WQ0018525_Residual Annual Report 2014_20150227

2014 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVI , ASTE AND HAULING, INC.
0018525
S&IIf [Pe"Tlo.1588-01-016
DWRSECTION
INFORMATION PROCESSING UNIT
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
S&ME, Inc.
8646 West Market Street, Suite 105
Greensboro, North Carolina 27409
February, 2015

February 19, 2015
NCDENR-DWQ/ Information Processing Unit
512 North Salisbury Street
Raleigh, North Carolina 27604
Reference: 2014 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling, Inc.
S&ME, Inc. Project No. 1588-01-016
Information Processing Unit:
t S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified
in the above referenced permit on behalf of Barnes Environmental Waste and Hauling, Inc.
(Barnes Environmental Waste) S&ME compiled this report using data gathered during the
compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this land application
i�
program please do not hesitate to contact Barnes Environmental Waste 252-241-5014 for
further assistance.
Sincerely,
S&ME, INC.
Martin Mabe Rob Willcox, L.S.S.
NC Land Application/Residuals Operator Natural Resources Services Leader
#22753
Enclosure(s)
cc Barnes Environmental Waste
T:\Projects\2001\ENV\1588-01-016 Barnes Environmental\2014\Annual Report\2014 ANNUAL REPORT.doc
i
I
I S&ME, INC. / 8646 W. Market Street, Suite 105 /Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com

TABLE OF CONTENTS
i SECTION NO. TITLE
I Certification Form
II Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
1 WQ Permit#: WQ0018525 County: Carteret Year: 2014
Facility Name (as shown on permit): Barnes Environmental Waste and Hauling, Inc.
Land Application Operator: Steven M. Barnes Phone: [phone] -
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No If No, skip Part A, and Part B and proceed to Part C. 'Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the ernit:
6
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
13.8
Total number of acres utilized for land application during the year:
24.7
Part B - Annual Compliance Statement:
Facility was compliant during calendar year 20,14 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached,
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. l 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 111, were complied with (applicable to 40 CFR Part 503
regulated facilities),
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received fiom the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and rermediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals fiom the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, trite, accurate,
and complete. I am aware that there are significant penalties for submitting false information, Including the possibility
-- of fines and imprisonment for knowing violations."
Steven M. Barnes, President
Permittee Name and Title (type or print), Signature of Permittee Date
Signature of Preparers` Date Signature of Land Applier Date
(if different fiom Permittee) (if different from Permittee and Preparer)
* Prepaivr is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 •(26) DENR FORM ACF (12/2006)

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

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Permit Number
Facility Name
NPOES #
W WTP Name
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attoott tNt Torrrtto Prethe wrraaPoatluy laboratory zw¢ab. aae rotothar Yom Petrtat may cotM1dit addes�eot Parameter W000125 to be aM"" Manitatae reprttaC to ba aamitnritea on tttis forrti 85
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See Below
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Laboratory 1 Environment 1. Inc
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SIG �7URE OF PREPALT
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I certify. under penalty of law, that this document was
to assure that qualified personnel properly gathered and a uafed Prepared mgmntonnayon submittina y direction or 1 am awarapa� with a system designed
penalties for submitting false information. including the possibility of fines and Imprisonment for knowing vtnattolaLons. are significant
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 16, 2014
Atlantic Station
0.60 /o oSolids Permit No. WQ0018525
12.15 pH taken from lime stabilization event)
Parameter
00
Mg/Kg Dry Weight
Pounds/Dry Ton
Nitrogen (TKN)
(% x 10,000)
(M /K
x 0.002)
0.723
28,963.000
57.926
Phosphorus
0.263
4,634.000
9.268
Potassium
0.449
3,102.000
6.204
PAN (injected)*
0.254
2,541.780
5.
PAN (surface)*
0.228
2,278.280
4.554
7
Ammonia Nitrogen
0.053
148.000
0.296
Calcium
3.558
32,003.000
64.006
Calcium Carbonate Eq.
___
Magnesium
--- . 735.000
5.470
Sodium
--- 25,160.000
50.320
Sulfur
Nitrate N / Nitrite N
Barium
--- 3.880
0.008
Chloride
Iron
Aluminum
--- 2,888.00
5.776
Arsenic
Cadmium
"' 2.50
0.005
Chromium
--- 0.50
0.001
'-- 14.000 ---
Co er
Lead
--- 699.00
1.398
Mercury
"- 14.00
0.0280.21
Molybdenum
---
0.000
Nickel
__
5.00
0.010
Selenium
8.00
0.016
Zinc
--- 5.00
0.010
--- 1,317.00
2.634
Environment 1, Incorporated 108A
"Determination of Plant Available Nitrogen
(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia
N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
= % PAN
for calculation purposes.

1085;`11.4OAKMONT'D131VE h
GREENVILLE,'N.C. 27835-7085
ATLANTIC STATION
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge "
PARAnIETERS Sample
Analysis Method
Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
2888
01/29/14 LFJ
EPA200.7
Arsenic (dry Wt. basis), mg/kg
Calcium (dry wt. Basis),. mg/kg
<2.5
01/30/14 MEL
311311-04
Cadmium (dry wt. basis), mg/kg
32003
R5
01/29/14 LFJ
02/06/14 MEL
EPA200.7
Copper (dry wt. basis), mg/kg " "
699
01/29/14 LFJ
3113B-04
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
14
01/29/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis),
14
02/04/14 ME, L
311311-04
mg/kg
Mercury (dry wt. basis), mg/kg
2735
01/29/14 LFJ
EPA200.7
Nickel (dry wt, basis), mg/kg
0.21
8
01/30/14 ADD
245.1 R3-94
Potassium (dry wt, basis), mg/kg
3102
01/29/14 LFJ
01/29/14 LFJ
EPA200.7
EPA200.7
Selenium (dry wt. basis), mg/kg
Sodium (dry basis),
<5.0
02/03/14 ME, L
311313-04
wt. mg/kg
Zinc (dry i1q. basis), mg/kg
25160
02/07/14 ADD
3111B-99
Total Solids, %
1317
01/31/14 ADD
311IB-99
TK- (dry wt.), mg/kg
0.60
28963
01/17/14 FD1ZB
01727/lA ANO
2540G-97
351.2 RZ-93
Anu[tunia \i[rogen !dr} -tomig/kQ
148
01123/1 { ANO
350.1 112-93
Nitrate-N*[rrite (dry irt.), mg/kg
4634
011I7114 ALB
365.4 -74
Plant Available Nitrogen, mg/kg
<3.88
8718
01/24/14 ANO
01/29/14 SEJ
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
01/29/14 LFJ
EPA200.7
,V
r. riuldt:(��1:7
FAX f252)`7
TD== 108 A
DATE COLLECTED: 01/16/14
DATE REPORTED ; 02/10/14
REVIEWED By:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 27, 2014
Beacons Reach 1.70 /o oSolids Permit No. WQ0018525
*Determination of Plant Available Nitrogen (PAN): mvironment I # J54A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +. Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
' 1

rinnnr1J/-NMrr,- —A (l fl_.._ _ _ __ n
BEACON'S REACH I/POND
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry rat, basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mglkg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge
Sample
(HYDROTECH)
7.0
3107
3
35647
1.3
2038
14
18
2564
0.37
9
2530
<5.0
17626
1103
1.7
2494
779
3.741
<3.82
< 5.0
Analysis Method
Date Analyst Code
01/28/14 TRB
4500HB-00
02/07/14 LFJ
EPA200.7
03/04/14 MEL
311313-04
02/07/14 LFJ
EPA200.7
03/09/14 MEL
311313-04
02/07/14 LFJ
EPA200.7
02/07/14 LFJ
EPA200.7
03/03/14 MEL
311313-04
02/07/14 LFJ
EPA200.7
02/11/14 ADD
245.1 R3-94
02/07114 LFJ
EPA200.7
02/07/14 LFJ
EPA200.7
03/10/14 NIEL
3113B-04
02/07/14 ADD
3111B-99
02/07/14 ADD
3111B-99
01/30/14 CMC
254OG-97
02/03/14 ANO
351.2 R2-93
01/30/14 ANO
350.1 R2-93
02/03/14 ALB
365.4 -74
01/31/14 ANO
353.2 R2-93
02/07/14 LFJ
EPA200.7
ID#: 554 A
DATE COLLECTED: 01/27/14
DATE REPORTED : 03/11/14
REVIEWED BY:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 31, 2014
Cape Royal Dolphin, 0.55 %Solids Permit No. WQ0018525
0
bnvirochem # 2014-16097
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate) (TKN-Ammonia N) + Ammonia N + Nitrate'N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

nvironmental Chemists, Inc.
6602 Windmill Way • Witmington, NC 28405
(910),392-0223 (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
pp [phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Fortin <,6,t Date of Report: Jan 20, 2015
post B 4WKC Customer PO #:
2894 Customer ID: 08100061
,Report #: 6
Projec Cape Royal Dolphin
Lab lit
- Cape'.R Collect D e/Time Matrix Sampled by
14-38 10:00 AM Solid/Sludge Client
T ;'
eth
Results
Date Analyzed
'Sludge
AluminLim
EPA 206.7
7330 mg/kg
01 /13/2016
EPA 200a
<17.5 mg/kg
01 /13/2016
Cadiz ;
EPA20D.7
<17.5 mglkg
01/13/2015
Qa1ciUM
EPA2oo.T
47300 mg/kg
01/12/2015
Ghro, Jl.ara
.A EPA20D.T
32.9 mglkg
01/13/2015
+COp
EPA2oo.7
1100 mg/kg
01/13/2015
iLead
EPAzooa
60.4 mglkg
01/13/2015
Allagnesruan
EPA200'7
5000mg/kg
01/12/2015
Molybdenwn
'EOA2DO.7
<17.5 mg/kg
01/13/2015
Nickel
EPA2oo.T
19.1 mg/kg
01/13/2015
Potassium
EPA2M
6730 mg/kg
01/12/2015
Selenium
EPA200.7 _
<17.5 mg/kg
01/13/2015
Sodiiam
EA200.T
34000 mg/kg
01/12/2015
?inc
EPA 2=7
3050 mg/kg
01/13/2015
Ammonia Nitrogen
EPA3W-1 "
8010 mg/kg
01/07/2015
Total Kjeldahl Nitrogen (TKN)
EPA351.2
85600 mg/kg
01/08/2015
Nitrate+Nitrite-Nitrogen
EPA3W-2
25.1 mg/kg
01/05/2015
total Solids (O!o)
SM2540 B
0.55 %
01/02/2015
PH
SiA4WD H B
6.86 units
01116/201-5
total Phosphorus
SM 45o0 P F
21400 mglkg
01/08/2015
ercury
sW807471B
<3.46 mg/kg
01/14/2015
comment: Results, except pH, re orted on'a dry weight basis. pH reported on an as received basis
Reviewed by:
:port1 "0' - -
A: 2014-16097
' Pagel of 1

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 31, 2014
Permit No. WQ00M25
CC Sass 6.88 % Solids
6.63 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(% x 10,000) (Mg/Kg(Mg/Kg x 0.002
Nitrogen (TKN) s ncnI , ,.,,
Phosphorus
1.810
18,100.000
iuy.uuu
36.200
Potassium
0.975
9,750.000
19.500
PAN (injected)*
1.657
16,569.300
33.139
AN (surface)*
1.642
16,424.800
32.850
Ammonia Nitrogen
0.029
289.000
0.578,,
Calcium
1.170
11,700.000
23.400
Calcium Carbonate E
___
Magnesium
---
5,020.000
10.040
Sodium
---
21,100.000
42.200
Sulfur
Nitrate N / Nitrite N
---
17.000
0.034
Barium
Chloride
Iron
Aluminum
---
638.00
1.276
Arsenic
---
11.40
0.023
Cadmium
---
11.40
0.023
Chromium
---
11.400
0.023
er
---
325.00
0.650
Lead
---
11.40
0.023
Mercury
---
2.16
0:004
Molybdenum'
---
11.40
0.023
Nickel
---
11.40
0.023
Selenium
-'-
11.40
0.023
Zinc
---
398.00
0.796
*Determination of Plant Available Nitrogen (PAN): Envirocherd # 2014-16099
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection_ limits
for calculation purposes.

_F Environmental Chemists, .Inc.
1 6602 Windmill Way • Wilmington, NC 28405
L.® [phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 4#37729
Fortin Contract Services
Post Office Box 4188 r
-. Emerald Isle NO 28594
Attention: Dan Fortin
Lab ID Sample ID: CCSASS
14-39220 Site: Sludge -
Collect Da
12/31/2014 1
Date of Report: Jan 20, 2015
Customer PO #:
Customer ID: 08100061
;Report #: 099
ID:
Proje CC -SASS
le Matrix Sampled by
AM Solid/Sludge Client
Test '
Met)ted
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
638 mg/kg
01/13/2015
;Arsenic
EPA200.7
<11.4 mg/kg
01/13/2015 .
Cadmium
EPA 200.7
<11.4 mg/kg
01/13/2015
Calcium
EPA 200.7
11700 mg/kg
01/12/2015
Chromium
EPA 200.7
<11.4mg/kg
01/13/2015
Copper
EPA 200.7
325 mg/kg
01/13/2015
Lead
EPA 200.7
<11.4 mg/kg
01I13/2015
Magnesium
EPA 200.7
5020 mg/kg
01/12/2015
Molybdenum
EPA 200.7
<11.4 mg/kg
01/13/2015
Nickel
EPA 200.7
<11A mg/kg
01/13/2015
?otassium
EPA 200.7
9760 mg/kg
01/1212015
oelenium
EPA 200.7
<11.4 mg/kg
01/13/2015
Sodium
EPA 200.7
21100 mg/kg
01/12/2015
?inc
EPA 200.7
398mg/kg
1 01/13/2015 ,
Ammonia Nitrogen
EPA350.1
289 mg/kg
01/07/2015
Total Kjeldahl Nitrogen (TKN)
EPA351-2
54500 mg/kg
01/08/2015
Nitrate+Nitrite-Nitrogen
EPA353.2
17.0 mg/kg
01/05/2015
Total Solids (%)
SM 2540 B
0.88 %
01/02/2015
pH
SM 4500 H s
6.63 units
01/16/2015
dotal Phosphorus
SM 4500 P F
18100 mg/kg
01/08/2015
mercury
Sw6487471B•
<2.16mg/kg
01/14/2015
"omment: Results, except pH, re orted on a dry weight basis. pH repdrted on an as received basis,
keviewed by:
point.: 20m-1eo8g
Page 1 of 1

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 31,2014
_ Cedar Point 0.54 %Solids Permit No. WQ0018525
rmvirochem # 2014-16100
*Determination of Plant Available Nitrogen (PAN): -
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

' Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
"f [phone] (Lab) • [phone] (Fax)
.;;N • - 710 Bowsertown Road • Manteo NC 27954
�.G [phone]
NCDENR. DWQ CERTIFICATE #94. US CERTIRCATE #37729
{ Pctt --
4188
uate or Report: Jan 20, 2015
`
Customer PO #:
�`aid b NC
28594
Customer ID: 08100061
-' A! 6= Dan Foitn
_,Report #:
Proj : Cedar Point Vilias
_ Lab tD Sample ID: -Cedar Point C ate/Time Matrix Sampled by
- 1 I She: Sludge
12/31/2014 ;38 AM Solid/Sludge Client
Tesf
Me
Results
Date Analyzed
Sludge Residuals
t'�uminucn
EpA2oo.7
5720 mg/kg
01/13/2015
A-sLr►ic
EPA 200.7
<17.8 mg/kg
01 /13/2015
-2 Cadmium
EPA 200.7
<17.8 mg/kg
01/13/2015
Calcium
EPA 200.7
29400 mg/kg
01/13/2015
i Chromium
EPA 200.7
<17.8 mg/kg
01/13/2015
Copper
EPA 2aD.7
359 mg/kg
01/13/2015
Lead
EPA 200.7
} <17.8 mg/kg
01/13/2015
Magnesium
HPA20D.7
3410mg/kg
'01/13/2015
Molybdenum
EPA 200.7
<17.8 mg/kg
01/13/2015
Nickel
EPA 200.7
<17.8 mg/kg
01/13/2015
;Potassium
EPA 200.7
6310 mg/kg
01113/2015
' Selenium
EPA 200.7
<17.8 mg/kg
01/13/2015
,—Sodium
EPA 200.7
29300 mg/kg 9 g
01/13/2015
.` �ZIrIC
EPA 200.7
707 mg/kg
:
01/13/2015
Ammonia Nitrogen
EPA 350.E
<37.0 mg/kg
01/07/2015
,rotal Kjeidahl Nitrogen (TKN)
EPA 351.2
64900 mg/kg
01/08/2015
Nitrate+Nitrite-Nitrogen
� EPA35s.2
,total Solids {%)
sM25ao a
3020 m /k
9 g
01/05/2015
pH
0,54 %
01/02/2015
a5oo H a
7.01 units
01/16/2015
trotal Phosphorus
8M4WO P F
16400 mg/kg
01/08/2015
ercury
swsas 7471e
<3.52 ing/kg
01/14/2015
^omment: Results, except
pH, reported on a dry weight basis. pH reported on an as received basis.
reviewed by:
Parg 10\ i

NJ
BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 4, 2014
o Permit No. WQ0018525
Colony By The Sea
0.54 /o Solids
*Determination of Plant Available Nitrogen (PAN): nuvironment 1 # b16A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not.Detected) or < detection limits are listed as detection limits
for calculation purposes.

1
}ENVILLE° N:C 27835 7085
COLONY BY THE SEA (HYDROTBCH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst Code -
Aluminum, (dry wt. basis), mg/kg
3725
03/24/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
2.8
03/24/14 bIEL
3113E-04.
Calcium (dry wt. basis), mg/kg
23503
03/24/14 LFJ
EPA200.7
Cadmium (dry wt, basis), mg/kg
1.1
03/26/14 lEL
3113B-04
Copper (dry wt. basis), mg/kg
286
03/24/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
16
03/24/14 LFJ
EPA200.7
Lead (dry weight -basis), mg/kg
21
04/03/14 11EL
3113B-04
Magnesium (dry wt. basis), mg/kg
2918
03/24/14 LFJ
EPA200.7
Dvlercury (dry wt. basis), mg/kg
0.21
03/20/14 IMLIM
245.1 R3-94
Nickel (dry wt. basis), mg/kg
10
04/04/14 LFJ
EPA200,7
Potassium (dry wt. basis), mg/kg
6839
03/24/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
04/01/14 MEL
3113E-04
Sodium (dry wt. basis), mg/kg
31869
03/21/14 ADD
3111B-99
Zinc (dry wt. basis), mg/kg
1690
03/21/14 ADD
3111B-99
Total Solids, %u
0.54
03/05/14 LW
2540G-97
TK T (dry wt.), mg/kg
5737
03/10/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
146
03/06/14 ANO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/lig
8540
03/10/14 ALB
365A -74
Nitrate -Nitrite (dry wt.), mg/kg
<3.64
03/07/14 ANO
353.2 R2-93
Plant Available Nitrogen, mg/kg
1750
03/10/14 SEJ
Molybdenum (dry wt. basis), mg/kg,
6
04/04/14 LFJ
EPA200.7
FAX
ID#: 616 A
DATE COLLECTED: 03/04/14
DATE REPORTED : 04/10/14
`t
REVIEWED BY:
G
<<< LABORATORY COPY >>>

BARNES ENVIRONMENTAL WASTE
LAND APPLIICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 16, 2014
Eight 1/2 Marina o /o Permit No. WQ0018525
0.43 Solids
*Determination of Plant Available Nitrogen (PAN): environment 1 # 196
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

icy fr�l�,IQf�'��f�[�(��1�
% hw
mUd
EIGHT & ONE-HALF MARINA VILLAGE
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4186
EMERALD ISLE ,NC 28594
Slude Analysis Method
PARAMETERS Sa Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Capper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/icg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt, basis), mglkg
Potassium (dry wt. basis), mg/kg.
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zbu (dry wt. basis), mg/kg
Total Solids,
TK.1ti' (dry ivt.), rug/kg
Ammonia \itrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
6002
01/29/14 LFJ
4
01/30/14 NIEL
3113B-04.
43064
01/29/14 LFJ
EPA200.7
"a2..
02/06/14 MEL
3113B-04
1660
01/29/14 LFJ
EPA200.7
23
01/29/14 LFJ
EPA200.7
27
02/04/14 N EL
3113B-04
3304
01/29/14 LFJ
EPA200.7
0.36
01/30/14 ADD
245.1 R3-94
9
01/29/14 LFJ
EPA200.7
4085
01/29/14 LFJ
EPA200.7
<5.0
02/03/14 MEL
3113B-04
23251
02/07/14 ADD
311IB-99
1883
01/3I/14 ADD
311IB-99
0.43
01/17/14 Hh'1B
254OG-97
38428
01/27/14 ANO
351.2 )L-93
119
01/23/14 ANO
350.1 112-93
7792
01/27/14 ALB
365.4 -74
<3.73
01/24114 ANO
353.2 R2-93
11552
01/29/14 SEJ
<5.0
01/29/14 LFJ
EPA200.7
ID#: 196
DATE COLLECTED: 01/16/14
DATE REPORTED 02/10/14
REVIEWED $X: ,. ,....

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 18, 2014
Permit No. WQ0018525
Genesis Condos WWTP
1.07 % Solids
*Determination of Plant Available Nitrogen (PAN); nnvvonment I # 68
Injected Application:
,(Mineralization Rate)(TKN-Ammonia,N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

&Wfl'ff@MH@[Ma T, 01mQpoQ ud
GENESIS CONDO ASSOCIATION(HYDROTECH
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magucsium (dry wt, basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt.. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %v
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg.
Phosphorus, T. (dry wt.), mg/lcg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wi, basis), mg/kg
L�
Sludge
Analysis
Method
Sample
Date Analyst Code
6.8
02/18/14 TRB
4500HB-00
2452
03/09/14 LFJ
EPA200.7
4
03/18/14 MEL
3113E-04
35740
03/05/14 LFJ'
EPA200.7
0.8
03/16/14 MEL
3113B-04
561
03/05/14 LFJ
EPA200.7
12
03/05/14 LFJ
EPA200.7
11
03/31/14 MEL
311313-04
4982
03/05/14 LFJ
EPA200.7
<0.02
02/26/14 ADD
245.1 R3-94
7
03/07/14 LFJ
EPA200.7
7395
03/05/14 LFJ
EPA200.7
<5.0
03/25/14 MEL
311313-04
21143
03/1.9114 114TM
3111B-99
942
03/10/14 ADD
3111B-99
1.0.7
02/19114'CMC
Z540G-97
6388
02/24/14 ANO
351.2 R2-93
2096
02/20/14 ANO
356.I R2-93
3721
02/24/14 ALB
365.4 -74
5.58
02/21/14 ANO
353.2 R2-93
<5.0
03/05/14 LFJ
EPA200.7
ID#: 68 C
DATE COLLECTED: 02/18/14
DATE REPORTED : 04/02/14
ItEVIEVdEb BX:
A,
•X��

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 6, 2014
Permit No. WQ0018525
Hampton Suites 1.37 % Solids
Lvuonmenr i, incorporated 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

a
FiAMPTON INN (HYDROTECi1)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE. ,NC 28594
PARAMETERS
PH (not to be used For reporting)
Aluminum, (dry wt. basis), mg/kg.
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mgAkg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/dig
Chromium,. T.(dry i t. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt, basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/lig
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt-),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/l:g
Molybdenum (dry wt. basis), mg/kg
Sludge
Analysis
Method
Sample
Date Analyst Code
6.9
01/07/14 TRB
4500HB-00
2130
01/13/14 LFJ
EPA200.7
<2.5
01/15/14 MEL
3113E-04
50920
01/13/14 LFJ
EPA200.7
0..7
01/17/14 MEL
3113B-04
1512
01/13/14 LFJ
EPA200.7
7
01/13/14 LFJ
EPA200.7
6
01/28/14 MEL
311313-04
3536
01/13/14 LFJ
EPA200.7
0.18
01/17/14 ADD
245.1 R3_94
9
01/13/14 LFJ
EPA200.7
3535
01/13/14 LFJ
EPA200.7
<5.0
01/16/14 MEL
3113B-04
33474
01/28/14 ADD
3111E-99
1273
01/16/14 ADD
3111E-99
1.37
01/09/14 CMC
254OG-97
45514
01/13/14 ANO
351.2 R2-93
413
01/14/14 ALB
350.1 R2-93
14902
01/13/14 ALB
365.4 74
240
01/10/14 ANO
353.2 R2-93
<5.0
01/13/14 LFJ
EPA200.7
ID#: 551 A
DATE COLLECTED: 01/06/14
DATE REPORTED : 01/3.3./14
REVIEWED BY:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 24, 2014
Mariners Point
Permit No. WQ0018525
0.65 % Solids
7.0 H
Parameter
%
Mg/Kg Dry Weight
Pounds /Dry Ton
(% x 10,000)
(M /K
x 0.002
Nitrogen (TKN)
3.406
34,061.000
'68.122
Phos horus
1.362
13,624.000
.
27.248
Potassium
0.344
3,444.000
6.888
PAN (injected)*
1.042
10,418.220
20.836
PAN (surface)*
1.029
10,288.720
20.577
Ammonia Nitrogen
0.026 259•.000
0.518
Calcium
5.990 59,895.000
119.790
Calcium Carbonate E
Magnesium
--- 4,382.000
8.764
Sodium
--- 9,014.000
18.028
Sulfur
-
Nitrate N / Nitrite N
=-- 18.620
Barium
0.037
Chloride
Iron
Aluminum
_
--- 4,273.00
8.546
Arsenic
Cadmium
--- 2.50
0.005
Chromium
--- 0.80
0.002
--- 31.000 ---
Co er
Lead �
--- 704.00
1.408
Mercury
'-- 18.00
0.036
Molybdenum
--- 0.36
0.001
Nickel
--- 5.00
0.010
Selenium
'-' 8.00
0.016
Zinc
--- 5.00
0.010
--- 4,790.00
9.580
*Determination of Plant Available Nitrogen (PAN): Environment 14 307
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

E��vir���rent 1, f
Peed
MARINERS POINT
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAIMETERS
Sludge
Sample
Analysis ilMethod
Date Analyst Code
PH (not to be used for reporting)
Aluminum, (dry basis),
7.0
04/24/14 TRB
4500HB-00
wt. mg/kg
Arsenic (dry wt. basis), mg/kg
4273
05/06/14 LFJ
EPA200.7
Calcium (dry wt. basis), mg/kg
<2.5
59895
05/07/14 iw1EL
05/06/14
3113E-04
Cadmium (dry wt. basis), mg/kg
0.8
LFJ
EPA200.7
Copper (dry wt. basis), mg/kg
704
05/15/14 MEL
3113E-04
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis),
31
05/06/14 LFJ
05/06/14 LFJ
EPA200.7
EPA200.7
mg/kg
i lMagnesium (dry wt. basis), mg/kg
18
Q382
05/06/14 X. EL
3113B-04
'Mercury (dry wt. basis), m /k
g g
0.36
OS/06114 LFJ
05/08/14 iYITM
E PA200.7
245.1 R3 94
Nickel (dry wt. basis), mg/kg kg
Potassium (dry wt. basis m
)� gig
8
05/06/14 LFJ
E PA200.7
Selenium (dry wt. basis), mg/kg
3444
<5.0
05106/14 LFJ
EPA200.7
Sodium (dry wt. basis), ibg/kg
9014
05/14/14 INIEL
3113E-04
Zinc (dry wt. basis), mg/kg
4790
05/06/14 INITNI
31118-99
Sodium Adsorption Ratio
05/07/14 INIUI
3111B-99
Total Solids, %
0.3
05/15/14 LFJ
TMN (dry wt.), mg/kg
0.65
04/25/14 CMC
2540G-97
Ammonia Nitrogen (dry wt.),mg/kg
34061
05/01/14 ANO
351.2 R2 93
Phosphorus, T. (dry wt.), mg/kg
259
13624
04/29/14 ALB
05/01/14 ALB
350.1 R2-93
Nitrate INitrite (dry wt.), mg/kg
Molybdenum (dry
18.62
04/30/14 ANO
365.4 -74
353,2 R2-93
wt. basis), mg/kg
<5.0
05/06/14 LFJ
EPA200.7
ID#: 307
DATE COLLECTED: 04/24/14
DATE REPORTED : 05/19/14
REVIEWED BY:t�J
V {
<<< LABORATORY COPY >>>

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 6, 2014
Permit No. WQ0018525
McGinnis Point 2.18 %Solids
*Determination of Plant Available Nitrogen (PAN): nnyironment 1 # JSS A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits.
for calculation purposes.

Own
W
ID#: 555 A
MCGINNIS POINT (HYDROTECH)
ATTN: DON O'MARA
O. BOX
P.DATE COLLECTED: 01/06/14
P.O. BOX 4602 EMRALD ISLE,NC 2$594 DATE REPORTED : 01/31/14
REVIEWED BY: /f
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Cade
PH (not to be used for reporting)
6.9
01/07/14 TRB
4500HB-00
Aluminum, (dry wt.. basis),. mg/kg
7408
01/13/14 LFJ
EPA200.7
Arsenic (dry wt: basis), mg/kg.
<2.5
01/15/14 MEL
311313-04
Calcium (dry wt. basis), mg/kg
52538
01/13/14. LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1
01/17/14 MEL
3113E-04
Copper (dry wt. basis), mg/kg
744
01/13/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
29
01/13/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
<2.5
01/28/14 MEL
3113E-04
Magnesium (dry wt. basis), mg/kg
2739
01/13/14 LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.44
01/17/14 ADD
245.1 R3-94
Nickel (dry wt. basis), mg/kg
10
01/13/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
1646
01/13/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/16/14 MEL
3113E-04
Sodium (dry wt. basis), mg/kg
13650
01/28/14 ADD
3111E-99
Zinc (dry wt. basis), mg/kg
1205
01/16/14 ADD
31IM99
Total Solids, %
2.18
01/09/14 CMC
2540G97
TKN (dry wt.), mg/kg
45775
01/13/14 ANO
351.2 RZ-93
Ammonia Nitrogen. (dry wt.),mg/kg
1235
01/14/14 ALB
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
17417
01/13/14 ALB
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
<3.80
01/10/14 ANO
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
01/13/14 LFJ
EPA200.7
9

( BARNES
'
ENVIRONMENTAL WASTE
LAND
APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater
Treatment Plant
Date
Sampled: January 16, 2014
NC Aquarium at Pine
Permit No. WQ0018525
0.63 % Solids
Knoll Shores
12.14 pH (taken from lime stabilization
event)
Parameter
% Mg/Kg Dry Weight Pounds/Dry Ton
=, Nitrogen (TKN)
(% x 10,000) /K
x 0.002)
4.523 45,233.000
90:466
Phos horus
2.018 20,176.000
40.352
Potassium
0.520 5,198.000
10.396
PAN (injected)*.
1.366 13,664.340
27.329
PAN (surface)*
1.360 13,600.34-0
27.201
Ammonia Nitrogen
0.013 128.000
0.256
Calcium
5.383 53,826.000
107.652
Calcium Carbonate E
Ma nesium
--- 11,509.000
23.018
Sodium
--- 102,989.000
205.978
Sulfur
Nitrate N / Nitrite N
--- 4.840
Barium
0.010.
Chloride
---
Iron
---
---
Aluminum
--- 1,164.00
2.328
Arsenic
--- 2.50
0,005
Cadmium
--- 43.00
0.0869.000
Chromium
---
er
Lead
--- 602.00
---
1.204
Mercury
23.00
0.046
Molybdenum
--- 0.20
0.000
Nickel
--- 5.00
0.010
Selenium
--- 13.00
0.026
Zinc
--- 5.00
0.010
--- 568.00
1.136
Environment 1 # 444 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
= % PAN
for calculation purposes.

i'.;. 13GX�708�
(11=iEENV1LLE;:
NC AQUARIUM AT PINE KNOLL SHOR3S
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
AlumUnun, (dry wt, basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T,(dry wt. basis),mg/kg
Lead (dry weight basis), ,tkg
Alagnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/ltg
Selenium (dry wt. basis), mg/]tg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Totat. Solids, %
TKN (dry wt.), . mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mglltg
Molybdenum (dry wt. basis), mg/kg
Sludge
Analysis
Method
Sample
Date Analyst Code
1164
01/29/14 LFJ
EPA2.00.7
<2.5
01/30/14 A1EL
3113E-04
53826
01/29/14 LFJ
EPA200.7
41> *3
03/09/14 AIEL
311313-04
602
01/29/14 LFJ
EPA200.7
9
01/29/14 LFJ
EPA200.7
23
02/04/14 ME, L
3113E-04
11$09
01/29/14 LFJ
EPA200.7
0.20
01/30/14 ADD
245.1 R3-94
13
01/29/14 LFJ
EPA200.7
5199
01/29/14 LFJ*
EPA200.7
<5.0
02/03/14 A'IEL
3113E-04
102989
02/07/14 ADD
3111B-99
568
01/31/14 ADD
3111B-99
0.63
01/17/14 11M
2540G97
45233
01127/14 ANO
351.2 R2.93
129
0I/23/14 ANO
350.1 R2-93
20176
01/27/14 ALB
365.4 -74
4.84
01/24/14 ANO
353.2 R2-93
13600
01/29/14 SEJ
<5.0
01/29/14 LFJ
EPA200.7
ID#: 444 A
DATE COLLECTED: 01/16/14
DATE REPORTED a 03/10/14
REVIEWED HY:
Is
P7551e:•

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 9, 2014
Ocean Club 0.53 %Solids Permit No. WQ0018525
12.14 H (taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
x 10,000) g/Kg x 0.002
Phosphorus
0.812
8,115.000
16.230
Potassium
0.989
9,891.000
19.782
PAN (in'ected)*
1.054
10,535.290
21.071
PAN (surface)*
Ammonia Nitrogen
1.028
0.052
10,277.290
516.000
20.555
1.032
Calcium
3.284
32,836.000
65.672
Calcium Carbonate E
--_
Magnesium
---
5,171.000
10.342
Sodium
---
26,322.000
52.644
Sulfur
Nitrate N / Nitrite N
---
3.790
0.008
Barium
---
Chloride
Iron
_
Aluminum
---
2,109.00
4.218
Arsenic
Cadmium
---
---
2.50 0.70
0.005
0.001
Chromium
---
10.000
Co er
Lead
---
---
542.00
8.00
1.084
0.016
Mercury
---
0.37
0.001
Molybdenum
---
5.00
0.010
Nickel
---
8.00
0.016
Selenium
---
5.00
0.010
Zinc
--- 1
1,707.00
3.414
*Determination of Plant Available Nitrogen (PAN): Environment 1 # 404 A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite'N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Majo
ID#: 404 A
OCEAN CLUB
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED:-01/09/14
EMERALD ISSLELE NC 28594
P.O. BOX DATE REPORTED : 02/10/14
A
PARAMETERS
Aluminum, On, •v-t. basis), mg/3,g
arsenic (dry Aq. basis), mg/kg
Calcium (dry art. basis), mg/kg
Cadmium On. -.m basis), mg/kg
Capper /dry art. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead. (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (.dry wL basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/l:g
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mglkg
\iz m— Nitrite. (dn jvt.), mg/kg .
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt, basis), mg/kg
REVIEWED BY:
Sludge
r
3,aalysis
lfethad
Sample
Date Analyst
Code
2109
01/29/14 LFJ
EPA200.7
<2.5
01/30/14 MEL
3113E-04
32836
01/29/14 LFJ
EPA200.7
6-7 .
02/06/14 MEL
3113B-04
542
01/29/14 LFJ
EPA200.7
10
01/29114 LFJ
EPA200.7
8
02/04/14 A1EL
3-113B-04
5171
01/29/14 LFJ
EPA200.7
0.37
01/17/14 ADD
245A R3-94
8
01/29/14 LFJ
EPA200.7
9891
01/29/14 LFJ
EPA200:7
<5.0
02/03/14 AWL
3113B-04
26322
01/28/14 ADD
31118-99
1707
01/31/14 ADD
3111B.99
0.53
01/13/14 HM33
2540G97
33901
01/16/14 ANO
351.2 R2-93
516
01/14/14 ALB
350.1 R2-93
8115
01116/14 ALB
365.4 -74 t
<3.79
01/15/14 ANO
353.2 R2.93
10274
01/22/14 SEJ
<5.0
01/29/14 LFJ
EPA200.7
It

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
-Date Sampled: February 18, 2014
Permit No. WQ0018525
Oceans Condominiums 1.22 % Solids
6.8 vH
FE:Parameter % Mg/Kg Dry Weight ==1
(% x 10,000)
Nitrogen (TKNI n zn A ,-
Phos horus
---
0.266
-.,—i.vvv
4,508.000
i5.LJ4
9.016
Potassium
0.504
5,622.000
11.244
PAN (injected)*
0.118
1,183.200
2.366
PAN (surface)*
0.105
1,048.700
2.097
Ammonia Nitrogen
0.027
2,999.000
5.998
Calcium
5.876
26,577.000
53.154
Calcium Carbonate E
___
Magnesium
0.418
3,519.000
7.038
Sodium
---
16,028.000
32.056
Sulfur
Nitrate N / Nitrite'N
---
5.800
0.012
Barium
Chloride
Iron
_
Aluminum
---
1741.000
3.482
Arsenic
---
2.50
0.005
Cadmium
---
0.70
0.001
Chromium
---
7.000
---
Co er
---
354.00
0.708
Lead
---
14.00
0.028
Mercury
---
0.14
0.000
Mol bdenum
---
5.00
0.010
Nickel
---
5.00
0.010
Selenium
---
5.00
0.010
Zinc
---
942.00
1.884
> nvironment 1 # 566 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application: '
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

�-„-��ro��mer�t 1, Incorporatec!
OCEANS CONDOMINImiS(HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EM$RALD ISLE ,NC 28594
Sludge
Analysis
Method
PA MVIETERS
Sample
Date Analyst Code
PH (not to be used for reporting)
6.8
02/18/14 TRB
• 4500HB-00
Aluminum, (dry wt. basis), mg/kg
1741
03/05/14 LFJ
EPA200.7
Arsenic (dry mt. basis), mg/kg
<2.5
03/18/14 IME,L
3113E-04
Calcium (dry wt. basis),, mg/kg
26577
03/05/14 LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.7
03/26/14 PMEL
311313-04
Copper (dry wt. basis), mg/kg
354
03/05/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
- 7
03/05/14 LFJ
EPA200.7
Lead (dry weight basis), 3ng/kg
14
03/31/14 MEL
3113B-04
Magnesium (dry wt. basis), mg/kg
3519
03/05/14 LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.14
02/26/14 ADD
245.1 R3-94
Nickel (dry wt. basis), mg/kg
5
03/07/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
5622
03/05/14 LFJ
.
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
03/25/14 NIEL
31138-04
Sodium (dry wt, basis), mg/kg
16028
03/19/14 Mnf
3111B-99
Zinc (dry wt, basis), mg/kg
Total Solids; %
942
03/10/14 ADD
311113-99
TION (dry wt.), mg/kg
1.22 "
02/19/14 CMC
2540G 97
Ammonia Nitrogen (dry wt.),mg/kg
4127
2999
02/24/14 ANO
351.2 R2-93
Phosphorus, T. (dry wt.), mg/kg
4508
02/20/14 ANO
02/24/14 ALIT
350.1 R2-93
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis),
5.80
02/21/14 ANO
353.2 R2-93-
mg/kg
<5.0
03/05/14 LFJ
EPA200.7
ID#: 566 A
DATE COLLECTED: 02/18/14
DATE REPORTED 04/02/14
F k
g
CE � jap �$�'/�{E r • f/ iSrl
�✓ [ L / �5Y ,,}
REVIM-IBD BY:
<<< LABORATORY COPY >>>

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 7, 2014
Permit No. WQ0018525
Ocean Terrace 1.22 % Solids
P7 *2 —u
= Parameter
% v
Mg/Kg Dry Weight
% x 10,000
Pounds/Dry Ton
/K x 0.002
Nitrogen (TKN)
5.050
50,498.000
100.996
Phos horus
1.595
15,947.000
31.894
Potassium
0.307
3,073.000
6.146
PAN (injected)*
1.541
15,412.810
30.826
PAN (surface)*
Ammonia Nitrogen
1.523.
0..037
15,227.310
371.000
30:455
0.742
Calcium
3.587
35,869.000
71.738
Calcium Carbonate E
Magnesium
---
3,268.000
6.536
Sodium"
---
18,883.000
37.766
Sulfur
-__
___
Nitrate N / Nitrite N
Barium
---
--_
3.710
0.007
Chloride
--_
---
Iron
_
Aluminum
---
6598.000
13.196
Arsenic
Cadmium
Chromium
---
---
---
3.00
1.00
20.000
0.006
0.002
---
Copper
Lead
---
---
1,739.00
36.00
3.478
0.072
Mercury
0.66
0.001
Molybdenum
---
5.00
0.010
Nickel
---
8.00
0.01.6
Selenium
---
5.00
0.010
Zinc
=--
2,278.00J��
4.556
*Determination of Plant Available Nitrogen (PAN): environment 1 # -*)J / A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes..

OCEAN TERRACE (iiYDROTECK)
ATTN: DON O' MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst Code
PH (not to be used for reporting)
7.3
01/07/14 TRB
4500HB-00
Alumm'un, (dry wt. basis), mg/kg
6598
01/13/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
3
01/15/14 AFL
3113E-04
Calcium (dry wt. basis), mg/kg
rCadmium
35869
01/13/14 LFJ
EPA200.7
(dry wt. basis), mg/kg
1
01/17/14 MEL
3113B-04
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
1739
20
01/13/14 LFJ
01/13/14
EPA200.7
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
36
01/28/14 MEL
3113B-04
Magneshun (dry wt. basis), mg/kg
3268
01/13/14 LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.66
01/17/14 ADD
245.1 R3-94
Nickel (dry wt. basis), mg/kg.
8
01/13/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3073
01/13/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/16/14 X EL
3113B-04
Sodium (dry wt. basis), mg/kg
18883
01/28/14 ADD
311IB-99
Zinc (dry wt, basis), mg/kg.
2278
01/16/14 ADD
311IB-99
Total Solids, %
1.22
01/09/14 CMC
2540G-97
TKN (dry wt.), mg/kg
50498
01/13/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
371
01/14/14 ALB
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
15947
01/13/14 ALB
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
<3.71
01/10/14 ANO
353.2 R2-93
Molybdenum (dry vvt. basis), mg/kg
<5.0
01/13/14 LFJ
EPA200.7
ID#: 557 A
DATE COLLECTED: 01/07/14
DATE REPORTED : 01/31/14
REVIEWED BY: /� -^

BARNES ENVIRONMENTAL WASTE '
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 27, 2014
Permit No. WQ0018525
Pebble Beach 1.70 % Solids
*Determination of Plant Available Nitrogen (PAN): rnvuonment 1 # 287A
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
j

EMNObBIMUM&N Flo kwoo umud.
PEBBLE. BEACH (HYDROTECH)
ATTN: DON O1MARA
HYDROTECH
P.Q. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), tug/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis),. mg/kg
Mercury (dry wt'. basis), mg/kg
Nickel (dry wt. basis); mg/kg
Potassium (dry Wt. basis),. mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis)., mg/kg
Zinc (dry Wt. basis), mg/kg
Total Solids, %n
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite. (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge
Analysis
Method
Sample
Date Analvst Code
6.6
01/28/14 TRB
4500HB-00
3760
02/07/14 LFJ
EPA200.7
<2.5
03/04114 MEL
311313-04
60439
02/07/14 LFJ
EPA200.7
1,4
03/09/14 AfE.L
3113B-04
2435
02/07/14 LFJ
EPA200.7
14
02/07/14 LFJ
EPA200,7
28
03/03/14 MEL
3113B-04
6344
02/07/14 LFJ
EPA200.7
0.23
02/11/14 ADD
24S.1 113-94
9
OV07114 LFJ
EPA200.7
2524
02/07/14 LFJ
EPA200.7
< 5.0
03110114. MEL
3113E-04
6021
02/07114 ADD
3111B-99
1685
02/07/14 ADD
3111B-99
1.7
01/30/14 CAZC
254OG-97
31113
02/03/14 ANO
351.2 R2-93
515
01/30/14 ANO
350.1 R2-93
9245
02/03/14 ALB
365.4 -74
<3.78
01/31/14 ANO
353.2 R2 93
9437
02/06/14 SEJ
<5.0
02/07/14 LFJ
EPA200.7
DATE COLLECTED:
DATE REPORTED :
REVIEWED BY:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 16, 2014
Permit No. WQ0018525
Peaaertree 0.68 % Solids
environment ] # 129
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

PEPPERTREE RESORTS
ATTN: MR. DAN FORTIN
P.O. BOX 1068.
ATLANTIC BEACH ,NC 28512
Sludge I Analysis ' Method
PARAXIETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry ivt. basis), mg/kg
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt, basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), ing/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TK\ (dry wt.), mg/kg
Ammonia Nitrogen (dry %vt.),mg/Itg
Phosphorus, T. (dry wt.), mg/kg
`citrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
2800
01/29/14 LFJ
EPA200.7
<2.5
01/30/14 il1EL
3113B-04
28814
01/29/14 LFJ
EPA200.7
Ct9 _
02/06/14 MEL
3113B-04
253
01/29/14 LFJ
EPA200.7
9
01/29/14 LFJ
EPA200.7
5
02/04/14 MEL
3113E-04
2948
01/29/14 LFJ
EPA200.7
0.19
01/30/14 ADD
245.1 R3-94
9
01/29/14 LFJ
EPA200.7
3646
01/29/14 LFJ
EPA200.7
<5.0
02/03/14 AM, L
3113B-04
15878
02/07/14 ADD
311IB-99
801
01/31/14 ADD
31I1B-99
0.68
01/17/14 MM
2540G-97
3575
01/27/1.4 ANO
35I.2 R2-93
254 .
01/23/14 ANO
350.1 R2-93
8043
01/27/14 ALB
365.4 -74
<3.74 .
01/24/14 ANO
353.2 R2-93
1455
01/2911.4 SEJ
<5.0
01/29/14 LFJ
EPA200.7
i0
ID#: 129
DATE COLLECTED: 01/16/14
DATE REPORTED : 02/10/14
REVIEWED BY: �...:'
a

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 7, 2014
Permit No. WQ0018525
Pine Knoll Townes 1.92 % Solids
r,nvironment 1 # -*)Jli A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N .% PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % 1
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EmwohmHOM I
Tmasd
PINE KNOLL TOWNES (HYDROTECH)
ATTN: DON O'MARA
HYDROTECS
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting)
7.2
01/07/14 TRB
4500IM-00
Aluminum, (dry wt. basis), mg/kg
3048
01/13/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
01/15/14 MEL
3113B-04
Calcium (dry wt, basis),. mg/kg
48145
01/13/14 LFJ
EPA200.7
Cadmium (dry wt, basis), mg/kg
0.7
01/17/14 MEL
3113B-04
Capper (dry wt. basis), mglkg
698
01/13/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
12
01/13/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
13
01/28/14 MEL
3113B-04
Magnesium (dry wt. basis), mglkg
2169
01/13/14 LFJ
EPA200.7
Mercury (dry WL basis), mg/kg
0.26
01/17/14 ADD
245.1 R3-94
Nickel (dry wt. basis), mg/kg
7
01/13/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
1353
01/13/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/16/14 MEL
3113B'-04
Sodium (dry wt. basis), mg/kg
9046
01/28/14 ADD
3111B-99
Zinc (dry wt. basis), mg/kg
1857.
01/16/14 ADD
3111B.99
Total Solids, %
TKN (dry wt.), mg/kg
1.92
01/09/14 CMC
2540G97
Ammonia Nitrogen (dry wt.),mglkg
41624
1046
01/13/14 ANO
01/14/14 ALB
351.2 R2-93
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
12056
01113/14 ALB
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
<3.96
01/10/14 ANO
353.2 R2=93
Molybdenum (dry wt. basis), mg/kg
<5.0
01/13114 LFJ
EPA200.7
ID#: 558 A
DATE COLLECTED: 01/07/14
DATE REPORTED : 01/31/14
REVIEW= BY: ^

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 6, 2014
Point Emerald Villas ' 0.70 %Solids Permit No. WQ0018525
c a _rt
Parameter
Nitrogen (TKN)
V
% v
5.254
JMg/KgDryWeight
(% x 10,000)
2,433.000
Pounds/Dry Ton
(M /K x 0.002)
4.866
Phos horns
1.482
1,293.000
2.586
Potassium
0.273
2,948.000
5.896
PAN (injected)*
1.600
16,003.710
32.007
PAN (surface)*
Ammonia Nitrogen
1.583
0.034
15,833.210
1,910.000
31.666
3.820
Calcium
4.028
40,275.000
80.550
Calcium Carbonate Eq.
___
---
Magnesium
---
3,480.000
6.960
Sodium
---
9,334.000
18.668
Sulfur
Nitrate N / Nitrite N
--- .
3.910
0.008
Barium
Chloride
___
---
Iron
Aluminum
---
2,709.00
5.418
Arsenic
Cadmium
---
---
2.50
2.00
0.005
0.004
Chromium
---
16.000
---
Cop er
Lead
---
---
1,228.00
45.00
2.456
0.090
Mercury
.0
0.30
0.0 01
01
Molybdenum
---
0.0 10
Nickel
---
16.00
0.032
Selenium
---
5.00
0.010
Zinc
---
1,555.00
3,110
*Determination of Plant Available Nitrogen (PAN): 1',nvironment 1 # 131
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

2 °.m.,...__._—n n n _ _
n
POINT -EMERALD VILLAS (BARNES)
ATTN: STEVE BARNES
P.O. BOX 654
NEWPORT ,NC 28570
PARAMETERS
PH, Units
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %.
TKN (dry wt.), mg/kg
Ammonia_ Nihogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.0
02/10/14 TRB
4500HB-00
2709
02/21/14 LFJ
EPA200.7
<2.5
03/04/14 NIEL
3113B-04
40278
02/21/14 LFJ
EPA200.7
. 2
03/19/14 NIEL
3113B-04
1228
02/21/14 LFJ
EPA200.7
16
02/21/14 LFJ
EPA200.7
45
03/03/14 IVIEL
3113B-04
3480
02/21/14 LFJ
EPA200.7
0.30
02/11/14 ADD
245.1 R3-94
16
02/21/14 LFJ
EPA200.7
2948
02/21/14 LFJ
EPA200.7
< 5.0
03/17/14 ' EL
3113E-04
9334
03/07/14 ADD
3111B-99
1555
02/17/14 ADD
3111E-99
0.70
02/11/14 CTVIC
2540G-97
2433
02/13/14 ANO
351,2 R2-93
1910
02/11/14 ALB
350.1 R2-93
1293
02/13/14 ALB
365.4 -74
< 3.91
02/12/14 ANO
353.2 R2-93
<5.0
02/21/14 LFJ
'EPA200.7
DATE COLLECTED: 02/06/14
DATE REPORTED 03/25/14
REVIEWED BX �t�.i/✓ � %�
j,
l �
f
<<< LABORATORY COPY >>>

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date. Sampled: December 31, 2014
Queens Court 1.03 %Solids Permit No. WQ0018525
eter
;(;K
[FNitrogen)
v
L-01-0
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(M /K x 0.002)
- 6.600
66;000.000
132.000
horus
2.020
20,200.000
40.400
Potassium
0.345
3,450.000
6.900
PAN (injected)*
2.184
21,840.300
43.681
PAN (surface)*
2.178
21,775.800
43.552
Ammonia Nitrogen
0.013
129.000
0.258
Calcium
2.510
25,100.000
50.200
Calcium Carbonate E
Magnesium
---
3,560.000
7.120
Sodium
---
25,200.000
50.400
Sulfur
___
Nitrate N / Nitrite N
---
1,950.000 .
3.900
Barium
Chloride
___
Iron
Aluminum
---
4,930.00
9.860
Arsenic
---
9.22
0.018
Cadmium
___
9.22
0.018
Chromium
---
15.500
---
Co er
---
1,310.00
2.620
Lead
---
54.56
0.109
Mercury
---
1.94
0.004 -
Molybdenum
---
9.22
0.018
Nickel
---
9.22
0.018
Selenium
___
9.22
0.018
Zinc'
---
1,550.00
3.100
*Determination of Plant Available Nitrogen (PAN): Envirochem # 2014-16095
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Fortin Contract Services
Date of Report: Jan 20, 2015
Post Office Box 4188
Customer PO #:
Emerald Isle NC
28594
Customer 1D: 08100061
Attention: Dan Fortin
Report #: 2014-16095
Project 10: Queens Court
Lab 1D Sample ID: Queens Court
Collect DatetTime Matrix 'Sampled by
14-39215 Site: Sludge
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
4930 mg/kg
01/13/2016
Arsenic
EPA200,7
<9,22mg/kg
01/13/2015
Cadmium
ePA2oo•7
<9.22mq/kg
01/13/2016
Calcium
EPA 200.7
25100 mg/kg
01112/2015
'Chromium
EPA200.7
15.5 mg/kg
01/13/2016
Copper
EPA200,7
1310 mg/kg
01/13/2015
Lead
EPA200.i
54.5 mq/kq
01/13/2016
Magnesium
EPA2007
3560mq/kq
01/12/2016
Molybdenum
EPA200.7
<9.22 mg/kg
01/13/2015
Nickel
EPA20o.7
<9,22mg/kg
01/13/2015
Potassium
EPA200.7
3450 mg/kg
01/12/2015
Selenium
EPA200.7
<9,22 mg/kg
01/13/2015
Sodium
EPA200.7
25200 mg/kg
01/12/2015
Zinc
EPA2oo,7
1550 m /k
g g
01/13/2015
Ammonia Nitrogen
EPA350.1
129 m/k
g g
01/02/2016
Total Kjeldahl Nitrogen (TKN)
EPA351.2
66000 mg/kg
01/06/2015
Nitrate+Nitrite-Nitrogen
EPA363.2
1950 m/k
g g
01/05/2015
Total Solids (%)
SM2540B
01/02/2015
PH
SM4500 H B
7.13 units
01/16/2015
Total Phosphorus
sM 4500 P F
20200 mg/kq -
01/06/2015
Mercury
swage 74718
<1.94 mq/kg
01/14/2015
Comment: Results, except PH, reported on a dry
weight basis. reported
pH on an as received basis.
Reviewed by:
Repor #.: 2014-10095
Page 1 of 1
4
• f

ENVIRONMENTAL CHEMISTS, INC
7lnalyfical $ Consul6ng Chemists NCOENR: DWQ CERTIFICATION # 94 NCDNHS: OLS CERnRCATION # 37729
COi.LE�T[ON AND CHAIN OF CUSTODY
CLIE{V'i°: PROJECT NAME' I I
c
6602 Windmill WAY Wilmington, NC 28405
OFFICE-t 910-39M223 FAX Sig-392-4424
info@en ironmentalchemists com
7;7j—lC
rz�poR�r �o:
CONTACT NAME: PO NO:
o Pv�.T To• �HON Ax:
t•lfPll7n• -
Temperature when.Received: Accepted:
iiapiVesed 1Received By;
inmxr�pxl9�c-

M
BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 27, 2014
Permit No. WQ0018525
Sands Villas 2.30 % Solids
7 n _TF i.._■___ r
Parameter
Nitrogen (TKN)
%
0.208
_ ��....... ...... .....0
Mg/Kg Dry Weight
x 10,000)
2,075.000
3Lauii,Fnuult event)
Pounds/Dry Ton
(Mg/Kgx 0.002)
4.150
Phos horus
0.180
1,799.000
3.598
Potassium
0.197
1,974.000
3.948
PAN (injected)*
0.138
1,382.770
2.766
PAN (surface)*
0:085
845.770
1.692
Ammonia Nitrogen
0.107
1,074.000
'2.148
Calcium
4.839
48,386.000
96.772
Calcium Carbonate E
Magnesium
---
2,538.000
5.016
Sodium
---
8,212.000
16.424
Sulfur
Nitrate N / Nitrite N
---
8.470
0.017
Barium
Chloride
Iron
Aluminum
---
4,227.00
8.454
Arsenic
Cadmium
---
---
2.50
2.30
0.005
0.005
Chromium
---
13.000
---
Cop er
Lead
---
---
399.00
9.00
0.798
0,018
Mercury
0.31
0.001
Molybdenum
---
_
5.00
0.010
Nickel
---
11.00
0.022
Selenium
---
5.00
0.010
Zinc
---
867.00
1.734
Environment 1 # 559
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Er�vironinent 1,1111c
SANDS VILLA MMROTECH)
DON 01MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,,NC 28594
Qa W
PARA_IMETERS
Sludge
Sample
Analysis Method
Date Analyst Code
PH (not to be used for reporting)
7.0
01/28/14 TRB
4500HB-00
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mglkg
4227
02/07/14 LFJ
EPA200.7
Calcium (dry wt. basis), mglkg
<2.5
48386
03/04/14 MEL
02/07/14 LFJ
311313-04
Cadmium (dry wt. basis), mg/kg
2.3
03/09/14 A EL
EPA200.7
311313-04
Cropper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
399
13
02/07/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
9
02/07/14 LFJ
EPA200:7
Magnesium (dry wt. basis), mglkg
2538
03/03/14 AIEL
02/07/14 LF J
3113B-04
EPA200.7
Mercury (dry wt. basis), mg/kg.
Nickel (dry wt. basis), mg/kg
0.31
02/11/14 ADD
245.1 R3-94
Potassium (dry wt. basis), mg/kg
11.
1974
02/07/14 LFJ
02/07/14 LFJ
EPA200.7
Selenium. (dry wt. basis), mg/kg
<S,0
CI3/10I1:4 A1EL
EPA200.7
3113B-04
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis),
8212
02l07/14 ADD
31I1B-99
mg/kg
Total Solids,
867
02/07/14 ADD
311.1B-99
TItN (dry wt.), mg/kg2.3
01/30/14 CMC
2540G97
Ammonia Nitrogen (dry wt,),mg/kg
2075
1074
OZ103/14 ANO
02/04l14 ALB
351.2 R2-93
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite. (dry
1799
02/03/14 ALB
350.1 RZ-93
365.4 -74
wt.), ruglkg
Molybdenum (dry wt. basis), mg/kg
8.47
<5.0
02/05/14 ANO
02/07/14
353.2 R2-93
LFJ
EPA200.7
ID#: 559
DATE COLLECTED: 01/27/14
DATE REPORTED : 03/11/1.4
REVIEWED BY:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 9, 2014
Permit No. WQ0018525
Sea Isle Plantation 0.32 % Solids
Parameter
Nitrogen (TKN)
--
% .
1.917
�.....�..0 v... ltlttc
Mg/Kg Dry Weight
(% x 10,000)
40,819.000
JtauLlLduon event)
Pounds/Dry Ton
(M /Kg x 0.002)
81.638
Phos horus
0.675
15,390.000
30.780
Potassium
0.452
12,022.000
24.044
PAN (injected)*
0.581
5,808.148
11.616
PAN (surface)*
0.577
5,769.328
11.539
Ammonia Nitrogen
0.008
160.000
0.320
Calcium
4.831
28,619.000
57.238
Calcium Carbonate E
___
___
---
Magnesium
---
4,598.000
9.196
Sodium
---
44,106.000
88.212
Sulfur
Nitrate N / Nitrite N
---
4.000
0.008
Barium
Chloride
Iron
Aluminum
---
39.49
0.079
Arsenic
---
2.50
0.005
Cadmium
---
0.90
0.002
Chromium
---
10.000
---
Copper
---
204.00
0.408
Lead
---
23.00
0.046
Mercury
---
0.12
0.000
Molybdenum
---
5.00
0.010
Nickel
---
8.00
0.016
Selenium
---
5.00
0.010
Zinc
---
1,039.00
2.078
Environment 14 96A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
,J
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

n n--
GREENVIL L*'E":
1
XD#: 96 A
SEA ISLE PLANTATION
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 418.8 DATE COLLECTED:, 01/09/14
EMERALD ISLE NC 28594 DATE REPORTED : 02/10/14
REVIEWED B-Y
Method.
Cc&
a
100
012r:
02W-MEI.
.7*
3113B-04
-.0 P-9114-
!'EF.4,200.7
.10
.01/29/14 LFJ
EPA200.7
LAad (dry' witht.basis), mg/kg'
02/04114 KEL
3113B-04
(dri Est. basis), m,-Ik,-,
4598
01/29114 LFJ
R PA200.7
Mercury (dry wt, basis), mg/kg
0.12
01/17/14 ADD
245.1 R3-94'
Nick -el (dry wt. basis), mg/kg
8
01/29/14 LFJ
EPA200.7
Potassium (dry wt, basis), mg/kg
12022
01129/14 LFJ
El PA200.7
Selenium (dry Wt. basis), mg/kg
<5-0
02/03114 ME, L
3113B-04
Sodium ( dry wt. basis), mg/kg
44106
01/28/14 ADD
3111E.99
Zinc (drN wt. basis), mg/kg
1039
01/31/14 ADD
311IB-99
Total Solids, %
0.32
01/13/14 IMM
2540G-97
TK-N (dry irt.), mg/kg
40819
01116114 ANO
351.2 R2-93
Nitrogen (dry Wt,),mg/kg
160
01/14/14 ALB
350.1 R2-93
-*tj),".rng/k-g
15390
01116114 ALB
365.4 -74
Nitrate Nitrite (dry WQ, mg/kg
<4.00
01115/14 ANO
353.2 R2.93
Plant Available Nitrogen, mg/kg
12278
01/22/14 SEJ
Molybdenum (dry wt. basis), ing/lig
<5.0
01/29/14 LFJ
EPA7481
IF

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
. Date Sampled: January 8, 2014
Permit No. WQ0018525
Sea Spray 0.60 % Solids
^7 2 -:T7
Parameter
% v
Mg/Kg Dry Weight
Pounds/Dry Ton
(% x 10,000)
(M /K x 0.002)
Nitrogen (TKN)
1.646
16,457.000
32.914
Phosphorus
0.456
4,560.000
9.120
Potassium
0.408
4,081.000
8.162
PAN (injected)*
0.528
5,275.800
10.552
PAN (surface)*
0.517
5,170.300
10.341
Ammonia Nitrogen
0.021
211.000
0.422
Calcium
4.777
47,768.000
95.536
Calcium Carbonate E
--_
_
Magnesium
---
3,548.000
7.096
Sodium
---
20,318.000
40.636
Sulfur
Nitrate N / Nitrite N
---
191.000 `�
0.382
Barium
Chloride
Iron
_
Aluminum
---
3,780.00
7.560
Arsenic
---
2.50
0.005
Cadmium
---
0.80
0.002
Chromium
---
11.000
Co er
---
1,307.00
2.614
Lead
---
11.00
0.022
Mercury
---
0.31
0.001
Mol bdenum
---
5.00
0.010
Nickel
---
10.00
0.020
Selenium
---
5.00
0.010
Zinc
---
1,046.00
2.092
*Determination of Plant Available Nitrogen (PAN): Environment ] # 560
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

mUd
r:u.. bUA AJ65, 114 OAKMONT
O EENVILLE, N.C. 278354085
SSA SPRAY (HYDROTECH)
DON O' bSARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAICETERS
Sludge
Sample
Analysis Method
Date Analyst Code
PH (not to be used for reporting)
7.3
01/09/14 TRB
4500HB-00
Aluminum, (dry wt. basis), nag/kg
3780
01/29/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
01/30/14 NIEL
31138-04
Calcium (dry wt. basis), mg/kg
47768
01/29/14 L' J
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.8
02/06/14 'NIEL
3113B-04
Copper (dry wt. basis), mg/kg
1307
01/29/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
11
01/29/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
11
02/04/14 NIEL
311313-04
Nfagnesium (dry wt. basis), mg/kg
illercury (dry basis),
3548
01/29/14 LFJ'
EPA200.7
wt. mg/kg
Nickel (dry wt. basis), mg/kg
0.31
01/17/14 ADD
245.1 R3-94
Potassium (dry wt. basis), mg/kg
10
4081
01/29/14 LFJ
01/29/14 LFJ
EPA200.7
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/03/14 NIEL
3113B-04 -
Sodium (dry wt. basis), mg/kg
20318
01/28/14 ADD
311113-99
Zinc (dry wt, basis), mg/kg
1046
01/31/14 ADD
3111E-99
Total Solids, %
TKN (dry wt.), mg/kg
0.60
01/13/14 M B
2540G-97
Ammonia Nitrogen (dry wt.),mg/kg
16457
211 '
01/21/14 ANO
351.2 R2-93
Phosphorus, T. (dry wt.), mg/kg
4560
01/14/14 ALB
01/21/14 ALB
3501 R2-93
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
i4iolybdenum (dry basis),
191
01/15/14 ANO
353.2 R2-93
wt. nng/kg
<5.0
01/29/14 LFJ
EPA200.7
FAX [phone]
1D#: 560
DATES COLLECTED: 01/08/14
DATE REPORTED 02/10/14
J F t
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REVIM-IRD BY
A
<<< LABORATORY COPY >>>

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 27, 2014
Permit No. WQ0018525
Southwinds Condominiums 1.60 %, Solids
*Determination of Plant Available Nitrogen (PAN): rnvironment 1 # J62
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Ef�virof�ment El M
SOUTHWINDS (HYDROTECH)
"DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,KC 28594
TMA
PARAMETERS
Sludge
Sample
Analysis Method
Date Analyst Code
PH (not to be used for reporting)
6.9
01/28/14 TRB
45001M.00
Alaminum,. (dry wt. basis), mg/kg
4423
02/07/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
<2.5
41823
03/04/14 MEL
3113B-04
Cadmium (dry wt. basis), mg/kg
1
02/07/14 LFJ
03/09/14 MEL
EPA200.7
Copper (dry wt. basis), mg/kg
11.01
OV07114 LFJ
3113B-04
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis),
11
02/07/14 LFJ
EPA200.7
mg/kg
Magnesium (dry N11. basis), mg/kg
12
2648
0310311.4 MEL
3113&04
Mercury (dry wt. basis), mg/kg
0.43
02/07/14 LFJ
02/11/14 ADD
EPA200.7
245.1 R3-94
Nickel(dry wt. basis), mg/kg
7
02/07/14 LrJ
EPA200.7
Potassium (dry wt, basis), mg/kg
Selenium (dry basis),
1891
02/07/14 LFJ
EPA200.7
wt, mg/kg
Sodium (dry wt. basis), mg/ltg
<5.0
03/10/14 DAL
3113B-04
Zinc (dry wt, basis), mg/kg1109
7098
02/07/14 ADD
02/07114 ADD
3111E-99
3111&99
Total Solids, 5'a
TKN (dry wt.), mg/kg
1.6
01/30/14 CMC
254OG-97
Ammonia Nitrogen (dry wt.),mg/kg
12488
02/03/14 ANO
351.2 112-93
Phosphorus, T. (dry wt.), mg/kg
627
2681
01/30/14 AA'O
02/03/14 ALB
350.1 112-93
365.4 -74
Nitrate -Nitrite (dry wC), mg/kg
Molybdenum (dry basis),
<3.87
01/31/14 ANO
353.2 112-93
wt, mg/kg
<5.0
02/07/14 LFJ
EPA200.7
ID#: 562
DATE COLLECTED: 01/27/14
DATE REPORTED : 03/3-1/14
REVIEWED BY: �--

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 27, 2014
Permit No. WQ0018525
Summer Winds 0.46. % Solids
L 7 _TT /a_ _ •
Parameter
%
uU.., 111I1C
SLUmuzanon event)
Mg/Kg Dry Weight
Pounds/Dry Ton
(% x 10,000)
(Mg,/Kg(Mg,/Kg x 0.002)
Nitrogen (TKN)
2.180
21,802.000
43.604
Phosphorus
0.448
4,477.000
8.954
Potassium
0.678
6,779.000
13.558
PAN_(in'ected)*
0.788
7,878.800
15.758
PAN (surface)*
0.693
6,925.800
13.852
Ammonia Nitrogen
0.191
1,906.000
3.812
Calcium
3.596
35,964.000
71.928
Calcium Carbonate E
Magnesium
---
3,897.000
7.794
Sodium
---
23,536.000
47.072
Sulfur
Nitrate N / Nitrite N
---
4.000
0.008
Barium
Chloride
Iron •
__
Aluminum
---
3,665.00
7.330
Arsenic
---
2.50
0.005
Cadmium
---
1.00
0.002
Chromium
---
8.000
---
Co er
---
482.00
0.964
Lead
---
10.00
0.020
Mercury .
---
0.20
0.000
Molybdenum
---
5.0
0.010
Nickel
---
11'.00
0.022
Selenium
---
5:00
0.010
Zinc
---
2,187.00
4.374
Lnvironment 1 # 119A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application.:
(Mineralization Rate)(TI<N-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

r=j r,
SUMMERWIND HOA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
F.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH' (not to be. used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mg/kg
Cadmium,(dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
11429neshxm (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry nit, basis),. mg/kg
Total solids, %
TKN (dry wi.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge
Analysis
Method
Sample
Date Analyst Code
6.7
01 /28/14 TRB
450OUB-00
3665
02/07/14 LFJ
EPA200.7
<2.5
03/04/14 MEL
3113B-04
35964
02/07/14 LFJ
EPA200.7
1
03/09/14 MEL
3113B-04
482
02/07/14 LFJ
EPA200.7
8
02/07/14 LFJ
EPA200.7
10
03/03/14 MEL
3113B-04
3897
02/07/14 LFJ
EPA200.7
0.20
02/11/14 ADD
245.1 R3-94
11.
02/07/14 LFJ
EPA200.7
6779
02/07/14 LFJ
EPA200.7
<5.0
03/10114 MEL
3113E-04
23536
02/07/14 ADD
3I11B-99
2187
02/07/14 ADD
311IR-99
0.46
01/30/14 CMC
2540G-97
21802
02/06/14 AN
351.2 R2-93
1906
02/04/14 ALB
350.1 R2-93
4477
02/06714 ALB
365.4 -74
<4.00
02/05/14 ANO
353.2 R2-93
<5.0
02/07/14 LFJ
EPA200.7
ID#: 119 A
DATE COLLECTED: 01/27/14
DATE REPORTED : 03/11/14
M7IEWED BY:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Was Treatment Plant
Date Sampled: April 24, 2014
Permit No. WQ0018525
Whaler Inn 0.58 % Solids
^7 A _TT
Pdrameter
%
Mg/Kg Dry Weight
x MIMI
Pounds/Dry Ton
x 0.002
Nitrogen (TKN)
1.601
37,258.000
74.516
Phos horns
0.397
11,425.000
22.850
Potassium
0.399
3,402.000
6.804
PAN (injected)*
0.516
5,164.200
10.328
PAN (surface)*
0.502
5,019.200
10.038
Ammonia Nitrogen
0.029
272.000
0.544
Calcium
5.591
44,302.000
88.604
Calcium Carbonate E
___
---
Magnesium
---
3,366.000
6.732
Sodium
---
31,852.000
63.704
Sulfur
--_
___
Nitrate N / Nitrite N
---
157.000
0.314
Barium
___
_
---
Chloride
-__
---
Iron
---
__
Aluminum
---
3,530.00
7.060
Arsenic
---
2.50
0.005
Cadmium
---
1.0.0
0.002
Chromium
---
14:000
---
Co er
---
2,368.00
4.736
Lead
---
18.00
0.036
Mercu
---
0.56
0.001
Molybdenum
---
5.00
0.010
Nickel
---
11.00
0.022
Selenium
---
5.00
0.010
Zinc
---
1,934.00
3.868
Environment I #E 70A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

GREENVILLE;
THE WHALER INN
0/0 MR. STANLEY BUCK
1745 BELGRADE-SWANSB0R0 RD.
MAYSVILLE ,NC 28555
PARAV�IERS
Sludge
Sample
Analysis Method
Date Analyst Code
PH (not to be used for reporting)
Aluminum, (dry basis),
7.4
• 04/24/14 TRB
4500HB-00
wt. mg/kg
Arsenic (dry Wt. basis), mg/kg
3530
05/06/14 LFJ
EPA200.7
Calcium (dry wt. basis), mg/kg,
<2.5
44302
05/07/14 IN EL
05/06/14 LFJ
3113B-04
Cadmium (dry wt. basis), mg/kg
Copper (dry basis),
1
05/15/14 VIEL
EPA200.7
3113E-04
wt. mg/kg
Chromium, T.(dry wt. basis),Tng/kg
2368
14
05/06/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
05/06/14 LFJ
'
EPA200.7
Magnesium (dry wt. basis), mg/kg
18
3366
05/06/14 11FL
05/06/14 LFJ
3113B-04
illercur Y (dry wt. basis), Ing/kg
Nickel (dry wt. basis),
0.56
05/08/14 ANITM
EPA200.7
245.1 R3-94
mg/kg
Potassium (dry wt, basis), mg/kg
11
05/06/14 LFJ'*
EPA200.7
Selenium (dry wt. basis), mg/kg
3402
05/06/14 LFJ
EPA200.7
Sodium (dry wt, basis), mg/kg
<5.0
31852
05/14/14 1vlFL
3113B-04
Zinc (dry wt. basis), mg/kg
05/06/14 NffM
3111B-99
Total Solids, %
1934
05/07/14 iViTIM'
3111B-99
WN (dry wt.), mg/kg
0.53
04/25/14 CIVIC
254OG-97
Ammonia Nitrogen (dry wt.),mg/kg
37258
272
05/01/14 ANO
351.2 R2-93
Phosphorus, T. (dry wt.), ng/l g
11425
04/29/14 ALB
05/01/14 ALB
350,1 R2-93
Nitrate -Nitrite (dry wt.), nng/kg
Plant Available Nitrogen,
157
04/30/14 ANO
365.4 -74
353.2 R2-93
mg/kg
Molybdenum (dry wt. basis), mg/kg
15087
05/02/14 SFJ
<5.0
05/06/14 LFJ
EPA200.7
FAX [phone]
ID#: 10 A
DATE COLLECTED: 04/24/14
DATE REPORTED : 05/19/14
r-�
�� `I Cam' � f 3( � •
REVIEWED B �{
<<< LABORATORY COPY >>>

l
PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING
f

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number- WQ0018525
WWTP Name: SEE ATTACHED LIST NPDES Number: SEE ATTACHED
Monitoring Period: From 1/1/2014 To 12/31/2014
—
atholren Reduction (15A WrAr n,7T I In4l IDI-- :.__,e__._ ,____.
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) [3 Alt. C P
{ riorTes `
• A1t.D (No i'rivr Test) ® Process to Further Reduce Puthugeags ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Rtvlt<tce 131atllogens'a
Compost © Heat Drying ❑ Heat Tivatinent ❑ Thernu.)philie ❑
Beta Ray ❑ Galnnla Ra I3 Ynsteurizution ❑
Class B: jAlt. (1) l;ecal Density❑ Alt. (2) Process to 5i};ttiiit;autl<y Reduce Piathoplis
If applicable to alteritotive perfortued (Class 11; ottls�) ittdlcltte �'Procrs5 t;o Slgttlficamtl}• Reduce IPutltvgent":
Air Dtytug
Lirne '❑ ❑ Cnnl 1L15ti11 A431k�bic I�igesiiotl ❑
tDigestion
Anaerobic [3zation
`:.'.;.<.;:_.::;:�':::.�>::���:�;.:�..:.:::.:. •:�;. :;;..::.:-;.:;:.::: ;:::::�;:.:.:.:.• ::::.
If Applicable to
alternative lerformed (Class A or Class B) complete the
following monitorin2 data:
Parameter
-Allowable Level
Pathogen
g
Density
ty
Number o
FExccc-requency
Sample
na ytica
Minimut
Goo. Mean
Maximus
Units
in Sludge
I nces
of Analysis
Type
fech-
2 x 10 to the MPN
6th power
per gram of
Fecal Colifornl
total solids CFII
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
eoliform
weight
Vector Attractinn
Roilurtinn !1 C A
lvr A F 7kTr
, i N .
m
-- - - ---- --- ^ _--� • _ .vwvv ...ua�•nw "AWK 1RULIVC pCrlurmeu:
Alt.1 (VS reduction) Cl Alt.2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 ($pe'c.,O�,uptake); ❑
Alt. 5 (14-Day Aerobic) [3Alt. 6 (Alk. Stabilization 0 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) �
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) [1 No vector attraction reduction alternatives were perforined ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you, Have not met one ol• both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties foi• false certification including tine and imprisonment."
Steven M. Barnes, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
/s
Signature of Pleparei * Date Signatute.of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

WWTP Name
NPDES #
Atlantic Station
WQ0004059
Beacons Reach
WonnigA7R
Cape Royal Dolphin
WQ0005173
CC Sass
VI-15-11
Cedar Point
VI-16-13
Colony By Sea
VI-14-13
Eight 1/2 Marina
VI-05-13
Genesis Condos
WQ0006863
Hampton Suites
VI-02-10
Mariners Pf I
VI-13-12
McGinnis Point
VI-01-12
NC Aquarium
WQ0019331
Ocean Club
WQ0018420
Oceans Condos
VI-08-11
Ocean Terrace
VI-07-09
Pebble Beach
WQ0002128
Peppertree
Pine Knoll Townes
Point Emerald Villas
Queens Court
WQ0011313
VI-18-13
WQ0000224
WQ0003437
Sands Villa
Sea Isle Plantation
WQ0000165
WQ0013027
Sea Spray
VI-03-92
Southwinds Condos.
Summer Winds
WQ0018992
VI-12-11
Whaler Inn
VI-20-10

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: �4 P.O.#
or Gallons
Uised:
Material Used For Stabilization: Lime
_Initial•
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC:
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: P.O.#
Batch Size (gallons): ���® Lbs. or Gallons Used: ®®
-
Material Used For Stabilization:
Lime
Date Initial pH >12 pH 2 Hour pH
Corr. Corrected Corr.
24 Dour pH
o erato
p
Corrected
pH Temp C Time. H Temp C Corr. Corrected
Factor+ H p ? Time pH . Temp C Time H
p - Factor+ pH p
Tem p
Corr: Corrected
C
Time
Initials
Factor pH
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC..
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: �' �,P.O.#
gy .�
Batch Size (gallons): t,` Lbs. or Gallons Used:
— • L- - Material Used For Stabilizatinne I imp
>12 PH
2
Hour
PH
24,Hour
PH
'+ O '� NV M M Cq Cq N N N r0 ram- � W CO
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N.
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tl!
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:
BARNES ENVIRONMENTAL WASTE AND HAULING,
INC;
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name:
,cS.S� P.O.#
Batch Size (gallons): 1p D Lbs. or Gallons Used: r (�
Material
Used For Stabilization:
Lime
Date
Initial pH
Corr. Corrected
Temp C Time
>12 pH
orr. .Corrected
O erato
p
2 Hour pH
24 Hour pH
pH
Factor+
pH
pH
Temp C
+
pH
Time
pH
Temp C
Corr.
Corrected
Time
p H
Temp
p
c Corr.
corrected
Time
Initials
[Factor
Factor+
pH
Factor
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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Batch Size (gallons): Lbs. or Gallons Used: 306
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER B10SOL1DS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: OC prxn -T-,Qd'rcwc P P:O.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ,� le- P.O.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: _ �r P.O.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: JbAq .c)�'Irl5 P.O.#
Batch Size (gallons): 7n 6r) Lbs. or Gallons Used:-- Material Used For -Stabilization: Lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ���-�' ���� P.O.#
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2014 APPLICATION SUMMARY

I
BARNES ENVIRONMENTAL WASTE
Permit # WQ 0018525
RESIDUALS APPLICATION
2014 APPLICATION SUMMARY
Will Turner
Site WT
2014
1
6.20
21,000
0.56
2.51
0.00
2014
2
5.00
91,000
4.22
13.06
0.00
2014
3
8.00
119,400
4.33
7.73
1.15
2014
5
2.60
63,000
2.62
6.64
2.49
2014
6
2.90
42,000
2.07
6.67
1.58
11

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes Environmental Waste&Haulio¢ Permit#:W00018525 Ann ual'bryTons Applied: 0.56
Owner. Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 2.2
Site #: WT Field #: I Acres Utilized: 6.26 Acres Permitted: 6.20
Application Method*: S Volatilization Rate'**: OS Mineralization Rate: 30 % Predominant Soil Series: GoA
:Gals:: -E
,11'hi9, ./:
' I'/n�
DT•/:
� Itesidn9� :
�Sit'e-
:1(RetBiS •(T�3%
= P10tSehtS
�fI(►S%
k�
7 kh
hid
N2N3
t201
7,000
1.129
0.88
0.04
CC Sass
G/D
0.001
0.001
0.027
0.001
0.000
0.001
0.001
0.001
0.033
1.36
1.50
R
4.52
0.02
0.00
7,000
1,129
0.63
0.03
re
G/D
0.000
0.003
0.036
0.001
0.000
0.000
0.001
0.000
0.034
0.81
1.20
Rye
2.69
0.01
0.00
3.500
565
0.53
0.01
Ofn Club
G/D
0.000
0.000
0.014
'0.000
0.000
0.000
0.000
0.000
0.043
0.26
0.20
Rye
0.85
0.01
0.00
20I4
3.500
565
0.32
0.01
Spa Iste Planation
G/D
0.000
0.000
0.003
0.000
0.000
0.000
0.000
0.000
0.016
0.09
0.23
Rye
0.6I
0.00
0.00
Total
21,000
Annual lbstacre 0.001 0.004 0.079 0.003 0.000 0.001 0.002 0.001 0.125 2.51 1 0.00 3.13 ",
Can cut Cumalative HWacre 0.04 0.03 12 58 0.21 0.00 0.07 010 0.06 14.42 136 50 Permit PAN Limt lst/2nd Crop
Prior YearsCumulativelbs/ 0.04 0.02 l250 0.21 0.00 0.07 010 0.06 14.29
Permitt C.P.LJL- 36 _ 34 I338 267 IS NIA 374 89 2498
"I certify under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." `
Lime App.
Date
Lbs/A
5/12
1.000
X yy�CX t !�, *Application Method: S - Surface, IN - Injection. INC - Incorporation
(Signature of Land Applier) Dat **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***.C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (V2002) Mod.
SWE, Inc.

ANNUAL LAND APPLICATION FIELD SUMMARY.FORM
Facility Name: Barmes Environmental waste & RaulinQ Permit tlti WOOOIS525 Annual Dry Tons Applied: 4.22
Owner. Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 5.2
Site,#: WT Field #: 2 Acres Utilized: 5.00 Acres Permitted: 5.00
Application Method*: S Volatilzation Rate**: 0.5 Mineralization Rate: 30 %
Predominant Soil Series: GoA
: 733te::
Aadk: '
Cr.Os l
: -Aiie :
: T$ :
;DIJ
:A,66:
: kfiaatrel::,
: $burc2 : -
:'kie
Conti:
1VI4t2fS ittis/aC :
• :
Flutrients Tlbo/ac
is :
:mod:
IG6= :
: 1'b: =
a
Mo :
: iYt :
Se:
• 1'h• :
PAPI I
.033
. •P• :
Crd 9•
Cro 2
:11N :
B :
NZ `l3
2014
7.000
1,400
0.60
0.04
AtlaaticSfation
G/D
0.000
0.000
0.049
0.001
0.000
0.000
0.001
0.000
0.092
0.16
0.32
Coastal
2.03
0.01
0.00
2014
14.000
2,800
I.70
0.20
Bwc""sReach
G/D
0.001
0.001
0.809
' 0.007
0.000
0.002
0.004
0.002
0.438
0.36
1.49
Coastal
0.99
0.31
0.00
2014
10.500
2,100
0.88
0.08
cc �s _
G/D
0.002
0.002
0.050
0:002
0.000
0.002
0.002
0.002
0.061
2.53
2.79'
Coastal
8.40
0.04
0.00 "
2014
3,500
700
0.55
0.02
Pe Ya
G/D
0.001
0.001
0.035
0.002
0.000
0.001
0.001
0.001
0,098
0.88
0,69
Coastal
2.75
0.26
0.00
2014
3.500
700
0.54
0.02
Cedar Point
G/D
0.001
0.001
0.011
0.001
0.000
0.001
0.001
0.001
0.022
0.71
0.52
Coastal
2.05
0.00
0.10
2014
3,500
700
1.37
0.04
HamPtonSuites
G/D
0.000
0.000
0.121
0,000
0.000
0.000
0.001
0.000
0.102
1,12
1.19
Coastal
3.64
0.03
0.02
2014
3,500
700
2.19 ,
0.06
McC"""'s Point
G/D
0.000
0.000
0.095
0,000
0.000
0.001
0.001
0.001
0.153
1.79
2.22
Coastal
5.83
0.16
OAO
2014
7.000
1400
0.53
0.03
OteanClub
G/D
10.000
0.000
0.034
0.000
0.000
0.000
0.000
1 0.000
0.106
0.64
0.50'1
Coastal
1 2.10
0.03
0.00
2014
3,500
700
1.22
0.04
0-T-c
G/D
0.000
0.000
0.124
0.003
1 0.0W
0.000.
0.001
0.000
0.162
1.08
1.14
Coastal
3.60
0.03
0.00
2014
10.500
2,100
1.70
0.15
Pebble Beach
G/D
0.001
0.000
0.725
0.008
0.000
0.001
0:003
0.001
0,502
0.73
2.75
Coastal
9.26
0.15
0.00
2014
14,000
2,800
0.68
0.09
PepPeuee
G/D
0.000
0.000
0.040
0.001
0.000
0.001
0.001
0.001
0.127
0.18
1.28
Coastal
0.57
0.04
0.00
2014
3,500
700
1.92
0.06
PtneKno
TOWSi
G/1)
0.000
0.000
0.078
0.001
0.0W
0,001
0.001
0.001
0.208
1.42
1.35
Coastal
4.67
0.12
0.00
2014
3.500
700
1.03
0.03
Queens Court
G/D
0.001
0.001
0.079_
0.003
0.000
0.001
0.001
0.601
0.093
1.31
1.21
Coastal
3.97
0.01
Oa2
2014
3,500
700
0.58
0.02
whal" in"
G/D
0.000
0.000
0.080
0.001
0.000
0.000
0.000
0.000
0.065
0.17
0.39
Coastal
1.26
0.01
0.01
Total
91,000
Annual lbs/acre 0.007 0.005 2330 0.031 0.001 0.010 0.016 0.010 1230 13.06 0.00 17:83
Current Cumulative lbshcm 1.80 0.06 65.8L24 0.45 0.22 0.82 0.56 74.84 299 50 Permit PAN Limt ist/2nd Crop
PriorYear: Cumulative ills! 1.80 0.06 63.50.80 0.55 72 6I 299PermittC.P.LR.*** 36' 34 1338 15 N/A 374 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information -submitted. I am aware that there are
significant penalties for submitting false information, Including the possibility of fares and imprisonment for knowing violations."
Lime
A
Date
Lbs/Ac
x ,Q o2 Zo 5
(Signature of Land Applier) Dat
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5. Injection/Incorporation - 1.0
***C.P.L.R: Cumulative Pollutant Loading Rate
S8'ME, Inc.
DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: $ernes Environmental wane & xaulinc Permit #: WOOOISS25 Annual Dry Tons Applied: 4.33
Owner: Will Turner Operator. Steve Dames Cation, Exchange Capacity ( non 503): 5.0
Site # WT Field #: 3 Acres Utilized: 8.00 Acres Permitted: 8.00
Application Method*: S Volatiliz2tion Rate**: OS Mineralization Rate: 30 % Predominant Soil :Series: GoA
GelaG
! :
x /.
: • Residu4l• :
a
et�Is ilbstaC} : ' • '
rie*fts:Flbs/ac)
• . •
13ANJ
PdNz
: P • -
1 J+rr
' 2
: TX5
:NI KS
NIT K`-3.
2014
11.900
1ASS
0.60
0.04
AtlaonoStaaoa
G/D
0,000
0.0001
0.052
10.001
0.000
0.000
1 0.001
0.000
0.099
0.07
0.10
0.34
Coastal
Rye
2.16
0.01
0.00
2014
3,500
438
1.70
0.03
Beacons Reach
GAD
0.000
0.0001
0.126
10.001
0.000
0.000
10.001
0.000
0.068
0.06
0.23
coastal
0.I5
0.05
0.00
2014
28.000
3.500
0.88
0.13
CC Sass
GAD
0.003
0-0031
0.083,1
0.003
0.001
0.003
0.003
0.003
0.102
3.16
1.05
4.65
coastal
Rye
14.00
0.07
0.00
7-500
313
0.54
0.D1
�v y e
Col2014
GAD
0.000
0.000
0.004
1 0.ODO
0.000
0.000
O.00D
0,000
0.024
1 0.02
1
0.12
Ceastai
0.09
0.00
0.00
2DI4
7.000
875
0.43
0.02
Pight11ZMa"-
G/D
10.000
0.000
0.052
0.001
0.0W
0.000
0.000
0.000
0,059
1 0.23
0.24
Coastat
1.21
0.00
0.00
2014
3.500
438
1.07
0.02
las0/1)
0.000
0.000
0.022
0.000
0.000
0.000
0.000
0.000
0.037
0.09
0.15
Coastal
0.25
0.08
0.00
2014
3,500
438
0.65
0.01
INadn-Point
G/D
10.000
0.000
0.017
0.000
0.000
0.000
0.000
0.000
0.114
0.24
0.32
coastal
0.81
0.01
0.00
2014
3.500
438
0.63
Q.OI
NC /+gvanuma,
G/D
0.000
0.001
0.014
0.001
0.000
0,000
0.000
0.000
0.013
0.31
OA6
coastal
1.04.
0.00
0.00
2014
-10.500
1.313
0.53
0.03
Ofnaub
G/D
0.OW
0.WO
0,031
0.000
0.000
0.000
0.000
0.000
0.099
0.60
0.47
coastat,
I.97
0,03
0.00
2014
3.500
438
0.68
0.01
Pepperuee
G/D
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.020
0.03
0.20
Coastal
0.09
0.01
O.DO
2014
7.000
975
1.03
0,04 .
Q's Cent
GM
0.001
0.001
0.098
0.004
0.OW
0.001
0.001
0.001
0.117
1.64
1.52
Coastal
4.96
0.01
0.15
2014
7,000
875
Z30
0.08
Sands Villas
G/D
0.000
0.000
0.067
0.002
0,OW
0.001
0.002
0.001
0.146
0.14
0.30
Coastal
035
0.13
0.00
2014
10,500
1.313
0,60
0.03
SnSfy
G/D
0.000
0.000
D.086
0.001
0.000
0.000
0.001
0.000
0.069
0.34
0.30
Coastal
1.08
0.Oi
0.01
2D14
7.000
875
1.6D
0.06
vmt a
G/D
0.000
0.000
0.129
1 0.001
0.000
0.001
0.001
0.0D1
0.129
0.45
0.31
Coastal
1.46
0.07
0.00
2014
10.500
1.313
0.46
0.03
summer words
GAD
0.000
0.000
0.024
10.001
0.000
0.000
0.001
10.000
D,110
035
0.23
coastal
1
1.10
0.10
1 0.00
Total
119.400
Annual lbslacre 0.006 0.006 0.812 0.016 0.010.007 0.011 0.007 1.204 7.73 1.15 9.85 r,
2" 50 Permit PAN Lunt lstand Crop
Canvmt Cusaulative lbs/acse 0.16 0.38 53.31 0.79 0.01 0.19 0.52 0.16 1249"S
Prior Yeas Cumulative lbsdacre 0.16 038 52.50 0.73 0.01�0.18 0.51 0.15
Permitt C P.LR ••• 36 34 1338 267 15 N/A 374 89
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations"
Lime A -
Date
Lbs/Ac
X a �s
Aw-
7(igtature of Land Applier) Drate
'Application Method: S - Surface, IN - Injection, INC - Incorporation
"VolatilizationRate: Surface - O.S.InjectiontIncorporation- 1.0
'"'C.P.L.R.: Cumulative Pollutant Loading Rate
S&ME, Inc.
DENR FORM FSF (7/2002) Mod,

ANNUAL LAND APPLICATION FIELD SUBUKARY FORM
Facility Name: tgarnes gwiromwntai waste & Planting Permit #: W00018525 Annual Dry Tons Applied: 0.00
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 10.4
Site #: WT Field #: 4 Acres utilized: 2030 Acres Permitted: 20.30
Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 ' %
Predominant Soil Series: GoA
Dale::::
Gi►ii: =
:C,,al3J
: Aire ; :
lo:
: `I� :
ix1 �:
:Acre:
1€es�J�la1=
:Spores : ' '
: ?Sitp
�Gonid.::
Metals= (11lsfaE}
:
i�UtttiBn
: i- -
i#s :::.Cd:::
Cu:::
ga :
: =kIA
::141e::
•: Nj = :
: Se:::
2;n :
i' P*N:1
)E'AN2
:: =P= ::
-
t rd k
Gro 'i
: �Klst
::N2-N3
Pines
Pines
Total
0
,..
Annual Ibs/acre 0.400 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.00 0.04 0.00 >,Q `. " r,: ,,i�«i,.a
Current Cumulative Ibs/acre 0.000 0.000 0.060 0.001 0.000 0.000 0.000 0.001 0.073 60 50 jPermit PA,-4 Lit Ist/2nd Crop
Prior Years Cumulative Ibs/acre 0.000 0.000 0.060 0.001 0.000 0.000 0.000 0.001 0.073
Permitt C.P.LIL*** 36 34 1338 267 15 N/A 374 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
' Lime A
Datelib,/A-,
Y. J&=2= ! r L /60,t o, : - &1a0115 *Application Method: S - Surface, IN - Injection INC - Incorporation
(Signature of land Applier) Date **Volatilization Rate: Surface - 0.5. Injection/Incorporation -1.0
***C.P.LR: Cumulative Pollutant Loading Rate
DENR FORM FSF (712002) Mod.
S&ME, Inc.

ANNUAL LAND APPLICATION FIELD SUAMARY FORM
Facility Name: Rases Environmental Waste &_Haulms Permit #: W00018525 Annual Dry Tons Applied: 2.62
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): ' 9.9
Site #: WT Field #: 5 Acres Utilized: 2.60 Acres Permitted: 2.60
Application Method*: S Volatilization Rate**: OS Mineralization Rate: 30 %
Predominant Soil Series: GoA
Date::':1GhHz
=:Ga19J
:Ad6:'::�
Jo:::111f�:
=
:Air
RlsiiiUsl=::Stitt
:,%A0ce:-,
.Gond::M:'•:Cd:::rii::::Pb::
=iV%ta13
(lbs/ae1:'
:
Ntt'tritntv:7tisla
::Zn::
PAXI
l'I GZ::'::I'::
Tco
7
Cr' '2::TK-JX
:_N-W:N2=--
2014
7.000
2.692
0.60
0.07
Atlantic Station
G/D
0.000
0.000
0-094
0.002-
0.000
0.00I
0.001
0.001 1
0.177
0.31
0.62
Coastal
3.90
0.02
0.00
2014
7,000
2,692
1.70
0.19
Beacons Reach
G/D
0.001
0,000
0.778'
0.007
0.000
0.002
0.003
0.002
0.421
0.35
1.43
Coastal
0.95
0.30
0.00
2014
7.000
2.692
0.88
0.10.
CC Sass
G/D
0.002
0.002
0.064
0.002
0.000
0.002
0.002
0.002
0.079
3.25
3.58
Coastal
10.71
0.06
0.00
2014
3,500
1,346
0.68
0.04
Peppettree
G/D
0.000
0.000
0.019
0.000
0.000
0.000
0.001
0.000
0.061
0.09
0.61 _
Coastal
0.27
0.02
0.00
2014
7,000
7,692
0.70
0.08
omt htneraid
villas
G/D
0.000
0.000
0.193
0.007
0.000
1 0.001
0.003
0.001
`0.244
2.49
0.20
Rye
0.38
0.30
0.00
2014-1
10.500
4.038
2.30
0.39
Sands villas
G/D
0.002
0.002
0.309
0.007
0.000
0.004
0.009
10.004
0.672
0.66
1.39
Coastal
1.61
0.83
0.01
2014
3,500
1.346
0.32
0.02
ea Isle
1 Plantation
G/D
10.000
0.000
0.007
0.001
0.000
0.000
0.000
0.000
0.037
0.21
0.55
Coastal
1
1.47
0.01
0.00
2014
17.500
6MI
0.46
0.13
Sammerwinds
G/D
0.001
0.000
0-124
0.003
0.000
0.001
0.003
0.001
0.565
1.79
1.16
Coastal
5:63
0.49
0.00
Total
63,000
Annual ibs/acre 0.007 0.005 1.590 0.029 0.001 0.011 0.022 0.011 2.256 6.64 2.49 9.55 •. ". MINOR ' l . "
Current Cumulative lbs/acre 0.007 0.005 1590 0.029 0.001 0.011 0.02210.01112.2561 299 50 JPermit PAIN Limt 1st/2nd Crop
Prior Years Cumulative Ibs/acre 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000
Permitt C-P.L-R.*** 36 34 1338 267 15 N/A 374 1 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Lime App.
DateILbs/Ac.
X 7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) D e **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1-0
***C.P.L,R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (712002) Mod.
S&ME, Inc.

ANNUAL LAND APPLICATION HELD SUMMARY FORM
Facility Name: Barnes Environmental Waste & ilaul"ms Permit #: W00018525 Annual Dry Tons Applied: 2.07
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity (.non 503): 9.6
Site #: WT Field #: 6 Acres Utilized: 2.90 Acres Permitted: 2.90
Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 %
Predominant Soil Series: GoA.
flake =':
a1s :
:Aire:::;
' °lo:
=
1}'F /:
ACle
pEesiYfUal '
:Smm'•ce-:.•
:bite=
Goilli
iVtet�Is ([b§/ae}
::: : = " ' ' ' '
.:
1�Utrient4
: .
::tlis;'
:Gd•:
:Ci1 :
: 1'1►:
::M9:
: �1 '
: Se;
Ott:
5.'MM
i2V2
: :-P :'::�
1
Cre '2
:TKl�T
:Nkt3
NZ-N3
2014
7.000
2.414
1.70
0.17
Beacons Reach
G/D
0.001
0.000
0.697
0.006
0.000
0.002
0.003
0.002
0.377
0.31
1.28
Coastal
0.85
2014
3,500
I,207
0.88
0.04
CC sass
G/D
0.001
0.001
0.029
0.001
0.000
0.001
0.001
0.001
0.035
1.45
L60
Rye
4.83
0.00
2014
3.500
1,207
0.54
0.03
Cedar Point
G/D
0.001
0.001
0.020
0.001
0.000
0.001
0.001
0.061
0.038
1.22
0.89
Coastal
3.53
0.16
2014
3,500
1,207
1.37
0.07
Hampton suites
G/D
0.000
0.000
0.209
0.001
0.000
0.001
0.001
0.001
0.176
1.93
2.05
Coastal
6.2$
d270.00
0.03
2014
3,500
1,207
0.63
0.03
quanum at
Pine Knoll Shores
G/D
0.000
0.003
0.038
0.001
0.000
0.000
0.001
0.000
0.036
0.86
1.28
Coastal
2.8-7
0.00
2014
7.000
2.414
0.53
0.05
ocean Club
G/D
0.000
0.000
0.058
0.001
0.000
0.001
0.001
0.001
0.182
1.10
0.87
Coastal
3.62
0.00
2014
3,500
1.207
1.22
0.06
earn
1 Condominium
G/D
J0.000
0.000
0.043
0.002
0.000
0.001
0.001
0.001
0.116
0.13
0.55
R
0.51
0.37
1.0.00
2014
10.500
3.621
1.70
0.26
Pebble Beach
G/D
0.001
0.001
1.250
0.014
0.000
0.003
0.005
0.003
0.865
I.25
4.75
Coastal
15.97
0.26
0.00
Total
42,000
Annual lbs/acre 0.005 0.006 2344 0.027 0.001 0.008 0.013 0.008 1.826 6.67 1.58 13.27 •'� ' }}
Current Cumulative lbs/acre 0.005 0.006 2.404 0.028, 0.001 0.008 0.013 0.009 1.899 299 50 Permit PAN Limt Ist/2nd-Cro
Prior Years Cumulative lbs/acre 0.000 0.000 0.060 0.001 0.000 0.000 0.000 0.001 0.073
Permitt C.P.L.R.*x* 1 36 34 1338 267 15 NIA 374 89 2498
"1 certify, under penalty of law, that this document was prepazed under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment forknowing violations."
Lime A
Date
Lbs/A
x A?.a5
(Signature of Land Applie) Dat
*Application Method: S - Surface, IN - Injection, INC -Incorporation
**Volatilization Rate: Surface:- 0.5, Injection/Incorporation -1.0
* * *C.P.L.R: Cumulative Pollutant Loading Rate
S&ME, Inc.
DENR FORM FSF (7/2002) Mod_

FIELD APPLICATION SUMMARIES
pl,

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Soybean
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Soybean
Rye
BARNES ENVIRONMENTAL WASTE
2014 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-01 6.2 ACRES TOTAL GALLONS 21.000
---------------
�0
111
0�00�0��000
111
00000000000000�
�0
111
�00000�00��
111
Ocean
Terrace—]L_.�
�ach[j��J[
Pine
Knoll
---------------
11
0�0��00�
11
00000
00000�00�00��00
---------------
11
000�0�0�
11
0�0�0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2014 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-02 5.0 ACRES
TOTAL GALLONS 91,000
.
..
Sea
..
S
---------------
---------------
---------------
---------------
---------------
---------------
111
111
1 11
11
11
0
11
0
0
0
0
0
0
11
0
7,000
14,000
10,500
3,500
3,500
0
3,500
0
0
0
0
0
0
3,500
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Ocean
Ocean
Ocean
Pebble
Pe er[ree
Pine
Point
ueens
Sands
Sea Island
Sea
Sound of
Sout hwin ds
Summer
1!7�
Club
Condos
Terrace
Beach
Resort
Knoll
Emerald
Court
Villa
Plantation
Spray
The Sea
Condos
Winds
3,500 3,500 10,500 3,500
3,500
3,500 3,500
3,500
3,500 3,500 3,500
7,000 0 3,500 10,500 14,000 3,500 0 3,500 0 0 0 0 0 0 3,500
7,000
0
3,500
10,500
14,000
3,500
0
3,500
0
0
0
0
0
0
3,500
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2014 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-03 8.0 ACRES
TOTAL GALLONS 119,400
Alantic
Station
Beacons
each
CC Sass
Cape Royal
Dolphin
Cedar
Point
Colon_ B
The Sea y
Hampton
Suites
Dunesca a
Ei ht 112
Marina
Emerald
Plantation
Island
Beach
Genessis
Condos
Mariner's
Point
McGinnis
Point
NC
Aquarium
7,000
"
3,500
3,500
1,400
14,000
3,500
3,500
2,500
7,000
3,500
7,000
7,000
11,900
3,500
28,000
0
0
2,500
0
0
7,000
0
0
3,500_
3,500
0
3;500
4,900
3,500
21,000
0
0
2,500
0
0
j 7,000
0
j 0
j 3,500
j 3,500
0
3,500
7,000
0
7,000
0
0
0
0
1 0
1 0
1 0
1 0
101
0
1 0
0
Ocean
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Peppertree
Resort
Pine
Knoll
Point
Emerald
Queens
Court 11
Sands
Villa
Sea Island
Plantation
Sea
Spray
Sound of
The Sea
Southwmds
Condos
Summer
Winds
Whaler Inn
3,500
`
3,500
7,000
7,000
7,000
10,500
3,500
3,500
10,500
10,500
0
0
0
3,500
0
0
7,000
7,000
0
10,500
0
7,000
10,500
0
10,_500
0
0
0
3,500
1 0
0
7,000
7,000
0
1 10,500
I 0
I 7,000
I 10,500
I 0
0
0
0
0
0
1 0
1 0
0
0
0
0
0
0
0
0

_._L]
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2014 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-05 2.6 ACRES TOTAL GALLONS 63,000
---------------
---------------
---------------
---------------
---------------
=--------------
---------------
---------------
---------------
---------------
111
111
1 1 1
000000000.000
111
111
111
OOOO�O�OO���
---------------
000000000000000
---------------
---------------
---------------
---------------
---------------
---------------
0
0
0
0
11
0
111
0
1 11
11
0
0
0
11
0
0000
11
000
1 11
11
0©0
11
O
---------------

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2014 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-06 2.9 ACRES
TOTAL GALLONS 42,000
---------------
---------------
---------------
---------------
---------------
----
-
-------
0
111
11
0
11
�
11
�
0
0
0
0
0
0
11
0
111
��
11
0
11
�0�00��
11
---------------
---------------
---------------
---------------
---------------
---------------
---------------
---------------
---------------
---------------
111
1 1
0
1 11
00.00000�000
0
11
00000000000�0

SOIL ANALYSIS REPORTS

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
ReportNo. FY14-SL028459
Client:
Barnes Environmental Inc.
Advisor:
Martin Mabe
Predictive
PO Box 654
S & ME, Inc.
�l
Newport, NC 28570
3718 Old Battleground
;' ���/F�/'
Mehlich-3 Extraction
Soil Re
Rd
+ '.ram!></''
N
Sampled County : Carteret
Greensboro,
NC 27410
Sampled: Received: 02/07/2014
Completed: 02/24/2014
Farm:
Links to Helpful Information
Sample ID: 001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean 0.7
0 0
110
25 25
0
0
0
0
Note: 3
2-
$pH
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.60 1.39
2.2 48 1.2 5.2 172 16
36 8
22
34
30
73
73
115
0.1 5
Sample ID: 002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu-
B
Information
Lime History:
1 -Bermuda hay/past., E 0.0
60-80 0
120
25 0
$
0
0
0
Note: 12 Note:
2 - Bermuda hay/past., A 0.0
180-220 0
220
$ 0
$
0
0
0
Note: 12 Note:
Test Results [units - WN in glcnr3; CEC and Na in meg1100 crrP; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-I
Mn-1
Mn-All Mn-AI2
Zn-I
Zen -AI
Cu-I
Na ESP
SS4 NO3-N
0.56 1.33
5.2 98 0.1 7.1 259 10
94 4
32
38
24 24
140
140
587
0.1 2
Sample ID: 003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
'Lime History:
1 -Bermuda hay/past., E 1.5
60-80 120
120
25 0
$
0
0
0
Note: 12 Note:
2 - Bermuda hay/past., h 0.0
180-220 120
210
$ 0
$
0
0
0
Note: 12 Note:
Test Results [units - WN in glca; CEC and Na in meq/100 cd; NO3-N in mg/drrr ]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K71
Ca% Mg%
S-I
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
2.52 1.14
5.0 47 2.7 5.2 11 12
41 4
49
7
21 21
35
35
106
0.1 2
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY14-SL028459
Page 2 of 3
Sample ID: 004
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Pine, E
0.0
0 0
60
25
0
0 0
Note: 11
2 - Pine, M
0.0
100-150 0
60
$
0
0 0
Note: 11 Note:
Test Results [units - W/V in g/crap; CEC and Na in meq/100 cd; NO3-N in mg/drr?]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-1
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
1.87 1.21 10.4 100 0.0 7.1
158 9
96 3 46
24
339
339
1051 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY14-SLO28459
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium.
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium.
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagrgov/agronomi/obpart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur. index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
Zn-I
zinc index
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm
for more information.

Page 1 of 2
Report Number: 15-049-0576
Account Number: 45470w
Send To: S&ME(USE THIS ACCOUNT)
www.aleastem.com
ACCOUNTS PAYABLE
8646 W MARKET ST
SUITE 105
GREENSBORO NC 27409
Date Received: 02/1812015 Date Of Analysis: 02/19/2015
A&L Eastern Laboratories
7621 Whitepme Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower: Submitted By: MARTIN MABE
WILLTURNER Farm ID:
JOB#1588-01-016
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 02/19/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
I Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
ENR
% Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
pp m
Rate
pH
Index
meq/100g
meq/100g
VVT 5
22190
1.8 L 72
413 VH
VL
L
1808
VH
VL
NC=344
127
NC=14
189
122
7.4
0.0
9.9
VVT6
22191
1.4 L 64
355 VH
23 VL
34 VL
1842
VH
20
VL
NC=296
NC=12
7.1
0.0
9.6
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Fed ID
K
I Mg
Ca
I Na
I H
NO3N
S
Zn
Mn
Fe
Cu
I
B
SS
Cl
Al
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm
Rate
ms/cm Rate
ppm Rate
ppm
VyT 5
27 H
49.0 VH
9 L
169
VH
15.7 VH
0.4
L
0.7
7.5
91.3
1.0
0.0
NC = 56
NC = 1225.0
NC = 56
NC = 785.0
18NC
26 VH
3 L
VH
10.9VH
VL
r-6
0.6
3.0
95.9
I 0.9
I 0.0
I
�247
I
10.3
= 371
NC = 650A
NC = 19
NC = 545.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. c
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: ? W'. m G
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary

M
Page 2 of 2
Report Number: 15-049-0576
Account Number: 45470
Send To: S&ME(USE THIS ACCOUNT)
ACCOUNTS PAYABLE
8646 W MARKET ST
SUITE 105
GREENSBORO NC 27409
Date Received: 02/18/2015
Date Of Report: 02/19/2015
w s A &LEastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern,com
Grower: Submitted By: MARTIN MABE
WILLTURNER Farm ID:
JOB#1588-01-016
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P20s
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
WT 5
Adjust pH to 6.0
0
0.0
0
I
3
I 0
WT-5
Rye
40
0.0
62
0
90
0
0
0
4
0
0
0.5
WT 6
Adjust pH to 6.0
0
I 0.0
46
4
0
WT-6
Rye
40
0.0
62
0
93
46
11
0
4
0
0
1.0
Comments:
Samples): WT-6 Crop: Rye
Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag.
Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate.
Boron recommendations are on a broadcast basis.
The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth
starts in the spring.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �1
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary