HomeMy WebLinkAboutWQ0019098_Residual Annual Report 2014_20150302TOWN OF HOLLY SPRINGS, NC
RESIDUALS LAND APPLICATION PROGRAM,
Permit No. WQ0019098
2014 ANNUAL REPORT
Town of Holly Springs, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit Number W00019098County Wake Year 2014
Facility Name (as shown on permit) Utley Creek WWTP NPDES No. NC0063096
Land Application Operator Synagro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A and Part Band proceed to the certification. Also, if residuals were generated
but not land applied, please attach an explanation on how the residuals were handled.
PART A
Total number of application fields in permit: 41
Total number of fields land application occurred during the year: 8
Total amount of dry tons applied during the year for all application sites: 377.66
Total number of acres land application occurred during the year: 265.5
PART B
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not
limited to items 1-12 below) issued by the Division of Water Quality X YES NO.
If no, Please provide a written description why the Facility was not compliant, the dates, and explain corrective action
taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3)
copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and
three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (Applicable to 40 CFR Part 503 regulated
facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (Applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality. Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and crops grown were removed in
accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations." ll (-"1 /-)
Seann Byrd Director of Water Quality
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9(r)
2015
Signature of Land Applier Date
(if different from Permittee and Preparer)
DENR FORM ACF (5/2003)
2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
HOLLY SPRINGS, NC
'' OLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
February 2014
601,400.00
G
45.14
D
40.94
March 2014
279,000.00
G
20.94
D
19.00
April 2014
750,200.00
G
55.38
D
50.22,
May 2014
204,600.00
G
15.11
D
13.70
June 2014
632,400.00
G
46.68
D
42.34
August 2014
1,215,200.00
G
85.14
D
77.21
October 2014
936,200.00
G
75.34
D
68.35
December 2014
421,600.00
G
33.93
D
30.78
YEARLY TOTAL
5,040,600.00
G
377.66
D
342.54
1/31/2015
2014 ANNUAL REPORT
PROJECT:
FACILITY:
WWTP NPDES NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
Town of Holly Springs, NC
Holly Springs, NC
Utley Creek WWTP
PO Box 8
Holly Springs, NC 27540
919-577-1090
NCO063096
Seann Byrd
Director of Water Quality
PO Box 8
Holly Springs, NC 27540
919-577-1090
Terry Foster, ORC
PO Box 8
Holly Springs, NC 27540
919-577-2273
Synagro Central, LLC
Contact: Marshall Puryear
(336) 998-7150 ext. 17
Page: 1 of 2
Report Number: 14-115-0205 J`1C?tL Easlem La_b®t"atpi1eS Inc.
Account Number: 46462 7621 WhitepmeRcad Richmond, ftht1a2323 _(60417434401Faxxp0Q 271-6946
Submltted By: WILL VARNER wwwsatesstem corn
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55031
Sample id HOLLY SPRINGS
Project: HOLLY SPRINGS
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/22/201414:00.00
Date Received: 04125/2014 00:00
Date Reported: 04/30/2014
Total Solids *
1.77
:17700
100.0
JM
04/251201414:30
Moisture •
98.23
100.0
JM
04125/201414:30
Total Kjeldahl Nitrogen
5.71
57100
10.0
JM
04/28/2014 09AO
Total Phosphorus
4.04
40400
100
KM
04/281201413:09
Total Potassium
0.74
7400
100.
KM
04/281201413:09
Total Sulfur
0.97
9720
100
KM
04/281201413:09
Total Calcium
1.82
=18200
100
KM
04/281201413:09
Total Magnesium
0.49
A850
100
KM
04/281201413:09
Total Sodium
0.51
R6140
100
KM
04/281201413:09
Total Iron
J000
100
KM
04128/201413:09
Total Aluminum
26900
100
KM
04/281201413:09
Total Manganese
696
5
KM
041281201413.09
Total Copper
; 297
5
KM
04/28/201413:09
Total Zinc
647
5
KM
04128/201413.09
Ammonia Nitrogen
0.57
5650
10.0
JM
04/28/2014 09:40
Organic N
5.14
51450
10.0
04/28/2014 09:40
Nitrate+Nitrite-N
56.5
2.00
JM
0412812014 09:40
Total Cadmium
'<2.0
2.0
KM
04/281201413:09
SM-2540G
SM-264OG
SM4500-NH3C TKN
SW 6010C
5W 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6610C
SW 6010C
SM-4500-NH3C
CALCULATION
SM450ONO3F
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis.
Our reports and letters are torthe exclusive and canfidenUal use of aurcllants, and may not be reproduced in whole or pan, nor may any reference be made
to the work, the result, or the company in any advertising, mews release, orothorpubllo announcements without obtaining ourpriorwn7ten authorketiotL
Debbie Holt
Page: 2of2
Report Number. 14-115-0205
Account Number: 46462
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC4HOLLY SPRINGS
Mary Brewer
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 55031
Sample ld : HOLLY SPRINGS
www.afopsfemcom
A&L Eastern Laboratories, Inc.
7021 V01toplat Read Mimond, Vifghtla 23237 1804)743-941 FaK(004)27i.0446
Project. HOLLY SPRINGS
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4122/2014 14:00=
Date Received: 04125/2014 010:00
Date Reported: 04130/2014 1
Total Chromium
�1-1 9
5
KM
04128/201413:09
SW 6010C
Total Nickel
13
5
KM
04/28/201413:09
SW 6010C
Total Lead
7
5
KM
04128/201413:09
SW 6010C
Total Arsenic
3.0
3.0
KM
04/2812014 13:09
SW 6010C
Total Mercury
0.5
0.4
KM
'04128/2014 09:00
SW-7471 B
Total Selenium
5.0
KM
04/28/201413:09
SW 6010C
pH .(Standard Units)
6.80
2.00
im
04/281201.4 09:40
SW-9045D
Total Molybdenum
-.—.9
5
KM
04/28/201413:09
SW 6010C
Comments:
T
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "At. ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Out reports and letters are for the exclusive and confidential use of our crionfs, and may not be reproduced In whole or part not may any reference be made
to the work, the results, orthe company In any advertising, news releaso, or otherpubfic announcements Wfhout obtalrdng our prior wdflan authorization.
Debbie Holt
... ..... .......... . .......
F
Page: i of 2
Report Number: 14-196-0202
Account Number: 46462
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56468
Sample Id". HOLLY SPRINGS
wwyyale�eterncatn
A&L Eastern Laboratories, Inc.
Ml Wbltepino lMd Rkhmond, virglnla 232ar 10041743 8M FaJOK 271.6446
Project HOLLY SPRINGS
NC CERT#257
REPORT OF ANALYSIS date samplers: 711112014 10.00:00
Date Received: 0711512014 00:00
Date Reported: 07/2V2014
Total Solids *
1.68
,16800
100,0
BW
07/151201415:00
Moisture *
98.32
100;0
BW
07115/201415:00
Total Kjeldahi Nitrogen
5.54
55400
10.0
MW
07/16/2014 07:59
Total Phosphorus
4.33
43300
100
BW
07/16/2014 09:30
Total Potassium
0.64
6420
100
BW
07/16/2014 09:30
Total Sulfur'
0.98.
%- 9820
100 :
BW .
07116/2014 09:30
Total Calcium
2.14
21400
100
BW
07/16/2014 09:30
Total Magnesium
0.63
;w6340
100
-SW
07/16/2014 09:30
Total Sodium
0.66
5500
100
BW
07/16/2014 09:30
Total Iron
4`
i2700
100
BW
07/16/2014 09:30
Total Aluminum
30300
100
BW
07/16/2014 09:30
Total Manganese
809
5
BW
07116/2014 09:30
Total Copper
328
5
BW
07/1812014 09:30
Total Zinc
646
5
BW
07/16/2014 09:30
Ammonia Nitrogen
0.60
5950
10.0
MW
07/16/2014 07:59
Organic N
4,94
49450
10.0
07/1612014 07:59
Nitrate+Nitrite-N
107
2.00
MW
07/16/2014 08:00
Total Cadmium
-,<2,0
2.0
BW
07/16/2014 09:30
Ail values are on a dry weight basis except as noted by asterisk. Defection limit on all N series Is on a wet basis.
Our reports and letters are for the exclusive and conrxientlet use of our d hents, and may ablU reproducad in whole or par, nornray any reference be made
Who work, the iesolts, orthe dompanyin anyadvertising, nawsrelaose, or otherpublfo announcements vAYhoul obtaining ourprlorvrn7len autho&a1W.
K.
Debbie Holt
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 601OC
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C
Page: 2 of 2
Report Number: 14-196-0202 A&L Eastem Laboratories, Inc.
Account Number: 46462 7621 WnitepMefiaad Richmond Wfglnia232$7 (804)74344pt Fax(884)271.844s
Submitted By: WILL VARNER WWWalbiaternXiiin
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56468
Sample id : HOLLY SPRINGS
Project: HOLLY SPRINGS
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 7/1112D1410:00:00
Date Received: 07/16/2014 00.00
Date Reported: 07/21/2014
Total Chromium =, 21
5
BW
Total Nickel „15
5
BW
Total Lead 8
5
BW
Total Arsenic .<3.0
3.0
BW
Total Mercury 1.2
0.4
JM
Total Selenlum 1,6.0
5.0
BW
pH (Standard Units) * 6.63
2.00
MW
Total Molybdenum
5
13W
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA
IS ACCEPTABLE.
07116/2014 09.30 .
SW 6b10C
07/16/2014 09:30
SW 6010C
07/16/2014 09:30
SW 6010C
07/16/2014 09:30
SW 6010C
07/16/2014 08:30
SW 7471 B
07/16/2014 09:30
SW 6010C
0711612014 09:04
SW-9045D
07/16/2014 00:30
SW 6010C
All values are on a dry weight basis except as noted by asEe sk. Detection limit on all-N series is on a wet basis.
Our reports and letters are for the exclusive and eonfidenUel use of our c *M% and may not be reproduced in whole or part, nor may any reference be made
to the work, the resufts, or the company in any advertising, news release, or otherpubfio announcements without obtafning our prior wriffeo authorhation.
Debbie Holt
Page: t or 2
Report Number: 14-281-0204
A&L Eastern Laboratories,
Inc.
Account Number: 46462
@Y
L.
7621 Whitepine Road Richmond,Virginta23237 (804)743.3401 Fax(804)271.6446
Submitted By: WILL VARNER
Wwwaleastermcom
Send To: SYNAGRO CENTRAL LLC/HOLLY
SPRINGS
Project: HOLLY SPRINGS
Mary Brewer
NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS
Date Sampled: 10/1/2014
15:00:00
Lab Number: 58006
Date Received: 10/08/2014 00:00
Sample Id; HOLLY SPRINGS
Date Reported: 10/17/2014
RESULT
QUANTITATION
LIMIT
ANALY�IS,".-
METHODRESULT
Total Solids `
1.93
19300
100,0
JM
10/081201413:45
SM-2540G
Moisture `
98.07
100.0
JM
10/08/2014 13:45
SM-2540G
Total Kjeldahl Nitrogen
4.51
45100
10.0
JM
10/09/2014 08:19 SM4500-NH3C-TKN
Total Phosphorus
4.73
47300
100
KM
10/17/2014 08:39
SW 6010C
Total Potassium
0.53
5310
100
KM
10/17/2014 08:39
SW 6010C
Total Sulfur
0.93
9250
100
KM
10/17/2014 08:39
SW 6010C
Total Calcium
2.60
26000
100
KM
10/17/2014 08:39
SW 6010C
Total Magnesium
0.56
5550
100
KM
10/17/2014 08:39
SW 6010C
Total Sodium
0.54
5430
100
KM
10/1712014 08:39
SW 6010C
Total Iron
13700
100
KM
10/17/2014 08:39
SW 6010C
Total Aluminum
36100
100
KM
10117/2014 08:39
SW 6010C
Total Manganese
761
5
KM
10/1712014 08:39
SW 6010C
Total Copper
340
5
KM
10/17/2014 08:39
SW 6010C
Total Zinc
754
5
KM
10/17/2014 08:39
SW 6010C
Ammonia Nitrogen
0.36
3630
10.0
JM
10/09/2014 08:19
SM-4500-NH3C
Organic N
4,15
41470
10.0
10/09/2014 08:19
CALCULATION
Nitrate•r Nitrite-N
3310
2,00
JM
10/09/2014 08:20
SM450ONO3P
Total Cadmium
<2.0
2.0
KM
10117/2014 08:39
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
Our repots and totters are for the exclusive and confidential use of ourdients, and
may not be reproduced in whole orpart, norinay
any reference be made
to the work. the results, or gte cornpany in any advertising, news release, or other public announcements without obtalaing our prior writlen auttwrization.
Debbie Holt
Page: 2 of 2
Report Number: 14-281-0204 @P.
A&L Eastern Laboratories, Inc.
Account Number: 46462 7621Whhepinelioad Ricimtond,Vlrginia23237 (804170-9401 Fax(8041271.4448
Submitted By: WILL VARNER wwtnvateastero,com
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project : HOLLY SPRINGS
Mary Brewer NC CERT#257
284 BOGER RD
MOCKSVILLE, NC 27028
REPORT OF ANALYSIS
Lab Number: 58006
Sample Id: HOLLY SPRINGS
Date Sampled: 10/1/2014 15.00:00
Date Received: 10108/2014 00:00
Date Reported: 1011712014
Total Chromium
22
5
KM
10/17/2014 08,39
SW 6010C
Total Nickel
17
5
KM
10/1712014 08:39
SW 6010C
Total Lead
9
5
KM
10/17/2014 08:39
SW 6010C
Total Arsenic
4.0
3.0
KM
10117/2014 08:39
SW 6010C
Total Mercury
0.6
0.4
KM
10/09/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
10/17/2014 08:39
SW 6010C
pH (Standard Units) * 5.89
2.00
JM
10/09/2014 08:19
SW-9045D
Total Molybdenum
13
5
KM
1011712014 08:39
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES,
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al",
"Mn", AND "Se".
ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and fetters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or pan, nor may any reference be rnade
to the rtfwk, lim results, or Ore company in any advertising, news release, or other public announcements without obtaining our prior writlen authorization.
Debbie Holt
A
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0019098 Laboratory
Facility Name: HOLLY SPRINGS, NC A&L Eastern Laboratories Inc.
NPDES# : NCO063096
or WQ# (residual only)
WWTP Name: HOLLY SPRINGS
Residuals Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or
01/21/14
04/22/14
07/11/14
10/01/14
Date Composited
Percent Solids
1.80
1.77
1.68
1.93
PARAMETERS (mg/kg
dry weight)
Arsenic
3
3
<3
4
Cadmium
<2
<2
<2
<2
Mercury
0.7
0.5
1.2
0.6
Chromium
15
19
21
22
Copper
279
297
328
340
Lead ,
7
7
8
9
Molybdenum
8
9
9
13
Nickel
13
13
15
17
Selenium
<5
<5
6
5
Zinc
634
647
646
754
Total Phosphorus
36000
40400
43300
47300
TKN
64400
57100
55400
45100
Ammonia -Nitrogen
3890
5650
5950
3630
Nitrate and Nitrite
361
56.5
107
3310
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for sub ' g false information, including the possibility of fines and imprisonment for knowing violations."
X
Cj.�- Date
`�
(SIGNATURE OF PREPARE
DENR FORM RSSF (5/2003) Printed: Saturday - January 31, 201.5 at 11:43:42 for: 2065 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0019098 Laboratory
Facility Name: HOLLY SPRINGS, NC A&L Eastern Laboratories Inc.
NPDES# : NCO063096
or WQ# (residual only)
WWTP Name: HOLLY SPRINGS
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Date Sampled (grab) or 01/21/14 04/22/14 07/11/14 10/01/14
Date Composited
Percent Solids 1.80 1.77 1.68 1.93
PARAMETERS (mg/kg dry weight)
Aluminum
21400
26900
30300
36100
Calcium
17700
18200
21400
26000
Magnesium
5330
4850
6340
5550
pH
6.72
6.80
6.63
5.89
Potassium
6620
7400
6420
5310
Sodium
4310
5140
5500
5430
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the'information submitted. I am aware that there are
significant penalties for submitting fal a information, including the possibility of fines and imprisonment for knowing violations."
X .-+-- Date
,TURE OF PREPARER)
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Saturday - January 31 2015 at 11:44:04 for: 2065 01
Page: 1 of 2
Report Number: 14-022-0204 A&L Eastern Laboratories,, Inc.
w
Account Number: 46462 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax(804) 271-6446
Submitted By: WILL VARNER wwwaleastem.com
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS Project: HOLLY SPRINGS
Mary Brewer NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS Date Sampled: 1/21/201410:00:00
Lab Number: 97591 Date Received: 01/22/2014 00:00
Sample Id : HOLLY SPRINGS Date Reported: 01/27/2014
Total Solids *
1.80
18000
1uu.0
JiVI
U i/LULU 14 13:1)U
OIVI-LJ'+U17
Moisture *
98.20
100.0
JM
01/22/2014 13:30
SM-2540G
Total Kjeldahl Nitrogen
6.44
64400
10.0
JM
01/23/2014 07:39
SM-4500-NH3C-TKN
Total Phosphorus
3.60
36000
100
KM
01/23/2014 15:23
SW 6010C
Total Potassium
0.66
6620
100
KM
01/23/2014 15:23
SW 6010C
Total Sulfur
0.95
9530
100
KM
01/23/2014 15:23
SW 6010C
Total Calcium
1.77
17700
100
KM
01/23/2014 15:23
SW 6010C
Total Magnesium
0.53
5330
100
KM
01/23/2014 15:23
SW 6010C
Total Sodium
0.43
4310
100
KM
01/23/2014 15:23
SW 6010C
Total Iron
16300
100
KM
01/23/2014 15:23
SW 6010C
Total Aluminum
21400
100
KM
01/23/2014 1"5:23
SW 6010C
Total Manganese
686
5
KM
01/23/2014 15:23
SW 6010C
Total Copper
279
5
KM
01/23/2014 15:23
SW 6010C
Total Zinc
634
5
KM
01/23/2014 15:23
SW 6010C
Ammonia Nitrogen
0.39
3890
10.0
JM
01/23/2014 07:39
SM-4500-NH3C
Organic N
6.05
60510
10.0
01/23/2014 07:39
CALCULATION
Nitrate+Nitrite-N
361
2.00
JM
01/23/2014 07:40
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
01/23/2014 15:23
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-022-0204
v
A&L Eastern Laboratories, Inc...
Account Number: 46462
7621 Whitepine Road Richmond,Virginia23237 (804)743-9401 Fax (804)271-6446
Submitted By: WILL VARNER
wwtwaleastern,com
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRINGS
Project: HOLLY SPRINGS
Mary Brewer
NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS Date Sampled: 1/21/2014 10:00:00
Lab Number: 97591
Date Received: 01/22/2014 00:00
Sample Id : HOLLY SPRINGS
Date Reported: 01/27/2014
PARAMETER RESULT
RESULT
QUANTITATION
METHOD
Total Chromium
15
5 KM 01/23/2014 15:23
SW 6010C
Total Nickel
13
5 KM 01/23/2014 15:23
SW 6010C
Total Lead
7
5 KM 01/23/2014 15:23
SW 6010C
Total Arsenic
3.0
3.0 KM 01/23/2014 15:23
SW 6010C
Total Mercury
0.7
0.4 KM. 01/23/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0 KM 01/23/2014 15:23
SW 6010C
pH (Standard Units) * 6.72
2.00 JM 01/23/2014 07:39
SW-9045D
Total Molybdenum
8
5 KM 01/23/2014 15:23
SW 6010C,
Comments: _
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Mg", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SAMPLING LOG #
CUSTOMER: SYNAGRO SOUTHEAST
At
L
`
22 0204
'I
i
I
464
IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIMINIIIII(IIIII�IInIiIII�
001.22-2014
SYNAGR.O CENTRAL
HOLLY SPRINGS r field sampling procedures
PROJECT MANAGER: 1! ! 4 f7� '� -- collection Qt these samples.
Phone:
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
CHAIN OF CUSTODY
RECORD & ANALYSIS
RECORD
�i��ry �ri�,�� ��r�•,•;.-. --'j f�.��n.� � 1 ~��-fir! !1� -�J /�i L ,��'f� `'/'
Relinquished by Samples' - - Date Time Recieved by: REMARKS:
Relinquished by: Date Time Rec' ved b
!t
Relinquished by: Date Time Recieved by:
SPECIAL INSTRUCTIONS:
C�� -, 1For monitoring purposes. PO#:
ANALYSIS REQUEST
SAMPLE
I.D.
SLII
SL2
NH -N
4
NO -N
s
Organic
N
Cd
Cr
Ni
Pb
As
Hg
Se
pH
CaGO.
e uiv.
Volatile
Solids
Mo
Cl
N027N
Por
Pori
1s'r
yt
400r
Poor
Poor
Por
Por
t000,
po
Ylf
Pow
Poor
SLt: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
White —A & L Canary — MANAGER COPY
A
Sodium Absorption Ratio calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 1/21/2014 1/112014-3/31/2014 0.9752
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (4310 x 1.8000) + 100 = 77.58
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (17700 x 1.8000) = 100 = 318.6
Mg mg/I = (mg mg/kg x % Solids) + 100 = (5330 x 1.8000) = 100 = 95.94
Na meq = Na mg/I _ Molec.Wgt.Na = 77.58 = 23 = 3.37304
Ca meq = Ca mg/I + Molec.Wgt.Ca = 318.6 + 20 = 15.93
Mg meq = Mg mg/I + Molec.Wgt.Mg = 95.94 _ 12 = 7.995
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.37304 _ SgrRoot[0.5(15.93+7.995)] = 0.975239
Printed: 1 /31 /2015
Page 1 11:44
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 4/22/2014 4/1/2014-6/30/2014 1.1599
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (5140 x 1.7700) = 100 = 90:978
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (18200 x 1.7700) =100 = 322.14
Mg mg/1= (mg mg/kg x % Solids) + 100 = (4850 x 1.7700) _ 100 = 85.845
Na meq = Na mg/I _ Molec.Wgt.Na = 90.978 _ 23 = 3.95557
Ca meq = Ca mg/I + Molec.Wgt.Ca = 322.14 = 20 = 16.107
Mg meq = Mg mg/I = Molec.Wgt.Mg = 85.845 + 12 = 7.15375
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)], = 3.95557 = SgrRoot[0.5(16.107+7.15375)] = 1.15988
Printed: 1 /31 /2015
Page 1 11:44
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 7/11/2014 7/112014-913012014 1.0964
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (5500 x 1.6800) _ 100 = 92.4
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (21400 x 1.6800) + 100 = 359.52
Mg mg/I = (mg mg/kg x % Solids) = 100 = (6340 x 1.6800) =100 = 106.512
Na meq = Na mg/I = Molec.Wgt.Na = 92.4 _ 23 = 4.01739
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 359.52 = 20 = 17.976
Mg meq = Mg mg/I = Molec.Wgt.Mg = 106.512 + 12 = 8.876
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.01739 = SgrRoot[0.5(17.976+8.876)] = 1.0964
Printed: 1/31/2015
Page 1 11:45
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2065-01-AEDLIQ-NC HOLLY SPRINGS, NC AEROBICALLY 10/1/2014 10/112014-12/31/2014 1.1048
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (5430 x 1.9300) =100 = 104.799
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (26000 x 1.9300) _ 100 = 501.8
Mg mg/I = (mg mg/kg x % Solids) = 100 = (5550 x 1.9300) =100 = 107.115
Na meq = Na mg/I = Molec.Wgt.Na = 104.799 _ 23 = 4.55648
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 501.8 = 20 = 25.09
Mg meq = Mg mg/I = Molec.Wgt.Mg = 107.115 _ 12 = 8.92625
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.55648 _ SgrRoot[0.5(25.09+8.92625)] = 1.10484
Printed: 1 /31 /2015
Page 1 11:45
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: JEAN REEVES
SITE #: NC CH 00023 FIELD# : CH 00023 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 46.68
OPERATOR: MIKE LAWRENCE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 40.60 ACRES PERMITTED: 40.60
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
DATE
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,'
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
6/13/14
210,800.00 (G)
5192.118
1.77
0.383
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00 p
56.50 p
18317
FESCUE
6/14/14
217,000.00 (G)
5344.828
1.77
0.395
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00 p
56.50 p
18317
FESCUE
6/16/14
136,400.00 (G)
3359.606
1.77
0.248
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00 p
56.50 p
18317
FESCUE
6/17/14
68,200.00 (G)
1679.803
1.77
0.124
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00 p
56.50 p
18317
1 FESCUE
Jun-14
632,400.00 (G)
15,576.355
Total Gallons/Ac: 15,576.35
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
42
Annual lbs/acre
0.007
0.005
0.044
0.683
0.016
0.001
0.021
0.030
0.012
1.488 92.89
Cumulative lbs/acre
0.041
0.019
0.410
3.578
0.170
0.009
0.109
0.229
0.082
8.978
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
Yyfi,Aa
) e
212
.,,
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A '= Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: REEVES FAMILY LP
SITE #: NC CH 00023 FIELD# : CH 00023 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 39.53
OPERATOR: MIKE LAWRENCE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.20 ACRES PERMITTED: 23.20
Page: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate-
and
PAN
Win)
Crop
MONTH
Total
Per Acre
Solids
8/5/14
155,000.00 (G)
6681.034
1.68
0.468
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
I FESCUE PASTURE
8/6/14
186,000.00 (G)
8017.241
1.68
0.562
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
I FESCUE PASTURE
8/7/14
223,200.00 (G)
9620.690
1.68
0.674
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
FESCUE PASTURE
Aug-14
564,200.00 (G)
24,318.965
Total Gallons/Ac: 24,318.97
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
61
Annual lbs/acre
0.010
0.007
0.072
1.118
0.027
0.004
0.031
0.051
0.020
2.201 147.54
Cumulative lbs/acre
0.057
0.027
0.478
5.533
1 0.240
0.014
0.150
0.310
0.123
12.375
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
158
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
X'^/Gy/�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: TMH ENTERPRISES PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 55.37
SITE #: NC CH 00024 FIELD# : CH 00024 0002 OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 46.20 ACRES PERMITTED: 46.20
Page : 1
Lime Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/17/14
130,200.00 (G)
2818.182
1.77
0.208
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100. p
5,650.00
p
56.50
p 18317
FESCUE
4/18/14
136,400.00 (G)
2952.381
1.77
0.218
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00
p
56.50
p 18317
FESCUE
4/21/14
161,200.00 (G)
3489.177
1.77
0.258
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00
p
56.50
p 18317
IFESCUE
4/22/14
136,400.00 (G)
2952.381
1.77
0.218
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00
p
56.50
p 18317
FESCUE
4/23/14
99,200.00 (G)
2147.186
1.77
0.158
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100.p
5,650.00
p
56.50
p 18317
FESCUE
4/24/14
86,800.00 (G)
1878.788
1.77
0.139
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100. p
5,650.00
p
56.50
p 18317
FESCUE
Apr-14
750,200.00 (G)
16,238.095
Total Gallons/Ac:
16,238.10
As Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P PAN
TOTALS:
44
Annuallbs/acre
0.007 0.005 0.046 0.712
0.017
0.001
0.022
0.031
0.012
1.551 96.84
Cumulative lbs/acre
0.038 0.016 0.205 2.962
0.111
0.010
0.088
0.145
0.051
6.945
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
250
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: BOBBY JOHNSON, POA
SITE #: NC CH 00026 FIELD# : CH 00026 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 40.92
OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.60 ACRES PERMITTED: 31.60
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Anm onia
Nitrogen
Nitrate
and
P,
Win)Crop
MONTH
Total
Per Acre
Solids
10/6/14
93,000.00 (G)
2943.038
1.93
0.237
HSAEDL
DRY
0-<I/2"
SUR
0.5
0.30
45,100.p
3,630.00 p
3,310.00p
17166
FESCUE
10/7/14
105,400.00 (G)
3335.443
1.93
0.268
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100.p
3,630.00 p
3,310.00p
17566
FESCUE
10/8/14
111,600.00 (G)
3531.646
1.93
0.284
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE
10/9/14
86,800.00 (G)
2746.835
1.93
0.221
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE
10/10/14
111,600.00 (G)
3531.646
1.93
0.284
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE
Oct-14
508,400.00 (G)
16,088.608
Total Gallons/Ac: 16,088.61
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
45
Annual lbs/acre
0.010
0.005
0.057
0.880
0.023
0.002
0.034
0.044
0.013
1.953 122.49
Cumulative lbs/acre
0.017
0.007
0.098
1.547
0.048
0.004
0.056
0.078
0.024
3.521
Permit PAN Limit (lbs/acre) '1stCrop/2ndCrop
„.w
*,?
g}
„�
174
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
f
1339.0
267.9
15.0 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
X /
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: BOBBY JOHNSON, POA
SITE #: NC CH 00026 FIELD# : CH 0,0026 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 80.04
OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 54.10 ACRES PERMITTED: 54.10
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/8/14
241,800.00 (G)
4469.501
1.68
0.313
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
I FESCUE
8/14/14
142,600.00 (G)
2635.860
1.68
0.185
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
I FESCUE
8/15/14
142,600.00 (G)
2635.860
1.68
0.185
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
Ij FESCUE
8/16/14
-124,000.00 (G)
2292.052
1.68
0.161
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
55,400. p
5,950.00 p
107.00 p
17917
FESCUE
Aug-14
651,000.00 (G)
12,033.273
10/13/14
117,800.00 (G)
2177.449
1.93
0.175
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
I FESCUE
10/14/14
24,800.00 (G)
458.410
1.93
0.037
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
I FESCUE
10/23/14
124,000.00 (G)
2292.052
1.93
0.184
HSAEDL
DRY
0-<I/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
I FESCUE
10/24/14
161,200.00 (G)
2979.667
1.93
0.240
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE
Oct-14
427,800.00 (G)
1 79907.578
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: BOBBY JOHNSON, POA
SITE #: NC CH 00026 FIELD# : CH 00026 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 80.04
OPERATOR: ALLEN PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 54.10 ACRES PERMITTED: 54.10
Page : 2
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 19,940.85
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
53
Annual lbs/acre
0.010
0.006
0.063
0.986
0.025
0.003
0.032
0.047
0.016
2.049
133.21
Cumulativelbs/acre
0.036
0.016
0.272
3.564
0.132
0.009
0.099
0.184
0.067
7:828
211
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 r. 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: HAROLD HOWARD
SITE #: NC CH 00041 FIELD# : CH 00041 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 69.97
OPERATOR: HAROLD HOWARD CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/14/14
136,400.00 (G)
4854.093
1.80
0.364
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,400. p
3,890.00 p
361.00 p
20459
FESCUE PASTURE
3/15/14
142,600.00 (G)
5074.733
1.80
0.381
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,400. p
3,890.00 p
361.00 p
20459
FESCUE PASTURE
Mar-14
279,000.00 (G)
9,928.826
5/2/14
142,600.00 (G)
5074.733
1.77
0.375
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100. p
5,650.00 p
56.50 p
18317
I FESCUE PASTURE
5/3/14
62,000.00 (G)
2206.406
1.77
0.163
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
57,100. p
5,650.00 p
56.50 p
18317
FESCUE PASTURE
May-14
204,600.00 (G)
7,281.139
12/11/14
192,200.00 (G)
6839.858
1.93
0.550
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE PASTURE
12/12/14
229,400.00 (G)
8163.701
1.93
0.657
HSAEDL
DRY
0-<1/2"
SUR
0.5
0.30
45,100. p
3,630.00 p
3,310.00 p
17566
FESCUE PASTURE
Dec-14
421,600.00 (G)
15,003.559
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: HAROLD HOWARD
SITE #: NC CH 00041 FIELD# : CH 00041 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 69.97
OPERATOR: HAROLD HOWARD CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10
Page : 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia ,
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppnl)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 32,213.52
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
93
Annuallbs/acre
0.017
0.010
0.096
1.556
0.040
0.003
0.053
0.074
0.025
3.461
211.31
Cumulativelbs/acre
0.044
0.022
0.301
4.225
0.164
0.008
0.133
0.222
0.085
10.168
,2":r';
187
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
s
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 , 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: HAROLD DIXON PERMIT #: W00019098
SITE #• NC HA 00008 FIELD# • HA 00008 0008 OPERATOR: HAROLD DIXON
RESIDUAL SOURCE(S):* See list at bottom of report
allons (G) or Cubic Yards (CY)
Dry
or Wet Tons (WT) (specify)
Tons
DATE or
%
Per
Residual
MONTH
Total
Per Acre
Solids
2/26/14
37,200.00 (G)
1978.723
1.80
0.149
HSAEDL
2/27/14
130,200.00 (G)
6925.532
1.80
0.520
HSAEDL
2/28/14
148,800.00 (G)
7914.894
1.80
0.594
HSAEDL
Feb-14
316,200.00 (G)
16,819.149
Total Gallons/Ac: 16,819.15
TOTALS:
Annual lbs/acre
Cumulative lbs/acre
ANNUAL DRY TONS APPLIED: 23.73
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.80 ACRES PERMITTED: 18.80
Site Inches Appli- Vola- Miner-
Cond. Precip. cation tili- ali- Ammonia
Dry, Wet, Pasts Method zation zation TKN Nitrogen
MOIST 1 0-<I/2" 1 SUR 0.5 0.30 64,400. p 3,890.00 p
MOIST 0-<1/2" SUR 0.5 0.30 64,400. p 3,890.00 p
MOIST 0-<1/2" 1 SUR 0.5 0.30 64,400. p 3,890.00 p
Nitrate PAN
and (ppm) I Crop
361.00 p 1 20459 CORN
361.00 p 20459 I CORN
361.00 p 20459 I CORN
Page: 1
Lime Applied ***
Date Lbs/Ac
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
52
0.008
0.005
0.038
0.704
0.018
0.002
0.020
0.033
0.013
1.601
90.90
0.203
0.203
1.877
15.807
1.415
0.052
0.660
1.782
0.229
42.773
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
131
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
C-, /-2- // -/5 -
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: HOLLY SPRINGS, NC
OWNER: HAROLD DIXON
SITE #: NC HA 00008 FIELD# : HA 00008 0009
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 21.41
OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 22.90 ACRES PERMITTED: 22.90
Page : 1
Lime Applied ***
Date Lbs Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
2/25/14
117,800.00 (G)
5144.105
1.80
0.386
HSAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,400. p
3,890.00 p
361.00 p
20459
I BERMUDAGRASS
2/26/14
167,400.00 (G)
7310.044
1.80
0.549
HSAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
64,400. p
3,890.00 p
361.00 p
20419
1 BERMUDAGRASS
Feb-14 1
285,200.00 (G)
12,454.149
Total Gallons/Ac: 12,454.15
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
38
Annuallbs/acre
0.006
0.004
0.028
0.522
0.013
0.001
0.015
0.024
0.009
1.185
67.31
Cumulative lbs/acre
0.152
0.134
1.433
12.121
1.139
0.040
0.500
1.375
0.183
31.184``'
r
°
»
165
Permit PAN Limit (lbs/acre) I st Crop/2nd Crop
.
.. ^
.. ,
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
3
34.8
([pP{
1339.0
267.9
15.0 375.0
89.0
2500.0 � ,.
.
HSAEDL = HOLLY SPRINGS, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
P,G�sVIR�4dfa91=N`PxxL'7€�i1P•1tSf��c=1E5z Btb�
r�rraP�itit=sl L.4iip('�tc7a•1�+5�
February 10, 2014
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Holly Springs
Dear Will Varner:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX. (330) 253-4489
Website: http://www.settek.com
Order No.: 14011399
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/22/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
N�
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, Califonua 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, hidiana C-01-1-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
01-12O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 6
r
o I.
Suminit Environmental Technologies, Inc.
3310 Win St.
Workorder
Sample Summary.
lPJIRQtPQEltitAL7
CtryahogaFalls,Ohio44223
+'rrirtiral fFa'A�'�I7t'�
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 14011399
v
Website: hQ.*1Avwiv.se1tek.com
10-Feb-14
CLIENT:
Synagro
Project:
Holly Springs
Lab SampleID Client Sample ID Tag No Date Collected
Date Received Matrix
14011399-001
Holly Springs
1/21/2014 12:00:00 PM
1/22/2014'9:50:00 AM Sludge
Page 2 of 6
Sununit Environmental Technologies, Inc.
S Q--�F M W& I t 3310 Win St.
FNVIRObIMENTALTECWdQI- GicS, NC Cuyahoga Falls, Ohio44223
Analyffr.'al LeUarahlriei; TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httn:/Aviviv.senek.com
WO#: 14011399
Date Reported: 2/10/2014
Company: Synagro
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/22/2014
Project#: Holly Springs
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Holly Springs
001
1/21/2014 TCLP Arsenic(As)
0.50 ND mg/L
Sludge
EPA 6010 C
1
5.0
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Barium(Ba)
5.0 ND mg/L
Sludge
EPA 6010 C
1
100
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Cadmium(Cd)
0.10 ND mg/L
Sludge
EPA 6010 C
1
1.0
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Chromium(Cr)
0.20 ND mg/L
Sludge
EPA 6010 C
1
5.0
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Lead(Pb)
0.50 ND mg/L
Sludge
EPA 6010 C
1
5.0
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Selenium(Se)
0.50 ND mg/L
Sludge
EPA 6010 C
1
1.0
2/5/2014
WK
Holly Springs
001
1/21/2014 TCLP Silver(Ag)
0.50 ND mg/L
Sludge
EPA 6010 C
1
5.0
2/5/2014
WK
TCLP Mercury Analysis (1311/7470)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Holly Springs
001
1/21/2014 TCLP Mercury
0.0020 ND mg/L
Sludge
EPA 7470 A
1
0.20
2/5/2014
ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Holly Springs
001
1/21/2014 Chlordane, total
0.010 ND mg/L
Sludge
EPA 8081 B
1
0.030
2/7/2014
JBN
Holly Springs
001
1/21/2014 Toxaphene
0.10 ND mg/L
Sludge
EPA 8081 B
1
0.50
2/7/2014
JBN
Holly Springs
001
1/21/2014 Endrin
0.0020 ND mg/L
Sludge
EPA 8081 B
1
0.020
2/7/2014
JBN
Holly Springs
001
1/21/2014 gamma-BHC
0.0020 ND mg/L
Sludge
EPA 8081 B
1
0.40
2/7/2014
JBN
Holly Springs
001
1/21/2014 Heptachlor
0.0020 ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/7/2014
JBN
Holly Springs.
001
'1/21/2014 Heptachlor epoxide
0.0020 ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/7/2014
JBN
Holly Springs
001
1/21/2014 Methoxychlor
0.0020 ND mg/L
Sludge
EPA 8081 B
1
10
2/7/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Holly Springs
001
1/21/2014 1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
2/5/2014
MES
Holly Springs
001
1/21/2014 1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/5/2014
MES
Holly Springs
001
1/21/2014 Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/5/2014
MES
Holly Springs
001
1/21/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/5/2014
MES
Holly Springs
001
1/21/2014 Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
2/5/2014
MES
Holly Springs
001
1/21/2014 Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
2/5/2014
MES
Holly Springs
001
1/21/2014 Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
2/5/2014
MES
Holly Springs
001
1/21/2014 Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/5/2014
MES
Holly Springs
001
1/21/2014 Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
2/5/2014
MES
Holly Springs
001
1/21/2014 MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
2/5/2014
MES
Page 3 of 6
M
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14011399
,
f6S4'IRCtidPatt',�!'PitLifC91e'�[]Ld�ls,sr1
Ctq,ahogaFalls, Ohio 44223
Date Reported:
2/10/2014
kaiyticaf rabangto i¢s
TEL: (330) 253-8211 FAX. • (330) 253-4489
Company:
Synagro
Wehsile: htip:/faviviv.settek.coni
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 1/22/2014
Project#: Holly Springs
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Holly Springs
001
1/21/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
2/7/2014
AKE
Holly Springs
001
1/21/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
2/7/2014
AKE
Holly Springs
001
1/21/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
2/7/2014
AKE
Holly Springs
001
1/21/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/7/2014
AKE
Holly Springs
001
1/21/2014 Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
2/7/2014
AKE
Holly Springs
001
1/21/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
2/7/2014
AKE
butadiene
Holly Springs
001
1/21/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/7/2014
AKE
Holly Springs
001
1/21/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
2/7/2014
AKE
Holly Springs
001
1/21/2014 Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
2/7/2014
AKE
Holly Springs
001
1/21/2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
2/7/2014
AKE
Holly Springs
001
1/21/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
2/7/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Holly Springs 001 1/21/2014 2,4-D
Holly Springs 001 1/21/2014 2,4,5-TP
5.0 ND mg/L Sludge EPA 8321 A 1 10 2/5/2014 AMZ
0.50 ND mg/L Sludge EPA 8321 A 1 1.0 2/5/2014 AMZ
Page 4 of 6
AMP
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14011399
t rffl RONM EINTAL t.OG1 ; 9NC
Cuyahoga Falls, Ohio 44223
Date Reported:
2/10/2014
/�rratl;tyca! t:nara3dt7e s
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro
Website: hity:/hviviv.seliek.cont
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/22/2014
Project#:
Holly Springs
Client ID#
Lab ID#
Collected Analyte
Result Units
Matrix
Method
DF
RL Run
Analyst
Holly Springs
Holly Springs
001
001
1/21/2014 Flashpoint (140T)
1/21/2014 Cyanide, Reactive
>140 T
ND ppm
Sludge
Sludge
EPA 1010
EPA 9014
1
1
1/24/2014
0.50 1/23/2014
TAH
TIR
Holly Springs 001 1/21/2014 pH 5.7 s.u. Sludge EPA 9045 D 1 1/22/2014 AYS
Holly Springs 001 1/21/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 1/23/2014 TIR
Page 5 of 6
(Q
(D
M
O
h
Summit Environmental Technologies, Inc.
3310 Win Strut Analysis Request/Chain of Custody
('uyaho �� , - For Summit Fnvircntniental Technologies, Inc. use only
�t Falb, Ohio 44_23 Tel: 330._53.8_1 1 Fax: 330._53.4489
me iPlcak Print)
Proycl Nautc
—
SAnalytical
Parameters and Methods
Compau� Addres
Project Address
Y
E
Client Phon
409 ��
Report to
3��
? e
Client Fax No. a% ResilIts.
POti
Client Email k cisc attuil I4•1ultSZ
Quote No.7.
Contact Peru71
Sampled by
C.ht.�ck if Ohio SAP samples
`.
`r
tt
nz
i #
Sample Identification
Date
'I�e
Collecied
Collected
U
L
`'o
< ✓
a
Z
Notcs/Commcuts:
Received in lab M: I Date I Time Rwsh Requested By: 1tu,t tv appi,
(w lah martag"
WNW and wilou Page, ,hould a:aonipana ,aniple, it, the lA utor . 7hc client rctaim du pink ppa,,c
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Holly Springs WQ Permit Number:
WWTP Name: Town of Holly Springs WWTP NPDES Number:
Monitoring Period: From 01/01/2014 To 3/31/2014
WQ0019098
NCO063096
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/11 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If anolicable to alternative nerformed (Class A or Class B) comnlete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6'h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
99354
150653
263158
CFU/g
0
Annually
Grab
SM9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying = Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one'or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I -am aware that there are significant penalties for false certification including fine and imprisonment."
Sean Byrd, Director of Public WorkN Lo+:i ( c*ja.$
PreName Title (t` e or print) Land Applier Name and Title (if applicable) (type or print)
Z-� -t
Signature of Prepareri Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
FECAL DATA SHEET
Lab result
Log
99354
5.00
Min
263158
5.42
Max
125000
5.10
Geometric Mean
179641
5.25
152047
5.18
138120
5.14
142857
5.15
Average
6.18
99354
263158
150653
Contact: Amy Moore
Client: holly Springs, Town of
PO Box 8
Holly Springs, NC 27540
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 1/21/2014
Date Sample Rcvd: 1/14/2014
Meritech Work Order #
01141433
Sample. Digester # 1 Grab
P ire
1/14/14
Parameters
esults
Analys� is Date- Reporting Lunit
Meth qualifier
%Total Solids
Fecal Coliform (Sludge)
123 %
99,354 col/gdrywt
1/14114 0-100 %
d
1/14/14 130 col /g rYwt
SM 2540B
SM 9222D B1
Meritech Work Order # 01141434 Sample: Digester # 2 Grab
Parameters
Results Analysis Date Reporting unit
1/14/14
Method QWHfer
% Total Solids
Fecal Coliform (Sludge)
1.90 %
263,158 col/g dry wt
1/14/14
1/14/14
0-100 %
130 col/g dry wt
SM. 2540B
SM 9222D B1
Meritech Work Order #
01141435
Sample: Digester # 3 Grab
1/14/14
Parameters
Resu is
Analysis to
Reporting Litmit
Rye od ualifier
% Total Solids
Fecal Coliform (Sludge)
1.84 %
125,000 col/9 dry wt
1/14114
1/14/14
0-100 %
130 col/g dry wt
SM 2540B
SM 9222D
Meritech Work Order #
01141436
Sample: Digester # 4 Grab
1/14114
Parameters
Results
Analysis Date Rgp rtingLimit
Method ualifier
% Total Solids
1.67 %
1/14/14 0-100 %
SM 2540E
Fecal-Coliform(Sludge)
179,641 col/gdrywt
1/14/14 130 col/gdrywt
SM9222D
Meritech Work Order #
01141437
Sample: Digester ## 5 Grab
1/14/14
Parameters
Results
Anal sisDate Reporting Limit
Method 0ualifier
% Total Solids
1.71 %
1/14/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
152,047 col/g dry wt
1/14/14 130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
teI:(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Y Laboratory Certification No.165
Page 2
Contact: Amy Moore ReportDate 1/21/2014
Client: Holly Springs, Town of
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 1/14/14.
Meritech Work Order # 01141438 Sample: Digester # 6 Grab 1/14/14
Parameters Results An 1 sis Date Reporting Limit QUAff ier
%Total Solids 1.81 % 1/14/14 0-100 °/a SM 2940B
Fecal Coiiform (Sludge) 138,120 caI/g drywt 1/14/14 130 col/g drywt SM 9222D
Meritech Work Order # 01141439 Sample: Digester # 7 Grab 1/14/14
Parameters
Results
Analysis Date
Rwortin Litnit
Metbad gg-ffler
Solids
1.82 %
1/14/14
0-100 %
SM 2540B
,Total
I A Coliform (Sludge)
142,857 col/g dry wt
1/14/14
130 col/g dry wt
SM 9222D
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is atotal of the counts on
all filters reported per 100 ml.
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
6hain Custody Record (COC)
)
NPDES# K:e 0(pr' L.._ �CZ=�
of
Phone:
/� I
■M■ER TECH, INC.
Client;
Flo G � ` n �
Fax:
Email:
ENVIRONMENTAL LABORATORIES
Address: �
Project#
o A D1111610n of !Water Technology and Controls, 0'
_, p (L im'"r1Z
S
p a• #
s• Phone: i-336-3+t2.4746
Tuirn Around Time*
*FLUSH work must have prior approval.
642 Tameo Rd. Fax: 1-336.342-9522
Reidsville, NC 27320 EmaWeb lSite: swww.maritech-labs.com
Attention;
db`�
Std 0 0 days)
3 - 5 Day
24 - 48 Hr
Required
Lab Use
Sample Sampling Dates
& Times
PersonTakin Sam le SI nature :
Method
Only
HO
pH OK?
{. START
Location/lD Time
END
Comp?
Grab?
#ot
Cants.
Tests Required
200.81200.7
012CK7
Date
Time
Date
^
OM
3%
( i q
ff
1
—Dechlorination (4-6 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done In the field prior to preservation.***
Compositor #
Comments:
.lug #
Method of Shipment:
Are these results ior regulatory purposes?
Repgrt results in an ice?
❑ ❑
Temperature On Receipt �� --
❑ UPS
YES NO ❑ mg/L ❑
olio uishedby Date
tri91K9 Ng1L
Tlme Re dby OF
Date Time ,
0 Fed i~x
- " i
.� Hand Delivery
uis ate
Time Received by
351
Date Time
the
Qr
Relinquished by Date
Time . Received at is by
Date Time
1 )' G
')f�; rx. r , 'lilrx}r�f silr S Specific Qxygen Uptake Rate (SOUR) for Aerobic Sludge
si3i
a.,a.....�..
est Performed By
Casey Denton Date:
ample Point
Digester Sample Time`.
Jr Temp (T1): 18.5 C
' s Sal 19.8 Celsius Initial
)perator Signature:
; +
,,....t.;i� 5 1CM ,...iY-. S..:i �,
a 3Y'.t�,.: .1 ., �. 5♦,_d3 r r ra.... >S „. SP �. n, ., .} 4. .. IfL
1-10-14
1406
8.03
- [ 02
minutes _.:.._. . .:.........,.r...r.:_,.. ::;--::•-;,.t,........r _ ;.;::
(Mg/L) .r,+. �.,.. .a,.�>;1,:� ,,t., ;.•a.:�s.••:,3,< .:a'f..�.,+r: "=�>';;:ai':r t
• '•:.;�:...:. � •� uL,<!:':.,:..,.:...,,::, ��, 3f. [ .t �o r�'i,,: `sir;
1 7.73 ;... ,....,...
+„yam
`i",.:::..:r •-. :..._....,, ,.:.:;o�,rv; :cam.•, i,. �::;•'-'% I `-
2 7.2
4
6.52
� f 4." L;,• .�1f: <i??,,"•.;,
q,rx
Dish Wet
Uish
5
��
6�
Start DO should be no less th an 6.Q mg/L
If dissolved 02 below 1.0 use that read as time'Dish
Wet
Dry
6
5.80
7'
5.42
in formula if nothing less than 1.0 use 15 min read.
Dry
8
5.03
Make sure which dissolved 02 used record minutes in
% Solid
9
4.64
formula below.
TS
10 4 25
I
:
TS
Test
11 3.891
Specific Oxvaen Uf
18.62 g / L
1.23 mg
X 1 hr'
I X 1.06"20
22.929
18.618
1.25 mg O2/g/hr at 20 Celsius ;
,Test PASSED To Pass needs to be below 1.5 mg 02/9lhr at 20 Celsi
41.4351 ! grams
2.6494 ,! grams
38.7857;gr� ams
3.37151 grams
0.7221 grams
18,6181 mg/L
18.62j911
PASSED I
1
8.51
2
8.21
3
8.11
4
8.04
5
8.01
6
7.97
7
7.95
8
7.93
9
7.91
10
7.89
11
7.87
12
7.85
13
7.84
14
7.82
15
7.80
Specific Oxygen Uptake Rate (SOUR) for Aerobic Sludge
Dish Wet
29.4702
grams
Dish
2.6594
grams
Start DO should be no less than 6.0 mg/L.
Wet
26.8108
4
grams
If dissolved OZ below 1.0 use that read as time #2
Dish Dry
3.1456
grams
in formula if nothing less than 1.0 use 15 min read.
Dry
�—
0.4862
grams
Make sure which dissolved 02 used record minutes in
% Solid
1.81
%
formula below.
TS
..18,134
mglL
TS
18.13
9/1
Test
PASSED
_ <2.0
Oxygen Consumption Rate (Slope), mg 02/EJmin'
8.51 mg/L Time 1 - 7.80'mg/L Time 2 ` 0.0507
mg 02/L/min
15 Time 2 (min) - 1 Time 1 (min)
Specific Oxygen Uptake Rate,mg 02Jg/hr at 20 degrees
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Holly Springs WQ Permit Number: WQ0019098
WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096
Monitoring Period: From 04/01/2014 To 6/30/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlirahi. +n a14PrnafivP nerf--il Win cc A nr (`lace Rl rnm"WP the fnllnwinu mnnitnrinu Antae
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61
MPN
MPN/g
Coliform
power per gram
of total solids
98458
167355
226227
CFU/g
0
Annually
Grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Mt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Sean Byrd, Director of Public Works
Prep Na Title (ty e or print) Land Applier Name and Title (if applicable) (type or print)
2
Signature of Preparer* I Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
FECAL DATA SHEET
Lab result
Log
226227
5.35
Min 98458
189781
5.28
Max 226227
160584
5.21
Geometric Mean 167355
172662
5.24
185606
5.27
169014
5.23
98458
4.99
Average
5.22
Meritech, Ines
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Amy Moore
Report Date:
4/24/2014
Client: Holly Springs, Town of
NPDES#:
NCO063096
PO Box 8
Holly Springs, NC 27540
Date Sample Rcvd:
4/14/2014
Meritech Work Order #
04141412 Sample: ICT Grab
4/14/14
Parameters
Result Anal sate
Reporting Limit
Method
% Total Solids
1.37 % 4115114
0-100 %
SM 2540B
Fecal Coliforni (Sludge)
226,227 col/gdrywt 4/14/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04141413 Sample: ICT Grab
4/14/14
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.37 % 4/15/14
0-100 %
SM 2540E
Fecal Coliform (Sludge)
189,781 col/g dry wt 4114/14
130 col/g dry wt
SM 9222D
i^
Meritech Work Order #
04141414 Sample: ICT Grab
4/14/14
Parameters
Result Analysis Date
ReporthigUrnit
Method
%Total Solids
1.37 % 4/15/14
0-100 %
SM 2540B
Fecal Coliform. (Sludge)
160,584 col/9 dry wt 4/14/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04141415 Sample: ICT Grab
4/14/14
Parameters
Result Analysis Date
Reporting Liinit
Method
% Total Solids
1.39 % 4/15/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
172,662 col/g dry wt 4/14/14
130 cal/g diy wt
SM 9222D
Meritech Work Order ## 04141416 Sample: ICT Grab 4/14/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.32 o/a 4/15/14 0-100 % SM 2540B _ _ _-
Fecal Coliform (Sludge) 185,606 col/g dry wt 4/14/14 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
r =
Environmental Laboratory
A
Laboratory Certification No.165
Page 2
Contact; Amy Moore
Report Date:
4/24/2014
Client: Holly Springs, Town of
NPDES#•
NCO063096
PO Box 8
Holly Springs, NC 27540
Date Sample Rcvd:
4/14/2014
Meritech Work Order # 04141417 Sample: ICT Grab
4114/14
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
1.42 % 4/15/14
0-100 %
SM 2540B
Fecal Coliforxn (Sludge) 169,014 col/g dry wt 4/14/14
130 col/g dry wt
SM 9222D
Meritech Work Order # 04141418 Sample: ICT Grab 4/14/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.385 % 4/15/14 0-100 % SM 2540B
Fecal Colifonn (Sludge) 98,458 col/g drywt 4/14114 130 col/g dry wt SM 9222D
I
I hereby certify thatX have reviewed and approve these data. �f _
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
Eel.(336)342-4743 fax.(336)342-1522
Chain of Custody Record (C®C)
Client:
Address:
Aitfention:
Holly Springs
Amy Moore
NPDEs#:
Phone: 1-919•-577-2273
Fax: -
Email:
Project:
Po #:
INC.MERITECH
Esavironmeutai. Laboratories
A. Division of Water Technology and Control, Inc.
642 Taman Rd Phone 1-336-34?,4748
Reidsville, NC Fax: 1-336-342-1522
27320 Email: wtelab ftelisouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
Std (Zo days)
r—�
a -s gay
r----7
24 -48 Itr
Sample
1,ocation/ID #
Sampling Dates & Times
Person Taking Sampie (signature):
.. '
Lab Use Only
START
END
comp?
Grab?
# of
Conts,
Tes Rea�uired
on
Ice?
pH OK?
C120K?
Date
Time
Date
Time
c
I/-1q_ y
roxo
10 z r
6-
)
k•-r�-ram
ry z �
�
�.5
L1- l
to Z If
Method of Shipment;
Comments:
❑ UPS
❑ Fed Ex
}land Delivery
El
Will these results be used for regulatory purposes?
Yes No
*RUSH workmusif be approved prior to submiffing samples.
Relinqulshed b Date: Time:
a, ! 7 IWO
Received b . l Date: Time: 3 O
Relinquished b Date: Time:
�� / I �SY0
Received b3r Date: Time:
Relinquished by: Date:
Time:
Received at lab
Date:
Time:
t
Meritech, Inc.
: Environmental Laboratory
�.. .N Laboratory Certification No.165
AV -
Page 1
Contact: Amy Moore Report Date: 4/17/2014
Client Holly Springs, Town of NPDES#: NCO063096
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 4/9/2014
Meritech Work Order # 04091462 Sample: Effluent Composite 4/6-7/14
Parameters
Re,�ults
Analysis Date
Reporting
Limit
Method
TKN
1.05 mg/L
4/15/14
0.20 mg/L
EPA 351.1
Nitrate/Nitrite, Nitrogen
4.06 mg/L
4/11/14
0.10 mg/L
EPA 353.2
Nitrogen, total
5.11 mg/L
4/16/14
0.20 mg/L
EPA 353.2
Meritech Work Order##
04091463 Sample: Effluent Composite
4/7-8/14
Parameters
Results
Analysis Date
Reparj=
Limit
Method
Nitrate, Nitrogen
2.87 mg/.L
4/9/14
0.10 mg/L
EPA 353.2
Meritech Work Order #
04091464 Sample: Effluent Composite
4/8-9/14
Parameters
Re ul
Analysis Date
Reporting
Limit
Method
Nitrate, Nitrogen
3.18 mg/L
4/9/14
0.10 mg/L
EPA 353.2
Meritech Work Order #
04091465 Sample: SWLI~ Composite
4/6-7/14
Parameters
Results
Analysis Date
Reporting
Limit
Method
TKN
66.0 mg/L
4/15/14
0.20 mg/L
EPA 351.1
Nitrate/Nitrite, Nitrogen
26.3 mg/L
4/9/14
0.10 mg/L
EPA 353.2
Nitrogen, total
92.3 mg/L
4/15/14
0.20 mg/L
EPA 353.2
Meritech Work Order #
04091466 Sample: Digester #1 Grab
4/9/14
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
2.22 %
4/11114
0-100 %
SM 2540B
Fecal Coliform (Sludge)
65,520 col/g drywt
4/9/14
130 col/g drywt
SM 9222D
Meritech Work Order #
04091467 Sample: Digester #2 Grab
4/9/14
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids 2.23 % 4/11/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 69,303 col/g drywt 4/9/14 130 col/g drywt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Amy Moore Report Date: 4/17/2014
Client: Holly Springs, Town of NPDES#: NCO063096
PO Box 8
Holly. Springs, NC 27540 Date Sample Rcvd: 4/9/2014
Meritech Work Order## 04091468 Sample: Digester #3 Grab 4/9/14
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.22 % 4/11/14
0-100 %
SM 2540B
Fecal Conform (Sludge)
73,710 col/g dry wt 4/9/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04091469 Sample: Digester 04 Grab
4/9/14
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.24 % 4/11/14
0-100 %
SM 2540B
Fecal CoIiform (Sludge)
89,286 col/g dry wt 4/9/14
130 col/g dry wt
SM. 9222D
Meritech Work Order #
04091470 Sample: Digester #5 Grab
4/9/14
Parameters
Results AnaIy!5iggDate
RepprtingUmit
Method
% Total Solids
2.24 % 4/11/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
68,993 col/g dry wt 4/9/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04091471 Sample: Digester #6 Grab
4/9/14
Parameters
Re ul ,Analysis Date
R@porting Limit
Method
%Total Solids
2.22 % 4/11/14
0-100 %
SM 2540B
.Fecal Coliform (Sludge)
77,805 col/g dry wt 4/9/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04091472 Sample: Digester #7 Grab
4/9/14
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.25 % 4/11/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
48,485 col/g dry wt 4/9/14
130 col/g dry wt
SM 9222D
I hereby certrf that I have reviewed and approve these data..
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel. (33 6) 342-4748 lax. (3 3 6) 342-15 22
�:_
r,
1fili
n Y^�r•a;x�v;
Contact: Amy Moore
Client: Holly Springs, Town of
PO Box 8
Holly Springs, NC 27540
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 6/11/2014
NPDES#: NCO063096
Date Sample Rcvd: 6/4/2014
Meritech Work Order #
06041436 . Sample: Digester #1 Grab
6/4/14
Parameters
Results
AnalvsisDate
RepgrdngLimit
Method
Qualiff r
% Total Solids
Fecal Coliform (Sludge)
2.79 %
2,260 col/g dry wt
6/5/14
6/5/14
0-100 %
130 coI/g dry wt
SM 2540B
SM 9222D
B1
Meritech Work Order #
06041437 Sample: Digester #2 Grab
6/4/14
Parameters
Results
Analysis ate
RgForting Umit
Method
ualifi r
% Total Solids
Fecal Coliform (Sludge)
2.66 %
2,371 col/g drywt
6/5/14
6/5/14
0-100 %
130 col/g drywt
SM 2540B
SM 9222D
B1
Meritech Work Order #
06041438 Sample: Digester #3 Grab
6/4/ 14
Parametgrs
Results
Analysis Date
Rwartinglimit
Method
Qualifier
% Total Solids
Fecal Coliform (SIudge)
2.74 %
1,644 col/g dry wt
6/5/14
6/S/14
0-100 %
130 col/g dry wt
SM 2540B
SM 9222D
B1
Meritech Work Order #
06041439 Sample; Interchange #4 Grab
6/4/14
Parameters
Results
Analysis Date
l2eng Limi
Method
Qualifier
% Total Solids
Fecal Coliform (Sludge)
1.45 %
56,426 col/g dry wt
6/5/14
6/5/14
0-100 %
130 col/g dry wt
SM 2540E
SM 9222D
B1
Meritech Work Order # 06041440 Sample: Interchange #5 Grab 6/4/14
Paramerer.q Results Analysis Date RgporRng%imig M t od Qualifier
% Total Solids 1.39 % 4111/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 39,241 col/gdry wt 4/9/14 130 col/gdry wt SM 9222D B1
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
' y all filters reported per 100 ml.
642 Tamco Road, Reidsville, North Carolina 27320
teI.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Envirolamental Laboratory
Laboratory Certification No.165
Contact: Amy Moore
Page 2
Client: Holly Springs, Town of Report Date:
6/11/2014
PO Box 8 NPDES#:
NCO063096
Holly Springs, NC 27540 Date Sample Rcvd:
6/4/2014
Meritech Work Order # 06041441 Sample: Interchange #6 Grab
�
6/4/14
Parameters R "7tS Aralvci,z Date Reportin¢ F unit
Method
ualSfi r
% Total Solids 1.45 % 6/5/14 0-100 %±ecal Coliform [SIudge)
,co/gdry wt 6/5/14
SM 2540B
130 col/g drywt
SM 9222D
B1
Meritech Work Order # 06041442 Sample: Interchange #7 Grab
6/4/14
Parayneters • 9esui nalysis Date R Aornna ; t
. P �, mi
Method
99ALIffur
%Total Solids 1.46 % 6/5/14 0-100 e/
Fecal Coliform (Sludge) 68,493 col/g drywt 6/5/14 130
SM 2540B
. col /g dry wt
SM 9222D
B1
131 Countable membranes with less than 20 colonies. Reported value is estimated or is a total ofthe counts on
all filters reported per 100 mi.
ram,
I hereby certtfy that I have reviewed and approve these data. (�
LaboratoryRepresento 've
642 Tatnco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Chain of Custody Record (COC)
_ NPDESI►:G.
Client:r,— � 1 i Phone;
Address: Fax:
Email:
Project:
P.0.9:
Attention: � 'ILL Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle a that apply: Email (preferred), Fax, Mail Sid x0 days) 3 - 5 Days 24s
�Use �—Q—n-l-yt
MER�� INC.
ENVIRONMENTAL LABORATORIES
r " d— 642 TamcoRd. Phone: 336-342-4748
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs,com
�-y-� f� -{'p/� �'1 y �1c YY1
W WW i l I 1 t �i l.� 1 I'�l �.! t.,J�7 co I I 1
Sample Location and/or ID #
Sampling ®aces &Times
person? gSample n t}; ,�Lab
Start
End
Con }
Grab?
It
Cont.
Test(s) Required
on ice?
e / No
pH OK?.
Cl OK?
Date
Time
Date
Time
(
6/,ql y
1035
:'#a2 rr tt
6lI ly
/637
OA16
-3 " t t
61911 r
ION
#q -T -lr e./
QYbyAc
#5
t' It r t
6Y lK
•r
Temperature Upon
Receipt:
`�
Method of
Shipment:
`** Dechlorination(<0.5
p m) of Ammonia, Cyanide, Phenol and TKN
samples
must be done in the Feld prior to reservation. ***
Comments:
Compositor It
JJug It
❑: UPS
0'. Fed Ex
Are these results for regulatory purposes? Yes 0• No Q:
Repo esults in: mg/t 0. mg/kg�. ug/I ��
(� Hand Delive
elinqu she, by:l : imes
5ry I �. Da� T
Re a Time:
e b • �,� l j f � 120.7
Q other
hell u d y: ally Time: /�
•tom
R ceiv d by; y pale: Time:
Relinquished by: Date: Time:
Received b obi �yte� } Tin
Test Performed By:
Samn-�e Paint:
Air Tern p (Ti;:
Operator Signature:
15 Time 2 (min) - '
1.48 mg 02/91hr,a
Test:, PASSED
Time uissoivetl:
(minutes) 02
{M)
1
7.23
2
6.28
3
5.41
Dish Wet,
33.0807
4 i
4.71
:
Dish
2.4248
5 `
4.23
Start DO should be no less than 6.0 mg/L.
Wet
30.6559
6
3.91
If dissolved 02 belaw 1.0 use that read as time #2
Dish Dry
2.9611
7
3.52
in formula if nothing less than 1.0 use 15 min read.
Dry
fl.5363
8
3.20
-
Make sure which dissolved 02 used record minutes in
% Solid
1.75
9
2.89
formula below.
TS
17,494
J 10
2.61
TS
17AS
11
2.30
...
Test
PASSED
12
2.03
13'
1.77
14
1.52
7
15
1.27......
.... ....
Oxygen Consumption Rate (Slope), mg`O21L/min
. . . . . . . . . . . .
7.23 mg/L Time 1
1 27 mglL Time 2
0 4257
mg OWU In
IS Time 2 (min) -
1 Tme 1 (min)
1.15 mg O2/g/h-rat 20 Celsius
Test: PASSED io P 2ss seeds fics €�e b(low 1.5 nig O21g/hr at 20 Gelspu:
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Holly Springs WQ Permit Number: WQ0019098
WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096
Monitoring Period: From 07/01/2014 To 9/30/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6`
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
506
2826
14916
CFU/g
0
Annually
Grab
SM9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Iniection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Sean Byrd, Director of Public Wm'1 "
Prepay 7e le (type or print) Land Applier Name and Title (if applicable) (type or print)
1 ' Z -A- l!
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
FECAL DATA SHEET
Lab result
Log
11107
4.05
Min 506
14916
4.17
Max 14916
8580
3.93
Geometric Mean 2826
7808
3.89
506
2.70
506
2.70
506
2.70
Average
3.45
Meritech, Inc.
Environmental Laboratory
r ' Laboratory Certification No.165
Page 1
Contact: Amy Moore Report Date: 8/7/2014
Client: Holly Springs, Town of NPDES#: NCO063096
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 7/31/2014
Meritech Work Order # 07311442 Sample: ICT- Digester 41 Grab 7131/14
Parameters
Results,
Ana ysis Date Reporting Limn
Method
Quailfer
%Total Solids
1.46 %
8/4/14 0-100 %
SM 2540E
B1
Fecal Coliform (Sludge)
11,107 col/g dry wt
7/31/14 130 col/g dry wt
SM 9222D
Meritech Work Order # 07311443 Sample: ICT- Digester #2 Grab
7131/14
Parameters
oils
Analysis Date Reporting Mtitit
ethod
Qualifie
°!o Total Solids
1.51 %
8/4/14 0-100 %
SM 2540E
Fecal Coliformn (Sludge)
14,916 col/g dry wt
7/31/14 130 col/g dry wt
SM 9222D
Meritech Work Order #
07311444 Sample: ICT- Digester #3 Grab
7/31/14
% Parameters
Results
Analysis Date Reporting niit
etb
lifie
%Total Solids
1.47 %
8/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
8,580 col/g dry wt
7/31/14 130 col/g dry wt
SM 9222D
B1
Meritech Work Order #
07311445 Sample:
ICT- Digester 04 Grab
7/31/14
Parameters
esults
Analysis Date Reporting Mini t
Method
Qualifler
% Total Solids
1.50 %
8/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
7,808 col/g dry wt
7/31/14 130 col/g dry wt
SM 9222D
B1
Meritech Work Order #
07311446 Sample: ICT- Digester #5 Grab
7/31/14
Parameters
Results
AnaWs s Date Reporting Limit
Method
Qualifier
% Total Solids
1.78 %
8/4/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 506 col/g dry wt
7/31/14 506 col/g dry wt
SM 9222D
B2
H1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 ml.
BZ Counts from all filters
were zero. The value reported is based on the number of colonies per 100 ml that
would have been reported if there had been one
colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
642 Tanico Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
1 Laboratory Certification No,165
r
Page 2
Contact: Amy Moore Report Date: 8/7/2014
Client: Holly Springs, Town of NPDES#: NCO063096
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 7/31/2014
Meritech Work Order # 07311447 Sample: ICT- Digester #6 Grab 7/31/14
Parameters
ults
Analysis Date Reporting Lhnit
Method Qualifier
% Total Solids
1.74 %
8/4/14 0-100 %
SM 2540E
Fecal Coliforin (SIudge)
< S06 col/g diy wt 7/31/14 506 col/g diy wt
SM 9222D B2
Meritech Work Order #
07311448
Saniple: I CT- Digester #7 Grab
7/31/14
Par-amet
Results
Analysis Date Reporting Limit
Method ualifier
%Total Solids 1.74 % 8/4/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 506 col/g drywt 7/31/14 .506 col/g diywt SM 9222D B2
r
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 nil.
B2 Counts fromall filters were zero. The value reported is based on the number of colonies per 100 all that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
I hereby certify thatl have reviewed and approve these data. it .
Laboratory Representative
642 Tanmco Road, Reidsville, North Carolina 27320
tel,(336)342-4748 fax,(336)342-1522
3•�o-��
Chain of Custody Record (COC)
C,
-
INC,PDES#:
Efie
Client: 2r w A . 5 r,bu s Phone: T9
`} 17
QW13
Address: Fax:
ENVIRONMENTAL LABORATORIES
Email:
iy
642 Tamco.Rd.. Phone: 336-342-4748
Project:
Reidsville NC 27320 Fax: 336-342-1522
P.O.#:
Email: info@meritech-labs.com
Attention:
Turn Around Time*
�'
ww,meritech—labs.com
How would you like your report sent? *RUSH work needs prior approval.
Std(10da 24-48Hrs
Circle all that apply: Email (preferred), Fax, Mail
s)
3-5 _Days
Sampling Dates & Times
Person 'raking Sample (5ign/Print):
,/
c"t %
Lab Use On]
Sample Location and/or ID #
Start
End
Comp?
pof
�-est��� Req��red
On Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yes o
: Cl OK?
Ts ci- fS 1L., e_.. IFe
Z
c)W
-
1
f >
L
Temperature upon
Method of
" * Dechiorination (<O.S ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Receipt'
,Y
Shipment-
Comments:
Compositor.#
Q. UPS
Q Fed EX
a these results for regulatory purposes? Yes -.1
No Report results in: mg/l. Q'
Jug #
mg/kg Q ug/L Q
Delivery
Reii quished Y: % at time:
,,, _�
Rec ' ed by:
ti
te•L
Time:
(:••tHarid
!- Other
Relin ishe by: ! D The:
/
lRenn'qu!Ked
eceiv by:
D e:
Time:
b . Date: Time:
Receivetlby Ly . b te:
(
Time ,
3
K
1
Test Performed.
Sample Point
Air Temp (T1): r
Operator Signat
Time ussv
(minutes) 01
(Mg,
1
7A5
2
6.93
3
6.66
4
6.44
628
i 6
6.09
7
5.82
8
5.69
9
5.58
10
5.42
11
5.33
12
f 5.21
13
5.10
14 '
4.99
15
4.87
Speck Oxygen Uptake Rate {SOUR) for Aerobic Sludge
a.
-Dish Wet
15.3805
s
grams
Dish
2.6390
grams
Start DO should be no less than 6.0 mg1L.
Wet
12.7415
grams
If dissolved 02 below 1.0 use that read as time #2
Dish Dry
2.8562
grams
In formula if nothing less than 1.0 use 15 min read.
Dry
0.2172
grams
Make sure which dissolved 02 used record minutes in
% Solid
1 70
%4...
formula below. -
TS
17 047
mg1L
TS
17 05
Test
PASSED
.:
Oa843 mg'02/UminX
11.057
17.047
01842
ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Holly Springs WQ Permit Number: W00019098
WWTP Name: Town of Holly Springs WWTP NPDES Number: NCO063096
Monitoring Period: From 10/01/2014 To 12/31/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to -Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahlP 4n a14Prna4ivP nerfnrmPrl (('lace A nr CI ace R) rmmnlPtP the fallnwina mnnitnrina dntn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6t
MPN
MPN/g
Coliform
power per gram
of total solids
435
556
862
CFU/g
0
Annually
Grab
SM9222D
CFU`
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Mt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Sean Byrd, Director of Public *Iet4m Qj4 f ; A:# S
Prep Name Title ( pe or print)
Signature of Preparev Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Amy Moore Report- Date: 10/13/2014
Client: Holly Springs, Town of NPDCSih NCO063096
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 10/1/2014
Meritechi Work Order # 10011440 Sample: Digester ##1 Grab
Parameters
Resul Analysis Date
10/1/14
Reporting Unii Method
% Total Solids
2.10 %
10/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 476 col/g dry wt 10/1/14
476 col/g dry wt
SM 9222D.
Meritech Work Order #
10011441
Sample: Digester #2 Grab
10/1/14
Parameters
Results
Analysis Date
ReVorting Lim i
Method
% Total Solids
2.09 %
10/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
862 col/g dry wt 10/1/14
130 col/g dry wt
SM 9222D
Meritech Work Order It '10011442
Sample: Digester #3 Grab
10/1/14
Parameters
Resul s
Analysis Date
Reporting Limit
Metho
%Total Solids
2.05 %
10/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 488 col/g dry wt 10/1/14
488 col/g dry wt
SM 9222D
Meritech Work Order #
10011443
Sample: Interchange ##4 Grab
..:................................................
.
10/1/14
Parameters
Results
Analysis Date
Reporting.l.intiC
�
%Total Solids
2.07 %
10/2/14
0-100 %
SM 2540E
Fecal Coliform (Sludge)
435 col/g dry wt
10/1/14
130 col/g dry wt
SM 9222D
Meritechi Work Order It 10011444 Sample: Interchange #5 Grab 10/1/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.16 a/o 10/2/14 0-100 % SM 2540B---
Fecal Coliform (Sludge) 834 col/g dry wt 10/1/14 506 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
rYx Environmental Laboratory
_g Laboratory Certification No.165
Page ..2
Contact: Amy Moore Report Date: 10/13/2014
Client: Holly Springs, Town of NPDES#: NC006'3096
PO Box 8
Holly Springs, NC 27540 Date Sample Rcvd: 10/1/2014
Meritech Work Order It 10011445 Sample: Interchange #6 Grab 10/1/14
Parametei Results Analysis Date Reporting Limit Method
% Total Solids 2.10 % 10/2/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 476 col/g dry wt 10/1/14 476 col/g dry wt SM 9222D
Meritech Work Order # 10011446 Sample: interchange ##7 Tank Grab 10/1/14
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
2.09 %
10/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 478 col/g dry wt
10/1/14
478 col/g dry wt
SM 9222D
1 herehy certify that-1 have reviewed and approve these data. (,
Labor-atmy Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Chair of Custody Record (COC)
rvPOEsa
9 @
INCENVIRONMENTAL LABORATORIES d
A Division of Water Technology and Controls, Inc.
r Phone: 1-336-342-4748
642 Tameo Rd. Fax: 1-336-342-1522
Reidsville, NC 27320 Entail: srtrtrtech@bellsouth.net
Web site: www.meritech4abs.corn
_
Client: "4o l
—,
Phone —
Fax:MEOTEC_
rGa
v
a ,'C �S'
Address: 1 � � ,
i i ,
i�
Email:
Project #
P.O. #
Attention:��e--
_
��
Std ([0 da
Sample Sampling Dates & Times
Location/$® START END
Date Time Date Time
Person ina Sam le si nature :
Comp?
Grab?
rret
Conts.�
ests Required
2. 0900 1
# *"*Decholrination (<4.5 ppm) of AmMonia, CY
Compositor
Jug # Comments:
Method of shipment: Are these results for egulatory purposes?
UPS YES NO [] mg/1
❑ Fed Ex Pulm&d--b
ois ed by Date
Hand Delivery Date
❑ Otheruished by Date
Around Time*
8 - 5 Day 24 - 48 Fir
Lab Use Only..
n pH Oki
Ce? C12 OK?
• tJ sC2L
ITA .
Phenol or TKN samples must be done in the field prior to preservation ***
Report results in .
mg/Kg Q Other
Time Received by
me Received by
Time a
*RUSH work must have prior approval.
Date e
/o///0 'Z7
Date Time
77a
Time
Meritech, Inc,
Environmental Laboratory
=
Laboratory Certification No.165
1
PagContact:
Am Moore
Y
Report Date:
12/9/2014
/9/
CIient- Holly Springs, Town of
PO Box 8
Holly Springs, NC 27540
Date Sample Rcvd:
11/26/2014
Meritech Work Order #
11261474 Sample: SIudge 01 Grab
11/26/14
Parameters
Results Analysis Date
Rego Ling Limit
Method
% Total Solids
1.99 % 12/2/14
0-100 %
SM 2540B
Fecal CoIiform (Sludge)
453 col/gdry wt 11/26/14
130 col/gdrywt
SM 9222D
Meritech Work Order #
11261475 Sample: SIudge 42 Grab
11/26/14
Parameters
Results AnalWs Date
Reporting Limit
Method
% Total Solids
2.01 % 12/2/14
0-100 %
SM Z540B
Fecal Conform (Sludge)
897 col/g drywt 11/26/14
130 coI/g dry wt
SM 9222D
Meritech Work Order #
11261476 Sample: Sludge #3 Grab
11/26/14
Parameters
Results Analysis Date
Reuorting Limit
Method
% Total Solids
2.02 % 12/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
1,338 col/g dry wt 11/26/14
130 col/g dry wt
SM 9222D
Meritech Work Order # 11261477
Sample: SIudge #4 Grab
11/26/14
Parameters
Results
AnalWs Date
R@porting Limit
Method
%Total Solids
1.98 %
12/2/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
901 col/g dry wt 11/26/14
130 col/g drywt
SM 9222D
Meritech Work Order##
11261478
Sample: SIudge #5 Grab
11/26/14
Parameters
Reg hs
Analysis Date
Reporting Limit
Method
%Total Solids
1.93 %
12/2114
0-100 %
SM 2540B
Fecal Coliform (Sludge)
4,668 col/g drywt 11/26/14
130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
teL(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental. Laboratory
Laboratory Certification No..165
Contact: Amy. Moore
Client: Holly Springs, Town of
PO Box 8
Holly Springs, NC 27540
Page 2
Report Date 12/9/2014
Date -Sample Rcvd: 11/26/14
Meritech Work Order•##
11261479
Sample: Sludge #6 Grab
11/26/14
Parameters
Results
Analysis Date
Reporting Limit
ethod
%Total Solids
2.O1. %.
12/2/14
0-100 %
SM 25408
Fecal Coliform (SIudge)
1,345 col/gdrywt 11/26/14
130 col/gdry wt
SM 9222D
Meritech Work Order #
11261480
Sample: Sludge #7 Grab
11/26/14
Parameters
Results
Analysis Date.
Reporting Limit
Method
%Total -Solids 1.93 % 12/2/14 0-100 % SM 2540B
Fecal Coliform CSludge) 937 col/g dry wt 11/26/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and .approve these data
Laboratory Representative
1 '
642 Tamco load, Reidsville, North Carolina 27320
teL(336)342-4748. fax.(336)342-1522
3-2&2013 Chain of Custody Record (COC)
Client: �� 1 Y L
NPDESU:
Phone:
It A IT C 6 I °
A
Address:
Fax:
ENVIRONMENTAL LABORATORIES�
Email:
'T.. .,
642 Tamco.Rd, Phone: 336-342-4748
Project: .
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs.com
Attentlon:
Urn Ar6und Time*
I
www,meritech-labs
HOW Would u like our report sent? *RUSH work needs prI4r approval.
Circle all thatepp E std coda' 33 5 Days zr -40Hrs
: ail(preferred), ax,
Mail
.Sampling Dates & Times
Perso T in Sample(Sgn/Print):
"�
,���/� Lab Use�Q—Y�ly
Sample Location and/or ID # Start End
Date Time Date time
Comp?
Grab?
pof
Test(s) Required
on Ice?
pH OK?
Cont.
Yes / No
GI OKI
°%, arq vt
'*2
Temperature Upon
Receipt:
Method of *** Dechlorination (<o.s p m) of Ammonia, C aside, Phenol and TKN samples must be done in the field rior to preservation. *' • : El
Comments:
Shipment;
Compositor A
[] UPS
Jug 9
0: Fed Ex Are -these results for regulatory purposes? Yes ..,,;
No Q< Report results in;
mg/t Wmg/kg Q. ug/l. E:
`Hand Delivery Rell qu x d by j (/yea. A Da_te:�l Time:
✓lil��Jt7b�JC
3_5f Received b �C
06 Time: / e
�:•7
CltileC ReNriquisha
�— a 6/,L Time:
5^� Received by:
Date: Time:
Relinquished by: Date: Time:
r
R Eeived hjr.
Lab result
Log
476 '
2.68
862
2.94
488
2.69
435
2.64
834
2.92
476
2.68
478
2.68
Average
2.75
FECAL DATA SHEET
Min 435
Max 862
Geometric Mean 556
Agricultural Lime Application Log
Year: 2014
Project: Holly Springs
Field
(state -county -site -field)
Soil
pH
Lime Requirement
from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applied
HA-8-8 (Harold Dixon)
6.9
0.0
HA-8-9 (Harold Dixon)
6.8
0.0
CH-24-2(Harold Howard)
6.2
0.0
CH-23-2(Jean Reeves)
6.1
0.0
CH-23-3(Jean Reeves)
6.1
0.0
CH-26-1 (Rachel Johnson)
6.0
0.0
CH-26-2 (Rachel Johnson)
6.2
0.0
CH-41-3(Harold Howard)
6.3
0.0
Page 1 of 2
Report Number: 15-036-0504� ((
Account Number: 46462
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIN
aleastem.com
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 02/05/2015 Date Of Analysis: 02/06/2015
A&L Eastern Laboratories
17621 Whitepihe Road Richmond, Virginia 23237 (804) 743 9401 Fax (804) 271.6446
Grower:
DIXON
SOIL ANALYSIS REPORT
Date Of Report: 02/06/2015
Submitted By: WILL VARNER
Farm ID: HA-8
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus "e
Potassium
:; Magnesium
Calcium
Sodium:
pH
y
Acidity
Sample ID
Lab
'Soil
"
Field
d ID,
Number`„
ENR
% Rate
Mehlich 3
Reserve
K`•
Mg"
Ca •
Na
Buffer
H
,
Ibs/A ,
pp m _°. Rate•
:ppm a.�; Rate.
ppm, " -,Rate
ppm Rate
ppm
Rate
,ppmRate`
`� pH
Index ,
m eq/100g
meg1100g"
8
15920
2.1 L 78
860 VH
34 VL
68 VL
1 1825
VH
15
VL
6.9
0.1
10.0
NC=717
NC=17
9
15922
2.7 M 91
1535 VH
58 L
77 L
1550
VH
123
VL
6.8
0.3
8.9
NC = 446
NC = 30
Percent'Base Saturation "''
" .
Nitra4e
Sulfur
<°Zinc
u. w
"Manganese
.. ,
". Iron` "-
...
Copper -°
,
Boron
Soluble"Salts
Chlorid' -
Aluintnuin.E,
Sample,ID
FieldID
K
K
Mg�
Ca�
a
Na
NOS
3
_
n
-Mnn
e
u
-
-
CI " .-Al'
-
� o ,
o
/o,
0 `-
0
/o-. ,
/o'
1
ni"
pp " Rate
ppm .;Rate
ppm°. Rate
Ppin - Rate
Rate
ppm , _
pp m, Rate-
p pm
".;Rate
;ms/cm to
m- Rate
PR"
PR _
8
18 M
20.4 VH
22 H
259 VH
4.5 VH
0.8
M
0.08 VL
0.9
5.7
91.3
0.7
1.4
NC=37
NC=510.0
NC=138
NC=225.0
9
21 M
VH
H
VH
VH
M
0.1 VL
1.7
7.2
87.1
1.1
2.9
115.3
123
1239
14.4
10.6
NC = 44
NC = 382.5
NC = 144
NC = 220.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pow'.Pow'.IV GP r
H (High), VH (Very High). ENR - Estimated Nitrogen Release. ,(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 2 of 2 ,
Report Number: 15-036-0504�
Account Number: 46462
www.Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIh'aleasterncom
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
i .
A&t Eastern Laboratories
7621 *111tepine.Road Richmond,_Virginla 23237 (804) 743,9401 Fax (864) 271-6446,
Grower:
DIXON
Date Received: 02/05/2015
Date Of Report: 02/06/2015 SOIL FERTILITY RECOMMENDATIONS
Submitted By: WILL VARNER
Farm ID: HA-8
x
s :>
;Nitro em;
„ P. hosptiate ,
Potash
;Ma nesium
"Sulfur
Zinc
Man anese
Iron
Co' "'"er ;
, Boron, <*
.Sam Ie;ID
P ..
ID'
Intend6 Crop ,
Yielti`.Goal,
>a: Lime'``
N.
"' PzOs ,4
KZO
Mg'
sS
Zn
Mn
Fe
Cu ' f
B
Fte1d
Tons/A
a
�
8
Adjust pH to 6.0
0
0.0
12
0
0
9
Adjust pH to 6.0
0
0.0
3
0
0
Comments:
Sample(s) : 9 Crop: Adjust pH to 6.0
_Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ �p and may not be reproduced in whole or part, nor may any reference be made to the TAWhA1t'a 1"F
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copyright 1977.
Pauric McGroary
Page 1 of 1
Report Number: 15-029-0596 w
Account Number: 46454
u�
Send To: SYNAGRO CENTRAUFARMVILLE wtluwaleastern:com
MARSHALL PURYEAR
284 BOGER RD
STE 204
MOCKSVILL` E NC 27028
Date Received: 01/29/2015 Date Of Analvsis: 01/30/2015
A&L-Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804),743-9401 Fax (804) 271,6446' _
Grower: Submitted By: WILL VARNER
REEVES, MIKE LAWRENCE Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 01/30/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
_
Sodipum: ,
pH. .
Acidity
C E.G,
SamplelD.
Lab
ENR
Mehlich3.;
Reserve
K
M g
Ca
Na _
Soil,
Buffer
H
Field ID_
Number'
% Rate Ibs/A
ppm - „ Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm- Rate
pH
Index
meq/100gf
,meq/100g
2
13225
7.7 VH 150
213 VH
103 L
281 H
1190
M
33 VL
6.1
6.79
1.4
10.1
CH-23
I
I NC = 177
NC = 53
3
13226
6.4 H 150
125 VH
50 VL
228 VH
1 1152
M
133 -VL
6.1
6.83
1.0
7.5
CH-23
NC = 104
NC = 26
Percent
Base Saturation
Nitrate ' "
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na.
H
NO3N
S,
Zn
Mn
Fe
Cu =
B
SS
CI
Al
Field ID
%
%,
% "
% `
% -
ppm Rate
ppm_ Rate
ppm Rate
ppm Rate
ppm
Rate
ppm.. Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
2
12 L
12.2 VH
139 VH
149
VH
2.9 H
0.6 M
0.1 VL
2.6
23.2
58.9
1.4
13.7
CH-23
NC = 25
1 NC = 305.0
1 NC = 869
1NC
= 145.0
3
11 L
H
101 VH
VH
2.1 H
0.5 L
VL
CH-23
1.7
25.3
56.8
1.9
13.6
NC = 23
17.1
NC = 177.5
NC = 631
1120
NC = 105.0
10.12
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: Ppylia IV 60w
Pauric McGroary
Page 1 of 1
Report Number: 15-029-0598 Y�
Account Number: 46462
wwwaleastern,com
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIT
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
A&L Eastern .Laboratories_
7621.Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 27176446
Grower:
TMH ENTERPRISES
SOIL ANALYSIS REPORT
Submitted By: WILL VARNER
Farm ID: CH-24
Analytical Method(s):
Mehlich 3
Date Received: 01/29/2015
Date Of Analysis: 01/30/2015 Date Of Report: 01/30/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate Ibs/A
PP m Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
P H
Index
meq/100 g
me 1100g
q
2
364 VH
307 VH
277 H
1415 M
29 VL
6.2
1.4
11.7
13228
9.4 VH 150
NC = 303
NC = 157
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
'Ca
Na
H
NON S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
%
%
%
%
%
ppm Rate ppm Rate
ppm Rate
ppm 'Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
2 9 VL 23.7 VH 95 VH 209 VH 13.9 VH 0.7 M 0.16 VL
6.7 19.7 60.5 1.1 12.1 NC = 19 NC = 592.5 NC = 594 NC = 695.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pwr. me GpWr
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
rr F c - r rl n FYrhnnna rnnsrity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 1 of 1
Report Number: 15-029-0600
Account Number: 46462�(
ww
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIGuvaleastern:com
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
nmp Rprpivpd- n1/99/2n15 Date OfAnalvsis: 01/30/2015
A&L Eastern Laboratories_
7621 Whitepine Road Richmond, Virginia 23237 (804),743.9401 - Fax (804) 271.5446
Grower:
RACHELJOHNSON
SOIL ANALYSIS REPORT
Date Of Report: 01/30/2015
Submitted By: WILL VARNER
Farm ID:
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field'ID
Number .
% Rate Ibs/A
ppm Rate
ppm' Rate
ppm - Rate
ppm Rate
ppm
Rate
ppm Rate
P H
Index
megl100g
meq/1009
1
13231
20.8 VH 150
195 VH
93 L
291 H
1198
M
42 VL
6.0
6.77
1.6
10.4
CH-26
NC = 162
NC = 48
Percent Base
Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride_
Aluminum
SamField PID le ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm -Rate
ppm Rate
ppm
1
14 L
7.2 H
90 VH
189 VH
2.5 H
0.7 M
0.11 VL
CH-26
2.3
23.3
57.6
1.8
15.5
NC = 29
NC = 180.0
NC = 563
NC = 125.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pw;. me G0w�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. 4
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
NCDA&CS nomic Division Phone: (919) 733-2665
r4�rul r. '
Predictive
s} Soil Report
Client: Johnson, Bob/Rachel
12193 US 64 West
Siler City, NC 27344
Mehlich-3 Extraction
Sampled County: Chatham
Report No. FY' ---iLO03226
Advisor: Synagro ATTN: Will
Varner
2828 Tryon Rd
/284 Boger Rd
Raleigh, NC 27603
Sampled: 08/13/2014 Received: 08/13/2014
Completed: 08/22/2014
Farm: CH-26
Links to Helpful Information
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
80
0 0
0 0
0 0
Note: 12
2 -
$pH
Test Results [units - WN in g/crrP; CEC and Na in meq/100 cm3; NO3-N in mg/dnt3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-1
Mn-All Mn-AI2
Zn-I Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.46 0.92
10.0 88 1.2 6.2 170 31
63 24
44 514
323
194 194
131 0.1 1
North Carolina
lbb::cco Tnlst rand ct:auaissiou
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture
NCDA&CS , ,,.; .comic Division Phone: (919) 733-2655 Website: www.i_u..gov/agronomi/
Report No. FY?h_-•_'D03226
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into -the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of '
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should a special attention to micronutrient levels. If $, pH$, $pH, C or Z
p pay p
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncaar.aov/agronomi/obpart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/v
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.aov/aaronomi/uvrst.htm
for more information.
Page 1 of 1
Report Number: 15-029-0599
Account Number: 46462
wwwaleasteraxom
Send To: SYNAGRO CENTRAL LLC/HOLLY SPRII�
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/29/2015
Sample ID
Field ID ,
3
CH-41
Sample ID
Field- ID
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446
Grower:
HAROLD HOWARD
Submitted By: WILL VARNER
Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Analysis: 01/30/2015 Date Of Report: 01/30/2015
Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
% - Rate ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H
Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pprri Rate pH Index meq/100g megl100g
13229 10.2 VH 150 434 VH 301 VH 308 H 1619 M 30 VL 6.3 1.4
NC=362 NC=154
Percent Base_ Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble'Salts Chloride
K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl
% I % % - % % ppm Rate ppm Rate ppm Rate ppm _ Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate
VH 84 VH 223 VH 14 1 VH 09 M 02 VL
Lab
Number
12.9
Aluminum
Al
ppm
3 12 L 29.1
CH-41 6.0 19.9 62.8 1.0 10.6
NC=25 NC=727.5 1 NC=525 NC=705.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by:
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation' Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary