WQ0014248_Residual Annual Report 2014_20150303

4K
ClqERAW
February 25, 2015
Mr. Ed Hardee
NCDENR/DWQ/Water Quality Section
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Mr. Hardee:
RECEIVENENOWR
MAR 0 3 2015
WaterQuajgy
Permitting Section
Enclosed is the annual Biosolids marketing and distribution report.
Please contact me if you have any questions or comments.
Sincerely,
Sherry Turner
Industrial Pretreatment Coordinator
QA/QC Director
Cheraw Public Utility Department
Post Office Box 219, Cheraw, South Carolina 29520
843.537.8440, Fax [phone]
www.cheraw.com
_w_
-�_A
- --
i

AININ U EiL LAIN L AYYL1%_A 11U1N %-r n 111' 1l .A 11UIN i' UJOUV1
i,,Permit#: _ 0001424A County: _h _mot rfi P1 � Year: 2014
Facility Name (as shown on permit).: Town of Cheraw
Land Application Operator: Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calender year?
® Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit: .
Total number of fields land application occurred during the year: _5_,
Total amount of dry tons applied during the year for all application sites: 6-9
Total number of acres land application occurred during the year: 1 33
Part B:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. ® Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates- in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ricky Ingram/Public' 0 ` Utility Director (�
Permittee Name and Title (type or print) Signature of ermitt Date
Or
Signature of reparer* D to
(if different from Permittee)
" Preparer is defined in 40 CFR Part 503.9 (r)
Signiture of Land Applier Date
(if different from Permittee and Preparer)
Author Daryl D. Merritt DENR FORM ACF (7/2002)

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: WQ0014248 FACILITY NAME: Town of Cheraw
PHONE: [phone] COUNTY: Chesterfield OPERATOR:
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? El Yes ❑No No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources s include NPDES # if
() (.
applicable)
Volume (dry tons)
Recipient Information
Admendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
SCO020249_
10.6
26.5
37.1
February
18.03
40.06
58.09
Vernon Dye
14-.29
Deer plot
March
11.28
24.00
35..28
April
31.72
57.68
89.40
Vernon Dye
12.61
Deer plot
May
0
0
0
June
7.58
12.64
20.22
July
10.73
17.30
28.03
August
0
0
0
September
4.63
7.35
11 98,
October
0
0
0
November
10.94
19.19
30.13
December
23.81
50.66
74.47
Totals:
Annual (dry tons):
129.32
255.38
384.70
26-90
Admendment(s) used:
I Lime
Bulking Agent(s) used:
* If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. ® Yes ❑ No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the perrpit and reported for the year as required and three (3) copies of certified laboratory results are attached
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization.was received from the Division of Water
Quality.
3. No contravention,of Ground Water Quality Standards occurred at a monitoring well,
"I certify, under penalty of law, that the above information is,.to the best of my knowledge and belief, true, accurate and complete. I am aware
that there are significant penalties for submitting false informaiton, including the possibility of fines and imprisonment for knowing violations."
Signature of P rmitte Date Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
Author Daryl D. Merritt DENR FORM DMSDF (7/2002)

TOWN OF CHERAW WASTEWATER TREATMENT FACILITY
BIOSOLIDS REPORT 2014
MONTH
PRESS
HOURS
DRY CAKE
SOLIDS T.
TONS LIME
USED
%
LIME
TOTAL
DRY PROD.
LIME $/
TON PROD.
POLY $/
TON CAKE
LBS. POLY/
TON CAKE
LBS. POLY
USED
JAN
59.90
26.50
10.60
40.00
37.10
70.25
5.52
2.08
55.00
FEB
92.20
40.06
18.03
45.01
58.09
79.23
7.30
2.75
110.00
MAR
45.30
24.00
11.28
47.00
35.28
82.73
18.29
6.88
165.00
APR
94.40
57.68
31.72
54.99
89.40
96.98
7.61
2.86
_ 165.00
MAY
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
JUN
26.40
12.64
7.58
59.97
20.22
105.76
11.57
4.35
55.00
JUL
33.70
17.30
10.73
62.02
28.03
109.17
8.46
3.18
55.00
AUG
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
SEP
12.80
7.35
4.63
62.99
11.98
110..88
59.71
22.45
165.00
OCT
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
NOV
35.30
19.19
10.94
57.01
30.13
307.89
38.12
14.33
275.00
DEC
107.70
50.66
23.81
47.00
74.47
373.83
17.33
2.17
330.00
TOT
507.70
255.38
129.32
_
384.70
1,375.00
AVG
42.31
21.28
10.78
52.89
32.06
111.39
14.49
5.38
114.58
MIN
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
MAX
107.70
57.68
31.72
62.99
89.40
373.83
59.71
22.45
330.00

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014248 Laboratory: 1) Davis & Brown Labs
Facility Name: Town Of Cheraw 2) Clemson University
NPDES # or
WQ#: SCO020249
WWTP Name: Town of Cheraw WWTP
Residual Analvsis nata
3)
4)
5)
Sample or
Composite Date
1 /15/14
1 /15/14
3/19/14
3/19/14
5/21 /14
5/21 /14
7/16/14
7/16/14
9/17/14
9/17/14
11 /19/1
1 /19/14
Percent Solids
54.50
47.58
48.30
52.60
62.60
62.22
81.40
62.29
86.1/0
719.41
77.70
81.40
Arsenic
3.10
0.967
0.966
1.26
1.93
0.861
Cadmium
0.969
0.967
0.966
0.982
2.43
0.861
Chromium
49.0
35.5
21.4
32.8
19.6
1.28
Copper
42.6
28.6
25.7
37.5
25.7
1.27
Lead
4.62
3.81
2.03
2.39
3.22
0.861
Mercury
0.039
0.039
0.034
0.041
0.040
0.040
Mol bdenum
3..88
3.87
9.66
78.5
9.74
3.45
Nickel
23.9
57.3
35.1
59.0
26.5
23.2
Selenium
0.969
0.967.
0.966
0.982
0.974
0.861
IQ
Zinc
238
166
173
191
181
9.28
v
TK
21826
117329
12737
12405
11151
13286
Ammonia -Nitro en
631
1331
964
311
0
491
Nitrate and Nitrite
3.99
2.00
428
4.00
152
4.00
Total Phosphorus
121379163
10760
9162
7789
7328
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Lfo l ,s
Signature of 4eparer Date
r
Author Daryl D. Merritt DENR FORM RSSF (7/2002)

ANNUAL METALS EIELD LOADING SUMMARY EURM
K
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Cheraw Total Dry Tons Applied (Annual): 6.1
WQ0014248 Cation Exchange Capacity (non 503 only):
VernonnDye Owner: Vernon Dye
7 Acres Permitted: Site #: 165 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
_hosEMEEEEEEEEEE
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
EMM
Total
h
..
"I certify, under penalty of law, that this document was prepared under my,direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted: I am aware that there are significant penalties for submitting false information,
includin jtthh possibility of fines .and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt ' DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. n
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw
Owner: Vernon Dye
Site #: 165 Field #:
Permit #: WQ0014248
Operator: Vernon _ Dye
Acres Utilized: 7
Annual Dry Tons Applied:' 6.1
Cation Exchange Capacity (non 503):
Acres Permitted:
A
SGalf
Totals
Per
Acre
Solids
As
Deci-
1
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
i e .
Cond.
Dry,
Wet,
Moist
Inches
Preci p'
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
`Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select .
Crop
P 1 or Crop
2
Cu.Yd.
Report
TTotals
Gal.
Crop 1
Crop 2
Feb
N/A
N/A`�'
.5104
.87
S
0.5
21826
631
3.99
i
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P 1PAN
1
PAN 2
Lime Ap lied
Annuallbs/acre
.01063
.00330
.16705
.14523
.01575
.00013
.01323
.08148
.00330
.08114
—41.378'1
1
Date
lbs/ac
Current Cumulative lbs/acre
.01063 .00330 .16705 .14523 .01575 .00013 .01323 .0814 .00330 .08114
_
Prior Years Cumulative lbs/acre
Permitted C. P. L. R. * *
Permit PAN Limit Ist/2nd Crop
-a certuy, unaer penalty or iaw, tnat tins a4
designed to assure that qualified personnel
significant penalties for submitting false im
Signature of Land
t was prepared under my direction or supervision in accordance with a system
ly gathered and evaluated the information submitted. I am aware that there are
on, including the possibility of fines and imprisonment for knowing violations."
Z =yo - l S *Application Method: S - Surface, IN - Injection, INC - Incorporation
Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation - LO
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)

606
0
0�
ABERDEEN 32 MI. 5053 IV NE
607 ROCKINGHAM 5 MI. 608 (ROCKINGHAM) ! 609 . 610 4
I {u
`I q(\�� /!�', �^Zs'o rn\'.._•-� .�`\ (� n" ///) it �� z5p -t� 1
>>�&05v� L
')) ° Vernon Dye site 165
G
�Z W34.8420914 7 acres �� n
N-79.813528 6.8 dmt �S

DIGGS QUADRANGLE
NORTH CAROLINA—SOUTH CAROLINA tplb5
7.5 MINUTE SERIES (TOPOGRAPHIC)
'52'30"
)000 FEET
C.)
;54

ANNUAL METALS FIELD LOADING SUMMARY YORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #: .
Total Dry Tons Applied (Annual):
WQ0014248 Cation Exchange Capacity (non 503 only):
Town of Cheraw
Operator: Vernon Dye Owner: Vernon Dye
Acres Used: 6 Acres Permitted: Site #: 166 Field #:
5.1.
Residual Analysis Data (Leavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
,LphorusEENEENEENEEN
Annual Heavy�Metal Field Loadings (Calculated in lbs/acre):
®
'
______�____
•
Phos-
EMENEENEENEEM
phorusTotal
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier. Bate
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANKYORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name: Town of Cheraw
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Permit #: WQ0014248 Annual Dry Tons Applied: 5.1
Owner: Vernon Dye Operator: _ Vernon Dye Cation Exchange Capacity (non 503):
Site #: 166 Field #: Acres Utilized: 6 Acres Permitted:
q
S'Galf
Totals
Per
Acre
Solids
As
Deci-
mal
Dry
Tons
� Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop
P 1 or Crop
2
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Feb
N/A
N/A
.5104
.85
S
0.5
21826
631
3.99
X
i
i
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
.00967
.00302
.15284
.13288
.01441
.00012
.0121
.07455
.00302
.74239
43.36
Date
lbs/ac
Current Cumulative lbs/acre
.00967 .00302 .15284 .13288 .01441 .00012 .0121 .07455 .00302 .74239
Prior'Years Cumulative lbs/acre
Permitted C. P. L. R. * * *
Permit PAN Limit..I st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S -Surface, IN Injection, INC -Incorporation
Signature of Land A er Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***C.P:L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)

4 4
606
5053 IV NE
607ABERDEEN ROCKINGH 32 Mf.AM 5 Mi. i 608 (ROCKINGHAM) ! 609
OCKIN_
Q Ij. it ,
NO
Vernon Dye site 166
W 34.8502977 6 acres
N-79.807177 5.6 dmt
1 ..
�LZoo

DIGGS QUADRANGLE
NORTH CAROLINA-SOUTH CAROLINA Soyl
7.5 MINUTE SERIES (TOPOGRAPHIC)
°52'30"
D 000 FEET
C.)
{54

ANNUAL ME'I'AL5 YIELD LUADING 6UMMAKY r'UKM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #: -
Town of Cheraw
WQ0014248
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
3.1
Operator: Vernon Dye Owner: Vernon Dye
Acres Used: 4 Acres Permitted: Site #: 167 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
I
Phos-
phorusEMENEEMENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
I
Total
Phos-
_phorus'EMENEEMENEENE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applie Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cheraw Permit #: W00014248
Owner: Vernon Dye Operator: Vernon Dye
Site #: 167 Field #:
Acres Utilized: 4
Annual Dry Tons Applied:" 3.1
Cation Exchange Capacity (non 503):
Acres Permitted:
q
Totals
Per
Acre
o
Solids
As
Dec*-
1
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
ois
Inches
Preci p'
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
nation
Rate
TKN
Ammo
nia=
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
-Specify
Gal.
CuNd.
Report
Totals
in Gal.
Crop 1
Crop 2
Feb
N/A
N/A
.5104
.77
S
0.5
21826
631
3.99
X
j
,h
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se.
Zn
P
PAN 1
PAN 2
Lime Ap
lied
Annuallbs/acre
.00876.00274
.13846.12037
.02202.00011
.01096
.06753
.00274 1.67251
39.28
Date
lbs/ac
Current Cumulative lbs/acre
.00876
00274
.13846 .12037 1.02202 .00011 .01096 .0675 .00274 .67251
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.*-**
Permit PAN Limit lst/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
i
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land plier I Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)

ABERDEEN 32 MI. 5053 IV NE
606 Q 607 ROCKINGHAM 5 mi., 608 (ROCKINGHAM) 1609
ILL
C�
11
Vernon Dye site 167 j(
�20`0) W 34.8444512 4 acres
N-79.801168 3.4 dmt
\
LN
) I,•",- '~' 1 `

DIGGS QUADRANGLE
NORTH CAROLINA—SOUTH CAROLINA yohl���`
7.5 MINUTE SERIES (TOPOGRAPHIC)
_ 7AeaS'
-52130"
D OOO FEET
C.)
154

ANNUAL METALS FIELD LOADING SUMMARY r'ORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres. Used:
Town of Cheraw
Total Dry Tons Applied (Annual): 6.3
WQ0014248 Cation Exchange Capacity (non 503 only):
Vernon Dye
8 Acres Permitted:
Owner: Vernon Dye
Site #: 169 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Em
. .
posite
Date
i
Offim
• •
_S�__-_�__�
Total
.,E
..
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
_Rhorus-�NMENEENEENEEM
"I certify, under penalty of law, that this ,document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
_cs
Signature of Land Applier. �/ Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name: Town of Cheraw
Owner: Vernon Dye
Site #: 169 Field #:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Permit #: WQ0014248 Annual Dry Tons Applied:
Operator:. Vernon Dye Cation Exchange Capacity (non 503):
Acres Utilized: 8 Acres Permitted:
6.3
�►
A
SGalf
Totals
Per
Acre
Solids
As
Deci-
al
Dry
Tons
Per
Acre
Residual
Sources
(Summarize
i e
Cond.
Dry,
Wet
ois
Inches
Preci p'
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
nation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1 Crop
P or P
2
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop2
Apr
N/A
N/A
50.45
.79
S
0.5
17329
1331
2.00
X
i
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Ap
lied
Annuallbs/acre
.00316
.00316
.11613
09356
.01246
00013
01266
18744
00316
.54302
27.53
Date
lbs/ac
Current Cumulative lbs/acre
00316
0 1
.11i61-3 .09356 .01246 .00013 .01266 18744 .00316 .54302
Prior'Years Cumulative lbs/acre
Permitted C. P. L. R. * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including .the possibility of fines and imprisonment for knowing violations."
2- -Z0, c s *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land—pp�lier ! Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt
DENR FORM FSF (7/2002)

i
LZ
Ll
w
3865
% 1,00Vernon Dye site 169
34.9105342 8 acres
-80.128398 7.0 dmt
•
5 5'
l t
\. �. ��` ^ � � h `4.. � 485 �.• I' '� 1. .,. � k ij ! 0 3863
�. .��'/i• (/�
� o � .l r �,J+ ,�,� I. /� ...� � ,�) � i .mil 'IlJ ~� � • �� •, 3362-
/ 1 `Y�( / 1 - i^ 38
ZIN
?l
1118.;h�/,/ .' I 1 ' may* r� \ I c ` �� ;JJ'/'/�cl J I\\ 3B60000m.N Q

RUSSELLVILLE QUADRANGLE
NORTH CAIZOLINA—ANSON CO. a
7.5 MINUTE SERIES (TOPOGRAPHIC)
m
Is 6
'30"

ANNUAL METALS kIELD LOADINU NUMAIARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Cheraw
Total Dry Tons Applied (Annual): 6.3
WQ0014248 Cation Exchange Capacity (non 503 only):
Vernon Dye Owner: Vernon Dye
8 Acres Permitted:
Site #: 170 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
INIM M.
Total
Phos-
__ph6rusEMEEEEEEEENEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
2=Zo-(S
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (712002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name: Town of Cheraw
Owner: Vernon Dye
Site #: 170
Field #:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Permit #: WQ0014248
Operator: Vernon Dye
Acres Utilized: g
Annual Dry Tons Applied:' 6.3
Cation Exchange Capacity (non 503):
Acres Permitted:
A
S�Galf
Totals
Per
Acre
Solids
As
Deci-
l
D
Dry
Tons
Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
is
Inches
Preci p'
Past 24
Hrs.
pp ._
A It
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
T
Ammo
nia-
Ni-
trogen
Ni-
trate-
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Apr
N/A
N/A
.5045
.79
S
0.5
-173291
133T
2.00
X
i
i
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
.00316
.00316
.11613
.09356
.01246
.00013
.01266
.18744
.00316
.54302
27.53
Date
lbs/a7
Current Cumulative lbs/acre
.00316 .00316 .11613 .09356 .01246 .00013 .01266 .18744 .00316 .54302
F== I
Prior'Years Cumulative lbs/acre
Permitted C. P. L. R. * * *
Permit PAN Limit Ist/2nd Crop
I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z Z� / s *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Appli Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (7/2002)

r;�r LC
Lj
W h
o p�
i0s
f� r 45 3B66
4Po ho o� J d
3865
sso �
ED
-
r.� (�'• �� 55'
Vernon Dye site 170
en '� W 34.8994830 8 acres
N.-80.127411 7.0 dmt
i
3862
i i � �' �.�%•� t � ���� .ram \ � � 1
4196' 38
61
Soo
71

RUSSELLVILLE QUADRANGLE
NORTH CAROLINA-ANSON CO. 5
7.5 MINUTE SERIES (TOPOGRAPHIC)
)0
)00
'30"

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: January 15, 2014
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
2.84
41.00
1.80
158.23
316.45
Cadmium, Total
0.89
39.00
1.70
478.07
956.14
Chromium, Total
44.95
1200.00
134.00
745.20
1490.41
Copper, Total
39.08
1500.00
67.00
428.58
857.16
Lead, Total
4.24
300.00
13.00
766.77
1533.55
Mercury, Total
0.04 '
17.00
0.75
5240.38
10480.77
Molybdenum, Total
3.56
18.00
0.80
56.19
112.37
Nickel, Total
21.93
420.00
18.70
213.21
426.42
Selenium, Total
0.89
36.00
4.50
1265.48
2530.96
Zinc, Total
218.35
1525.00
125.00
143.12
286.24
PCB
BDL
1.60
Actual metal content less than amount indicated
Biosolids
Biosolids Maximum
Maximum
Nutrient
Nutrient Crop/Soil Application
Application
Content,
Content, Requirement, Rate,
Rate,
ppm
% #/Acre" DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
315.26
0.03
Organic Nitrogen
10597.94
1.06
Incorporated Available Nitrogen
6615.17
0.66 120.00 4.54
9.07
Surface Available Nitrogen
6520.60
0.65 120.00 4.60
9.20
Phosphorus as P205
6068.73
0.61 80.00 3.30
6.59
Potassium as K20
903.74
0.09 50.00 13.83
27.66
Calcium, Total
133611.81
13.36
Calcium as CaO
167056.54
18.71
Calcium as CaCO3 (CCE)
317660.75
31.77 2000.00 1.57
3.15
Magnesium, Total
1197.98
0.12
Manganese
42.03
0.00
Sulfur
1749.68
0.17
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids.
WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: B43-537-8442
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:

Client:
CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact:
SHERRY TOLSON
Client #:
168
Sample Date:
15-Jan-14
SDG #:
SDG-097062
Parameter
Davis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
South Carolina Certification Number: 21117
Receipt Date: 16-Jan-14
Report Date: 07-Feb-14
Approved By:
Reporting
Result Limit Unit Method
Van Ward
Lab Director
Flag Date Time Analyst
LSID-214633
1001-C
Acid Digestion (Liquids)
YES
EPA 200.2
1/20/2014
1:00
JR
Chromium, Total
0.005
0.005
mg/L
EPA 200.7
1/20/2014
13:40
JR
Copper, Total
0.283
0.005
mg/L
EPA 200.7
1/20/2014
13:40
JR
Manganese, Total
0.066
0.005
mg/L
EPA 200.7
1/20/2014
13:40
JR
Zinc, Total
0.029
0.005
mg/L
EPA 200.7
1/20/2014
13:40
JR
LSID-214634
1002-C
Acid Digestion (Liquids)
YES
EPA 200.2
1/20/2014
1:00
JR
Copper, Total
0.332
0.005
mg/L
EPA 200.7
1/21/2014
-10:07
JR
Zinc, Total
0.102
0.005
mg/L
EPA 200.7
1/21/2014
10:07
JR
LSID-214635
1-15-14-500 BIO SOILDS
Arsenic, TCLP
<0.050
0.05
mg/l
1311/6010C/7470
S16
1/24/2014
9:59
ALT
Barium, TCLP
0.41
0.15
mg/1
1311/6010C/7470
S16
1/24/2014
9:59
ALT
Cadmium, TCLP
<0.050
0.05
mg/1
1311/6010C/7470
S16
1/24/2014
12:48
JDG
Chromium, TCLP
<0.050
0.05
mg/l
1311/6010C/7470
S16
1/24/2014
9:59
ALT
Lead, TCLP
<0.050
0.05
mg/l
1311/6010C/7470
S16
1/24/2014
9:59
ALT
Mercury, TCLP
<0.001
0.001
mg/1
1311/6010C/7470
S16
1/21/2014
10:43
ClIM
Page 2

1
Avis&.Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TOLSON
Client #: 168
Sample Date: 15-Jan-14
SDG #: SDG-097062
Parameter
Result
Selenium, TCLP
<0.050
Silver,TCLP
<0.050
TCLP Extraction
YES
TCLP Metals
PASS
Ignitability
>170
Acid Digestion (Solids)
YES
Selenium, Total
<0.969
TCLP, Pesticides
BDL
TCLP, Herbicides
BDL
pH (Waste)
13
pH (Waste) measured in water at
21.1
TCLP
PASS
Percent Moisture
45.5
Aluminum, Total
6050
Arsenic, Total
3.10
Cadmium, Total
<0.969
Chromium, Total
49.0
Copper, Total
42.6
Lead, Total
4.62
Molybdenum, Total
<3.88
Nickel, Total
23.9
Reporting
Limit Unit
0.05 mg/l
0.05 mg/l
0.969
0.1
3.9
0.959
0.969
0.969
0.969
0.969
3.88
0.969
P/F
Deg. F
mg/kg
mg/L
mg/L
S.U.
Deg. C.
P/F
wt%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
South Carolina Certification Number: 21117
Receipt Plate: 16-Jan-14
Report Date: 07-Feb-14
Approved By: ziey— Al
Van Ward
Lab Director
Method Flag
1311/6010C/7470 S16
1311/6010C/7470 S16
1311/6010C/7470 S16
1311/6010C/7470 S16
D93 / 1010A S16
EPA 200.2
EPA 7010
EPA 8081A S16
EPA 8151A S16
EPA 9045D S 16
EPA 9045D S16
SW-846 S16
SW846 3540
SW846 6010C
SW846 6010C
SW846 6010C
SW846 6010C
SW846 6010C
SW846 6010C
SW846 6010C
SW846 6010C
Date
1/24/2014
1/24/2014
1/19/2014
1/24/2014
1/25/2014
1/21/2014
1/30/2014
1/23/2014
1/22/2014
1/20/2014
1/20/2014
1/24/2014
1/20/2014
1/27/2014
1/30/2014
1/27/2014
1/27/2014
1/27/2014
1/27/2014
1/27/2014
1/27/2014
Time
9:59
9:59
9:09
12:48
11:40
9:00
10:54
11:59
22:15
12:26
12:26
9:59
16:34
12:23
10:54
11:02
11:02
11:02
11:02
12:23
11:02
Analyst
ALT
ALT
JDG
AS
JR
JR
CBB
KLM
MGM
MGM
ALT
JW
JR
JR
JR
JR
JR
JR
JR
JR
Page 3

avis & Brown
PO Box 1503S
Quinby, SC 29506
[phone] FAX: [phone]
Certificate ®f Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TOLSON
Client #: 168
Sample Date: 15-Jan-14
SDG #: • SDG-097062
Reporting
Parameter
Result
Limit
Unit
Zinc, Total
238
0.969
mg/kg
Mercury, Total
<0.039
0.039
mg/kg
PCB
BDL
mg/kg
Reactivity, Cyanide
<0.125
0.125
mg/kg
Reactivity, Sulfide
<25
25
mg/kg
Paint Filter
PASS
P/F
South Carolina Certification Number: 21117
Receipt Date: 16-Jan-14
Report Date: 07-Feb-14
Approved By: 1
Van Ward
Lab Director
Method
Flag
Date
Time
Analyst
SW846 6010C
- 1/27/2014
11:02
JR
SW846 7470A
1/24/2014
10:00
Co
SW846 8082A
S16
1/23/2014
10:58
ND
SW846 9010
S16
1/22/2014
22:01
NJM
SW846 9030
S16
1/22/2014
16:00
DJD
SW846 9095
S16
1/20/2014
9:51
JBG
Page 4

Analytical Environmental Services, Inc
Date: 30-Jan-14
Client: Davis & Brown
Project: 214631 Dates Report
Lab Order: 1401 E22
Lab Sample ID Client Sample ID
1401E22-001A 214631
Collection Date Matrix Test Name
1/15/2014 9:10:OOAM Aqueous Inorganic Anions by IC
TCLP Date Prep Date Analysis Date
01/22/2014
Page 6 of 6

Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 214631
Worlcorder: 1401E22
Date: 30-Jan-14
ANALYTICAL QC SUMMARY REPORT
Batc11ID: R260072
Sample ID: MB-11260072
Client ID:
Units: urg/L
Prep Date:
Run No: 260072
SampleType: MBLK
TestCode: Inorganic Anions by IC E300.0
BatchID: R260072
Analysis Date: 01/22/2014
Seq No: 5466355
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Fluoride BRL 0.200
Sample ID: LCS-R260072
Client ID:
Units: mg/L
Prep Date:
Run No: 260072
SampleType: LCS
TestCode: Inorganic Astons by IC F300.0
BatcbID: IZ260072
Analysis Date: 01/22/2014
Seq No: 5466350
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Fluoride 4.784 0.200 5.000 95.7 90 110
Sample ID: 1401E81-001EMS
Client ID:
Units: ing/L
Prep Date:
Run No: 260072
SampleType: MS
TestCode: Inorganic Anions by IC E300.0
MOM R260072
_ Analysis Date: 01/22/2014
Seq No: 5466375
Analyte
Result RPT Limit SPK value SPIC Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Fluoride 5.040 0.200 5.000 101 90 110
Sample ID: 1401E81-001EMSD
- Client ID:
Units: ing/L
Prep Date:
Run No: 260072
SampleType: MSD
TestCode: Inorganic Anions by IC EMU
Batc11ID: R260072
Analysis Date: Ol/22/2014
Seq No: 5466376
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Fluoride 5.123 0.200 5.000 102 90 110 5.040 1.64 20
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantilation range)
N Analytenot NELACcertified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 6 of 6

Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
Date Received_
Description
Sample ID
Collected By
Collection Date :
January 17, 2014
214635
01/15/14 13:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
January 27,2014
ESC Sample # L678659-01
Site ID
Project #
Parameter
Dry Result
Det. Limit
Units
Method
Date
Analyst
Total Solids
61.2
0.100
%
2540
G-20
01/20/14
1512
KDW
Polychlorinated Biphenyls
PCB 1016
BDL
0.028
mg/kg
8082
A
01/23/14
1056
ND
PCB 1221
BDL
0.028
mg/kg
8082
A
O1/23/14
105B
ND
PCB 1232
BDL
0.028
mg/kg
8082
A
01/23/14
1058
ND
PCB 1242
BDL
0.028
mg/kg
8082
A
O1/23/14
1058
ND
PCB 1248
BDL
0.028
mg/kg
8082
A
O1/23/14
1058
ND
PCB 1254
BDL
0.028
mg/kg
8082
A
O1/23/14
105E
ND
PCB 1260
BDL
0.028
mg/kg
8082
A
O1/23/14
1058
ND
PCBs Surrogates
Decachlorobiphenyl
71.5
% Rec.
8082
A
O1/23/14
1058
ND
Tetrachloro-m-xylene
70.2
o Rec.
8082
A
O1/23/14
105E
ND
i
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Laboratory Certification Numbers:
AIHA - 100789, AL - 40660, CA - I-23271 CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - B4004, TN - 2006, VA - 00109, WV - 233
Note: AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 01/27/14 10:09 Printed: 01/27/14 10:09
Page 2 of 6

Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
Date Received January 17, 2014
Description
Sample ID 214635
Collected By
Collection Date 01/15/14 13:00
Parameter
Ignitability
pH
Paint Filter Test
Reactive CN (SWB46 7.3.3.2)
Reactive Sulf.(SW846 7.3.4.1)
TCLP Extraction
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
TCLP ZHE Extraction
TCLP Volatiles
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichlorcethene
2--Butanone (MEK)
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogate Recovery
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax;I.D. 62-0814289
Est. 1970
January 27,2014
ESC Sample # : L678659-02
Site ID
Project # .
Result
Det. Limit
Units
Method
Date/Time
Analyst D.
See Footnote
Deg. F
D93/1010A
O1/25/14
1140
AS 1
13.
su
9045D
O1/20/14
1226
MGM 1
See Footnote
o
9095B
O1/20/14
0951
JBG 1
BDL
0.125
mg/kg
9012B
O1/22/14
2201
NJM 1
BDL
25.
mg/kg
9034/9030
01/22/14
1600
DJD 1
-
1311
01/19/14
0909
MVE 1
BDL
0.0010
mg/l
7470A
O1/21/14
1043
CHM 1
BDL
0.050
mg/l
6010C
O1/24/14
0959
ALT 1
0.41
0.15
mg/1
6010C
O1/24/14
0959
ALT 1
BDL
0.050
mg/l
6010C
O1/24/14
1248
JDG 1
BDL
0.050
mg/l
6010C
O1/24/14
0959
ALT 1
BDL
0.050
mg/l
6010C
O1/24/14
0959
ALT 1
BDL
0.050
mg/1
6010C
O1/24/14
0959
ALT 1
BDL
0.050
mg/l
6010C
O1/24/14
0959
ALT 1
-
1311
01/21/14
0701
LJN 1
BDL
0.050
mg/1
8260B
O1/22/14
0127
RB 1
BDL
0.050
mg/l
B260B
O1/22/14
0127
RB 1
BDL
0.050
mg/1
8260B
01/22/14
0127
RB 1
BDL
0.25
mg/l
8260B
01/22/14
0127
RB 1
BDL
0.050
mg/1
8260B
O1/22/14
0127
RB 1
BDL
0.050
mg/l
8260B
01/22/14
0127
RB 1
BDL
0.50
mg/1
8260B
O1/22/14
0127
RB 1
BDL
0.050
mg/1
8260B
O1/22/14
0127
RB 1
BDL
0.050.
mg/l
8260B
O1/22/14
0127
RB 1
BDL
0.050
mg/l
8260B
01/22/14
0127
RB 1
106.
% Rec.
6260B
O1/22/14
0127
RB 1
104.
% Rec.
8260B
O1/22/14
0127
RB 1
103.
% Rec.
8260B
O1/22/14
0127
RB 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Notes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC.
L678659-02 (PAINT) - Contains No Free Liquid
L678659-02 (PH) - [e-mail]
L678659-02 (IGNITABILITY) - Did Not Ignite @ 170 F
Page 3 of 6

