WQ0018087_Residual Annual Report 2014_20150223

17
®AIK Americas
January 30, 2015
Certified Mail
Return Receipt Requested
Department of Environmental & Natural Resources
Division of Water Quality
Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
2014 Surface Disposal of Wastewater Residuals
DAK Americas LLC, Cape Fear Plant PERMIT 9 WQ0018087
Dear Sir/Madam:
Attached are the data for our 12 -acre lagoon, which is now classified as a "Surface
Disposal Site". There were 9.29 dry tons applied in 2014.
Also attached is the remaining volume in the 12 acre surface disposal site in cubic yards
and an estimate of the remaining useful disposal life for the 12 acre surface disposal site
in years. Should you have any questions, please contact Larry N. Young our "Operator in
Responsible Charge", on [phone].
Sincerely,
Penny Mahoney
Operations Director
Sustainability and Operations
Support RECEIVEDMENNIND
VVIR
FEB 2 3 2015
PenneSection
Cape Fear Site o 3500 Daniels Road NE -o P.O. Box 2260-o Leland, NC 28451
877-432-2766(toll-free) o 910-371-4000(phone) o 910-371-4179(fax)
mm. da GLamer9ca5.com

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0012759 County: Brunswick Year: 2014
Facility Name (as shown on permit): DAK Americas LLC, Cape Fear Site
Land Application Operator: Larry N. Young Sr. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
® Yes p No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Part B:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. ® Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
- .1. -Only residuals approved for this permit were applied to the permitted sites. -
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached. -
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediation.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowi violations."
Penny C. Mahoney, Sustainability & Oper. 'X3 �e1�
Permittee Name and Title (type or print) Signa of Permittee Date
a 0 v'
Fgnatur of Prep rer* Date _ Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)
DFNR FORM ACF (5/2003)

int
ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: WQ0018087 FACILITY NAME: DAK Americas LLC, Cape Fear Site
PHONE: [phone] COUNTY: Brunswick OPERATOR: - Larry N. Young, Sr.
FACILITY TYPE (please check one): 21 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year?, 21 Yes ®No No If No skip parts A, B, C and certify form below
* If more space than given is required, please attach additional information sheet(s). ® Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. Rl Yes ® No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I cer 'fy, under penalty of law, that the above information is, to the best of 'my knowledge and belief, true, accurate and complete. I ani aware
t ere si fic t penalties for submitting fal a inf rmation, inclu i e possibility of fine and imprisonment for knowing violations."
39
Signa a of Permittee Date Signature of P eparer* * Date
(if different from Permi ee) * *Preparer is defined in 40 CFR Part 503.9(r)
nFNR FORM nm.,;nF ti /9nn.ri1
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent Residual In Product Out
Volume (dry
Name(s) tons) Intended use(s)
January
NC0000663
0
1.64
0
February
NC0000663
0
0.15
0
March
NC0000663
0
0.23
0
April
NC0000663
0
0.61
0
May
NC0000663
0
0.24
0
June
KC0000663
0
0.49
0
July
NC0000663
0
0.2
0
August
NC0000663
0
0.27
0
September
NC0000663
0
0
0
October
NC0000663
0
3.64
0
November
NC0000663
0
1.3 1
0
December
NC0000663
0
0.52
0
Totals:
Annual (dry
tons
0
9.29
0
', H 0 4
Amendments used: I
None
Bulkin Agent(s)
used: I
None
* If more space than given is required, please attach additional information sheet(s). ® Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. Rl Yes ® No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I cer 'fy, under penalty of law, that the above information is, to the best of 'my knowledge and belief, true, accurate and complete. I ani aware
t ere si fic t penalties for submitting fal a inf rmation, inclu i e possibility of fine and imprisonment for knowing violations."
39
Signa a of Permittee Date Signature of P eparer* * Date
(if different from Permi ee) * *Preparer is defined in 40 CFR Part 503.9(r)
nFNR FORM nm.,;nF ti /9nn.ri1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this, form.
Permit Number: WQ0018087
Facility Name: DAK Americas LLC, Cape Fear Site
NPDES # or NC0000663
WQ#:
WWTP Name: DAK Americas LLC, Cape Fear Site
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
5)
Environmental Chemist
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significantpenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prep Date
DENR FORM RSSF (5/2003)
Sample or
Composite Date
5 M 19 174
Breffi 101TO", Me
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significantpenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prep Date
DENR FORM RSSF (5/2003)

Environmental Chemists, Inc.
6602 Windmill Way - Wilmington, NC 28405
[phone] (Lab) - (910) 3924424 (Fax)
® 710 Bowsertown Road - Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DES CERTIFICATE #37729
DAK Americas Date of Report: Jan 27, 2014
Post Office Box 2260 Customer PO #:
Leland NC 28451 Report #: 2014-00768
Attention: Larry Young Report to: Larry Young
Project ID: Aerobic Digester
Lata ID Sample ID: Collect Date/Time Matrix Sampled by
14-01894 Site: Aerobic Digester 1/20/2014 10:45 AM Solid/Sludge Larry Young
Test Method Results Date Analyzed
Arsenic
EPA 240.7
<19.3 mg/kg
01/22/2014
Chromium
EPA 200.7
37.8 mg/kg
01/22/2014
Nickel
EPA 20D.7
93.1 mg/kg
01/22/2014
Total Solids (%}
SM 2540 a
0.45%
01 12 012 0 1 4
pH
SM 4800 H B
7.42 units
01/23/2014
Comment:- -Results,
except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
M011A Ok
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Report#:: 2014-00788 _ Pages I of 1

NCDEn' DWQ CaUffoateON, DLS Cedif ede1437119
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Wilmington, NC 28405
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PAA Acyuestea:

Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) 9 [phone](Fax)
© 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CETrPIFICATE #94. DIS CERTIRCATE #37729
DAK Americas
Date of Report:
May 05, 2014
Post Office Box 2260
Customer PO #:
EPA 200.7
Leland NC 28451
Report #:
2014-04703
Attention: Larry Young
Report to:
Larry Young
Total Solids (%}
Project ID:
0.47%
Lab ID Sample ID:
Collect DatelTime Matrix
Sampled by
14.11319 Site: Aerobic Digester
4/23/2014 11:00 AM Solid/Sludge
Larry Young
Test
Results - - Date Analyzed
Arsenic
EPA 200.7
<18.7 mg/kg
04/28/2014
Chromium
EPA 200.7
30.0 mg/kg
04/28/2014
Nickel
EPA 200.7
84.0 mg/kg
04128/2014
Total Solids (%}
SM 2540 a
0.47%
04/23/2014
pH
SM 4500 H e_
7.48 units
05/01/2014
- Comment: Results, except
pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
np�
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Repolitt 2014-04703 Page 1 of 1

Analytical & Consulting Chemists
NCDBMii DWQ Cett eate994, DLS Cerfficate#37779
Samule Colleefig � and Chain of Custody
Wilmington, NC 28405
Phone; (910) 392`0223
Fax: [phone]
4061, lJ •hranbi�s:a,i;;D.�asae�
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14-4-703
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Received 0,:D Date:
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Environmental Chemists,, Inc.
6602 Windmill Way '• Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIRCATE #94. DLS CERTIFICATE #37729
DAK.Americas Date of Report: Jul 29, 2014
3147 S. 17th Street Suite 300 Customer PO #:
Wilmington NC 28412 Customer ID: 08100044
Attention: Larry Young Report#: 2014-07967
Project ID: Aerobic Digester
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-19625 Site: Aerobic Digester 7/7/2014 9:00 AM Solid/Sludge Larry Young
Test Method Results Date Analyzed
Arsenic
-.-. EPA 2003
<15.0 mg/kg
07/22/2014 -
Chromium
EPA 200.7 -
<36.77 mg/kg
07/22/2014
Nickel
EPA 200.7
<35.77 mg/kg
07/22/2014
Total Solids (%)
_ SM rAD s
0.26%
07107/2014
pH
= SM 4600 tl s
7.77 units
07/10/2014
Comment:- - ---Results,-except
po ed
pH, reon a dry weight basis. pH reported on an as received basis.
C
Reviewed by:
/ Mo 110 / 0 '
Peport#:: 2014-07967 Page i of 1

NCALMa.s AWQ Certilientetl?d, DL5 Certtticnte$37779
Sample Collection. and Chain of Custody
Analytleal & Consulting Chemists
Wilmington, NC 28405
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DAK Americas Date of Report: Nov 04, 2014
3147 S. 17th Street Suite 300 Customer PO #:
Wilmington NC 28412 Customer ID: 08100044
Attention: Larry Young Report #: 2014-13120
Project ID: Wastewater
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
14-32249 Site: Aerobic Digester
10/23/2014 8:30 AM
Water Larry Young
Test
Method
Results Date Analyzed
Arsenic _. - --
EPA200.7--
<0.010 mg/L
10/29/2014
Chromium
EPA 200.7
0.027 mg/L
10/29/2014
Nickel
EPA 200.7
0.056 mg/L
10/29/2014
Total Solids
SM 2540 B -
<0.1 %
-10/24/2014
pH
SM 4500 H B
1.36 units
10/30/2014
Result estimated, below calibration range.
Comment: Results reported on 2n as received basis.
Reviewed by:

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Analytical & Consulting Chemists
NCDENR: DWQ CertiticuteH94, DLS Certificate 1137129
Sample Collection and Chain of Custody
AVilmington, NC 28405
P110 lie' [phone]
MIX: (91.0) 392-4424
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Environmental Chemists, Inc.
f 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729
OAK Americas
Date of Report: Oct 06, 2014
3147 S. 17th Street Suite 300
Customer PO #:
Wilmington NC 28412
Customer ID: 08100044
Attention: Larry Young
Report #: 2014-10214
Project ID: Aerobic Digester
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-25082 Site: Aerobic Digester
8/20/2014
8:40 AM Solid/Sludge Larry Young
Test
Method
Results Date Analyzed
Total Solids (%) _
SM 2540 s =- , .
0.17%
08/21/2014
Chlordane
Sw846 Method 8oS1BM510
<0.05 mg/L
08/23/2014
Endrin
SW846 Method 80S1 M510
<0.0005 mg/L
08/23/2014
Heptachlor
sw 846 Method eosmwio
<0.0005 mg/L
08/23/2014
Heptachlor epoxide -
Sw 846 Method 80S1 BI3510
<0.0005 mg/L
08/23/2014
Lindane
Sw 646 Method 80818/3510
<0.0005 mg/L
08/23/2014 -
Methoxychlor
SW W Method 80818/3510
<0.0005 mg/L
08/23/2014
Toxaphene
SW 846 Method 80818/3510
<0.05 mg/L
08123/2014
1,4 -Dichlorobenzene (TCLP)
SW 646 method 8276/3510
<0.050 mg/L
08/22/2014
2,4,5 -Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
08/22/2014
2,4,6 -Trichlorophenol (TCLP)
SW846 method 8270/3510
<0.050 mg/L
08/22/2014
2,4-Dinitrotoluene (TCLP)
SwU6 method 8270/3510
<0.050 mg/L
08/22/2014
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
0812.212014
Hexachloro-l;3-butadiene (TCLP)
SW 646 method 627013510
<0.050 mg/L
08/22/2014
Hexachlorobenzene (TCLP)
Sw846 method 8270r3510
<0.050 mg/L
08/22/2014
Hexachloroethane (TCLP)
Sw 646 method 8270/3510
<0.050 mg/L
08/22/2014
m + p -Cresol (TCLP)
sw W method 8276/3510
<0.050 mg/L
08/22/2014
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
08/22/2014
o -Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
08/22/2014
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
08/2212014
Pyridine (TCLP)
SW 646 method 827013510
<0.050 mg/L
08/22/2014
1,1-Dichloroethylene
SW846 Method S26o/5030
< 0.01 mg/L
9/13/2014
1,2-Dichloroethane
Swe46 Method 8260/5030
< 0.01 mg/L
9/13/2014
Benzene
SWM Method 8260/5030
< 0.01 mg/L
9/13/2014
Carbon Tetrachloride
SW846 Method 82WIW30
< 0.01 mg/L
9/13/2014
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg1L
9/13%2014
Report # : 2014-10214 Page 1 of 2

Environmental Chemists, Inc.
env
6602 WindmillWay • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE 437729
DAK Americas
3147 S. 17th Street Suite 300
Wilmington NC 28412
Attention: Larry Young
Chloroform
Methyl ethyl ketone
Tetrachloroethylene
Trichloroethylene
Vinyl Chloride
RCI
Cyanide
pH
Sulfide
Ignitability
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
Date of Report: Oct 06, 2014
Customer PO #:
Customer ID: 08100044
Report #: 201410214
Project ID: Aerobic Digester
SW846 Method 626015030
< 0.01 mg/L
9/13/2014
SWM Method 8260/5030
< 0.05 mg/L
9/13/2014
SW846 Method OMOS030
< 0.01 mg/L
9/13/2014
SWM Method 826015030
< 0.01 mg/L.
.9/13/2-014
SW846'Method 828015030
< 0.01 mg/L
9/13/2014
EPA 3WA
<0.124 mg/kg
09/11/2014
SM4500 H B
8.14 units
08/27/2014
SM 4500 S D .- _ .
<0.248 mg/kg
08/26/2014
SW 846 method 1010
>212 OF
08/29/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA200.7
<0.100 mg/L
08/25/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA 200.7
<0.100 mg/L
08/25/2014
EPA 245.1
<0.0020 mg/L
08/27/2014
Comment RCI reported on an as received basis.
Reviewed
Report #.: 2014-10214 Page 2 of 2

Maw
HCDEiYikt DWQ Certiticatef{9q, DLS CetiiQcntefP37719
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AnalyticaI & Cansuiting Chemists
Wilmington, NC x8405
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DAK Americas LLC 2.015 Current Year
Cape, Fear Site 1984 Year Spray Fields were discontinued
3500 Daniels Road, N.E. 1974 Year Sludge Lagoon was constructed
Leland, NC 28451 12 Acreage of 12 -acre lagoon
Permit No. WQ0018087
12 -acre Sludge Lagoon Capacity :
Assume 0 inch freeboard
Elevations
Date
1
2
Base
Sludge
Top of
Levee
Space
Available
Rate of Sludge
Accumulation
(Estimate)
Remaining
Useful Disposal
Life (Estimate)
Cumulative
Volume
Remaining
Volume
Low
High
Low
High
ft
ft
ft
in
in/year
in/year
yr
yr
yd3
yd3
1 08/03/2006
22.5
30.4
31.2
9.2
3.0
4.3
2.1
3.1
152,945
14,849
2 11/07/2006
22.5
30.5
31.2
8.0
3.0
4.4
1.8
2.7
- 154,881
12,913
3 05/08/2007
22.5
- 30.2.
- =:31.2
-12.0
2.8
4.0
-.3.0
4.3
-149,073
19,360
4 02/04/2008
22.5
30.2
31.2
, 12.0
2.7
3.9
3.1
4.4
149,073
19,360
5 07/30/2008
22.5
30.9
31.2
3.9
3.0
.4.2
0.9
1.3
162,141
6,292
3 "12/05/2008
22.5
30.4
31.2
10.2
2.8
3.9
2.6
3.7
151,977
16,456
7 04/07/2009
22.5
30.6_
31.2
6.8
2.8
3.9,
1.8
2.5
157,397
11,035
3 10/09/2009
22.5
30.4
31.2
9.6
2.7
3.8
2.5
3.5
152,945
15,488
a 01/14/2010
22.5
30.6'
31.2
7.2
2.7
3.7
1.9
2.7
156,817
11,616
0 10/08/2010
22.5
31.4
35.4
48.8
3.0
4.1
11.9
16.5
171,724
78,796
02/18/2011
22.5
31.0
35.4
52.9
2.8,
3.8
14:0
19.1
165,114
85,406
06/15/2011
22.5
31.1
35.4
-52.6
2.8
3.8
13.8
19.0
=165,667
84,852
12/30/2011
22.5
31.0
35.4
.53.3
2.8
.3.8
14.1
19.3
164,561
85,959
03/23/2012
22.5
30.9
35.4
.55.0
2.6
3.6
;15.4
20.8
161,795
88,724
06/26/2012
22.5
30.8
35.4
55.9
2.6
3.6.
15.7
21.3
160,412
90,107
10/12/2012
22.5
31.2
35.4
50.5
2.8
3.7
13.5
18.3
168,986
,81,534
12/14/2012
22.5
31.0
35.4
53.1
2.7
3.6
14.6
19.8
164,837
,85,682
03/28/2013
22.5
31.1
35.4
51.9
2.7
3.6
14.6
19.6
166,773
83,746
12/23/2013
22.5
31.3
35.4
", 49.2
2.7
3.6
13.5,
18.2
170,369
79,376
03/10/2014
22.5
31.1
35.4
51.3
2.6
3.4
14.9
19.9
166,912
82,833
06/05/2014
22.5
31.2
35.4
'50.5
0.25
0.50
-101.0
202.1
168,239
81,506
09/15/2014
22.5
31.5
35.4
'46.8
0.25
0.50
93.6
187.1
174,268
75,477
12/10/2014
_22.5
31.3
35.4
49.6
0.25
0.50
99.2
198.4
169,733
80,012