HomeMy WebLinkAboutWQ0018352_Residual Annual Report 2014_20150302. 9 0--r' I� 3
Town of Boiling Springs
P.O. BOX 1014
BOILING SPRINGS, NC 28017
Telephone 704434-2357
Fax 704-434-2358
www.boilingspringsnc.net
February 24, 2015
NCDENR-Division of Water Quality
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2014 Annual Land Application of Residuals
Town of Boiling Springs
Permit # WQ0018352
To Whom It May Concern:
Please find enclosed the original and (2) copies of all applicable forms and test results for
the Annual Land Application Report for the Town of Boiling Springs. Aerobic digested
biosolids continue to be land applied to permitted fields for beneficial reuse as a soil
conditioner and a fertilizer supplement.
Please give me a call if you have any questions or if additional information is needed at
(704) 434-2357.
Sincerely,
'/;L c.
Tom Hart
Town Manager RECEIVEDIDENRI®WR
MAR - 2 2015
cc: File
Permitting Section
Enclosures
,i A,
ANNUAL LAND APPLICATION
OF RESIDUALS
2014 ANNUAL REPORT
TOWN OF BOILING SPRINGS
Permit No. WQ0018352
CERTIFICATION FORM
s ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0018352 County: Cleveland Year:. 2014
Facility Name (as shown on permit): Town of Boiling Springs
Land Application Operator: Mike Gibert Phone: 704-434-2357
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summaa.-
Total number of application fields in the permit:
3
Total number of fields utilized for land application during the year:
2
Total amount of dry tons applied during the year for all application sites:
14.63
Total number of acres utilizes for land application during the year:
26.2
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted, as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are .
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Tom Hart Town Manager C.
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0018352 FACILITY NAME: Town of Boiling Springs
PHONE: 704-434-2357 COUNTY: Cleveland OPERATOR: Mike Gibert
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes No --► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
NC 0071943
0
February
NC 0071943
0
March
NC 0071943
3.22
April
NC 0071943
4.23
May
NC 0071943
0
June
NC 0071943
0
July
NC 0071943
~
2.24
August
NC 0071943
2.52
September
NC 0071943
l
0
October
NC 0071943
0
November
NC 0071943
2.42
December
NC 0071943
0
Total from FORM DMSDF (su)�.
Totals:
I Annual (dry tons):,.,.,,
- 0" '
14 63
0- _
0;
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit '✓Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: No 0, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, .under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
v
Signature of Permittee Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
rx445
Date
DENR FORM DMSDF (12/2006)
RESIDUALS SAMPLING FORM
k
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0018352
Facility Name: Town of Boiling Springs
Residual Source WQ # or
NPDES #:
NC 0071943
WWTP Name: Town of Boiling Springs WWTP
Residual Analvsis Data
Laboratory: 1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
8-20-14
Percent Solids (%)
NA
2.3
Arsenic
75
<37.9
Cadmium
85
<3.8
Copper
4,300
179
Chromium
NA
<25
Lead
840
<19
Mercury
57
ND
Molybdenum
75
<19
Nickel
420
<19
Selenium
100
<37.9
Zinc
7,500
523
Total Phosphorus
NA
848
TKN
NA
27700
Ammonia -Nitrogen
NA
<423
Nitrate and Nitrite
NA
6600
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1,--,1 �z .,�
Signature of Preparer *
Date
0-1
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T..1102 (26)
DENR FORM RSSF (12/2006)
tW�
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ 0018352
Facility Name: Town of Boiling Springs
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
NC 0071943
Town of Boiling Springs WWTP
Laboratory:
1)
2)
3)
4)
5)
Pace Analytical Services
Parameter
(mg/kg)
Sample or • •• Date
1 I
• 1
----------
Potassium
------------
----------
------------
----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF - B (12/2006)
METALS FIELD LOADING SUMMARY
olp
LAND APPLICATION FIELD SUMMARY
FORMS
1
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: Town of Boiling Springs
Land Owner: James Petty
Operator: Mike Gibert
Crop 1 Name: Fescue
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0018352 Field #: 1
Annual Dry Tons Applied: Site Site #: JPI
Predominant Soil Series: Pacolet-Bethlehem
Crop 1 Max. PAN:
250
Crop 2 Name:
Acres Utilized: 9.84
Acres Permitted: 22.41
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
L o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Moist
Precip.
Past 24
Hrs.
inches
>
q ' 0
a
o
w w
*
7
_w -,
CD w
* w
TKN
mg/kg
Z Y
o E9
ao o
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(-lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3-11-14
28600
2.7
0.32T.:..
NCO071943
Dry
0
S
0.5
0.3
27700
423
6600
=9,814'-
. ; �NA,
fescue
4-2-14
12900
2.5
0.137'.'-
NCO071943
Dry
0
S
0.5
0.3
27700
423
6600
'4:099 �
." "Nk
fescue
4-3-14
25600
2.7
;0.193 .-.
NCO071943
Dry
0
S
0.5
0.3
27700
423
6600
.8."-784
NA-:
fescue
7-1-14
23400
2.3
6.228,
NCO071943
Dry
0
S
0.5
0.3
27700
423
6600
:6.840v,`
fescue
8-28-14
25200
2.4.,.�.0.256,"
NC0071943
Dry
0
S
0.5
0.3
27700
423
66007:686
_NA,'
fescue
° `0.000-
`-'0.000-_
- 000z
o:000
0.000`
000.
0.0oo,
: 0:000':-
o:000a �.
"0:000-.�
0.000..
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form)
TOTAi :
= �a'.;, ��:o
� .Ii5700
;n.%- ,-- ,
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
1, 3.7.223
''.0:000,
Lime Applied
Annual lbs/acre
0.094". °,
0.327
6A21 `; ° °�
36
_::0.00,9'<;
0.049
;0".058 ;
34
, 0.444`;
1.931
- 2.375.;.
1338
0:062„: �
0.215
"; 4.277
n/a
,0.047 ;
0.251
::'0.298,.,'
267
, O.000;;
0.008
;A.608
15
; ;O:Q47r `
0:252
'6 _
`0"209,
n/a
: 0.047:, ;
0.252
:A.299' �
374
.0 094 "
0.505
-�0.599' ,
89
:;,1:298 :
5.898
, 7:196
2498,.
; 2 105 F :b " ` ,°,. . `.. ,
Date
lbs/ac
Prior Years Cumulative lbs/ac
t>na/ia
3417
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop`nj
. 4 _r
2s
"°I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
'77 ?tt ;2- ' 2-`'�— « **Volatilization Rate: Surface - 0.5. Iniection/Incomoration - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinL- Rate
DENR FORM FSF (12/2006)
`) ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Boiling Springs WWTP Total Dry Tons Applied (Annual):
WQ0018352 Cation Exchange Capacity (non 503 only):
Mike Gibert Owner: James Petty Predominant Soil Series:
9.84 Acres Permitted: Site #: JP 1
Paco let -Beth lehem
Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kff. % Solids use Raw Percent 41:
Sample or
Com-
posite
Date
8-20-14
8-20-14
8-20-14
8-20-14
8-20-14
% Solids
2.3
2.3
2.3
2.3
2.3
Arsenic
37.9
37.9
37.9
37.9
37.9
Cadmium
3.8
3.8
3.8 -
3.8
3.8
Copper
179
179
179
179
179
Chromium
25
25
25
25
25
Lead
19
19
19
19
19
Mercury
0.2
0.2
0.2
0.2
0.2
Molyb-
19
19
19
19
19
Nickel
19
19
19
19
19
Selenium
37.9
37.9
37.9
37.9
37.9
Zinc
523
523
523
523
523
Total
Phos-
horus
848
848
848
848
848
Annual eavy Metal Field Loa din s Calculated in lbs/acre :
Total
DT/Ac./-
App.
Event
0.33
0.14
0.29
0.23
0.26
H
0
y
Arsenic
= 0.025
'-'A'010',
-'. 022 '
' :0:017
°,.0:0-19�
" 0.000'
,. 0:000
; "0:000
0:000
`0:000
0:000'
0.000
0:094�
Cadmium
'0.002 .
'0.001- '
`.0.002
0.002 '
0.002
0:000
.6.000.
, 0:000 .
0.000
: 0:000
0:000.
0.000
'0 000 .
Copper
„� 0.1:17
-..0:049 -
..;0.1�05
' 0.082 ;
,0 092��.'
_O:a000�,
�000���
0:0,00�,:
� 0`600
.�0:00.0��.
"0:000�'�
, 0:000�,
.0:4'44°.
Chromi
' `_0.016, `
' A.00T
'`0:015"
0.011 °
0.013 '
',0.000
0,000 -
" 0 000:
6000 :
" 0.000.
0-.000 :
0:000-
'0:062
Lead
='0012 .
. 0.005
A.011
0.009 „
0:010
0.000
0.000
0000.
0.400
0.000 '.
OA000 ,
'0,.000.��
. `0.047__
Mercury
0;:000
0:000
'�,0:000.
,M0:000
Fl _0.000
0:000 o
"�0.000
0:000�
0.,000:
`,0.000
A:00.0
0.000'
_.0000
Molyb-
�0:012,
0.005
4011
0.009
-0.010
0.000
0.000'
0.000'
0.000demim
a
' .0.000
0:000
0.00.0
0047
Nickel
`; 0:012 �.
A:005
� 0.011.
',n0:009
0.010
0.00�0, .
A.00�0�
..
0,�000.,
. "0�000,
_
.�;0:000 _
. �ro0.000
0:0W
' O:047� ;
Selenium
.0.025'
,�0:010
`,0:022
"0:01:7.
0.019
a000
0:000
�A:000
0:000�,�
0.00,0'�.
"0.000,
0.000`
�0:094.
Zinc
0342
:0.143
0.106
0.238
0:268 '
0.000
"0.000,
0.000
0.000
'-O:000
0:000 -
p.000`
.1.298 `.
Total
Phos-
horus
it
0;555
,
0.232
1 0:497
0387
O' 34
�_0:000
0.000
0 000'
°0'000 '
0.600
0.000
0:000
- 2.105
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Boiling Springs WQ Permit #: WQ0018352 Field #: 2 Acres Utilized: 16.36
Land Owner: James Petty
Operator: Mike Gibert
Crop 1 Name: Fescue
Annual Dry Tons Applied: 2.4169
Site #: JP2
Acres Permitted:
Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 250 Crop 2 Name:
Crop 2 Max. PAN:
o
�
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Moist)
Precip.
Past 24
Hrs.
inches
a
4.6
CD 'a
0 R
*
o
w
* �.
w Q
E.
N'
* K
Z
TKN
mg/kg
Z %
o B
o
R.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
11-12-14
25200
2.3
-0.148
NCO071943
Dry
0
S
0.5
0.3
27700
423
6600
4.430
NA
fescue
0.000
0.000 .
0.000
0.000
0.000 "
'0.000-
0.000
0.0.00
0.000
0.000
0.000
`0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000,
' A000
0.000
0.000
.0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALSI
01
25200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
4.430
0.000
Lime Applied
Annual lbs/acre
0.011
0.001
0.053
0:007
0.006 `
0.000
0.006 .
0.006
0.011
0.155.
. 0.251
Date
Ibs/ac
Prior Years Cumulative lbs/ac
0.1
0.019
0.522
0.008
0.091
0.001
0.091
0.091
0.181
1.31
Current Cumulative lbs/ac
0.111
0.020
0.575
0.015
0.097
0.001
0.097
0.097
0.192
1.465,
Permitted C. P. L. R.****
36
34
1338
n/a
1 267
1 15
1 n/a
1 374
89
2498
Permit PAN Limit 1 st/2nd Crop
250.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinLy Rate
DENR FORM FSF (12/2006)
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual):
Permit #:
Operator:
Acres Used:
WQ0018352
Mike Gibert Owner:
9.84 Acres Permitted:
Cation Exchange Capacity (non 503 only):
James Petty Predominant Soil Series: Pacolet-Bethlehem
Site #: JP2 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample 1 2 3 4 5 6 7 8 9 10 1 12
or Com-
posite
Date 8-20-14
% Solids 2.3
Arsenic 37.9
Cadmium 3.8
Copper 179
Chromium.25
Lead 19
Mercury 0.2
Molyb- 19
denum
Nickel 19
Selenium 37.9
Zinc 523
Total
Phos- 848
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations". -
z
Signature of sand Applier Date
RE: Residuals Generated But Not Land Applied
The Town of Boiling Springs WWTP land applied 14.63 dry tons of biosolids
to permitted fields in 2014. The remainder of the biosolids, were hauled to
the Cliffside Sanitary District WWTP permit # NC0004405 during periods of
wet weather. These biosolids were introduced at the headworks of the
plant and treated through the facilities processes.
1
RESIDUALS ANALYSIS LAB SHEETS
r-g,o i t_.�
•
/
WIN
ter-
z�raw.
.ate
mac
sac r
TC L P LABORATORY SHEETS
Inalytical
wwpamiabs.com
ANALYTICAL RESULTS
Project: TCLP Sludge Analysis
Pace Project No.: 92214172
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: TCLP Sludge Lab ID: 92214172001 Collected: 08/20/14 08:30 Received: 08/20/14 14:34 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081 Preparation Method: EPA 351.0
Leachate Method/Date: EPA
1311; 08/21/14 17:00
gamma-BHC (Lindane)
ND ug/L
0.50
1
08/22/14 10:27
08/26/14 04:42
58-89-9
Chlordane (Technical)
ND ug/L
3.0
1
08/22/14 10:27
08/26/14 04:42
57-74-9
Endrin
ND ug/L
0.50
1
08/22/14 10:27
08/26/14 04:42
72-20-8
Heptachlor epoxide
ND ug/L
0.50
1
08/22/14 10:27
08/26/14 04:42
1024-57-3
Methoxychlor
ND ug/L
1000
1
08/22/14 10:27
08/26/14 04:42
72-43-5
Toxaphene
ND ug/L
3.0
1
08/22/14 10:27
08/26/14 04:42
8001-35-2
Surrogates
Decachlorobiphenyl (S)
65 %
10-138
1
08/22/14 10:27
08126/14 04:42
2051-24-3
Tetrachloro-m-xylene (S) .
60 %
10-110
1
08/22/14 10:27
08/26/14 04:42
877-09-8
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151 Preparation Method: EPA 3510
2,4-D
ND mg/L
0.44
1
08/28/14 08:20
08/29/14 02:12
94-75-7
2,4,5-TP (Silvex)
ND mg/L
0.44
1
08/28/14 08:20
08/29/14 02:12
93-72-1
Surrogates
2,4-DCAA (S)
91 %
42-142
1
08/28/14 08:20
08/29/14 02:12
19719-28-9
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
6510 mg/kg
379
1
08/22/14 19:20
08/27/14 23:42
7429-90-5
Arsenic
ND mg/kg
37.9
1
08/22/14 19:20
08/2911413:44
7440-38-2
Cadmium
ND mg/kg
3.8
1
08/22/14 19:20
08/27/14 23:42
7440-43-9
Calcium
31500 mg/kg
379
1
08/22/14 19:20
08/27/14 23:42
7440-70-2
Copper
179 mg/kg
19.0
1
08/22/14 19:20
08/27/14 23:42
7440-50-8.
Lead
ND mg/kg
19.0
1
08/22/14 19:20
08/27/14 ?3:42
7439-92-1
Magnesium
1760 mg/kg
379
1
08/22/14 19:20
08/27/14 23:42
7439-95-4
Molybdenum
ND mg/kg
19.0
1
08/22/14 19:20
08/27/14 23:42
7439-98-7
Nickel
ND mg/kg
19.0
1
08/22/14 19:20
08/27/14 23:42
7440-02-0
Potassium
ND mg/kg
19000
1
08/22/14 19:20
08/27/14 23:42
7440-09-7
Selenium
ND mg/kg
37.9
1
08/22/14 19:20
08/27/14 23:42
7782-49-2
Sodium
ND mg/kg
19000
1
08/22/14 19:20
08/27/14 23:42
7440-23-5
Zinc
523- mg/kg
37.9
1
08/22/14 19:20
08/27/14 23:42
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311: 08/25/14 20:00
Arsenic
ND mg/L
0.050
1
08/26/14 15:00
08/26/14 22:50
7440-38-2
Barium
0.40 mg/L
0.25
1
08/26/14 15:00
08/26/14 22:50
7440-39-3
Cadmium
ND mg/L
0.0050
1
08/26/14 15:00
08/26/14 22:50
7440-43-9
Chromium
ND mg/L
0.025
1
08/26/14 15:00
08/26/14 22:50
7440-47-3
Lead
ND mg/L
0.025
1
08/26/14 15:00
08/26/14 22:50
7439-92-1
Selenium
ND mg/L
0.10
1
08/26/14 15:00
08/27/14 14:06
7782-49-2
Silver
ND mg/L
0.025
1
08/26/14 15:00
08/26/14 22:50
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA
1311; 08/25/14 20:00
Mercury
ND ug/L
0.20
1
08/26/1415:30
08/27/14 11:55
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/04/2014 03:33 PM without the written consent of Pace Analytical Services, Inc..
Page 4 of 27
.y aceAnalytical
f www.pacelabs.com
j
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: TCLP Sludge Analysis
Pace Project No.: 92214172
Sample: TCLP Sludge
Lab ID: 92214172001
Collected: 08/20/14 08:30
Received: 08/20/14 14:34 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
7471 Mercury
Analytical Method: EPA7471 Preparation Method:
EPA7471
Mercury
0.18 mg/kg
0.17
1
08/26/14 13:15
08/26/14 16:40
7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Leachate Method/Date: EPA 1311; 08/21/14 17:00
1,4-Dichlorobenzene
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
106-46-7
2,4-Dinitrotoluene
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
121-14-2
Hexachlorobenzene
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
118-74-1
Hexachloroethane
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
67-72-1
2-Methylphenol(o-Cresol)
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
95-48-7
3&4-Methylphen6l(m&p Cresol)
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
Nitrobenzene
ND. ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
98-95-3
Pentachlorophenol
ND ug/L
100
1
08/22/14 10:27
08/24/14 23:03
87-86-5
Pyridine
ND ug/L
50.0
1
08%22/14 10:27
08/24/14 23:03
110-86-1
2,4,5-Trichlorophenol
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
95-95-4
2,4,6-Trichlorophenol
ND ug/L
50.0
1
08/22/14 10:27
08/24/14 23:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
54 %
12-102
1
08/22/14 10:27
08/24/14 23:03
4165-60-0
2-Fluorobiphenyl (S)
73 %
13-107
1
08/22/14 10:27
08/24/14 23:03
321-60-8
Terphenyl-d14(S)
80 %
21-132
1
08/22/14 10:27
08/24/14 23:03
1718-51-0
Phenol-d6 (S)
21 %
10-110
1
08/22/14 10:27
08/24/14 23:03
13127-88-3
2-Fluorophenol (S)
35 %
10-110
1
08/22/14 10:27
08/24/14 23:03
367-12-4
2,4,6-Tribromophenol (S)
73 %
27-108
1
08/22/14 10:27
08/24/14 23:03
118-79-6
8260 MSV TCLP
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 08/21/14
14:30
4
Benzene
ND ug/L
5.0
1
09/04/14 06:43
71-43-2
2-Butanone (MEK)
ND ug/L
10.0
1
09/04/14 06:43
78-93-3
Carbon tetrachloride
ND ug/L
5.0
1
09/04/14 06:43
56-23-5
Chlorobenzene
ND ug/L
5.0
1
09/04/14 06:43
108-90-7
Chloroform
ND ug/L
5.0
1
09/04/14 06:43
67-66-3-
1,4-Dichlorobenzene
ND ug/L
5.0
1
09/04/14 06:43
106-46-7
1,2-Dichloroethane
ND ug/L
5.0
1
09/04/14 06:43
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
09/04/14 06:43
75-35-4
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
09/04/14 06:43
87-68-3
Tetrachloroethene
ND ug/L
5.0
1
09/04/14 06:43
127-18-4
Trichloroethene
ND ug/L
5.0
1
09/04/14 06:43
79-01-6
Vinyl chloride
ND ug/L
5.0
1
09/04/14 06:43
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
09/04/14 06:43
17060-07-0
Toluene-d8 (S)
99 %
67-135
1
09/04/14 06:43
2037-26-5
4-Bromofluorobenzene (S)
101 %
70-130
1
09/04/14 06:43
460-00-4
Percent Moisture
-Analytical Method: ASTM D2974-87
Percent Moisture
97.7 %
0.10
1
08/28/14 08:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/04/2014 03:33 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27
Analytical
mmpacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1o0
Huntersville, NC 28078
(704)875-9092
Project: TCLP Sludge Analysis
Pace Project No.: 92214172
Sample: TCLP Sludge
Lab ID: 92214172001 Collected: 08/20/14 08:30
Received: 08/20/14 14:34 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
2.3 %
0.000010
1
08/27/14 14:12
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.1 Std. Units
0.10
1
08/22/14 12:17
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
14900 mg/kg
0.12
1
09/03/14 17:23
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/kg
423
1
08/28/14 15:39 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
27700 mg/kg
1570
1
09/02/14 11:34 7727-37-9
353.2 Nitrogen, NO2iNO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
Nitrogen, Nitrite
6600 mg/kg
86.1
1
08/26/14 15:09
Nitrogen, NO2 plus NO3
ND mg/kg
6600 mg/kg
43.1
1
08/26/14 15:09
86.1
1
08/26/14 15:09
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
848 mg/kg
84.6
1
08/29/14 13:55 7723-14-0
Date: 09/04/2014 03:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
N2
Page 6 of 27
„V `44
HA9 -d F-CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUh4ENT, All relevant Fields mint be completed accurately-
-PaceA j
i www.paeeiabs.cam Page: °f
Section f3 Section C t� y ,
n Section A Invoice InFonnallon: 1 4 � � ,A'
Required Project Informxliorr,
i Required Client Information: tantrnn.
Repor9To „„........ ,r5"1`_' i;;�^%'?Y��itsie�: At ... ^..� ::•..,;
be'� L7 : r G1�1i4�1'OFiY;AGENGY:�t%„,<::'. "`,';";'�`•'`
r � Company Name: RE
Copy To: _ S' • "�}/ { DRINKING WATER
cadre pp nj j . `; j JJ n r , NPDES i GROUhtD N ATER ,
}� 1. UST 1 W RCIZA Tm'- --._..--------.�._.
OTHCR
t >Z.3, t d _ l"9 a. N., j,K ..73 "c C.ti' Par:�Quata
¢ Purchase OMer No
fYeferenca:
Emwl T ,�y ro d d' � g"[,QCa-lion
7-!Pow Project F:SI
Project Name:
Phone: Pax:ParaProgke,Y:
`
Protect Number.
Requested Due DateITAT: ;3 YIN
':.Requisteti;!1eia6ysis:filterel( ,j,. >::; `
Section D Matrix Codes 5 a Preserv8Uves
_ _ COLLECTED
ti tF%I ,C4Jt. 0 0
•_ RequiredGlient Lilerma�ai � Y'-.d � 7 ”. .
Drinking Water DINL: 4
Weter `NT U cae<, o.ttE. carxrosrr= r'"' z,; -, , z
WastaW'aier WVt m %Thg7 etacwoaao r -
PrOiloduct P I Kzy j/J j r✓
SoWSolid SL K t°iz " o i
SAMPLE ID Wipa OL v � a3
WP e, z f .V .�
(A-Z. rkI-1 A Alr AR 0
9C7
Samplo IDs MUST BE UNIQUE Tissue TS O ° 'N` J v
z
a
Other 0'1 o O
c 0 N, z c5 w Pace project No.1 Lab I.D.
w2 in DATE TIME DATE TIME m a = S Z Z
fir, y ., ..
J 1
REWNCIUI5HEC1.6Y7AFFILWTI4N . DATE• TIME:::, ACCEPTED`SYl;AFILIATtt)N iFA7E' SIh1E. .
SAMPLE CONDITIONS
� S(`� ++f/`��''� a. ..--""'�,• ; c��G,r`^'c' 1 r" �'"' l �y,�/'�'j' /� /W� vyD *�/ i j o�/�,r�
d'""....+' i ._� i.. i�. .w"". ...•..mow �} Y ti ".�"',r.`( l 8 L°' Y/ !s� 7'-f 4
"T t� rAa
y — w ( :SAMPLERNAIVSE'ANaSIGNATURE ` �. a ci`z' Z
ORIGINAL lam. - . ... t9, .n
PRINT Name of SAMPLER: �� ��„„;,, ti , � a r m � E
.. i-.."�11 DATE Signed z�-�,c,.�r!'%,r t- rr v ra
SIGNATURE of SAMPLER: <- Y� .�r� IMMIDDtYY)' — FF.ALL-0-020rev.07, 15-itfay-2007
Important rdo;a: By signing IMz 101m you a+u acca )fing Paces NET 3n dTy payment torn and agrea:ng [01a4s eY�arge;s ni t.5k. per merrih to arty rrvntces r<a1=F d wilh7n 3U +ays.
PATHOGEN & VECTOR ATTRACTION
REDUCTION FORMS
• ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boiling Springs
WQ Permit Number: WQ0018352
WWTP Name: Town of Boiling Springs WWTP NPDES Number: NCO071943
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applica
le to a
ternative pelrform
d (Class I
only) indic to "Prot
s to Furtl
er Reduc4
Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 ❑x
Alternative 2 ❑
If applicable to alternative
performed (Class B
only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑
Aerobic Digestion ❑x
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<1266
1486
!27140
MPN/g
0
7/year
Grab
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑x
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Gibert Mike Gibert Public Works Director
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1•
� 7Ll - � -z4-r s
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
( r Y
Annual Pathogen and Vector Reduction Summary
Town of Boiling Springs permit # WQ0018352
Fecal Coliform - Class B
There were seven (7) test results provided by Pace Analytical Services in Huntersville.
The calculated Geo Mean for the Fecal Coliform samples was 1486 MPN/g.
Vector Attraction Reduction
Option 4 - Sour test results are reported in the attached data showing seven (7)
test results at 0.12 mg Oxygen/g/hr or less for Specific Oxygen Uptake Rate.
End temperature for each test result was under 30 Degrees Celsius and the percent
solids were under 2% for each result.
'_1 , --
Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville NC 28078
Entered 8/28/2014
Reported: 9/2/2014
For:
92215108 Aerobic Dig 8/27
Sample ID
Parameter
Cust ID
Result
Units
Method
Date Analyzed
Analyst
140828-10.1
% Solids
001
1.52
%
SM254013-
8/28/14
WL
140828-10.1
Fecal Coliform MTF
001
16
MPN/g
SM9221 CE-
8/28/14
WL
140828-10.1
Geometric Mean
001,
1486
MPN/g
dry wt. basis
9/2/14
CL-...
140828-10.2
% Solids
602
1.58
%
SM25406-
8/28/14
WL
140828-10.2
Fecal Coliform MTF
002
<1266
MPN/g
SM9221 CE-
8/28/14
WL
140828-10.3
% Solids
003
1.46
%
SM254013-
8/28114
WL
140828-10.3
Fecal Coliform MTF
003
2740
MPN/g
SM9221 CE-
8/28/14
WL
140828-10.4
% Solids
004
1.37
%
SM254013-
8/28/14
WL
140828-10.4
Fecal Coliform MTF
004
1460
MPN/g
SM9221 CE-
8/28/14
WL
140828-10.5
% Solids
005
1.49
%
SM254013-
8/28/14
WL
140828-10.5
Fecal Coliform MTF
005
1342
MPN/g
SM9221 CE-
8/28/14
WL
140828-10.6
%° Solids
006
1.55
%
SM254013-
8/28/14
WL
140828-10.6
Fecal Coliform MTF
006
1290
MPN/g
'SM9221 CE-
8/28/14
WL
140828-10.7
% Solids
007
1.44
%
SM2540B-
8/28/14
WL
140828-10.7
Fecal Coliform MTF
007
1389
MPN/g
SM9221 CE-
8/28/14
WL
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 * Statesville, North Carolina 28687 * 704/872/4697
Page 11 of 11
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis DatelTime
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
Town of Boiling S rin
s,NC
WQ0018352
82714
26.1
8 27 14 1000
TERRY
8 27 14 1001
TERRY
1000
1.52
26.1
26
(minutes)
m /1)
0
1
6.97
2
6.94
3
6.93
4
6.90
5
6.88
6
6.87
7
6.85
8
6.82
9
6.80
10
6.79
11
6.78
12
6.76
13
6.74
14
6.72
15
6.71
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.0
1.0
milliliters
Yo Dry Solids
Degrees Celsius
Degrees Celsius
1.12 mg Oxygen/hr
0.07 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Cl) 2 3 4 5 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(m /I)
0
7.02
1
7.00
2
6.97
3
6.97
4
6.95
5
6.93
6
6.90
7
6.87
8
6.85
9
6.82
10
6.80
11
6.78
12
6.76
13
6.75
14
6.73
15
6.70
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Town of Boiling S rin
s,NC
WO0018352
82714
26.1
8 27 14 1015
TERRY
8 27 14 1016
TERRY
1000
1.58
26.1
25.9
0.0
7.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.30 mg Oxygen/hr
0.08 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 20 3 4 5 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) m /I)
0
7.01
1
6.99
2
6.95
3
6.91
4
6.89
5
6.85
6
6.83
7
6.80
8
6.78
9
6.75
10
6.71
11
6.71
12
6.68
13
6.66
14
6.63
15
5.99
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling S rin
s,NC
WO0018352
82714
26.1
8 27 14 1030
TERRY
8 27 14 1031
TERRY
1000
1.46
26.1
26.1
0.0
7.1
0.8
milliliters
Yo Dry Solids
Degrees Celsius
Degrees Celsius
2.42 mg Oxygen/hr
0.17 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.12 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2(1 4 5 6 7
Circle Test #
0 , , 1
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen level
(minutes)
m /1)
0
6.97
1
6.93
2
6.89
3
6.85
4
6.85
5
6.82
6
6.80
7
6.78
8
6.75
9
6.73
10
6.71
11
6.69
12
6.65
13
6.64
14
6.61
15
5.98
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin
s,NC
WO0018352
82714
26.1
8 27 14 1045
TERRY
827141046
TERRY
1000
1.37
26
26
0.0
7.0
0.8
milliliters
Yo Dry Solids
Degrees Celsius
legrees Celsius
2.25 mg Oxygen/hr
0.16 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.12 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 g 5 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date.
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (m /I
0
6.97
1
6.93
2
6.90
3
6.90
4
6.87
5
6.85
6
6.82
7
6.80
8
6.77
9
6.75
10
6.72
11
6.70
12
6.68
13
6.66
14
6.65
15
6.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin
s,NC
WO0018352
82714
26.1
827141100
TERRY
8 27 14 1101
TERRY
1000
1.49
26.1
26
0.0
7.0
1.0
milliliters
Yo Dry Solids
Degrees Celsius
legrees Celsius
1.36 mg Oxygen/hr
0.09 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.07 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4CY 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) m /I
0
6.95
1
6.93
2
6.90
3
6.88
4
6.87
5
6.85
6
6.81
7
6.79
8
6.76
9
6.73
10
6.70
11
6.67
12
6.64
13
6.61
14
6.58
15
6.56
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin
s,NC
WO0018352
82714
25.9
8 27 14 1115
TERRY
8 27 15 1116
TERRY
1000
1.55
25.9
25.8
0.0
7.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.60 mg Oxygen/hr
0.10 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.08 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 6` 7
Circle Test #
t 4 , 1
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
Town of Boiling Sprin
s,NC
WO0018352
82714
25.9
8 27 14 1130
TERRY
8 27 14 1131
TERRY
1000
1.44
25.9
25.8
(minutes) (m /I
0
6.93
1
6.90
2
6.88
3
6.85
4
6.81
5
6.78
6
6.75
7
6.71
8
6.68
9
6.65
10
6.62
11
6.60
12
6.57
13
6.55
14
6.51
15
6.49
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.80 mg Oxygen/hr
0.13 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate:1 0.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 6
Circle Test #
A" ( )� y
SOIL ANALYSIS REPORT
go
A&L EasternLaboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
www,aleastern.com
l+All A\IAI V
JUDmlttea t3y: IAW
I r'IA UAI.AL
--
I-
Client:
Grower:
Report No:
14-241-0575
PACE ANALYTICAL CHARLOTTE (for
92215122
Cust No:
05755
Tabitha Dacal)
SAMPLING 8/26
Date Printed:
09/02/2014
TABITHA M DACAL
Date Received :
08/29/2014
9800 KINCEY AVE - STE 100
Date Analysis :
09/02/2014
HUNTERSVILLE NC 28078
Page :
1 of 2
PO: TMD13658
Lab Number: 07815 Field Id : Sample Id: JOHN PETTY
Test
Results
SOIL TEST RATINGS
Calculated Caton
Exchange Capacity
e Medium 0' ..
Soil pH
5.5
10.2
meq/100g
Buffer pH
6.67
Phosphorus (P)
171 ppm
M. :•,• w-F.
raj m
Calculated Cation'
Saturation
Potassium (K)
Calcium (Ca)
Magnesium (Mg)
365 ppm
1000 ppm
176 ppm
%K 9.2
%Ca 49.0
%Mg 14.4
%H 25.7
Hmeq 2.6
%Na 1.4
Sulfur (S)
24 ppm
Boron (B)
Copper (Cu)
0.9 ppm
3.2 ppm
Iron (Fe)
125 ppm
_
ff-swimm
§
Winn -WE
Manganese (Mn)
13 ppm
K:,MgRatio a
Zinc (Zn)
8.4 ppm
0.64
Sodium (Na)
33 ppm
Ca : Mg Ratio'
Soluble Salts
3.40
Organic Matter
6.9 % ENR 150
Nitrate Nitrogen
SOIL FERTILITY GUIDELINES
ram.,.. • l \Alf INPW1 Rec Units: LB/1000 SF
jibs) LIME (tons)
N
PQ 05
K 20
Mg '
S
B
Cu
Mn
Zn
Fe
71
3.5
0
0
0
0.23
0
0
1 0.05
1 0
0
Crop : Rec Units:
Comment:
Analysis prepared by: A&L Eastern Laboratories, Inc.
Page 5 of 6
Pauric McGroary
A &L Eastern Laboratories
Llk! J 7621' Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax (804) 271-6446
www.aleastem.com
1uomltrea tiy: IAbl
I HA UAGAL VIZIZU14 JUIL ANALT010
Client:
Grower:
Report No: 14-241-0575
PACE ANALYTICAL CHARLOTTE (for
' 92215122
Cust No: 05755
Tabitha Dacal)
SAMPLING 8/26
Date Printed: 09/02/2014
TABITHA M DACAL
Date Received : 08/29/2014
9800 KINCEY AVE - STE 100
Date Analysis : 09/02/2014
HUNTERSVILLE NC 28078
Page : 2 of 2
_
PO: TMD13658
,
Lab Number: 07815 Field Id: Sample Id: JOHN PETTY
SUGGD_�FERTILIZATION._PROGRAM�:
First A' licationSecond
PP
Application; :
Third Applicatiop; . " ..
- Fourth Application
Mob Ft. . Ft`;
Fertilizes
#lAOOO;Sq Ft::
:Fertilizer
#/1000.Sq. Ft.'
Fert)lizer
: #/1000 Sq. Ft..
Fertilizer.
6
21-0-0
6
21-0-0
6
21-0-0
Comments:
Lawn(New)
Limestone application is targeted to bring soil pH to 6.2.
Apply the amount of lime recommended in first page to raise pH
For existing lawns, lime applications should NOT exceed 50 pounds per 1000 sq. feet per application. Split and apply every 4 to 6
month until the recommended amount is completed.
--I -• Lime is insoluble in water thus move very slowly downward in the soil to raise the pH: For new Lawn,, the best result -is -to broadcast
all the recommended lime over the surface, incorporate and mix 6 inches into the soil. If lime is not incorporated and mixed into the
soil, lime application should NOT exceed 50 pounds per 1000 sq. feet per application. Split and apply every 4 to 6 month until the
recommended amount is completed.
• The amount of fertilizer recommended on the first page is the total amount needed for the entire growing season. Split into 3-4
applications to keep the lawn green and prevent fertilizer loss. You should not apply more than 0.7 Ibs of soluble nitrogen per 1000
square feet in a 30 day period. Or more than 0.9 Ibs of nitrogen per 1000 square feet if you are using a slow or controlled release
product in a 30 day per)od.Custom blend is best to meet exactly the requirement, if this is impossible, the above specific fertilizer
application is a general guideline, if the specified grades can not be found, replace with fertilizer having similar N:P:K ratio. The best
time to apply fertilizer for cool season grass (bluegrass, fescue, ryegrass) is in the Fall when the grass is growing. For Mid -Atlantic
region the time is from late August to November. For Northeast region the time is from mid August to October. Fall application should
start as soon as the day time high temperature is below 80-85F, apply with the interval of one month. If you start application late in the
Fall and do not finish all three applications, repeat the same applications in the Fall of next year. Spring application is recommended
when exceptional fertilizer loss due to heavy spring rain leaching and the grasses look pale green. Spring application can start as soon
as the grass starts to grow in April. In the case of exceptional warm spring, the application can be made earlier.
• For a more in depth explanation of the soil test and recommendations, go to our website www.aleastern.com and select the "Lawn
and Garden" tab at the top of home page. Under the "How to Understand a Soil Test Report". header you will find the _link to the article
"Soil Test Report & Fertilizer Recommendation Explained".
Page 6 of 6
Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary