WQ0014885_Residual Annual Report 2014_20150225

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HARNETT COUNTY WTP, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014885
2014 ANNUAL REPORT
RECEIVEDIDENRIDWR
• FEB 215 2015
wabPQuell
PefMitung se bon

11
•
Barnett County WTP, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00014885 County Harnett Year 2014
Facility Name (as shown on permit) Hamett County Utilities Regional WTP PWS ID No. 00-076-84
• Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 626.84
Total number of acres utilized for land application during the year: 123.8
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . 1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, incl ding th possibility of fines and imprisonment for
knowing violations." 2
Steve Ward Director of Public Utiliti s
7Permittee)
tpeyp it) Signa re of P rmittee Date
ignature o Date Signature of Land Applier Date
(if differen(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
C7

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
HARNETT CO. UTILITIES, NC
WARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
MONTHNEAR
April 2014
May 2014
June 2014
July 2014
August 2014
September 2014
October 2014
November 2014
December 2014
YEARLY TOTAL
•
AMOUNT UNIT DRY TONS UNIT
421,600.00
G
50.45
D
440,200.00
G
52.68
D
731,600.00
G
87.55
D
874,200.00
G
104.62
D
936,200.00
G
94.10
D
1,271,000.00
G
127.73
D
390,600.00
G
39.25
D
229,400.00
G
23.05
D
589, 000.00
G
47.41
D
5,883,800.00
G
626.84
D
DRY METRIC
TONS
45.77
47.78
79.42
94.90
85.33
115.84
35.60
20.91
43.00
2/10/2015

•
PROJECT:
FACILITY:
2014 ANNUAL REPORT
HARNETT CO. REGIONAL WTP
PWS PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
0
Harnett County, NC
Harnett County Regional WTP
310 West Duncan St
Lillington, NC 27546
910-893-7575
NC 00-076-84
Steve Ward
Director of Public Utilities
PO Box 759
Lillington, NC 27546
910-893-7575
Allan O'Briant, Superintendent (WTP)
310 West Duncan St
Lillington, NC 27546
910-893-7575
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

•
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885 Laboratory
Facility Name: HARNETT CO. UTILITIES, NC A&L Eastern Laboratories Inc.
NPDES# : NC0007684
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type
WPL
WPL
WPL
WPL
Date Sampled (grab) or 02/05/14
04/22/14
08/04/14
12/03/14
Date Composited
Percent Solids
2.74
2.87
2.41
1.93
PARAMETERS (mg/kg dry weight)
Arsenic
7
8
17
14
Cadmium
<2
<2
<2
<2
Mercury
<0.4
<0.4
<0.4
<0.4
Chromium
40
35
37
24
Copper
383
539
264
531
Lead
14
10
8
<5
Molybdenum
<5
<5
16
19
Nickel
17
17
17
13
Selenium
<5
<5
<5
<5
Zinc
136
361
276
180
Total Phosphorus
1860
1940
3550
3110
TKN
8760
9410
12000
15000
Ammonia -Nitrogen
1460
697
6640
2590
Nitrate and Nitrite
172
<2
<2
130
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and aluated the information submitted. I am aware that there are
significant penalties for submitting false infor including th ossibility of fines and imprisonment for knowing violations."
•
X � Date
(SIGNATURE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Tuesday - February 10, 2015 at 16:32:21 for: 2037 01

•
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885 Laboratory
Facility Name: HARNETT CO. UTILITIES, NC A&L Eastern Laboratories Inc.
NPDES# : NC0007684
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL WPL WPL WPL
Date Sampled (grab) or 02/05/14 04/22/14 08/04/14 12/03/14
Date Composited
Percent Solids 2.74 2.87 2.41 1.93
PARAMETERS (mglkg dry weight)
Aluminum
118000
113000
121000
115000
Calcium
3390
1320
2700
5930
Magnesium
1610
1600
1190
1120
pH
5.48
5.76
5.88
5.58
Potassium
1040
3140
628
568
Sodium
313
332
634
965
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluato the information submitted. I am aware that there are
significant pe_naltigs for.su�mitting faI§a!QformatioDjnaLuding the possiW of fines and imprisonment for knowing violations."
i'zrJ a
(SI TUR OF PREPARER)
NR - Data Not Reported or Data Not Required
•
Date
DENR FORM RSSF-B (7/2002) Printed: Tuesday - February 10, 2015 at 16:32:42 for: 2037 01

•
Page: 1 of 2
Report Number: 14-041-0201
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97848
Sample Id : HARNETT WTP
u A&L Eastern Laboratories, Inc.
4
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271,6446
wwwaleastem.COM
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 2/5/2014 09:00:00
Date Received: 02/10/2014 00:00
Date Reported: 02/12/2014
Total Solids *
2.74
27400
100.0
JM
02/10/2014 15:15
SM-2540G
Moisture *
97.26
100.0
JM
02/10/2014 15:15
SM-2540G
Total Kjeldahl Nitrogen
0.88
8760
10.0
JM
02/11/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
0.19
1860
100
KM
02/11/2014 11:31
SW 6010C
Total Potassium
0.10
1040
100
KM
02/11/2014 11:31
SW 6010C
Total Sulfur
0.97
9690
100
KM
02/11/2014 11:31
SW 6010C
Total Calcium
0.34
3390
100
KM
02/11/2014 11:31
SW 6010C
Total Magnesium
0.16
1610
100
KM
02/11/2014 11:31
SW 6010C
Total Sodium
0.03
313
100
KM
02/11/2014 11:31
SW 6010C
Total Iron
34400
100
KM
02/11/2014 11:31
SW 6010C
Total Aluminum
118000
100
KM
02/11/2014 11:31
SW 6010C
Total Manganese
916
5
KM
02/11/2014 11:31
SW 6010C
Total Copper
383
5
KM
02/11/2014 11:31
SW 6010C
Total Zinc
136
5
KM
02/11/2014 11:31
SW 6010C
Ammonia Nitrogen
0.15
1460
10.0
JM
02/11/2014 09:00
SM-4500-NH3C
Organic N
0.73
7300
10.0
02/11/2014 09:00
CALCULATION
Nitrate+Nitrite-N
172
2.00
JM
02/11/2014 09:00
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
02/11/2014 11:31
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. (/��i'
Alza
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , L. 69
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

•
Page: 2 of 2
Report Number: 14-041-0201
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97848
Sample Id : HARNETT WTP
•
A&L Eastern Laboratories, Inc.
7621 Whftepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 2/5/2014 09:00:00
Date Received: 02/10/2014 00:00
Date Reported: 02/12/2014
Total Chromium
40
5
KM
02/11/2014 11:31
SW 6010C
Total Nickel
17
5
KM
02/11/2014 11:31
SW 6010C
Total Lead
14
5
KM
02/11/2014 11:31
SW 6010C
Total Arsenic
7.0
3.0
KM
02/11/2014 11:31
SW 6010C
Total Mercury
<0.4
0.4
KM
02/11/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
02/11/2014 11:31
SW 6010C
pH (Standard Units) 5.48
2.00
JM
02/11/2014 09:00
SW-9045D
Total Molybdenum
<5
5
KM
02/11/2014 11:31
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE
PURPOSES.
QUALIFIER: THE LRB AND MATRIX SPIKE WERE OUT OF LIMITS FOR "NO3/NO2-N".
THE MATRIX SPIKE WAS
OUT OF LIMITS FOR "Al", "Fe",
AND "Se".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SAMf?Ll.NG LOG #
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REMARKS:
Dait Trrre
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For. .... monitoring, purposes, PO#:.
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Sodium Absorption Ratio Calculation (SAR)
0
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 2/5/2014 1/112014-3131/2014 0.1828
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (313 x 2.7400) = 100 = 8.5762
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (3390 x 2.7400) _ 100 = 92.886
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1610 x 2.7400) =100 = 44.114
Na meq = Na mg/I _ Molec.Wgt.Na = 8.5762 = 23 = 0.372878
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 92.886 = 20 = 4.6443
Mg meq = Mg mg/I = Molec.Wgt.Mg = 44.114 + 12 = 3.67617
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.372878 = SgrRoot[0.5(4.6443+3.67617)] = 0.182813
•
Printed: 2/10/2015
Page 1 16:33

•
Page: 1 of 2
Report Number: 14-115-0203
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55029
Sample Id : HARNETT WTP
Y A&L Eastern Laboratories, lnc.
` 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W6
wwwaleastem.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/22/2014 11:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Solids *
2.87
28700
100.0
JM
04/25/2014 14:30
SM-2540G
Moisture *
97.13
100.0
JM
04/25/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
0.94
9410
10.0
JM
04/28/2014 09:40
SM-4500-NH3C-TKN
Total Phosphorus
0.19
1940
100
KM
04/28/2014 13:09
SW 6010C
Total Potassium
0.31
3140
100
KM
04/28/2014 13:09
SW 6010C
Total Sulfur
1.04
10400
100
KM
04/28/2014 13:09
SW 6010C
Total Calcium
0.13
1320
100
KM
04/28/2014 13:09
SW 6010C
Total Magnesium
0.16
1600
100
KM
04/28/2014 13:09
SW 6010C
Total Sodium
0.03
332
100
KM
04/28/2014 13:09
SW 6010C
Total Iron
25500
100
KM
04/28/2014 13:09
SW 6010C
Total Aluminum
113000
100
KM
04/28/2014 13:09
SW 6010C
Total Manganese
1210
5
KM
04/28/2014 13:09
SW 6010C
Total Copper
539
5
KM
04/28/2014 13:09
SW 6010C
Total Zinc
361
5
KM
04/28/2014 13:09
SW 6010C
Ammonia Nitrogen
0.07
697
10.0
JM
04/28/2014 09:40
SM-4500-NH3C
Organic N
0.87
8713
10.0
04/28/2014 09:40
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/28/2014 09:40
SM-450ONO3F ,
Total Cadmium
<2.0
2.0
KM
04/28/2014 13:09
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , A&UM9
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-115-0203
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55029
Sample Id : HARNETT WTP
•
A&L Eastern Laboratories, Inc.
V
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/22/2014 11:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Chromium
35
5
KM
04/28/2014 13:09
SW 6010C
Total Nickel
17
5
KM
04/28/2014 13:09
SW 6010C
Total Lead
10
5
KM
04/28/2014 13:09
SW 6010C
Total Arsenic
8.0
3.0
KM
04/28/2014 13:09
SW 6010C
Total Mercury
<0.4
0.4
KM
04/28/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/28/2014 13:09
SW 6010C
pH (Standard Units)
5.76
2.00
JM
04/28/2014 09:40
SW-9045D
Total Molybdenum
<5
5
KM
04/28/2014 13:09
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
ron-77-3usn. P

Sodium Absorption Ratio Calculation (SAR)
0
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 4/22/2014 411/2014-7/3112014 0.2449
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (332 x 2.8700) _ 100 = 9.5284
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (1320 x 2.8700) + 100 = 37.884
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1600 x 2.8700) =100 = 45.92
Na meq = Na mg/I _ Molec.Wgt.Na = 9.5284 _ 23 = 0.414278
Ca meq = Ca mg/I + Molec.Wgt.Ca = 37.884 _ 20 = 1.8942
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 45.92 = 12 = 3.82667
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg .meq)] = 0.414278 _ SgrRoot[0.5(1.8942+3.82667)] = 0.244949
C,
Printed: 2/10/2015
Page 1 16:33

•
Page: 1 of 2
Report Number: 14-218-0209
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56876
Sample Id: HARNETT
A&L EasternLaboratories, Inc.
@P.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-WG
wwwaleastem.com
Project: HARNETT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/4/2014 11:13:00
Date Received: 08/06/2014 00:00
Date Reported: 08/11/2014
Total Solids *
2.41
24100
100.0
MW
08/07/2014 07:59
SM-2540G
Moisture *
97.59
100.0
MW
08/07/2014 07:59
SM-2540G
Total Kjeldahl Nitrogen
1.20
12000
10.0
MW
08/07/2014 08:15
SM-4500-NH3C-TKN
Total Phosphorus
0.36
3550
100
KM
08/07/2014 11:58
SW 6010C
Total Potassium
0.06
628
100
KM
08/07/2014 11:58
SW 6010C
Total Sulfur
1.25
12500
100
KM
08/07/2014 11:58
SW 6010C
Total Calcium
0.27
2700
100
KM
08/07/2014 11:58
SW 6010C
Total Magnesium
0.12
1190
100
KM
08/07/2014 11:58
SW 6010C
Total Sodium
0.06
634
100
KM
08/07/2014 11:58
SW 6010C
Total Iron
20500
100
KM
08/07/2014 11:58
SW 6010C
Total Aluminum
121000
100
KM
08/07/2014 11:58
SW 6010C
Total Manganese ,
2590
5
KM
08/07/2014 11:58
SW 6010C
Total Copper
264
5
KM
08/07/2014 11:58
SW 6010C
Total Zinc
276
5
KM
08/07/2014 11:58
SW 6010C
Ammonia Nitrogen
0.66
6640
10.0
MW
08/07/2014 08:15
SM-4500-NH3C
Organic N
0.54
5360
10.0
08/07/2014 08:15
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
MW
08/07/201414:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
08/07/2014 11:58
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-218-0209
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56876
Sample Id: HARNETT
@go
A&L EasternLaboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: HARNETT
NC CERT#257
REPORT OFANALYSIS Date Sampled: 8/4/2014 11:13:00
Date Received: 08/06/2014 00:00
Date Reported: 08/11/2014
Total Chromium
37
5
KM
08/07/2014 11:58
SW 6010C
Total Nickel
17
5
KM
08/07/2014 11:58
SW 6010C
Total Lead
8
5
KM
08/07/2014 11:58
SW 6010C
Total Arsenic
17.0
3.0
KM
08/07/2014 11:58
SW 6010C
Total Mercury
<0.4
0.4
KM
08/07/2014 14:00
SW-7471 B
Total Selenium
5.0
5.0
KM
08/07/2014 11:58
SW 6010C
pH (Standard Units)
5.88
2.00
MW
08/07/2014 08:19
SW-9045D
Total Molybdenum
16
5
KM
08/07/2014 11:58
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As", ALL OTHER QUALITY CONTROL WAS WITHIN LIMITS.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart; nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

Sodium Absorption Ratio Calculation (SAR)
i
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 8/4/2014 811/2014-11/30/2014 0.3955
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (634 x 2.4100) + 100 = 15.2794
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (2700 x 2.4100) + 100 = 65.07
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1190 x 2.4100) + 100 = 28.679
Na meq = Na mg/I + Molec.Wgt.Na = 15.2794 + 23 = 0.664322
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 65.07 + 20 = 3.2535
Mg meq = Mg mg/I + Molec.Wgt.Mg = 28.679 + 12 = 2,38992
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.664322 + SgrRoot[0.5(3.2535+2.38992)] = 0.395478
Printed: 2/10/2015
Page 1 16:33

•
Page: 1 of 2
Report Number: 14-343-0202
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59147
Sample Id: HARNETT WTP
99, A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/3/2014 14:00:00
Date Received: 12/09/2014 00:00
Date Reported: 12/16/2014
Total Solids *
1.93
19300
100.0
JM
12/09/2014 15:00
SM-254OG
Moisture *
98.07
100.0
JM
12/09/201415:00
SM-2540G
Total Kjeldahl Nitrogen
1.50
15000
10.0
JM
12/15/2014 09:04
SM-4500-NH3C-TKN
Total Phosphorus
0.31
3110
100
KM
12/10/2014 12:07
SW 6010C
Total Potassium
0.06
568
100
KM
12/10/2014 12:07
SW 6010C
Total Sulfur
1.39
13900
100
KM
12/10/2014 12:07
SW 6010C
Total Calcium
0.59
5930
100
KM
12/10/2014 12:07
SW 6010C
Total Magnesium
0.11
1120
100
KM
12/10/2014 12:07
SW 6010.0
Total Sodium
0.10
965
100
KM
12/10/2014 12:07
SW 6010C
Total Iron
13000
100
KM
12/10/2014 12:07
SW 6010C
Total Aluminum
115000
100
KM
12/10/2014 12:07
SW 6010C
Total Manganese
1140
5
KM
12/10/2014 12:07
SW 6010C
Total Copper
531
5
KM
12/10/2014 12:07
SW 6010C
Total Zinc
180
5
KM
12/10/2014 12:07
SW 6010C
Ammonia Nitrogen
0.26
2590
10.0
JM
12/11/2014 08:39
SM-4500-NH3C
Organic N
1.24
12410
10.0
12/11/2014 08:39
CALCULATION
Nitrate+Nitrite-N
130
2.00
JM
12/10/2014 08:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
12/10/2014 12:07
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

E
Page: 2 of 2
Report Number: 14-343-0202
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59147
Sample Id : HARNETT WTP
•
AFL Eastern Laboratories, Inc.
@P. 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/3/2014 14:00:00
Date Received: 12/09/2014 00:00
Date Reported: 12/16/2014
Total Chromium
24
5
KM
12/10/2014 12:07
SW 6010C
Total Nickel
13
5
KM
12/10/2014 12:07
SW 6010C
Total Lead
<5
5
KM
12/10/2014 12:07
SW 6010C
Total Arsenic
14.0
3.0
KM
12/10/2014 12:07
SW 6010C
Total Mercury
<0.4
0.4
KM
12/11/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
12/10/2014 12:07
SW 6010C
pH (Standard Units) " 5.58
2.00
JM
12/10/2014 08:24
SW-9045D
Total Molybdenum
19
5
KM
12/10/2014 12:07
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "TKN".
THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Fe",
"Mg", AND "P". ALL OTHER QC DATA
IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
0-
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 12/3/2014 1211/2014-12/31/2014 0.4175
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (965 x 1.9300) _ 100 = 18.6245
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (5930 x 1.9300) =100 = 114.449
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1120 x 1.9300) = 100 = 21.616
Na meq = Na mg/I _ Molec.Wgt.Na = 18.6245 = 23 = 0.809761
Ca meq = Ca mg/I t- Molec.Wgt.Ca = 114.449 _ 20 = 5.72245
Mg meq = Mg mg/I = Molec.Wgt.Mg = 21.616 _ 12 = 1.80133
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.809761 = SgrRoot[0.5(5.72245+1.80133)] = 0.417497
Printed: 2/10/2015
Page 1 16:33

0-
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HAROLD DIXON
SITE #: NC HA OOOX8 FIELD# : HA OOOX8 0009
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00014885 ANNUAL DRY TONS APPLIED: 50.46
OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 22.90 ACRES PERMITTED: 22.90
Page : 1
Lime Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/25/14
198,400.00 (G)
8663.755
2.87
1.037
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093
BERMUDAGRASS
4/26/14
223,200.00 (G)
9746.725
2.87
1.166
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093
BERMUDAGRASS
Apr-14 1
421,600.00 (G)
1 18,410.480
Total Gallons/Ac: 18,410.48
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual Ibs/acre 9
0.035 0.009 0.154 2.375 0.044 0.002 0.022 0.075 0.022 1.591 8.55
Cumulative lbs/acre 0.035 0.009 0.154 2.375 0.044 0.002 0.022 0.075 0.022 1.591
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
` "
165
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8ME
1339.0
267.9
15.0
375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
ar
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

•
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETT COUNTY
SITE #: NC HA OOX43 FIELD# : HA OOX43 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 436.15
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
•
Page : 1
Lune Applied *'*
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dr,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (W1) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pprn)
Crop
MONTH
Total
Per Acre
Solids
7/7/14
124,000.00 (G)
3155.216
2.87
0.378
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.Op
697.00 p
2.00 p
2093 I
BERMUDAGRASS
7/8/14
80,600.00 (G)
2050.891
2.87
0.245
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093 Ij
BERMUDAGRASS
7/9/14
37,200.00 (G)
946.565
2.87
0.113
HCUCOHV
DRY
0-<I/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093 I
BERMUDAGRASS
7/10/14
93,000.00 (G)
2366.412
2.87
0.283
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093
BERMUDAGRASS
7/11/14
124,000.00 (G)
3155.216
2.87
0.378
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.O p
697.00 p
2.00 p
2093
BERMUDAGRASS
7/25/14
229,400.00 (G)
5837.150
2.87
0.699
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093
BERMUDAGRASS
7/26/14
186,000.00 (G)
4732.824
2.87
0.566
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.O,p
697.00 p
2.00 p
2093
BERMUDAGRASS
Jul-14
874,200.00 (G)
22,244.274
8/6/14
18,600.00 (G)
473.282
2.41
0.048
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
8/7/14
111,600.00 (G)
2839.695
2.41
0.285
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
8/8/14
111,600.00 (G)
2839.695
2.41
0.285
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394 I
BERMUDAGRASS
8/12/14
148,800.00 (G)
3786.260
2.41
0.381
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394 I
BERMUDAGRASS
8/13/14
155,000.00 (G)
3944.020
2.41
0.396
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394 I
BERMUDAGRASS
8/28/14
198,400.00 (G)
5048.346
2.41
0.507
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
Ij BERMUDAGRASS
8/29/14
192,200.00 (G)
4890.585
2.41
0.491
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
Aug-14
936,200.00 (G)
23,821.883
9/3/14
142,600.00 (G)
3628.499
2.41
0.365
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
I BERMUDAGRASS
9/4/14
161,200.00 (G)
4101.781
2.41
0.412
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
I BERMUDAGRASS
9/5/14
179,800.00 (G)
4575.064
2.41
0.460
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
I BERMUDAGRASS
9/6/14
74,400.00 (G)
1893.130
2.41
0.190
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
9/11/14
210,800.00 (G)
5363.868
2.41
0.539
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
I BERMUDAGRASS
9/12/14
136,400.00 (G)
3470.738
2.41
0.349
HCUCOHV
MOIST
0-<I/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
9/29/14
204,600.00 (G)
5206.107
2.41
0.523
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
9/30/14
161,200.00 (G)
4101.781
2.41
0.412
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
Sep-14
1,271,000.00 (G)
32,340.968
10/23/14
229,400.00 (G)
5837.150
2.41
0.587
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
10/24/14
161,200.00 (G)
4101.781
2.41
0.412
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
Oct-14
390,600.00 (G)
9,938.931
11/25/14
229,400.00 (G)
5837.150
2.41
0.587
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
12,000. p
6,640.00 p
2.00 p
4394
BERMUDAGRASS
Nov-14
229,400.00 (G)
5,837.150
12/1/14
136,400.00 (G)
3470.738
1.93
0.279
HCUCOHV
DRY
0- 1/2"
SUR
0.5
0.20
15,000. p
2,590.00 p
130.00 p
3907
I BERMUDAGRASS
12/17/14
241,800.00 (G)
6152.672
1.93
0.495
HCUCOHV
DRY
0-<I/2"
SUR
0.5
0.20
15,000. p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
12/18/14
210,800.00 (G)
5363.868
1.93
0.432
HCUCOHV
DRY
0-<I/2"
SUR
0.5
0.20
15,000. p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
Dec-14
589,000.00 (G)
14,987.278

•
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETT COUNTY
SITE #: NC HA 0OX43 FIELD# : HA 0OX43 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: W00014885 ANNUAL DRY TONS APPLIED: 436.15
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
•
Page : 2
Lime Applied ***
Date LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
T Per Acre
Solids
Total Gallons/Ac: 109,170.48
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
84
Annuallbs/acre
0.322
0.044
0.779
7.968
0.181
0.009
0.304
0.368
0.111
6.347
69.16
Cumulative lbs/acre
0.322
0.044
0.181
0.009
0.368
0.111
6.347
0.779
7.968
0.304
Permit PAN Limit (lbslacre) 1st Crop/2 nd Crop
��
€
ME
147
g
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0 r x �
i
'4
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
X 2-17-
%.11
(SIGNATUROF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hnjection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

•
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: JAMES FARRAR
SITE #: NC HA OX124 FIELD# : HA OX124 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GILEAD
PERMIT #: NC-HA-X124 ANNUAL DRY TONS APPLIED: 113.53
OPERATOR: JAMES FARRAR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90
Page : I
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/22/14
248,000.00 (G)
9219.331
2.87
1.103
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.Op
697.00 p
2.00 p
2093
I BERMUDAGRASS
5/23/14
192,200.00 (G)
7144.981
2.87
0.855
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.Op
697.00 p
2.00 p
2093
BERMUDAGRASS
May-14
440,200.00 (G)
16,364.312
6/20/14
279,000.00 (G)
10371.747
2.87
1.241
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.Op
697.00 p
2.00 p
2093
I BERMUDAGRASS
6/23/14
192,200.00 (G)
7144.981
2.87
0.855
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,410.Op
697.00 p
2.00 p
2093
I BERMUDAGRASS
6/24/14
37,200.00 (G)
1382.900
2.87
0.166
HCUCOHV
MOIST
0-<I/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
2093
BERMUDAGRASS
Jun-14
508,400.00 (G)
18,899.628
Total Gallons/Ac: 35,263.94
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.068
0.017
0.295
4.550
0.084
0.003
0.042
0.143
0.042
3.047 16.37
18
Cumulativelbs/acre
0.068
0.017
1 0.295
1 4.550
0.084
0.003
0.042
0.143
0.042
3.047
�.
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
,;°
1
�� z C
`�u .
n
i,"r ..,X 'n.
r;,ie�#' „^ d ;r" `kt
��, t�
°'•�'
_ 3•..sA".ek•`=
160
x>w.":
d
Via; -
;,"� �
-
FD Cumulative Pollutant LoadingRate Limit Ibs/acre�J
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
X
m
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: . Surface 0.5, Injection/Incorporation 1.0
" Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

L
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: JAMES FARRAR
SITE #: NC HA OX124 FIELD# : HA OX124 0006
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GILEAD
PERMIT #: NC-HA-X124 ANNUAL DRY TONS APPLIED: 26.71
OPERATOR: JAMES FARRAR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 34.70 ACRES PERMITTED: 34.70
•
Page: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Are
Solids
6/4/14
223,200. 00 (G)
6432.277
2.87
0.770
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
9,410.0 p
697.00 p
2.00 p
F 2 993
BERMUDAGRASS
Jun-14
1 223,200.00 (G)
1 6,432.277
1
Total Gallons/Ac: 6,432.28
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.012
0.003
0.054
0.830
0.015
<.001
0.008
0.026
0.008
0.556 2.99
3
Cumulative lbs/acre
0.012
0.003
0.054
0.830
0.015
<,001
0.008
0.026
0.008
0.556
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop„
M
160
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 11 ��
375.0
89.0
2500.0 = 0-4
+ ° a , .
- E5,,,ssF
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
X
42
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hmcorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

Summit Environmental Technologies, Inc.
MSUMMOOF 3310 Win St.
EN k' I RO H hi F N TAL TECH N10.Lt7LIiES; INN Cuyahoga Falls, Ohio 44223
nit�r2zCo1"L Ra F3tpt1G TEL: [phone] FAX. • [phone]
Website: hM2.1Avivw.se11ek.com
February 18, 2014
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Harnett WTP
Order No.: 14020583
Dear Will Varner:
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/10/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
•

•
is
Summit Environmental Technologies, Inc.
ffl�zummmar 3310 Win St.
El' VIROMMEi�c5, �P1C. Cuyahoga Falls, Ohio 44223
r3cill "ii1lri1t l TEL: [phone] FAX. • [phone]
Website: &W.-I/www.settelccant
CLIENT: Synagro
Project: Harnett WTP
Lab SampleID Client Sample ID
14020583-001 Hamett WTP
Tag No Date Collected
2/5/2014 9:00:00 AM
Workorder
Sample Summary
WO#: 14020583
18-Feb-14
Date Received Matrix
2/10/2014 9:50:00 AM Sludge

40 _ Summit Environmental Technologies, Inc.
Case Narrative
3310 Win St.
fidV1 �f1t�9Ei Ti L C CHt 6L�' das' INC. Cuyahoga Falls, Ohio 44223 WO#: 14020583
` rtW,yc dRi oraipr TEL: [phone] FAX. [phone]
Website: htty.1Avww.settek.con: Date: 2/18/2014
CLIENT: Synagro
Project: Harnett WTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
L

V Summit Environmental Technologies, Inc. WO#: 14020583
3310 Win St.
b`4PIdt4fd�et3dTAL tti6 �t ti"Glee �fiC Cuyahoga Falls, Ohio 44223 Date Reported: 2/18/2014
"' eQstal flcal 1latsa�lorl6 TEL: [phone] FAX. [phone] Company: Synagro
Website: httP.11www.settekcom Address: 284 Boger Rd.
Mocksville NC 27028
Received: 2/10/2014
Project#: Harnett WTP
TCLP Metals Analysis (6010)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Harnett WTP 001 2/5/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 2/14/2014 WK
Harnett WTP 001 2/5/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 2/14/2014 WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Harnett WTP 001 2/5/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 2/14/2014 ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harnett WTP
001
2/5/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
2/14/2014
JBN
Harnett WTP
001
2/5/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
2/14/2014
JBN
Harnett WTP
001
2/5/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
2/14/2014
JBN
Harnett WTP
001
2/5/2014
gamma-BHC
0.6020
ND mg/L
Sludge
EPA 8081 B
1
0.40
2/14/2014
JBN
Harnett WTP
001
2/5/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/14/2014
JBN
Harnett WTP
001
2/5/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/14/2014
JBN
Harnett WTP
001
2/5/2014
Methoxychlor
0.0020
-ND mg/L
Sludge
EPA 8081 B
1
10
2/14/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harnett WTP
001
2/5/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70 .
2/14/2014
MES
Harnett WTP
001
2/5/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/14/2014
MES
Harnett WTP
001
2/5/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/14/2014
MES
Harnett WTP
001
2/5/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/14/2014
MES
Harnett WTP
001
2/5/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
2/14/2014
MES
Harnett WTP
001
2/5/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
2/14/2014
MES
Harnett WTP
001
2/5/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
2/14/2014
MES
Harnett WTP
001
2/5/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/14/2014
MES
Harnett WTP
001
2/5/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
2/14/2014
MES
Harnett WTP
001
2/5/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
2/14/2014
MES
1�
u

Summit Environmental Technologies, Inc.
WO#:
14020583
3310 Win St.
OFdvIRQ3ttF�i�2�'I�AL l c4it Ot i l S, inG
C aho a Falls, Ohio 44223
uy g
Date Reported:
2/18/2014
. Arr a€f�af al wucratomeii
TEL: [phone] FAX. • [phone]
Company:
Synagro
Website: htty.1Avww.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
2/10/2014
Project#:
Harnett WTP
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harnett WTP
001
2/5/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
2/14/2014
AKE
Harnett WTP
001
2/5/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
2/14/2014
AKE
Harnett WTP
001
2/5/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
2/14/2014
AKE
Harnett WTP
001
2/5/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
2/14/2014
AKE
butadiene
Harnett WTP
001
2/5/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
2/14/2014
AKE
Harnett WTP
001
2/5/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
2/14/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harnett WTP
001
2/5/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
2/14/2014
AMZ
Harnett WTP
001
2/5/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
2/14/2014
AMZ
0

sm"My
Summit Environmental Technologies, Inc.
in St
3310 Win St.sCuyahoga
WO#: 14020583
ef-t
IRC9EM INCiNC
Falls, Ohio .Date
Reported: 2/18/2014
/,tr;�l �t,szly a
TEL: [phone] FAX. [phone]
Company: Synagro
Website: http://`viviv.settek.com
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 2/10/2014
Project#: Harnett WTP
Client ID#
Lab ID# Collected Analyte
Result Units
Matrix Method DF RL
Run Analyst
Harnett WTP
001 2/5/2014
Flashpoint (140°F)
>200 °F
Sludge EPA 1010 1
2/12/2014 TJR
Harnett WTP
001 2/5/2014
Cyanide, Reactive
ND ppm
Sludge EPA 9014 1 0.50
2/11/2014 TIR
Harnett WTP
001 2/5/2014
pH
5.0 s.u.
Sludge EPA 9045 D 1
2/10/2014 AYS
Harnett WTP
001 2/5/2014
Sulfide, Reactive
ND ppm
Sludge EPA 9034 1 25
2/11/2014 TIR
0

Summit Environmental Technologies, Inc. Analysis Request/Chain of Custody
3310 Will Street For Su nimit Env iron mentallechnologgics, Inc. use only
CLIY�&Ogil Falk,•Ohio, 44223 Tel: [phone] Fdx: 330.253.448.9 Page - of- I SU No,
Coinp:my Nallic (Please print}
Prqject Nanic
AItilij'tiCal'Param6tei-s",and'Metliod's
57j/
ComiYany Addv(Ss
FrOJCCt AU(IrCS'S
lot
4-�
.Client
L
Client Fax No. �UJM- El
Po#
4,
Client Etnail Pim"mail Re"witsZ Lj,Quote'No.
Contact lk-n-()n
—Ps
Sampled bv
Ched, if Ohh) VA
CA
.0
E,
A
Date
limp
�ampleldenfirjcatitm
Coilecteil
Collectod"A'
MEN
Cam..............
NP-MMME
NONE
NEON
�i
■
iiiiiiiiiiiiiii
I Man
Received in'tab,kv: Rush tiequested-1ky. Must tv. approved
by lab-vnaaiigcr
White and yellompagas should ac6urnpanys.,unpleN 96 the laboratory. The client page.
1 .8

•
Rev. 12
Date: 07/27/13
Summit Environmebtai Technologies, Inc.
Cooler Receipt Form
Initials of person inspecting cooler and samples: y�
Client:_ _ � ri�t
Order Number:
tt d r 1
Dale Received �' t. `. Time Receved:'� ' `! Date cooler(s) opened and samples inspected L%IIC.� t ) i
Number of Co lerslBo s.�
N/A
Shipper: FED EX 6 DHL Airborne US Postal Walk-in Pickup Other;
r
Packaging: Peanuts Btbble Wrap
Paper Foam None Other'.
Tape on cooleribox:
N N/A
Custody Seals intact
ILY) N NA
C-O-C in plastic
N N/A
Ice Btue,ice
present I absent / melted ° N/ 4
Sample Temperature IR Gun #I§QZM CF
'C °C NIA
Radiological Testing Instrument serial #jag?
Y N NIA
(sea page 2 for scan results),
-Use 1'speet'per sample for Radiological Testing.
If sample is HOT, the Radiological Safety Officer must be notified
immediately.
C-O-C filled out properly
N NIA
Samples In separate bags
r
Y N C\NtD
Sample containers intact*
N NIA
'If no, list broken sampie(s):
Sample label(s) complete (ID, date, etc.)U
N
NIA
Label(s) agree with C-O+ C
N
NIA
Correct containers usedy
N
NIA
Sufficient sample received
(Y)
N
NIA
Bubbles absent from 40 mL vials"
Y
N
NIA
•' Samples with bubbles <6mm are acceptable:
Indicate bubble size If >6mm.
Was client contacted about samples
. Y N
Will client send new samples
Y N
Client contact:
DateTme,
Logged in by.
0
G:IQC SHAREDTocument Control Templates - TrackinglCooler receipt form Rev. 12 07-27-13.doc Page 1 of 2

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number: WQ0014885
WWTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 01/01/14 To 3/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If aw licable to alternative performed (Class A or Class B) comnlete the following monitorine data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 0
CFU
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
ND
ND
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt 5
Option/Alt. 6
Option/Alt 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Igiection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment"
•Allan Rex O'Briant, WTP Superintendent
Pr er dt 01T`� / Land Applier Name and Title (if applicable) (type or print)
ignature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

aceAnalydcal
www.pacelab&com
February 18, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 04, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Y
Jon D Bradley
[e-mail]
Project Manager
Enclosures
�ACCRF
�O
�eORiCi�yf
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalytical
www.pacelabs.com
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification M 67
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99006001
•
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 11

/55'neAnalyfical
4www.pacefabacom
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92188411001 Harnett WTP 1 ASTM D2974-87
LLW
1
PASI-C
SM9221C E (MPN) 503
NAW
1
PASI-R
92188411002 Harnett WTP 2 ASTM D2974-87
LLW
1
PASI-C
SM9221C E (MPN) 503
NAW
1
PASI-R
is
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

ANALYTICAL RESULTS
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Harnett WTP 1 Lab ID: 92188411001 Collected: 02/03/14 14:00 Received: 02/04/14 09:30 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.6 % 0.10 1 02/11/14 14:42
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN ND MPN/g 74.1 100 02/04/14 11:35
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/18/2014 04:31 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11

aceAnalytical
www.pacelabacom
ANALYTICAL RESULTS
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Harnett WTP 2 Lab ID: 92188411002 Collected: 02/03/14 14:00 Received: 02/04/14 09:30 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.6 % 0.10 1
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN ND MPN/g 74.1 100
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/18/2014 04:31 PM without the written consent of Pace Analytical Services, Inc..
02/11 /14 14:42
02/04/14 11:35
Page 5 of 11

aceAnalytical
www.pacelabs.corn
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
QC Batch: PMST/6239
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92188411001, 92188411002
SAMPLE DUPLICATE: 1136398
Parameter Units
Percent Moisture %
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92189027002 Dup
Result Result RPD Qualifiers
20.4 18.4 11
SAMPLE DUPLICATE: 1136399
92189294006 Dup
Parameter Units Result Result RPD
Percent Moisture % 25.1 24.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/18/2014 04:31 PM without the written consent of Pace Analytical Services, Inc..
4
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11

aceAnalydca(
www.pacddacom
QUALITY CONTROL DATA
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
QC Batch: RBIO/3637 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92188411001, 92188411002
METHOD BLANK: 1134176
Associated Lab Samples: 92188411001, 92188411002
Parameter Units
Fecal Coliforms, MPN MPN/g
SAMPLE DUPLICATE: 1134177
Parameter
Fecal Coliforms, MPN
•
Date: 02/18/2014 04:31 PM
Units
MPN/g
Matrix: Solid
Blank
Reporting
Result
Limit Analyzed Qualifiers
ND
0.018 02/04/1411:35
92188411002
Dup
Result
Result RPD Qualifiers
ND
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11

QUALIFIERS
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
DEFINITIONS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
is
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in -full,
Date: 02/18/2014 04:31 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Harnett WTP 02/03/14
Pace Project No.: 92188411
Lab ID
Sample ID
QC Batch Method
QC Batch
92188411001
Harnett WTP 1
ASTM D2974-87
PMST/6239
92188411002
Harnett WTP 2
ASTM D2974-87
PMST/6239
92188411001
Harnett WTP 1
SM9221C E (MPN) 503
RBI0/3637
92188411002
Harnett WTP 2
SM9221C E (MPN) 503
RBI0/3637
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/18/2014 04:31 PM without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
Page 9 of 11

•
.7
Where Asftev41 a. : [ .Bien f aleigh
Catlrler (Ctrafej: Fed ®c UPS USPS ol3ent 'Commerclat Pace Other___-_.__
CCrstodySeal an CooierlSaxF'teseni: Q yes no ' Seafs'fnhacEs'YeS no
Packing iVifedal: E3ubblaWrap _ NOthar�r; .._
Mole Therm ttt�feQ sed; lt� Aun :129QW87 Of 10
Wet ue Nolte [J N� on ice, ceoling pm�ess begun
IR Gun Up Ti
Temp,CrreofianFabtorAdd I bY t g
. .ti_1..- _L:.i .tt,.l �v T....c.. • - � _ - 'f! ' .:Blofeafe8l f fS.?�tt•�.[��iI�7�»i I,B9 �/� • • •'•:-k'dtiei7e��71 ��'.' .�
r w, •r a ...+� .r.,w.... - _ -_ - _ _ _
' 1"ield i}ata Reciiiired?, Y f
• �G14at�t�iottficat9anf lte§o(ti�loiiti "- -
Pmon 6ntaoted eCCiYnfi
CommejW Resolu8otb
Piaos la6.elhm.
ecutp POvl �..
S�Y Re iow:
i�iote: Wherteverlfietgisadisorel�ancYafleetirig'i`ioith�at�il�aompilxnQe e�fluttiber .• - -
F toUteAtotthDxi $r
_ . _...:._.... -• tnc�"rescEoontaSi�ers) • , � �� � � � ! � - - . • '
Page 10 of 11

1�;alceAnalyticallt Chain of Custody
i www.pacelabs.com
6701 Conference Drive, fieleigh, NC 27607
-6497
NCert#67,C WCert
(WWC8N()N37731
W.O. #
Report Results To: Bill To:
Company: �rfiT ei Oro Project Reference:
Address:
_ N-_3
Project Number:
AM. �_ Purchase Order #:
Phone:., �° ��` ❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
Fax: _ "Rush projects are subject to prior approval by
the laboratory
Sampled by (signature) Requested Due Date:
WTP7LY,'mdr ► fGrs�A,J.
Z. l Ll C"O
17,
Ae{in
ived e)
Date
14
Time
Relinquished by (signature)
Received by (signs re)
D to
Time
Relinquished by (signature)
Received by (signature)
Data
Time
Receipt w wwons tL )
❑ 4t2°C ❑ Temp: °C
Res. Chlorine:
❑ Absent ❑ Present ❑ n/a
Add preserv. <27
❑Yes ❑No ❑We
Base preserv.>127
❑Yes ❑No ❑Na
Page 11 of 11

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
•
Facility Name: Harnett County WTP WQ Permit Number: WQ0014885
WWTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From
4/01//14 To 6/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp)
Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
5.8
5.8
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt.-6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (please note if you check this statement attach an
explanation why you have not met one or both of the requirements.) — See Tab #1
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
•Allan Rex O'Briant, WTP Superintendent
Pr er d I p It) � Land Applier Name and Title (if applicable) (type or print)
/r/5_
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

aceAnalyfical
www.pacelabs.com
April 28, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett WTP
Pace Project No.: 92198298
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 22, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jon D Bradley
[e-mail]
Project Manager
Enclosures
" Nx„
�g8o� Via,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnaljftal
imm..pace/abacom
CERTIFICATIONS
Project: Harnett WTP
Pace Project No.: 92198298
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607 North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification M 67 North Carolina Drinking Water Certification #: 37731
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification M E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification M 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9B00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 10

aceAnalytical
www.pacefabs.cam
i
Project: Harnett WTP
Pace Project No.: 92198298
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92198298001 Harnett WTP 1, 2 ASTM D2974-87 LLW 1 PASI-C
SM9221C E (MPN) 503 JW1 1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

aceAnalytical
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ANALYTICAL RESULTS
Project: Harnett WTP
Pace Project No.: 92198298
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Harnett WTP 1, 2 Lab ID: 92198298001 Collected: 04/22/14 12:05 Received: 04/22/14 14:10 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 96.9 % 0.10 1 04/24/14 15:52
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 5.8 MPN/g 0.58 1 04/22/14 14:48 1g
C7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2014 05:22 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

aceAnalytical
www.pacelabs.cwn
QUALITY CONTROL DATA
Project: Harnett WTP
Pace Project No.: 92198298
QC Batch: PMST/6494 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92198298001
SAMPLE DUPLICATE: 1184261
92198463001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 19.9 22.1 10
SAMPLE DUPLICATE: 1184262
92198298001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 96.9 96.8 0
•
Date: 04/28/2014 05:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 10

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Harnett WTP
Pace Project No.: 92198298
QC Batch: RBIO/3937 Analysis Method: SM9221 C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92198298001
METHOD BLANK: 1183443
Associated Lab Samples: 92198298001
Parameter Units
Fecal Coliforms, MPN MPN/g
SAMPLE DUPLICATE: 1183444
Parameter
Fecal Coliforms, MPN
•
Date: 04/28/2014 05:22 PM
Units
MPN/g
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.018 04/22/1414:48
92198277002 Dup
Result Result RPD Qualifiers
4650 49400 166
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 10

aceAnalytical
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QUALIFIERS
Project: Harnett WTP
Pace Project No.: 92198298
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2014 05:22 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
w w.pacelabs.c=
Project: Harnett WTP
Pace Project No.: 92198298
Lab ID
92198298001
92198298001
•
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Sample ID
Harnett WTP 1, 2
Harnett WTP 1, 2
Date: 04/28/2014 05:22 PM
QC Batch Method
QC Batch
ASTM D2974-87
SM9221C E (MPN) 503
PMST/6494
RBI0/3937
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
Page 8 of 10

.nWAn;2W1ca1"
• r: .
t
Document Name: Sample Condition Upon
Document No.:
SAL-CS-001-rev.02
Revised: April 04,
Pane 1 of 2
Issuing
Pace Ashev
Client NameQX1Y
Where Received: Q Muntersville
❑ Asheville
Eden (�
Raleigh
Courier (Circle): • Fed Ex UPS USPS lient
Commercial Pace
.uh
Custody Seal on Cooler]Box Present: j]
yes no
Seats intact, �i( yes
no
Packing Material: Q Bubble Wrap ags None Other—.hes
ice: Wet Blue None
Q Samples on Ica. cooling process begun
Circle Thermometer Used: IR Gun :122065387T
i of
IR Gun
Date and initials of pe son examining
Temp Correction Factor: Ad Subtract
1 C
Biological Tissue
Is Frozen: Yes N
NIA
co o Pre
check
Corrected cooler Temp-, �
C
Comments:
Temp should be above freezing to 6T
Chain of Custod Present:
Yes ONo
❑WA 1:
Chain of Custod Filled Out:
Yes ❑No
❑WA 2.
Chain of Custod Relin wished:
Yes ❑No
❑NIA 3.
Sam ler Name & Signature on COC:
Yes []No
DNlA 4.
Samples Arrived within Hold Time:
Yea , ❑No
❑WA 6.
Short Hold Time Anal sls Cf2hr):
Yes ❑No
❑WA t3
Flush Turn Around Yirne Requested:
yeso
_
❑WA 7.
a
,.,..., .• - -
3orrebt containers Used:
r,—iAnpm.
-Pace Containers Used:
0.1]1.volume•received
*-
for bissotved tests12.Sample
Labels match COC:l
JI containers needing preservation have been checked. Ysg pNo ❑N1A 13.
ill containers needing preservation arefound to be in fir', es ❑No ❑N1A
;ompiiance with EPA recommendation.
es ONO
ixceptbns: VoA, Ootiform,TOC)0&G,WI-0R4(water) Yes ❑� f]N!A 14.
samples checked for dechiorination: WA 15.
Oyes ONO
Heads ace in VOA Vials >6mm):
❑yss [IN. WA 16. -
Trip Blank Present:
❑Yes ONO IJIA
Trip Blank Custody Seats Present
�
Pats Tri Blank Lot # if purchased : Field Data Required? Y •1 N
Client Notification! Resolution: Date/Time,
Person Contactod:
Comments/ Resolution:
SCURF 1SRF L�J Date:
ti �?-1
Review::
Note: Whenever there is a discrepancy affocting North Carolina compliance
samples, a copy of thls form will bo sent to the North Carolina DEHNR
Certification•office (1.e out of hold, incorrect preservative, out of temp,
• incorrect contalnere)
Place label here
OR
Handwrite project number
(if no label available)
Page 9 of 10

aceAnalytical
' www.pacelabs.com
6701 Conference Drive, Raleigh, NC V607
ph: [phone], fax: [phone]
NCWW Cert#67, NCDW Cert#37731
Chain of Custody W.O. it g4,15 k K
Report Results To: Bill To:
�- 1 tt '
Company: �6 ,-C, _ -� AG y r0 Project Reference: N4>*A-0/� W�
V
Address:
Project Number:
Attn: ' I U� .- Purchase Order #:
Phone:%y7 �Co ❑ Standard Report Delivery
4' �+j, �,� ❑ Rush Report Delivery (w/surcharge)
Fax:�%IN C -Rush projects are subject to prior approval by
the laboratory
Sampled by (signature .
Requested Due Date:
Relin red s
Re co ed by n re)
Dat
Ti
i 10
Relinquished by (signature)
Received by (signatu )
Date
Time
Relinquished by (signature)
Received by (signature)
Date
Time
Di
Receipt Conditions (nlY)
❑ 4t2°C ❑Temp: °C
Res. Chlorine:
❑ Absent ❑ Present ❑ n/a
Acid preserv. <2?
❑ Yes ❑ No ❑ n/a
Base preserv. >12?
❑ Yes 0 No ❑ n/a.
t
Page 10 of 10

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number: WQ0014885
•WWTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 07/01/14 To 09/30/14 '
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. _5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
11.7
11.7
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
Option/Alt. 1
Option/Alt. 2
(VS reduction)
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
Option/Alt. 4
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 7
Option/Alt. 8
(Drying — Stable)
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
•Allan Rex O'Briant, WTP Superintendent
Pre er Vd titl r *- Land Applier Name and Title (if applicable) (type or print)
(lpgnature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 4 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

aeeAnalytieal o
www.pacdabs.com
•
August 07, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett WTP
Pace Project No.: 92211797
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 04, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless -
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jon D Bradley
jon. [e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

Project: Harnett WTP
Pace Project No.: 92211797
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99006001
is
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

aceAnalyfical
wvmpacalabs com
SAMPLE ANALYTE COUNT
Project: Harnett WTP
Pace Project No.: 92211797
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID
Method
Analytes
Analysts Reported
Laboratory
92211797001 Harnett WTP
ASTM D2974-87
ACS 1
PASI-C
SM9221C E (MPN) 503
JW1 1
PASI-R
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 10

aceAnalytical
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ANALYTICAL RESULTS
Project: Harnett WTP
Pace Project No.: 92211797
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Harnett WTP Lab ID: 92211797001 Collected: 08/04/14 12:15 Received: 08/04/14 14:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 98.5 % 0.10 1 08/07/14 15:01
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 11.7 MPN/g 0.018 1 08/05/14 09:19 1 g
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2014 06:55 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

acMnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Harnett Wt-P
Pace Project No.: 92211797
QC Batch: PMST/6894 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92211797001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 1258542
92212326001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 79.8 79.7 0
SAMPLE DUPLICATE: 1258543
92212271006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 10.6 11.7 11
• Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2014 06:55 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 10

lceAnalytical
tvww.pacefabs.com
QUALITY CONTROL DATA
Project: Harnett WTP
Pace Project No.: 92211797
QC Batch: RBIO/4287 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92211797001
METHOD BLANK: 1256426 Matrix: Solid
Associated Lab Samples: 92211797001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 08/05/14 09:19
SAMPLE DUPLICATE: 1256427
92211797001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 11.7 11.7 0 1g
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
• Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2014 06:55 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

Pace'Analytical Services, Inc.
Kincey Ave.
te 100
aceAnal cal ® 9800Huntersv Ile, NC1
Y�i28078
www.pacelabscom [phone]
QUALIFIERS
Project: Harnett WTP
Pace Project No.: 92211797
DEFINITIONS
DF - Dilution. Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2014 06:55 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

amAnalytical
www.pac"S.com
Project: Harnett WTP
Pace Project No.: 92211797
Lab ID
Sample ID
92211797001
92211797001
Harnett WTP
Harnett WTP
•
Date: 08/07/2014 06:55 PM
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
ASTM D2974-87
SM9221 C E (MPN) 503
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
PMST/6894
RB10/4287
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 8 of 10

C,
Document No.:
Revised: April 04, 2013
Pace 1 of 2
Client Name: t`MV\( U1 Yn
Where Received: I] Huntersville Asheville C]r Eden Raleigh
Courier (Circle): Fed Fx UPS USPS Client Commercial Pace .Other
Custody Seal on Gooler/Box Present: El yes no Seals intact: yes [1 no
Packing Material: Q Bubble Wrap a s No� Other
Circle Thermometer Used: IR Gun :1220853Si7ype Ice: Wet Blue Nona 0 Samples on ice, coaling process has begun
IRGunB t
`� C Ehock
and Initials of pcirson oxamining
Temp Correction Factor: Add ubtract t n rrese ti 1
CorrecEed Coaler7emp C Biological Ttssue is Frozen: vas No y
Temp. should be above freezing to 6°C Comments:
'Chain of Custod Present. '
es ONo �IWA1.. ... .. _ .. .. _
Chain of CustodyFilled Out es ❑No E2.Chainof Custody Relinquished:Yec ❑No
& Signature on CO
d within Hold Time:
Around
Containers Used:
❑No
ONO ❑NIA
Filtered volume received for Dissolved tests ❑yes ❑No )Z)wA Iti.
Sample Labels match COC:
f�Yes, QN.
/
❑wA
12.
-includes date(ffineAD/Mal sis Matrix
.All containers needing preservation have been ohs ed.
❑N,
❑wA
13.
/yes
Ali containers needing preservation are found to be irl
r nyes ❑No
❑wA
compliance with EPA recommendation.
/
axceptans: VOA. poaform.TOC,O&G,wl-DRO(vmter)
Oyes ON
'
Samples checked fordechiorination:
Yes ❑No
❑wA
14.
Heads ace in VOA Vials (>6mm):
Dyes ONO
NIA
16.
Trip Blank Present:
❑Ye9 ❑No
—/WA
16.
Trip Blank Custody Seals Present
[IYes ❑No
LLwA
Pace Trip Blank Lot# if purchased):.
Field Data Required? Y / N
Client Notification/ Resolution:
Person Contacted:
Datefrime: /biI
St•Y'�^ r'/.7 i�l/ll?H✓L �;'
Comments/Resolution: (� Ui G,�
ut �
'Zlt
g k t y Place label here
SCURF 1SRIF Date, ^
Review:: OR
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be Sent to the North Carolina DEHNR Handwrite project number
Codification Office t I,e out of hold. Incorrect preservative, out of temp, (if no label available)
incorrect containers)
�jZ2�77%
•
afF
Page 9 of 10

. Chain of Custody
aceAnalytical W.o. # q zz < <? ,�?
r [xww.paeelabs.com
6701 Conference Drive, Raleigh, NC 27607
Ph:
[phone],fax: [phone]W NCW Cen#67. NCDW Cert#37731
Report Results o: Bill To:
Company: %6. _� r ci / 19�( /tea Project Reference:
Address:
Project Number:
Attn: e!" )7 (y�v.+� Purchase Order#:
Phone: 34i 9 -� ❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
Fax: "Rush projects are subject to prior approval by
the laboratory
Sampled by (signature): � Requested Due Dale:
ReceiptCondiitions(la Only)
❑ 4t2°C ❑ Temp: °C
Rea. Chlorine:
❑ Absent ❑Preseru ❑ Na
Acid preserv. <27
❑Yes ❑ ❑ Na
Race preseN.>12127
❑ Yes ❑ No ❑ Mill
Peiinqu' (s n )
ieceived
1ved (sl ture)
D le'
Time
I
n
(•'
Relinquished by (s gnature)
by (slgna )
D to
Time
Relinquished by (slgnature)
Received by (eignalure)
Date
Time
�6(
Page 10 of 10

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number: WQ0014885
•WWTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 10/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
U nnnlirnhln *n alternatives narfnrmad tri—e A nr ri... Rl nmm-lo+. Fl.n f ll...v:...........:F..:... A..4...
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6h
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
9.7
9.7
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
Coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(A& Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
• Allan Rex O'Briant, WTP Superintendent
rtit or Land Applier Name and Title (if applicable) (type or print)
of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 4 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

aceAnalytieal
www.pacelabs.com
October 15, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett WTP 110/9
Pace Project No.: 92221018
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
• pC�i
ge�BA��y,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalytical
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Project: Harnett WTP 110/9
Pace Project No.: 92221018
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
•
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification M 37731
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
West Virginia Certification M 357
VirginiaNELAP Certification M 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 11

aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: Harnett WTP 110/9
Pace Project No.: 92221018
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92221018001 HARNETi WTP 1 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92221018002 HARNETT WTP 2 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

aceAnalXica(
www.pacelabs.c=
ANALYTICAL RESULTS
Project: Harnett WTP 110/9
Pace Project No.: 92221018
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: HARNETT WTP 1 Lab ID: 92221018001 Collected: 10/09/14 15:30 Received: 10/10/14 08:30 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.7 % 0.10 1 10/15/14 13:56
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 9.7 MPN/g 0.018 1 10/10/14 11:22 1g
C7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2014 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11

aceAnalytical
www.pam1abs.c=
ANALYTICAL RESULTS
Project: Harnett WTP 110/9
Pace Project No.: 92221018
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: HARNETT WTP 2 Lab ID: 92221018002 Collected: 10/09/14 15:30 Received: 10/10/14 08:30 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.8 % 0.10 1 10/15/14 13:56
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 23.4 MPN/g 0.018 1 10/10/14 11:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2014 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11

aceAnalytical
MM..pacetabs.com
Project: Harnett WTP 110/9
Pace Project No.: 92221018
QC Batch: PMST/7126
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92221018001, 92221018002
SAMPLE DUPLICATE: 1306022
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 1306023
Parameter Units
Percent Moisture %
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92221108001 Dup
Result Result RPD Qualifiers
8.8 9.3 5
92221124001 Dup
Result Result RPD Qualifiers
40.7 41.9 3
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
• Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2014 04:54 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

,5a'cielAnalydcal
wwpacelabs.com
4
Project: Harnett WTP 110/9
Pace Project No.: 92221018
QUALITY CONTROL DATA
QC Batch: RBIO/4445 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92221018001, 92221018002
METHOD BLANK: 1304979 Matrix: Solid
Associated Lab Samples: 92221018001, 92221018002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 10/10/14 11:22
SAMPLE DUPLICATE: 1304980
92221018002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 23.4 10.1 79 1g
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
• Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2014 04:54 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 11

awAnalytical
www.pacelabs.com
QUALIFIERS
Project: Harnett WTP 110/9
Pace Project No.: 92221018
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Chai1otte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1 g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2014 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

aceAnalytical
www.pacelabs.cw
•
Project: Harnett WTP 110/9
Pace Project No.: 92221018
Lab ID
92221018001
92221018002
92221018001
92221018002
•
Sample ID
QUALITY CONTROL DATA CROSS REFERENCE TABLE
HARNETT WTP 1
HARNETT WTP 2
HARNETT WTP1
HARNETT WTP 2
Date: 10/15/2014 04:54 PM
QC Batch Method
ASTM D2974-87
ASTM D2974-87
SM9221C E (MPN) 503
SM9221C E (MPN) 503
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
PMST/7126
PMST/7126
RB10/4445
RB10/4445
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 9 of 11

aeeAnaliftal S
• www.pacelabs.com
6701 Conference Drive, Raleigh, NO 27607
ph: [phone], fax: [phone]
NCWW Cerl#67, NCDW Cert#37731
4
Report Results To:
Company: �lQ �► G/i t�
Address:
Chain of Custody MO.#
Attn:
Phone• :3LG f -) >
Fax:
Sampled by (signature)*
Bill To:
Project Reference: ` r �'�{ �f LIT—P
Project Number.
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
"Rush projects are subject to prior approval by
the laboralory
Requested Due Date:
re)
Received b Jsllure,�
Da
L0
( f
Time
rRelinquishedre
rMlanature))
Received by (signatur
Dat
Time
Received by (signature)
Date
Time
Receipt Condatons (Ltee I�Only)
❑ 4t2°C ❑ Temp: i °C
Res. Chlorine:
❑ Absent ❑ Present ❑ Na
Acid preserv. <2?
❑ Yes ❑ No ❑ nra
Base preserv. }127
❑ Yes ❑ No 0 nfa
Page 10 of 11

a
2cqAnalylical'
Document Name: Sample Condit[an Upvn Document pevised: April 04, 2013
Recei t S.CUR Pa e1of2
issuing Authorities:
••- .V„ wnno�,r,nR�d„ Document No.:
_. en_ n..nlrhr (lfflrA
Client Name:,"-'
Where Received: [j Huntersville (] Asheville Eden F2aleigFt
Courier (Circle): - Fed Ex UPS USPS Cllen Commercial Pars Other
Custody Seal on Cooler/Box Present: [] yes pl no Seals intact yes [] no
Packing Material: ❑ Bubble Wrap [] Bubble B(a'gs ,¢j None Other. ��
� "' � Samples on Ice, cool
process has prochas begun
Circle Thermometer Used: IR Gun 0653 ypo of.lce: Wet Blue None
IR Gun B 7
Date and Inkfals of person examining
Temp Correction Factor: Ad Subtrac C co t p ati n
Corrected Cooler Temp.: C. Biological Tissue Is Frozen: Yos No NIA check; b 0 I
Temp should be above freezing to 6°C Comments:
Ctrdtn of Custody Present: Yes F]No ❑NIA 1-. -
Chain of Custody Pilled Out:_
Chain ofCustody Relin dish,
Sam ler Name & Signature c
Sam tea Arrived within Hold
Short Hold Time Analysts-(
Rush Turn Around Time Ri
Sufriclent Volume:
Correct Containers Used:
-Pace-Containers Used:
Containers Intact:
Filtered volume -received for
Sample Labels match COC:
-includes dateAlme/1131Ar
JAJI containers noading preserve",
es ❑No
0NIA 12.
gd;
Yes No
OwA 3.
)n COC:
Yes ONo
EIWA 4.
Time:
Yes ONo
ONIA b.
in :
Yes [No
❑NIA 6.
!quested:
OYea RIN.
Yes EN.
13 8.
ONallo
❑NA 9. '
ON IA
Ye❑
eODNO
wA 10.
Dissolved tests
Oft ©No
RfNIA 11.
es QRo
All
0NIA 12.
.._._.._
1AII containers needing preservation are found to be In
comaltancewith EPA recommendation.
(A'Yes CINO EINIA 13-
I'Yes []No G'hlfA
Yes LINO
r r 14
Samples checked for dechlorination:
Oyes
-
Heads ace in VOA Vials >6mm :
OYes I N/A 15.
(Trip
OYes ONO NU1 16.
Blank Present:
Trip Blank Custody Seals Present
OYes ONo WA
Pace Trip Blank Lot # (ifpurchased)
Field Data Required? Y I N
Client Notifieationf Resolution:
Person Contacted',
Date/Time'
Comments/ Resolution:
date:
r��"•(I��•4O+'e E
SCURF 1SRF
/p r 3 i
i
• Review::
Note: Whenever there is a discrepancy affecting
florin Carolina compliance
i
samples, a copy of this form WO be sent to the North Carolina DEHNR
temp,
Certificetion Office ( Le out of hold, incorrect preservatNo, out of
incorrect conlainers)
- • w - -- " `
Page 11 of 11

SOUTH HARNETT COUNTY WWTP, NC
CLASS A CAKE RESIDUALS PROGRAM
Permit No. WQ0014885
2014 ANNUAL REPORT
0

C,
•
Date
T1
T2
T3
T4
T5
pH
1/17/2014
158.1
159.4
143
15.1
141.4
11.6
1/21/2014
152.8
157.1
148
147.6
148
11.3
1/31/2014
152.6
156.4
151.1
149.7
148.11
11.3
2/8/2014
153
154.8
154.6
163.5
135.9
11.3
2/19/2014
149.2
151.7
152.2
155.5
152.3
10.9
3/10/2014
172.8
184.5
150.6
151.6
150.2
11.3
3/20/2014
153.9
162.5
166.9
151.1
150.7
11.12
3/20/2014
3/22/2014
145.6
150.9
154.7
177.7
158.1
11
3/23/2014
3/27/2014
146.2
151.3
155.2
163.4
157.3
11.3
3/28/2014
145.4
148.2
149.1
153.8
161.1
11.2
4/4/2014
170.1
149.2
150.1
147.6
145.3
11.1
4/8/2014
4/11/2014
163
154.3
155.1
152.6
150.7
11.3
4/14/2014
4/22/2014
157.4
155.1
154.3
151.9
151
11.6
4/28/2014
5/2/2014
5/9/2014
151.2
153.4
152.2
152
151.4
11.2
5/16/2014
149.1
151.1
151.7
151
149.71
11.3
5/20/2014
5/21/2014
5/27/2014
7/14/2014
147.3
1491
150.8
151.3
149.3
11.5
7/23/2014
8/27/2014
8/30/2014
148
148.9
150.1
154.7
173.1
11.6
9/5/2014
9/10/2014
140.4
146
145.9
147.4
142.1
11.3
9/25/2014
144.3
147
147.3
148
147.4
11.6
10/31/2014
144.2
146.5
147
147.5
146.3
11.3
11/4/2014
144
146.4
147.5
147.61
147.1
10.8
11/13/20141
143.7
146.1
146.31
147.1
148.2
11.9
Temperatures are in Farenheit Degrees

South Harnett County WWTP Class A Cake Distribution Control
Wet Tons
Date
Location
pH
75
1/17/2014
Carolina Lakes
11.6
150
1/21/2014
Carolina Lakes
11.3
60
1/31/2014
Farrar Dairy Farm
11.3
100
2/8/2014
Farrar Dairy Farm
11.3
40
2/19/2014
Farrar Dairy Farm
10.9
132
3/10/2014
Farrar Dairy Farm
11.3
48
3/20/2014
Farrar Dairy Farm
11.12
48
3/20/2014
Carolina Lakes
36
3/22/2014
Danny McDonald
11
48
3/23/2014
Carolina Lakes
48
3/27/2014
Danny McDonald
11.3
132
3/28/2014
Farrar Dairy Farm
11.2
42
4/4/2014
Danny McDonald
11.1
42
4/8/2014
Danny McDonald
156
4/11/2014
Farrar Dairy Farm
11.3
48
4/14/2014
Farrar Dairy Farm
72
4/22/2014
Farrar Dairy Farm
11.6
42
4/28/2014
Farrar Dairy Farm
30
5/2/2014
Farrar Dairy Farm
192
5/9/2014
Farrar Dairy Farm
11.2
6
5/16/2014
Farrar Dairy Farm
11.3
6
5/20/2014
Farrar Dairy Farm
24
5/21/2014
Tony Dickens
6
5/27/2014
Tony Dickens
42
7/14/2014
Harnett Co. Landfill
11.5
66
7/23/2014
T. Wombles
6
8/27/2014
Carolina Lakes
84
8/30/2014
T. Wombles
11.6
78
9/5/2014
Carolina Lakes
24
9/10/2014
Carolina Lakes
11.3
60
9/25/2014
Carolina Lakes
11.6
72
10/31/2014
Harnett Co. Landfill
11.3
66
11/4/2014
Harnett Co. Landfill
10.8
42
11/13/2014
Harnett Co. Landfill
11.9
Total Wet Tons
2123
Dry Tons
424.6
is

Meritech, Inc.
Environmental Laboratory
,a ry
• R Laboratory Certification No. 165
Contact: Gabe Gutierrez Report Date: 10/27/2014
Client: Harnett County NPDES#: NC0088366
3224 Shady Grove Rd P.O.#: 051805
Spring Lake, NC 28390 Date Sample Rcvd: 10/2/2014
Meritech Work Order # 10021489 Sample: South Harnett Regional Cake Grab 10/2/14
Parameters Result Analysis Date Reporting Limit Method Qualifier
% Solids
44.0 %
10/7/14
0.2 %
SM 2540B
TKN
17,500 mg/kg
10/6/14
20 mg/kg
EPA 351.1
Nitrate, Nitrogen
< 22.7 mg/kg
10/6/14
22.7 mg/kg
EPA 353.2
Nitrite, Nitrogen
< 22.7 mg/kg
10/6/14
22.7 mg/kg
EPA 353.2
Aluminum, total
3,610 mg/kg
10/13/14
2.50 mg/kg
EPA 200.7
Ammonia, Nitrogen
217 mg/kg
10/6/14
10 mg/kg
EPA 350.1
Arsenic, total
< 1.14 mg/kg
10/13/14
1.14 mg/kg
EPA 200.7
Cadmium, total
1.84 mg/kg
10/13/14
0.200 mg/kg
EPA 200.7
Calcium, total
241,000 mg/kg
10/13/14
10.0 mg/kg
EPA 200.7
Copper, total
119 mg/kg
10/13/14
1.00 mg/kg
EPA 200.7
Lead, total
16.4 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
Magnesium, total
2,090 mg/kg
10/13/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.239 mg/kg
10/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
0.665 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
Nickel, total
8.02 mg/kg
10/13/14
2.0 mg/kg
EPA 200.7
Phosphorus, total
6,910 mg/kg
10/13/14
2.00 mg/kg
EPA 200.7
Potassium, total
684 mg/kg
10/13/14
20.0 mg/kg
EPA 200.7
Selenium, total
2.80 mg/kg
10/13/14
0.50 mg/kg
EPA 200.7
Sodium, total
295 mg/kg
10/13/14
20.0 mg/kg
EPA 200.7
Zinc, total
461 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
SAR
0.232
10/13/14
- -
-
Fecal Coliform
< 23 col/g dry wt
10/3/14
23 col/g dry wt
SM 9222D B2
B2 Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
I hereby certify that have reviewed and approve these data.
• ,Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
• Laboratory Certification No.165
Contact: Gabe Gutierrez
Report Date:
10/27/2014
Client: Harnett County
3224 Shady Grove Rd.
Date
Sample Rcvd:
10/2/2014
Spring Lake, NC 28390
Meritech Work Order #
10021489A Sample: Sludge Storage Tank
Collection Date:
10/2/2014
1311-
TCLP Metals
Parameter
Results
Analysis
Det- Limit
Reg. Limit
Method
Arsenic
< 0.100 mg/L
10/16/14
0.100
5.0
EPA 200.7
Barium
0.664 mg/L
10/16/14
0.050
100.0
EPA 200.7
Cadmium
< 0.020 mg/L
10/16/14
0.020
1.0
EPA 200.7
Chromium
< 0.050 mg/L
10/16/14
0.050
5.0
EPA 200.7
Lead
0.236 mg/L
10/16/14
0.100
5.0
EPA 200.7
Mercury
< 0.02 mg/L
10/10/14
0.02
0.2
EPA 245.1
Selenium
< 0.100 mg/L
10/16/14
0.100
1.0
EPA 200.7
Silver
< 0.050 mg/L
10/16/14
0.050.
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis
Method
Pesticides 8080
Attached
10/16/14
8080
Volatiles 8260
Attached
10/8/14
8260
Semi Vol. 8270
Attached
10/10/14
8270
Herbicides 8150
Attached
10/16/14
8150
Other Tests
Parameter
Resultk
Analysis
Repgrtina Limit
Method
Cyanide, total
< 0.5 mg/kg
10/3/14
0.5 mg/kg
EPA 335.4
Flash Point
> 140 OF
1013/14
- -
EPA 1020E
Ignitability
Will not ignite
10/3/14
- -
EPA 1030
pH
10.1 S.U.
10/8/14
1.0 - 14.0 S.U.
SM 4500 HB
Sulfide, total
< 3.5 mg/kg
10/3/14
3.5 mg/kg
SM 4500 SD
0
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Gabe Gutierrez
Client: Harnett County
3224 Shady Grove Rd.
Spring Lake, NC 28390
Meritech Work Order # 10021489A
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: Sludge Storage Tank
Report Date: 10/27/2014
Date Sample Rcvd: 10/2/2014
Collection Date: 10/2/2014
13 11 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Analyst: Summit
Analysis Date:
10/16/14
Parameter
Results
Det Limit
Reg. Limit Dilution
Factor
Heptachlor Epoxide
< 0.002 mg/L
0.002
0.008
1
Endrin
< 0.002 mg/L
0.002
0.02
1
Chlordane
< 0.010 mg/L
0.01
0.03
1
Gamma - BHC
< 0.002 mg/L
0.002
0.4
1
Toxaphene
< 0.10 mg/L
0.1
0.5
1
Methoxychlor
< 0.002 mg/L
0.002
10.0
1
Heptachlor
< 0.002 mg/L
0.002
0.008
1
Lindane
< 0.002 mg/L
0.002
0.4
1
Herbicides - SW-846L3151A
Analyst Summit Analysis Date: 10/22/14
Parameter Results Dgt Limit Reg, Limit Dilution Factor
2,4-D < 0.10 mg/L 0.10 10.0 1
2,4,5-TP (Silvex) < 0.10 mg/L 0.10 1.0 1
I hereby certify that I have reviewed and approve these data. Q&4a
Laboratory Representative
•
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
• -� Environmental Laboratories
ffi Laboratory Certificate #165
Client: Harnett County
Project: TCLP
Client Sample ID: South Harnett Regional Cake
Sample Collection: 10/02/14
Meritech Sample ID: 10021489
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 10/08/ 14
Extracted:
10/06/14
Analyst: VWV
Parameter
Result
Units
Det_ Limit
Reg. Limit
Dilution Factor
Benzene
<0.0200
mg/L
0.0100
0.50
20
Carbon Tetrachloride
<0.0200
mg/L
0.0100
0.50
20
Chlorobenzene
<0.0200
mg/L
0.0100
I00
20
Chloroform
<0.0200
mg/L
0.0100
6.0
20
1,2-Dichloroethane
<0.0200
mg/L
0.0I00
0.50
20
1,1-Dichloroethene
<0.0200
mg/L
0.0100
0.70
20
Methyl Ethyl Ketone
<0.200
mg/L
0.100
200
20
Tetrachloroethylene
<0.0200
mg/L
0.0100
0.70
20
Trichloroethene
<0.0200
mg/L
0.0100
0.50
20
Vinyl Chloride
<0.040
mg/L
0.020
0.20
20
Semi-Volatiles= SW-846 8270
Extraction: 10/04/14
Analysis: 10/10/14
Analyst:
PM
Parameter
Result
Units
Det. Limit
Rea, Limit
Dilution Factor
IA-Dich;orobenzene
<0.100
mg/L
0.I00
7.5
10
Hexachlorobenzene
<O.100
mg/L.
0.100
0.13
10
He%achloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100•
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mJL
0.100
0.13
10
lrereby certify that I have reviewed and approve these data.'f�
Laboratory Representative
642 Tamco Road * Reidsville, NC
27320
[phone] Ph *
[phone] Fax

I-
•
3-20.2013 Chain of Custody Record (COC)
NPDES#:
Client 0—a i—plc '14 ('�- ,,,�.�� Phone:
MERITECH, INC.
Address: -o Fax:
ENVIRONMENTAL LABORATORIES
Email:
642 TamcoRd. Phone: [phone]
ti
t �_�
�- � � tng •�y"�� r .�,�:�'4..G Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Turn Around Time*
he
www.meritech-labs.com m
How would you like your report sent? *RUSH work needs prior approval.
Std 10 days) 3-5 Da 24-48Hrs
I
s
Circle all that apply: Email (preferred), Fax, Mail
-Sampling
.Sam Iln Dates &Times
Person Taking Sample (Sign/Print):
Lab Use Only
Sample Location and/or ID #
Start
End
comp?
It of
�°
Required
ce?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
I est(s)
'Yes),
l OK?
SOQHI 071 V1Gf f— it7ttc.)
�
�i1 �S A"sl r A7.4 W q
`
.5
L
'� ccti
Temperature Upon
Receipt:
L
Method of
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to reservation. ***
Shipment:
Comments:
Compositor It
Jug #
❑ UPS
�.. Fed Ex
Are these results for regulatory purposes? Yes No_Uport
I mg/L mg/kg ug/L
Q Hand Delivery
Relinquished by: Date: Time:
Rece' Y D e
Q Other
Relin Dat : Time: 96
eceived by: Date: Time:
ived a Dat
Relin shed by: ate: Time:
r

Meritechy Inc,
Environmental Laboratory
Laboratory Certification No.165
Contact: Gabe Gutierrez
Client: Harnett County
3224 Shady Grove Rd
Spring Cake, NC 28390
Report Date: 6/23/2014
NPDES#: NCO088366
Date Sample Rcvd: 6/19/2014
Meritech Work Order # 06191410 Sample: Cake Grab
6/19/14
Parameters
Result
Analysis Date
Reporting Limit
Mgthod
% Solids
95.6 %
6/19/14
0.2 %
SM 2540B
Fecal Coliform (Sludge)
< 9 col/g dry wt
6/19/14
9 col/g dry wt
SM 9222D
Cadmium, total
1.21 mg/kg
6/20/14
0.200 mg/kg
EPA 200.7
Copper, total
56.7 mg/kg
6/20/14
1.00 mg/kg
EPA 200.7
Lead, total
15.7 mg/kg
6/20/14
0.500 mg/kg
EPA 200.7
Mercury, total
0.152 mg/kg
6/23/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
1.08 mg/kg
6/20/14
0.500 mg/kg
EPA 200.7
Nickel, total
7.31 mg/kg
6/20/14
2.0 mg/kg
EPA 200.7
Selenium, total
1.78 mg/kg
6/20/14
0.50 mg/kg
EPA 200.7
Zinc, total
205 mg/kg
6/20/14
0.500 mg/kg
EPA 200.7
• I hereby certify that I have reviewed and approve these data.
Laborator3iRepre entative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Ah
r _1
3.20-2013
Chain of Custody Record (COC)
NPDES#: /YC,, 01.6
Client: /``7//0 / n e,-1-1 "76 Phone: 9/0 /3o"
Address: ?,, Fax:
Email: LJ elf' C f r ,
Project:
P.O.#:
Attention: (qazc: dfi /��� Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email (per,, erred^ , Fax, Mail Std(to da s) 3 5 Da 24- as Hrs
p�
B W . EITE C H, INC.
ENVIRONMENTAL LABORATORIES
j 642 Tamco.Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www , m e ri to e h - (a bs . C o m
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample (Sign/Print .
tee. 6 Via`
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
TeSt(s) Required -
Ice?
Yes No
PH OK?
Cl OK?
Date
Time
Date
Time
�t.�c:
� �� «
o��
. � - �
/� ov
O
� �a ✓� ' . C� �\ i1 Iry � � � ; S �
Z
/as 0
a(-/ yG
/000
C,-
l
V
Temperature Upon
Receipt:
-2.
Method of
Shipment:
*** Dechlorination
(<0.5 pm) of Ammonia, Cyanide, Phenol
and TKN
samples must be done in the field prior to preservation. ***
Comments:
JJUg
Compositor #
It
0: UPS
E` Fed Ex
Are these results for regulatory purposes? Yes - P
No QJ`
Report results in: mg/La mg/kg Q ug/L Q,
Hand Delivery4.
Relinquished by: Date: Time:
l ,,'�, d
r'/
0:. Other
Relinquis ed b D e: f me:
l
Received by: Date: Time:
Relinquished by: Date: Time:
eive y La f t f' Da�eq ,.T�ni
Cp C i t
W

Meritech,
Inc.
Environmental Laboratory
• ""=
Laboratory Certification No.165
Contact: Gabe Gutierrez
Report Date:
10/27/2014
Client: Harnett County
NPDES#:
NCO088366
3224 Shady Grove
Rd
P.O.#:
051805
Spring Lake, NC 28390
Date Sample Rcvd:
10/2/2014
Meritech Work Order # 10021489
Sample:
South Harnett Regional Cake Grab
10/2/14
Parameters
Re ult
Analysis Date
Rgportine Limit
Method Qualifigr
% Solids
44.0 %
10/7/14
0.2 %
SM 2540B
TKN
17,500 mg/kg
10/6/14
20 mg/kg
EPA 351.1
Nitrate, Nitrogen
< 22.7 mg/kg
10/6/14
22.7 mg/kg
EPA 353.2
Nitrite, Nitrogen
< 22.7 mg/kg
10/6/14
22.7 mg/kg
EPA 353.2
Aluminum, total
3,610 mg/kg
10/13/14
2.50 mg/kg
EPA 200.7
Ammonia, Nitrogen
217 mg/kg
10/6/14
10 mg/kg
EPA 350.1
Arsenic, total
< 1.14 mg/kg
10/13/14
1.14 mg/kg
EPA 200.7
Cadmium, total
1.84 mg/kg
10/13/14
0.200 mg/kg
EPA 200.7
Calcium, total
241,000 mg/kg
10/13/14
10.0 mg/kg
EPA 200.7
Copper, total
119 mg/kg
10/13/14
1.00 mg/kg
EPA 200.7
Lead, total
16.4 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
Magnesium, total
2,090 mg/kg
10/13/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.239 mg/kg
10/7/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
0.665 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
Nickel, total
8.02 mg/kg
10/13/14
2.0 mg/kg
EPA 200.7
Phosphorus, total
6,910 mg/kg
10/13/14
2.00 mg/kg
EPA 200.7
Potassium, total
684 mg/kg
10/13/14
20.0 mg/kg
EPA 200.7
Selenium, total
2.80 mg/kg
10/13/14
0.50 mg/kg
EPA 200.7
Sodium, total
295 mg/kg.
10/13/14
20.0 mg/kg
EPA 200.7
Zinc, total
461 mg/kg
10/13/14
0.500 mg/kg
EPA 200.7
SAR
0.232
10/13/14
- -
-
Pecal CoIiform
< 23 col/g dry wt
10/3/14
23 col/g dry wt
SM 9222D B2
82 Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
I hereby certify that I have reviewed and approve these data. �(
• ;Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
• Laboratory Certification No.165
Contact: Gabe Gutierrez Report Date: 10/27/2014
Client: Harnett County
3224 Shady Grove Rd. Date Sample Rcvd: 10/2/2014
Spring Lake, NC 28390
Meritech Work Order # 10021489A Sample: Sludge Storage Tank Collection Date: 10/2/2014
1311-
TCLP Metals
Parameter
Results
Analysis
Det, Limit
Reg. Limit
Method
Arsenic
< 0.100 mg/L
10/16/14
0.100
5.0
EPA 200.7
Barium
0.664 mg/L
10/16/14
0.050
100.0
EPA 200.7
Cadmium
< 0.020 mg/L
10/16/14
0.020
1.0
EPA 200.7
Chromium
< 0.050 mg/L
10/16/14
0.050
5.0
EPA 200.7
Lead
0.236 mg/L
10/16/14
0.100
5.0
EPA 200.7
Mercury
< 0.02 mg/L
10/10/14
0.02
0.2
EPA 245.1
Selenium
< 0.100 mg/L
10/16/14
0.100
1.0
EPA 200.7
Silver
< 0.050 mg/L
10/16/14
0.050-
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis
M! thQd
Pesticides 8080
Attached
10/16/14
8080
Volatiles 8260
Attached
10/8/14
8260
Semi Vol. 8270
Attached
10/10/14
8270
Herbicides 8150
Attached
10/16/14
8150
Other Tests
Parameter Results Analysis Reporting Limit Method
Cyanide, total
< 0.5 mg/kg
10/3/14
0.5 mg/kg EPA 335.4
Flash Point
> 140 OF
10/3/14
- - EPA 1020B
Ignitability
Will not ignite
10/3/14
- - EPA 1030
PH
10.1 S.U.
10/8/14
1.0 -14.0 S.U. SM 4500 HB
Sulfide, total
< 3.5 mg/kg
10/3/14
3.5 mg/kg SM 4500 SD
U
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Gabe Gutierrez
Client: Harnett County
3224 Shady Grove Rd.
Spring Lake, NC 28390
Meritech Work Order # 10021489A
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: Sludge Storage Tank
ReportDate: 10/27/2014
Date Sample Rcvd: 10/2/2014
Collection Date: 10/2/2014
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8481A
Analyst: Summit
Analysis Date: 10/16/14
Parameter
Results
Det Limit
Reg. Limit
Dilution Factor
Heptachlor Epoxide
< 0.002 mg/L
0.002
0.008
1
Endrin
< 0.002 mg/L
0.002
0.02
1
Chlordane
< 0.010 mg/L
0.01
0.03
1
Gamma - BHC
< 0.002 mg/L
0.002
0.4
1
Toxaphene
< 0.10 mg/L
0.1
0.5
1
Methoxychlor
< 0.002 mg/L
0.002
10.0
1
Heptachlor
< 0.002 mg/L
0.002
0.008
1
Lindane
< 0.002 mg/L
0.002
0.4
1
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Analyst Summit
Results
< 0.10 mg/L
< 0.10 mg/L
Det Limit Reg, Limit
0.10 10.0
0.10 1.0
Analysis Date: 10/22/14
Dilution Factor
1
1
I hereby certify that I have reviewed and approve these data. �, Nza
Laboratory Representative
9
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC,
• Environmental Laboratories
Laboratory Certificate #165
Client: Harnett County
Project: TCLP
Client Sample ID: South Harnett Regional Calve
Sample Collection: 10/02/14
Meritech Sample ID: 10021489
1311 - TCLP Oroanics
Volatiles: SW-846 8260
Analysis: 10/08/14
Extracted:
10/06/14
Analyst: VW
V
Parameter
Result
Units
Det. Limit
ReQ. Limit
Dilution Factor
Benzene
<0.0200
mJL
0.0100
0.50
20
Carbon Tetrachloride
<0.0200
mg/L
0.0100
0.50
20
Chlorobenzene
<0.0200
mg/L
0.0100
100
20
Chloroform
<0.0200
mg/L
0.0100
6.0
20
1,2-Dichloroethane
<0.0200
mg/L
0.0100
0.50
20
1,1-Dichloroethene
<0.0200
mg/L
0.0100
0.70
20
Methyl Ethyl Ketone
<0.200
mg/L,
0.100
200
20
Tetrachloroethylene
<0.0200
mg/L
0.0100
0.70
20
Trichloroethene
<0.0200
mg/L
0.0100
0.50
20
Vinyl Chloride
<0.040
mg/L
0.020
0.20
20
Semi-Volatiless- SW-846 8270
Extraction: 10/04/14
Analysis: 10/10/14
Analyst:
PM
Parameter
Result
Units
Det. Limit
Rev. Limit
Dilution Factor
1.4-Dich:orobenzene
<0.100
mg/L
0.I00
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachlorocthane
<0.100
mg/L
0.100 -
3.00
10
o-cresol
<0,100
mg/L,
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mJL
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L,
0.100
400
10
2,4,6-Triehlorophenol
<0.100
MWL
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mJL
0.100
0.13
10
I hereby certify that I have reviewed and approve these data.
4a
•
Laboratory Representative
642 Tameo Road * Reidsville, NC 27320
[phone] Ph *
[phone] Fax

r7
3.20-I013
Chain of Custody Record (COC)
NPDES#:
Client: �cA�h y,.f� ,Pr,t,-,•�..�� Phone:
Address: -3y M C. K1;a>ti v im. ,, Fax:
�._f;���� Email:
Project:
P.O.th ' "
Attention: Turn Around Time*
* How would you like your report sent? RUSH work needs prior approval.
Circle all that apply: Email(preferred), Fax, Mail Std 10 days) 3-5 pays 2a rs
MER ���� INC,
*' ENVIRONMENTAL LABORATORIES
' .. 642 Tamco.Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com YY� 1
Sample Location and/or ID #
Sampling Dates �c Times
p g
Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test (s) Required
ce?
Yes—Cl
pH OK?
OK?
Date
Time
Date
Time
�UV�'1 � q�r ✓1G'"F-�f" irjrip.I
,,..._�
.�(%
A
C, — l
_CGtI (
Temperature Upon
Recelpt: .
Method of
Shipment:
*" Dechlorination
<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field prior
to preservation. *"'
Comments:
Compositor tf
Jug tt
❑ UPS
El Fed Ex
Are these results for regulatory purposes? Yes
No 0'
e ort '
i mg/L Q
mg/kg Q. ug/L Q
❑-Hand Delivery
Relinquished by; eDate:� Time:3JRece'
Other
ti
Relin Dat : Tinie:
-°6
eceived by:
Date: Time:
Relin fished by: ate: Time: 6ived
a 0 Dat y_, e;

•
Page: i of 2
Report Number: 15-029-0200
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59905
Sample Id : SOUTH HARNETT
99 zL A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www,aleastem.com
Project: SOUTH HARNETT/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/22/2015 15:30:00
Date Received: 01/29/2015 00:00
Date Reported: 02/02/2015
Total Solids *
40.26
402600
100.0
JM
01/29/2015 14:15
SM-254OG
Moisture *
59.74
100.0
JM
01/29/2015 14:15
SM-254OG
Total Kjeldahl Nitrogen
1.45
14500
10.0
JM
01/30/2015 08:50
SM-4500-NH3C-TKN
Total Phosphorus
0.74
7380
100
KM
01/30/2015 12:51
SW 6010C
Total Potassium
0.06
584
100
KM
01/30/2015 12:51
SW 6010C
Total Sulfur
0.45
4530
100
KM
01/30/2015 12:51
SW 6010C
Total Calcium
31.00
310000
100
KM
01/30/2015 12:51
SW 6010C
Total Magnesium
0.29
2850
100
KM
01/30/2015 12:51
SW 6010C
Total Sodium
0.03
321
100
KM
01/30/2015 12:51
SW 6010C
Total Iron
6100
100
KM
01/30/2015 12:51
SW 6010C
Total Aluminum
4200
100
KM
01/30/2015 12:51
SW 6010C
Total Manganese
117
5
KM
01/30/2015 12:51
SW 6010C
Total Copper
167
5
KM
01/30/2015 12:51
SW 6010C
Total Zinc
471
5
KM
01/30/2015 12:51
SW 6010C
Ammonia Nitrogen
0.04
397
10.0
JM
01/30/2015 08:50
SM-4500-NH3C
Organic N "
1.41
14103
10.0
01/30/2015 08:50
CALCULATION
Nitrate+Nitrite-N
405
2.00
JM
01/30/2015 08:45
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
01/30/2015 12:51
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

0
Page: 2 of 2
Report Number: 15-029-0200
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59905
Sample Id: SOUTH HARNETT
•
A&L Eastern Laboratories, Inc.
@P, 7621 W�hitepine Road Richmond, Virginia 23237 IBM) 743-9401 Fax [phone]
www.aleistern.com
Project: SOUTH HARNETT/NC CERT#257
REPORT OFANALYSIS Date Sampled: 1/22/2015 15:30:00
Date Received: 01/29/2015 00:00
Date Reported: 02/02/2015
Total Chromium
22
5
KM
01/30/2015 12:51
SW 6010C
Total Nickel
11
5
KM
01/30/2015 12:51
SW 6010C
Total Lead
12
5
KM
01/30/2015 12:51
SW 6010C
Total Arsenic
<3.0
3.0
KM
01/30/2015 12:51
SW 6010C
Total Mercury
<0.4
0.4
KM
01/30/2015 09:00
SW-7471B
Total Selenium
<5.0
5.0
KM
01/30/2015 12:51
SW 6010C
pH (Standard Units) *
12.24
2.00
JM
01/30/2015 08:50
SW-9045D
Calcium Carbonate Equivalent
74.20 742000
100
JM
01/30/2015 12:15
AOAC 955.01
Total Molybdenum
5
5
KM
01/30/2015 12:51
SW 6010C
Comments:
CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca" AND "Se". ALL OTHER QC DATA IS
ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

•
Page: 1 of 2
Report Number: 15-043-0205
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 60193
Sample Id : SOUTH HARNETT
A&L Eastern Laboratories, Inc.
7621 whitepine Road Richmond, Virginia 23237 (804) 743,9401 Fax [phone]
wlww,aleastom.com
Project: SOUTH HARNETT/NC CERT#257
REPORT OFANALYSIS
Date Sampled: 2/10/2015 11:00:00
Date Received: 02/12/2015 00:00
Date Reported: 02/19/2015
Total Solids *
35.12
351200
100.0
JM
02/13/2015 08:30
SM-2540G
Moisture *
64.88
100.0
JM
02/13/2015 08:30
SM-254OG
Total Kjeldahl Nitrogen
2.12
21200
10.0
JM
02/13/2015 09:15
SM-4500-NH3C-TKN
Total Phosphorus
0.92
9200
100
KM
02/13/2015 11:15
SW 6010C
Total Potassium
0.08
837
100
KM
02/13/2015 11:15
SW 6010C
Total Sulfur
0.47
4650
100
KM
02/13/2015 11:15
SW 6010C
Total Calcium
27.50
275000
100
KM
02/13/2015 11:15
SW 6010C
Total Magnesium
0.30
3000
100
KM
02/13/2015 11:15
SW 6010C
Total Sodium
0.04
360
100
KM
02/13/2015 11:15
SW 6010C
Total Iron
7520
100
KM
02/13/2015 11:15
SW 6010C
Total Aluminum
5000
100
KM
02/13/2015 11:15
SW 6010C
Total Manganese
305
5
KM
02/13/2015 11:15
SW 6010C
Total Copper
145
5
KM
02/13/2015 11:15
SW 6010C
Total Zinc
490
5
KM
02/13/2015 11:15
SW 6010C
Ammonia Nitrogen
0.05
541
10.0
JM
02/13/2015 09:15
SM-4500-NH3C
Organic N
2.07
20659
10.0
02/13/2015 09:15
CALCULATION
Nitrate+Nitrite-N
220
2.00
JM
02/13/2015 09:15
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
02/13/2015 11:15
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Llw
Our reports and letters are for- the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made mez-
to the work, the rest ills, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

•
Page: 2 of 2
Report Number: 15-043-0205
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 60193
Sample Id: SOUTH HARNE17
•
Vy AFL Eastern Laboratories, Inc.
A� 7621 Whltepine Road Richmond; Virginia 23237 [phone] Fax (804) 271-WS
www,aleastern.com
Project: SOUTH HARNETT/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 2/10/2015 11:00:00
Date Received: 02/12/2015 00:00
Date Reported: 02/19/2015
Total Chromium
27
Total Nickel
12
Total Lead
7
Total Arsenic
<3.0
Total Mercury
<0.4
Total Selenium
<5.0
pH (Standard Units) `
12.13
Calcium Carbonate Equivalent
61.90 619000
Total Molybdenum
<5
Comments:
CCE, SULFUR AND ORGANIC NITROGEN
NOT FOR COMPLIANCE PURPOSES.
AG TO FOLLOW
5
KM
02/13/2015 11:15
SW 6010C
5
KM
02/13/2015 11:15
SW 6010C
5
KM
02/13/2015 11:15
SW 6010C
3.0
KM
02/13/2015 11:15
SW 6010C
0.4
KM
02/12/2015 09:00
SW-7471 B
5.0
KM
02/13/2015 11:15
SW 6010C
2.00
JM
02/13/2015 09:15
SW-9045D
100
JM
02/16/2015 13:45
AOAC 955.01
5
KM
02/13/2015 11:15
SW 6010C
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn" AND "NA". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

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SL,2: Basic `less SU phis Sulrur, CAlcium, Magbvs um.Sodl'um. lion. Aluminum, Manprmse.. Copper And Zinc
6.03 Metals: Arsenic, Cadmium,.Qhromium, Mercury, Molybdenum", -Lead, Nickel,:Seleniuryv
(Copper & Zinc included in SL:2)
Nitrogko Ser m: Total'Kialdahl. Arru"wn; Nitrate&Qrpnie Nitruimn.
CCE; Calclum Carbonate'EgUIValent or Total neutralization Value (For Lime Treated Sludge)

•
•
South Harnett County WWTP Class A Cake Distribution Control
Wet Tons
Date
Location
pH
75
1/17/2014
Carolina Lakes
11.6
150
1/21/2014
Carolina Lakes
11.3
60
1/31/2014
Farrar Dairy Farm
11.3
100
2/8/2014
Farrar Dairy Farm
11.3
40
2/19/2014
Farrar Dairy Farm
10.9
132
3/10/2014
Farrar Dairy Farm
11.3
48
3/20/2014
Farrar Dairy Farm
11.12
48
3/20/2014
Carolina Lakes
36
3/22/2014
Danny McDonald
11
48
3/23/2014
Carolina Lakes
48
3/27/2014
Danny McDonald
11.3
132
3/28/2014
Farrar Dairy Farm
11.2
42
4/4/2014
Danny McDonald
11.1
42
4/8/2014
Danny McDonald
156
4/11/2014
Farrar Dairy Farm
11.3
48
4/14/2014
Farrar Dairy Farm
72
4/22/2014
Farrar Dairy Farm
11.6
42
4/28/2014
Farrar Dairy Farm
30
5/2/2014
Farrar Dairy Farm
192
5/9/2014
Farrar Dairy Farm
11.2
6
5/16/2014
Farrar Dairy Farm
11.3
6
5/20/2014
Farrar Dairy Farm
24
5/21/2014
Tony Dickens
6
5/27/2014
Tony Dickens
42
7/14/2014
Harnett Co. Landfill
11.5
66
7/23/2014
T. Wombles
6
8/27/2014
Carolina Lakes
84
8/30/2014
T. Wombles
11.6
78
9/5/2014
Carolina Lakes
24
9/10/2014
Carolina Lakes
11.3
60
9/25/2014
Carolina Lakes
11.6
72
10/31/2014
Harnett Co. Landfill
11.3
66
11/4/2014
Harnett Co. Landfill
10.8
42
11/13/2014
Harnett Co. Landfill
11.9
Total Wet Tons
2123
Dry Tons
1 424.6

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WWTi' WQ Permit Number: WQ0007066
WWTP Name: South Harnett Regional WWTP NPDES Number: NCO088366
Monitoring Period: From 01/01/2014 To 6/30/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) X Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitorine data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Steve Ward D' ector of Public Utilities
Preparer N and TitlVATe or print)
Signature 6f Prepare * Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
¢Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

•
•
Date
Tl
T2
T3
T4
T5
pH.
1/17/2014
158.1
159.4
143
15.1
141.4
11.6
1/21/2014
152.8
157.1
148
147.6
148
11.3
1/31/2014
152.6
156.41
151.1
149.7
148.1
11.3
2/8/2014
153
154.8
154.6
163.5
135.9
11.3
2/19/2014
149.2
151.7
152.2
155.5
152.3
10.9
3/10/2014
172.8
184.5
150.6
151.6
150.21
11.3
3/20/2014
153.9
162.5
166.9
151.1
150.7
11.12
3/20/2014
3/22/2014
145.6
150.9
154.7
177.7
158.1
11
3/23/2014
3/27/2014
146.2
151.3
155.2
163.4
157.3
11.3
3/28/2014
145.4
148.2
149.1
153.8
161.1
11.2
4/4/2014
170.1
149.2
150.1
147.61
145.3
11.1
4/8/2014
4/11/2014
163
154.3
155.1
152.6
150.71
11.3
4/14/2014
4/22/2014
157.4
155.1
154.3
151.9
151
11.6
4/28/2014
5/2/2014
5/9/2014
151.2
153.4
152.2
152
151.4
11.2
5/16/2014
149.1
151.1
151.7
151
149.71
11.3
5/20/2014
5/21/2014
5/27/2014
7/14/2014
147.3
149
150.8
151.3
149.31
11.5
7/23/2014
8/27/2014
8/30/2014
148
148.9
150.1
154.7
173.1
11.6
9/5/2014
9/10/2014
140.4
146
145.9
147.4
142.1
11.3
9/25/2014
144.3
147
147.3
148
147.4
11.6
10/31/2014
144.2
146.5
147
147.5
146.31
11.3
11/4/20141
1441
146.4
147.5
147.6
147.1
10.8
11/13/2014
143.7
146.11
146.3
147.1
148.2
11.9
Temperatures are in Farenheit Degrees

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WWTP WQ Permit Number: WQ0007066
WWTP Name: South Harnett Regional WWTP NPDES Number: NCO088366
Monitoring Period: From 07/01/2014 To 10/31/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) X Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlienhle to alternative norfnrmpd lClace A nr rlace Rl ommnlatn the fnlinwino mnnitnrinn da+a•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Steve Ward Director A Publi Utilities
Preparer Name and tle ( r print) r Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

•
Date
T1
T2
T3
T4
T5
pH
1/17/2014
158.1
159.4
143
15.1
141.4
11.6
1/21/2014
152.8
157.1
148
147.6
148
11.3
1/31/2014
152.6
156.41
151.1
149.7
148.1
11.3
2/8/2014
153
154.8
154.6
163.5
135.9
11.3
2/19/2014
149.2
151.7
152.2
155.5
152.3
10.9
3/10/2014
172.8
184.5
150.6
151.6
150.2
11.3
3/20/2014
153.9
162.5
166.9
151.1
150.71
11.12
3/20/2014
3/22/2014
145.6
150.9
154.7
177.7
158.1
11
3/23/2014
3/27/2014
146.2
151.3
155.2
163.4
157.31
11.3
3/28/2014
145.4
148.2
149.1
153.8
161.1
11.2
4/4/2014
170.1
149.2
150.1
147.6
145.3
11.1
4/8/2014
4/11/2014
163
154.3
155.1
152.6
150.71
11.3
4/14/2014
4/22/2014
157.4
155.1
154.3
151.9
151
11.6
4/28/2014
5/2/2014
5/9/2014
151.2
153.4
152.2
152
151.4
11.2
5/16/2014
149.1
151.1
151.7
151
149.7
11.3
5/20/2014
5/21/2014
5/27/2014
7/14/2014
147.3
149
150.8
151.3
149.3
11.5
7/23/2014
8/27/2014
8/30/2014
148
148.9
150.1
154.7
173.1
11.6
9/5/2014
9/ 10/2014
140.4
146
145.9
147.4
142.1
11.3
9/25/2014
144.3
147
147.3
148
147.4
11.6
10/31/2014
144.2
146.5
147
147.5
146.3
11.3
11/4/2014
144
146.41
147.5
147.6
147.1
10.8
11/ 13/2014
143.7
146.1
146.3
147.1
148.2
11.9
Temperatures are in Farenheit Degrees

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
i
Facility Name: Harnett County WWTP WQ Permit Number:
WWTP Name: South Harnett Regional WWTP NPDES Number:
Monitoring Period: From 11/01/2014 To 11/30/2014
WQ0007066
NCO088366
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) X Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahle to alternative norfnrmod Win.,Q A nr Claw R) rmmAete the follnwina manitnrinu data!
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 0 h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Mt. 3 Option/Mt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Steve Ward,DirectPr of Public Utilities
0 Preparer Name Title pe or print)
, ^ n--? f
Signature of e-
parer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

i
•
Date
Tl
T2
T3
T4
T5
pH
1/17/2014
158.1
159.4
143
15.1
141.4
11.6
1/21/2014
152.8
157.1
148
147.6
148
11.3
1/31/2014
152.6
156.4
151.1
149.7
148.1
11.3
2/8/2014
153
154.8
154.6
163.5
135.9
11.3
2/19/2014
149.2
151.7
152.2
155.5
152.3
10.9
3/10/2014
172.8
184.5
150.6
151.6
150.2
11.3
3/20/2014
153.9
162.5
166.9
151.1
150.7
11.12
3/20/2014
3/22/2014
145.6
150.9
154.7
177.7
158.1
11
3/23/2014
3/27/2014
146.2
151.3
155.2
163.4
157.3
11.3
3/28/2014
145.4
148.21
149.1
153.8
161.1
11.2
4/4/2014
170.1
149.2
150.1
147.6
145.3
11.1
4/8/2014
4/11/2014
163
154.3
155.1
152.6
150.7
11.3
4/14/2014
4/22/2014
157.4
155.1
154.3
151.9
151
11.6
4/28/2014
5/2/2014
5/9/2014
151.2
153.4
152.2
152
151.4
11.2
5/16/2014
149.1
151.1
151.7
151
149.7
11.3
5/20/2014
5/21/2014
5/27/2014
7/14/2014
147.3
149
150.8
151.3
149.3
11.5
7/23/2014
8/27/2014
8/30/2014
148
148.9
150.1
154.7
173.1
11.6
9/5/2014
9/10/2014
140.4
146
145.9
147.4
142.1
11.3
9/25/2014
144.3
147
147.3
148
147.4
11.6
10/31/2014
144.2
.146.5
147
147.5
146.3
11.3
11/4/2014
1441
146.4
147.51
147.6
147.11
10.8
11/ 13/2014
143.7
146.11
146.3
147.1
148.2
I 11.9
Temperatures are in FRrenheit Degrees

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WWTP WQ Permit Number: WQ0007066
WWTP Name: South Harnett Regional WWTP NPDES Number: NCO088366
Monitoring Period: From 12/01/2014 'To 12/31/2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) X Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
U nnnlicahle to alternative nerfarmed (Class A or Class R1 rmmnlete the fnllnwino mnnitnrino data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6'h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
— explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Steve Ward,DirecA of PYQic Utilities
Preparer Name X16e or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

•
Date
Tl
T2
T3
T4
T5
pH
1/17/2014
158.1
159.4
143
15.1
141.4
11.6
1/21/2014
152.8
157.1
148
147.6
148
11.3
1/31/2014
152.6
156.41
151.1
149.7
148.1
11.3
2/8/2014
153
154.8
154.6
163.5
135.9
11.3
2/19/2014
149.2
151.7
152.2
155.5
152.3
10.9
3/10/2014
172.8
184.5
150.6
151.6
150.2
11.3
3/20/2014
153.9
162.5
166.9
151.1
150.71
11.12
3/20/2014
3/22/2014
145.6
150.9
154.7
177.7
158.1
11
3/23/2014
3/27/2014
146.2
151.3
155.2
163.4
157.3
11.3
3/28/2014
145.4
148.2
149.1
153.8
161.1
11.2
4/4/2014
170.1
149.2
150.1
147.6
145.3
11.1
4/8/2014
4/11/2014
163
154.3
155.1
152.6
150.7
11.3
4/14/2014
4/22/2014
157.4
155.1
154.3
151.9
151
11.6
4/28/2014
5/2/2014
5/9/2014
151.2
153.4
152.2
152
151.4
11.2
5/16/2014
149.1
151.1
151.7
151
149.7
11.3
5/20/2014
5/21/2014
5/27/2014
7/14/2014
147.3
149
150.8
151.3
149.31
11.5
7/23/2014
8/27/2014
8/30/2014
148
148.9
150.1
154.7
173.11
11.6
9/5/2014
9/10/2014
140.4
146
145.9
147.4
142.1
11.3
9/25/2014
144.3
147
147.3
148
147.4
11.6
10/31/2014
144.2
146.5
147
147.5
146.3
11.3
11/4/20141
144
146.4
147.51
147.6
147.1
10.8
11/13/2014
143.7
146.1
146.3
147.1
148.2
11.9
Temperatures are in Farenheit Degrees