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HomeMy WebLinkAboutNCG080775_Initial Abatement Report_20191001Speedway LLC Speedway Office 500 Speedway Drive Enon, OH 45323 Telephone 937-864-3000 March 29, 2019 Submitted via electronic mail to liz.aricena ncdenr.aov Ms. Liz Price North Carolina Department of Environmental Quality Wilmington Regional Office Division of Waste Management - UST Section 127 Cardinal Drive Extension Wilmington, North Carolina 28405 Re: Initial Abatement Action Report Speedway No. 8189 8221 US Highway 117 Rocky Point, Pender County, North Carolina NCDEQ Facility ID No. 0-036761 Dear Ms. Price: Please find attached the Initial Abatement Action Report associated with the oil/water separator release and corresponding excavation and sampling with the above referenced site. These services were provided by our consultant, ATC Associates of North Carolina, P.C. (ATC). An unknown quantity of diesel and diesel impacted water was released from the site's oil/water separator (OWS) during heavy rainfall associated with Hurricane Florence on September 13 and 14, 2018. Due to the massive amounts of rainfall associated with the hurricane, the released material impacted grassy areas onsite and portions of the Rocky Point United Methodist Church property ("Church"), which is located immediately north of the site and across North Carolina Highway 210. During area reconnaissance conducted on October 1, 2018, by Environmental Protection Agency (EPA) personnel to identify potential underground storage tank (UST) releases as a result of Hurricane Florence, areas of dead grass were observed on the Speedway and Church properties. EPA subsequently notified the NCDEQ, who telephoned Speedway and ATC on October 2, 2018. On October 9, 2018, the NCDEQ issued its Notice of Regulatory Requirements Letter to Speedway directing initial abatement action (IAA) activities. During an October 10, 2019, onsite meeting between ATC, EPA, NCDEQ, and Speedway personnel, it was determined the site's OWS had overflowed during the hurricane, and its contents spread via the hurricane's floodwaters to areas onsite and portions of the Church property. Due to the extensive flooding at the time of the OWS overflow, EPA and the NCDEQ agreed scraping the impacted areas to a depth of six inches would be adequate initial abatement action activities. On February 12 through 19, 2019, ATC oversaw Hazmat Emergency Response and Remediation (HERR) excavate the impacted areas on the site and the Church property. All excavated material was transported to an offsite facility for proper disposal. ATC personnel collected 62 soil samples (identified as SB-1 and SB-02 through SB-62) within the five excavation areas for delineation Ms. Liz Price North Carolina Department of Environmental Quality Wilmington Regional Office March 29, 2019 Page 2 purposes. Laboratory analytical results for the soil samples collected during these activities indicate the estimated extent of impacted soil appears limited to the area immediately northeast of the OWS. Laboratory analytical results for the soil samples collected from the excavations on the Church property did not detect TPH DRO and TPH GRO concentrations greater than their respective NCDEQ Action Levels. Additionally, laboratory analytical results of the soil samples collected from all excavation areas did not detect any sampled constituents greater than their respective Soil -to -Groundwater MSCCs. Based on the findings and conclusions of this report documenting soil concentrations of TPH DRO and TPH GRO exceeding their respective NCDEQ Action Levels in the area immediately northeast of the OWS, Speedway recommends the completion of a Limited Site Assessment for the Speedway property. Additionally, no further assessment should be required for the Church property. If you have any questions or require additional information, please contact me at 937- 863-6507 or by email at bmwitt@speedway.com. Sincerely, Speedway LLC 1�k Bryan M. Witt Environmental Representative Attachment cc: ATC Associates of North Carolina, P.C., 2725 East Millbrook Road, Suite 121, Raleigh, NC 27604 Initial Abatement Action Report Prepared for: Speedway LLC March 29, 2019 E ,ty, North Carolina )36761 8901 ATC GROUP SERVICES LLC Initial Abatement Action Report Speedway No. 8189 Document Information Prepared for Speedway LLC Project Name Speedway No. 8189 File Reference SW 8189—March 2019—Initial Abatement Report Job Reference SWDP818901 Date March 29, 2019 Contact Information ATC Associates of North Carolina, P.C. 2725 East Millbrook Road, Suite 121 Raleigh, North Carolina 27604 Telephone: 919.871.0999 Facsimile: 919.871.0335 www.atqs.com Document Control Draft 3-27-19 Robert Winfield RW Bob Bolton BB Final 3-28-19 D.T. Hurdle DTH Bob Bolton BB L� Bob Bolton Senior Project Manager for ATC Group Services LLC Direct Line +1 803.223.0793 Email: bob. bolton(c�atcgs.com Robert Winfield Project Scientist for ATC Group Services LLC Direct Line +1 910.465.9580 Email: robert.winfield(cbatcgs.com a Donald T. Hurdle, P.G. Project Manager for ATC Group Services LLC Direct Line +1 757.364.6739 Email: donald.hurdle(a)atcgs.com SEAL March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 Site Information Site Name: Speedway Store No. 8189 Site Address: 8221 US Highway 117 Rocky Point, Pender County, North Carolina Facility I.D.: 0-036761 Latitude: 34.439683' N Source: Google Earth UST Owner: Speedway LLC Address: 500 Speedway Drive Enon, Ohio 45323 Telephone (937) 863-7642 Property Owner: Speedway LLC Address: 500 Speedway Drive Enon, Ohio 45323 Telephone (937) 863-7642 Consultant: ATC Associates of North Carolina, P.C. Address: 2725 East Millbrook Road, Suite 121 Raleigh, North Carolina 27604 Telephone (919) 871-0999 Analytical Laboratory: Pace Analytical Address: 12065 Lebanon Road Mt. Juliet, Tennessee 37122 Telephone (615) 758-5858 Release Information Date Discovered: Estimated Quantity Of Release: Cause of Release: UST Information: October 1, 2018 UST Incident Number (if known): 43131 Longitude: 77.876676° W UST Operator: Speedway LLC Address: 500 Speedway Drive Enon, Ohio 45323 Telephone (937) 863-7642 Property Occupant: Speedway LLC Address: 500 Speedway Drive Enon, Ohio 45323 Telephone (937) 863-7642 State Certification No. ENV375/DW21704/1310041 Unknown Oil/Water Separator Overflow One 20,000-gallon regular unleaded gasoline UST, one 8,000-gallon premium unleaded gasoline UST, one 20,000-gallon diesel UST, and one 8,000-gallon kerosene UST. Additionally, the oil/water separator's volume is 3,000 gallons. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 Executive Summary ATC Associates of North Carolina, P.C., (ATC) on behalf of Speedway LLC (Speedway), conducted initial abatement action activities at Speedway Facility No. 8189. An unknown quantity of diesel and diesel impacted water was released from the site's oil/water separator (OWS) during heavy rainfall associated with Hurricane Florence on September 13 and 14, 2018. Due to the massive amounts of rainfall associated with the hurricane, the released material impacted grassy areas onsite and portions of the Rocky Point United Methodist Church property ("Church"), which is located immediately north of the site and across North Carolina Highway 210. During area reconnaissance conducted on October 1, 2018, by Environmental Protection Agency (EPA) personnel to identify potential underground storage tank (UST) releases as a result of Hurricane Florence, areas of dead grass were observed on the Speedway and Church properties. EPA subsequently notified the NCDEQ, who telephoned Speedway and ATC on October 2, 2018. On October 9, 2018, the NCDEQ issued its Notice of Regulatory Requirements Letter to Speedway directing initial abatement action (IAA) activities. During an October 10, 2019, onsite meeting between ATC, EPA, NCDEQ, and Speedway personnel, it was determined the site's OWS had overflowed during the hurricane, and its contents spread via the hurricane's floodwaters to areas onsite and portions of the Church property. Due to the extensive flooding at the time of the OWS overflow, EPA and the NCDEQ agreed scraping the impacted areas to a depth of six inches would be adequate initial abatement action activities. On February 12 through 19, 2019, ATC oversaw Hazmat Emergency Response and Remediation (HERR) excavate the impacted areas on the site and the Church property. All excavated material was transported to an offsite facility for proper disposal. ATC personnel collected 62 soil samples (identified as SB-1 and SB-02 through SB-62) within the five excavation areas for delineation purposes. Laboratory analytical results for the soil samples collected during these activities indicate the estimated extent of impacted soil appears limited to the area immediately northeast of the OWS. Laboratory analytical results for the soil samples collected from the excavations on the Church property did not detect TPH DRO and TPH GRO concentrations greater than their respective NCDEQ Action Levels. Additionally, laboratory analytical results of the soil samples collected from all excavation areas did not detect any sampled constituents greater than their respective Soil -to -Groundwater MSCCs. Based on the findings and conclusions of this report documenting soil concentrations of TPH DRO and TPH GRO exceeding their respective NCDEQ Action Levels in the area immediately northeast of the OWS, Speedway recommends the completion of a Limited Site Assessment for the Speedway property. Additionally, no further assessment should be required for the Church property. March 29, 2019 ATC Associates of North Carolina, P.C. iv Initial Abatement Action Report Speedway No. 8189 Table of Contents Site Information Executive Summary iv 1 Introduction 1 1.1 UST Owner and Operator Information 1 1.2 UST Information 1 1.3 AST Information 1 1.4 Release Information 1 2 Site Characteristics 3 2.1 Site Status 3 2.2 Surrounding Property Use 3 2.3 Site Geology/Hydrogeology 3 2.4 Limited Receptor Survey 3 2.5 Initial Abatement Actions 3 3 Site Check Report 4 3.1 Tightness Testing 4 3.2 Site Check 4 4 Initial Response Actions 5 4.1 Notifications 5 4.2 Residual Material 5 4.3 Source Control Actions 5 4.4 Contaminant Migration Control Measures 5 4.5 Measures to Identify and Mitigate Hazards 5 4.6 Contaminated Media Storage, Treatment, and/or Disposal 5 4.7 Free Product Assessment and Removal 5 4.8 Soil Excavation Activities 5 4.9 Site Investigation 5 5 UST Closure Report 6 5.1 Closure Preparation 6 5.2 Closure Procedures 6 5.3 Closure Samples 6 5.4 Residual Material 6 5.5 Initial Response Actions 6 5.6 Soil Excavation Activities 6 5.7 Site Investigation 6 6 Over Excavation Activities 7 6.1 Source and Estimated Extent of Soil Contamination 7 6.2 Excavation Process 7 6.3 Post -Excavation Soil Sample Results 7 7 Groundwater Assessment Activities 8 8 Groundwater Sampling and Results 9 March 29, 2019 ATC Associates of North Carolina, P.C. v Initial Abatement Action Report Speedway No. 8189 9 Conclusions and Recommendations 10 9.1 Conclusions 10 9.2 Recommendations 10 10 Report Limitations 11 Table TABLE 1 Summary of Soil Analytical Results Figures FIGURE 1 Topographic Map FIGURE 2 Site Map FIGURE 3A Excavation Area #1 and Sampling Locations Map FIGURE 3B Excavation Area #2 and Sampling Locations Map FIGURE 3C Excavation Area #3 and Sampling Locations Map FIGURE 3D Excavation Area #4 and Sampling Locations Map FIGURE 3E Excavation Area #5 and Sampling Locations Map Appendices APPENDIX A Laboratory Analytical Reports APPENDIX B Waste Manifests March 29, 2019 ATC Associates of North Carolina, P.C. vi Initial Abatement Action Report Speedway No. 8189 1 Introduction Speedway LLC (Speedway) contracted ATC Associates of North Carolina, P.C. (ATC) to conduct initial abatement action (IAA) activities at Speedway No. 8189 as a result of its oil/water separator (OWS) overflowing during Hurricane Florence. Specifically, an unknown quantity of diesel and diesel impacted water was released from the site's OWS during heavy rainfall associated with Hurricane Florence on September 13 and 14, 2018. Due to the massive amounts of rainfall associated with the hurricane, the released material impacted grassy areas onsite and portions of the Rocky Point United Methodist Church property ("Church"), which is located immediately north of the site and across North Carolina Highway 210. Figure 1 shows the site on a topographic map, and a site map is presented as Figure 2. The site currently operates as a Speedway convenience store with retail fuel sales. During area reconnaissance conducted on October 1, 2018, by Environmental Protection Agency (EPA) personnel to identify potential UST releases as a result of Hurricane Florence, areas of dead grass were observed on the Speedway and Church properties. EPA subsequently notified the North Carolina Department of Environmental Quality (NCDEQ), who telephoned Speedway and ATC on October 2, 2018. On October 9, 2018, the NCDEQ issued its Notice of Regulatory Requirements Letter to Speedway that directed the IAA activities. During an October 10, 2019, onsite meeting between ATC, EPA, NCDEQ, and Speedway personnel, it was determined the site's OWS had overflowed during the hurricane, and its contents spread via the hurricane's floodwaters to areas onsite and portions of the Church property. Due to the extensive flooding at the time of the OWS overflow, EPA and the NCDEQ agreed scraping the impacted areas to a depth of six inches would be adequate IAA activities. 1.1 UST Owner and Operator Information Four underground storage tanks (USTs) and one oil/water separator (OWS) are currently in operation at the referenced facility. The USTs and their appurtenances are owned and operated by Speedway LLC of Enon, Ohio. Information regarding each of the tanks is provided below. 1.2 UST Information RELEASE UST ID PRODUCT CAPACITY MATERIALS INSTALLATION UST ASSOCIATED (gals.) DATE STATUS (Yes/No) 1 Gasoline 20,000 Doublewall 08/01/2005 Active No Re ular Fiberglass/Steel 2 Gasoline 8,000 Doublewall 08/01/2005 Active No (Premium)Fiberglass/Steel 3 Diesel 20,000 Doublewall 08/01/2005 Active No Fiberglass/Steel 4 Kerosene 8,000 Doublewall 08/01/2005 Active No Fiberglass/Steel NA OWS 3,000 Unknown 12/03/2012 Active Yes 1.3 AST Information No ASTs were observed on the site. 1.4 Release Information An unknown quantity of diesel and diesel impacted water was released from the site's OWS during heavy rainfall associated with Hurricane Florence on September 13 and 14, 2018. Due to the massive amounts of rainfall March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 associated with the hurricane, the released material impacted grassy areas onsite and portions of the Rocky Point United Methodist Church property ("Church"), which is located immediately north of the site and across North Carolina Highway 210. During area reconnaissance conducted on October 1, 2018, by EPA personnel to identify potential UST releases as a result of Hurricane Florence, areas of dead grass were observed on the Speedway and Church properties. EPA subsequently notified the NCDEQ, who telephoned Speedway and ATC on October 2, 2018. On October 9, 2018, the NCDEQ issued its Notice of Regulatory Requirements Letter to Speedway that directed IAA activities. During an October 10, 2019, onsite meeting between ATC, EPA, NCDEQ, and Speedway personnel, it was determined the site's OWS had overflowed during the hurricane, and its contents spread via the hurricane's floodwaters to areas onsite and portions of the Church property. Due to the extensive flooding at the time of the OWS overflow, EPA and the NCDEQ agreed scraping the impacted areas to a depth of six inches would be adequate initial abatement action activities. Due to Church access issues and weather delays, the IAA activities didn't commence until mid -February. On February 12 through 19, 2019 ATC personnel oversaw Hazmat Emergency Response and Remediation (HERR) excavate the impacted areas on both properties to an approximate depth of six inches. All excavated material (approximately 160.81 tons) was placed in dump trucks and transported under non -hazardous waste manifests to S&R Farms in Fair Bluff, North Carolina for proper disposal. During the excavation activities, ATC personnel collected 62 soil samples (identified as SB-1 and SB-02 through SB-62) within the five excavation areas for delineation purposes. All 62 samples were placed in resealable bags and submitted to the mobile onsite laboratory operated by RED Lab, LLC [5598 Marvin Moss Lane, Suite 2003, Wilmington, North Carolina 29409, (844) 384- 7815] for total petroleum hydrocarbons (TPH) diesel range organics (DRO) and gasoline range organics (GRO) by QED UVF analysis. Additionally, samples SB-1, SB-04, SB-11, SB-15, SB-18, SB-26, SB-28, SB-37, SB-45, SB-50, SB-55, SB-58, and SB-61 were placed in laboratory -supplied containers, entered into chain -of -custody control, placed on ice, and shipped via FedEx to Pace Analytical (PACE) [12065 Lebanon Road, Mt. Juliet, Tennessee 37122, North Carolina Laboratory Certification Number ENV375/DW21704/B10041, (615) 758-5858] for benzene, toluene, ethylbenzene, total xylenes (BTEX), methyl tert-butyl ether (MTBE), naphthalene, and di - isopropyl ether analysis by EPA Method 8260B; TPH DRO and TPH GRO analysis by EPA Method 8015; polycyclic aromatic hydrocarbons (PAH) by EPA Method 8270; and Massachusetts Department of Environmental Protection (MADEP) Methods for extractable petroleum hydrocarbon (EPH) and volatile petroleum hydrocarbons (VPH). The five excavation areas were backfilled with clean topsoil and topped with grass seed and straw. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 2 Site Characteristics 2.1 Site Status Presently, the site is an active convenience store with retail fuel sales. The USTs and their appurtenances are in operation at the referenced facility. Surface cover at the site consists of asphalt and concrete; however, surface cover of the OWS is soil and grass. 2.2 Surrounding Property Use Properties surrounding the subject facility are zoned GB General Business. Commercial businesses and restaurants characterize the surrounding area. Rocky Point United Methodist Church is to the north of the site. A McDonald's restaurant is located to the east of the site, a Wendy's restaurant to the south, and a Taqueria Durango restaurant to the west. 2.3 Site Geology/Hydrogeology The site is located within the Tidewater Region of the Coastal Plain Physiographic Region of North Carolina. Within most areas of Pender County, the surficial aquifer lies within 20 feet of ground surface, yielding sufficient water supply for domestic use. Although the source area is located where recharge to the surficial aquifer has the potential to occur, water from the surficial aquifer in this area is not likely to be used for potable water supply. The area receives its potable water from the Pender County Utilities (Rocky Top Water and Sewer District). Throughout the Coastal Plain groundwater system, recharge to aquifers can be expected to occur in interstream areas, but under most conditions, streams and flood plains act as discharge areas. Such points of discharge may exist in proximity to the Northeast Cape Fear River, which is located approximately two miles east of the site. Based on observations made during site activities, the surface soils consisted of brown/tan silty sand. 2.4 Limited Receptor Survey A limited receptor survey was not completed during initial abatement activities. 2.5 Initial Abatement Actions Refer to Section 1.4 in regard to information regarding this site. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 3 Site Check Report 3.1 Tightness Testing Tightness testing of the system was not performed. 3.2 Site Check On February 12, 2019 through February 19, 2019, ATC oversaw HERR conduct the soil excavation activities on both properties. ATC collected soil samples from all five excavation areas for delineation purposes. HERR excavated all five of the excavation areas to an approximate depth of six inches, except near the base of a large oak tree in excavation area #2 where only three inches of soil could be excavated. ATC collected, by hand, 62 soil samples (SB-1 and SB-02 through SB-62) in the five excavation areas. All 62 samples were analyzed onsite by a mobile laboratory operated by RED Lab LLC for TPH DRO and TPH GRO by QED UVH. The soil samples exhibiting the highest concentrations in each excavation area were additionally submitted to PACE for further analysis. Onsite laboratory analytical results indicated concentrations of TPH DRO were detected greater than its NCDEQ Action Level in samples SB-1, SB-04, SB-11, SB-12, SB-13, SB-15, SB-16, and SB-26. Additionally, onsite laboratory analytical results indicated concentrations of TPH GRO were detected greater than its NCDEQ Action Level in samples SB-12, SB-13, SB-15, and SB-16. It should be noted all these sample location are on the Speedway property and not on the Church property. The soil sample locations are depicted in Figures 3A through 3E. The soil samples (SB-1, SB-04, SIB-1 1, SB-15, SB-18, SB-26, SB-28, SB-37, SB-45, SB-50, SB-55, SB-58, and SB-61) collected for further analysis were placed in laboratory -supplied containers, entered into chain -of -custody control, placed on ice, and shipped via FedEx to PACE for BTEX, MTBE, naphthalene, and di -isopropyl ether analysis by EPA Method 826013; TPH DRO and TPH GRO analysis by EPA Method 8015; PAH by EPA Method 8270; and MADEP Methods for EPH and VPH. Laboratory analytical results did not detect any concentrations of sampled constituents greater than their respective Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs) in these additional soil samples. The laboratory reports are included in Appendix A. The laboratory analytical results are summarized in Table 1. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 4 Initial Response Actions 4.1 Notifications The NCDEQ notified Speedway and ATC via telephone call on October 2, 2018, of the OWS release, and the Notice of Regulatory Requirements Letter, dated October 9, 2018, was issued to Speedway via Certified Mail. 4.2 Residual Material Residual material was not encountered during these activities. 4.3 Source Control Actions Source control actions were not necessary during these activities. 4.4 Contaminant Migration Control Measures No other source control actions were performed. 4.5 Measures to Identify and Mitigate Hazards Other than removal of soils from the area of impact, no other source control actions were performed. 4.6 Contaminated Media Storage, Treatment, and/or Disposal During initial abatement activities, approximately 160.81 tons of petroleum impacted soil were removed from the site and the Church property for offsite disposal. The soil was transported under non -hazardous waste manifests by HERR for proper disposal at S&R Farms in Fair Bluff, North Carolina. Copies of the manifests and weight tickets are presented in Appendix B. 4.7 Free Product Assessment and Removal Free phase product was not identified during site activities. 4.8 Soil Excavation Activities See Section 1.4 for discussion of soil excavation activities performed at the site. 4.9 Site Investigation Refer to Section 1.4 for information on assessment activities. March 29, 2019 ATC Associates of North Carolina, P.C. 5 Initial Abatement Action Report Speedway No. 8189 5 UST Closure Report 5.1 Closure Preparation USTs were not closed as part of these activities. 5.2 Closure Procedures USTs were not closed as part of these activities. 5.3 Closure Samples USTs were not closed as part of these activities. 5.4 Residual Material Refer to section 4.2 for information on residual material. 5.5 Initial Response Actions Refer to Sections 1.4 and 3.2 for information on initial response actions. 5.6 Soil Excavation Activities See Section 1.4 for detailed information on soil excavation activities. 5.7 Site Investigation Refer to Section 3.2 for information on additional investigation activities. March 29, 2019 ATC Associates of North Carolina, P.C. 6 Initial Abatement Action Report Speedway No. 8189 6 Over Excavation Activities 6.1 Source and Estimated Extent of Soil Contamination Based on the laboratory analytical results of the soil samples collected during these activities, the estimated extent of impacted soil appears limited to the area immediately northeast of the OWS. Laboratory analytical results for the soil samples collected from the excavations on the Church property did not detect TPH DRO and TPH GRO concentrations greater than their respective NCDEQ Action Levels. Additionally, laboratory analytical results of the soil samples collected from all excavation areas did not detect any sampled constituents greater than their respective Soil -to -Groundwater MSCCs. 6.2 Excavation Process Refer to Section 1.4 for the excavation process. 6.3 Post -Excavation Soil Sample Results Refer to Sections 1.4 and 3.2 for information on soil sampling and results. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 7 Groundwater Assessment Activities Groundwater assessment activities were not conducted at this time as groundwater was not encountered. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 8 Groundwater Sampling and Results Groundwater sampling activities were not conducted at this time as groundwater was not encountered. March 29, 2019 ATC Associates of North Carolina, P.C. Initial Abatement Action Report Speedway No. 8189 9 Conclusions and Recommendations 9.1 Conclusions Based on the information obtained during initial abatement activities, the following conclusions are made: • A petroleum release occurred when the OWS overflowed during heavy rains associated with Hurricane Florence in September 2018; • An unknown quantity of diesel and diesel impacted water was released when the OWS overflowed, and this mixture was spread on the Speedway and Church properties with the floodwaters from Hurricane Florence. As a result, areas of grass died on both properties; • During site restoration activities, approximately 160.81 tons of petroleum impacted soil were removed and transported for proper disposal; • Groundwater was not encountered during the IAA activities; • Laboratory analytical results of the soil samples collected in excavation area #1 onsite indicate concentrations of TPH DRO and TPH GRO exceeding their respective NCDEQ Action Levels; • Laboratory analytical results of the soil samples collected from the Church property did not detect concentrations of TPH DRO and TPH GRO greater than their respective NCDEQ Action Levels; and • Laboratory analytical results of the soil samples collected from all excavation areas did not detect any sampled constituents greater than their respective Soil -to -Groundwater MSCCs. 9.2 Recommendations Based on the findings and conclusions of this report documenting soil concentrations of TPH DRO and TPH GRO exceeding their respective NCDEQ Action Levels in the area immediately northeast of the OWS, Speedway recommends the completion of a Limited Site Assessment for the Speedway property. Additionally, no further assessment should be required for the Church property. March 29, 2019 ATC Associates of North Carolina, P.C. 10 Initial Abatement Action Report Speedway No. 8189 10 Report Limitations This investigation is intended to be a non -biased assessment of on -site environmental conditions proximate to the location of the former and/or current UST system. Subsurface investigative and remedial methodologies were performed in general accordance with applicable state and federal regulatory requirements. The information presented in this report is based upon site -specific observations, generally accepted geological and environmental consulting practices, and analytical results for environmental samples collected at the time the field investigation was performed. The data presented in this report are believed to represent subsurface conditions at the facility; however, data may not be completely representative of subsurface conditions at every location. ATC assumes no liability arising from environmental impact to, or from, the site, regardless of the date of impact occurrence or findings. March 29, 2019 ATC Associates of North Carolina, P.C. 11 Initial Abatement Action Report Speedway No. 8189 Speedway No. 8189 TABLE March 29, 2019 TABLET SUMMARY OF SOIL ANALYTICAL RESULTS SPEEDWAY NO. 8189 8221 US HIGHWAY 117 SOUTH ROCKY POINT, FENDER COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0.036761 ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP818901 Soil Sample ID Sample Depth (feet) Sampling Date Property Location Excavation Area PID Reading Parts Per Million (PPm) EPA Method 8260 QED UVH m c H d u w X H m d d �, a a u t a 2 y t m o a !_ O O O M Q. O C M Q. Soil -to -Groundwater MSCCs 0.0056 4.3 4.9 4.6 0.091 0.16 0.370 NCDEQ Action Residential MSCCs 18 1,200 1,560 3,129 -- 350 313 156 n1o. Industrial/Commercial MSCCs 164 32.000 40,000 81,760 3 000 8 776 4 088 50 SB-1 0.5 2/13/19 Speedway 1 0.7 <0.0012 0.00722 <0.00306 <0.00796 0.00722 <0.00122 0.0204 <0.00122 <1.5 330.8 SB-02 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.3 72.8 SB-03 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.4 19.7 SB-04 0.5 2/13/19 Speedway 1 4.3 <0.00118 <0.00591 <0.00295 <0.00768 --- <0.00118 <0.0148 <0.00118 <1.4 473.2 SB-05 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.2 19.1 SB-06 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.2 12.8 SB-07 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.3 13.3 SB-08 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA 6.8 39.3 SB-09 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.1 22.6 SB-10 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.3 19.4 SB-11 0.5 2/13/19 Speedway 1 88.9 <0.00115 <0.00574 <0.00287 0.0894 0.0894 <0.00115 <0.0143 <0.00115 <1.5 319.5 SB-12 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA 157.6 342.6 SB-13 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA 1,596 6,657 SB-14 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.5 13.5 SB-15 0.5 2/13/19 Speedway 1 77.2 <0.00115 <0.00574 0.0029 0.0333 0.0362 <0.00115 <0.0144 <0.00115 722.9 2,017 SB-16 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA 1,163 3,952 SB-17 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA 3.3 1.3 SB-18 0.5 2/13/19 Speedway 1 13.3 <0.00116 <0.00581 <0.00291 <0.00756 --- <0.00116 <0.0145 <0.00116 <1.1 62.5 SB-19 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.3 99.4 SB-20 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.6 58.6 SB-21 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <1.3 31.4 SB-22 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <0.67 32.9 SB-23 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <0.45 10.6 SB-24 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <0.32 1.6 SB-25 0.5 2/13/19 Speedway 1 NS NA NA NA NA NA NA NA NA <0.62 10.1 SB-26 0.5 2/14/19 Speedway 1 2.9 <0.00117 <0.00586 <0.00293 <0.00762 --- <0.00117 <0.0146 <0.00117 40.3 135.9 SB-27 0.5 2/14/19 Speedway 1 NS NA NA NA NA NA NA NA NA <0.54 2.8 SB-28 0.25 2/14/19 Church 2 45.9 <0.00121 <0.00604 <0.00302 <0.00785 --- <0.00121 <0.0151 <0.00121 <0.57 32.1 SB-29 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.56 1.3 SB-30 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.6 1.5 SB-31 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.49 0.91 SB-32 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.52 4.9 SB-33 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.63 0.96 SB-34 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.57 6.9 SB-35 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.49 6.3 SB-36 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.66 3.2 SB-37 0.5 2/14/19 Church 2 32.3 <0.00111 <0.00557 <0.00279 <0.00725 --- <0.00111 <0.0139 <0.00111 <0.73 7.5 SB-38 0.5 2/14/19 Church 2 NS NA NA NA NA NA NA NA NA <0.45 0.98 SB-39 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.54 2.5 SB-40 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.48 0.21 SB-41 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.55 19.8 SB-42 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.57 1.1 SB-43 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.6 0.89 SB-44 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.51 0.42 SB-45 0.5 2/14/19 Church 3 7.7 <0.00115 <0.00576 <0.00288 <0.00748 --- <0.00115 <0.0144 <0.00115 5.9 93 SB-46 0.5 2/14/19 Church 3 NS NA NA NA NA NA NA NA NA <0.64 31 SB-47 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.65 5.3 Page 1 of 2 TABLET SUMMARY OF SOIL ANALYTICAL RESULTS SPEEDWAY NO. 8189 8221 US HIGHWAY 117 SOUTH ROCKY POINT, FENDER COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0.036761 ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP818901 Soil Sample ID Sample Depth (feet) Sampling Date Property Location Excavation Area PID Reading Parts Per Million (PPm) EPA Method 8260 QED UVH m c H d u w X H m r d d �, a a u t a 2 y t m o a !_ O O O M H O C M H Soil -to -Groundwater MSCCs 0.0056 4.3 4.9 4.6 0.091 0.16 0.370 NCDEQ Action Level Residential MSCCs 18 1,200 1,560 3,129 - - 350 313 156 100 Industrial/Commercial MSCCs 164 32 000 40 000 81 760 3 000 8 776 4 088 50 SB-48 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.77 1.8 SB-49 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.63 4.1 SB-50 0.5 2/14/19 Church 4 13.1 <0.00119 <0.00594 <0.00297 <0.00772 --- <0.00119 <0.0149 <0.00119 <0.74 5.1 SB-51 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.64 4.5 SB-52 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.49 1.4 SB-53 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.62 1.9 SB-54 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.68 1.3 SB-55 0.5 2/14/19 Church 4 5.4 <0.00116 <0.00581 <0.00291 <0.00756 --- <0.00116 <0.0145 <0.00116 <0.72 5.3 SB-56 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.59 1.8 SB-57 0.5 2/14/19 Church 4 NS NA NA NA NA NA NA NA NA <0.65 4.4 SB-58 0.5 2/14/19 Church 5 15.5 <0.00123 <0.00616 <0.00308 <0.00801 --- <0.00123 <0.0154 <0.00123 <0.66 2.4 SB-59 0.5 2/14/19 Church 5 NS NA NA NA NA NA NA NA NA <0.58 1.7 SB-60 0.5 2/14/19 Church 5 NS NA NA NA NA NA NA NA NA <0.65 3.7 SB-61 0.5 2/14/19 Church 5 10.4 <0.00121 <0.00604 10.00302 <0.00786 --- <0.00121 <0.0151 <0.00121 <0.46 5.8 SB-62 0.5 2/14/19 Church 5 NS NA NA NA NA NA NA NA I NAL <0.48 5 Notes: 1. Concentrations reported in milligrams per kilogram (mg/kg). 2. MSCCs = Maximum Soil Contaminant Concentration. 3. Italics type denotes concentration equals or exceeds Soil -to -Groundwater MSCCs. 4. BOLD type denotes concentration equals or exceeds Residential MSCCs or NCDEQ Action Level. 5. BOLD/Underline denotes concentration equals or exceeds Industrial/Commercial MSCCs. 6. "<" denotes compound not detected above laboratory method detection limit. 7. TPH data is from RED Lab, LLC. 8. NA=Not Analyzed. 9. NS = Not Screened. Page 2 of 2 Initial Abatement Action Report Speedway No. 8189 Speedway No. 8189 FIGURES March 29, 2019 03 28 2019 8:53am — SThompson — H:\125 — ATC 1254410_p1-10-05-18.dwg SOURCE FILE: SPEEDWAY #8189 TOPO WILMINGTON 1990. ` Airiio Ttnvrr stso Pah St Fleldla 40 sp 1 - i = Store r u. - j-11j1��4 s fi r � AiMae'�; JI e16y A'!' 1JA t� ,.-, c p Ut•', r) P� ..'�,,' it rr ` Y'r SITE-, ,' ,,, •:� >.'� �.`._ rmop 41 rK IN jo 7 eh { Lan rng J r � , `4 .t � `,,. � j1 t_. � �- � '~• _ .� : arm-r�-r_ � r owl co r+, i vr: �- fr + •/ aafigs j - i y % y �f 0 2000' 4000' SCALE IN FEET TITLE FIGURE 1'D No. 0-036761 0 SITE TOPOGRAPHIC MAP SPEEDWAY No. 8189 8221 U.S. HIGHWAY 117 SOUTH Raleigh, North Carolina 27604 ENVIRONMENTAL • GEOTECHNICAL 2725 E. Millbrook Road, Suite 121 ROCKY POINT, NORTH C A R O L I N A (919) 871-0999 FAX (919) 871-0335 BUILDING SCIENCES • MATERIALS TESTING CAD FILE PREP. BY REV. BY SCALE DATE PROJECT NO. 1254410.DWG RW BB 1"=2000' 03-20-2019 SWDP818901 ROCKY POINT'-- NITED METHODIST CHURCH r TAQUERIA DURANGO MEXICAN RESTAURANT ZZ 0 40' 80' SCALE IN FEET RETENTION POND OUTFALL GRAVEL OIL/WATER SEPARATOR DRIVE —\ DISCHARGE POINT —\ , �AO XIN DRAINS (TYP.) MIN L/WATER Z SEPARATO RETENTIO UBS POND (3) VENT INES RIP -RAP DRAIN a a a CONTAINMENT n BARRIER U ,ALLON KEROSENE FUEL— ,U U ANWAYS (TYP.) DISPENSERS (TYP.) o GASOLINE nnninnv I LLON DIE (2) TREE' 0,000-G) 8.000-GALLON PREMIUM UNLEADED GASOLINE UST BASIN c G7 Z o U_ H Z 00 Z ui U O Q O w ' 00 0 u a a 07 z w 0 000 > co wo � J N m o 0 N � M M O N Q I co N U) C 0 O Tv Cc O L o w co ��� _� < II z° o U twV_ N _ N c0 m r> j m OI w m 0 O Z Q �z m �J J O O w� a Q I� O cy w _ w ❑ i Z 00 Q� wa ~ 00 z N O CD �_2 z=z Ld Ix o CD DQ QU)� LL- Lu W � W W N U Ln LU_ ENO oN � � � 00 � U 66 w 0 z r DIESEL CANOPY 40 B-18 SB-17 SB-230 SB-080 • SB-19 SB-25• AREA OF EXCAVATION SB-06 • • SB-22 • SB-05 SB -07 • SB-20• SB 21 SB- SB-11• S B-15 SB-16 -•0 090 SB•0 SB- •S8�14 OIL/WATER • SEPARATOR SB-02 SB- CONTAINMENT BARRIER go SPEEDWAY STORE No. 8189 PROPERTY \\— UST BASIN f. 6 . wa 4L komwl-- /N al� 1 1 ILI - ✓ "� -IL�W ER ,ARAroR i ow, ! � irrc 0— crF -�� %I IW , 1 SOIL SAMPLE LOCATION � ► lift Opp • . 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Q w W �t U W N U Ln X a- N O o N F-- W (f) 00 l 4 SOIL SAMPLE LOCATION J 0 20' 40' SCALE IN FEET +.. r47 .w • � 1 • r ' ` t 1P •C 1 • _ qV, CD Z o U_ H Z 00 DU Z � U Q -J)0 w O ' 00 O Of Q c ul Z 000 w > co W O J N m w o 0 N � M M O N o, N (n W 0 oO rn O v o U- W O rn o-m 0 I Z f o U) tujn N _ � N � V) z } O m m w m a U O J Ld d J w OOam 0 a � Q Q = o O 07 W p > a z = M� O(D Q Z=Z Ld CD o O Q (/) a C� < D Q p Lv w u, O Lv N U LL Ln x0NO oN W (n 00 4 I ' Z T CD SOIL SAMPLE LOCATION . . < U) °z • \ z � U �_ CD m 00 • w O a- O Lu of Elia J v ' ` W / _ W W L J N 414P SERVICE • �r N .� STATION • �� M M CANOPY O N O O • N (n W l' o, C 0 40 O XXd •, U O LL W O 0 a rn v II 1 - Zoo V = w t n • Wto N _ � N � co - � z } O j m "too"'! AREA O Q 111 m K OF • U o O Z J � '1' � z m J L J Q O E a � Q U' Z w • 1 ❑ Z � 00 % ~ Lu Q O a Q 00 . •of 0 CID CD waz=z z U 3: wO Qvna o 681%HS #4 j LL Q Ld w U W N U LL Ln w N tz X N O o ROCKY- POINT Q L4 UNITE ME DIST a o ff, #3 N 7 • U O 443N p [.J O 2CONTAI *_ _ W 0 _ O - � DIESEL W ,1 • J J � CANOPY J Immw - SCALE IN FEET Wv � J SOIL SAMPLE LOCATION , s 0 20' 40' SCALE IN FEET - ■ 1 - • � Z ` 0 Tl. U � ui Z 00 ZE U U ¢ ' 00 7 ui ~O W O •� LU U d • � '• r - � w w Z U) • M � W B-58 a 60 . SB-6i' • SB-62- t - r• � z w a O N m o O N � M M O N o, .5 N (n W t6 "O � 0O rn O cc U o LL W O rn 0�� z f o ca> II U) x t ujn W- V) O } w m a U 0 —i J �z m J Q o W .� Q �Q Z W Q _ CY) F-- ❑ 0 � 00 Q O Q00�z MLLJ O CD Q Z2z CD O _ 3 O _ S p Q LL.I — y t W W O W CV U LL� xa-cv0 oN W (n 00 (Y- 6 4 Initial Abatement Action Report Speedway No. 8189 Speedway No. 8189 APPENDIX A Laboratory Analytical Reports March 29, 2019 Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS FZ05 Hydrocarbon Analysis Results Client: ATC Samples taken Wednesday, February 13, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Wednesday, February 13, 2019 SUITE 200-34 Samples analysed Wednesday, February 13, 2019 WILMGINTON, NC 28412 Contact: ROBERT WINFIELD Operator DAVIS MARTINEC Project: SPEEDWAY # 8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10- C18 C10 C18 Soil SB-01 58.5 <1.5 <1.5 330.8 330.8 145.5 7.6 0.044 0 95.3 4.7 V.Deg.PHC 74.5%,(FCM) Soil SB-02 53.4 <1.3 <1.3 72.8 72.8 35.6 1.9 0.021 0 92.6 7.4 V.Deg.PHC 73.3%,(FCM) Soil SB-03 57.9 <1.4 <1.4 19.7 19.7 8.9 0.44 0.009 0 91.7 8.3 V.Deg.PHC 72.9%,(FCM) Soil SB-04 56.9 <1.4 <1.4 473.2 473.2 270.1 16.7 0.02 0 99.2 0.8 Deg.Fuel69%,(FCM) Soil SB-05 47.0 <1.2 <1.2 19.1 19.1 8.5 0.43 0.008 0 91.9 8.1 V.Deg.PHC 72.6%,(FCM) Soil SB-06 47.7 <1.2 <1.2 12.8 12.8 5.6 0.3 0.003 0 92.1 7.9 V.Deg.PHC 76.2%,(FCM),(P) Soil SB-07 52.1 <1.3 <1.3 13.3 13.3 3.5 0.23 0.0031 0 93.9 6.1 Deg.PHC 74.1%,(FCM),(P) Soil SB-08 51.7 <1.3 6.8 39.3 46.1 8.8 0.99 0.004 26.5 71.7 1.8 Deg.PHC 80.4%,(FCM) Soil SB-09 45.9 <1.1 <1.1 22.6 22.6 11 0.6 0.007 0 92 8 V.Deg.PHC 75.1%,(FCM) Soil SB-10 53.9 <1.3WO 19.4 19.4 8.5 0.46 0.007 0 92.1 7.9 V.Deg.PHC 76.5%,(FCM) E�ia7l Calibrato Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS FZ05 Hydrocarbon Analysis Results Client: ATC Samples taken Wednesday, February 13, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Wednesday, February 13, 2019 SUITE 200-34 Samples analysed Wednesday, February 13, 2019 WILMGINTON, NC 28412 Contact: ROBERT WINFIELD Operator DAVIS MARTINEC Project: SPEEDWAY # 8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10- C18 C10 C18 Soil SB-01-2 58.5 <1.5 <1.5 505.2 505.2 221.4 11.5 0.058 0 95.9 4.1 V.Deg.PHC 75.2%,(FCM) Soil SB-04-2 56.9 <1.4 <1.4 650.1 650.1 368.7 23.1 0.025 0 99.3 0.7 Deg.Fuel69.2%,(FCM) Soil S13-11 59.0 <1.5 <1.5 319.5 319.5 145.8 18.7 0.31 0 95.1 4.9 Pyrogenic HC 60%,(FCM) Soil SB-12 214.0 <10.7 157.6 342.6 500.2 212.4 7.3 0.004 47.2 52.4 0.5 Deg.Diesel85.7%,(FCM) Soil SB-13 1525.0 <38.1 1596 6657 8253 1973 66.9 <0.46 49.3 50.5 0.2 Undeg.Diesel93%,(FCM) Soil SB-14 60.2 <1.5 <1.5 13.5 13.5 5.2 0.28 0.003 0 92.1 7.9 Deg.PHC 87.3%,(FCM) Soil SB-15 1747.0 <43.7 722.9 2017 2740 353.8 44 <0.521 42.6 57 0.5 Deg.Diesel84.5%,(FCM) Soil SB-16 1629.0 <40.7 1163 3952 5115 1731 59.7 <0.49 44.7 55.1 0.2 Deg.Diesel93.6%,(FCM) Soil SB-17 45.3 <1.1 3.3 1.3 4.6 1.2 0.13 <0.014 77 21.5 1.4 No HC Match. Estimated values,(FCM) Soil SB-18 45.3 <1.1 <1.1 62.5 62.5 30.51 0.85 0.0031 01 96.81 3.2 V.Deg.PHC 71.4%,(FCM) ial C ' Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS FZ05 Hydrocarbon Analysis Results Client: ATC Samples taken Wednesday, February 13, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Wednesday, February 13, 2019 SUITE 200-34 Samples analysed Wednesday, February 13, 2019 WILMINGTON NC 28412 Contact: ROBERT WINFIELD Operator DAVIS MARTINEC Project: SPEEDWAY #8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10 C18 c10 C18 Soil SB-19 52.5 <1.3 <1.3 99.4 99.4 38.3 2.8 0.006 0 98.4 1.6 Deg.Fuel67.5%,(FCM) Soil SB-20 66.0 <1.6 <1.6 58.6 58.6 29 4.4 0.23 0 90.8 9.2 Pyrogenic HC 69.9%,(FCM) Soil SB-21 51.7 <1.3 <1.3 31.4 31.4 16.3 0.76 0.006 0 94.8 5.2 Deg.PHC 67.3%,(FCM),(P) Soil SB-22 26.9 <0.67 <0.67 32.9 32.9 15 0.76 0.004 0 95.8 4.2 Deg.PHC 83.9%,(FCM),(P) Soil SB-23 17.9 <0.45 <0.45 10.6 10.6 2.4 0.26 0.001 0 97.9 2.1 Deg.PHC 78.2%,(FCM) Soil SB-24 12.7 <0.32 <0.32 1.6 1.6 0.55 0.03 <0.001 0 90.9 9.1 Deg.PHC 84.8%,(FCM) Soil SB-25 24.8 <0.62 <0.62 10.1 10.1 4.7 0.26 0.0051 0 87.3 12.7 V.Deg.PHC 51.6%,(FCM),(P) ial C Final FEi C Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser rxeo�n6 Q,ED 0-Pos Client: ATC Address: 2512 INDEPENDENCE BLVD SUITE 200-34 WILMINGTON NC 28412 Contact: ROBERT WINFIELD Project: SPEEDWAY #8189 Matrix I Sample ID rocarbon Analvsis Results Dilution I BTEX GRO I DRO TPH - ; 16 EPA used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) Aromatics PAHs (C10-C35) Samples taken Samples extracted Samples analysed BaP Soil SB - 26 24.3 <0.61 40.3 135.9 176.2 85.1 3.6 0.008 Soil SB - 27 21.5 <0.54 <0.54 2.8 2.8 1.1 0.06 0.001 Soil SB - 28 22.8 <0.57 <0.57 32.1 32.1 16.5 0.77 0.002 Soil SB - 29 22.4 <0.56 <0.56 1.3 1.3 0.68 0.03 <0.007 Soil SB - 30 24.1 <0.6 <0.6 1.5 1.5 0.71 0.04 <0.007 Soil SB - 31 19.4 <0.49 <0.49 0.91 0.91 0.42 0.02 <0.006 Soil SB - 32 20.8 <0.52 <0.52 4.9 4.9 2.1 0.09 0.001 Soil SB - 33 25.2 <0.63 <0.63 0.96 0.96 0.47 0.03 0.001 Soil SB - 34 22.8 <0.57 <0.57 6.9 6.9 3 0.16 0.001 Soil ISB - 35 19.4 <0.49 ial Calffirntnr <0.49 6.3 6.3 2.31 0.12 0.001 Operator % Ratios C5- C10 C10- C18 C18 36.3 62.8 1 0 92.9 7.1 0 97 0 93.3 6.7 0 84.6 15.4 0 85.6 14.4 0 93 7 0 78.6 21.4 0 94.2 5.E 01 93.51 6.E LQC Check. OKJ Thursday, February 14, 2019 Thursday, February 14, 2019 Thursday, February 14, 2019 JENN RYAN HC Fingerprint Match eg.PHC 74.3% eg.PHC 87.4%,(FCM) eg.PHC 81.4%,(FCM) yrogenic HC 57.1%,(FCM) .Deg.PHC 51.2%,(FCM) yrogenic HC 59.1 %,(FCM) yrogenic HC 76.3%,(FCM),(P) .Deg.PHC 45.5%,(FCM) .Deg.PHC 89.2%,(FCM) eg.PHC 74.4%,(FCM) >ncentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. )breviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser Ao- Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS Pos Hydrocarbon Analysis Results Client: ATC Samples taken Thursday, February 14, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Thursday, February 14, 2019 SUITE 200-34 Samples analysed Thursday, February 14, 2019 WILMINGTON NC 28412 Contact: ROBERT WINFIELD Operator JENN RYAN Project: SPEEDWAY #8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10- C18 C10 C18 Soil SB - 36 26.3 <0.66 <0.66 3.2 3.2 1.6 0.09 0.001 0 90.3 9.7 V.Deg.PHC 74.5%,(FCM) Soil SB - 37 29.2 <0.73 <0.73 7.5 7.5 3.6 0.19 0.002 0 92.8 7.2 V.Deg.PHC 76.5%,(FCM) Soil SB - 40 19.3 <0.48 <0.48 0.21 0.21 0.2 0.02 <0.006 0 86.3 13.7 Residual HC Soil SB - 41 21.8 <0.55 <0.55 19.8 19.8 1.6 0.17 0.001 0 97 3 No Match found Soil SB - 42 22.8 <0.57 <0.57 1.1 1.1 0.47 0.02 <0.007 0 93.7 6.3 V.Deg.PHC 73%,(FCM) Soil SB - 43 24.1 <0.6 <0.6 0.89 0.89 0.43 0.02 <0.007 0 94 6 Pyrogenic HC 74.2%,(FCM) Soil SB - 44 20.3 <0.51 <0.51 0.42 0.42 0.4 0.04 <0.0061 0 96.1 3.9 PHC ND,(FCM) Soil SB - 45 24.5 <0.61 5.9 92.6 98.5 54.9 2.1 0.001 11.5 87.6 0.9 Deg.Diesel 73.4%,(FCM) Soil SB - 47 26.0 <0.65 <0.65 5.3 5.3 2.6 0.14 0.001 0 92.4 7.6 V.Deg.PHC 75.5%,(FCM) Soil SB - 48 31.0 <0.77 <0.77 1.8 1.8 0.881 0.05 <0.0091 0 87.4 12.6 V.Deg.PHC 70.5%,(FCM) ial C QC Chec O Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser Ao- Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS Pos Hydrocarbon Analysis Results Client: ATC Samples taken Thursday, February 14, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Thursday, February 14, 2019 SUITE 200-34 Samples analysed Thursday, February 14, 2019 WILMINGTON NC 28412 Contact: ROBERT WINFIELD Operator JENN RYAN Project: SPEEDWAY #8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10- C18 C10 C18 Soil SB - 49 25.2 <0.63 <0.63 4.1 4.1 2 0.1 0.001 0 90.8 9.2 V.Deg.PHC 73.8%,(FCM) Soil SIB - 50 29.5 <0.74 <0.74 5.1 5.1 1.9 0.1 0.001 0 92.2 7.8 Deg.PHC 84.7%,(FCM) Soil SIB - 51 25.5 <0.64 <0.64 4.5 4.5 1.7 0.09 0.001 0 91.8 8.2 Pyrogenic HC 83.4%,(FCM) Soil SIB - 52 19.5 <0.49 <0.49 1.4 1.4 0.7 0.03 <0.006 0 88.5 11.5 V.Deg.PHC 70.7%,(FCM) Soil SIB - 53 24.8 <0.62 <0.62 1.9 1.9 0.78 0.04 <0.007 0 87.9 12.1 V.Deg.PHC 72%,(FCM) Soil SIB - 54 27.4 <0.68 <0.68 1.3 1.3 0.65 0.03 <0.008 0 85.9 14.1 V.Deg.PHC 56%,(FCM) Soil SIB - 55 28.9 <0.72 <0.72 5.3 5.3 3 0.13 <0.0091 0 95.6 4.4 Deg.PHC 84%,(FCM) Soil SIB - 56 23.4 <0.59 <0.59 1.8 1.8 0.88 0.04 0.001 0 90.1 9.9 V.Deg.PHC 75.7%,(FCM) Soil SIB - 58 26.5 <0.66 <0.66 2.4 2.4 1.2 0.07 0.001 0 86.1 13.9 V.Deg.PHC 54%,(FCM) Soil SIB - 59 23.2 <0.58 <0.58 1.7 1.7 0.631 0.04 0.002 0 84.9 15.1 1Pyrogenic HC 62.6%,(FCM) ial C QC Chec O Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser Ao- Q,ED wPvlo ErJ vluoNrviENTP� o1PGHOSTIGS Pos Hydrocarbon Analysis Results Client: ATC Samples taken Thursday, February 14, 2019 Address: 2512 INDEPENDENCE BLVD Samples extracted Thursday, February 14, 2019 SUITE 200-34 Samples analysed Thursday, February 14, 2019 WILMINGTON NC 28412 Contact: ROBERT WINFIELD Operator JENN RYAN Project: SPEEDWAY #8189 H09382 Matrix Sample ID Dilution BTEX GRO DRO TPH Total Aromatics 16 EPA BaP % Ratios HC Fingerprint Match used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) (C10-C35) PAHs C5- C10- C18 C10 C18 Soil SB - 60 26.0 <0.65 <0.65 3.7 3.7 1.8 0.08 0.001 0 91.7 8.3 V.Deg.PHC 73%,(FCM) Soil SIB - 61 18.3 <0.46 <0.46 5.8 5.8 2.2 0.12 0.001 0 93.9 6.1 Deg.PHC 75.9%,(FCM) Soil SIB - 62 19.3 <0.48 <0.48 5 5 2.5 0.12 0.001 0 94.2 5.8 Deg.PHC 85%,(FCM) Soil SIB - 38 17.8 <0.45 <0.45 0.98 0.98 0.47 0.03 <0.005 0 84.4 15.6 V.Deg.PHC 54.3%,(FCM) Soil SIB - 39 21.7 <0.54 <0.54 2.5 2.5 0.78 0.06 <0.007 0 97.7 2.3 Deg.PHC 85.5%,(FCM) Soil SIB - 46 25.7 <0.64 <0.64 31 31 16.1 1.1 0.001 0 98.1 1.9 Deg Fuel 74.1%,(FCM) Soil SIB - 57 26.0 <0.65 <0.65 4.4 4.4 2.1 0.1 <0.0081 0 93.7 6.3 V.Deg.PHC 74.3%,(FCM) ial C Final FEi C Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification. Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result. % Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser aceAnalytical ® ANALYTICAL REPORT National Center for Testing & Innovation March 01, 2019 ATC Group Services - SC - Speedway Sample Delivery Group: L1071390 Samples Received: 02/19/2019 Project Number: SWDP818901 Description: SW 8189 Rocky point INC Site: 0008189 0-036761 Report To: Mr. Bob Bolton 7499 Parklane Road, Suite 112 Columbia, SC 29223 Entire Report Reviewed By: John Hawkins Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304, 1 lip -74 %. .. — - _mv� dol r L TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results SIB-1 L1071390-01 SB-04 L1071390-02 SB-11 L1071390-03 SB-15 L1071390-04 SB-18 L1071390-05 SB-26 L1071390-06 SB-28 L1071390-07 SB-37 L1071390-08 SB-45 L1071390-09 SB-50 L1071390-10 SB-55 L1071390-11 SB-58 L1071390-12 SB-61 L1071390-13 Qc: Quality Control Summary Total Solids by Method 2540 G-2011 Volatile Petroleum Hydrocarbons by Method MADEPV Volatile Organic Compounds (GC) by Method 8015D/GRO Volatile Organic Compounds (GC/MS) by Method 8260D Semi -Volatile Organic Compounds (GC) by Method 8015C Semi -Volatile Organic Compounds (GC) by Method MADEPE Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 2 3 7 8 8 10 12 14 16 18 20 22 24 26 28 30 32 34 34 36 37 38 40 41 43 45 46 47 CID ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 2 of 48 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time S13-1 L1071390-01 Solid Robert Winfield 02/13/1912:50 02/19/1909:00 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1913:43 02/20/1913:43 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1914:16 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1915:18 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 50 02/19/19 21:26 02/20/1914:32 KME Mt. Juliet, TN [Cn] Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 23:40 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 5 02/20/19 08:31 02/22/1913:21 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 05:56 DMG Mt. Juliet, TN FSr Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 20 02/20/1915:55 02/21/19 06:58 DMG Mt. Juliet, TN FC Collected by Collected date/time Received date/time SB-04 L1071390-02 Solid Robert Winfield 02/13/1912:58 02/19/1909:00 GI Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FAI Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1914:16 02/20/1914:16 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1914:37 ACE Mt. Juliet, TN FSC Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1915:37 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1911:54 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 02:08 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1911:18 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 03:11 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time SB-11 L1071390-03 Solid Robert Winfield 02/13/1913:25 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1914:49 02/20/1914:49 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1914:58 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1915:57 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 20 02/19/19 21:26 02/20/1913:31 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 03:44 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 5 02/20/19 08:31 02/22/1912:57 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 5 02/20/19 08:31 02/22/1919:14 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 20 02120/1915:55 02/21/1916:53 LEA Mt. Juliet, TN Collected by Collected date/time Received date/time SB-15 L1071390-04 Solid Robert Winfield 02/13/1913:35 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1915:22 02/20/1915:22 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1915:20 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1916:16 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 50 02/19/19 21:26 02/20/1915:09 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 20 02/20/19 08:31 02/22/1912:33 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 20 02/20/19 08:31 02/22/1918:50 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 20 02/20/1915:55 02/21/19 09:47 DMG Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 3 of 48 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time SB-18 L1071390-05 Solid Robert Winfield 02/13/1914:23 02/19/1909:00 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1915:55 02/20/1915:55 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1915:41 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1916:35 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 5 02/19/19 21:26 02/20/1914:57 KME Mt. Juliet, TN [Cn] Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1913:45 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1918:27 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 04:13 DMG Mt. Juliet, TN FSr Collected by Collected date/time Received date/time QC SB-26 L1071390-06 Solid Robert Winfield 02/14/1909:50 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location GI date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN FAI Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1916:28 02/20/1916:28 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1916:02 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1916:54 BMB Mt. Juliet, TN FSC Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1910:25 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 3 02/20/19 08:31 02/21/19 23:44 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 3 02/20/19 08:31 02/22/19 08:54 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/20/19 23:24 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time SB-28 L1071390-07 Solid Robert Winfield 02/14/1910:15 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1917:01 02/20/1917:01 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1916:24 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1917:13 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 5 02/19/19 21:26 02/20/1914:44 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 02:32 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1911:44 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02120/1915:55 02/21/19 03:32 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time SB-37 L1071390-08 Solid Robert Winfield 02/14/1911:08 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1917:34 02/20/1917:34 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1916:45 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1917:32 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1911:42 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 02:55 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1912:09 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 03:52 DMG Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 4 of 48 SAMPLE SUMMARY Collected by SB-45 L1071390-09 Solid Robert Winfield ONE LAB. NATIONWIDE. Collected date/time Received date/time 02/14/1911:48 02/19/19 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239619 1 02/20/19 09:26 02/20/19 09:37 JD Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50.5 02/20/1918:07 02/20/1918:07 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25.25 02/19/19 23:14 02/20/1917:06 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1.01 02/19/19 23:14 02/20/1917:51 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1912:06 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 00:08 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 09:19 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/20/19 23:45 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time SB-50 L1071390-10 Solid Robert Winfield 02/14/1912:48 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239620 1 02/20/1916:25 02/20/1916:45 KBC Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1918:40 02/20/1918:40 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1917:28 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1918:10 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1911:30 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 01:44 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1910:54 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 02:51 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time SB-55 L1071390-11 Solid Robert Winfield 02/14/1913:00 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239620 1 02/20/1916:25 02/20/1916:45 KBC Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1919:13 02/20/1919:13 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1917:49 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1918:29 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1910:38 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 00:32 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 09:42 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02120/1915:55 02/21/19 00:05 DMG Mt. Juliet, TN FP1 FTC M [Cn] FSr FC-1 F, FAI FSC SB-58 L1071390-12 Solid Collected by Robert Winfield Collected date/time 02/14/1913:05 Received date/time 02/19/1909:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1239620 1 02/20/1916:25 02/20/1916:45 KBC Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/1919:46 02/20/1919:46 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1918:10 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1918:48 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1911:06 KME Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 00:57 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1910:06 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 00:26 DMG Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 5 of 48 SB-61 L1071390-13 Solid SAMPLE SUMMARY Collected by Robert Winfield Collected date/time 02/14/1913:13 ONE LAB. NATIONWIDE. Received date/time 02/19/1909:00 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Total Solids by Method 2540 G-2011 WG1239620 1 02/20/1916:25 02/20/1916:45 KBC Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1239645 50 02/20/19 20:19 02/20/19 20:19 BMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1239646 25 02/19/19 23:14 02/20/1918:31 ACE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1239740 1 02/19/19 23:14 02/20/1919:07 BMB Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1239459 1 02/19/19 21:26 02/20/1911:18 KME Mt. Juliet, TN [Cn] Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/19 01:20 SHG Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method MADEPE WG1239744 1 02/20/19 08:31 02/22/1910:31 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM WG1239461 1 02/20/1915:55 02/21/19 00:47 DMG Mt. Juliet, TN FSr RC F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 6 of 48 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. John Hawkins Project Manager FP1 FTC FSS FSr 6 QC �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 7 of 48 SAMPLE RESULTS - 01 L1071390 ONE LAB. NATIONWIDE. SB-1 Collected date/time: 02/13/19 12:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 81.7 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 6.12 50 02/20/201913:43 WG1239645 Unadjusted C9-C12 Aliphatics ND 6.12 50 02/20/201913:43 WG1239645 Unadjusted C9-C10 Aromatics ND 6.12 50 02/20/201913:43 WG1239645 Total VPH ND 6.12 50 02/20/201913:43 WG1239645 (S)2,5-Dibromotoluene(FID) 114 70.0-130 02/20/201913:43 WG1239645 (S)2,5-Dibromotoluene(PID) 107 70.0-130 02/20/201913.43 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction 4.24 B 3.06 25 02/20/201914:16 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 102 77.0-120 021201201914:16 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00122 1 02/20/201915:18 WG1239740 Toluene 0.00722 0.00612 1 02/20/201915:18 WG1239740 Ethylbenzene ND 0.00306 1 02/20/201915:18 WG1239740 Total Xylenes ND 0.00796 1 02/20/201915:18 WG1239740 Methyl tert-butyl ether ND 0.00122 1 02/20/201915:18 WG1239740 Naphthalene 0.0204 0.0153 1 02/20/201915:18 WG1239740 Di -isopropyl ether ND 0.00122 1 02/20/201915:18 WG1239740 (S) Toluene-d8 94.7 75.0-131 021201201915:18 WG1239740 (S) a,a,a-Trifluorotoluene 105 80.0-120 021201201915:18 WG1239740 (S)4-Bromof/uorobenzene 105 67.0-138 021201201915:18 WG1239740 (S)1,2-Dichloroethane-d4 112 70.0-130 021201201915:18 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction ND 245 50 02/20/201914:32 (S) o-Terpheny/ 78.5 J7 18.0-148 02/20/201914:32 Sample Narrative: L1071390-01 WG1239459: Cannot run at lower dilution due to viscosity of extract Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octodecone (S) 2-F/uorobiphenyl Batch WG1239459 WG1239459 Result (dry) Qualifier RDL (dry) Dilution Analysis Batch mg/kg mg/kg date / time ND 7.96 1 02/22/2019 23:40 WG1239744 59.8 7.96 1 02/22/2019 23:40 WG1239744 170 39.8 5 02/22/2019 13:21 WG1239744 234 7.96 1 02/22/2019 23:40 WG1239744 64.3 40.0-140 021221201913:21 WG1239744 54.9 40.0-140 021221201923.40 WG1239744 98.7 40.0-140 021221201913:21 WG1239744 105 40.0-140 021221201913:21 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 8 of 48 ONE LAB. NATIONWIDE. SB-1 SAMPLE RESULTS - 01 Collected date/time: 02/13/19 12:50 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Analyte mg/kg mg/kg date / time Anthracene 0.268 0.00735 1 02/21/2019 05:56 Acenaphthene 0.0436 0.00735 1 02/21/2019 05:56 Acenaphthylene ND 0.00735 1 02/21/2019 05:56 Benzo(a)anth race ne 2.66 V_ 0.00735 1 02/21/2019 05:56 Benzo(a)pyrene 3.21 V_ 0.00735 1 02/21/2019 05:56 Benzo(b)fluoranthene 5.17 V_ 0.147 20 02/21/2019 06:58 Benzo(g,h,i)perylene 2.82 V_ 0.00735 1 02/21/2019 05:56 Benzo(k)fluoranthene 0.883 V_ 0.00735 1 02/21/2019 05:56 Chrysene 3.66 V_ 0.00735 1 02/21/2019 05:56 Dibenz(a,h)anthracene 0.697 V_ 0.00735 1 02/21/2019 05:56 Fluoranthene 6.86 V_ 0.147 20 02/21/2019 06:58 Fluorene 0.0478 0.00735 1 02/21/2019 05:56 Indeno(1,2,3-cd)pyrene 2.80 V_ 0.00735 1 02/21/2019 05:56 Naphthalene ND 0.0245 1 02/21/2019 05:56 Phenanthrene 1.45 V_ 0.00735 1 02/21/2019 05:56 Pyrene 5.44 V_ 0.147 20 02/21/2019 06:58 1-Methylnaphthalene ND 0.0245 1 02/21/2019 05:56 2-Methylnaphthalene ND J3 0.0245 1 02/21/2019 05:56 2-Chloronaphthalene ND 0.0245 1 02/21/2019 05:56 (S) Nitrobenzene-d5 56.0 14.0-149 0212112019 05:56 (S) Nitrobenzene-d5 42.5 J7 14.0-149 0212112019 06:58 (S) 2-F/uorobipheny/ 56.2 J7 34.0-125 0212112019 06:58 (S) 2-Fluorobiphenyl 63.2 34.0-125 0212112019 05:56 (S) p-Terphenyl-d14 58.3 J7 23.0-120 0212112019 06:58 (S) p-Terphenyl-d14 69.1 23.0-120 0212112019 05:56 Batch WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 WG1239461 FP FTc FS Fn FC] F FAI FSC ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 9 of 48 SAMPLE RESULTS - 02 L1071390 ONE LAB. NATIONWIDE. SB-04 Collected date/time: 02/13/19 12:58 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 84.6 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.91 50 02/20/201914:16 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.91 50 02/20/201914:16 WG1239645 Unadjusted C9-C10 Aromatics ND 5.91 50 02/20/201914:16 WG1239645 Total VPH ND 5.91 50 02/20/201914:16 WG1239645 (S)2,5-Dibromotoluene(FID) 113 70.0-130 021201201914:16 WG1239645 (S)2,5-Dibromotoluene(PID) 107 70.0-130 021201201914:16 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.95 25 02/20/201914:37 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 98.9 77.0-120 027207201914:37 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00118 1 02/20/201915:37 WG1239740 Toluene ND 0.00591 1 02/20/201915:37 WG1239740 Ethylbenzene ND 0.00295 1 02/20/201915:37 WG1239740 Total Xylenes ND 0.00768 1 02/20/201915:37 WG1239740 Methyl tert-butyl ether ND 0.00118 1 02/20/201915:37 WG1239740 Naphthalene ND 0.0148 1 02/20/201915:37 WG1239740 Di -isopropyl ether ND 0.00118 1 02/20/201915:37 WG1239740 (S) Toluene-d8 96.1 75.0-131 027207201915:37 WG1239740 (S) a,a,a-Trifluorotoluene 113 80.0-120 02/20/201915:37 WG1239740 (S)4-Bromof/uorobenzene 100 67.0-138 027207201915:37 WG1239740 (S)1,2-Dichloroethane-d4 104 70.0-130 02/207201915:37 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 65.2 4.73 1 02/20/201911:54 WG1239459 (S) o-Terphenyl 36.7 18.0-148 027207201911:54 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octodecone (S) 2-F/uorobiphenyl (S) 2-Bromonaphtha/ene Result (dry) mg/kg Qualifier RDL (dry) mg/kg 18.2 7.68 26.1 7.68 16.3 7.68 60.6 7.68 59.0 40.0-140 45.9 40.0-140 97.4 40.0-140 104 40.0-140 Dilution Analysis Batch date / time 1 02/22/2019 02:08 WG1239744 1 02/22/2019 02:08 WG1239744 1 02/22/201911:18 WG1239744 1 02/22/201911:18 WG1239744 021221201911:18 WG1239744 0212212019 02:08 WG1239744 021221201911:18 WG1239744 021221201911:18 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 10 of 48 SB-04 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 02/13/19 12:58 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00709 1 02/21/2019 03:11 WG1239461 FTc Acenaphthene ND 0.00709 1 02/21/2019 03:11 WG1239461 Acenaphthylene ND 0.00709 1 02/21/2019 03:11 WG1239461 Benzo(a)anthracene 0.0663 0.00709 1 02/21/2019 03:11 WG1239461 FS Benzo(a)pyrene 0.0895 0.00709 1 02/21/2019 03:11 WG1239461 Benzo(b)fluoranthene 0.147 0.00709 1 02/21/2019 03:11 WG1239461 [Cn] Benzo(g,h,i)perylene 0.122 0.00709 1 02/21/2019 03:11 WG1239461 Benzo(k)fluoranthene 0.0521 0.00709 1 02/21/2019 03:11 WG1239461 Chrysene 0.0966 0.00709 1 02/21/2019 03:11 WG1239461 Dibenz(a,h)anthracene 0.0201 0.00709 1 02/21/2019 03:11 WG1239461 Fluoranthene 0.154 0.00709 1 02/21/2019 03:11 WG1239461 6 QC Fluorene ND 0.00709 1 02/21/2019 03:11 WG1239461 Indeno(1,2,3-cd)pyrene 0.110 0.00709 1 02/21/2019 03:11 WG1239461 7 Naphthalene ND 0.0236 1 02/21/2019 03:11 WG1239461 GI Phenanthrene 0.0440 0.00709 1 02/21/2019 03:11 WG1239461 Pyrene 0.170 0.00709 1 02/21/2019 03:11 WG1239461 FAI 1-Methylnaphthalene ND 0.0236 1 02/21/2019 03:11 WG1239461 2-Methylnaphthalene ND 0.0236 1 02/21/2019 03:11 WG1239461 2-Chloronaphthalene ND 0.0236 1 02/21/2019 03:11 WG1239461 FSC (S) Nitrobenzene-d5 52.9 14.0-149 0212112019 03:11 WG1239461 (S) 2-Fluorobiphenyl 48.2 34.0-125 0212112019 03:11 WG1239461 (S) p-Terphenyl-d14 53.7 23.0-120 0212112019 03:11 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 11 of 48 SAMPLE RESULTS - 03 L1071390 ONE LAB. NATIONWIDE. SB-11 Collected date/time: 02/13/19 13:25 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 87.2 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.74 50 02/20/201914:49 WG1239645 Unadjusted C9-C12 Aliphatics 24.4 5.74 50 02/20/201914:49 WG1239645 Unadjusted C9-C10 Aromatics 33.2 5.74 50 02/20/2019 14:49 WG1239645 Total VPH 59.8 5.74 50 02/20/201914:49 WG1239645 (S)2,5-Dibromotoluene(FID) 975 70.0-130 021201201914:49 WG1239645 (S)2,5-Dibromotoluene(PID) 94.7 70.0-130 021201201914:49 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction 23.2 2.87 25 02/20/201914:58 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 95.5 77.0-120 021201201914:58 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00115 1 02/20/201915:57 WG1239740 Toluene ND 0.00574 1 02/20/201915:57 WG1239740 Ethylbenzene ND 0.00287 1 02/20/201915:57 WG1239740 Total Xylenes 0.0894 0.00746 1 02/20/201915:57 WG1239740 Methyl tert-butyl ether ND 0.00115 1 02/20/201915:57 WG1239740 Naphthalene ND 0.0143 1 02/20/201915:57 WG1239740 Di -isopropyl ether ND 0.00115 1 02/20/201915:57 WG1239740 (S) Toluene-d8 975 75.0-131 02/20/201915:57 WG1239740 (S) a,a,a-Trifluorotoluene 106 80.0-120 02/20/201915:57 WG1239740 (S)4-Bromof/uorobenzene 122 67.0-138 02/20/201915:57 WG1239740 (S)1,2-Dichloroethane-d4 113 70.0-130 02/20/201915:57 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 1820 91.8 20 02/20/201913:31 WG1239459 (S) o-Terpheny/ 0.000 J7 18.0-148 021201201913:31 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octadecane (S)1-Chloro-octadecane (S) 2-F/uorobiphenyl (S) 2-Bromonaphtha/ene Result (dry) Qualifier RDL (dry) mg/kg mg/kg 866 37.3 359 7.46 447 37.3 1680 37.3 80.3 40.0-140 42.9 40.0-140 63.0 40.0-140 107 40.0-140 138 40.0-140 Dilution Analysis date / time 5 02/22/201919:14 1 02/22/2019 03:44 5 02/22/201912:57 5 02/22/201912:57 021221201912:57 0212212019 03.44 021221201919:14 021221201912:57 021221201912:57 Batch WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 12 of 48 SB-11 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 02/13/19 13:25 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time Anthracene 0.756 0.138 20 02/21/201916:53 WG1239461 Z Tc Acenaphthene ND 0.138 20 02/21/201916:53 WG1239461 Acenaphthylene ND 0.138 20 02/21/201916:53 WG1239461 Benzo(a)anthracene 0.813 0.138 20 02/21/201916:53 WG1239461 Fs Benzo(a)pyrene 1.03 0.138 20 02/21/201916:53 WG1239461 Benzo(b)fluoranthene 1.71 0.138 20 02/21/201916:53 WG1239461 FC n Benzo(g,h,i)perylene 1.47 0.138 20 02/21/201916:53 WG1239461 Benzo(k)fluoranthene 0.578 0.138 20 02/21/201916:53 WG1239461 Chrysene 1.28 0.138 20 02/21/201916:53 WG1239461 Dibenz(a,h)anthracene ND 0.138 20 02/21/201916:53 WG1239461 Fluoranthene 2.71 0.138 20 02/21/201916:53 WG1239461 FQc Fluorene ND 0.138 20 02/21/201916:53 WG1239461 Indeno(1,2,3-cd)pyrene 1.11 0.138 20 02/21/201916:53 WG1239461 Naphthalene ND 0.459 20 02/21/201916:53 WG1239461 FGI Phenanthrene 0.715 0.138 20 02/21/201916:53 WG1239461 Pyrene 2.28 0.138 20 02/21/201916:53 WG1239461 $AI 1-Methylnaphthalene ND 0.459 20 02/21/201916:53 WG1239461 2-Methylnaphthalene ND 0.459 20 02/21/201916:53 WG1239461 2-Chloronaphthalene ND 0.459 20 02/21/201916:53 WG1239461 FSC (S) Nitrobenzene-d5 257 J7 14.0-149 02/21/201916:53 WG1239461 (S) 2-Fluorobiphenyl 70.3 J7 34.0-125 021211201916:53 WG1239461 (S) p-Terphenyl-d14 68.2 J7 23.0-120 021211201916:53 WG1239461 Sample Narrative: L1071390-03 WG1239461: Dilution due to matrix. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 13 of 48 SAMPLE RESULTS - 04 L1071390 ONE LAB. NATIONWIDE. SB-15 Collected date/time: 02/13/19 13:35 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 87.0 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.74 50 02/20/201915:22 WG1239645 Unadjusted C9-C12 Aliphatics 16.8 5.74 50 02/20/201915:22 WG1239645 Unadjusted C9-C10 Aromatics 16.9 5.74 50 02/20/2019 15:22 WG1239645 Total VPH 33.7 5.74 50 02/20/201915:22 WG1239645 (S)2,5-Dibromotoluene(FID) 96.5 70.0-130 02/20/201915:22 WG1239645 (S)2,5-Dibromotoluene(PID) 95.5 70.0-130 02/20/201915:22 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction 5.38 B 2.87 25 02/20/201915:20 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 970 77.0-120 02/20/201915:20 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00115 1 02/20/201916:16 WG1239740 Toluene ND 0.00574 1 02/20/201916:16 WG1239740 Ethylbenzene 0.00290 0.00287 1 02/20/201916:16 WG1239740 Total Xylenes 0.0333 0.00747 1 02/20/201916:16 WG1239740 Methyl tert-butyl ether ND 0.00115 1 02/20/201916:16 WG1239740 Naphthalene ND 0.0144 1 02/20/201916:16 WG1239740 Di -isopropyl ether ND 0.00115 1 02/20/201916:16 WG1239740 (S) Toluene-d8 93.4 75.0-131 021201201916:16 WG1239740 (S) a,a,a-Trifluorotoluene 108 80.0-120 021201201916:16 WG1239740 (S)4-Bromof/uorobenzene 120 67.0-138 021201201916:16 WG1239740 (S)1,2-Dichloroethane-d4 116 70.0-130 021201201916:16 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction T 5000 230 50 02/20/201915:09 WG1239459 (S) o-Terpheny/ 0.000 J7 18.0-148 021201201915:09 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics 1930 149 20 02/22/201918:50 WG1239744 Unadjusted C19-C36 Aliphatics 1750 149 20 02/22/201918:50 WG1239744 Unadjusted C11-C22 Aromatics 1340 149 20 02/22/201912:33 WG1239744 Unadjusted Total Petroleum 5020 149 20 02/22/201918:50 WG1239744 Hydrocarbons (S) o-Terphenyl 76.9 J7 40.0-140 02122120191233 WG1239744 (S)1-Chloro-octodecone 55.6 J7 40.0-140 021221201918:50 WG1239744 (S) 2-F/uorobipheny/ 106 J7 40.0-140 02122120191233 WG1239744 (S) 2-Bromonaphtha/ene 138 J7 40.0-140 02122120191233 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 14 of 48 SB-15 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 02/13/19 13:35 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time Anthracene 0.668 0.138 20 02/21/2019 09:47 WG1239461 FTc Acenaphthene ND 0.138 20 02/21/2019 09:47 WG1239461 Acenaphthylene ND 0.138 20 02/21/2019 09:47 WG1239461 Benzo(a)anthracene ND 0.138 20 02/21/2019 09:47 WG1239461 Fs Benzo(a)pyrene ND 0.138 20 02/21/2019 09:47 WG1239461 Benzo(b)fluoranthene ND 0.138 20 02/21/2019 09:47 WG1239461 FC n Benzo(g,h,i)perylene ND 0.138 20 02/21/2019 09:47 WG1239461 Benzo(k)fluoranthene ND 0.138 20 02/21/2019 09:47 WG1239461 Chrysene ND 0.138 20 02/21/2019 09:47 WG1239461 Dibenz(a,h)anthracene ND 0.138 20 02/21/2019 09:47 WG1239461 Fluoranthene ND 0.138 20 02/21/2019 09:47 WG1239461 FQc Fluorene 0.187 0.138 20 02/21/2019 09:47 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.138 20 02/21/2019 09:47 WG1239461 Naphthalene ND 0.460 20 02/21/201909:47 WG1239461 FGI Phenanthrene 0.206 0.138 20 02/21/2019 09:47 WG1239461 Pyrene 1.30 0.138 20 02/21/2019 09:47 WG1239461 $AI 1-Methylnaphthalene ND 0.460 20 02/21/2019 09:47 WG1239461 2-Methylnaphthalene ND 0.460 20 02/21/2019 09:47 WG1239461 2-Chloronaphthalene ND 0.460 20 02/21/2019 09:47 WG1239461 FSC (S) Nitrobenzene-d5 0.000 J7 14.0-149 0212112019 09:47 WG1239461 (S) 2-Fluorobiphenyl 90.5 J7 34.0-125 0212112019 09:47 WG1239461 (S) p-Terphenyl-d14 112 J7 23.0-120 0212112019 09:47 WG1239461 Sample Narrative: L1071390-04 WG1239461: Dilution due to matrix. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 15 of 48 SAMPLE RESULTS - 05 L1071390 ONE LAB. NATIONWIDE. SB-18 Collected date/time: 02/13/19 14:23 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 86.0 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.81 50 02/20/201915:55 WG1239645 Unadjusted C9-C12 Aliphatics 8.94 5.81 50 02/20/201915:55 WG1239645 Unadjusted C9-C10 Aromatics ND 5.81 50 02/20/201915:55 WG1239645 Total VPH 14.4 B 5.81 50 02/20/201915:55 WG1239645 (S)2,5-Dibromotoluene(FID) ill 70.0-130 02/20/201915:55 WG1239645 (S)2,5-Dibromotoluene(PID) 106 70.0-130 02/20/201915:55 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.91 25 02/20/201915:41 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 99.1 77.0-120 02/20/201915.41 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00116 1 02/20/201916:35 WG1239740 Toluene ND 0.00581 1 02/20/201916:35 WG1239740 Ethylbenzene ND 0.00291 1 02/20/201916:35 WG1239740 Total Xylenes ND 0.00756 1 02/20/201916:35 WG1239740 Methyl tert-butyl ether ND 0.00116 1 02/20/201916:35 WG1239740 Naphthalene ND 0.0145 1 02/20/201916:35 WG1239740 Di -isopropyl ether ND 0.00116 1 02/20/201916:35 WG1239740 (S) Toluene-d8 95.7 75.0-131 02/20/201916:35 WG1239740 (S) a,a,a-Trifluorotoluene 120 80.0-120 02/20/201916:35 WG1239740 (S)4-Bromof/uorobenzene 99.4 67.0-138 02/20/201916:35 WG1239740 (S)1,2-Dichloroethane-d4 120 70.0-130 02/20/201916:35 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 23.2 23.2 5 02/20/201914:57 (S) o-Terpheny/ 54.3 18.0-148 021201201914:57 Sample Narrative: L1071390-05 WG1239459: Cannot run at lower dilution due to viscosity of extract Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octodecone (S) 2-F/uorobiphenyl Batch WG1239459 WG1239459 Result (dry) Qualifier RDL (dry) Dilution Analysis Batch mg/kg mg/kg date / time 17.8 7.56 1 02/22/2019 18:27 WG1239744 21.4 7.56 1 02/22/2019 18:27 WG1239744 18.1 7.56 1 02/22/201913:45 WG1239744 57.3 7.56 1 02/22/2019 18:27 WG1239744 78.0 40.0-140 021221201913.45 WG1239744 72.9 40.0-140 021221201918:27 WG1239744 98.9 40.0-140 021221201913.45 WG1239744 104 40.0-140 021221201913.45 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 16 of 48 S B-18 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE. Collected date/time: 02/13/19 14:23 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00697 1 02/21/2019 04:13 WG1239461 FTc Acenaphthene ND 0.00697 1 02/21/2019 04:13 WG1239461 Acenaphthylene ND 0.00697 1 02/21/2019 04:13 WG1239461 Benzo(a)anthracene ND 0.00697 1 02/21/2019 04:13 WG1239461 FS Benzo(a)pyrene ND 0.00697 1 02/21/2019 04:13 WG1239461 Benzo(b)fluoranthene 0.0122 0.00697 1 02/21/2019 04:13 WG1239461 [Cn] Benzo(g,h,i)perylene 0.00817 0.00697 1 02/21/2019 04:13 WG1239461 Benzo(k)fluoranthene ND 0.00697 1 02/21/2019 04:13 WG1239461 Chrysene 0.00710 0.00697 1 02/21/2019 04:13 WG1239461 Dibenz(a,h)anthracene ND 0.00697 1 02/21/2019 04:13 WG1239461 Fluoranthene 0.00956 0.00697 1 02/21/2019 04:13 WG1239461 6 QC Fluorene ND 0.00697 1 02/21/2019 04:13 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00697 1 02/21/2019 04:13 WG1239461 7 Naphthalene ND 0.0232 1 02/21/2019 04:13 WG1239461 GI Phenanthrene ND 0.00697 1 02/21/2019 04:13 WG1239461 Pyrene 0.0123 0.00697 1 02/21/2019 04:13 WG1239461 FAI 1-Methylnaphthalene ND 0.0232 1 02/21/2019 04:13 WG1239461 2-Methylnaphthalene ND 0.0232 1 02/21/2019 04:13 WG1239461 2-Chloronaphthalene ND 0.0232 1 02/21/2019 04:13 WG1239461 FSC (S) Nitrobenzene-d5 58.9 14.0-149 0212112019 04:13 WG1239461 (S) 2-Fluorobiphenyl 62.4 34.0-125 0212112019 04:13 WG1239461 (S) p-Terphenyl-d14 59.4 23.0-120 0212112019 04:13 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 17 of 48 SAMPLE RESULTS - 06 L1071390 ONE LAB. NATIONWIDE. SB-26 Collected date/time: 02/14/19 09:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 85.3 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.86 50 02/20/201916:28 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.86 50 02/20/201916:28 WG1239645 Unadjusted C9-C10 Aromatics ND 5.86 50 02/20/201916:28 WG1239645 Total VPH ND 5.86 50 02/20/201916:28 WG1239645 (S)2,5-Dibromotoluene(FID) 114 70.0-130 021201201916:28 WG1239645 (S)2,5-Dibromotoluene(PID) 110 70.0-130 021201201916:28 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.93 25 02/20/201916:02 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 96.1 77.0-120 02/20/201916:02 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00117 1 02/20/201916:54 WG1239740 Toluene ND 0.00586 1 02/20/201916:54 WG1239740 Ethylbenzene ND 0.00293 1 02/20/201916:54 WG1239740 Total Xylenes ND 0.00762 1 02/20/201916:54 WG1239740 Methyl tert-butyl ether ND 0.00117 1 02/20/201916:54 WG1239740 Naphthalene ND 0.0146 1 02/20/201916:54 WG1239740 Di -isopropyl ether ND 0.00117 1 02/20/201916:54 WG1239740 (S) Toluene-d8 100 75.0-131 02/20/201916:54 WG1239740 (S) a,a,a-Trifluorotoluene 99.5 80.0-120 02/20/201916:54 WG1239740 (S)4-Bromof/uorobenzene 102 67.0-138 02/20/201916:54 WG1239740 (S) 1,2-Dichloroethane-d4 84.7 70.0-130 02/20/2019 16:54 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 30.1 4.69 1 02/20/201910:25 WG1239459 (S) o-Terpheny/ 71.0 18.0-148 02/20/201910:25 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Analyte mg/kg mg/kg Unadjusted C9-C18 Aliphatics ND 22.9 Unadjusted C19-C36 Aliphatics ND 22.9 Unadjusted C11-C22 Aromatics ND 22.9 Unadjusted Total Petroleum 46.1 22.9 Hydrocarbons (S) o-Terphenyl 86.9 40.0-140 (S)1-Chloro-octodecone 75.6 40.0-140 (S) 2-F/uorobipheny/ 96.9 40.0-140 (S) 2-Bromonaphtha/ene 102 40.0-140 Sample Narrative: L1071390-06 WG1239744: Dilution due to matrix impact during extraction procedure ACCOUNT: PROJECT: ATC Group Services - SC - Speedway SWDP818901 Dilution Analysis date / time 3 02/21/2019 23:44 3 02/21/2019 23:44 3 02/22/2019 08:54 3 02/22/2019 08:54 0212212019 08:54 0212112019 23.44 0212212019 08:54 0212212019 08:54 Batch WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc SDG: DATE/TIME: PAGE: L1071390 03/01/19 12:25 18 of 48 S B- 2 6 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 09:50 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00703 1 02/20/2019 23:24 WG1239461 FTc Acenaphthene ND 0.00703 1 02/20/2019 23:24 WG1239461 Acenaphthylene ND 0.00703 1 02/20/2019 23:24 WG1239461 Benzo(a)anthracene 0.00929 0.00703 1 02/20/2019 23:24 WG1239461 FS Benzo(a)pyrene 0.0152 0.00703 1 02/20/2019 23:24 WG1239461 Benzo(b)fluoranthene 0.0301 0.00703 1 02/20/2019 23:24 WG1239461 [Cn] Benzo(g,h,i)perylene 0.0230 0.00703 1 02/20/2019 23:24 WG1239461 Benzo(k)fluoranthene 0.00920 0.00703 1 02/20/2019 23:24 WG1239461 Chrysene 0.0186 0.00703 1 02/20/2019 23:24 WG1239461 Dibenz(a,h)anthracene ND 0.00703 1 02/20/2019 23:24 WG1239461 Fluoranthene 0.0251 0.00703 1 02/20/2019 23:24 WG1239461 6 QC Fluorene ND 0.00703 1 02/20/2019 23:24 WG1239461 Indeno(1,2,3-cd)pyrene 0.0185 0.00703 1 02/20/2019 23:24 WG1239461 7 Naphthalene ND 0.0234 1 02/20/2019 23:24 WG1239461 GI Phenanthrene ND 0.00703 1 02/20/2019 23:24 WG1239461 Pyrene 0.0272 0.00703 1 02/20/2019 23:24 WG1239461 FAI 1-Methylnaphthalene ND 0.0234 1 02/20/2019 23:24 WG1239461 2-Methylnaphthalene ND 0.0234 1 02/20/2019 23:24 WG1239461 2-Chloronaphthalene ND 0.0234 1 02/20/2019 23:24 WG1239461 FSC (S)Nitrobenzene-d5 68.1 14.0-149 021201201923.24 WG1239461 (S) 2-Fluorobiphenyl 57.1 34.0-125 0212012019 23:24 WG1239461 (S)p-Terphenyl-d14 54.6 23.0-120 021201201923.24 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 19 of 48 SAMPLE RESULTS - 07 L1071390 ONE LAB. NATIONWIDE. SB-28 Collected date/time: 02/14/19 10:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 82.8 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 6.04 50 02/20/201917:01 WG1239645 Unadjusted C9-C12 Aliphatics ND 6.04 50 02/20/201917:01 WG1239645 Unadjusted C9-C10 Aromatics ND 6.04 50 02/20/201917:01 WG1239645 Total VPH ND 6.04 50 02/20/201917:01 WG1239645 (S)2,5-Dibromotoluene(FID) 113 70.0-130 02/20/201917.-01 WG1239645 (S)2,5-Dibromotoluene(PID) 107 70.0-130 021201201917:01 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 3.02 25 02/20/201916:24 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 977 77.0-120 02/20/201916:24 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00121 1 02/20/201917:13 WG1239740 Toluene ND 0.00604 1 02/20/201917:13 WG1239740 Ethylbenzene ND 0.00302 1 02/20/201917:13 WG1239740 Total Xylenes ND 0.00785 1 02/20/201917:13 WG1239740 Methyl tert-butyl ether ND 0.00121 1 02/20/201917:13 WG1239740 Naphthalene ND 0.0151 1 02/20/201917:13 WG1239740 Di -isopropyl ether ND 0.00121 1 02/20/201917:13 WG1239740 (S) Toluene-d8 99.0 75.0-131 021201201917.73 WG1239740 (S) a,a,a-Trifluorotoluene 99.5 80.0-120 021201201917.-13 WG1239740 (S)4-Bromof/uorobenzene 99.0 67.0-138 021201201917.73 WG1239740 (S)1,2-Dichloroethane-d4 82.0 70.0-130 021201201917:13 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 46.4 24.2 5 02/20/201914:44 WG1239459 (S) o-Terpheny/ 69.1 18.0-148 021201201914:44 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octodecone (S) 2-F/uorobiphenyl (S) 2-Bromonaphtha/ene Result (dry) mg/kg Qualifier RDL (dry) mg/kg 14.5 7.85 19.9 7.85 12.8 7.85 47.2 7.85 84.2 40.0-140 79.7 40.0-140 98.5 40.0-140 104 40.0-140 Dilution Analysis Batch date / time 1 02/22/2019 02:32 WG1239744 1 02/22/2019 02:32 WG1239744 1 02/22/201911:44 WG1239744 1 02/22/201911:44 WG1239744 021221201911.44 WG1239744 0212212019 02:32 WG1239744 021221201911.44 WG1239744 021221201911.44 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI Fc ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 20 of 48 SB-28 SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 10:15 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00725 1 02/21/2019 03:32 WG1239461 FTc Acenaphthene ND 0.00725 1 02/21/2019 03:32 WG1239461 Acenaphthylene ND 0.00725 1 02/21/2019 03:32 WG1239461 Benzo(a)anthracene 0.0245 0.00725 1 02/21/2019 03:32 WG1239461 FS Benzo(a)pyrene 0.0326 0.00725 1 02/21/2019 03:32 WG1239461 Benzo(b)fluoranthene 0.0572 0.00725 1 02/21/2019 03:32 WG1239461 [Cn] Benzo(g,h,i)perylene 0.0349 0.00725 1 02/21/2019 03:32 WG1239461 Benzo(k)fluoranthene 0.0193 0.00725 1 02/21/2019 03:32 WG1239461 Chrysene 0.0364 0.00725 1 02/21/2019 03:32 WG1239461 Dibenz(a,h)anthracene ND 0.00725 1 02/21/2019 03:32 WG1239461 Fluoranthene 0.0574 0.00725 1 02/21/2019 03:32 WG1239461 6 QC Fluorene ND 0.00725 1 02/21/2019 03:32 WG1239461 Indeno(1,2,3-cd)pyre ne 0.0316 0.00725 1 02/21/2019 03:32 WG1239461 7 Naphthalene ND 0.0242 1 02/21/2019 03:32 WG1239461 GI Phenanthrene 0.0143 0.00725 1 02/21/2019 03:32 WG1239461 Pyrene 0.0670 0.00725 1 02/21/2019 03:32 WG1239461 FAI 1-Methylnaphthalene ND 0.0242 1 02/21/2019 03:32 WG1239461 2-Methylnaphthalene ND 0.0242 1 02/21/2019 03:32 WG1239461 2-Chloronaphthalene ND 0.0242 1 02/21/2019 03:32 WG1239461 FSC (S) Nitrobenzene-d5 65.3 14.0-149 0212112019 0332 WG1239461 (S) 2-Fluorobiphenyl 77.0 34.0-125 0212112019 03:32 WG1239461 (S) p-Terphenyl-d14 81.2 23.0-120 0212112019 0332 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 21 of 48 SAMPLE RESULTS - 08 L1071390 ONE LAB. NATIONWIDE. S B-37 Collected date/time: 02/14/19 11:08 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 89.7 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.57 50 02/20/201917:34 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.57 50 02/20/201917:34 WG1239645 Unadjusted C9-C10 Aromatics ND 5.57 50 02/20/201917:34 WG1239645 Total VPH ND 5.57 50 02/20/201917:34 WG1239645 (S)2,5-Dibromotoluene(FID) 118 70.0-130 02/20/201917.34 WG1239645 (S)2,5-Dibromotoluene(PID) ill 70.0-130 02/20/201917.34 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.79 25 02/20/201916:45 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 97.3 77.0-120 02/20/201916.45 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00111 1 02/20/201917:32 WG1239740 Toluene ND 0.00557 1 02/20/201917:32 WG1239740 Ethylbenzene ND 0.00279 1 02/20/201917:32 WG1239740 Total Xylenes ND 0.00725 1 02/20/201917:32 WG1239740 Methyl tert-butyl ether ND 0.00111 1 02/20/201917:32 WG1239740 Naphthalene ND 0.0139 1 02/20/201917:32 WG1239740 Di -isopropyl ether ND 0.00111 1 02/20/201917:32 WG1239740 (S) Toluene-d8 101 75.0-131 02/20/201917.32 WG1239740 (S) a,a,a-Trifluorotoluene 98.9 80.0-120 02/20/201917.32 WG1239740 (S)4-Bromof/uorobenzene 99.9 67.0-138 02/20/201917.32 WG1239740 (S)1,2-Dichloroethane-d4 83.7 70.0-130 02/20/201917.32 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 5.79 4.46 1 02/20/201911:42 WG1239459 (S) o-Terpheny/ 88.2 18.0-148 02/20/201911.42 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics ND 7.25 1 02/22/2019 02:55 WG1239744 Unadjusted C19-C36 Aliphatics ND 7.25 1 02/22/2019 02:55 WG1239744 Unadjusted C11-C22 Aromatics ND 7.25 1 02/22/201912:09 WG1239744 Unadjusted Total Petroleum 7.86 7.25 1 02/22/201912:09 WG1239744 Hydrocarbons (S) o-Terphenyl 83.5 40.0-140 021221201912:09 WG1239744 (S)1-Chloro-octodecone 74.6 40.0-140 0212212019 02:55 WG1239744 (S) 2-F/uorobipheny/ 96.4 40.0-140 021221201912:09 WG1239744 (S) 2-Bromonaphtha/ene 101 40.0-140 021221201912:09 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 22 of 48 SB-37 SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 11:08 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00669 1 02/21/2019 03:52 WG1239461 FTc Acenaphthene ND 0.00669 1 02/21/2019 03:52 WG1239461 Acenaphthylene ND 0.00669 1 02/21/2019 03:52 WG1239461 Benzo(a)anthracene ND 0.00669 1 02/21/2019 03:52 WG1239461 FS Benzo(a)pyrene ND 0.00669 1 02/21/2019 03:52 WG1239461 Benzo(b)fluoranthene 0.00818 0.00669 1 02/21/2019 03:52 WG1239461 [Cn] Benzo(g,h,i)perylene ND 0.00669 1 02/21/2019 03:52 WG1239461 Benzo(k)fluoranthene ND 0.00669 1 02/21/2019 03:52 WG1239461 Chrysene ND 0.00669 1 02/21/2019 03:52 WG1239461 Dibenz(a,h)anthracene ND 0.00669 1 02/21/2019 03:52 WG1239461 Fluoranthene ND 0.00669 1 02/21/2019 03:52 WG1239461 6 QC Fluorene ND 0.00669 1 02/21/2019 03:52 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00669 1 02/21/2019 03:52 WG1239461 7 Naphthalene ND 0.0223 1 02/21/2019 03:52 WG1239461 GI Phenanthrene ND 0.00669 1 02/21/2019 03:52 WG1239461 Pyrene 0.00706 0.00669 1 02/21/2019 03:52 WG1239461 FAI 1-Methylnaphthalene ND 0.0223 1 02/21/2019 03:52 WG1239461 2-Methylnaphthalene ND 0.0223 1 02/21/2019 03:52 WG1239461 2-Chloronaphthalene ND 0.0223 1 02/21/2019 03:52 WG1239461 FSC (S) Nitrobenzene-d5 75.6 14.0-149 0212112019 03.52 WG1239461 (S) 2-Fluorobiphenyl 76.5 34.0-125 0212112019 03:52 WG1239461 (S) p-Terphenyl-d14 95.9 23.0-120 0212112019 03.52 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 23 of 48 SAMPLE RESULTS - 09 L1071390 ONE LAB. NATIONWIDE. SB-45 Collected date/time: 02/14/19 11:48 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 87.7 1 02/20/2019 09:37 WG1239619 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.76 50.5 02/20/201918:07 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.76 50.5 02/20/201918:07 WG1239645 Unadjusted C9-C10 Aromatics ND 5.76 50.5 02/20/201918:07 WG1239645 Total VPH ND 5.76 50.5 02/20/201918:07 WG1239645 (S)2,5-Dibromotoluene(FID) 115 70.0-130 02/20/201918:07 WG1239645 (S)2,5-Dibromotoluene(PID) 109 70.0-130 021201201918:07 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.88 25.25 02/20/201917:06 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 97.8 77.0-120 021201201917:06 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00115 1.01 02/20/201917:51 WG1239740 Toluene ND 0.00576 1.01 02/20/201917:51 WG1239740 Ethylbenzene ND 0.00288 1.01 02/20/201917:51 WG1239740 Total Xylenes ND 0.00748 1.01 02/20/201917:51 WG1239740 Methyl tert-butyl ether ND 0.00115 1.01 02/20/201917:51 WG1239740 Naphthalene ND 0.0144 1.01 02/20/201917:51 WG1239740 Di -isopropyl ether ND 0.00115 1.01 02/20/201917:51 WG1239740 (S) Toluene-d8 94.7 75.0-131 021201201917:51 WG1239740 (S) a,a,a-Trifluorotoluene 99.7 80.0-120 021201201917.-51 WG1239740 (S)4-Bromof/uorobenzene 101 67.0-138 021201201917:51 WG1239740 (S) 1,2-Dichloroethane-d4 85.2 70.0-130 0212012019 17:51 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 105 4.56 1 02/20/201912:06 WG1239459 (S) o-Terpheny/ 63.3 18.0-148 021201201912:06 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Analyte Unadjusted C9-C18 Aliphatics Unadjusted C19-C36 Aliphatics Unadjusted C11-C22 Aromatics Unadjusted Total Petroleum Hydrocarbons (S) o-Terphenyl (S)1-Chloro-octodecone (S) 2-F/uorobiphenyl (S) 2-Bromonaphtha/ene Result (dry) Qualifier RDL (dry) Dilution Analysis Batch mg/kg mg/kg date / time 12.2 7.41 1 02/22/2019 00:08 WG1239744 16.2 7.41 1 02/22/2019 00:08 WG1239744 9.61 7.41 1 02/22/2019 09:19 WG1239744 38.0 7.41 1 02/22/2019 09:19 WG1239744 78.4 40.0-140 0212212019 09:19 WG1239744 67.5 40.0-140 0212212019 00:08 WG1239744 95.1 40.0-140 0212212019 09:19 WG1239744 100 40.0-140 0212212019 09:19 WG1239744 FP1 FTC FSS 4 Cn Fc R, FAI FSC ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 24 of 48 SB-45 SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 11:48 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00684 1 02/20/2019 23:45 WG1239461 FTc Acenaphthene ND 0.00684 1 02/20/2019 23:45 WG1239461 Acenaphthylene ND 0.00684 1 02/20/2019 23:45 WG1239461 Benzo(a)anthracene ND 0.00684 1 02/20/2019 23:45 WG1239461 FS Benzo(a)pyrene 0.00740 0.00684 1 02/20/2019 23:45 WG1239461 Benzo(b)fluoranthene 0.0124 0.00684 1 02/20/2019 23:45 WG1239461 [Cn] Benzo(g,h,i)perylene 0.00731 0.00684 1 02/20/2019 23:45 WG1239461 Benzo(k)fluoranthene ND 0.00684 1 02/20/2019 23:45 WG1239461 Chrysene 0.00952 0.00684 1 02/20/2019 23:45 WG1239461 Dibenz(a,h)anthracene ND 0.00684 1 02/20/2019 23:45 WG1239461 Fluoranthene 0.0172 0.00684 1 02/20/2019 23:45 WG1239461 6 QC Fluorene ND 0.00684 1 02/20/2019 23:45 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00684 1 02/20/2019 23:45 WG1239461 7 Naphthalene ND 0.0228 1 02/20/2019 23:45 WG1239461 GI Phenanthrene ND 0.00684 1 02/20/2019 23:45 WG1239461 Pyrene 0.0188 0.00684 1 02/20/2019 23:45 WG1239461 FAI 1-Methylnaphthalene ND 0.0228 1 02/20/2019 23:45 WG1239461 2-Methylnaphthalene ND 0.0228 1 02/20/2019 23:45 WG1239461 2-Chloronaphthalene ND 0.0228 1 02/20/2019 23:45 WG1239461 FSC (S)Nitrobenzene-d5 81.5 14.0-149 021201201923.45 WG1239461 (S) 2-Fluorobiphenyl 75.1 34.0-125 0212012019 23:45 WG1239461 (S)p-Terphenyl-d14 69.1 23.0-120 021201201923.45 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 25 of 48 SAMPLE RESULTS - 10 L1071390 ONE LAB. NATIONWIDE. SB-50 Collected date/time: 02/14/19 12:48 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 84.1 1 02/20/201916:45 WG1239620 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.94 50 02/20/201918:40 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.94 50 02/20/201918:40 WG1239645 Unadjusted C9-C10 Aromatics ND 5.94 50 02/20/201918:40 WG1239645 Total VPH ND 5.94 50 02/20/201918:40 WG1239645 (S)2,5-Dibromotoluene(FID) ill 70.0-130 021201201918.40 WG1239645 (S)2,5-Dibromotoluene(PID) 107 70.0-130 021201201918.40 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.97 25 02/20/201917:28 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 97.0 77.0-120 02/20/201917.28 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00119 1 02/20/201918:10 WG1239740 Toluene ND 0.00594 1 02/20/201918:10 WG1239740 Ethylbenzene ND 0.00297 1 02/20/201918:10 WG1239740 Total Xylenes ND 0.00772 1 02/20/201918:10 WG1239740 Methyl tert-butyl ether ND 0.00119 1 02/20/201918:10 WG1239740 Naphthalene ND 0.0149 1 02/20/201918:10 WG1239740 Di -isopropyl ether ND 0.00119 1 02/20/201918:10 WG1239740 (S) Toluene-d8 97.3 75.0-131 021201201918:10 WG1239740 (S) a,a,a-Trifluorotoluene 114 80.0-120 021201201918:10 WG1239740 (S)4-Bromof/uorobenzene 101 67.0-138 021201201918:10 WG1239740 (S)1,2-Dichloroethane-d4 971 70.0-130 021201201918:10 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 17.5 4.75 1 02/20/201911:30 WG1239459 (S) o-Terpheny/ 64.2 18.0-148 021201201911:30 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics ND 7.72 1 02/22/2019 01:44 WG1239744 Unadjusted C19-C36 Aliphatics ND 7.72 1 02/22/2019 01:44 WG1239744 Unadjusted C11-C22 Aromatics ND 7.72 1 02/22/201910:54 WG1239744 Unadjusted Total Petroleum 15.7 7.72 1 02/22/201910:54 WG1239744 Hydrocarbons (S) o-Terphenyl 79.3 40.0-140 021221201910:54 WG1239744 (S)1-Chloro-octodecone 72.0 40.0-140 0212212019 01.44 WG1239744 (S) 2-F/uorobipheny/ 99.1 40.0-140 021221201910:54 WG1239744 (S) 2-Bromonaphtha/ene 104 40.0-140 021221201910:54 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 26 of 48 S B - 5 0 SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 12:48 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00713 1 02/21/2019 02:51 WG1239461 FTc Acenaphthene ND 0.00713 1 02/21/2019 02:51 WG1239461 Acenaphthylene ND 0.00713 1 02/21/2019 02:51 WG1239461 Benzo(a)anthracene ND 0.00713 1 02/21/2019 02:51 WG1239461 FS Benzo(a)pyrene ND 0.00713 1 02/21/2019 02:51 WG1239461 Benzo(b)fluoranthene ND 0.00713 1 02/21/2019 02:51 WG1239461 [Cn] Benzo(g,h,i)perylene ND 0.00713 1 02/21/2019 02:51 WG1239461 Benzo(k)fluoranthene ND 0.00713 1 02/21/2019 02:51 WG1239461 Chrysene ND 0.00713 1 02/21/2019 02:51 WG1239461 Dibenz(a,h)anthracene ND 0.00713 1 02/21/2019 02:51 WG1239461 Fluoranthene ND 0.00713 1 02/21/2019 02:51 WG1239461 6 QC Fluorene ND 0.00713 1 02/21/2019 02:51 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00713 1 02/21/2019 02:51 WG1239461 7 Naphthalene ND 0.0238 1 02/21/2019 02:51 WG1239461 GI Phenanthrene ND 0.00713 1 02/21/2019 02:51 WG1239461 Pyrene ND 0.00713 1 02/21/2019 02:51 WG1239461 FAI 1-Methylnaphthalene ND 0.0238 1 02/21/2019 02:51 WG1239461 2-Methylnaphthalene ND 0.0238 1 02/21/2019 02:51 WG1239461 2-Chloronaphthalene ND 0.0238 1 02/21/2019 02:51 WG1239461 FSC (S) Nitrobenzene-d5 58.3 14.0-149 0212112019 02:51 WG1239461 (S) 2-Fluorobiphenyl 59.8 34.0-125 0212112019 02:51 WG1239461 (S) p-Terphenyl-d14 73.4 23.0-120 0212112019 02:51 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 27 of 48 SAMPLE RESULTS - 11 L1071390 ONE LAB. NATIONWIDE. SB-55 Collected date/time: 02/14/19 13:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 86.0 1 02/20/201916:45 WG1239620 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 5.81 50 02/20/201919:13 WG1239645 Unadjusted C9-C12 Aliphatics ND 5.81 50 02/20/201919:13 WG1239645 Unadjusted C9-C10 Aromatics ND 5.81 50 02/20/201919:13 WG1239645 Total VPH ND 5.81 50 02/20/201919:13 WG1239645 (S)2,5-Dibromotoluene(FID) 114 70.0-130 021201201919:13 WG1239645 (S)2,5-Dibromotoluene(PID) 108 70.0-130 021201201919:13 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 2.91 25 02/20/201917:49 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 95.0 77.0-120 02/20/201917.49 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00116 1 02/20/201918:29 WG1239740 Toluene ND 0.00581 1 02/20/201918:29 WG1239740 Ethylbenzene ND 0.00291 1 02/20/201918:29 WG1239740 Total Xylenes ND 0.00756 1 02/20/201918:29 WG1239740 Methyl tert-butyl ether ND 0.00116 1 02/20/201918:29 WG1239740 Naphthalene ND 0.0145 1 02/20/201918:29 WG1239740 Di -isopropyl ether ND 0.00116 1 02/20/201918:29 WG1239740 (S) Toluene-d8 97.4 75.0-131 021201201918:29 WG1239740 (S) a,a,a-Trifluorotoluene 112 80.0-120 021201201918:29 WG1239740 (S)4-Bromof/uorobenzene 100 67.0-138 021201201918:29 WG1239740 (S)1,2-Dichloroethane-d4 109 70.0-130 021201201918:29 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 4.81 4.65 1 02/20/201910:38 WG1239459 (S) o-Terpheny/ 78.4 18.0-148 021201201910:38 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics ND 7.56 1 02/22/2019 00:32 WG1239744 Unadjusted C19-C36 Aliphatics ND 7.56 1 02/22/2019 00:32 WG1239744 Unadjusted C11-C22 Aromatics ND 7.56 1 02/22/2019 09:42 WG1239744 Unadjusted Total Petroleum ND 7.56 1 02/22/2019 09:42 WG1239744 Hydrocarbons (S) o-Terphenyl 74.1 40.0-140 0212212019 09.42 WG1239744 (S)1-Chloro-octodecone 71.1 40.0-140 0212212019 00:32 WG1239744 (S) 2-F/uorobipheny/ 94.2 40.0-140 0212212019 09.42 WG1239744 (S) 2-Bromonaphtha/ene 98.3 40.0-140 0212212019 09.42 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 28 of 48 SB-55 SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 13:00 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00698 1 02/21/2019 00:05 WG1239461 FTc Acenaphthene ND 0.00698 1 02/21/2019 00:05 WG1239461 Acenaphthylene ND 0.00698 1 02/21/2019 00:05 WG1239461 Benzo(a)anthracene ND 0.00698 1 02/21/2019 00:05 WG1239461 FS Benzo(a)pyrene ND 0.00698 1 02/21/2019 00:05 WG1239461 Benzo(b)fluoranthene ND 0.00698 1 02/21/2019 00:05 WG1239461 [Cn] Benzo(g,h,i)perylene ND 0.00698 1 02/21/2019 00:05 WG1239461 Benzo(k)fluoranthene ND 0.00698 1 02/21/2019 00:05 WG1239461 Chrysene ND 0.00698 1 02/21/2019 00:05 WG1239461 Dibenz(a,h)anthracene ND 0.00698 1 02/21/2019 00:05 WG1239461 Fluoranthene ND 0.00698 1 02/21/2019 00:05 WG1239461 6 QC Fluorene ND 0.00698 1 02/21/2019 00:05 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00698 1 02/21/2019 00:05 WG1239461 7 Naphthalene ND 0.0233 1 02/21/2019 00:05 WG1239461 GI Phenanthrene ND 0.00698 1 02/21/2019 00:05 WG1239461 Pyrene ND 0.00698 1 02/21/2019 00:05 WG1239461 FAI 1-Methylnaphthalene ND 0.0233 1 02/21/2019 00:05 WG1239461 2-Methylnaphthalene ND 0.0233 1 02/21/2019 00:05 WG1239461 2-Chloronaphthalene ND 0.0233 1 02/21/2019 00:05 WG1239461 FSC (S) Nitrobenzene-d5 76.8 14.0-149 0212112019 00:05 WG1239461 (S) 2-Fluorobiphenyl 71.8 34.0-125 0212112019 00:05 WG1239461 (S) p-Terphenyl-d14 79.7 23.0-120 0212112019 00:05 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 29 of 48 SAMPLE RESULTS - 12 L1071390 ONE LAB. NATIONWIDE. SB-58 Collected date/time: 02/14/19 13:05 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 81.2 1 02/20/201916:45 WG1239620 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 6.16 50 02/20/201919:46 WG1239645 Unadjusted C9-C12 Aliphatics ND 6.16 50 02/20/201919:46 WG1239645 Unadjusted C9-C10 Aromatics ND 6.16 50 02/20/201919:46 WG1239645 Total VPH ND 6.16 50 02/20/201919:46 WG1239645 (S)2,5-Dibromotoluene(FID) ill 70.0-130 021201201919:46 WG1239645 (S)2,5-Dibromotoluene(PID) 106 70.0-130 021201201919:46 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 3.08 25 02/20/201918:10 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 98.6 77.0-120 021201201918:10 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00123 1 02/20/201918:48 WG1239740 Toluene ND 0.00616 1 02/20/201918:48 WG1239740 Ethylbenzene ND 0.00308 1 02/20/201918:48 WG1239740 Total Xylenes ND 0.00801 1 02/20/201918:48 WG1239740 Methyl tert-butyl ether ND 0.00123 1 02/20/201918:48 WG1239740 Naphthalene ND 0.0154 1 02/20/201918:48 WG1239740 Di -isopropyl ether ND 0.00123 1 02/20/201918:48 WG1239740 (S) Toluene-d8 97.8 75.0-131 021201201918.48 WG1239740 (S) a,a,a-Trifluorotoluene 109 80.0-120 021201201918.48 WG1239740 (S)4-Bromof/uorobenzene 104 67.0-138 02/20/201918.48 WG1239740 (S)1,2-Dichloroethane-d4 141 11 70.0-130 02/20/201918.48 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction ND 4.93 1 02/20/201911:06 WG1239459 (S) o-Terpheny/ 77.4 18.0-148 021201201911:06 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics ND 8.01 1 02/22/2019 00:57 WG1239744 Unadjusted C19-C36 Aliphatics ND 8.01 1 02/22/2019 00:57 WG1239744 Unadjusted C11-C22 Aromatics ND 8.01 1 02/22/201910:06 WG1239744 Unadjusted Total Petroleum ND 8.01 1 02/22/201910:06 WG1239744 Hydrocarbons (S) o-Terphenyl 66.9 40.0-140 021221201910:06 WG1239744 (S)1-Chloro-octodecone 64.8 40.0-140 0212212019 00:57 WG1239744 (S) 2-F/uorobipheny/ 99.2 40.0-140 021221201910:06 WG1239744 (S) 2-Bromonaphtha/ene 105 40.0-140 021221201910:06 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 30 of 48 SB-58 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 13:05 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00739 1 02/21/2019 00:26 WG1239461 FTc Acenaphthene ND 0.00739 1 02/21/2019 00:26 WG1239461 Acenaphthylene ND 0.00739 1 02/21/2019 00:26 WG1239461 Benzo(a)anthracene ND 0.00739 1 02/21/2019 00:26 WG1239461 FS Benzo(a)pyrene ND 0.00739 1 02/21/2019 00:26 WG1239461 Benzo(b)fluoranthene ND 0.00739 1 02/21/2019 00:26 WG1239461 [Cn] Benzo(g,h,i)perylene ND 0.00739 1 02/21/2019 00:26 WG1239461 Benzo(k)fluoranthene ND 0.00739 1 02/21/2019 00:26 WG1239461 Chrysene ND 0.00739 1 02/21/2019 00:26 WG1239461 Dibenz(a,h)anthracene ND 0.00739 1 02/21/2019 00:26 WG1239461 Fluoranthene ND 0.00739 1 02/21/2019 00:26 WG1239461 6 QC Fluorene ND 0.00739 1 02/21/2019 00:26 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00739 1 02/21/2019 00:26 WG1239461 7 Naphthalene ND 0.0246 1 02/21/2019 00:26 WG1239461 GI Phenanthrene ND 0.00739 1 02/21/2019 00:26 WG1239461 Pyrene ND 0.00739 1 02/21/2019 00:26 WG1239461 FAI 1-Methylnaphthalene ND 0.0246 1 02/21/2019 00:26 WG1239461 2-Methylnaphthalene ND 0.0246 1 02/21/2019 00:26 WG1239461 2-Chloronaphthalene ND 0.0246 1 02/21/2019 00:26 WG1239461 FSC (S) Nitrobenzene-d5 75.6 14.0-149 0212112019 00:26 WG1239461 (S) 2-Fluorobiphenyl 67.2 34.0-125 0212112019 00:26 WG1239461 (S) p-Terphenyl-d14 74.3 23.0-120 0212112019 00:26 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 31 of 48 SAMPLE RESULTS - 13 L1071390 ONE LAB. NATIONWIDE. SB-61 Collected date/time: 02/14/19 13:13 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 82.7 1 02/20/201916:45 WG1239620 Volatile Petroleum Hydrocarbons by Method MADEPV Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C5-C8 Aliphatics ND 6.04 50 02/20/2019 20:19 WG1239645 Unadjusted C9-C12 Aliphatics ND 6.04 50 02/20/2019 20:19 WG1239645 Unadjusted C9-C10 Aromatics ND 6.04 50 02/20/2019 20:19 WG1239645 Total VPH ND 6.04 50 02/20/2019 20:19 WG1239645 (S)2,5-Dibromotoluene(FID) 112 70.0-130 021201201920:19 WG1239645 (S)2,5-Dibromotoluene(PID) 107 70.0-130 021201201920:19 WG1239645 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 3.02 25 02/20/201918:31 WG1239646 (S) a, a, a-Trifluorotoluene(FID) 98.5 77.0-120 021201201918:31 WG1239646 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00121 1 02/20/201919:07 WG1239740 Toluene ND 0.00604 1 02/20/201919:07 WG1239740 Ethylbenzene ND 0.00302 1 02/20/201919:07 WG1239740 Total Xylenes ND 0.00786 1 02/20/201919:07 WG1239740 Methyl tert-butyl ether ND 0.00121 1 02/20/201919:07 WG1239740 Naphthalene ND 0.0151 1 02/20/201919:07 WG1239740 Di -isopropyl ether ND 0.00121 1 02/20/201919:07 WG1239740 (S) Toluene-d8 98.1 75.0-131 021201201919:07 WG1239740 (S) a,a,a-Trifluorotoluene 112 80.0-120 021201201919:07 WG1239740 (S)4-Bromof/uorobenzene 100 67.0-138 021201201919:07 WG1239740 (S)1,2-Dichloroethane-d4 118 70.0-130 021201201919:07 WG1239740 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 6.21 4.84 1 02/20/201911:18 WG1239459 (S) o-Terpheny/ 68.7 18.0-148 021201201911:18 WG1239459 Semi -Volatile Organic Compounds (GC) by Method MADEPE Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Unadjusted C9-C18 Aliphatics ND 7.86 1 02/22/2019 01:20 WG1239744 Unadjusted C19-C36 Aliphatics ND 7.86 1 02/22/2019 01:20 WG1239744 Unadjusted C11-C22 Aromatics ND 7.86 1 02/22/201910:31 WG1239744 Unadjusted Total Petroleum 10.9 7.86 1 02/22/201910:31 WG1239744 Hydrocarbons (S) o-Terphenyl 60.3 40.0-140 021221201910:31 WG1239744 (S)1-Chloro-octodecone 60.0 40.0-140 0212212019 01:20 WG1239744 (S) 2-F/uorobipheny/ 96.8 40.0-140 021221201910:31 WG1239744 (S) 2-Bromonaphtha/ene 101 40.0-140 021221201910:31 WG1239744 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 32 of 48 SB-61 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE. Collected date/time: 02/14/19 13:13 L1071390 Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM Result (dry) Qualifier RDL (dry) Dilution Analysis Batch I Cl7 Analyte mg/kg mg/kg date / time u Anthracene ND 0.00725 1 02/21/2019 00:47 WG1239461 FTc Acenaphthene ND 0.00725 1 02/21/2019 00:47 WG1239461 Acenaphthylene ND 0.00725 1 02/21/2019 00:47 WG1239461 Benzo(a)anthracene ND 0.00725 1 02/21/2019 00:47 WG1239461 FS Benzo(a)pyrene ND 0.00725 1 02/21/2019 00:47 WG1239461 Benzo(b)fluoranthene ND 0.00725 1 02/21/2019 00:47 WG1239461 [Cn] Benzo(g,h,i)perylene ND 0.00725 1 02/21/2019 00:47 WG1239461 Benzo(k)fluoranthene ND 0.00725 1 02/21/2019 00:47 WG1239461 Chrysene ND 0.00725 1 02/21/2019 00:47 WG1239461 Dibenz(a,h)anthracene ND 0.00725 1 02/21/2019 00:47 WG1239461 Fluoranthene ND 0.00725 1 02/21/2019 00:47 WG1239461 6 QC Fluorene ND 0.00725 1 02/21/2019 00:47 WG1239461 Indeno(1,2,3-cd)pyrene ND 0.00725 1 02/21/2019 00:47 WG1239461 7 Naphthalene ND 0.0242 1 02/21/2019 00:47 WG1239461 GI Phenanthrene ND 0.00725 1 02/21/2019 00:47 WG1239461 Pyrene ND 0.00725 1 02/21/2019 00:47 WG1239461 FAI 1-Methylnaphthalene ND 0.0242 1 02/21/2019 00:47 WG1239461 2-Methylnaphthalene ND 0.0242 1 02/21/2019 00:47 WG1239461 2-Chloronaphthalene ND 0.0242 1 02/21/2019 00:47 WG1239461 FSC (S) Nitrobenzene-d5 70.4 14.0-149 0212112019 00:47 WG1239461 (S) 2-Fluorobiphenyl 70.0 34.0-125 0212112019 00:47 WG1239461 (S) p-Terphenyl-d14 80.4 23.0-120 0212112019 00:47 WG1239461 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 33 of 48 WG1239619 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 L1071390-01,02,03,04,05,06,07,08,09 Method Blank (MB) (MB) R3385659-1 02/20/19 09:37 MB Result MB Qualifier MB MDL MB RDL Analyte % % % Total Solids 0.00100 L1071390-01 Original Sample (OS) • Duplicate (DUP) (OS) L1071390-01 02/20/19 09:37 • (DUP) R3385659-3 02/20/19 09:37 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 81.7 81.9 1 0.289 10 Laboratory Control Sample (LCS) (LCS) R3385659-2 02/20/19 09:37 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. FP1 FTc FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 34 of 48 WG1239620 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 L1071390-10,11,12,13 Method Blank (MB) (MB) R3385703-1 02/20/1916:45 MB Result MB Qualifier MB MDL MB RDL Analyte % % % Total Solids 0.00200 L1071390-11 Original Sample (OS) • Duplicate (DUP) (OS) L1071390-11 02/20/1916:45 • (DUP) R3385703-3 02/20/1916:45 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 86.0 86.4 1 0.469 10 Laboratory Control Sample (LCS) (LCS) R3385703-2 02/20/1916:45 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 35 of 48 WG1239645 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Petroleum Hydrocarbons by Method MADEPV L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 Method Blank (MB) (MB) R3386778-3 02/20/1912:52 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Unadjusted C5-C8 Aliphatics U 1.67 5.00 Unadjusted C9-C12 Aliphatics U 1.67 5.00 Unadjusted C9-C10 Aromatics U 1.67 5.00 Total VPH 2.03 J_ 1.67 5.00 (S)2,5-Dibromotoluene(FID) 112 70.0-130 (S)2,5-Dibromotoluene(PID) 105 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3386778-1 02/20/1910:06 • (LCSD) R3386778-2 02/20/1910:39 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Unadjusted C5-C8 Aliphatics 1.20 1.11 1.01 92.5 84.5 70.0-130 9.08 25 Unadjusted C9-C12 Aliphatics 1.40 1.34 1.28 95.5 91.1 70.0-130 4.67 25 Unadjusted C9-C10 Aromatics 0.200 0.173 0.164 86.7 81.8 70.0-130 5.81 25 Total VPH 2.80 2.62 2.45 93.7 87.6 70.0-130 6.66 25 (S)2,5-Dibromotoluene(FID) 114 115 70.0-130 (S)2,5-Dibromoto/uene(PID) 110 110 70.0-130 L1071390-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071390-07 02/20/1917:01 • (MS) R3386778-4 02/20/19 20:52 • (MSD) R3386778-5 02/20/19 21:25 Spike Amount (dry) Original Result (dry) MS Result (dry) MSD Result (dry) MS Rec. MSD Rec. Analyte mg/kg mg/kg mg/kg mg/kg % % Unadjusted C5-C8 Aliphatics 1.45 ND 67.8 68.4 93.5 94.4 Unadjusted C9-C12 Aliphatics 1.69 ND 89.4 89.9 101 102 Unadjusted C9-C10 Aromatics 0.242 ND 12.1 12.3 100 101 Total VPH 3.38 ND 169 170 97.9 98.6 (S) 2,5-Dibromotoluene(FID) 115 112 (S) 2,5-Dibromoto/uene(PID) 110 109 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 50 70.0-130 0.913 25 50 70.0-130 0.539 25 50 70.0-130 1.29 25 50 70.0-130 0.711 25 70.0-130 70.0-130 FP1 FTc FSS [Cn] FSr �GI FAI [Sc ACCOUNT: ATC Group Services - SC - Speedway PROJECT: S W DP818901 SDG: DATE/TIME: L1071390 03/01/19 12:25 PAGE: 36 of 48 WG1239646 Volatile Organic Compounds (GC) by Method 8015D/GRO Method Blank (MB) QUALITY CONTROL SUMMARY L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 (MB) R3385572-2 02/20/19 11:28 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) Low Fraction 0.0246 J 0.0217 0.100 (S) o, o, o-Trifluorotoluene(FID) 95.3 77.0-120 Laboratory Control Sample (LCS) (LCS) R3385572-1 02/20/1910:45 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg % % TPH (GC/FID) Low Fraction 5.50 6.30 115 72.0-127 (S) 115 77.0-120 a, a, a- Trifluorotoluene(FID) L1071180-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071180-01 02/20/1913:55 • (MS) R3385572-3 02/20/1919:35 • (MSD) R3385572-4 02/20/1919:57 Spike Amount (dry) Original Result (dry) MSD Result MS Result (dry) (dry) MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/kg mg/kg mg/kg mg/kg % % % % TPH (GC/FID) Low Fraction 7.17 333 483 582 83.3 139 25 10.0-151 E E 18.6 oo-Trifluorotoluene(FID) a,, 105 109 77.0-120 ONE LAB. NATIONWIDE. RPD Limits 28 FP1 FTc FSS H 5 Sr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 37 of 48 WG1239740 Volatile Organic Compounds (GC/MS) by Method 8260D Method Blank (MB) (MB) R3386800-2 02/20/1914:35 MB Result Analyte mg/kg Benzene U Di -isopropyl ether U Ethylbenzene U Methyl tert-butyl ether U Naphthalene U Toluene U Xylenes, Total U (S) Toluene-d8 97.6 (S) a,a,a-Trifluoroto/uene 113 (S) 4-Bromof/uorobenzene 100 (S) 1,2-Dlch/oroethone-d4 105 MB Qualifier MB MDL mg/kg 0.000400 0.000350 0.000530 0.000295 0.00312 0.00125 0.00478 Laboratory Control Sample (LCS) QUALITY CONTROL SUMMARY L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 MB RDL mg/kg 0.00100 0.00100 0.00250 0.00100 0.0125 0.00500 0.00650 75.0-131 80.0-120 67.0-138 70.0-130 ONE LAB. NATIONWIDE. (LCS) R3386800-1 02/20/19 12:54 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg % % Benzene 0.125 0.105 84.2 70.0-123 Di -isopropyl ether 0.125 0.0787 63.0 60.0-136 Ethylbenzene 0.125 0.116 93.0 74.0-126 Methyl tert-butyl ether 0.125 0.103 82.5 66.0-132 Naphthalene 0.125 0.116 93.2 59.0-130 Toluene 0.125 0.114 91.3 75.0-121 Xylenes, Total 0.375 0.360 96.0 72.0-127 (S) Toluene-d8 94.0 75.0-131 (S) a, a, a-Trifluoroto/uene 110 80.0-120 (S) 4-Bromofluorobenzene 113 67.0-138 (S)1,2-Dich/oroethone-d4 120 70.0-130 L1071410-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071410-01 02/20/19 21:21 • (MS) R3386800-3 02/20/19 21:40 • (MSD) R3386800-4 02/20/19 21:59 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Benzene 0.131 2.08 4.49 3.94 92.1 71.1 20 10.0-149 13.0 37 Di -isopropyl ether 0.131 U 2.10 1.79 80.1 68.5 20 10.0-147 15.6 36 Ethylbenzene 0.131 189 244 210 2100 793 20 10.0-160 E V E V 15.1 38 Methyl tert-butyl ether 0.131 U 2.41 2.15 92.2 82.2 20 11.0-147 11.5 35 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 38 of 48 FP1 FTc FSS [Cn] FSr �GI FAI [Sc WG1239740 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 L1O7141O-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071410-01 02/20/19 21:21 • (MS) R3386800-3 02/20/19 21:40 • (MSD) R3386800-4 02/20/19 21:59 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % Naphthalene 0.131 29.7 32.4 29.1 101 0.000 Toluene 0.131 191 242 228 1940 1410 Xylenes, Total 0.392 520 827 634 3910 1450 (S) Toluene-d8 94.3 144 (S) o,o,o-Trifluorotoluene 107 877 (S) 4-Bromofluorobenzene 161 105 (S)1,2-Dichloroethone-d4 ill 83.4 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 20 10.0-160 V_ 10.5 20 10.0-156 E V E V 5.81 20 10.0-160 E V E V 26.4 75.0-131 11 80.0-120 67.0-138 11 70.0-130 ONE LAB. NATIONWIDE. RPD Limits 36 38 38 FP1 FTc FSS H FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 39 of 48 WG1239459 Semi -Volatile Organic Compounds (GC) by Method 8015C Method Blank (MB) (MB) R3385452-1 02/20/19 09:48 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) High Fraction U 0.769 4.00 (S) o-Terpheny/ 91.1 18.0-148 QUALITY CONTROL SUMMARY L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3385452-2 02/20/1910:01 • (LCSD) R3385452-3 02/20/1910:13 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % TPH (GC/FID) High Fraction 50.0 45.2 37.6 90.4 75.2 50.0-150 18.4 20 (S) o-Terpheny/ 110 88.0 18.0-148 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 40 of 48 FP1 FTc FSS [Cn] s Sr �GI FAI [SC WG1239744 QUALITY CONTROL SUMMARY Semi -Volatile Organic Compounds (GC) by Method MADEPE L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 Method Blank (MB) (MB) R3386148-1 02/21/1914:57 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Unadjusted C9-C18 Aliphatics U Unadjusted C19-06 Aliphatics U Unadjusted Total Petroleum U Hydrocarbons (S)1-Chloro-octadecane 80.1 Method Blank (MB) (MB) R3386148-4 02/21/1916:09 MB Result Analyte mg/kg Unadjusted C11-C22 Aromatics U (S) o-Terpheny/ 91.4 (S) 2-Fluorobiphenyl 97.4 (S) 2-Bromonaphtha/ene 102 2.17 2.17 MB Qualifier MB MDL mg/kg 2.17 6.50 6.50 40.0-140 MB RDL mg/kg 6.50 40.0-140 40.0-140 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3386148-2 02/21/1915:21 • (LCSD) R3386148-3 02/21/1915:45 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Unadjusted C9-C18 Aliphatics 39.9 29.0 29.7 72.7 74.4 40.0-140 2.39 25 Unadjusted C19-C36 Aliphatics 53.2 45.4 44.9 85.3 84.4 40.0-140 1.11 25 (S)1-Chloro-octadecane 69.5 675 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3386148-5 02/21/1916:34 • (LCSD) R3386148-6 02/21/1916:58 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyte mg/kg mg/kg mg/kg % % % % Unadjusted C11-C22 Aromatics 113 90.9 92.2 80.4 81.6 40.0-140 1.42 (S) o-Terphenyl (S) 2-Fluorobiphenyl (S) 2-Bromonaphtha/ene 85.7 85.7 40.0-140 976 95.9 40.0-140 102 99.8 40.0-140 RPD Limits 25 ONE LAB. NATIONWIDE. FP1 FTc FSS [Cn] FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 41 of 48 WG1239744 QUALITY CONTROL SUMMARY Semi -Volatile Organic Compounds (GC) by Method MADEPE L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 L1O71O64-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071064-02 02/21/19 21:20 • (MS) R3386148-7 02/21/19 21:43 • (MSD) R3386148-8 02/21/19 22:07 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/kg mg/kg mg/kg mg/kg % % Unadjusted C9-C18 Aliphatics 39.9 U 30.6 29.0 76.7 72.7 Unadjusted C19-06 Aliphatics 53.2 2.60 51.0 49.6 91.0 88.3 (S)1-Chloro-octodecone 70.7 67.3 ONE LAB. NATIONWIDE. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 40.0-140 5.37 50 1 40.0-140 2.78 50 40.0-140 L1071064-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071064-02 02/21/19 21:20 • (MS) R3386148-9 02/22/19 06:56 • (MSD) R3386148-10 02/22/19 07:19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/kg mg/kg mg/kg mg/kg % % Unadjusted C11-C22 Aromatics 113 U 96.4 94.4 85.3 83.5 (S) o-Terpheny/ 9t 5 90.0 (S) 2-F/uorobipheny/ 99.2 99.2 (S) 2-Bromonophtho/ene 105 104 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 40.0-140 2.10 50 40.0-140 40.0-140 40.0-140 FP1 FTc FSS [Cn] FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 42 of 48 WG1239461 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3385635-3 02/20/19 23:03 MB Result MB Qualifier Analyte mg/kg Anthracene U Acenaphthene U Acenaphthylene U Benzo(a)anth race ne U Benzo(a)pyrene U Benzo(b)fluoranthene U Benzo(g,h,i)perylene U Benzo(k)fluoranthene U Chrysene U Dibenz(a,h)anthracene U Fluoranthene U Fluorene U Indeno(1,2,3-cd)pyrene U Naphthalene U Phenanthrene U Pyrene U 1-Methylnaphthalene U 2-Methylnaphthalene U 2-Chloronaphthalene U (S) Nitrobenzene-d5 71.3 (S) 2-Fluorobiphenyl 75.2 (S) p-Terphenyl-d14 86.1 MB MDL mg/kg 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.000600 0.00200 0.000600 0.000600 0.00200 0.00200 0.00200 MB RDL mg/kg 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.00600 0.0200 0.00600 0.00600 0.0200 0.0200 0.0200 14.0-149 34.0-125 23.0-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3385635-1 02/20/19 22:22 • (LCSD) R3385635-2 02/20/19 22:43 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Anthracene 0.0800 0.0529 0.0481 66.1 60.1 50.0-126 9.50 20 Acenaphthene 0.0800 0.0579 0.0566 72.4 70.8 50.0-120 2.27 20 Acenaphthylene 0.0800 0.0586 0.0563 73.3 70.4 50.0-120 4.00 20 Benzo(a)anth race ne 0.0800 0.0526 0.0499 65.8 62.4 45.0-120 5.27 20 Benzo(a)pyrene 0.0800 0.0488 0.0462 61.0 57.8 42.0-120 5.47 20 Benzo(b)fluoranthene 0.0800 0.0501 0.0531 62.6 66.4 42.0-121 5.81 20 Benzo(g,h,i)perylene 0.0800 0.0517 0.0556 64.6 69.5 45.0-125 7.27 20 Benzo(k)fluoranthene 0.0800 0.0612 0.0657 76.5 82.1 49.0-125 7.09 20 Chrysene 0.0800 0.0628 0.0598 78.5 74.8 49.0-122 4.89 20 Dibenz(a,h)anth racene 0.0800 0.0500 0.0569 62.5 71.1 47.0-125 12.9 20 Fluoranthene 0.0800 0.0581 0.0561 72.6 70.1 49.0-129 3.50 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 43 of 48 FP1 FTc FSS [Cn] FSr �GI FAI [Sc WG1239461 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E-SIM L1071390-01,02,03,04,05,06,07,08,09,10,11,12,13 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3385635-1 02/20/19 22:22 • (LCSD) R3385635-2 02/20/19 22:43 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Fluorene 0.0800 0.0552 0.0555 69.0 69.4 49.0-120 0.542 20 Indeno(1,2,3-cd)pyrene 0.0800 0.0582 0.0656 72.8 82.0 46.0-125 12.0 20 Naphthalene 0.0800 0.0569 0.0555 71.1 69.4 50.0-120 2.49 20 Phenanthrene 0.0800 0.0550 0.0533 68.8 66.6 47.0-120 3.14 20 Pyrene 0.0800 0.0717 0.0659 89.6 82.4 43.0-123 8.43 20 1-Methylnaphthalene 0.0800 0.0598 0.0610 74.8 76.3 51.0-121 1.99 20 2-Methylnaphthalene 0.0800 0.0595 0.0570 74.4 71.3 50.0-120 4.29 20 2-Chloronaphthalene 0.0800 0.0580 0.0595 72.5 74.4 50.0-120 2.55 20 (S) Nitrobenzene-d5 85.6 80.9 14.0-149 (S) 2-Fluorobiphenyl 79.3 87.1 34.0-125 (S) p-Terphenyl-d14 85.9 80.2 23.0-120 L1071390-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1071390-01 02/21/19 05:56 • (MS) R3385635-4 02/21/19 06:17 • (MSD) R3385635-5 02/21/19 06:38 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % Anthracene 0.0965 0.268 0.418 0.365 155 105 Acenaphthene 0.0965 0.0436 0.122 0.0996 81.5 60.8 Acenaphthylene 0.0965 ND 0.0639 0.0497 63.9 51.6 Benzo(a)anth race ne 0.0965 2.66 3.67 3.18 1050 572 Benzo(a)pyrene 0.0965 3.21 3.94 3.48 761 293 Benzo(b)fluoranthene 0.0965 5.93 8.00 7.29 2140 1480 Benzo(g,h,i)perylene 0.0965 2.82 3.60 2.62 812 0.000 Benzo(k)fluoranthene 0.0965 0.883 1.40 1.03 532 156 Chrysene 0.0965 3.66 4.70 4.13 1080 505 Dibenz(a,h)anth racene 0.0965 0.697 0.960 0.890 273 210 Fluoranthene 0.0965 5.85 7.41 6.76 1610 984 Fluorene 0.0965 0.0478 0.122 0.105 77.0 61.7 Indeno(1,2,3-cd)pyre ne 0.0965 2.80 3.71 2.78 939 0.000 Naphthalene 0.0965 ND 0.0775 0.0656 60.8 50.8 Phenanthrene 0.0965 1.45 1.91 1.67 482 239 Pyrene 0.0965 6.28 7.05 6.12 799 0.000 1-Methylnaphthalene 0.0965 ND 0.0664 0.0506 64.3 50.2 2-Methylnaphthalene 0.0965 ND 0.0650 0.0480 62.0 46.4 2-Chloronaphthalene 0.0965 ND 0.0599 0.0487 62.1 52.9 (S) Nitrobenzene-d5 57.1 48.7 (S) 2-Fluorobiphenyl 68.2 56.4 (S) p-Terphenyl-d14 73.0 66.1 Dilution Rec. Limits 1 10.0-145 1 14.0-127 1 21.0-124 1 10.0-139 1 10.0-141 1 10.0-140 1 10.0-140 1 10.0-137 1 10.0-145 1 10.0-132 1 10.0-153 1 11.0-130 1 10.0-137 1 10.0-135 1 10.0-144 1 10.0-148 1 10.0-142 1 10.0-137 1 29.0-120 14.0-149 34.0-125 23.0-120 MS Qualifier V U EV V V V V EV V V EV MSD Qualifier RPD 13.5 20.4 25.0 V 14.3 V_ 12.5 E V 9.29 V_ 31.5 V 30.5 V_ 13.0 V 7.54 E V 9.16 15.5 V 28.7 16.6 V 13.7 E V 14.1 27.0 J3 30.1 20.5 ONE LAB. NATIONWIDE. RPD Limits o� 30 27 25 30 31 36 33 31 30 31 33 29 32 27 31 35 28 28 24 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: ATC Group Services - SC - Speedway SWDP818901 SDG: L1071390 DATE/TIME: 03/01/19 12:25 PAGE: 44 of 48 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. RDL (dry) Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J The identification of the analyte is acceptable; the reported value is an estimate. J1 Surrogate recovery limits have been exceeded; values are outside upper control limits. J3 The associated batch QC was outside the established quality control range for precision. J7 Surrogate recovery cannot be used for control limit evaluation due to dilution. v The sample concentration is too high to evaluate accurate spike recoveries. FP1 FTC FSS [Cn] FSr RC FAI FSC ACCOUNT: ATC Group Services - SC - Speedway PROJECT: SDG: DATE/TIME: PAGE: SWDP818901 L1071390 03/01/19 12:25 45 of 48 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T104704245-18-15 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID T WI NY SD WY MI NV T NE IA OH T PA T f IL Ills WY vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: ATC Group Services - SC - Speedway SWDP818901 L1071390 03/01/19 12:25 ME PAGE: 46 of 48 Ic--.a^cr '.n11yss%--rta nerj P-Pservative Chain of Custody Page of 11 ATC Group Services - SC - Speedway Accounts Payable Pres 7499 Parklane Rd., Ste 112 cnk aceAnal tala 7499 Parklane Road, Suite 112 Columbia, SC 29223a+eoaa. Columbia, SC 29223 E i x O QJ doss Lebanon Rd R1NrR Report to: Email To: Mr. Bob Bolton bob.bokon@atcassoclates.com;john.taylor@atcass . VI ar 0. `� Q 61S-djubet, 8-58s 3 L^C tiF�-4'J Pnone:6tsasa-sass t Phone: Phone: BW767�sas: 1� ra+-sts-Ise-sass ❑o,,,�,; Project SW 8189 Rocky NC City/State Collected: �Or.1-}, NL Description: point / ? U E L # Phone: 803-735-0003 Client Project # Lab Project # Swg/S%�� / pTCCSCSSA-8189 a H242 Fax r N z x - Collected by (print): Site/Facility ID # P.O. # < j R0� 00081890-036761 a j Ac<tnum:ATCCSCSSA Q d E C z Tem Iate:T145953 p Prelogin: P693373 Collect d y (signature): - RushT (Lab MUST Be Notified) Quote # ZGA✓/ Same Day _Five Day —Next U z Day —5 Day (Red OnHI Date Result Needed I N CO U w TSR: 341- John Hawkins Immediately Two Day _ 10 Day (Red Only) (' Ci No. S�GI �I C�F( eD y ,., O H m PB: 1- Packed on Ice IN Y� Three Day — of > N U n N O O iN Shipped Via: Fed EX Ground ntrs Sample 10 Comp/Grab Matrix • Depth Date Time cc Bemaks Sampinuiab onlyl > s[i o ss 6 1-7341 1250 X of Ski — 0111 SS I ZS$ X X x J� - l ss 13 ZS X X�i sB-/S ss 13351 X '1 sa - Ss ! 23 X X >s S a- Z 6 SS z-1 - so 3( x �- 33-ze ss 3 /0t5 XX x UI s8-3 7 ss 6" /InO Ci XX >( A SQ - 5- ss 1 l'18 I X 68 -s0 ss zy8 X * ( • Matrix:Remarks: _ _ Sarole Receipt Checklist COc Seal Present/Tntact NP ♦ N COC signed/Accurate: fL N Bottles arrive intact. —N SS - Soil AIR - Air F-Filter GW- Groundwater 8-Bioassay n� pH Temp ��r�s p tea' p MR1 r SrF`^-lv�J WW - WasteWater flnu Flow Other Correct bottles used: N DW- Drinking Water O7-Other Samples returned via: /_ 11P5 dFedEx Courier Trackin il g i�1C'—t �/O d� \ y(/a{ S �g'(�S 3 DG sufficient volume sent: _N If Arolicable (J / D i i VOA Zero Needspace: Y N Preservation Correct/Checked: _Y _N Relinquished by: (Signature) Date'. Time Received by (Signatire) Received Trip Blank Received: o T_ —' I �y �/(� Z— 1 V —1 / OO / MeoH G r/ TBR Relinquished by: (Signature) Date: Time: Received by: (Signature) Temp: _C Battles Received: If preservation required by Login: Date/Time bit-oi� SZ Relinquished by: (Signature) Date: Time: Receive for lab by: (Signature) Date Time: 2/19/l"1 Hold: Condition. NCF / OK � m00 ATC Group Services - SC - Speedway 7499 Parklane Road, Suite 112 Columbia, SC 29223 Billing Information Accounts Payable 'Pres 7499 Parklane Rd., Ste 112 JChk Columbia, SC 29223 Analysis/Container/Preservative Chain of Custody Page '7-of_ �JceA a! /cal' N.a„.c.,a �? 12065 Lebanon Rd O O Mount luliep TN 37122 Y Phone: 615]585s5s Phone'. 800-]6]-5959 :T� Fax 6l5J5s-5659 �,-; I, ` d 2 U H Cp F- vt Q 1' e0 ,>jr 0 to a` 0 Z -0 E xT U W N at a Zr U ,-Oy O E x O v AD E Q E o a U x Q. Z w p 10 > rN Report to: Mr. Bob Bolton Email To. bob.bollon@atcassociates.com;john.taylor@atcass Project Description: SW 8189 Rocky point INC City/State Collected R0J POf.T} �` LM J 1 D Phone: 803-735-0003 Fax Client Project 11 S(,t/+1�J gf gq OJ Lab Project a ATCCSCSSA-8189 Table N Collected by (print): ;� g4t771 � Site/Facility 10 x 0008189 0-036761 P.O. R Acctnum: ATCCSCSSA Tem late:T145953 p Prelogim P693373 TSR: 341-John Hawkins PB J / Collected by (signature): j /'✓/- Immediately Packed on Ice N_ Y_X RUshl (Lab MUST Be Notified) QYOt01i _Same Day Five Day _Next Day _5 Day (Red only) Date Results Needed Two Day 10Day (Rod Only) J No. _Three Day 5,��lF%Q .of shipped Via: Fed EX Ground Sample ID Comp/Grab Matrix' Depth Dale Time ntrs 11—ks Sarre r:ilebonlyi S%-55 G ss rJ—IH-I 1300 y X 513 —S ss 13Of S _ ss r 313 iX ,Y i 3 "Matrix: SS -Sail AIR -Air F- Filter GW- Groundwater B- Bioassay WW - Waste Water DW- Drinking Water OT - Other emafks: FEN: <0.5 m Pg1r pH temp [�� _. t- Flow_ Other Samples re�reed Via: _UPS =Ex _Courier Tracking If Sarple Rereipt Checklist CDC Seal Presenc/Intacc: _NP _N COC signed/Accurate: g _N �Y Bottles arrive intact: y _N Correct bottles used: Y/ N Sufficient volume sent: _$ _N I£ Applicable VOA Zero Headspace: Y N Preservation Correct/Checked: _Y _N Relinquished by : (Signature) 7 Gam/ —11-7Z Date: Z —18 —1 1q Time: 1 700 t Received by: (Signaure) Trip Blank Received: GYN. L MeoH TBR Relinquished by: (Signature) Date: Time: Received by: (Signature) Temp: °C Bottles Received: F If preservation required by Login: Date/Time Relinquished by : (Signature) Date: Time'. Received for lab by: (Signature) /� Date. p //!. Time p: �l �fl("I O (QO Hold: Conditioryr NCF / t� Initial Abatement Action Report Speedway No. 8189 Speedway No. 8189 APPENDIX B Waste Manifests March 29, 2019 . , 1 NON -HAZARDOUS WASTE MANIFEST Please print or type (Form designed for use on elite (12 pitch) typewriter) NON -HAZARDOUS WASTE MANIFEST 1 1. Gene tor's US EPA ID No. Manifest Document No. 2. Page 1 ti of 3. Generators Name and Mailing Address / � r Yr FfI- V s'#Vf,, 7 e 4. Generator's Pnone o C N 5,Transporter 1 Comp y Name 6. _ EPA ID,Number r A. S€ateTransorters ID '7 B.Transporter I Phone {�..60- 7. Transporter 2 Company Name 8. US EPA P flumber C. State Transporter's ID O. Transporter 2 Phone 9. Designated Facility Name and Site Address 10. US EPA ID Number E. State Facility's JD MR FARMS, LLC MONROE ENZOR RD FAIR BLUFF, NC 28439 F. Facility's Phone P0 BOX 381 TABOR CITY NC 28463 910-640-2608 11. WASTE DESCRIPTiflN 12. Containers 18. 14 Total Unit No. Type quantity Wt.Atol. a. PETROLEUM CONTAMINATED SOILS / 913 T G b. ( �J E N E R e. A T O R d. W H in CCG. Additonal Descriptions for Materials Listed Above CIO O�� �O 1 o H � �7 M 44 k 15. Special Handling Instructions and Additional Information z EMERGENCY PHONE # 910-625-a012 O z WWJ LJC WEIGHMASTER SIRES T NE -30 5--/�t._C H. Handling Codes for Wastes Listed Above 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shtpment are fully and accurately described and are in all respects in proper conditlon for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Date Printed(Typed Name ,t Signature Month Day Year T 17. Transporter 1 Acknowledgement of Receipt of Materials Date A Printed/Typed Name . Signature Month DaY Year P h 18. Transporter 2 Acknowledgement of Receipt of Materials k R Date T Printedllyped Name Signature Month Day Year fi F 19. Discrepancy Indication Space A C I L 20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. Date T Y Prints peame . r, lame � � /� _ _ Signature D � Month � ­, Day Year , . �.. n IABELIhAS FR 3(300) 621-5808 www.iabolmaster.com �Rev. a195 PRINFED ON RECYCLED PAP rvll�rro vnra �l IISIN� SIIYRFEN INV lyw.�w�M WEIGHT TICKET DRIVER ON ❑ IIYA �LNHCGH TEFL ©RIVER OFFUCEN❑ SE EXPIRES JUNE' 30, 2019 BAN Co _ 41409 IINALI© NLESS Sl NED SELLER BUYER ADDREE COMMC REMARKS # ❑2718 GROSS] TARE NET GROSS SHIPPER TARE NEIGHER NET/777 C) NON -HAZARDOUS WASTE MANIFEST Please print or type (Form designed for use on elite (12 pitch) typewriter) NON —HAZARDOUS 1. Generator's US EPA ID No. Manifest WASTE MANIFEST. 111A Document No. 3. Generator's Name and Mailing Address �.` . j�.�� �� (h Z-Z ( Us i- Wj ( l 7 4. Generator's Pnone !mod , Al(_ 5. Transporter 1 Company Name 6. US EPA IQ Number 7. Transporter 2 Company Name 8. US EPA ID Number 9. Designated Facility Name and Site Address 10. US EPA ID Number S&R FARMS, LLC MONROE ENZOR RD. FAIR BLUFF, NO 28439 PG BOX 381 TABOR C" NO 28463 11. WASTE DESCRIPTION a. PETROLEUM CONTAMINATED SOILS AIM E N E R e. A T O R d- W v G. Additonai Descriptions for Materials Listed Above a Q15. Special Handling Instructions and Additional Information zIlk EMERGENCY PHONE # 910-625-W12 O Z A. State Transorters ID 2. Page 1 of l L. Transporter 1 Phone R j 17 Z4 0' � C. State Transporter's ID D. Transporter 2 Phone E. State Facility's ID j F. Facility's Phone 910-UO-2608 12. Containers 13. Total No, Type Quantity 'SJ E3o, H. Handling Codes for Wastes Listed Above 16. GENERATOR'S CERTIFICATION. I hereby certify that the contents of this shipment are fuify and accurately described and are in all respects in proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Printed/Typed Name / _ ) / R,04,1+ I,/i St-IGj Signature TR 17. Transporter 1 Acknowledgement of Receipt of Materials N PdntedpGetl ma/ L]j% .. Signat e - P t O 19.T porter 2 Acknowied ent of Reoe of Materials E Printedfryped Name Signature R F 19. Discrepancy Indication Space A C 1 20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. T Y Printedffy Name �Z/I ;-t _ „ � _ _ i Signature 14. Unfit WtJVo1, T Date Month Day Year 1� Date K Alf h Day I1L1 /� Month Day Year Date F-14 ®206{ LA$ELM` .ASTER (RBOO) 621-SBOB www.labolmaster.com Rev. 3/95 P/ PRIMED ON RECYCLED PAPER L-T WAN USING SOYBEAN INK ur WEIGHT TICKET DRIVER ON ❑ �OLINA � wl= DRIVER OFF ❑ P(RESJ: WVALlD UjVLES it SELLE BUYEI ADDR COMB REMARKS GROSS TARE NET "' ^� GROSS,r SHIPPER �. !`^' TARE !� WEIGHER NET 7 - ,1 3 NON -HAZARDOUS WASTE MANIFEST Please print or type fForm designed for use on PIRA 119 nitrhl WritArti W H u} U) 0 0 a N a z z 0 z NON -HAZARDOUS 1. Generator's US EPA ID No. Manliest 2, Page 1 Document No. WASTE MANIFEST IV/1 of 3. Generator's Name and Mailing Address w,� ,�47 /'Fj (� �t { j ' 4. Generators Pnane ( ) f�Ql '�7`j A 5. Transporter 1 Company Name H' 9 6. " ' , US EPA ID Number ✓ A. State Transorter's ID "7 / ✓ J 6. Transporter 1 Phone Aq 7. Transporter 2 Company Name 6. US EPA ID Number C. State Transporters ID D, Transporter 2 Phone 9. Designated Faciiity Name and Site Address 10. MR FARMS, LLC US EPA ID Number F. State Facility's ID MONROE ENZOR RQ FAIR BLUFF, NC 28439 PQQ BOX 38_ 1 TABOR C" NC 28463 F. Facility's Phone 910-640.2608 11. WASTE DESCRIPTION 12. Containers 13. 14. No. Type Total Quantity Unit Wt./Vol. a. PMOLEUM CONTAMINATED SOILS ^7 3 (' �7 °tom T G b. E N E R c. T O EXPIRES JUNE 3c 2019 R d. L D SS GN G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above 03 15. Special Handling Instructions and Additfenai Information EMERGENCY PHONE # 81"25-5012 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fWy and accurately described and are in ail respects in proper condition for transport. The materials described on this manifest are not subject to federal -hazardous waste regulations. b Date Printed/Typed Name e 90&e_ i n t c Signature Month Day Year T 17. Transporter 1 Acknowledgement of Receipt of Materials Dare Priy�ted/Typed Name � Signature / Mor11h Da Year p !f(` ! f}'t ✓ t lam` 'Yl ��y R16. Transporter 2 Admowlecigement of Receipt of Materials Date T E Printedrryped Name Signature Month Day Year R F 19. Discrepancy indication Space A b f L 20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. Date T T Printe e ed Na ry / i nature Manlh Day Y r � Q Q F-14 ®2[)02 LABE[NfASTFR �800) 62]-5808 www.labelmaster.cpm pR1NFH1 ON NECYCLEO PAPER Rev. 3/95 !// IIA HN�1EV WnM IISINf, S[IYBFAN INK / C1114/�MK WEIGHT TICKET DRIVER ON ❑ NOWC0L1NA DRIVER OFF ❑ LOPl S "FUME 30, X10 COY� I41400 SELLER BUYER ADDRESS COMMODITY_ REMARKS #�,r1w9 --Fo # 122755 GROSS -50 EJ 7dL [� TARE NET CUSTOMER NO. ' CITY 0 PRICE DATE GROSS 79 SHIPPER (��TARE a WEIGHER NET1 22c) NON -HAZARDOUS WASTE MANIFEST Please print of tvoe (Form dasirrnari rnr isca nn a)it, !i � . i,..hr > W H N 0 a� a N a z z NON -HAZARDOUS 1 1.GeneraAto�r US EPA No. \ n+� /} WASTE MANIFEST 04 � CAS/� Manifest 2. Paget Document No. /Y pl of 3. Generators Name and Mailing Address z e 1 'vJr IA1r! 4. Generators Pnone { } �.] I 5. Transporter t Company Name 6. - U&fPi ID Number A. State Transorter's ID Q .Q B.TransporterlPhone 7. Transporter 2 Company Name 8. u5 Eipl irAumber C. State Transporters ID D. Transporter 2 Phone 9. Designated Facility Name and Site Address 10, US EPA ID Number SBtR FARMS, LLC E. State Facility's ID MONROE ENZOR RD FAIR BLUFF, NC 28439 F. Facility's Phone 910-6402608 PO BOX 381 TABOR C" NC 28463 %�� �` /9` j CA b�t� 11. WASTE DESCRIPTION 12. Containers 13. 14. Na. Total Unit Type Quantity Wt'NbI. a. PETROLEUM CONTAMINATED SOILS J_ �.. i 9 T E N E R c. A WEIGHMASTER T O EXPIRES JUKE 30, f . R d• G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above 15. Special Handling Instructions and Additional Information EMERGENCY PHONE # 910-625-5012 E -�. x , .'fk' . �"'yP .A �. ;ar--,� fi..x'T -:- w ^i�'i x'1.'-`'T�-� � k..b -.tit' '.:.7^'t • �°r' - "'"i�':4 � ^^�.' e 16. GENERATOR'S CERnFICATION: I hereby certify that the contents of this shipment are fully -and accurately described and are in all respects in proper condition for transport, The materials described on this manifest are not subject to federal hazardous waste regulations. a Hate Printed(Typed Name Signature %� tt Month Day �C.iC.� t z Year t ,\ :: p 0 v T17. Transporter 1 Acknowledgement of Receipt of Materials - Date ateDaY NPrirytedlfyped Name Signature Month Year a1 R 16. Transporter 2 Acknowledgement of Receipt of Materials Data E Printed/Typed Name Signature Month t]ay Year R F 19, Discrepancy Indication Space A C L20, Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. I Date T Y Printi ped ame Signatur Month ay Ye C O 2 F-140/002 LAREAASTF.RCR800)(121-5008 www.labolmaster.com/1% Rev. PRINTER OH RECYCLE6 PAPEJjjk R ilFyrtY mrx IIFINf FnYRFAN INN IUIf WEIGHT TICKET DRIVER ON ❑ NMNCARMIN. RoxwEmMASTER DRIVER OFF ❑ � m'[fZ�S JEQ2,, l�Cl SELLER BUYER ADDRE,r COMMC REMARKS GROSS TARE JS' NET 27 910 7 GROSS 10,? SHIPPER TARE �� J WEIGHER NET J �7, 9/0 NON -HAZARDOUS WASTE MANIFEST Please print or type {Form designed for use on elite (12 pitch) typewriter) NON -HAZARDOUS 1. Generator's US EPA ID No. WASTE MANIFEST Manifest 2. Page 1 Document No. 3. Generator's Name and Mailing Address C r A s ?/ Q of ✓i/ I�1 �I�i��►� ll7 f u't� 4. Genorator's Phone { ) 41 1 AJ 5. Transporter 1 Company Name 6. S EPA iD Number A. State Transorter s [D 7.Transporter2 Company Name 8. U8 EPAfbiflumber B.Trenspbrier 4 Phone C. State Transporters ID D. Transporter 2 Phone F. State Faciliys ID 9. Designated Facility Name and Site Address to. US EPA ID Number SM FARMS, LL.0 MONROE ENZOR RD FAIR BLUFF, NC 28439 F. Facirty's Phone 910-6402608 PQ BOX 381 TABOR WY NC 28463 14. WASTE DESCRIPTION 12. Containers 13. 14. No. Total Unit Type quantity Wt.Nol. a. PETROLEUM CONTAMINATED SOILS �. (!5 T G b. E N E R c. A . p EXFfRIvS ,[IJIVE 30. % R d. W � Q G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above V) o_ �lo 4 T1 F7433 cc a Q15. Special Handling tnslructions and Additional Information z EMERGENCY PHONE # 910-625-5012 O 16, GENERATOR'S CERTIFICATION: I hereby corhfy that the contents of this shipment are fully and accurately described and are in ail respects in proper condition for transport.The materials described on this manifest are not subject to federal hazardous waste regulations. Date 9Pmd�jr/�Ay �� Signat SA/J Month Day Year LL R7. Transporter 1 Ack wiedgement of Receipt of Materials Date ire I�Fd14� iE Signature $— P � J Month DaY Year Q0 18. Transporter 2 Acknowiedgement of Receipt of Materials A pale T Printed/Typed Name Signature Month pay Year 19. Discrepancy Indication Space A C 20. Facility Owner or Operator, Certification of receipt of the waste materials covered by this maifest, except as noted in item 19, Data T Signature Month Day Year A 'a P-14 ® 2 LARELAAMU (R800) 621.5808 www..labelmastencom ®PRfNTED ON RECYCLED PAP r�iRrro wire USINGSOYBEAN Rev. 3195 IN Jctyvty![ WEIGHT TICKET DRIVER ON ❑ NORMCARMIM PUBMWEIGHMMTER DRIVER OFF ❑ L'CE nfzl-�-EXPIRES JUNE 3p2019 3ELLER 3UYER NDDRE: �OMMC 3EMARKS GROSSl TARE NET GROSS SHIPPER TARE s�j / L-0 NEIGHER NET -2 �j J -11 NON -HAZARDOUS WASTE MANIFEST Please t3r€nt or tVDe Morrn rlwsinnr l fnr ­ nr, alit, rin ..ii.. } ---- NON -HAZARDOUS 1. Generator v Alp o. Manifest Page 1 WASTE MANIFEST �rC ��/� T2. DocumentNc. .}%0� of 3. Generators Name and Maii€ng Address b� �/ F9 4. Generator's Pnone ( } 1� 5.Transporter 1 Wy Na a 6. EPA ID Numb r A. State Transortees ID fZ B. Transporter 1 Phone Q 1. 7. Transporter 2 Company Name 8. US EPA I mhor C. State Transporters ID - D. Transporter 2 Phone a. Designated Facility Name and Site Address 14. US EPA ID Number SSR FARMS, LLC E. State Facility's ID MONROE ENZOR RQ FAIR BLUFF, NC 28439 I 1 arity's Phone 910-640-2808 RQ BOX 381 TABOR WY NC 28463 ���— 11. WASTE DESCRIPTION 12. Containers 13. 14. N, Total Unit Type Quantity WL/VoL a. PETROLEUM CONTAMINATED SOILS l0 q T G b. E N E R c- A .. WEfGHMASTE T EVIREIS JUNE 30, O 19 R d. A �Imm ©� �Sl G. Additenai Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above 15. Special HandNng Instructions and Additional information EMERGENCY PHONE # 910-626-N12 HOC' 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects in proper condition for transport. The materiais described on this manifest are not sublect to tederal Hazardous waste regulations. .e. Date Printed/Typed Name ,+p Q 1 % �/} ttl3 CAA 4't�ilf b� �K7+,./s11 Signature �' // z L./ Month Day JYear 2 r' 1 TR 17. Transporter 1 Acknowledgement of Receipt of Materials Date A N P6ntedlfyped Name Sfgnatu Month Day_ Year ? 4 �� R18. Transpe r 2 Acknowledgement of Receipt of Materia€s t Date T E Printed/Typed Name Signature Month Day Year R 19. Discrepancy Indication Space A C 1 20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this rnaifest, except as noted in item 19. �4 42 Date T Y Vrint7ed me a A e /,;"Ajlj =Q '--A4 )�-_) Signature ` Month DaI ;2- y Ysa F-14 ® 2 L4Bt L ASrFR41(ti00) 621-5848 wwW.laholmasiercam A� Rev.3/95 PRINTED ON RECYCLED PAP PRiMTE6 W11X actor enwrxu ieov 1 n......... WEIGHT TICKET DRIVER ON ❑ MORT"CAR�IGI HMMTER DRIVER OFF ❑ LCEW , "RES � UNE 3012010 41409 SELLER BUYER ADDREE ll=MARKS GROSS `f !�J 9 TAREQ'l7 NET 0 <), 77 GROSS T�iJ 3� C) SHIPPER TARE Z> AIEIGHER % NET C /- o NON -HAZARDOUS WASTE MANIFEST Please print or type (Form desioned for use on elite 112 nitchl tvnewritPr) UJ H N 0 0 a N Q z 0 z NON —HAZARDOUS WASTE 1. Generator's US EPA ID No. Manifest Document No. 2. Page 1 MANIFEST 11114 of 3. Generator's Name and Mailing Address Sf - _1 carat 61?7 �i2,1 V D 17�i✓ 117 4. GeneratDeS Phone { �QCA/y/ 01,41 ✓� 5.Transporter 1 Company Name 6. US EPA ID Number A. State Transorter's ID B.Transpdrter l Phone Ito �J--Z£y1J .�4 7. Transporter 2 Company dams a. US EPA ID Number C. State Transporter's ID D. Transporter 2 Phone 9. Designated Facility Name and Site Address 10, US EPA ID Numbor MR FARMS, LLC E. State Facility's ID MONROE ENZOR RD FAIR BLUFF, NC 28439 PQ BOX 381 TABOR CITY NO 28463 1 F. Facility's Phone 910-8402608 11. WASTE DESCRIPTION 12. Containers 13. 14, No. Type Total Quantity Unil WI.Nol. a. PETROLEUM CONTAMINATED SOILS s irT G b. E N E R e- WEfGHMASTER pA ElCP1EF5 JUNE 30, 2 19 R d. 41 �� UN G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above Alt,5,zg jZ I S 15. Special Handling Instructions and Additional Information EMERGENCY PHONE # 910-825-W12 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects In proper condition for transport.The materials described on this manifest are not subject to federal hazarclous waste regulations. Date pPrinttedfryped Namef r / PZt� Wfl? �i( cr TL "r • .a169 Signature ` Month Day Year TR 17. Transporter 1 Acknowledgement of Receipt of Materials Date Print yped ar+ J Signature Month Day Year 5 P e" R 18. Transporter 2 Ackn dgement of Receipt of Materials Dale T Printed/Typed Name Signature Month Day Year R 19. Discrepancy Indication Space A C L20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. Date T Y PrintedrT d Na a Signature Month Day YearIIIJ F-14 Q 91 L V TM 0t640) 621-5808 www.labalmaster.com AM pPoNTEO ON RECYCUtl ?AP R,K,- x-.,,, Rev. 3195 t1SENG SOYBEAN INK Cnvwr WEIGHT TICKET DRIVER ON ❑ CAMXNA DRIVER OFF ❑ � R E EXPIRES JUKE , PA 00 SELLER BUYER ADDRESS COMMODITY REMARKS :# ,5Fl,V4 # 122761 GROSS 7X0 TARE NET 76 o CUSTOMER NO.li L X- CITY PRICE DATEc� GROSS �j 7XO SHIPPER) g fb TARE WEIGHER �L NET 'v NON -HAZARDOUS WASTE MANIFEST Please print or type (Form designed for use on elite (12 pitch) typewriter) NOWHAZARDOUS I- Generators US EPA ID No. Manifest WASTE MANIFEST Document No, 3. Generator's Name and Mailing Address d1,�P�� t 17/y9 '�•z 1 fAvvl % cA w-k1-1 4, Generators Phone ( ) S. Transporter 1 Company Name 6. S EPA ID Number A S T at 7. Transporter 2 Companv Name & US EPA 9. Designated Facility Name and Site Address 10. US EPA ID Number S&R FARMS, LLC MONROE ENZOR RD FAIR BLUFF, NC 28439 PQ BOX 381 TABOR C" NG 2840 11. WASTE DESCRIPTION a. PETROLEUM CONTAMINATED SOILS G b. E N E R c. A T 0 W R a. CUD G. Additonal Descriptions for ateriels Listed Above #o� 1z� 1�o )7.61( % Q15. Special Handling Instructions and Additional Information EMERGENCY PHONE # 91Q-625-5092 z 2.Page 1� of late ransorters ID H. Transporter 1 Phone Q r� C. State transporters ID D. Transporter 2 Phone - E. State Facility's ID F. Facility's Phone 914-1640-2608 12. Containers 13. Total No. Type puantity J- IR JUNE 30, H. Handling Codes for Wastes Listed Above 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fuliy�and accurately described and are in all respects in proper condition for transport. The materials described on this manifest are not subject to f deral hazardous waste regulations. PrintedtTyped Name �( r Signature �r'f A L R a e�zl, l R17. Transporter I Acknowledgement of Receipt of aterials APri hyped a '" Slgnatur S P QS 18. Transports 2 Ack dgoment of Receipt of Materials EPrinted/Typed Name Signature R F 19. Discrepancy Indication Space A L20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19, T PrintedM Nam I% Signature Y ,V/TON �ri7 i,.�i 14. Unit WWoI, T Date Month Day Year Ar ! Date Month DaY Year Date Month Day Year Date Month Day Year F•14 0 200/ LABEu-tgal tIt IR800) 621-5808 wvnv.fabalmastercom/6 � JJ PRiMEUO; RELY 0IAPE rrun¢o _ Re. '�g5 t15}NG SOYaERN fN / envrur WEIGHT TICKET DRIVER ON ❑ DRIVER OFF ❑ � 16 WEIG� R �'AN EXplRC S _1 ME {?. 20 �� EER BUYER /I 3UYER kDDRESS---i COMMODITY , REMARKS GROSS �p2� / C . Q TARE c -o NET 27 J 7/Gf k 6) CUSTOMER NO. 1 . 4 NC I CITY PRICE DATE,-,l -1 GROSS TARE' SHIPPERS !� NEIGHER NET 37J 7/ ' NON -HAZARDOUS WASTE MANIFEST Please print or type (Form desianed for use on elite 112 nitchl tvnewritart NON -HAZARDOUS I - Genemtors US EPA ID No. Manifest 1 MANIFEST . °ocument"°WASTE r2P,ge 3. Generators Name and Mailing Address wy 117r��-�, 4. Generators Phone ( ) C 5,Transporter 1 Company Name 6. PA ID Number A. StateTransorters ID B.Transporteri Phone Q, 7.Transporter 2 Company Name 8. US EPA:P Aumber C. State Transporters ID D. Transporter 2 Phone 9. Designated Facility Name and Site Address 10. US EPA ID Number S&R FARMS, LLC E. State Facility's ID MONROE ENZOR RDA FAIR BLUFF, NC 28439 Pa BOX 38.1 TABOR CITY NO 28463 1 F. Facility's Phone 910-640-2608 11. WASTE pESCRIPTION 12. Containers 13. 14. No. Type Total Quantity Unit Wtivol. a. PETROLEUM CONTAMINATED SOILS i'"� G b. E N E R c. A T O Ll FIRES JUKE 30, 19 R d. G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above Ja 701y:) f S. Special Handling Instructions and Additional Information EMERGENCY PHONE # 910-525-5012 16. GENERATOR'S CERTIFICATION, I hereby certify that the contents of this shipment are f0y-and accurately described and are in al€ respects in proper condition for transport The materials described on this manifest are not subject to federai'hazardous waste regulations, Date Printedrlyped Name ft kok.,� Signature Month Day Year k1;, %r1C/ iC 0� a' r 2— is- TT 17. Transporter 1 Acknowledgement of Receipt of Materials Date A Print ypedName 7 SignatureN Month Year A ?paS' 0 1 S. Transporter 2 Acknowledgement of Receipt of Materials Date T E PrintedTTyped Name Signature Month Day Year R F 19. Discrepancy Indication Space A C [ L 20. Facility Owner or Operator; Certification of receipt of the waste materials covered by this maitest, except as noted in item 19. [ Date T Printe d N e Signature Mn fh Day Year Y 1 4?—. / 1LLk' - - 1'(Y-V Y F-1402 2 LABEMAS Q000)621-5808 www.labelmastercom Pa1NTE00r1RFCYCLEp PAPf;r rniMno wrtn Rev. 3195 116) Mi,ip cnvaonu iu�r ,,,,.r WEIGHT TICKET DRIVER ON ❑ DRIVER OFF ❑�ER I G MASS TER 110aE EXPIRES JUKE 30, 2019 RBI Cow C 4140g 3ELLER 3UYER %DDREc, 10MMC 3EMARKS # 122762 GROSSI-��(?J 00 TARE J �J2,yo NET ?-�/oc) GROSS SU J / O -0 SHIPPER TARE. NEIGHER NET 27 Q o r l \i 0 ,S �-, S) NON -HAZARDOUS WASTE MANIFEST Please print or type (Farm designed for use on elite N2 ritch5 fVneWrii W I-_ CA W a Ix z Z NON -HAZARDOUS 1. Ge�ner/afors US EPA ID No. Manifest 1 Document No. WASTE MANIFEST 4 T2-ge 3. Generator's Name and Mailing Address [^� � � VIp ey 8zar vs HWY 1(17 6;6,9 .�, 4. Generators Prone 5.Transporter 1 Company Name _ 6. US EPAIA Number A. StateTmnsorter's ID B. Transporter 4 Phone ��® --6,ygg �6 ,/ tl,4 7. Transporter 2 Company Name 8. US EPA ID Number C. State Transporter's ID D. Transporter 2 Phone 9. �DDe�ssi��g9nnatteedAFFaacility Name and Site Address 10. US EPA ID Number S&R FARMS, LLC E. State Facility's ID MONROE ENZOR RD FAIR BLUFF, NC 28439 P10. BOX 381 TABOR 0" NC 28463 F. Facility's Phone 910-640-2608 11. WASTE DESCRIPTION 12. Containers 13. 14. 14 No, Type Total Quantity Unit Wt.Nol. a. PEMOLEUM CONTAMINATED SOILS / # 4 _- T G b. E N E R c. A PU �,�5 C WEIGH' 0 EXJUNE 3D R d 41MO G. Additonal Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above Il ti, 15. Special Handling Instructions and Additional Information P , . EMERGENCY PHONE # 910-025-5012 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully_ and accurately descrbed and are in all respects in proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Date PrinfedlTyped Name / r�Or �T WfhT,s t/Cl e/T� n La' l o Signature Month Day_ Year TT 17. Transporter 1 Acknowledgement of Receipt of Materials Date A Pr dlTyped Name SignatQre Month Day Year o 18. Transporter 2 Ackn owl ed gems nt of Receipt of Materials Date T E Printedlryped Name Signature Month Day Year F1 F 19. Discrepancy Indication Space A C 1il 20. Facity Owner or Operator; Certification of receipt of the waste materials covered by this maifest, except as noted in item 19. Date T Y ed(F � Nam PrintjeZ Signature Day Year �h F-140L.ABELAASMR800) 621-6608 www.labelmastercom PRINTED ON RECYCL£Q PAPE �rEo wnx Rev. 3195 AS USING SDYBEA14,-1 SOIViNK WEIGHT TICKET DRIVER ON ❑ NORM DRIVER OFF ❑ le W--kxft m4swrr WF!qHW8TER � 3 41409 SELLER BUYER ADDRE,c COMMC REMARKS # 122763 GROSs,f�77v TARE NET GROSS � 7 t7 SHIPPER �j- n-C> TARE c WEIGHER NET fi