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HomeMy WebLinkAboutWQ0019098_Residual Annual Report 2014_20150302TOWN OF HOLLY SPRINGS, NC RESIDUALS LAND APPLICATION PROGRAM, Permit No. WQ0019098 2014 ANNUAL REPORT Town of Holly Springs, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM Permit Number W00019098County Wake Year 2014 Facility Name (as shown on permit) Utley Creek WWTP NPDES No. NC0063096 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A and Part Band proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. PART A Total number of application fields in permit: 41 Total number of fields land application occurred during the year: 8 Total amount of dry tons applied during the year for all application sites: 377.66 Total number of acres land application occurred during the year: 265.5 PART B Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality X YES NO. If no, Please provide a written description why the Facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (Applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality. Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ll (-"1 /-) Seann Byrd Director of Water Quality Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9(r) 2015 Signature of Land Applier Date (if different from Permittee and Preparer) DENR FORM ACF (5/2003) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION HOLLY SPRINGS, NC '' OLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID DRY METRIC MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS February 2014 601,400.00 G 45.14 D 40.94 March 2014 279,000.00 G 20.94 D 19.00 April 2014 750,200.00 G 55.38 D 50.22, May 2014 204,600.00 G 15.11 D 13.70 June 2014 632,400.00 G 46.68 D 42.34 August 2014 1,215,200.00 G 85.14 D 77.21 October 2014 936,200.00 G 75.34 D 68.35 December 2014 421,600.00 G 33.93 D 30.78 YEARLY TOTAL 5,040,600.00 G 377.66 D 342.54 1/31/2015 2014 ANNUAL REPORT PROJECT: FACILITY: WWTP NPDES NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: Town of Holly Springs, NC Holly Springs, NC Utley Creek WWTP PO Box 8 Holly Springs, NC 27540 919-577-1090 NCO063096 Seann Byrd Director of Water Quality PO Box 8 Holly Springs, NC 27540 919-577-1090 Terry Foster, ORC PO Box 8 Holly Springs, NC 27540 919-577-2273 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 Page: 1 of 2 Report Number: 14-115-0205 J`1C?tL Easlem La_b®t"atpi1eS Inc. Account Number: 46462 7621 WhitepmeRcad Richmond, ftht1a2323 _(60417434401Faxxp0Q 271-6946 Submltted By: WILL VARNER wwwsatesstem corn Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55031 Sample id HOLLY SPRINGS Project: HOLLY SPRINGS NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/22/201414:00.00 Date Received: 04125/2014 00:00 Date Reported: 04/30/2014 Total Solids * 1.77 :17700 100.0 JM 04/251201414:30 Moisture • 98.23 100.0 JM 04125/201414:30 Total Kjeldahl Nitrogen 5.71 57100 10.0 JM 04/28/2014 09AO Total Phosphorus 4.04 40400 100 KM 04/281201413:09 Total Potassium 0.74 7400 100. KM 04/281201413:09 Total Sulfur 0.97 9720 100 KM 04/281201413:09 Total Calcium 1.82 =18200 100 KM 04/281201413:09 Total Magnesium 0.49 A850 100 KM 04/281201413:09 Total Sodium 0.51 R6140 100 KM 04/281201413:09 Total Iron J000 100 KM 04128/201413:09 Total Aluminum 26900 100 KM 04/281201413:09 Total Manganese 696 5 KM 041281201413.09 Total Copper ; 297 5 KM 04/28/201413:09 Total Zinc 647 5 KM 04128/201413.09 Ammonia Nitrogen 0.57 5650 10.0 JM 04/28/2014 09:40 Organic N 5.14 51450 10.0 04/28/2014 09:40 Nitrate+Nitrite-N 56.5 2.00 JM 0412812014 09:40 Total Cadmium '<2.0 2.0 KM 04/281201413:09 SM-2540G SM-264OG SM4500-NH3C TKN SW 6010C 5W 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6610C SW 6010C SM-4500-NH3C CALCULATION SM450ONO3F SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis. Our reports and letters are torthe exclusive and canfidenUal use of aurcllants, and may not be reproduced in whole or pan, nor may any reference be made to the work, the result, or the company in any advertising, mews release, orothorpubllo announcements without obtaining ourpriorwn7ten authorketiotL Debbie Holt Page: 2of2 Report Number. 14-115-0205 Account Number: 46462 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL LLC4HOLLY SPRINGS Mary Brewer 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 55031 Sample ld : HOLLY SPRINGS www.afopsfemcom A&L Eastern Laboratories, Inc. 7021 V01toplat Read Mimond, Vifghtla 23237 1804)743-941 FaK(004)27i.0446 Project. HOLLY SPRINGS NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4122/2014 14:00= Date Received: 04125/2014 010:00 Date Reported: 04130/2014 1 Total Chromium �1-1 9 5 KM 04128/201413:09 SW 6010C Total Nickel 13 5 KM 04/28/201413:09 SW 6010C Total Lead 7 5 KM 04128/201413:09 SW 6010C Total Arsenic 3.0 3.0 KM 04/2812014 13:09 SW 6010C Total Mercury 0.5 0.4 KM '04128/2014 09:00 SW-7471 B Total Selenium 5.0 KM 04/28/201413:09 SW 6010C pH .(Standard Units) 6.80 2.00 im 04/281201.4 09:40 SW-9045D Total Molybdenum -.—.9 5 KM 04/28/201413:09 SW 6010C Comments: T SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "At. ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Out reports and letters are for the exclusive and confidential use of our crionfs, and may not be reproduced In whole or part not may any reference be made to the work, the results, orthe company In any advertising, news releaso, or otherpubfic announcements Wfhout obtalrdng our prior wdflan authorization. Debbie Holt ... ..... .......... . ....... F Page: i of 2 Report Number: 14-196-0202 Account Number: 46462 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 56468 Sample Id". HOLLY SPRINGS wwyyale�eterncatn A&L Eastern Laboratories, Inc. Ml Wbltepino lMd Rkhmond, virglnla 232ar 10041743 8M FaJOK 271.6446 Project HOLLY SPRINGS NC CERT#257 REPORT OF ANALYSIS date samplers: 711112014 10.00:00 Date Received: 0711512014 00:00 Date Reported: 07/2V2014 Total Solids * 1.68 ,16800 100,0 BW 07/151201415:00 Moisture * 98.32 100;0 BW 07115/201415:00 Total Kjeldahi Nitrogen 5.54 55400 10.0 MW 07/16/2014 07:59 Total Phosphorus 4.33 43300 100 BW 07/16/2014 09:30 Total Potassium 0.64 6420 100 BW 07/16/2014 09:30 Total Sulfur' 0.98. %- 9820 100 : BW . 07116/2014 09:30 Total Calcium 2.14 21400 100 BW 07/16/2014 09:30 Total Magnesium 0.63 ;w6340 100 -SW 07/16/2014 09:30 Total Sodium 0.66 5500 100 BW 07/16/2014 09:30 Total Iron 4` i2700 100 BW 07/16/2014 09:30 Total Aluminum 30300 100 BW 07/16/2014 09:30 Total Manganese 809 5 BW 07116/2014 09:30 Total Copper 328 5 BW 07/1812014 09:30 Total Zinc 646 5 BW 07/16/2014 09:30 Ammonia Nitrogen 0.60 5950 10.0 MW 07/16/2014 07:59 Organic N 4,94 49450 10.0 07/1612014 07:59 Nitrate+Nitrite-N 107 2.00 MW 07/16/2014 08:00 Total Cadmium -,<2,0 2.0 BW 07/16/2014 09:30 Ail values are on a dry weight basis except as noted by asterisk. Defection limit on all N series Is on a wet basis. Our reports and letters are for the exclusive and conrxientlet use of our d hents, and may ablU reproducad in whole or par, nornray any reference be made Who work, the iesolts, orthe dompanyin anyadvertising, nawsrelaose, or otherpublfo announcements vAYhoul obtaining ourprlorvrn7len autho&a1W. K. Debbie Holt SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 601OC SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-196-0202 A&L Eastem Laboratories, Inc. Account Number: 46462 7621 WnitepMefiaad Richmond Wfglnia232$7 (804)74344pt Fax(884)271.844s Submitted By: WILL VARNER WWWalbiaternXiiin Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 56468 Sample id : HOLLY SPRINGS Project: HOLLY SPRINGS NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/1112D1410:00:00 Date Received: 07/16/2014 00.00 Date Reported: 07/21/2014 Total Chromium =, 21 5 BW Total Nickel „15 5 BW Total Lead 8 5 BW Total Arsenic .<3.0 3.0 BW Total Mercury 1.2 0.4 JM Total Selenlum 1,6.0 5.0 BW pH (Standard Units) * 6.63 2.00 MW Total Molybdenum 5 13W Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. 07116/2014 09.30 . SW 6b10C 07/16/2014 09:30 SW 6010C 07/16/2014 09:30 SW 6010C 07/16/2014 09:30 SW 6010C 07/16/2014 08:30 SW 7471 B 07/16/2014 09:30 SW 6010C 0711612014 09:04 SW-9045D 07/16/2014 00:30 SW 6010C All values are on a dry weight basis except as noted by asEe sk. Detection limit on all-N series is on a wet basis. Our reports and letters are for the exclusive and eonfidenUel use of our c *M% and may not be reproduced in whole or part, nor may any reference be made to the work, the resufts, or the company in any advertising, news release, or otherpubfio announcements without obtafning our prior wriffeo authorhation. Debbie Holt Page: t or 2 Report Number: 14-281-0204 A&L Eastern Laboratories, Inc. Account Number: 46462 @Y L. 7621 Whitepine Road Richmond,Virginta23237 (804)743.3401 Fax(804)271.6446 Submitted By: WILL VARNER Wwwaleastermcom Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project: HOLLY SPRINGS Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 10/1/2014 15:00:00 Lab Number: 58006 Date Received: 10/08/2014 00:00 Sample Id; HOLLY SPRINGS Date Reported: 10/17/2014 RESULT QUANTITATION LIMIT ANALY�IS,".- METHODRESULT Total Solids ` 1.93 19300 100,0 JM 10/081201413:45 SM-2540G Moisture ` 98.07 100.0 JM 10/08/2014 13:45 SM-2540G Total Kjeldahl Nitrogen 4.51 45100 10.0 JM 10/09/2014 08:19 SM4500-NH3C-TKN Total Phosphorus 4.73 47300 100 KM 10/17/2014 08:39 SW 6010C Total Potassium 0.53 5310 100 KM 10/17/2014 08:39 SW 6010C Total Sulfur 0.93 9250 100 KM 10/17/2014 08:39 SW 6010C Total Calcium 2.60 26000 100 KM 10/17/2014 08:39 SW 6010C Total Magnesium 0.56 5550 100 KM 10/17/2014 08:39 SW 6010C Total Sodium 0.54 5430 100 KM 10/1712014 08:39 SW 6010C Total Iron 13700 100 KM 10/17/2014 08:39 SW 6010C Total Aluminum 36100 100 KM 10117/2014 08:39 SW 6010C Total Manganese 761 5 KM 10/1712014 08:39 SW 6010C Total Copper 340 5 KM 10/17/2014 08:39 SW 6010C Total Zinc 754 5 KM 10/17/2014 08:39 SW 6010C Ammonia Nitrogen 0.36 3630 10.0 JM 10/09/2014 08:19 SM-4500-NH3C Organic N 4,15 41470 10.0 10/09/2014 08:19 CALCULATION Nitrate•r Nitrite-N 3310 2,00 JM 10/09/2014 08:20 SM450ONO3P Total Cadmium <2.0 2.0 KM 10117/2014 08:39 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repots and totters are for the exclusive and confidential use of ourdients, and may not be reproduced in whole orpart, norinay any reference be made to the work. the results, or gte cornpany in any advertising, news release, or other public announcements without obtalaing our prior writlen auttwrization. Debbie Holt Page: 2 of 2 Report Number: 14-281-0204 @P. A&L Eastern Laboratories, Inc. Account Number: 46462 7621Whhepinelioad Ricimtond,Vlrginia23237 (804170-9401 Fax(8041271.4448 Submitted By: WILL VARNER wwtnvateastero,com Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project : HOLLY SPRINGS Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE, NC 27028 REPORT OF ANALYSIS Lab Number: 58006 Sample Id: HOLLY SPRINGS Date Sampled: 10/1/2014 15.00:00 Date Received: 10108/2014 00:00 Date Reported: 1011712014 Total Chromium 22 5 KM 10/17/2014 08,39 SW 6010C Total Nickel 17 5 KM 10/1712014 08:39 SW 6010C Total Lead 9 5 KM 10/17/2014 08:39 SW 6010C Total Arsenic 4.0 3.0 KM 10117/2014 08:39 SW 6010C Total Mercury 0.6 0.4 KM 10/09/2014 09:00 SW-7471 B Total Selenium 5.0 5.0 KM 10/17/2014 08:39 SW 6010C pH (Standard Units) * 5.89 2.00 JM 10/09/2014 08:19 SW-9045D Total Molybdenum 13 5 KM 1011712014 08:39 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES, QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Mn", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and fetters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or pan, nor may any reference be rnade to the rtfwk, lim results, or Ore company in any advertising, news release, or other public announcements without obtaining our prior writlen authorization. Debbie Holt A ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0019098 Laboratory Facility Name: HOLLY SPRINGS, NC A&L Eastern Laboratories Inc. NPDES# : NCO063096 or WQ# (residual only) WWTP Name: HOLLY SPRINGS Residuals Analysis Data Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ Date Sampled (grab) or 01/21/14 04/22/14 07/11/14 10/01/14 Date Composited Percent Solids 1.80 1.77 1.68 1.93 PARAMETERS (mg/kg dry weight) Arsenic 3 3 <3 4 Cadmium <2 <2 <2 <2 Mercury 0.7 0.5 1.2 0.6 Chromium 15 19 21 22 Copper 279 297 328 340 Lead , 7 7 8 9 Molybdenum 8 9 9 13 Nickel 13 13 15 17 Selenium <5 <5 6 5 Zinc 634 647 646 754 Total Phosphorus 36000 40400 43300 47300 TKN 64400 57100 55400 45100 Ammonia -Nitrogen 3890 5650 5950 3630 Nitrate and Nitrite 361 56.5 107 3310 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for sub ' g false information, including the possibility of fines and imprisonment for knowing violations." X Cj.�- Date `� (SIGNATURE OF PREPARE DENR FORM RSSF (5/2003) Printed: Saturday - January 31, 201.5 at 11:43:42 for: 2065 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0019098 Laboratory Facility Name: HOLLY SPRINGS, NC A&L Eastern Laboratories Inc. NPDES# : NCO063096 or WQ# (residual only) WWTP Name: HOLLY SPRINGS Residuals Analysis Data Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ Date Sampled (grab) or 01/21/14 04/22/14 07/11/14 10/01/14 Date Composited Percent Solids 1.80 1.77 1.68 1.93 PARAMETERS (mg/kg dry weight) Aluminum 21400 26900 30300 36100 Calcium 17700 18200 21400 26000 Magnesium 5330 4850 6340 5550 pH 6.72 6.80 6.63 5.89 Potassium 6620 7400 6420 5310 Sodium 4310 5140 5500 5430 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the'information submitted. I am aware that there are significant penalties for submitting fal a information, including the possibility of fines and imprisonment for knowing violations." X .-+-- Date ,TURE OF PREPARER) NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) Printed: Saturday - January 31 2015 at 11:44:04 for: 2065 01 Page: 1 of 2 Report Number: 14-022-0204 A&L Eastern Laboratories,, Inc. w Account Number: 46462 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax(804) 271-6446 Submitted By: WILL VARNER wwwaleastem.com Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project: HOLLY SPRINGS Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 1/21/201410:00:00 Lab Number: 97591 Date Received: 01/22/2014 00:00 Sample Id : HOLLY SPRINGS Date Reported: 01/27/2014 Total Solids * 1.80 18000 1uu.0 JiVI U i/LULU 14 13:1)U OIVI-LJ'+U17 Moisture * 98.20 100.0 JM 01/22/2014 13:30 SM-2540G Total Kjeldahl Nitrogen 6.44 64400 10.0 JM 01/23/2014 07:39 SM-4500-NH3C-TKN Total Phosphorus 3.60 36000 100 KM 01/23/2014 15:23 SW 6010C Total Potassium 0.66 6620 100 KM 01/23/2014 15:23 SW 6010C Total Sulfur 0.95 9530 100 KM 01/23/2014 15:23 SW 6010C Total Calcium 1.77 17700 100 KM 01/23/2014 15:23 SW 6010C Total Magnesium 0.53 5330 100 KM 01/23/2014 15:23 SW 6010C Total Sodium 0.43 4310 100 KM 01/23/2014 15:23 SW 6010C Total Iron 16300 100 KM 01/23/2014 15:23 SW 6010C Total Aluminum 21400 100 KM 01/23/2014 1"5:23 SW 6010C Total Manganese 686 5 KM 01/23/2014 15:23 SW 6010C Total Copper 279 5 KM 01/23/2014 15:23 SW 6010C Total Zinc 634 5 KM 01/23/2014 15:23 SW 6010C Ammonia Nitrogen 0.39 3890 10.0 JM 01/23/2014 07:39 SM-4500-NH3C Organic N 6.05 60510 10.0 01/23/2014 07:39 CALCULATION Nitrate+Nitrite-N 361 2.00 JM 01/23/2014 07:40 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/23/2014 15:23 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-022-0204 v A&L Eastern Laboratories, Inc... Account Number: 46462 7621 Whitepine Road Richmond,Virginia23237 (804)743-9401 Fax (804)271-6446 Submitted By: WILL VARNER wwtwaleastern,com Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project: HOLLY SPRINGS Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 1/21/2014 10:00:00 Lab Number: 97591 Date Received: 01/22/2014 00:00 Sample Id : HOLLY SPRINGS Date Reported: 01/27/2014 PARAMETER RESULT RESULT QUANTITATION METHOD Total Chromium 15 5 KM 01/23/2014 15:23 SW 6010C Total Nickel 13 5 KM 01/23/2014 15:23 SW 6010C Total Lead 7 5 KM 01/23/2014 15:23 SW 6010C Total Arsenic 3.0 3.0 KM 01/23/2014 15:23 SW 6010C Total Mercury 0.7 0.4 KM. 01/23/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/23/2014 15:23 SW 6010C pH (Standard Units) * 6.72 2.00 JM 01/23/2014 07:39 SW-9045D Total Molybdenum 8 5 KM 01/23/2014 15:23 SW 6010C, Comments: _ SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Mg", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLING LOG # CUSTOMER: SYNAGRO SOUTHEAST At L ` 22 0204 'I i I 464 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIMINIIIII(IIIII�IInIiIII� 001.22-2014 SYNAGR.O CENTRAL HOLLY SPRINGS r field sampling procedures PROJECT MANAGER: 1! ! 4 f7� '� -- collection Qt these samples. Phone: SAMPLER A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED CHAIN OF CUSTODY RECORD & ANALYSIS RECORD �i��ry �ri�,�� ��r�•,•;.-. --'j f�.��n.� � 1 ~��-fir! !1� -�J /�i L ,��'f� `'/' Relinquished by Samples' - - Date Time Recieved by: REMARKS: Relinquished by: Date Time Rec' ved b !t Relinquished by: Date Time Recieved by: SPECIAL INSTRUCTIONS: C�� -, 1For monitoring purposes. PO#: ANALYSIS REQUEST SAMPLE I.D. SLII SL2 NH -N 4 NO -N s Organic N Cd Cr Ni Pb As Hg Se pH CaGO. e uiv. Volatile Solids Mo Cl N027N Por Pori 1s'r yt 400r Poor Poor Por Por t000, po Ylf Pow Poor SLt: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc White —A & L Canary — MANAGER COPY A Sodium Absorption Ratio calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 1/21/2014 1/112014-3/31/2014 0.9752 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (4310 x 1.8000) + 100 = 77.58 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (17700 x 1.8000) = 100 = 318.6 Mg mg/I = (mg mg/kg x % Solids) + 100 = (5330 x 1.8000) = 100 = 95.94 Na meq = Na mg/I _ Molec.Wgt.Na = 77.58 = 23 = 3.37304 Ca meq = Ca mg/I + Molec.Wgt.Ca = 318.6 + 20 = 15.93 Mg meq = Mg mg/I + Molec.Wgt.Mg = 95.94 _ 12 = 7.995 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.37304 _ SgrRoot[0.5(15.93+7.995)] = 0.975239 Printed: 1 /31 /2015 Page 1 11:44 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 4/22/2014 4/1/2014-6/30/2014 1.1599 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (5140 x 1.7700) = 100 = 90:978 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (18200 x 1.7700) =100 = 322.14 Mg mg/1= (mg mg/kg x % Solids) + 100 = (4850 x 1.7700) _ 100 = 85.845 Na meq = Na mg/I _ Molec.Wgt.Na = 90.978 _ 23 = 3.95557 Ca meq = Ca mg/I + Molec.Wgt.Ca = 322.14 = 20 = 16.107 Mg meq = Mg mg/I = Molec.Wgt.Mg = 85.845 + 12 = 7.15375 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)], = 3.95557 = SgrRoot[0.5(16.107+7.15375)] = 1.15988 Printed: 1 /31 /2015 Page 1 11:44 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 7/11/2014 7/112014-913012014 1.0964 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (5500 x 1.6800) _ 100 = 92.4 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (21400 x 1.6800) + 100 = 359.52 Mg mg/I = (mg mg/kg x % Solids) = 100 = (6340 x 1.6800) =100 = 106.512 Na meq = Na mg/I = Molec.Wgt.Na = 92.4 _ 23 = 4.01739 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 359.52 = 20 = 17.976 Mg meq = Mg mg/I = Molec.Wgt.Mg = 106.512 + 12 = 8.876 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.01739 = SgrRoot[0.5(17.976+8.876)] = 1.0964 Printed: 1/31/2015 Page 1 11:45 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 10/1/2014 10/112014-12/31/2014 1.1048 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (5430 x 1.9300) =100 = 104.799 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (26000 x 1.9300) _ 100 = 501.8 Mg mg/I = (mg mg/kg x % Solids) = 100 = (5550 x 1.9300) =100 = 107.115 Na meq = Na mg/I = Molec.Wgt.Na = 104.799 _ 23 = 4.55648 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 501.8 = 20 = 25.09 Mg meq = Mg mg/I = Molec.Wgt.Mg = 107.115 _ 12 = 8.92625 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.55648 _ SgrRoot[0.5(25.09+8.92625)] = 1.10484 Printed: 1 /31 /2015 Page 1 11:45 FACILITY NAME: HOLLY SPRINGS, NC OWNER: JEAN REEVES SITE #: NC CH 00023 FIELD# : CH 00023 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 46.68 OPERATOR: MIKE LAWRENCE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 40.60 ACRES PERMITTED: 40.60 Page : 1 Lime Applied *** Date Lbs/Ac DATE or DATE allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet,' Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/13/14 210,800.00 (G) 5192.118 1.77 0.383 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 6/14/14 217,000.00 (G) 5344.828 1.77 0.395 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 6/16/14 136,400.00 (G) 3359.606 1.77 0.248 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 6/17/14 68,200.00 (G) 1679.803 1.77 0.124 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 1 FESCUE Jun-14 632,400.00 (G) 15,576.355 Total Gallons/Ac: 15,576.35 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 42 Annual lbs/acre 0.007 0.005 0.044 0.683 0.016 0.001 0.021 0.030 0.012 1.488 92.89 Cumulative lbs/acre 0.041 0.019 0.410 3.578 0.170 0.009 0.109 0.229 0.082 8.978 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop Yyfi,Aa ) e 212 .,, FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A '= Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: HOLLY SPRINGS, NC OWNER: REEVES FAMILY LP SITE #: NC CH 00023 FIELD# : CH 00023 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 39.53 OPERATOR: MIKE LAWRENCE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 23.20 ACRES PERMITTED: 23.20 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate- and PAN Win) Crop MONTH Total Per Acre Solids 8/5/14 155,000.00 (G) 6681.034 1.68 0.468 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 I FESCUE PASTURE 8/6/14 186,000.00 (G) 8017.241 1.68 0.562 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 I FESCUE PASTURE 8/7/14 223,200.00 (G) 9620.690 1.68 0.674 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 FESCUE PASTURE Aug-14 564,200.00 (G) 24,318.965 Total Gallons/Ac: 24,318.97 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 61 Annual lbs/acre 0.010 0.007 0.072 1.118 0.027 0.004 0.031 0.051 0.020 2.201 147.54 Cumulative lbs/acre 0.057 0.027 0.478 5.533 1 0.240 0.014 0.150 0.310 0.123 12.375 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 158 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID X'^/Gy/� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: HOLLY SPRINGS, NC OWNER: TMH ENTERPRISES PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 55.37 SITE #: NC CH 00024 FIELD# : CH 00024 0002 OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 46.20 ACRES PERMITTED: 46.20 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/17/14 130,200.00 (G) 2818.182 1.77 0.208 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100. p 5,650.00 p 56.50 p 18317 FESCUE 4/18/14 136,400.00 (G) 2952.381 1.77 0.218 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 4/21/14 161,200.00 (G) 3489.177 1.77 0.258 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 IFESCUE 4/22/14 136,400.00 (G) 2952.381 1.77 0.218 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 4/23/14 99,200.00 (G) 2147.186 1.77 0.158 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100.p 5,650.00 p 56.50 p 18317 FESCUE 4/24/14 86,800.00 (G) 1878.788 1.77 0.139 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100. p 5,650.00 p 56.50 p 18317 FESCUE Apr-14 750,200.00 (G) 16,238.095 Total Gallons/Ac: 16,238.10 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 44 Annuallbs/acre 0.007 0.005 0.046 0.712 0.017 0.001 0.022 0.031 0.012 1.551 96.84 Cumulative lbs/acre 0.038 0.016 0.205 2.962 0.111 0.010 0.088 0.145 0.051 6.945 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 250 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: HOLLY SPRINGS, NC OWNER: BOBBY JOHNSON, POA SITE #: NC CH 00026 FIELD# : CH 00026 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 40.92 OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 31.60 ACRES PERMITTED: 31.60 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Anm onia Nitrogen Nitrate and P, Win)Crop MONTH Total Per Acre Solids 10/6/14 93,000.00 (G) 2943.038 1.93 0.237 HSAEDL DRY 0-<I/2" SUR 0.5 0.30 45,100.p 3,630.00 p 3,310.00p 17166 FESCUE 10/7/14 105,400.00 (G) 3335.443 1.93 0.268 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100.p 3,630.00 p 3,310.00p 17566 FESCUE 10/8/14 111,600.00 (G) 3531.646 1.93 0.284 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE 10/9/14 86,800.00 (G) 2746.835 1.93 0.221 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE 10/10/14 111,600.00 (G) 3531.646 1.93 0.284 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE Oct-14 508,400.00 (G) 16,088.608 Total Gallons/Ac: 16,088.61 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 45 Annual lbs/acre 0.010 0.005 0.057 0.880 0.023 0.002 0.034 0.044 0.013 1.953 122.49 Cumulative lbs/acre 0.017 0.007 0.098 1.547 0.048 0.004 0.056 0.078 0.024 3.521 Permit PAN Limit (lbs/acre) '1stCrop/2ndCrop „.w *,? g} „� 174 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 f 1339.0 267.9 15.0 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID X / (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: HOLLY SPRINGS, NC OWNER: BOBBY JOHNSON, POA SITE #: NC CH 00026 FIELD# : CH 0,0026 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 80.04 OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 54.10 ACRES PERMITTED: 54.10 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/8/14 241,800.00 (G) 4469.501 1.68 0.313 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 I FESCUE 8/14/14 142,600.00 (G) 2635.860 1.68 0.185 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 I FESCUE 8/15/14 142,600.00 (G) 2635.860 1.68 0.185 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 Ij FESCUE 8/16/14 -124,000.00 (G) 2292.052 1.68 0.161 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 55,400. p 5,950.00 p 107.00 p 17917 FESCUE Aug-14 651,000.00 (G) 12,033.273 10/13/14 117,800.00 (G) 2177.449 1.93 0.175 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 I FESCUE 10/14/14 24,800.00 (G) 458.410 1.93 0.037 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 I FESCUE 10/23/14 124,000.00 (G) 2292.052 1.93 0.184 HSAEDL DRY 0-<I/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 I FESCUE 10/24/14 161,200.00 (G) 2979.667 1.93 0.240 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE Oct-14 427,800.00 (G) 1 79907.578 FACILITY NAME: HOLLY SPRINGS, NC OWNER: BOBBY JOHNSON, POA SITE #: NC CH 00026 FIELD# : CH 00026 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 80.04 OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 54.10 ACRES PERMITTED: 54.10 Page : 2 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 19,940.85 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 53 Annual lbs/acre 0.010 0.006 0.063 0.986 0.025 0.003 0.032 0.047 0.016 2.049 133.21 Cumulativelbs/acre 0.036 0.016 0.272 3.564 0.132 0.009 0.099 0.184 0.067 7:828 211 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 r. 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: HOLLY SPRINGS, NC OWNER: HAROLD HOWARD SITE #: NC CH 00041 FIELD# : CH 00041 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 69.97 OPERATOR: HAROLD HOWARD CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/14/14 136,400.00 (G) 4854.093 1.80 0.364 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 64,400. p 3,890.00 p 361.00 p 20459 FESCUE PASTURE 3/15/14 142,600.00 (G) 5074.733 1.80 0.381 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 64,400. p 3,890.00 p 361.00 p 20459 FESCUE PASTURE Mar-14 279,000.00 (G) 9,928.826 5/2/14 142,600.00 (G) 5074.733 1.77 0.375 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100. p 5,650.00 p 56.50 p 18317 I FESCUE PASTURE 5/3/14 62,000.00 (G) 2206.406 1.77 0.163 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 57,100. p 5,650.00 p 56.50 p 18317 FESCUE PASTURE May-14 204,600.00 (G) 7,281.139 12/11/14 192,200.00 (G) 6839.858 1.93 0.550 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE PASTURE 12/12/14 229,400.00 (G) 8163.701 1.93 0.657 HSAEDL DRY 0-<1/2" SUR 0.5 0.30 45,100. p 3,630.00 p 3,310.00 p 17566 FESCUE PASTURE Dec-14 421,600.00 (G) 15,003.559 FACILITY NAME: HOLLY SPRINGS, NC OWNER: HAROLD HOWARD SITE #: NC CH 00041 FIELD# : CH 00041 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 69.97 OPERATOR: HAROLD HOWARD CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10 Page : 2 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia , Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppnl) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 32,213.52 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 93 Annuallbs/acre 0.017 0.010 0.096 1.556 0.040 0.003 0.053 0.074 0.025 3.461 211.31 Cumulativelbs/acre 0.044 0.022 0.301 4.225 0.164 0.008 0.133 0.222 0.085 10.168 ,2":r'; 187 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop s FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 , 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: HOLLY SPRINGS, NC OWNER: HAROLD DIXON PERMIT #: W00019098 SITE #• NC HA 00008 FIELD# • HA 00008 0008 OPERATOR: HAROLD DIXON RESIDUAL SOURCE(S):* See list at bottom of report allons (G) or Cubic Yards (CY) Dry or Wet Tons (WT) (specify) Tons DATE or % Per Residual MONTH Total Per Acre Solids 2/26/14 37,200.00 (G) 1978.723 1.80 0.149 HSAEDL 2/27/14 130,200.00 (G) 6925.532 1.80 0.520 HSAEDL 2/28/14 148,800.00 (G) 7914.894 1.80 0.594 HSAEDL Feb-14 316,200.00 (G) 16,819.149 Total Gallons/Ac: 16,819.15 TOTALS: Annual lbs/acre Cumulative lbs/acre ANNUAL DRY TONS APPLIED: 23.73 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 18.80 ACRES PERMITTED: 18.80 Site Inches Appli- Vola- Miner- Cond. Precip. cation tili- ali- Ammonia Dry, Wet, Pasts Method zation zation TKN Nitrogen MOIST 1 0-<I/2" 1 SUR 0.5 0.30 64,400. p 3,890.00 p MOIST 0-<1/2" SUR 0.5 0.30 64,400. p 3,890.00 p MOIST 0-<1/2" 1 SUR 0.5 0.30 64,400. p 3,890.00 p Nitrate PAN and (ppm) I Crop 361.00 p 1 20459 CORN 361.00 p 20459 I CORN 361.00 p 20459 I CORN Page: 1 Lime Applied *** Date Lbs/Ac As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 52 0.008 0.005 0.038 0.704 0.018 0.002 0.020 0.033 0.013 1.601 90.90 0.203 0.203 1.877 15.807 1.415 0.052 0.660 1.782 0.229 42.773 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 131 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID C-, /-2- // -/5 - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: HOLLY SPRINGS, NC OWNER: HAROLD DIXON SITE #: NC HA 00008 FIELD# : HA 00008 0009 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 21.41 OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 22.90 ACRES PERMITTED: 22.90 Page : 1 Lime Applied *** Date Lbs Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/25/14 117,800.00 (G) 5144.105 1.80 0.386 HSAEDL MOIST 0-<1/2" SUR 0.5 0.30 64,400. p 3,890.00 p 361.00 p 20459 I BERMUDAGRASS 2/26/14 167,400.00 (G) 7310.044 1.80 0.549 HSAEDL MOIST 0-<I/2" SUR 0.5 0.30 64,400. p 3,890.00 p 361.00 p 20419 1 BERMUDAGRASS Feb-14 1 285,200.00 (G) 12,454.149 Total Gallons/Ac: 12,454.15 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 38 Annuallbs/acre 0.006 0.004 0.028 0.522 0.013 0.001 0.015 0.024 0.009 1.185 67.31 Cumulative lbs/acre 0.152 0.134 1.433 12.121 1.139 0.040 0.500 1.375 0.183 31.184``' r ° » 165 Permit PAN Limit (lbs/acre) I st Crop/2nd Crop . .. ^ .. , FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 3 34.8 ([pP{ 1339.0 267.9 15.0 375.0 89.0 2500.0 � ,. . HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 P,G�sVIR�4dfa91=N`PxxL'7€�i1P•1tSf��c=1E5z Btb� r�rraP�itit=sl L.4iip('�tc7a•1�+5� February 10, 2014 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Holly Springs Dear Will Varner: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://www.settek.com Order No.: 14011399 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/22/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, N� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, Califonua 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, hidiana C-01-1-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 01-12O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 6 r o I. Suminit Environmental Technologies, Inc. 3310 Win St. Workorder Sample Summary. lPJIRQtPQEltitAL7 CtryahogaFalls,Ohio44223 +'rrirtiral fFa'A�'�I7t'� TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14011399 v Website: hQ.*1Avwiv.se1tek.com 10-Feb-14 CLIENT: Synagro Project: Holly Springs Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14011399-001 Holly Springs 1/21/2014 12:00:00 PM 1/22/2014'9:50:00 AM Sludge Page 2 of 6 Sununit Environmental Technologies, Inc. S Q--�F M W& I t 3310 Win St. FNVIRObIMENTALTECWdQI- GicS, NC Cuyahoga Falls, Ohio44223 Analyffr.'al LeUarahlriei; TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httn:/Aviviv.senek.com WO#: 14011399 Date Reported: 2/10/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Holly Springs TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 2/5/2014 WK Holly Springs 001 1/21/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/5/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 2/5/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 2/7/2014 JBN Holly Springs 001 1/21/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 2/7/2014 JBN Holly Springs 001 1/21/2014 Endrin 0.0020 ND mg/L Sludge EPA 8081 B 1 0.020 2/7/2014 JBN Holly Springs 001 1/21/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 2/7/2014 JBN Holly Springs 001 1/21/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 2/7/2014 JBN Holly Springs. 001 '1/21/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 2/7/2014 JBN Holly Springs 001 1/21/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 2/7/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 2/5/2014 MES Holly Springs 001 1/21/2014 1,2-Dichloroethane 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 2/5/2014 MES Holly Springs 001 1/21/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 2/5/2014 MES Holly Springs 001 1/21/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 2/5/2014 MES Holly Springs 001 1/21/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 2/5/2014 MES Holly Springs 001 1/21/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 2/5/2014 MES Holly Springs 001 1/21/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 2/5/2014 MES Holly Springs 001 1/21/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 2/5/2014 MES Holly Springs 001 1/21/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0.20 2/5/2014 MES Holly Springs 001 1/21/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 2/5/2014 MES Page 3 of 6 M Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14011399 , f6S4'IRCtidPatt',�!'PitLifC91e'�[]Ld�ls,sr1 Ctq,ahogaFalls, Ohio 44223 Date Reported: 2/10/2014 kaiyticaf rabangto i¢s TEL: (330) 253-8211 FAX. • (330) 253-4489 Company: Synagro Wehsile: htip:/faviviv.settek.coni Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Holly Springs SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 2/7/2014 AKE Holly Springs 001 1/21/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 2/7/2014 AKE Holly Springs 001 1/21/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 2/7/2014 AKE Holly Springs 001 1/21/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 2/7/2014 AKE Holly Springs 001 1/21/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 2/7/2014 AKE Holly Springs 001 1/21/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 2/7/2014 AKE butadiene Holly Springs 001 1/21/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 2/7/2014 AKE Holly Springs 001 1/21/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 2/7/2014 AKE Holly Springs 001 1/21/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 2/7/2014 AKE Holly Springs 001 1/21/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 2/7/2014 AKE Holly Springs 001 1/21/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 2/7/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Holly Springs 001 1/21/2014 2,4-D Holly Springs 001 1/21/2014 2,4,5-TP 5.0 ND mg/L Sludge EPA 8321 A 1 10 2/5/2014 AMZ 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 2/5/2014 AMZ Page 4 of 6 AMP Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14011399 t rffl RONM EINTAL t.OG1 ; 9NC Cuyahoga Falls, Ohio 44223 Date Reported: 2/10/2014 /�rratl;tyca! t:nara3dt7e s TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: hity:/hviviv.seliek.cont Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Holly Springs Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Holly Springs Holly Springs 001 001 1/21/2014 Flashpoint (140T) 1/21/2014 Cyanide, Reactive >140 T ND ppm Sludge Sludge EPA 1010 EPA 9014 1 1 1/24/2014 0.50 1/23/2014 TAH TIR Holly Springs 001 1/21/2014 pH 5.7 s.u. Sludge EPA 9045 D 1 1/22/2014 AYS Holly Springs 001 1/21/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 1/23/2014 TIR Page 5 of 6 (Q (D M O h Summit Environmental Technologies, Inc. 3310 Win Strut Analysis Request/Chain of Custody ('uyaho �� , - For Summit Fnvircntniental Technologies, Inc. use only �t Falb, Ohio 44_23 Tel: 330._53.8_1 1 Fax: 330._53.4489 me iPlcak Print) Proycl Nautc — SAnalytical Parameters and Methods Compau� Addres Project Address Y E Client Phon 409 �� Report to 3�� ? e Client Fax No. a% ResilIts. POti Client Email k cisc attuil I4•1ultSZ Quote No.7. Contact Peru71 Sampled by C.ht.�ck if Ohio SAP samples `. `r tt nz i # Sample Identification Date 'I�e Collecied Collected U L `'o < ✓ a Z Notcs/Commcuts: Received in lab M: I Date I Time Rwsh Requested By: 1tu,t tv appi, (w lah martag" WNW and wilou Page, ,hould a:aonipana ,aniple, it, the lA utor . 7hc client rctaim du pink ppa,,c ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Holly Springs WQ Permit Number: WWTP Name: Town of Holly Springs WWTP NPDES Number: Monitoring Period: From 01/01/2014 To 3/31/2014 WQ0019098 NCO063096 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/11 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If anolicable to alternative nerformed (Class A or Class B) comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6'h MPN MPN/g Coliform power per gram of total solids CFU 99354 150653 263158 CFU/g 0 Annually Grab SM9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying = Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one'or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I -am aware that there are significant penalties for false certification including fine and imprisonment." Sean Byrd, Director of Public WorkN Lo+:i ( c*ja.$ PreName Title (t` e or print) Land Applier Name and Title (if applicable) (type or print) Z-� -t Signature of Prepareri Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 99354 5.00 Min 263158 5.42 Max 125000 5.10 Geometric Mean 179641 5.25 152047 5.18 138120 5.14 142857 5.15 Average 6.18 99354 263158 150653 Contact: Amy Moore Client: holly Springs, Town of PO Box 8 Holly Springs, NC 27540 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 1/21/2014 Date Sample Rcvd: 1/14/2014 Meritech Work Order # 01141433 Sample. Digester # 1 Grab P ire 1/14/14 Parameters esults Analys� is Date- Reporting Lunit Meth qualifier %Total Solids Fecal Coliform (Sludge) 123 % 99,354 col/gdrywt 1/14114 0-100 % d 1/14/14 130 col /g rYwt SM 2540B SM 9222D B1 Meritech Work Order # 01141434 Sample: Digester # 2 Grab Parameters Results Analysis Date Reporting unit 1/14/14 Method QWHfer % Total Solids Fecal Coliform (Sludge) 1.90 % 263,158 col/g dry wt 1/14/14 1/14/14 0-100 % 130 col/g dry wt SM. 2540B SM 9222D B1 Meritech Work Order # 01141435 Sample: Digester # 3 Grab 1/14/14 Parameters Resu is Analysis to Reporting Litmit Rye od ualifier % Total Solids Fecal Coliform (Sludge) 1.84 % 125,000 col/9 dry wt 1/14114 1/14/14 0-100 % 130 col/g dry wt SM 2540B SM 9222D Meritech Work Order # 01141436 Sample: Digester # 4 Grab 1/14114 Parameters Results Analysis Date Rgp rtingLimit Method ualifier % Total Solids 1.67 % 1/14/14 0-100 % SM 2540E Fecal-Coliform(Sludge) 179,641 col/gdrywt 1/14/14 130 col/gdrywt SM9222D Meritech Work Order # 01141437 Sample: Digester ## 5 Grab 1/14/14 Parameters Results Anal sisDate Reporting Limit Method 0ualifier % Total Solids 1.71 % 1/14/14 0-100 % SM 2540B Fecal Coliform (Sludge) 152,047 col/g dry wt 1/14/14 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 teI:(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Y Laboratory Certification No.165 Page 2 Contact: Amy Moore ReportDate 1/21/2014 Client: Holly Springs, Town of PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 1/14/14. Meritech Work Order # 01141438 Sample: Digester # 6 Grab 1/14/14 Parameters Results An 1 sis Date Reporting Limit QUAff ier %Total Solids 1.81 % 1/14/14 0-100 °/a SM 2940B Fecal Coiiform (Sludge) 138,120 caI/g drywt 1/14/14 130 col/g drywt SM 9222D Meritech Work Order # 01141439 Sample: Digester # 7 Grab 1/14/14 Parameters Results Analysis Date Rwortin Litnit Metbad gg-ffler Solids 1.82 % 1/14/14 0-100 % SM 2540B ,Total I A Coliform (Sludge) 142,857 col/g dry wt 1/14/14 130 col/g dry wt SM 9222D B1 Countable membranes with less than 20 colonies. Reported value is estimated or is atotal of the counts on all filters reported per 100 ml. I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 6hain Custody Record (COC) ) NPDES# K:e 0(pr' L.._ �CZ=� of Phone: /� I ■M■ER TECH, INC. Client; Flo G � ` n � Fax: Email: ENVIRONMENTAL LABORATORIES Address: � Project# o A D1111610n of !Water Technology and Controls, 0' _, p (L im'"r1Z S p a• # s• Phone: i-336-3+t2.4746 Tuirn Around Time* *FLUSH work must have prior approval. 642 Tameo Rd. Fax: 1-336.342-9522 Reidsville, NC 27320 EmaWeb lSite: swww.maritech-labs.com Attention; db`� Std 0 0 days) 3 - 5 Day 24 - 48 Hr Required Lab Use Sample Sampling Dates & Times PersonTakin Sam le SI nature : Method Only HO pH OK? {. START Location/lD Time END Comp? Grab? #ot Cants. Tests Required 200.81200.7 012CK7 Date Time Date ^ OM 3% ( i q ff 1 —Dechlorination (4-6 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done In the field prior to preservation.*** Compositor # Comments: .lug # Method of Shipment: Are these results ior regulatory purposes? Repgrt results in an ice? ❑ ❑ Temperature On Receipt �� -- ❑ UPS YES NO ❑ mg/L ❑ olio uishedby Date tri91K9 Ng1L Tlme Re dby OF Date Time , 0 Fed i~x - " i .� Hand Delivery uis ate Time Received by 351 Date Time the Qr Relinquished by Date Time . Received at is by Date Time 1 )' G ')f�; rx. r , 'lilrx}r�f silr S Specific Qxygen Uptake Rate (SOUR) for Aerobic Sludge si3i a.,a.....�.. est Performed By Casey Denton Date: ample Point Digester Sample Time`. Jr Temp (T1): 18.5 C ' s Sal 19.8 Celsius Initial )perator Signature: ; + ,,....t.;i� 5 1CM ,...iY-. S..:i �, a 3Y'.t�,.: .1 ., �. 5♦,_d3 r r ra.... >S „. SP �. n, ., .} 4. .. IfL 1-10-14 1406 8.03 - [ 02 minutes _.:.._. . .:.........,.r...r.:_,.. ::;--::•-;,.t,........r _ ;.;:: (Mg/L) .r,+. �.,.. .a,.�>;1,:� ,,t., ;.•a.:�s.••:,3,< .:a'f..�.,+r: "=�>';;:ai':r t • '•:.;�:...:. � •� uL,<!:':.,:..,.:...,,::, ��, 3f. [ .t �o r�'i,,: `sir; 1 7.73 ;... ,....,... +„yam `i",.:::..:r •-. :..._....,, ,.:.:;o�,rv; :cam.•, i,. �::;•'-'% I `- 2 7.2 4 6.52 � f 4." L;,• .�1f: <i??,,"•.;, q,rx Dish Wet Uish 5 �� 6� Start DO should be no less th an 6.Q mg/L If dissolved 02 below 1.0 use that read as time'Dish Wet Dry 6 5.80 7' 5.42 in formula if nothing less than 1.0 use 15 min read. Dry 8 5.03 Make sure which dissolved 02 used record minutes in % Solid 9 4.64 formula below. TS 10 4 25 I : TS Test 11 3.891 Specific Oxvaen Uf 18.62 g / L 1.23 mg X 1 hr' I X 1.06"20 22.929 18.618 1.25 mg O2/g/hr at 20 Celsius ; ,Test PASSED To Pass needs to be below 1.5 mg 02/9lhr at 20 Celsi 41.4351 ! grams 2.6494 ,! grams 38.7857;gr� ams 3.37151 grams 0.7221 grams 18,6181 mg/L 18.62j911 PASSED I 1 8.51 2 8.21 3 8.11 4 8.04 5 8.01 6 7.97 7 7.95 8 7.93 9 7.91 10 7.89 11 7.87 12 7.85 13 7.84 14 7.82 15 7.80 Specific Oxygen Uptake Rate (SOUR) for Aerobic Sludge Dish Wet 29.4702 grams Dish 2.6594 grams Start DO should be no less than 6.0 mg/L. Wet 26.8108 4 grams If dissolved OZ below 1.0 use that read as time #2 Dish Dry 3.1456 grams in formula if nothing less than 1.0 use 15 min read. Dry �— 0.4862 grams Make sure which dissolved 02 used record minutes in % Solid 1.81 % formula below. TS ..18,134 mglL TS 18.13 9/1 Test PASSED _ <2.0 Oxygen Consumption Rate (Slope), mg 02/EJmin' 8.51 mg/L Time 1 - 7.80'mg/L Time 2 ` 0.0507 mg 02/L/min 15 Time 2 (min) - 1 Time 1 (min) Specific Oxygen Uptake Rate,mg 02Jg/hr at 20 degrees ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Holly Springs WQ Permit Number: WQ0019098 WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096 Monitoring Period: From 04/01/2014 To 6/30/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion if annlirahi. +n a14PrnafivP nerf--il Win cc A nr (`lace Rl rnm"WP the fnllnwinu mnnitnrinu Antae Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 61 MPN MPN/g Coliform power per gram of total solids 98458 167355 226227 CFU/g 0 Annually Grab SM9222D CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Mt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment." Sean Byrd, Director of Public Works Prep Na Title (ty e or print) Land Applier Name and Title (if applicable) (type or print) 2 Signature of Preparer* I Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 226227 5.35 Min 98458 189781 5.28 Max 226227 160584 5.21 Geometric Mean 167355 172662 5.24 185606 5.27 169014 5.23 98458 4.99 Average 5.22 Meritech, Ines Environmental Laboratory Laboratory Certification No.165 Page 1 Contact: Amy Moore Report Date: 4/24/2014 Client: Holly Springs, Town of NPDES#: NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 4/14/2014 Meritech Work Order # 04141412 Sample: ICT Grab 4/14/14 Parameters Result Anal sate Reporting Limit Method % Total Solids 1.37 % 4115114 0-100 % SM 2540B Fecal Coliforni (Sludge) 226,227 col/gdrywt 4/14/14 130 col/g dry wt SM 9222D Meritech Work Order # 04141413 Sample: ICT Grab 4/14/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.37 % 4/15/14 0-100 % SM 2540E Fecal Coliform (Sludge) 189,781 col/g dry wt 4114/14 130 col/g dry wt SM 9222D i^ Meritech Work Order # 04141414 Sample: ICT Grab 4/14/14 Parameters Result Analysis Date ReporthigUrnit Method %Total Solids 1.37 % 4/15/14 0-100 % SM 2540B Fecal Coliform. (Sludge) 160,584 col/9 dry wt 4/14/14 130 col/g dry wt SM 9222D Meritech Work Order # 04141415 Sample: ICT Grab 4/14/14 Parameters Result Analysis Date Reporting Liinit Method % Total Solids 1.39 % 4/15/14 0-100 % SM 2540B Fecal Coliform (Sludge) 172,662 col/g dry wt 4/14/14 130 cal/g diy wt SM 9222D Meritech Work Order ## 04141416 Sample: ICT Grab 4/14/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.32 o/a 4/15/14 0-100 % SM 2540B _ _ _- Fecal Coliform (Sludge) 185,606 col/g dry wt 4/14/14 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. r = Environmental Laboratory A Laboratory Certification No.165 Page 2 Contact; Amy Moore Report Date: 4/24/2014 Client: Holly Springs, Town of NPDES#• NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 4/14/2014 Meritech Work Order # 04141417 Sample: ICT Grab 4114/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.42 % 4/15/14 0-100 % SM 2540B Fecal Coliforxn (Sludge) 169,014 col/g dry wt 4/14/14 130 col/g dry wt SM 9222D Meritech Work Order # 04141418 Sample: ICT Grab 4/14/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.385 % 4/15/14 0-100 % SM 2540B Fecal Colifonn (Sludge) 98,458 col/g drywt 4/14114 130 col/g dry wt SM 9222D I I hereby certify thatX have reviewed and approve these data. �f _ Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 Eel.(336)342-4743 fax.(336)342-1522 Chain of Custody Record (C®C) Client: Address: Aitfention: Holly Springs Amy Moore NPDEs#: Phone: 1-919•-577-2273 Fax: - Email: Project: Po #: INC.MERITECH Esavironmeutai. Laboratories A. Division of Water Technology and Control, Inc. 642 Taman Rd Phone 1-336-34?,4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtelab ftelisouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (Zo days) r—� a -s gay r----7 24 -48 Itr Sample 1,ocation/ID # Sampling Dates & Times Person Taking Sampie (signature): .. ' Lab Use Only START END comp? Grab? # of Conts, Tes Rea�uired on Ice? pH OK? C120K? Date Time Date Time c I/-1q_ y roxo 10 z r 6- ) k•-r�-ram ry z � � �.5 L1- l to Z If Method of Shipment; Comments: ❑ UPS ❑ Fed Ex }land Delivery El Will these results be used for regulatory purposes? Yes No *RUSH workmusif be approved prior to submiffing samples. Relinqulshed b Date: Time: a, ! 7 IWO Received b . l Date: Time: 3 O Relinquished b Date: Time: �� / I �SY0 Received b3r Date: Time: Relinquished by: Date: Time: Received at lab Date: Time: t Meritech, Inc. : Environmental Laboratory �.. .N Laboratory Certification No.165 AV - Page 1 Contact: Amy Moore Report Date: 4/17/2014 Client Holly Springs, Town of NPDES#: NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 4/9/2014 Meritech Work Order # 04091462 Sample: Effluent Composite 4/6-7/14 Parameters Re,�ults Analysis Date Reporting Limit Method TKN 1.05 mg/L 4/15/14 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 4.06 mg/L 4/11/14 0.10 mg/L EPA 353.2 Nitrogen, total 5.11 mg/L 4/16/14 0.20 mg/L EPA 353.2 Meritech Work Order## 04091463 Sample: Effluent Composite 4/7-8/14 Parameters Results Analysis Date Reparj= Limit Method Nitrate, Nitrogen 2.87 mg/.L 4/9/14 0.10 mg/L EPA 353.2 Meritech Work Order # 04091464 Sample: Effluent Composite 4/8-9/14 Parameters Re ul Analysis Date Reporting Limit Method Nitrate, Nitrogen 3.18 mg/L 4/9/14 0.10 mg/L EPA 353.2 Meritech Work Order # 04091465 Sample: SWLI~ Composite 4/6-7/14 Parameters Results Analysis Date Reporting Limit Method TKN 66.0 mg/L 4/15/14 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 26.3 mg/L 4/9/14 0.10 mg/L EPA 353.2 Nitrogen, total 92.3 mg/L 4/15/14 0.20 mg/L EPA 353.2 Meritech Work Order # 04091466 Sample: Digester #1 Grab 4/9/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.22 % 4/11114 0-100 % SM 2540B Fecal Coliform (Sludge) 65,520 col/g drywt 4/9/14 130 col/g drywt SM 9222D Meritech Work Order # 04091467 Sample: Digester #2 Grab 4/9/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.23 % 4/11/14 0-100 % SM 2540B Fecal Coliform (Sludge) 69,303 col/g drywt 4/9/14 130 col/g drywt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Amy Moore Report Date: 4/17/2014 Client: Holly Springs, Town of NPDES#: NCO063096 PO Box 8 Holly. Springs, NC 27540 Date Sample Rcvd: 4/9/2014 Meritech Work Order## 04091468 Sample: Digester #3 Grab 4/9/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.22 % 4/11/14 0-100 % SM 2540B Fecal Conform (Sludge) 73,710 col/g dry wt 4/9/14 130 col/g dry wt SM 9222D Meritech Work Order # 04091469 Sample: Digester 04 Grab 4/9/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.24 % 4/11/14 0-100 % SM 2540B Fecal CoIiform (Sludge) 89,286 col/g dry wt 4/9/14 130 col/g dry wt SM. 9222D Meritech Work Order # 04091470 Sample: Digester #5 Grab 4/9/14 Parameters Results AnaIy!5iggDate RepprtingUmit Method % Total Solids 2.24 % 4/11/14 0-100 % SM 2540B Fecal Coliform (Sludge) 68,993 col/g dry wt 4/9/14 130 col/g dry wt SM 9222D Meritech Work Order # 04091471 Sample: Digester #6 Grab 4/9/14 Parameters Re ul ,Analysis Date R@porting Limit Method %Total Solids 2.22 % 4/11/14 0-100 % SM 2540B .Fecal Coliform (Sludge) 77,805 col/g dry wt 4/9/14 130 col/g dry wt SM 9222D Meritech Work Order # 04091472 Sample: Digester #7 Grab 4/9/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.25 % 4/11/14 0-100 % SM 2540B Fecal Coliform (Sludge) 48,485 col/g dry wt 4/9/14 130 col/g dry wt SM 9222D I hereby certrf that I have reviewed and approve these data.. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel. (33 6) 342-4748 lax. (3 3 6) 342-15 22 �:_ r, 1fili n Y^�r•a;x�v; Contact: Amy Moore Client: Holly Springs, Town of PO Box 8 Holly Springs, NC 27540 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 1 Report Date: 6/11/2014 NPDES#: NCO063096 Date Sample Rcvd: 6/4/2014 Meritech Work Order # 06041436 . Sample: Digester #1 Grab 6/4/14 Parameters Results AnalvsisDate RepgrdngLimit Method Qualiff r % Total Solids Fecal Coliform (Sludge) 2.79 % 2,260 col/g dry wt 6/5/14 6/5/14 0-100 % 130 coI/g dry wt SM 2540B SM 9222D B1 Meritech Work Order # 06041437 Sample: Digester #2 Grab 6/4/14 Parameters Results Analysis ate RgForting Umit Method ualifi r % Total Solids Fecal Coliform (Sludge) 2.66 % 2,371 col/g drywt 6/5/14 6/5/14 0-100 % 130 col/g drywt SM 2540B SM 9222D B1 Meritech Work Order # 06041438 Sample: Digester #3 Grab 6/4/ 14 Parametgrs Results Analysis Date Rwartinglimit Method Qualifier % Total Solids Fecal Coliform (SIudge) 2.74 % 1,644 col/g dry wt 6/5/14 6/S/14 0-100 % 130 col/g dry wt SM 2540B SM 9222D B1 Meritech Work Order # 06041439 Sample; Interchange #4 Grab 6/4/14 Parameters Results Analysis Date l2eng Limi Method Qualifier % Total Solids Fecal Coliform (Sludge) 1.45 % 56,426 col/g dry wt 6/5/14 6/5/14 0-100 % 130 col/g dry wt SM 2540E SM 9222D B1 Meritech Work Order # 06041440 Sample: Interchange #5 Grab 6/4/14 Paramerer.q Results Analysis Date RgporRng%imig M t od Qualifier % Total Solids 1.39 % 4111/14 0-100 % SM 2540B Fecal Coliform (Sludge) 39,241 col/gdry wt 4/9/14 130 col/gdry wt SM 9222D B1 B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on ' y all filters reported per 100 ml. 642 Tamco Road, Reidsville, North Carolina 27320 teI.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Envirolamental Laboratory Laboratory Certification No.165 Contact: Amy Moore Page 2 Client: Holly Springs, Town of Report Date: 6/11/2014 PO Box 8 NPDES#: NCO063096 Holly Springs, NC 27540 Date Sample Rcvd: 6/4/2014 Meritech Work Order # 06041441 Sample: Interchange #6 Grab � 6/4/14 Parameters R "7tS Aralvci,z Date Reportin¢ F unit Method ualSfi r % Total Solids 1.45 % 6/5/14 0-100 %±ecal Coliform [SIudge) ,co/gdry wt 6/5/14 SM 2540B 130 col/g drywt SM 9222D B1 Meritech Work Order # 06041442 Sample: Interchange #7 Grab 6/4/14 Parayneters • 9esui nalysis Date R Aornna ; t . P �, mi Method 99ALIffur %Total Solids 1.46 % 6/5/14 0-100 e/ Fecal Coliform (Sludge) 68,493 col/g drywt 6/5/14 130 SM 2540B . col /g dry wt SM 9222D B1 131 Countable membranes with less than 20 colonies. Reported value is estimated or is a total ofthe counts on all filters reported per 100 mi. ram, I hereby certtfy that I have reviewed and approve these data. (� LaboratoryRepresento 've 642 Tatnco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record (COC) _ NPDESI►:G. Client:r,— � 1 i Phone; Address: Fax: Email: Project: P.0.9: Attention: � 'ILL Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle a that apply: Email (preferred), Fax, Mail Sid x0 days) 3 - 5 Days 24s �Use �—Q—n-l-yt MER�� INC. ENVIRONMENTAL LABORATORIES r " d— 642 TamcoRd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs,com �-y-� f� -{'p/� �'1 y �1c YY1 W WW i l I 1 t �i l.� 1 I'�l �.! t.,J�7 co I I 1 Sample Location and/or ID # Sampling ®aces &Times person? gSample n t}; ,�Lab Start End Con } Grab? It Cont. Test(s) Required on ice? e / No pH OK?. Cl OK? Date Time Date Time ( 6/,ql y 1035 :'#a2 rr tt 6lI ly /637 OA16 -3 " t t 61911 r ION #q -T -lr e./ QYbyAc #5 t' It r t 6Y lK •r Temperature Upon Receipt: `� Method of Shipment: `** Dechlorination(<0.5 p m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the Feld prior to reservation. *** Comments: Compositor It JJug It ❑: UPS 0'. Fed Ex Are these results for regulatory purposes? Yes 0• No Q: Repo esults in: mg/t 0. mg/kg�. ug/I �� (� Hand Delive elinqu she, by:l : imes 5ry I �. Da� T Re a Time: e b • �,� l j f � 120.7 Q other hell u d y: ally Time: /� •tom R ceiv d by; y pale: Time: Relinquished by: Date: Time: Received b obi �yte� } Tin Test Performed By: Samn-�e Paint: Air Tern p (Ti;: Operator Signature: 15 Time 2 (min) - ' 1.48 mg 02/91hr,a Test:, PASSED Time uissoivetl: (minutes) 02 {M) 1 7.23 2 6.28 3 5.41 Dish Wet, 33.0807 4 i 4.71 : Dish 2.4248 5 ` 4.23 Start DO should be no less than 6.0 mg/L. Wet 30.6559 6 3.91 If dissolved 02 belaw 1.0 use that read as time #2 Dish Dry 2.9611 7 3.52 in formula if nothing less than 1.0 use 15 min read. Dry fl.5363 8 3.20 - Make sure which dissolved 02 used record minutes in % Solid 1.75 9 2.89 formula below. TS 17,494 J 10 2.61 TS 17AS 11 2.30 ... Test PASSED 12 2.03 13' 1.77 14 1.52 7 15 1.27...... .... .... Oxygen Consumption Rate (Slope), mg`O21L/min . . . . . . . . . . . . 7.23 mg/L Time 1 1 27 mglL Time 2 0 4257 mg OWU In IS Time 2 (min) - 1 Tme 1 (min) 1.15 mg O2/g/h-rat 20 Celsius Test: PASSED io P 2ss seeds fics €�e b(low 1.5 nig O21g/hr at 20 Gelspu: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Holly Springs WQ Permit Number: WQ0019098 WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096 Monitoring Period: From 07/01/2014 To 9/30/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6` MPN MPN/g Coliform power per gram of total solids CFU 506 2826 14916 CFU/g 0 Annually Grab SM9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Iniection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Sean Byrd, Director of Public Wm'1 " Prepay 7e le (type or print) Land Applier Name and Title (if applicable) (type or print) 1 ' Z -A- l! Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 11107 4.05 Min 506 14916 4.17 Max 14916 8580 3.93 Geometric Mean 2826 7808 3.89 506 2.70 506 2.70 506 2.70 Average 3.45 Meritech, Inc. Environmental Laboratory r ' Laboratory Certification No.165 Page 1 Contact: Amy Moore Report Date: 8/7/2014 Client: Holly Springs, Town of NPDES#: NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 7/31/2014 Meritech Work Order # 07311442 Sample: ICT- Digester 41 Grab 7131/14 Parameters Results, Ana ysis Date Reporting Limn Method Quailfer %Total Solids 1.46 % 8/4/14 0-100 % SM 2540E B1 Fecal Coliform (Sludge) 11,107 col/g dry wt 7/31/14 130 col/g dry wt SM 9222D Meritech Work Order # 07311443 Sample: ICT- Digester #2 Grab 7131/14 Parameters oils Analysis Date Reporting Mtitit ethod Qualifie °!o Total Solids 1.51 % 8/4/14 0-100 % SM 2540E Fecal Coliformn (Sludge) 14,916 col/g dry wt 7/31/14 130 col/g dry wt SM 9222D Meritech Work Order # 07311444 Sample: ICT- Digester #3 Grab 7/31/14 % Parameters Results Analysis Date Reporting niit etb lifie %Total Solids 1.47 % 8/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) 8,580 col/g dry wt 7/31/14 130 col/g dry wt SM 9222D B1 Meritech Work Order # 07311445 Sample: ICT- Digester 04 Grab 7/31/14 Parameters esults Analysis Date Reporting Mini t Method Qualifler % Total Solids 1.50 % 8/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) 7,808 col/g dry wt 7/31/14 130 col/g dry wt SM 9222D B1 Meritech Work Order # 07311446 Sample: ICT- Digester #5 Grab 7/31/14 Parameters Results AnaWs s Date Reporting Limit Method Qualifier % Total Solids 1.78 % 8/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 506 col/g dry wt 7/31/14 506 col/g dry wt SM 9222D B2 H1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 ml. BZ Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been reported if there had been one colony on the filter representing the largest filtration volume (reported as a less than "<" value). 642 Tanico Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory 1 Laboratory Certification No,165 r Page 2 Contact: Amy Moore Report Date: 8/7/2014 Client: Holly Springs, Town of NPDES#: NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 7/31/2014 Meritech Work Order # 07311447 Sample: ICT- Digester #6 Grab 7/31/14 Parameters ults Analysis Date Reporting Lhnit Method Qualifier % Total Solids 1.74 % 8/4/14 0-100 % SM 2540E Fecal Coliforin (SIudge) < S06 col/g diy wt 7/31/14 506 col/g diy wt SM 9222D B2 Meritech Work Order # 07311448 Saniple: I CT- Digester #7 Grab 7/31/14 Par-amet Results Analysis Date Reporting Limit Method ualifier %Total Solids 1.74 % 8/4/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 506 col/g drywt 7/31/14 .506 col/g diywt SM 9222D B2 r B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 nil. B2 Counts fromall filters were zero. The value reported is based on the number of colonies per 100 all that would have been reported if there had been one colony on the filter representing the largest filtration volume (reported as a less than "<" value). I hereby certify thatl have reviewed and approve these data. it . Laboratory Representative 642 Tanmco Road, Reidsville, North Carolina 27320 tel,(336)342-4748 fax,(336)342-1522 3•�o-�� Chain of Custody Record (COC) C, - INC,PDES#: Efie Client: 2r w A . 5 r,bu s Phone: T9 `} 17 QW13 Address: Fax: ENVIRONMENTAL LABORATORIES Email: iy 642 Tamco.Rd.. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritech-labs.com Attention: Turn Around Time* �' ww,meritech—labs.com How would you like your report sent? *RUSH work needs prior approval. Std(10da 24-48Hrs Circle all that apply: Email (preferred), Fax, Mail s) 3-5 _Days Sampling Dates & Times Person 'raking Sample (5ign/Print): ,/ c"t % Lab Use On] Sample Location and/or ID # Start End Comp? pof �-est��� Req��red On Ice? pH OK? Date Time Date Time Grab? Cont. Yes o : Cl OK? Ts ci- fS 1L., e_.. IFe Z c)W - 1 f > L Temperature upon Method of " * Dechiorination (<O.S ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. Receipt' ,Y Shipment- Comments: Compositor.# Q. UPS Q Fed EX a these results for regulatory purposes? Yes -.1 No Report results in: mg/l. Q' Jug # mg/kg Q ug/L Q Delivery Reii quished Y: % at time: ,,, _� Rec ' ed by: ti te•L Time: (:••tHarid !- Other Relin ishe by: ! D The: / lRenn'qu!Ked eceiv by: D e: Time: b . Date: Time: Receivetlby Ly . b te: ( Time , 3 K 1 Test Performed. Sample Point Air Temp (T1): r Operator Signat Time ussv (minutes) 01 (Mg, 1 7A5 2 6.93 3 6.66 4 6.44 628 i 6 6.09 7 5.82 8 5.69 9 5.58 10 5.42 11 5.33 12 f 5.21 13 5.10 14 ' 4.99 15 4.87 Speck Oxygen Uptake Rate {SOUR) for Aerobic Sludge a. -Dish Wet 15.3805 s grams Dish 2.6390 grams Start DO should be no less than 6.0 mg1L. Wet 12.7415 grams If dissolved 02 below 1.0 use that read as time #2 Dish Dry 2.8562 grams In formula if nothing less than 1.0 use 15 min read. Dry 0.2172 grams Make sure which dissolved 02 used record minutes in % Solid 1 70 %4... formula below. - TS 17 047 mg1L TS 17 05 Test PASSED .: Oa843 mg'02/UminX 11.057 17.047 01842 ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Holly Springs WQ Permit Number: W00019098 WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096 Monitoring Period: From 10/01/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to -Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlirahlP 4n a14Prna4ivP nerfnrmPrl (('lace A nr CI ace R) rmmnlPtP the fallnwina mnnitnrina dntn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6t MPN MPN/g Coliform power per gram of total solids 435 556 862 CFU/g 0 Annually Grab SM9222D CFU` 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Mt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) _ Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Sean Byrd, Director of Public *Iet4m Qj4 f ; A:# S Prep Name Title ( pe or print) Signature of Preparev Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 1 Contact: Amy Moore Report- Date: 10/13/2014 Client: Holly Springs, Town of NPDCSih NCO063096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 10/1/2014 Meritechi Work Order # 10011440 Sample: Digester ##1 Grab Parameters Resul Analysis Date 10/1/14 Reporting Unii Method % Total Solids 2.10 % 10/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 476 col/g dry wt 10/1/14 476 col/g dry wt SM 9222D. Meritech Work Order # 10011441 Sample: Digester #2 Grab 10/1/14 Parameters Results Analysis Date ReVorting Lim i Method % Total Solids 2.09 % 10/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) 862 col/g dry wt 10/1/14 130 col/g dry wt SM 9222D Meritech Work Order It '10011442 Sample: Digester #3 Grab 10/1/14 Parameters Resul s Analysis Date Reporting Limit Metho %Total Solids 2.05 % 10/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 488 col/g dry wt 10/1/14 488 col/g dry wt SM 9222D Meritech Work Order # 10011443 Sample: Interchange ##4 Grab ..:................................................ . 10/1/14 Parameters Results Analysis Date Reporting.l.intiC � %Total Solids 2.07 % 10/2/14 0-100 % SM 2540E Fecal Coliform (Sludge) 435 col/g dry wt 10/1/14 130 col/g dry wt SM 9222D Meritechi Work Order It 10011444 Sample: Interchange #5 Grab 10/1/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.16 a/o 10/2/14 0-100 % SM 2540B--- Fecal Coliform (Sludge) 834 col/g dry wt 10/1/14 506 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. rYx Environmental Laboratory _g Laboratory Certification No.165 Page ..2 Contact: Amy Moore Report Date: 10/13/2014 Client: Holly Springs, Town of NPDES#: NC006'3096 PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 10/1/2014 Meritech Work Order It 10011445 Sample: Interchange #6 Grab 10/1/14 Parametei Results Analysis Date Reporting Limit Method % Total Solids 2.10 % 10/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 476 col/g dry wt 10/1/14 476 col/g dry wt SM 9222D Meritech Work Order # 10011446 Sample: interchange ##7 Tank Grab 10/1/14 Parameters Results Analysis Date Reporting Limit Method %Total Solids 2.09 % 10/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 478 col/g dry wt 10/1/14 478 col/g dry wt SM 9222D 1 herehy certify that-1 have reviewed and approve these data. (, Labor-atmy Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chair of Custody Record (COC) rvPOEsa 9 @ INCENVIRONMENTAL LABORATORIES d A Division of Water Technology and Controls, Inc. r Phone: 1-336-342-4748 642 Tameo Rd. Fax: 1-336-342-1522 Reidsville, NC 27320 Entail: srtrtrtech@bellsouth.net Web site: www.meritech4abs.corn _ Client: "4o l —, Phone — Fax:MEOTEC_ rGa v a ,'C �S' Address: 1 � � , i i , i� Email: Project # P.O. # Attention:��e-- _ �� Std ([0 da Sample Sampling Dates & Times Location/$® START END Date Time Date Time Person ina Sam le si nature : Comp? Grab? rret Conts.� ests Required 2. 0900 1 # *"*Decholrination (<4.5 ppm) of AmMonia, CY Compositor Jug # Comments: Method of shipment: Are these results for egulatory purposes? UPS YES NO [] mg/1 ❑ Fed Ex Pulm&d--b ois ed by Date Hand Delivery Date ❑ Otheruished by Date Around Time* 8 - 5 Day 24 - 48 Fir Lab Use Only.. n pH Oki Ce? C12 OK? • tJ sC2L ITA . Phenol or TKN samples must be done in the field prior to preservation *** Report results in . mg/Kg Q Other Time Received by me Received by Time a *RUSH work must have prior approval. Date e /o///0 'Z7 Date Time 77a Time Meritech, Inc, Environmental Laboratory = Laboratory Certification No.165 1 PagContact: Am Moore Y Report Date: 12/9/2014 /9/ CIient- Holly Springs, Town of PO Box 8 Holly Springs, NC 27540 Date Sample Rcvd: 11/26/2014 Meritech Work Order # 11261474 Sample: SIudge 01 Grab 11/26/14 Parameters Results Analysis Date Rego Ling Limit Method % Total Solids 1.99 % 12/2/14 0-100 % SM 2540B Fecal CoIiform (Sludge) 453 col/gdry wt 11/26/14 130 col/gdrywt SM 9222D Meritech Work Order # 11261475 Sample: SIudge 42 Grab 11/26/14 Parameters Results AnalWs Date Reporting Limit Method % Total Solids 2.01 % 12/2/14 0-100 % SM Z540B Fecal Conform (Sludge) 897 col/g drywt 11/26/14 130 coI/g dry wt SM 9222D Meritech Work Order # 11261476 Sample: Sludge #3 Grab 11/26/14 Parameters Results Analysis Date Reuorting Limit Method % Total Solids 2.02 % 12/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,338 col/g dry wt 11/26/14 130 col/g dry wt SM 9222D Meritech Work Order # 11261477 Sample: SIudge #4 Grab 11/26/14 Parameters Results AnalWs Date R@porting Limit Method %Total Solids 1.98 % 12/2/14 0-100 % SM 2540B Fecal Coliform (Sludge) 901 col/g dry wt 11/26/14 130 col/g drywt SM 9222D Meritech Work Order## 11261478 Sample: SIudge #5 Grab 11/26/14 Parameters Reg hs Analysis Date Reporting Limit Method %Total Solids 1.93 % 12/2114 0-100 % SM 2540B Fecal Coliform (Sludge) 4,668 col/g drywt 11/26/14 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 teL(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental. Laboratory Laboratory Certification No..165 Contact: Amy. Moore Client: Holly Springs, Town of PO Box 8 Holly Springs, NC 27540 Page 2 Report Date 12/9/2014 Date -Sample Rcvd: 11/26/14 Meritech Work Order•## 11261479 Sample: Sludge #6 Grab 11/26/14 Parameters Results Analysis Date Reporting Limit ethod %Total Solids 2.O1. %. 12/2/14 0-100 % SM 25408 Fecal Coliform (SIudge) 1,345 col/gdrywt 11/26/14 130 col/gdry wt SM 9222D Meritech Work Order # 11261480 Sample: Sludge #7 Grab 11/26/14 Parameters Results Analysis Date. Reporting Limit Method %Total -Solids 1.93 % 12/2/14 0-100 % SM 2540B Fecal Coliform CSludge) 937 col/g dry wt 11/26/14 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and .approve these data Laboratory Representative 1 ' 642 Tamco load, Reidsville, North Carolina 27320 teL(336)342-4748. fax.(336)342-1522 3-2&2013 Chain of Custody Record (COC) Client: �� 1 Y L NPDESU: Phone: It A IT C 6 I ° A Address: Fax: ENVIRONMENTAL LABORATORIES� Email: 'T.. ., 642 Tamco.Rd, Phone: 336-342-4748 Project: . Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs.com Attentlon: Urn Ar6und Time* I www,meritech-labs HOW Would u like our report sent? *RUSH work needs prI4r approval. Circle all thatepp E std coda' 33 5 Days zr -40Hrs : ail(preferred), ax, Mail .Sampling Dates & Times Perso T in Sample(Sgn/Print): "� ,���/� Lab Use�Q—Y�ly Sample Location and/or ID # Start End Date Time Date time Comp? Grab? pof Test(s) Required on Ice? pH OK? Cont. Yes / No GI OKI °%, arq vt '*2 Temperature Upon Receipt: Method of *** Dechlorination (<o.s p m) of Ammonia, C aside, Phenol and TKN samples must be done in the field rior to preservation. *' • : El Comments: Shipment; Compositor A [] UPS Jug 9 0: Fed Ex Are -these results for regulatory purposes? Yes ..,,; No Q< Report results in; mg/t Wmg/kg Q. ug/l. E: `Hand Delivery Rell qu x d by j (/yea. A Da_te:�l Time: ✓lil��Jt7b�JC 3_5f Received b �C 06 Time: / e �:•7 CltileC ReNriquisha �— a 6/,L Time: 5^� Received by: Date: Time: Relinquished by: Date: Time: r R Eeived hjr. Lab result Log 476 ' 2.68 862 2.94 488 2.69 435 2.64 834 2.92 476 2.68 478 2.68 Average 2.75 FECAL DATA SHEET Min 435 Max 862 Geometric Mean 556 Agricultural Lime Application Log Year: 2014 Project: Holly Springs Field (state -county -site -field) Soil pH Lime Requirement from soil analysis) Tons/Acre Applied(CCE Eq.) Date Applied HA-8-8 (Harold Dixon) 6.9 0.0 HA-8-9 (Harold Dixon) 6.8 0.0 CH-24-2(Harold Howard) 6.2 0.0 CH-23-2(Jean Reeves) 6.1 0.0 CH-23-3(Jean Reeves) 6.1 0.0 CH-26-1 (Rachel Johnson) 6.0 0.0 CH-26-2 (Rachel Johnson) 6.2 0.0 CH-41-3(Harold Howard) 6.3 0.0 Page 1 of 2 Report Number: 15-036-0504� (( Account Number: 46462 Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIN aleastem.com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 02/05/2015 Date Of Analysis: 02/06/2015 A&L Eastern Laboratories 17621 Whitepihe Road Richmond, Virginia 23237 (804) 743 9401 Fax (804) 271.6446 Grower: DIXON SOIL ANALYSIS REPORT Date Of Report: 02/06/2015 Submitted By: WILL VARNER Farm ID: HA-8 Analytical Method(s): Mehlich 3 Organic Matter Phosphorus "e Potassium :; Magnesium Calcium Sodium: pH y Acidity Sample ID Lab 'Soil " Field d ID, Number`„ ENR % Rate Mehlich 3 Reserve K`• Mg" Ca • Na Buffer H , Ibs/A , pp m _°. Rate• :ppm a.�; Rate. ppm, " -,Rate ppm Rate ppm Rate ,ppmRate` `� pH Index , m eq/100g meg1100g" 8 15920 2.1 L 78 860 VH 34 VL 68 VL 1 1825 VH 15 VL 6.9 0.1 10.0 NC=717 NC=17 9 15922 2.7 M 91 1535 VH 58 L 77 L 1550 VH 123 VL 6.8 0.3 8.9 NC = 446 NC = 30 Percent'Base Saturation "'' " . Nitra4e Sulfur <°Zinc u. w "Manganese .. , ". Iron` "- ... Copper -° , Boron Soluble"Salts Chlorid' - Aluintnuin.E, Sample,ID FieldID K K Mg� Ca� a Na NOS 3 _ n -Mnn e u - - CI " .-Al' - � o , o /o, 0 `- 0 /o-. , /o' 1 ni" pp " Rate ppm .;Rate ppm°. Rate Ppin - Rate Rate ppm , _ pp m, Rate- p pm ".;Rate ;ms/cm to m- Rate PR" PR _ 8 18 M 20.4 VH 22 H 259 VH 4.5 VH 0.8 M 0.08 VL 0.9 5.7 91.3 0.7 1.4 NC=37 NC=510.0 NC=138 NC=225.0 9 21 M VH H VH VH M 0.1 VL 1.7 7.2 87.1 1.1 2.9 115.3 123 1239 14.4 10.6 NC = 44 NC = 382.5 NC = 144 NC = 220.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pow'.Pow'.IV GP r H (High), VH (Very High). ENR - Estimated Nitrogen Release. ,(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 , Report Number: 15-036-0504� Account Number: 46462 www.Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIh'aleasterncom Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 i . A&t Eastern Laboratories 7621 *111tepine.Road Richmond,_Virginla 23237 (804) 743,9401 Fax (864) 271-6446, Grower: DIXON Date Received: 02/05/2015 Date Of Report: 02/06/2015 SOIL FERTILITY RECOMMENDATIONS Submitted By: WILL VARNER Farm ID: HA-8 x s :> ;Nitro em; „ P. hosptiate , Potash ;Ma nesium "Sulfur Zinc Man anese Iron Co' "'"er ; , Boron, <* .Sam Ie;ID P .. ID' Intend6 Crop , Yielti`.Goal, >a: Lime'`` N. "' PzOs ,4 KZO Mg' sS Zn Mn Fe Cu ' f B Fte1d Tons/A a � 8 Adjust pH to 6.0 0 0.0 12 0 0 9 Adjust pH to 6.0 0 0.0 3 0 0 Comments: Sample(s) : 9 Crop: Adjust pH to 6.0 _Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ �p and may not be reproduced in whole or part, nor may any reference be made to the TAWhA1t'a 1"F work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copyright 1977. Pauric McGroary Page 1 of 1 Report Number: 15-029-0596 w Account Number: 46454 u� Send To: SYNAGRO CENTRAUFARMVILLE wtluwaleastern:com MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILL` E NC 27028 Date Received: 01/29/2015 Date Of Analvsis: 01/30/2015 A&L-Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804),743-9401 Fax (804) 271,6446' _ Grower: Submitted By: WILL VARNER REEVES, MIKE LAWRENCE Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 01/30/2015 Organic Matter Phosphorus Potassium Magnesium Calcium _ Sodipum: , pH. . Acidity C E.G, SamplelD. Lab ENR Mehlich3.; Reserve K M g Ca Na _ Soil, Buffer H Field ID_ Number' % Rate Ibs/A ppm - „ Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm- Rate pH Index meq/100gf ,meq/100g 2 13225 7.7 VH 150 213 VH 103 L 281 H 1190 M 33 VL 6.1 6.79 1.4 10.1 CH-23 I I NC = 177 NC = 53 3 13226 6.4 H 150 125 VH 50 VL 228 VH 1 1152 M 133 -VL 6.1 6.83 1.0 7.5 CH-23 NC = 104 NC = 26 Percent Base Saturation Nitrate ' " Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na. H NO3N S, Zn Mn Fe Cu = B SS CI Al Field ID % %, % " % ` % - ppm Rate ppm_ Rate ppm Rate ppm Rate ppm Rate ppm.. Rate ppm Rate ms/cm Rate ppm Rate ppm 2 12 L 12.2 VH 139 VH 149 VH 2.9 H 0.6 M 0.1 VL 2.6 23.2 58.9 1.4 13.7 CH-23 NC = 25 1 NC = 305.0 1 NC = 869 1NC = 145.0 3 11 L H 101 VH VH 2.1 H 0.5 L VL CH-23 1.7 25.3 56.8 1.9 13.6 NC = 23 17.1 NC = 177.5 NC = 631 1120 NC = 105.0 10.12 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by: Ppylia IV 60w Pauric McGroary Page 1 of 1 Report Number: 15-029-0598 Y� Account Number: 46462 wwwaleastern,com Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIT Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 A&L Eastern .Laboratories_ 7621.Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 27176446 Grower: TMH ENTERPRISES SOIL ANALYSIS REPORT Submitted By: WILL VARNER Farm ID: CH-24 Analytical Method(s): Mehlich 3 Date Received: 01/29/2015 Date Of Analysis: 01/30/2015 Date Of Report: 01/30/2015 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate Ibs/A PP m Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100 g me 1100g q 2 364 VH 307 VH 277 H 1415 M 29 VL 6.2 1.4 11.7 13228 9.4 VH 150 NC = 303 NC = 157 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg 'Ca Na H NON S Zn Mn Fe Cu B SS Cl Al Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm 'Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 2 9 VL 23.7 VH 95 VH 209 VH 13.9 VH 0.7 M 0.16 VL 6.7 19.7 60.5 1.1 12.1 NC = 19 NC = 592.5 NC = 594 NC = 695.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pwr. me GpWr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. rr F c - r rl n FYrhnnna rnnsrity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 15-029-0600 Account Number: 46462�( ww Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIGuvaleastern:com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 nmp Rprpivpd- n1/99/2n15 Date OfAnalvsis: 01/30/2015 A&L Eastern Laboratories_ 7621 Whitepine Road Richmond, Virginia 23237 (804),743.9401 - Fax (804) 271.5446 Grower: RACHELJOHNSON SOIL ANALYSIS REPORT Date Of Report: 01/30/2015 Submitted By: WILL VARNER Farm ID: Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field'ID Number . % Rate Ibs/A ppm Rate ppm' Rate ppm - Rate ppm Rate ppm Rate ppm Rate P H Index megl100g meq/1009 1 13231 20.8 VH 150 195 VH 93 L 291 H 1198 M 42 VL 6.0 6.77 1.6 10.4 CH-26 NC = 162 NC = 48 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride_ Aluminum SamField PID le ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl Al % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm -Rate ppm Rate ppm 1 14 L 7.2 H 90 VH 189 VH 2.5 H 0.7 M 0.11 VL CH-26 2.3 23.3 57.6 1.8 15.5 NC = 29 NC = 180.0 NC = 563 NC = 125.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pw;. me G0w� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. 4 C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary NCDA&CS nomic Division Phone: (919) 733-2665 r4�rul r. ' Predictive s} Soil Report Client: Johnson, Bob/Rachel 12193 US 64 West Siler City, NC 27344 Mehlich-3 Extraction Sampled County: Chatham Report No. FY' ---iLO03226 Advisor: Synagro ATTN: Will Varner 2828 Tryon Rd /284 Boger Rd Raleigh, NC 27603 Sampled: 08/13/2014 Received: 08/13/2014 Completed: 08/22/2014 Farm: CH-26 Links to Helpful Information Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 80 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - WN in g/crrP; CEC and Na in meq/100 cm3; NO3-N in mg/dnt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.46 0.92 10.0 88 1.2 6.2 170 31 63 24 44 514 323 194 194 131 0.1 1 North Carolina lbb::cco Tnlst rand ct:auaissiou Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS , ,,.; .comic Division Phone: (919) 733-2655 Website: www.i_u..gov/agronomi/ Report No. FY?h_-•_'D03226 Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into -the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of ' K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should a special attention to micronutrient levels. If $, pH$, $pH, C or Z p pay p M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncaar.aov/agronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/v weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.aov/aaronomi/uvrst.htm for more information. Page 1 of 1 Report Number: 15-029-0599 Account Number: 46462 wwwaleasteraxom Send To: SYNAGRO CENTRAL LLC/HOLLY SPRII� Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/29/2015 Sample ID Field ID , 3 CH-41 Sample ID Field- ID A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: HAROLD HOWARD Submitted By: WILL VARNER Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analysis: 01/30/2015 Date Of Report: 01/30/2015 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % - Rate ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pprri Rate pH Index meq/100g megl100g 13229 10.2 VH 150 434 VH 301 VH 308 H 1619 M 30 VL 6.3 1.4 NC=362 NC=154 Percent Base_ Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble'Salts Chloride K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl % I % % - % % ppm Rate ppm Rate ppm Rate ppm _ Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate VH 84 VH 223 VH 14 1 VH 09 M 02 VL Lab Number 12.9 Aluminum Al ppm 3 12 L 29.1 CH-41 6.0 19.9 62.8 1.0 10.6 NC=25 NC=727.5 1 NC=525 NC=705.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation' Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary