cation Exchange Capacity (non 503 only): Operator: Nancy Ross Owner: _ Nancy Ross Predominant Soil Series: Acres Used: 19.4 Acres Permitted: 19.4 Site #: R-01 Field #: 30.50 Hayesville R-01 Residual Analysis Data (Heavy Metals and -Total Phosphorus use mg/kg, % Solids use Raw Percent ft positeMOV-001 Com- Date , on Total • .. ��� Annual Heavy Metal I ield Loadings (Calculated in lbs/acre): Total 1 1 2 3 4 5 6 71 0 11 12 DT/Ac./ c App. >v Event 1.57 y Arsenic 1 0.063 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.063 Cadmium 0.025 0.000 0.000 0.000 .0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Copper 1.078 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.078 Chromium ###### 0.000 0.000 0.000 ;0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.157 0.006 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.157 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.000 0.000 0.000 0.003 enum d enum 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Nickel 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Selenium 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.063 Zinc 2.867 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.867 Total Phos- 86.146 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 86.146 horus "I certify, under penalty, of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there arje significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations1P. Sign ture of Land Applie i Date DENR FORM MFLSF (12/2006) 4 rIIIIIUAu IVM115Uk5.V ,L,i1 LVAU11Vli 6Ul INLA-KY VV"l" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 16.26 Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Nancy Ross Owner: _ Nancy Ross Predominant Soil Series: Hayesyille. Acres Used: : 22.9 Acres Permitted: _ 22.9 Site #: R-02 Field #: R-02 Residual Analvsis Data (Heave Metal. and Tntal Phncnhnrnc ,woo It r/L," o/ .. posite non Date Total Phos- phorus a a iv..♦J lriar.,ssa 1'la:lu XJV"UluGa k..ait;UIKtUU in iusiacre): Total Ljj , 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ c App. Event 0.71 14 Arsenic 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.487 0.000 0.000 0.000 :0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.487 Chromium ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.071 0.000 0.000 0.000 :0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Mercury 0.001 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.028 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel 0.020 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Selenium 0.028 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 1.295 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.295 Total Phos- 38.908 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 38.908 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed t)o assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of L Applie', Date DENR FORM MFI SF (1?1?(1nR) AIIIN VEiL 1ViL' IAUn 1+1L' LL LVA1 IUNV 6UlV11V1AKV ffVK1VI' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 12.88 Permit #: : WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Mario DeLuca Owner: _ Anna Deebold Predominant Soil Series: Hayesville Acres Used: 16 Acres Permitted: _ 16 Site #: K-01 Field #: K-01 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids nse Raw PPrrPnt m. . Com- posite Date, B la Total P .. Annual heavy MOM r ON Loaf Ings (Ualculated in lbs/acre): Total _Lj 1 2 3 1 4 15 6 L2J 8 9 10 11 12 DT/Ac./ c App. Event 0.81 Arsenic 0.032 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Cadmium 0.013 0.000 0.000 0.000 `0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 0.552 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.552 Chromium###### 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.080 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molybdenum. denum 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Nickel 0.023 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Selenium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Zinc 1.468 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.468 Total Phos- 44.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 44.114 horus n I certify, under penalty, of law, that this document was prepared under my direction or supervision in accordance With a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there aloe significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Si ature of Land Applies Date DENR FORM MFLSF f19/9nm 1-1111\ V t-11, lvl r, l AJU3 r MIAJ L V AUlLv lT K�) V 1V11V1AK Y P VK1V1''' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 31.18 Permit #: ;WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Mario DeLuca Owner: _ Anna Deebold Predominant Soil Series: Hayesville Acres Used: 3 5. 8 Acres Permitted: 35.8 Site #: K-02 Field #: K-02 Residual Analysis Date (Heavy Metals and Total Phosphorus use ing/lig, % Solids use Raw Percent Com- posite Date _ffii I - - Total Phos- phorus .., Annual Heavy ivletal t leld Loadings (Ualculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ 0 App. Event 0.87 Arsenic 0.035 1 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Cadmium 0.014 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 0.598 0:000; 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.598 Chromium ###### 0.000; 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###4## Lead 0.087 1 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 Mercury 0.001 0.0001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb0.035 denum denum 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Nickel 0.025 0.0001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Selenium 0.035 0.0001, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Zinc 1.589 0.0001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.589 Total Phos- 47.731 0.000- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 47.731 horus 1 cer[lly, unuer penau.y� of haw, mat this document was prepared under my direction or supervision in accordance with a system designed tp assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signa re of Land Applier Date DENR FORM MFLSF (1212006) t-VI'Ni1 Urki., lvlx.itu.L5 r MLu LVAUJIN u NUlv11V1.ARY 1+'ORM-T` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: _City of Marion Total Dry Tons Applied (Annual): Permit #:, WQ0019960 Cation Exchange Capacity (non 503 only): Operator: James Fisher Owner: _ James Fisher Predominant Soil Series: Acres Used:, 11.4 Acres Permitted: - 11.4 Site #: F-03 Field #: 14.23 Hayesville F-03 Residual Analysis Dafa (:EIeavy Metals and Total Phosphorus use mg/k 0/ SolidP #s R Sample 1 2 3 2:1 LIU— 6LZJ g, o use aw ercent }: or 110111 12 Com- posite Date 4/7/14 % Solids 2.5 Arsenic 19.9 Cadmium 7.95 Copper 343 Chromium NA Lead 49.8 Mercury 0.8 Molyb- 19.9 denum Nickel 14.2 Selenium 19.9 Zinc 912 Total Phos- 27400 horus Annn0l TTnn-AT-7-1 �':,.1,7 T . 75��__ /!I_t___i_. ■ - 11-Y I-L-al VIM 1jundings ll.nicula.Led In Ingh9 `rPI' Total 1 2 3 L4-j L 51 1 6 7 8 9 10 11 12 DT/Ac./ y App.° >v Event 1.25 " Arsenic 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Cadmium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Copper 0.856 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.856 Chromium ###### 0.000' 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.124 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.124 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0'.000 0.000 0.002 Molyb- enum denum 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Nickel 0.035 0.000 0.000 0.000 0.0,00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Selenium 0.050 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Zinc 2.276 0.000; 0.000 0.000 0.0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.0 00 2.276 Total Phos- 68.390 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.390 horus "I certify under enaltyl of Ilaw th t tl ' d , p a lls ocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applieri Date I DFNR FnRhA hAFI cF (1911�nnrn JUNIN ua.L ivy; VALS FIEU) LOADING SUMMARY FORM* ' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 12.19 Permit #: WQ0019960 Cation Exchange Capacity (non 5o3 only): Operator: James Fisher Owner: _ James Fisher Predominant Soil Series: Hayesville Acres Used: 8.2' Acres Permitted: _ 8.2 Site #: F-04 Field #: F-04 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Ll I L?J3 4 5 6 7 8 9 10 11 12 Com- posite Date 4/7/14 % Solids 2.5 Arsenic 19.9 Cadmium 7.95 Copper 343 Chromium NA Lead 49.8 Mercury 0.8 Molyb- denum Nickel 14.2 Selenium 19.9 Zinc 912 Total Phos- 27400 eld T.nndinare Wal- 1-4-..a I- vi--i- Total DT/Ac./ App. Event 1 1.49 2 3 -tom- \ - 4 �-�.--.-vvw 5 au aR/.J/ 6L7J Nor= Vl• La 9 10 Arsenic Cadmium Copper Chromi 0.059 0.024 1.020 ###### 0.000i 0.0001 0.000 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 Lead Mercury Molyb- denum enum 0.148 0.002 0.059 0.000 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Nickel Selenium Zinc Total Phos- horus "I eerhfv..nn(ier '0.042 0.059 2.712 81.488 nr=nalty 0.000; 0.0001 0.000' 0.000 of 0.000 0.000 0.000 0.000 lov +1,.,� 0.000 0.000 0.000 0.000 ��.. a_______ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0-00 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 H 0 0.000 0.000 0.059 0.000 0.000 0.024 0.000 0.000 1.020 0.000 0.000 ###### 0.000 0.000 0.148 0.000 0.000. 0,002 0.000 0.000 0.059 0.0 00 0.000 0.042 0.000 0.000 0.059 0.000 0.000 2.712 0.000 1 0.000 181.488 - - - ���u=•=�u� ri"a, prepareu unuer my direction or supervision in accordance with a system designed to; assure that qualified personnel properly gathered and evaluated the information submitted. . I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Lan Applier ; Date r%MKIM %.-I -- .... ... ..__. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK. OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: R-01 Acres Utilized: 19.4 Land Owner: Nancy Ross Annual Dry Tons Applied: 30.4931 Site #• R-01 Acres Permitted: 19.4 Operator: Nancy Ross Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN: O .� Volume applied enter one Solids/ ( ) o /o Volume Applied Residual Sources Soil Cond. Precip. a D . C o 4 . 0 Z a H Nitrate PAN Applied Name of Crop Type p yp Y o Liquid Solids per Acre (NPDES #, WQ#, (Dry, Past 24 r: �? � w. ° " w w � TICN o ° and lbs/acre ) Receiving Residual g Q Fert., Animal Wet Hrs. o w ¢ N * � Nitrite Application Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Moist) inches o R ° o o ° mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 5-2014 292500 2.5 1 1.572 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 56.868 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0--000T 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 OA00 0.000 O.Cv"""v 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: 0 292500 _ As Cd Cu Cr Pb H Mo Ni Se Zn P:868 0.000 Lime 4lbs/ac knnuallbs/acre 'rior 0.063 0.025 1.078 ####### 0.157 0.003 0.063 0.04`5 0.063 2.867 86.146Date Years Cumulative lbs/ac 0.064 0.0437.723 1.348 1.203 0.05 0.068 8.80! ####### 1 1.360 0.053 1.201 1.264 0.495 0.102 0.540 0.165 19.6 22.467 10-14 +:., Vutuulallve lbs/ac V.127 1 'ermitted C. P. L. R.**** 36 34 NA 1338 267 15 NA 374 89 2498 'ermit PAN Limit l st/2nd Crop I -EE] 2 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a s. +o,,, ,a ed �� � �L �5.....a ue�igua,u w assure LllQt lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties_for_submitto ass re. - - - - -- "-- --- - -- ----------- --- - _ nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: R-02 Acres Utilized: 22.9 Land Owner: Nancy Ross Annual Dry Tons Applied: 16.2630 Site #: R-02 Acres Permitted: 22.9 Operator: Nancy Ross Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503): Crop I Name: Fescue Crop 1 Max. PAN: - 202 Crop 2 Name: Crop 2 Max. PAN: Volume applied PP ° (enter one) Solids/ "�o ° >~ Volume Applied per PP P Soil Residual Sources Preci Cond. P' (NPDES #, WQ#, Past 24 L? C ° w Z s Z o Nitrate PAN Applied Name of Crop Type Liquid Solids Acre Fert., Animal (Dry' Firs. o a r m TKN * �; and (lbs/acre) Receiving Residual Q Cu. Yds Gallons (Dry Tons/Ac) We a Waste, etc) inches Moist) ° �' * o' w Nitrite Application 5-2014 156000 2.5 0.710 WQ0019960 dry 0 0.5 mg/kg mg/kg �2000 mg/kg Crop 1 Crop 2 Crop 1�Crop s 0.3 55800 949.97 25.694 NA Fescue [uTALS:l 01 1560001 _- Annual lbs/acre ?rior Years Cumulative lbs/ac �lirrent Cumuulative ibs/ac ?ermitted C. P. L. R.**** 'ermit PAN Limit 1 st/2nd Crop 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this As Cd Cu Cr Pb IH Mo Ni Se I Zn 0.028 0.011 0.487 #####4# 0.071 1 0.001 0.028 0.020 0.028 0.038 0.037 6.481 0.0278 0.796 0.326 0.715 0.354 0.057 R.fl 0.066 0.048 6.768 04#44 0.867 1 0.327 0.743 0.374 1 0.085 1 16.045 36 34 NA 1338 267 15 NA 374 89 2498 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 P 1 25.694 38.908 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Date lbs/ac 10-14 2000 .202 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system desigLed t;, assure that lualifred personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting -false nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Anna Deebold Operator: Mario DeLuca Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: K-01 Annual Dry Tons Applied: 12.8749 Site #: K-01 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 16 Acres Permitted: 16 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D (Dry, We Moist) Preci . P Past 24 His. inches > =' o w a # 0 C o ;�CD � CD N M o o 4 w �' 0 TKN mg/kg Z cj �o o o �• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of CropType Receiving Residual Application Crop 1 FCrop2 Crop 1 Crop 2 12-14 123500 2.5 0.805 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 29.113 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: o ,. 123500 ... As Cd Cu Cr I Pb I H2 Mo Ni Se Zn P 29.113 0:000 Lime Applied %nnuallbs/acre 0.032 0.161 0.193 1 36 0.013 0.114 0.127 34 0.552 17.065 17.617 NA ####### 0.94 ####### 1338 0.080 2.215 2.295 267 0.001 0.102 0.103 15 0.032 2.442 2.474 NA 0.023 1.015 1.038 374 0.032 0.245 0.277 89 1.468 39.249 40.717 2498 44.114 Date lbs/ac 'rior Years Cumulative lbs/ac :urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermrt PAN Limit is 2nd Crop _.. 202 '1 certify, under Denalty of law, that this document was prepared under my direction or supervision in accordance with a system .resigned to assure that lualified personnel properly gathered and evaluated the information submitted. I am aware that there are si nificant penalties_for submitting -false nformation, including the possibility of fines and imprisonment for knowing violations." _ *Application Method: S Surface, IN - Injection, INC - Incorporation �I ��� cl ' [ **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw'sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Anna Deebold Operator: Mario DeLuca Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: K-02 Annual Dry Tons Applied: 31.1708 Site #: K-02 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 35.8 Acres Permitted: 35.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° +� �? o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NPDES #, W # Q ' Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches y 4 a '6 i o a o � o %h w = '* P * R 0 w c^c w * K' �' TKN mg/kg i1 � O w mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( Ibs/acre) Name of Crop Type Receiving Residual APP lication Crop 1 Crop 2 Crop 1 Crop 2 12-14 299000 2.5 1 0.871 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 31.502 NA Fescue 0.000 L 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: _ 6 29900o : As Cd I Cu I Cr Pb I Hg I Mo I Ni I Se I Zn P 31.502 0.000 LimeApplied Unuallbs/acre 0.035 0.014 0.598 1 ####### 0.087 0.001 0.035 0.025 0.035 1.589 47.731 Date lbs/ac 'rior Years Cumulative lbs/ac 0.159 0.194 36 0.117 0.131 j 34 1 17.67 1 18.268 j NA 1 0.997 1 ####### 1 1338 2.29 1 2.377 j 267 0.105 0.106 15 2.452 1 2.487 1 NA 1 1.042 1 1.067 1 374 1 0.243 0.278 89 39.914 41.503 2498 ,urrent Cumulative Ibs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit 1 st/2nd Crop ;I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system deCigned to ass1ire the lualified personnel properly gathered and evaluated the information submitted. I am_ aware that there are significant penalties for submitting false _ nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation -"_? , 2-y'i **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) As Residuals Applications Cd Cu totals I Cr on FORM FSF I Pb I H 0.050 0.020 0.856 ####### 0.124 0.002 0.042 0.018 2.531 1.763 0.475 0.019 0.092 0 n38 37 ## 938 .59 0.021 3 6 34 NA 4- 26 ipp ( attach FORM FSF .MO Ni Se 0.050 0.035 0.050 0.09 0.219 0.038 0.140 0.254 0.088 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE Facility Name: City of Marion WQ Permit #• WQ0019960 Field.#: F-03 . Land Owner: James Fisher � Acres Utilized: 11.4 Annual Dry Tons Applied: 14.2301 Site #: F-03 Acres Permitted: 11.4 Operator: James Fisher Predominant Soil Series: Hayesville "Cation Capacity Exchange g p ty (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop -2Name: Crop 2 Max. PAN: Volume a lied S '1 o PP (enter one) Solids/ Volume oho Applied per Residual Sources (NpDES # WQ#, 01 Cond. Precip, past 24 a 4 � C m xy Z Nitrate PAN Applied Name of Crop Type i C) Liquid Solids Acre Fert., Animal (Dry, Hrs. cD a g' e w N o R 7KN o°o o 0 ' and PP ( lbs/acre) Receiving Residual Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, ¢ o' # �' ° * w o Nitrite Application 12-14 136500 2.5 1 248 WQ0019960 Moist inches ° ° o m /k m /k g g g g m /k g g Crop 1 Crop 2 Crop I Crop 2 0.000 UIFY 0 s 0.5 0.3 55800 2000 949.97 45.162 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ^v.^vv^"v G.000 0.000 0.000 0.000 0.000 F0TALS:1 01 136500 Annual lbs/acre Prior Years Cumulative lbs/ac �urrent Cumulative lbs/ac Permitted C. P. L. R.**** 0.000 0.000 p to this form): Zn P 1 45.162 2.276 68.390 9.034 11.3I0 NA 'ennit PAN Li374 89 2498 mit 1st/2nd Crop `I certify, under penalty 2 of law, that this document was prepared under my direction or supervision in accordance with a systefL desi;,ed to assure that _ f•r , luaiailed personnel properly gathered and evaluated the information submitted. I am awa_r_e_th_a_t__t_hereare significant penalties_for_subm_itting false- nformation; including -the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation J� **Volatilization Rate: Surface - 0.5, InjectionAncorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate Lime Applied Date I lbs/ac DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: James Fisher Operator: James Fisher Crop 1 Name: Fescue WQ Permit #: W4)0019960 Field #: I+-04 Annual Dry Tons Applied: 12.1973 Site #: F-04 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 8;2 Acres Permitted: 8.2 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre D TonslAc (w ) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (D Wet Moist ) Precip. Past 24 Hrs. inches Y cu S o a o 7y ; K' R 4 CD w • N *w TKN mg/kg g z o w m /k 9 9 Nitrate and Nitrite m !k 9 9 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 p Crop 2 p Crop 1 p Crop 2 p 12-14 117000 2.5 1.487 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 53.817 14A Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 C.v^^v^v ^v.00G 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: -.. o - 117000, As Cd Cu Cr Pb H Mo Ni Se Zn P - 5-81 0.000 Lime Applied \nnuallbs/acre 0.059 0.024' 1.020 ####### 0.148 6.002 0.059 0.042 0.659 2.712 81.488 Date lbs/ac 'rior Years Cumulative lbs/ac 0.066 0.035 6.114 2.109 0.904 0.036 0.165 0.409 0.076 14.495 0.125 1 0.059 1 7.134 1#######1 1.052 1 0.038 1 0.224 1 0.451 0.135 17.207 36 34 NA 1338 267 15 NA 374 89 2498 :urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit 1st/2nd Crop 'i certify,tinder malty of law that this dG�cL:nl:nt was prepared ��nrinr my directi32L or 3'.:^e'.'vi3i0u i:: accordance itu +o••+ a� a - «4L 1� ✓ p Y J N 1� a System designed to assure h 4. lualifigd personnel_ -properly_ gathered and evaluated the information_submitted._I_am_awar_e that there ar_e significant_penalties_for-submitting_false,._ nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation tom..1171, If **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006), YI � / �•j ,SA ;,'��'"`r+.i+i l Environmental Testing Solutions, Inc. Prt;ject name: i@'tarion WW'I•P Collection date: 14-Apr-14 _ Date received: 14-Apr-14 Certificate of Analysis Sample identification; CC Sludge #4 - Grab PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: 140414.502 Sample number: 115180 Parameter Method Result RL, Units Date Analyst Footnotes Analyzed %I'S SM 2540 G 2.6 0.10 % 14-Apr-14 KEK MulitpleTubc Fermentation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KEK Sample identification: CC Sludge 951- Grab _ Sample number: 115181 Parameter Method Result RL units AnalyzIalyz ed Analyst Footnotes %I•S SM 2540 G 2.6 0.10 % 14-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KfSK Sample identification: CC Sludge 461- Grab Sample number: 115182 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.6 0.10 % 14-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KEK Sample identification: CC Sludge Grab Sample number: 115183 Parameter Method Result RL units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.6 0.10 % 14-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 92214, 5200 4.7 MPN 7-Apr-14 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 Signature; This report should not be reproduced,, exept in its entirety, without the written consent of Environmental Testing Solutions, inc. � rho results in this report relate only to the samples submitted for analysis _ Environmental Testing Solutions, Inc Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-931i8 Project name: Marion VV®' TP Project number: Collection date: 7-Apr-14 Date received: 7-Altr-14` Sample identification: CC Sludge #1 - Grab Sample number: 140407.503 114920 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.5 0.10 % 7-Apr-14 KRK Mulitple'rubc Fermentation Procedure SM 9221-E 19500 4.5 MPN 7-Apr-14 KEK Sample identification: CC Sludge #Z - Grab Sample number: 114921 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.6 0.10 % 7-Apr-14 KICK Mulitple Tube Fermentation Procedure SM 9221-E 59800 4.7 MPN :Apr-1.1 KFK Sample identification: CC Sludge #3 Grab Sample number: 114922 _ Parameter Method Result RL Units date Analyst Footnotes Analyzed %'1 S SM 2540 G 2.6 0.10 % 7-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 9221-8 33800 4.7 A"N 7-Apr-t4 KF.,K Footnotes: RL = Reporting Limit. Values are reported doN n to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley F. keenan SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 Signature: ,proaucea; exept in its entirety, without the written consent or unwronmental I estmg The results in this report relate only to the samples submitted for analysis. PO Box 7565 Asheville, NC 28802 r Phone: (828) 350-9364 RFt Fax: (828) 350-93ti8 *Y Environmental Testing Solutions, Inc. Certificate O1F Analysis Project name: MarionWWTP; Project number: 140407,504 Collection date: 7-Apr-14 Date received: 7-Apr _14 Sample identification: CC Sludge, - Grab Sample number: 114923 _ Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 2.50 0.10 % 9-Apr-14 ASB 1 Mercury 747113 0.80 0.79 mg/kg )6-Apr-14 DER I Aluminum 6010C 11800 1990 mg/kg 10-Apr.14 MEC I Arsenic 6010C <19.9 19.9 mg/kg 10-Apr.14 MEC I Cadmium 6010C <7.95 7.95 mg/kg 10-Apr-14 MEC 1 Calcium 6010C 13300 1990 mg/kg 10-Apr-14 MEC 1 Copper 6010C 343 7.95 mg/kg 10-Apr.14 MEC 1 Lead 6010C 49.8 19.9 mg/kg 10-Apr-14 MEC I Magnesium 6010C 6320 1990 mg/kg 10-Apr-14 MEC I Molybdenum 6010C <19.9 19.9 mg/kg lo-Apr-14 MEC 1 Nickel 6010C 14.2 7.95 mg/kg 10-Apr-14 NEC 1 Potassium 6010C 7010 39.8 mg/kg 10-Apr-14 MEC 1 Selenium 6010C <19.9 19.9 mg/kg Io-Apr-14 MEC 1 Sodium I 6010C 2850 1990 mg/kg 10-Apr-14 MEC 1 Zinc .6010C 912 19.9 mg/kg 10-Apr-14 MFC 1 Nitrate + Nitrite as N 949.97 160.59 mg/kg 16-Apr-14 LDP/REH 1,3 Total Phosphorus 6010C 27400 795 mg/kg 10-Apr-14 MEC 1 Total Kjeldahl Nitrogen351.2 55800 1070 mg/kg 23-Apr-14 LDP I Total Nitrogen I Calculation 56800 1070 mg/kg 23-Apr-14 LDP I Ammonia Nitrogen SM 4500 NH3 D 2000 150 mg/kg I I-Apr-14 KEK Percent Solids SM 2540 G 2.7 % 7-Apr.14 KEK pH in Liquid SW 846 9045C 6.6 S.U. 7-Apr-14 KEK 4 Reactive Cyanide 335.4 <0.134 0.134 mg/kg 23-Apr.14 ECIIEM 2 Reactive Sulfide SM 4500 S D 0.67 mg/kg 23-Apr-14 ECHEM 2 Ignitability SW 846 1010 >212 212 OF 11-Apr-14 FCHEM 2 N-PAV Calculation 1645950 29-Apr-14 KEK Sodium Absorption Rate Calculation 46 29-Apr-14 KEK Footnotes: RL = Retorting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by'Rogers & Callcott Environmental. 2. Sample analyzed by,Enviro Chemists, Inc. 3. Methods EPA 9210A;and SM 450ONO2 B by LDP and REH. 4. Sample analyzed outside hold time. Date reviewed; �i�•�4i (� Data reviewed by: i Kelley IE. Keenan tA_. NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 Signature. i - This report should riot be reproduced ex6pt in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 40 11 12 13. 14 15 Total :Solids: Beginning Temperature: End Temperature: Dissolved OxygeniLevel Facility ,Name: Biosolids Permit Number: Digester Temperature: 18 Sampling Date/Time: 4/28/14 0825 sampled By: Lee -Estes -- Analysis Date/Time: 4/28/14 0954 Analy$ed By: R: Carter - -1000 milliliters :-0,84 % Dry -Solids 25 degrees Celsius 25 degrees Celsius !Slope: 0.3 Intercept: 6-.2- Correlation CoeAclent: 1.0 Oxygen Uptake Rate: 15.87 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.89 mg Oxygen/g/hr Average Tempe ature: 25 degrees Celsius Temperature Correction Factor: 0.783626166 Temperature Corrected Specific Oxygen Uptake Rate: 1.48 mg Oxygen/g/hr Instructions: Enter Data- In the Blue Boxes, The- Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: .... :�TcataL.Sialids; Beginning Temperature: End Temperature: Slope: Intercept: Correlation Coefficient: /25/14 0815 ee-Estes 125/14 0956 Carter --. 10 0.3 7.0, 1.0 % Dry.Solids degrees Celsius degrees Celsius Oxygen Uptake Rate: 15.77 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.95 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.53 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR i Facility ame:pCorpenirnqCreek Biosolids Permit Nu ber:0019960 JDate:4/24/2014 Digester Temp( Sampling Date Samr Analysis Dab Analy -Sample- . Total Beginning Temp( End Temp( Dissolved Oxygen By: re: By: 3. Ililiters Dry Solids grees Celsius green Celsius Slope: 0.2 Inte�cept: 6.7 Correlation Coefficient: 1.0 Oxygen Uptake ate: 13.95 mg Oxygen/hr Ambient Specific Oxygen Uptake ate: 1.77 mg Oxygen/g/hr Average Temper, ture: 25 degrees Celsius Temperature Correction F�ctor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate:, 1.38 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 .8 9 10 11 12 13 14 15 Facility Biosolids Permit N Digester Temp( Sampling Dat( Samr Analysis Dat( Anraly, Sample .... Total. Beginning Temp( End Temp( Dissolved Oxygen S Correlation Coefl Oxygen Uptake Ambient Specific Oxygen Uptake Average Temper Temperature Correction F Temperature Corrected Spec Instructions: Enter Data in the Blue,B By: 4 0816 14/4/14 0910 1 -- - -- 1000 milliliters _ - 0.,9 %- Dry Solids 25 degrees Celsius 25 degrees Celsius )e: 0.3 pt: 6.9 nt: 1.0 te: 16.99 mg Oxygen/hr te: 1.89 mg Oxygen/g/hr ,e: 25 degrees Celsius )r: 0.783526166 Oxygen Uptake Rate: 1.48 mg Oxygen/g/hr s. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Biosolids Permit N Digester Tempe Sampling Dat( Samp Analysis Dat( Analy: Sample Beginning Temp( End Temp( Dissolved Oxygen Inte Correlation Coeffi Oxygen Uptake Ambient Specific Oxygen Uptake Average Temper Temperature Correction F Temperature Corrected Spec Instructions: Enter Data in the Blue B( e: 1 -__ -0.86 %o-Dry.Solids. 25 degrees Celsius 25 dearses Celsius 4.0 e: 0.3 7.0 1.0 .e: 16.45 mg Oxygen/hr :e: 1.91 mg Oxygen/g/hr e: 25 degrees Celsius )r: 0.783526166 Oxygen Uptake Rate: . 1.50 mg Oxygen/g/hr s. The Calculation and the Spreadsheet execute automatically. h ' � Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample -Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Cor enin Creek WQ 0019960 4/2/2014 18 4/2/14 0817 Lee -Estes 4/2/14 0930 R. Carter -- - - - 1000 25 25 Slope: 0.3 Intercept: 7.5 Correlation Coefficient: 1.0 milliliters % Dry Solids degrees Celsius degrees Celsius Oxygen Uptake Rate: 17.45 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 2.01 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: '1.57 mg Oxygen/g/hr Instructions: Enter Data in the Blue�Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: T'gtal.Solds Beginning Temperature: End Temperature: Slope: Intercept: Correlation Goefficient: Worpeninq Creek I 1411114 0752 1 0.3 6;9 1.0 milliliters %_Dry. Solids degrees Celsius deqrees Celsius Oxygen Uptake Rate: 15.30 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.72 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166. Temperature Corrected Specific Oxygen Uptake Rate:1 1.35 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Environmen'tal Chemists, Inc. IV e 6602 Windmill Way o Wilmington, NC 28405 (910) 392-0223 (Lab) o (910) 392-4424 (Fax) 710 Bowsertown Road o Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIECATE 4194. DL8 CERMCATE #37729 Environmental Testing Solutions, Inc. Post Office Box 7565 Asheville NC 28802 Attention: Kelley Keenan (ETS) Lab ID sample ID: 14-09977 • Site: CC - Sludge Test Method Date of Report: Apr 24, 2014 Customer PO #: Report #: 2014-04144 Report to: Kelley Keenan (ETS) Project ID: Marion WV► TP . Collect Date/Time Matrix Sampled by 4/7/2014 7:05 AM Solid/Sludge Client RCI Cyanide EPA MA Sulfide SM4600 s D lgnitability SW W method 1010 Comment: Reviewed by: "� l Results Date Analyzed <0.134 mglkg 04/23/20.14 0.67 mg/kg 04/2312Q14 >212'OF 04/11/2014 deport#.. 2014-04144 Page l ofl ru.i� utit, r A1r1VULA ;A D VECTOR ATTRACTION REDUCTION FORM (02T Rules) Y < - Facility Name: City of Marion WWTP Name: Corpening'Creek �'Q Permit Number: _ WQ0019960 Monitoring Period: From 1/1/2014 NPDES Number: _ NCO031879 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved: and. alternative. performed: Class A Alt. A (t'ime/tem �) ' ❑ Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑ A1t.D (No Prior est) ❑ Process to Further Reduce Patho en s ❑ If applicable to alternative perfoi•me (Class A only) indicate "Process to Further Reduce Pathogeris'g Compost ❑ Heat Drying ❑ Heat Treatment ❑ Beta Ray ❑ Gamma Ra' Thermophilic ❑ ® Pasteurization ❑ Class B: jAlt. (1) Fecal lac Density Alt. (2) Process to Significantly Reduce Pathogens'''❑ ' If applicable to alternative Perfoi•me (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com osting ❑ Aerobic Digestion ❑ Anaerobic Digestion If a li bl c a e t Pp, . o alternative perfored Class A or Class B complete the following monitorm data: Parameter Allowable Level Pathogen Density Fj!j a ytica in Sludge Sample M�nim Geo. M!arnm Units Type Tech- 2x 10 to theWN 5200 11481.00 MPN6th powE;r per gram of grab sm9221 e Fecal ,Coliform total solids CFU 1000 mpn per gram of total solid (dry baimonella bacteria 3 WN per 4:grams (in lieu of fecal total solid (dry coljform) weight) Vector;Attractiori Reductia n MA CAC 02T .1107) -Please indicate alternative'performed,: Alt.1 (,S reduction) ❑ Alt: la 2 4 - - ( Y bench) ❑ Alt. 3 (30-day bench) ❑ Alt.4(S pec" A uptake) (� Alt. 5 (14-Day Aerobic) [l Alt. 6 (A k: Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. g Alt. 9 (Injection) [� Alt. 10 co oration (Drying - Unstabl'e) ❑ ( ) ❑ No vector attraction reduction alternatives were p(;i formed CERTIFICATION STATEMENT please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reductioyi requirement in 15A NCAC 02T .1107 have been met." ® "I certify, under penalty 9f law, that the pathogen requirements in 15A NCAC 02T :1106 and. the vector attraction reduction requirement in 15A NCAC 02T .1101have not been met." (Please -note if you check this. statement attach an explanation why you have not met one or both': of the requirements.) "This determination has been made junder my direction and supervision in accordance with the system designed to ensure that qualified pe :sonnel properly gather and evaluate the information used, to determine that the pathogen and vector.attractlon reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer`'Name and Title (type 'or print). Signa of Preparer* Date Dennis Key Southern Soil Builders, Inc. _ Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9�(r) and 15A NCAC 2T .1102 (26) M_. 1- .-...... -. . - - rayc r Ui z- Report Number: 14-349-0719 AY 1 Account Number:46381 wwwaleastern.com Send To: SOUTHERN SOIL BUILDERS DENNI!S KEY 958 HOOTS ROAD ROARING RIVER NC 28669 Date Received: 12/15/2014 Date Of Analysis: 12/16/2014 A &L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (8041743-9401 Fax (804) 271-644.6 Grower: SOUTHERN SOIL BUILDERS SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 12/16/2014 r_-._ rmno tv: Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number o ENR /o Rate Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate opm Rate opm Rate , ppm Rate , pH Index r„oQ/lnng megl1QQg K1 46 M 49 VL 237 VH 851 M 16 VL 11778 5-1 H 142 6-4 0-6 7-1 I I I "lC=38 I I NC=25 I I I I I I 1 I K2 130 VH 99 M 328 VH 1084 M 17 VL 11779 4.3 M 124 6.9 0.1 8.6 NC=108 NC=51 d0ft L VL 163 H 678 M 23 VL 11780 4.3 M 128 124 131 5.9 6.83 1.0 5.9 NC=20 NC=16 H 123 M 155 H 735 M 21 VL 11781 5.3 H 146 182 5.5 6.74 1.9 7.2 NC=68 NC=63 I 46 M 74 L 191 H M 21 VL 11783 3.6 M 111 17110 5.6 6.75 1.8 7.5 NC = 38 NC = 38 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS cl AI % % % % % ppm Rate ppm Rate i ppm Rate ppm Rate ppm Rate ppm Rate I ppm Rate !rs/cm Rate I ppm Rate ppm K1 14 L 2.5 M 26 H 183 VH 2.5 H 0.4 L 1 27.8 59.9 1.0 .9 NC NC=62-5 NC = 163 NC = 125.0 K2 L 4.5 H H VH VH L 3.0 31-8 63.0 0.9 1.4 �13 135 1182 14.4 10.5 NC=27 NC=112.5 NC=219 NC=220.0 M H 101 VH VH 6.5 VH 0-4 L 1.3 23.0 57.5 1.7 17.3 116 14.8 193 NC=33 NC=120.0 NC=631 NC=325.0 18 M H 28 H VH VH L 4.4 17.9 51.0 1.3 25.9 17.3 1170 15.7 10.4 l NC = 37 NC = 182.5 NC = 175 NC = 285.0 15 L 4.0 H 76 VH 117 VH 4.8 VH 0.3 VL 2.5 212 52.0 1.2 23 4 NC = 31 I NC = 100.0 I NC = 475 1 I NC = 240.0 /slues on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a :oil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. mo Gw� i (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: I fl "'Z. :.E-C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006830 Predictive Client: Southern Soil Builders, Inc. 958 Hoots Rd Advisor: t = may, '� ; •'Iti = = r� Soil Re o Mehlich-3 Extraction _ p Roaring River, NC 28669 Sampled County: McDowell Sampled- Received: 09/25/2014 Completed: 10/06/2014 Farm: Links to Helpful Informations Sample ID: F3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrassrrim, 1 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- es= Resr:';s t::: i`s - i . y/,.r:r ; CEC and .:a :n .ieq/i00 CAll ; tiv3-1': in �i�yiGoj: SOii Class: rviinerai HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.12 8.0 82 1.4 6.2 107 38 54 26 36 159 110 121 121 226 0.1 1 Sample ID: F4 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 40 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cmP; NO3-N in mg/dnr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.56 1.10 7.6 79 1.6 5.9 119 49 52 24 37 127 93 137 137 236 0.1 1 Sample ID: R1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 70 100 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in glcO; CEC and Na in meq/100 crr?; NO3-N in mg/drrP]: Soil Class: Mineral - HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.00 8.3 84 1.4 5.9 27 21 57 25 47 58 52 62 62 103 0.2 2 North Carolina Jt ti L;lt�t 71111.:i % 1tit:or Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006830 ,y Page 2 of 3 Sample ID: R2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.8 120-200 120 110 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dry]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.46 1.09 6.0 68 1.9 5.6 11 15 46 21 40 133 97 27 27 42 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006830 Page 3 of 3"-I Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% - % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-1 copper index ESP exchangeable sodium percent 1 er llizer Hid% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer -blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I M-O manganese index mineral -organic soil class notations appear on the soil report, refer to sNote: secondary Nutrients and Niicronutrients• In -general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomilpubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit wyjw.ncagr qov/agronomi/obpart4.htm#fs to find P4 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P20s phosphate S-1 sulfur index Test Results SS -I soluble salt index WN weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 P-I K-I Ca% M % Mn-1, Mn All Mn-AI2 Zn-I ZnAI Cu-I SASSANa, ESP SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr".qov/agronomi/uyrst.htm for more information.