n
Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
Date Received January 17, 2014
Description
Sample ID 214635
Collected By
Collection Date 01/15/14 13:00
Parameter
TCLP Pesticides
Chlordane
Endrin
Heptachlor
Lindane
Methoxychlor
Toxaphene
Surrogate Recovery
Decachlorobiphenyl
Tetrachloro-m-xylene
TCLP Herbicides
2,4,5-TP (Silvex)
2,4-D
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
TCLP Semi-Volatiles
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,67Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
2-Fluorobiphenyl
p-Terphenyl-d14
Phenol-d5
2-Fluorophenol
2,4,6-Tribromophenol
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
January 27,2014
ESC Sample # L678659-02
Site ID
Project #
Result Det. Limit Units Method Date/Time Analyst Dil.
BDL
0.0050
mg/l
8081B
01/23/14
1159
CBB 1
BDL
0.0050
mg/l
80BlB
01/23/14
1159
CBB 1
BDL
0.0050
mg/l
8081B
01/23/14
1159
CBB 1
BDL
0.0050
mg/l
8081B
01/23/14
1159
CBB 1
BDL
0.0050
mg/l
8081B
01/23/14
1159
CBB 1
BDL
0.010
mg/l
8081B
01/23/14
1159
CBB 1
79.8
% Rec.
8081B
01/23/14
1159
CBB 1
80.7
% Rec.
8081B
01/23/14
1159
CBB 1
BDL
0.0020
mg/l
8151A
01/22/14
2215
KIM 1
BDL
0.0020
mg/1
8151A
01/22/14
2215
KLM 1
59.6
% Rec.
B151A
01/22/14
2215
KLM 1
BDL
0.10
mg/1
B270C
01/22/14
0346
KMF 1
BDL
0.10
mg/1
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/1
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/1
B270C
01/22/14
0346
KMF 1
BDL
0.10
mg/1
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/l
8270C
01/22/14
0346
KMF 1
BDL
0.10
mg/1
8270C
01/22/14
0346
KMF 1
51.5
% Rec.
8270C
01/22/14
0346
KMF 1
54.6
% Rec.
8270C
01/22/14
0346
KMF 1
52.7
% Rec.
8270C
01/22/14
0346
KMF 1
14.5
% Rec.
8270C
01/22/14
0346
KMF 1
16.6
% Rec.
8270C
01/22/14
0346
KMF 1
43.7
% Rec.
9270C
01/22/14
0346
KMF 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Notes:
The reported analytical results relate only to the sample submitted
This report shall not be reproduced, except in full, without the written approval from ESC
All samples analyzed in accordance with 40 CFR, Part 136.3
Reported: 01/27/14 10:09 Printed: 01/27/14 10:09
L678659-02 (PAINT) - Contains No Free Liquid
L678659-02 (PH) - 13@21.1c
L678659-02 (IGNITABILITY) - Did Not Ignite @ 170 F
Page 4 of 6

i
x
Mr. Scott Fields
Davis & Brown
P.O. Box 15038
Quinby, SC 29506
Report Summary
Monday January 27, 2014
Report Number: L678659
Samples Received: 01/17/14
Client Project:
Description:
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814269
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By. 4
T. Alan Harvill , ESC Representative
Laboratory Certifcation Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND.- R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
,by ESC Lab Sciences.
Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 6

Sample
Number
L678659-02
Work
Group
WG702490
WG702175
Attachment A
List of Analytes with QC Qualifiers
Sample
Type Analyte
SAMP 2,4-D
SAMP Paint Filter Test
Run
ID Qualifier
R2878767 J5
R2877673 L3T4
Page 5 of 6

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J5 The sample matrix interfered with the ability to make any accurate
determination; spike value is high
L3 (ESC) Sample reanalysis and/or spiking could not be performed due to lack
of additional volume.
T4 (ESC) - Additional method/sample information: QNS - Quantity Not Sufficient
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. 'These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 6 of 6

4 6
Summary of Remarks For Samples Printed
O1/27/14 at 10:09:28
TSR Signing Reports: 364
R5 - Desired TAT
CLIENT PAYS SHIPPING BOTH WAYS - ASK FOR SHIPPING CHARGES FOR KITS LOGIN: ALWAYS COMMENT: ICP
METALS BY 6010C
Sample: L678659-01 Account: DAVBRO Received: 01/17/14 09:30 Due Date: 01/24/14 00:00 RPT Date: 01/27/14 10:09
Sample: L678659-02 Account: DAVBRO Received: 01/17/14 09:30 Due Date: 01/24/14 00:00 RPT Date: 01/27/14 10:09
ICP Metals to be done by 6010C

D) x(_ iLI _,4 0-on F125
DAVIS & BROWN. 124 W. MCIverRoad PH: 843485-e74Ett
Florence, FAX. [phone]/t PAGE # OF
REGULATORY: YES NO
,SC29501
CHAIN O V/� U$T0D//.7E6i0RD
TURNAROUND TIME: _Pi
CLIENT:
_STANDARD RUSH _P2
SAMPLE
ANALYSIS
REQUESTED
USE CODES TO INDICTATE IF SAMPLE WAS.
L[.0 tG1
FILTERED OR PRESERVED: A = HNO,
ADDRESS: m
B - HCL D = H=SO, F = FILTRATION
W
C = NAOH E = NA25202 G = ZINCACETATE
N Z
PROGRAMAREA:. D=DRINIONGWATER '
G = GROUNDWATER S =SOLID SL= SLUDGE
E Z
U
-'
r.
¢¢
m LL
PHONE: O
W
W=WASTEWATER O OTHER
FAX:
.
rL
J
<
o
PLEASE PRINT LEGIBLY
-SHADED AREAS"FOR LAB'USE ONLY .
SAMPLE ID DATE I TIME INEfIAL
NOTES
LA6 ID ."
Oof_
Fileioahe.NuinberoE:Conlainerstfor.'EACI3
- OL
00
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SAMPLER SIGNATURE
FLOWINFO
E; ICE
YES NO PACK
ECEIPF
f
•
FR]EMP.I.I.O C
R by: Dat : Tlme:
ire'
Relinquished 6 Date: Time:
Relinquished by: Dale: Time:
.
Receed by: Date: T
Received b Dale; Time:
�2L�
Received by: Date: Tana:
Comments:
n
ISSUED: NOVEMBER 2012
,�>� bc�. / J-M 7

Data QualffFers
Within the -attached report, some analytical data may be reported as Qualified Data as
indicated by Data Qualifier or flag next to the result. The data qualifier "S"
indicates that the analysis was performed by another South Carolina certified
lab. This table summarizes the South Carolina Lab Certification Lumbers for
those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
94002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultaral Service Laboratory Clemson University
S7
South Carolina Lab CertificationNumbcr:
36001-
S8
Lab samples were subcontracted. See attached documentation.
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 10
South Carolina Lab Certification Number:
84009
Sl l
South Carolina Lab Certification Number: 96026; 96031; 98001; 73006; 98016
Note: S 11A indicates AES Laboratory; S 11 G indicates GCAL Laboratory
S 12
AASHTO R18 Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002
S15�
S 16
South Carolina Lab Certification Number:
84004
S 17
South Carolina Lab Certification Number:
96037001
S IS
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sample was analyzed by N icrosee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 (Wilson Division NC00120)
S27
South Carolina Lab Certification Number:
40569
S28
South Carolina Lab Certification Number: 32571
Revision 05/13 Dataqual (SubLabs) .wpd

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4/16/2014 wAw.clemson.edu/agiabresults/COMRLBRTOLSON, SHERRY1401270838311.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 10082 Clemson University
4:
TOLSON, SHERRY ACCOUNT COMRLBR
PO BOX 219 DATE 01/24/2014
CHERAW SC 29520 [e-mail]
SAMPLE NO. 01151450 MANURE: OTHER STORAGE: UNCOVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS--------------
lbs/ton
Ammonium Nitrogen
0.03
%
0.60
Organic Nitrogen
1.01
%
20.17
Nitrate Nitrogen
---------------------------------------------------------------
1.90
ppm
0.00
INCORPORATED AVAILABLE NITROGEN ESTIMATE
12.59
SURFACE AVAILABLE
---------------------------------------------------------------
NITROGEN ESTIMATE
12.41
Phosphorus as P205
0.58
%
11.55
Potassium as K20
0.09
%
1.72
Calcium
12.71
%
254.29
Magnesium.
0.11
%
2.28
Sulfur
0.17
%
3.33
Zinc
214.13
ppm
0.43
Copper
32.83
ppm
0.07
Manganese
39.97
ppm
0.08
Sodium
154.17
ppm
0.31
Moisture
52.42
%
Calcium Carbonate
Equivalency 30.23
%
604.61
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
,organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the

% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
52.42
47.58
951.6
475800
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.03
300
0.6
0.063052
630.517
1.261034
Organic Nitrogen
1.0085
10085
20.17
2.119588
21195.88
42.39176
Nitrate Nitrogen
0.000190
1.9
0.0038
0.000399
3.993274
0.007987
Incorporated Available Nitrogen Estimate
0.6295
6295
12.59
1.323035
13230.35
26.4607
Surface Available Nitrogen Estimate
0.6205
6205
12.41
1.304119
13041.19
26.08239
Phosphorus as P205
0.5775
5775
11.55
1.213745
12137.45
24.27491
Potassium as K20
0.086
860
1.72
0.180748
1807.482
3.614964
Calcium
12.7145
127145
254.29
26.72236
267223.6
534.4472
Magnesium
0.114
1140
2.28
0.239596
2395.965
4.791929
Sulfur
0.1665
1665
3.33
0.349937
3499.369
6.998739
Zinc
0.021413
214.13
0.42826
0.045004
450.042
0.900084
Copper
0.003283
32.83
0.06566
0.0069
68.99958
0.137999
Manganese
0.003997
39.97
0.07994
0.008401
84.00588
0.168012
Sodium
0.015417
154.17
0.30834
0.032402
324.0227
0.648045
Calcium Carbonate Equivalency
30.2305
302305
604.61
63.53615
635361.5
1270.723
January 2014

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: March 19, 2014
Biosolids
Maximum
Maximum
Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr.
DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
1.00 `
41.00
1.80
449.53
899.07
Cadmium, Total
1.00
39.00
1.70
424.56
849.12
Chromium, Total
36.75
1200.00
134.00
911.58
1823.15
Copper, Total
29.61
1500.00
67.00
565.75
1131.50
Lead, Total
3.94
300.00
13.00
824.02
1648.03
Mercury, Total
0.04
17.00
0.75
4644.23
9288.46
Molybdenum, Total
4.01
18.00
0.80
49.92
99.84
Nickel, Total
59.32
420.00
18.70
78.81
157.63
Selenium, Total
1.00
36.00
4.50
1123.84
2247.67
Zinc, Total
171.84
1525.00
125.00
181.85
363.70
PCB
BDL
1.60
Actual metal content less than amount indicated
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil Application
Application
Content,
Content,
Requirement, Rate,
Rate,
ppm
%
#/Acre " DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
665.40
0.07
Organic Nitrogen
7999.05
0.80
Incorporated Available Nitrogen
5332.70
0.53
120.00 5.63
11.25
Surface Available Nitrogen
5133.08
0.51
120.00 5.84
11.69
Phosphorus as P205
4581.75
0.46
80.00 4.37
8.73
Potassium as K20
B41.25
0.08
50.00 14.86
29.72
Calcium, Total
137994.30
13.80
Calcium as CaO
193192.02
19.32
Calcium as CaCO3 (CCE)
345342.21
34.53
2000.00 1.45
2.90
Magnesium, Total
998.10
0.10
Manganese
28.52
0.00
Sulfur
1302.28
0.13
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids.
WT is Wet
Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P.O. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: [phone]
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:

Davis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TOLSON
Client #: 168
Sample Date: 19-Mar-14
SDG #: SDG-098118
Lab Sample ID: LSID-216845
Sample ID: BIO SOILDS-3-19-14-500
Parameter
Acid Digestion (Solids)
Selenium, Total
Percent Moisture
Aluminum, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Copper, Total
Lead, Total
Molybdenum, Total
Nickel, Total
Zinc, Total
Mercury, Total
PCB
South Carolina Certification Number: 21117
Receipt Date: 20-Mar-14
Report Date: 03-Apr-14
Approved By: 71
Van Ward
Lab Director
Result
Reporting
Limit
Unit
Method Flag
Date
Time
Analyst
YES
EPA 200.2
3/24/2014
10:00
JR
<0.967
0.967
mg/kg
EPA 7010
4/2/2014
11:35
JR
51.7
0.1
wt%
SW846 3540
3/26/2014
11:15
JW
4230
19.3
mg/kg
SW846 6010C
3/25/2014
13:41
JR
<0.967
0.967
mg/kg
SW846 6010C
4/2/2014
11:35
JR
<0.967
0.967
mg/kg
SW846 6010C
3/26/2014
10:57
JR
35.5
0.967
mg/kg
SW846 6010C
3/26/2014
10:57
JR
28.6
0.967
mg/kg
SW846 6010C
3/26/2014
10:57
JR
3.81
0.967
mg/kg
SW846 6010C
3/26/2614
10:57
JR
<3.87
3.87
mg/kg
SW846 6010C
3/25/2014
13:41
JR
57.3
0.967
mg/kg
SW846 6010C
3/26/2014
10:57
JR
166
0.967
mg/kg
SW846 6010C
3/26/2014
10:57
JR
<0.039
0.039
mg/kg
SW846 7470A
3/25/2014
13:45
CG
BRL
mg/kg
SW846 8082A S11A
3/26/2014
12:13
SN
Page 5

Data Qualifiers
Within the attached report, some analytical data may be reported as Qualified Data as
indicated by Data Qualifier or flag next to the result. The data qualifier "S"
indicates that the analysis Was performed by another South Carolina certified
lab. This table summarizes the South Carolina Lab Certification Numbers for
those laboratories.
S
South Carolina Lab Certification Number:
23101
S 1
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
$8
Lab samples were subcontracted. See attached documentation.
S9
South Carolina Lab Certification Number:
94014001; 94014002
S 10
South Carolina Lab Certification Number:
84009
S 11
South Carolina Lab Certification Number: 96026; 96031; 98001; 73006; 98016
Note: S 1 lA indicates AES Laboratory; S 11 G indicates GCAL Laboratory
S 12
AASHTO R18 Certified
S 13 I'
South Carolina Lab Certification. Number:
96012
S 14
South- Carolina Lab Certification Number:
89002
S15
*****
S 16
South Carolina Lab Certification Number:
84004
S 17 .
South Carolina Lab Certification Number:
96037001
S 18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sample was analyzed by Microsee s, Inc Laboratory
S26
North Carolina Lab Certification Number:
21 (Wilson Division NC00120)
S27
South Carolina Lab Certification Number:
40569
S28
South Carolina Lab Certification Number: 32571
Revision 05/13 Dataqual (SubLabs) .wpd

CHAIN OF CUSTODY RECORD
Page of I
Post Office Box 15039 124 West McIver Road
Qulnby, South Carolina 29506 Florence, South Carolina 29501
Telephone (043) OW-U740
C1911Ql
ma7va
Use Codes in t1te boxes to indicate
Code: HNO3 -A W404 a D
Iloiloll!illlmmmlp111111111
A
I
mommillll
million
m;
NINON
NINON
MINION
NINON
I
ONION
111111mill
NINON
111111i�
loons
MININNIN
!win-
0 Program Area: D — Drinking Water / G — Groundwater / S — Solid / W — Waste Water / N — NPDES 1 0 — Other

4/16/2014 wawvclemson.edu/aglabresults/COMRLBRTOLSON, SHERRY1404011507221.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 30485 Clemson University
TOLSON, SHERRY ACCOUNT COMRLBR
PO BOX 219 DATE 04/01/2014
CHERAW SC 29520 [e-mail]
SAMPLE NO. 03191450 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.07
%
1.40
Organic Nitrogen
0.84
%
16.83
Nitrate Nitrogen
---------------------------------------------------------------
1.05
ppm
0.00
INCORPORATED AVAILABLE NITROGEN
ESTIMATE
11.22
SURFACE AVAILABLE NITROGEN ESTIMATE
---------------------------------------------------------------
10.80
Phosphorus as P205
0.48
%
9.64
Potassium as K20
0.09
%
1.77
Calcium
14.52
%
290.34
Magnesium
0.11
%
2.10
Sulfur
0.14
%
2.74
Zinc
163.06
ppm
0.33
Copper
26.83
ppm
0.05
Manganese
31.03
ppm
0.06
Sodium
150.96
ppm
0.30
Moisture
47.40
%
Calcium Carbonate Equivalency
36.33
%
726.60
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the

moisture
solids
lbs. solids/ton
lbs. solids/500 tons
47.4
52.6
1052
526000
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.07
700
1.4
0.13308
1330.798
2.661597
Organic Nitrogen
0.8415
8415
16.83
1.59981
15998.1
31.9962
Nitrate Nitrogen
0.000105
1.05
0.0021
0.000200
1.996198
0.003992
Incorporated Available Nitrogen Estimate
0.561
5610
11.22
1.06654
10665.4
21.3308
Surface Available Nitrogen Estimate
0.54
5400
10.8
1.026616
10266.16
20.53232
Phosphorus as P205
0.482
4820
9.64
0.91635
9163.498
18.327
Potassium as K20
0.0885
885
1.77
0.168251
1682.51
3.365019
Calcium
14.517
145170
290.34
27.59886
275988.6
551.9772
Magnesium
0.105
1050
2.1
0.19962
1996.198
3.992395
Sulfur
0.137
1370
2.74
0.260456
2604.563
5.209125
Zinc
0.016306
163.06
0.32612
0.031
310
0.62
Copper
0.002683
26.83
0.05366
0.005101
51.0076
0.102015
Manganese
0.003103
31.03
0.06206
0.005899
58.9924
0.117985
Sodium
0.015096
150.96
0.30192
0.0287
286.9962
0.573992
Calcium Carbonate Equivalency
36.33
363300
726.E
69.06844
690684.4
1381.369
March 2014-

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: May 21, 2014
Biosolids Maximum Maximum Maximum Maximum
Metal Allowable Allowable Application Application
Content, Metal App. Rate, Rate, Rate,
METALS ppm Content, ppm #/Acre/Yr. DT/Acre/Yr. WT/Acre/Yr.
Arsenic, Total
0.77 '
41.00
1.80
583.23
1166.46
Cadmium, Total
0.77
39.00
1.70
550.83
1101.66
Chromium, Total
17.09
1200.00
134.00
1959.91
3919.81
Copper, Total
20.53
1500.00
67.00
815.99
1631.98
Lead, Total
1.62
300.00
13.00
2004.43
4008.87
Mercury, Total
0.03
17.00
0.75
6904.41
13808.82
Molybdenum, Total
7.72 '
18.00
0.80
25.92
51.84
Nickel, Total
28.04
420.00
18.70
166.75
333.51
Selenium, Total
0.77
36.00
4.50
1458.07
2916.15
Zinc, Total
138.18
1525.00
125.00
226.16
452.31
PCB
BDL
1.60
' Actual metal content less than amount indicated.
Biosolids Biosolids Maximum Maximum
Nutrient Nutrient Crop/Soil Application Application
Content, Content, Requirement, Rate, Rate,
ppm % #/Acre " DT/Acre/Yr. WT/Acre/Yr.
Ammonium Nitrogen
482.16
0.05
Organic Nitrogen
5886.37
0.59
Incorporated Available Nitrogen
4259.08
0.43
120.00
7.04
14.09
Surface Available Nitrogen
4114.43
0.41
120.00
7.29
14.58
Phosphorus as P205
5380.10
0.54
80.00
3.72
7.43
Potassium as K20
1024.59
0.10
50.00
12.20
24.40
Calcium, Total
147356.16
14.74
Calcium as CaO
206298.62
20.63
Calcium as CaCO3 (CCE)
333964.16
33.40
2000.00
1.50
2.99
Magnesium, Total
2250.08
0.23
Manganese
40.18
0.00
Sulfur
1100.93
0.11
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. 0. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: B43-537-8442
PRODUCT USER NAME:
ADDRESS:
RECEIVED BY:

Davis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certifleat' of Analysis
Client:
CHERAW, TOWN OF
South Carolina Certification Number: 21117
P.O.SOX 219
CHERAW, SC 29520
Contact:
SHERRY TOLSON
Receipt Date:
22-May-14
Client #:
168
Report Date:
10-Jun-14
Sample Date:
21-May-14
Approved By:
SDG 9:
SDG-099248
Van
Ward
Lab Director
Reporting
Parameter
Result
Limit
Emit
Method Flag
Date
Time Analyst
Silver, Total
<0.005
0.005
mg/L
EPA 200.7 / 200.8
5/26R014
15:37
JR
LSID-219345
1094-C
Acid Digestion (Liquids) YES
EPA 200-2
5/262014
1:00
1R
Cadmium, Total
<0.005
0.005
mg/L
EPA 200.7
526f2014
16:44
JR
Chromium, Total
0.041
0.005
mgfL
EPA 200.7
5260-014
16:44
JR
Copper, Total
0.034
0.005
mg/L
EPA 200.7
51260-014
16:44
JR
Lead, Total
<0.005
0.005
mg/L
EPA 2017
5262014
16:44
JR
Nickel, Total
0.127
0.005
mg/L
EPA 200.7
526/2014
16:44
JR
Zinc, Total
0.046
0.005
mgJL
EPA 200.7
5/262014
16:44
JR
Silver, Total
<0.005
0.005
mg/L
EPA 200.7 / 200.8
5262014
15:08
JR
LSID-219346
BIO SOLIDS 5-21-14-500
Acid Digestion (Solids) YES
EPA 200.2
5232014
10:00
JR
Selenium, Total
<0.966
0.966
mglkg
EPA 7010
6/32014
9:30
JR
Percent Moisture
37.4
0.1
wt%
SW846 3540
5/23/2014
15:50
JW
Aluminum, Total
4610
9.7
mglkg
SW846 6010C
529/2014
10:20
JR
Arsenic, Total
<0.966
0.966
mglkg
SW8466010C
6/3/2014
9:30
JR
Cadmium, Total
<0.966
0.966
mglkg
SW846 6010C
6/32014
9:54
JR
Chromium, Total
21.4
0.966
mglkg
SW846 6010C
6/32014
9:54
JR
Copper, Total
25.7
0.966
mg/kg
SW8466010C
6/32014
9:54
JR
Page 2

•
Client:
Contact:
Client #:
Sample date:
SiDG 9:
CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
SHERRY TOLSON
168
21-May-14
SDG-099248
South Carolina Certification Number: 21117
Receipt Date: 22-May-14
Report Date: 10-Jun-14
?/ •y /�
Approved By: C/ �_ 21 4i
Van Ward
Lab Director
Reporting
Parameter
Result
Lindt
Unit
Method Flag Date
Time Analyst
Lead, Total
2.03
0.966
mgh:g
SW846 6010C.
6/3/2014
9:54
JR
Molybdenum, Total
<9.66
9.66
mg/kg
SW846 6010C
5/29/2014
10:20
JR
Nickel, Total
35.1
0.999
mgft
SW846 6010C
6/3/2014
9:54
JR
Zinc, Total
173
0.966
mg/kg
SW846 601CC
6/3/2014
9:54
JR
Mercury, Total
<0.034
0.034
mg/kg
SW846 7470A
5/26/2014
13:30
CG
PCB
BRL
mg/kg
SW846 8082A S11A
5/312014
1:59
KD
Page 3

G. r
I
Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 219346
Lab 11D: 1405M49-001
Date: 3-Jun-14
Client Sample la: 219346
Collection !Date: 5/21/2014 1:00:00 PM
Matrix: Soil
-Analyses
&Zesalt
Fiepartiag
Units
Dilution
?�atchFlD
®ate Analyzed Analyst
Limit
Factor
Factor
POLYCHL.ORIN'ATF-E) HIPHENYiS
SW8082A
(Snc 35§0C)
Aroclor 1016
BRL
50
ugh s-dry
191765 1
05/312014 01:59
KB
Aroclor 1221
BRL
50
uWKg-dry
191765 1
05/31/2014 01:59
KD
Aroclor 1232
BRL
50
ug/Kg-dry
191765 I
05/312014 01:59
KD
ArociDr 1242
BRL
50
nglKg-dry
191765 I
05/31/2014 01:59
KD
Aroclor 1248
BRL
50
ug/KS-dry
191765 1
05/312014 01:59
KD
Aroclor 1254
BRL
50
uglKg-dry
191765 1
051312014 01:59
KD
Aroclor 1260
BRL
50
u;(Ks-dry
191765 1
05/312014 01:59
KD
Surr: Dccachlorobiphenyl
78.4
35.2-148
'REC
191765 1
05/312014 01:59
KD
Suer. Tetrachloro-tn-xylene
57.7
26.2-120
%REC
191765 l
0513112014,01:59
KD
PERCENT MOISTURE €D2216
Percent Moist= `
32.9
0
wt%
R269760 l
05292014 17:00
EH
QueaBen: Value exceeds maximum contsmimmi level
BRL Below reporting lnxut
H Haldma times for Weparsaan or aalyas ezt:eeded
la Analyze on: NELAC certified
B Analym dato=d in the -aimed method blank
Greece d m Result slue
E Estimatad (value above qumatatirm range)
S Spike Recovery outside limits due to s ma rut
Nar Seecsseourmve
NC Not confirmed
< L. than Result value
J Fstimaed vales dsto_ted below Repotitins Limmt
Page 3 of 6

AccEsS
ANALYICAL, INC.
Sk
ANALYTICAL REPORT
CLIENT
Davis & Brown
P.Q. Box 15038
Quinby SC 29506
ATTENTION
Scott Fields
PROJECTID
219346
LABORATORY REPORT NUMBER
1405M49
DATE .
June 03, 2014
Primary Data Review By
COK"Aao
Chantelle Kanhai
Project Manager, AES
PLEASE NOTE:
Secondary Data review By
Ashley Amick
Project Manager, Access Analytical'
[e-mail]
Unless othenvise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3M Presidential give, Atlanta, GA 30340.
- AES.is SCIDHEC certified Iaboratory # 48016, NCIDENR certified lob # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SCNC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.791.4243 or toll fee at 893.315.4243
Page 1 of 6

-i
-u
4n-Joe-c- I X& S
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SC 20501 FAK. 84W3-060-2208 PAGE# OF
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REGMTORY. YES
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•
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CmMli E.r"Ai%% (;CWOAMATE
ADDRESS:
—PRWRAMAREA: OnDRINKINOWATER
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WnWASTEWATER OtOWER
can
ILL
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a
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SAMPLE ID --V--ATE
TIME
INITIAL
NOTES
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NEW
mm
ft-69
am
a
w
vem
00it
3M
am
wa
gt
gq
-w
gm
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Repdved py Date: Theo; RMtnd Date. fRR I m hW d b Y: Timoi
issum. NOVEMBER 2012

J
Analytic iciM Zuvirotzinvent al Services, Inc.
Sample/Cooler Receipt Checklist
Client i Work OrderNumber &D vxat e,
Checklist comoleted b;.
Signature
Daft
Carrier Courier 'Client US I&U Other
Shipping c
Custody §4
CUS64 S!
Container/
Cooler 91
Chain of c
Chain of
Chain of c
SP__nPles ii
! V=Ple cc
suffident
in good condition?, Yes No Not Prescat
ipping containerlcooler? Yes Na Not Present
mple bottles? Yes No Not Present
np=ature in compliance? (4*C--2)* Yes NO
Cooler 93
si,&=4:�ben relinquished and received?
sample labels?
for indicated test?
Coolerf.4 Coolm*5 Cooler
Yes
Yes No
Yes No
Yes No
Yes - No
Yes / NO.
All sample's received vifthmi bowing time? Yes No
Was TAT on tiie COC? Yes No
Proceed vAth Standard TAT as par project history? Yes NO Not Applicable —
Water -VbAjj&shRV'ezeroh=lsp=d? No VOA vials st Vrnined Yes NO
Water PA ao:ieptable upon receipt? Yes Na Not Applicable
Adjusted? Checked by
Sample CoIndition: (;6od �OthMExplain)
for dM*L-ve -samples or AMA lead) Is a known blank included? Yes No
See Case ariadve fmr Tesobation of the Non -Conformance.
S=O- do naLn to comply with the given range for ommin p=memm
VQ=Tity "u=NChocklists P--du= Sign-OffTcmplftS\Cheddis&Samplr- Receipt Chzckl2=LSAmple_Cooler _Receipt Checklist
Cbeck
Page 4 of-6

Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 219346
Worlrorder: 1405M48
Date: 3-Jun-14
ANALYTICAL QC SUMMARY REPORT
BatchlD: 191765
Sample ID: MD-191765
Client ID:
Units: ug/ICg
Prep Date: 05/30/2014
Run No: 268894
SampleType: MBLIC
TestCode: POLVCIILORINATED BIPHENVLS SWUM
BatchlD: 191765
Analysis Date: 05/30/2014
Seq No: 5672476
Analyte
Result RPT Limit SPK vnlue SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
BRL
33
Aroclor 1221
BRL
33
Aroclor 1232
BRL
33
Aroclor 1242
BRL
33
Aroclor 1249
BRL
33
Aroclor 1254
BRL
33
Aroclor 1260
BRL
33
Sun: Decachlorobiphenyl
11.67
0 16.67 70.0 70 130
Surr: Tetrachloro-m-xylene
11.97
0 16.67 71.8 70 130
Sample ID: LCS-191765
Client ID:
Units: ug/Kg
Prep Date: 0.5/30/2014
Run No: 268894
SamplCType: LCS
TestCode: POLVCHLORINATED WIIENYLS Sw8092A
MOM: 191765
Analysis Date: 05/30/2014
Seq No: 5672478
Analyze
Result RPT Limit SPK value SPK Rcf Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua]
Aroclor 1016
129.1
33
166.7
77.5
70
130
Aroclor 1260
118.4
33
166.7
71.1
70
130 .
Surr: Decachlorobiphenyl
12.02
0
16.67
72.1
70
130
Surr: Tetrachloro-m-xylene
11.89
0
16.67
71.3
70
130
Sample ID: 1405M93-027CMS
Client ID:
Units: ug/ICg-dry Prep Date: 05/3012014
Run No: 268894
SampleType: MS
TestCode: POLYCHLORINATED BIPHENVLS MOM
BatchlD: 191765 Analysis Dole: 05/30/2014
Seq No: 5672480
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qua[
I
Aroclor 1016
138.2
34
171.5
80.6
41.8
140
Aroclor 1260
126.8
34
171.5
74.0
39.4
140
Surr: Deeneblorobiphenyl
13.74
0
17.15
90.1
35.2
148
Sun: Tetrachloro-m-xylene
12.34
0
17.15
71.9
26.2
120
Quounen: > Grutw dun Result wlue < Ltrs thin Retult vil ua - B Ana)yte detttled m the moeiafed method blank
BRL Below repotting limit a Rmmatcd (value above qurntitation range) H Ifolding tunes fat pteparation at onrlyrir exceeded
1 Cltimildd value detected below Reporting Limit N Analyid not NBLAC certified R RPD outride limits due to matrix
Rpt Lim Reporting Limit s Spike Recovery outride limits dud to matrix
Page 5 of

Analytical Environmental Services, Inc Date: 3-Jun-14
Client: Davis & Brown ANALYTICAL QC SUMMARY REPORT
Project Name: 219346
Workorder: 1405M48 BatchlD: 191765
Sample lD: 1405M93-027CNISD
Client lD:
Units: ug/Kg-dry Prep Date: 0.5/3012014
Run No: 268894
SampleType: MSD
TestCode: POLYCHLORINATED BIPIIENYLS SW0002A
BatchlD: 191765 Analysis Dale: OSf31/2014
Seq No: 5672481
Analyle
Result RPT Limit SPK value SPK Ref Val
%RFC Low Limit High Limit RPD Ref Val %RPD
I
RPD Limit Qual
Aroclor 1016
138.9
34
171.5
81.0
-41.8
140
138.2
0.521
32.4
Aroclor 1260
132.5
34
171.5
77.3
39.4
140
126.8
4.38
32.7
Sury Decachlorobiphenyl
13.98
0
17.15
91.5
35.2
148
13.74
0
0
Surr: Tetrachloro-m-xylene
11.17
0
17.15
65.1
26.2
120
12.34
0
-0
()nallatn: > GrestesdimReNltvalue
BILL Below "ring limit
' 1 estimzted value dejected below Reporting Limit
Rpl1Am Reporting Limit
Page 6 of 6
< Less thin Result value
E Estimsted(valuesbovequaatitsmenInge)
N Analylenot NELACcertified
S Spike Recovery outside limits due to tnatrix
B Analyze detocted In the asoociittd method blank
n Llolding times fat ptepatatmn ar wlysos exceeded
R Rt'D outside limits due to nutrix

Data Qualifiers
Within the attached report, some analytical data may be reported as Qualified Data as
indicated by Data Qualifier or'flag next to the result. The data qualifier "S"
indicates that the analysis was performed by another South Carolina certified
lab. This table summarizes the South Carolina Lab Certification Numbers for'
those laboratories.
S
South Carolina Lab Certification Number:
23101
S I
South Carolina Lab Certification Number:
93013
S2
South Carolina Lab Certification Number:
23105
S3
South Carolina Lab Certification Number:
10120
S4
South Carolina Lab Certification Number:
84002
S5
South Carolina Lab Certification Number:
32117
S6
Agricultural Service Laboratory Clemson University
S7
South Carolina Lab Certification Number:
36001
S8
Lab samples were subcontracted. See attached documentation.
S9
South Carolina Lab Certification Number:
94014001; 94014002
S I O
South Carolina Lab Certification Number:
84009
S11
South Carolina Lab Certification Number: 96026; 96031; 98001; 73006; 99016
Note: S I I A. indicates AES Laboratory; S 11 G indicates GCAL Laboratory
S 12
AASHTO RI Certified
S 13
South Carolina Lab Certification Number:
96012
S 14
South Carolina Lab Certification Number:
89002
S15>fi>a*>x
S 16
South Carolina Lab Certification Number:
94004
S 17
South Carolina Lab Certification Number:
96037001
S18
South Carolina Lab Certification Number:
95005
S 19
South Carolina Lab Certification Number:
23104
S20
South Carolina Lab Certification Number:
96027001
S21
South Carolina Lab Certification Number:
21005
S22
South Carolina Lab Certification Number:
24110
S23
South Carolina Lab Certification Number:
84001001
S24
South Carolina Lab Certification Number: 82014001
S25
Sample was analyzed by Microsee s, Inc Laborato
S26
North Carolina Lab Certification Number:
21 Wilson Division NC00120
-527
South Carolina Lab Certification Number: 40569
S28
South Carolina Lab Certification Number: 32571
Revision 05113 Dtuaqual (Subinbs).%Td

CHAIN OF CUSTODY RECORD
Page—L— Gf—I—
DAVIS & BROWN
Pont off tco Box 15038 124 West McIver Road
Ownby, South Carolina 29506 Florence, SotAh Carolina 29501
Telephone [phone]
Clean: Nam: I I:acdtty Nune
SAMPLE
ANALYSIS
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I
7/23/2014 wain.clemson.edu/aglabresults/COMRLBRTOLSON, SHERRY1405281612582.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 50818 Clemson University
TOLSON, SHERRY ACCOUNT COMRLBR
PO BOX 219 DATE 05/28/2014
CHERAW SC 29520 [e-mail]
SAMPLE NO. 05211450 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS--------------------
lbs/ton
Ammonium Nitrogen
0.06
%
1.20
Organic Nitrogen
0.73
%
14.65
Nitrate Nitrogen
---------------------------------------------------------------
266.31
ppm
0.53
INCORPORATED AVAILABLE
NITROGEN ESTIMATE
10.60
SURFACE AVAILABLE NITROGEN ESTIMATE
---------------------------------------------------------------
10.24
Phosphorus as P205
0.67
%
13.39
Potassium as K20
0.13
%
2.55
Calcium
18.34
%
366.74
Magnesium
0.28
%
5.60
Sulfur
0.14
%
2.74
Zinc
262.58
ppm
0.53
Copper
51.65
ppm
0.10
Manganese
51.65
ppm
0.10
Sodium
200.36
ppm
0.40
Moisture 37.78 %
Calcium Carbonate Equivalency 41.56 % 831.17
------------------------------------------------------------------------------
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
http://WAw.cl emson.edu/ag labresults/COM RLBRTOLSON,%20SH ERRY1405281612582.htm

% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
37.78
62.22
1244.4
622200
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.06
600
1.2
0.096432
964.3202
1.92864
Organic Nitrogen
0.7325
7325
14.65
1.177274
11772.74
23.54548
Nitrate Nitrogen
0.026631
266.31
0.53262
0.042801
428.0135
0.856027
Incorporated Available Nitrogen Estimate
0.53
5300
10.6
0.851816
8518.161
17.03632
Surface Available Nitrogen Estimate
0.512
5120
10.24
0.822887
8228.865
16.45773
Phosphorus as P2O5
0.6695
6695
13.39
1.076021
10760.21
21.52041
Potassium as K2O
0.1275
1275
2.55
0.204918
2049.18
4.098361
Calcium
18.337
183370
366.74
29.47123
294712.3
589.4246
Magnesium
0.28
2800
5.6
0.450016
4500.161
9.000321
Sulfur
0.137
1370
2.74
0.220186
2201.864
4.403729
Zinc
0.026258
262.58
0.52516
0.042202
422.0186
0.844037
Copper
0.005165
51.65
0.1033
0.008301
83.01189
0.166024
Manganese
0.005165
51.65
0.1033
0.008301
83.01189
0.166024
Sodium
0.020036
200.36
0.40072
0.032202
322.0186
0.644037
Calcium Carbonate Equivalency
41.5585
415585
831.17
66.79283
667928.3
1335.857
May 2014

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: July 16, 2014
METALS
Biosolids
Metal
Content,
ppm
Maximum
Allowable
Metal
Content, ppm
Maximum Maximum
Allowable Application
App. Rate, Rate,
#/Acre/Yr. DT/Acre/Yr.
Maximum
Application
Rate,
WT/Acre/Yr.
Arsenic, Total
0.77
41.00
1.80
581.43
1162.86
Cadmium, Total
0.60
39.00
1.70
704.58
1409.16
Chromium, Total
20.15
1200.00
134.00
1662.74
3325.49
Copper, Total
23.03
1500.00
67.00
727.17
1454.35
Lead, Total
1.47
300.00
13.00
2213.81
4427.62
Mercury, Total
0.03
17.00
0.75
7445.12
14890.24
Molybdenum, Total
48.22
18.00
0.80
4.15
8.30
Nickel, Total
36.24
420.00
18.70
129.00
258.00
Selenium, Total
0.60
36.00
4.50
1865.07
3730.14
Zinc, Total
117.32
1525.00
125.00
266.36
532.72
PCB
BDL
1.60
' Actual metal content less than amount indicated.
Biosolids Biosolids Maximum Maximum
Nutrient Nutrient Crop/Soil Application Application
Content, Content, Requirement, Rate, Rate,
ppm % #/Acre " DT/Acre/Yr. WT/Acre/Yr.
Ammonium Nitrogen
155.55
0.02
Organic Nitrogen
6046.82
0.60
Incorporated Available Nitrogen
3756.42
0.38
120.00
7.99
15.97
Surface Available Nitrogen
3709.75
0.37
120.00
8.09
16.17
Phosphorus as P205
4580.81
0.46
80.00
4.37
8.73
Potassium as K20
843.83
0.08
50.00
14.81
29.63
Calcium, Total
174300.05
17.43
Calcium as CaO
244020.07
24.40
Calcium as CaCO3 (CCE)
346997.98
34.70
2000.00
1.44
2.88
Magnesium, Total
1298.80
0.13
Manganese
35.00
0.00
Sulfur
1298.B0
0.13
Percent Moisture
50.00
These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (B43-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. O. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: [phone]
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:

bavis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF
South Carolina Certification Number: 21117
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TURNER
Receipt hate: 17-Jul-14
Client #: 168
Report Date: 11-Aug14
Sample Date: 17-Jul-14
SDG#: SDG-100268
Approved By:
Van Ward
`
Lab Director
Reporting
Parameter
Result Limit
Unit
Method Flag
Date
Time
Analyst
LSID-221619 LFF. PQL 7-16-14-001
Acid Digestion (Liquids)
YES
EPA 200.2
7/21/2014
1:00
JR
Copper, Total
0.007 0.005
mg/L
EPA 200.7
7/21/2014
12:06
JR
Lead, Total
<0.001 0.001
mg/L
SM 3113B-2010
7/25/2014
10:00
CG
LSID-221620 1001-B
Oil & Grease, Hexane
12.9 5
mg/L
EPA 1664A
7/28/2014
8:00
CG
LSED-221621 1002-B
Oil & Grease, Hexane
12.6 5
mg/L
EPA 1664A
7/28/2014
8:00
CG
LSID-221622 1001-X
Cyanide
<0.010 0.01
mg/L
SM 4500 CN-C & S11A
7/25/2014
16:00
LW
LSID-221623 1002-X
Cyanide
<0.010 0.01
mg/L
SM4500 CN-C & S11A
7/25/2014
16:00
LW
LSID-221624 1001-C
Acid Digestion (Liquids)
YES
EPA 200.2
7/21/2014
1:00
JR
Cadmium, Total
<0.005 0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Page 1

0
Davis & Brown
P® Bog 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF South Carolina Certification Number: 21117
P.O.BOX 219
CHERAW, SC 29520
Contact:
SHERRY TURNER
Receipt Date:
17-Jul-14
Client #:
168
Report Date:
11-Au, 14
Sample Date:
16-Jul-14
SDG #:
Approved By:
,1
SDG-100268
Van Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method Flag Plate
Time
Analyst
Chromium, Total
0.142
0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Copper, Total
0.033
0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Lead, Total
<0.005
0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Nickel, Total
0.242
0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Zinc, Total
0.079
0.005
mg/L
EPA 200.7
7/21/2014
12:09
JR
Silver, Total
<0.005
0.005
mg/L
EPA 200.7 / 200.8
7/24/2014
11:59
JR
LSFD-221625
1002-C
Acid Digestion (Liquids)
YES
EPA 200.2
7/21/2014
1:00
JR
Cadmium, Total
<0.005
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Chromium, Total
0.007
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Copper, Total
0.011
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Lead, Total
<0.005
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Nickel, Total
0.062
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Zinc, Total
0.286
0.005
mg/L
EPA 200.7
7/21/2014
12:13
JR
Silver, Total
<0.005
0.005
mg/L
EPA 200.7 / 200.8
7/24/2014
12:02
JR
LSID-221626 7-16-14-500
Acid Digestion (Solids) YES EPA 200.2 7/21/2014 10:00 JR
Percent Moisture 18.6 0.1 wt% SW846 3540 7/18/2014 14:49 JW
Aluminum, Total 6560 78.5 mg/kg SW846 6010C 7/30/2014 13:08 JR
Page 2

R
Client:
CHERAW, TOWN OF
South Carolina Certification Number: 21117
P.O.BOX 219
CHERAW, SC 29520
Contact:
SHERRY TURNER
Receipt Date:
17-Jul-14
Client #:
168
Report Date:
11-Aub 14
Sample Date:
16-Jul-14
SDI #:
Approved By:
€,
SDG-100268
Van
Ward
Lab Director
Reporting
Parameter
Result
Limit
Unit
Method Flag Date
Time Analyst
Arsenic, Total
1.26
0.05
mg/kg
SW846 6010C
7/28/2014
14:31
JR
Cadmium, Total
<0.982
0.982
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Chromium Total
32.8
0.982
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Copper, Total
37.5
0.982
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Lead, Total
2.39
0.005
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Molybdenum, Total <78.5
78.5
mg/kg
SW846 6010C
7/30/2014
13:08
JR
Nickel, Total
59.0
0.982
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Zinc, Total
191
0.982
mg/kg
SW846 6010C
7/24/2014
13:49
JR
Mercury, Total
0.041
0.04
mg/kg
SW846 7470A
7/24/2014
14:00
CG
PCB
BRL
mg/kg
SW8468082A35 S11A
7/21/2014
20:28
RS
Selenium, Total
<0.982
0.982
mg/kg
SW846-6010C
7/28/2014
14:31
JR
Page 3

.i t
DAVIS OWN
CHAT( � � OF CUSTODY
T RECORD
CORD Post Office Box 15036 1'?+ W051 McIver Road
(, Umby, South (.4-wolirla P�1506 FlorerlCo, South Carolina 29501
Paf: —L of, Taltlp110110 [phone]
-l:IlemNat Ile It',nellit} tdn­II e
Collected In
lI)
.IUOI-'C
Its v��C
f{cl
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by (SI(:ri+l MIRE)•
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.
Date Time
I)n[c Time
WHO Comments �__ _ _.Iteguhtpq
I'rolpani Area: G J) lul;ing Water / G -- Groundwaler / S -- Solid / W-1Yunte Water / N ._ NUDES / Q -- 01her,

r..
ANALYTICAL REPORT
CLIENT
Davis & Brown
P.O. Box 15038
Quinby SC 29506
ATTENTION
Scott Fields
PROJECT ID
221626
LABORATORY REPORT NUMBER
1407G58
DATE
July 23, 2014
Primary Data Review By Secondary Data Review By
Chantelle Kanhai
Project Manager, AES
PLEASE NOTE:
Ashley Amick
Project Manager, Access Analytical
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # EL-E87582,
NELAP certified laboratory # E87582
- Local supportservices for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Pace 1 of 6

K-e:> P.O. * �k-A -� - t tq�
tq(D-If:�573 —
124 W. McIver Road PH. 843-6656746 PAGE# � OF
DAvis & BROWN Florence, SC 294501 FAX. [phone]el-I
CHA IN OF CUSTODY RECORD
TURNAROUND 77M,-.1 _P1
REGULATORY- YES NO
ATANDARD RUSH P2
CLIENT:
SAMPLE
ANALYSIS
REQUESTED
USE CODES TO INDICTAM IF SAMPLE WAS
FILTERED OR PRESERVED: A = HN0,j
13-11CL -D=HzSO, F FILTFATION
C=NAOH E=NAAO, G=ZINCACETATE
p m.
ADDRESS:
to
PROGRAM4 D = DRINKING WATER
z
G4GROUNDWATER $=SOLID SL=,SLUU(§r=
Q
8
W=WASTEWATER MOTHER
-IT—
,:.a
WE
U-
0
PL--AgEPRINT LE_GIBLY
PHONE-. FAX:
SHADED, -AA-ASFQR'LAB USE ONLY
SAMPLE ID
DATE
TIME
IN
INITIAL
NOTES
LAB ID
MeMftbe.
ist" -
...........
1-14
F-T'
2Q.. rM
M"'...
. . . . . . . . . . . . . .
1V
Ej�'TRR
we
k�==:Ua'EEE
ma
m
SA—iAOJLER SIGNATURE
FLOW
ICE'
YES' NO ;PACK
R6CFJP`r
Tzwp-.t
Relinquish by D te. Thne.
Relinquished by Date: Time!
Relinquished by: bite. Time:
ak
(0
Date-, Mine-
Received - I
Received by Date: Time.,
Received by. Date; Time:
comments:
ISSUED., NOVEMSM2012

Analytical Environmental Services, Inc
Bate: 24-Jul-14
Client:
Davis & Brown
Client Sample YID:
221626
Project Name:
221626
Collection Date:
7/16/2014 1:00:00 PM
Lab ID:
1407G58-001
Matrix:
Soil
Analyses
Result
Reporting
Limit
Qual Units
BatchlD
Dilution
Factor
Date Analyzed Analyst
POLYCBLORINATElD BTLPHENYLS
SW8082A
(Srar►'3550C)
Aroclor 1016
BRL
40
ugTg-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1221
BRL
40
ug/Kg-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1232
BRL
40
ug/Kg-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1242
BRL
40
ug/Kg-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1248
BRL
40
ug/Kg-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1254
BRL
40
u9'K9-dry
193842
1
07/21/2014 20:28
RS
Aroclor 1260
BRL
40
ug/KKg-dry
193842
1
07/21/2014 20:28
RS
Surr: Decachlorobiphenyl
61.3
35.2-148
' REC
193842
1
07/21/2014 20:28
RS
Surr: Tetrachloro-m-xylene
64.5
26.2-120
%REC
193842
1
07/21/2014 20:28
RS
PERCENT MOISTURE bD2216
Percent Moisture
17.8
0
wto/o
R272117
1
07/21/201413:00
SG
Qualitiets: c Value exceeds maximum contaminant level E Estimated (value above quantitation range)
BRL Below reporting limit S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded Narr See case narrative
N Analyte not NELAC certified NC Not confirmed
B Analyte detected in the associated method blank < Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Paae 3 of 6

Analytical Environmental Services, Inc.
Sample/Cooler Receipt Checklist
Client _ _ Aam
Work Order Number
I
pry
Checklist completed by ! t t,f too!`3 [ t b l lt(
Signature U Date
Carrier name: FedEx -U-PS _ Courier— Client— US IVlail _ Other
Shipping container/cooler in good condition? Yes No
Custody seals intact on shipping container/cooler? Yes _ No _
Custody seals intact on sample bottles? Yes _ No _
Container/Temp Blank temperature in compliance? (40C=2)* Yes No _
/,
Not Present _
Not Present V'
Not Present
Cooler #I Cooler#2 Cooler##3 Cooler-94 Coolerff5 Cooler#G
Chain of custody present?
Yes
No _
Chain of custody signed when relinquished and received?
Yes
No
Chain of custody agrees with sample labels?
Yes
No _
Samples in proper container/bottle?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test?
Yes
`�
No
All samples received tivithin holding tine?
Yes
No _
Was TAT marked on the COC?
Yes
No LZ
Proceed with Standard TAT as per project history?
Yes
No _
Water - VOA vials have zero headspace? No VOA vials submitted Yes _
Water- pH acceptable upon receipt?
Yes
_
No —
/ Adjusted? Checked by
Sample Condition: Good V Other(Explain)
(For diffusive samples or AIPIA lead) Is a known blank included? Yes _
See Case Narrative for resolution of the Non -Conformance.
Not Applicable
No _
Not Applicable t/
No �
* Samples do not have to comply with the given range for certain parameters.
li 1Quality AssuraneelChecklists Procedures Sign-0 ffTemplateACheckifstslSample Receipt ChecklistslSainple_Cooler_Receipt Checklist
Page 4 of 6

Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 221626
Workorder: 1407G58
Date: 23-Jul-14
ANALYTICAL QC SUMMARY REPORT
BatchID: 193842
Sample ID: MB-193842
Client ID:
Units: ug/Kg
Prep Date: 07/21/2014
Run No: 272161
SampleType: MBLK
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 193842
Analysis Date: 07/21/2014
Seq No: 5743604
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
BRL
33
Aroclor 1221
BRL
33
Aroclor 1232
BRL
33
Aroclor 1242
BRL
33
Aroclor 1248
BRL
33
Aroclor 1254
BRL
33
Aroclor 1260
BRL
33
Surr: Decachlorobiphenyl
16.62
0 16.67 99.7 70 130
Surr: Tetrachloro-m-xylene
14.46
0 16.67 86.7 70 130
Sample ID: LCS-193842
Client ID:
Units: rtg/Kg
Prep Date: 07/21/2014
Run No: 272161
SampleType: LCS
TestCode: POLYCHLORINATED BIPHENYLS Sw3082A
BatchID: 193842
Analysis Date: 07/21/2014
Seq No: 5743607
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
164.5
33
166.7
98.7
70
130
Aroclor 1260
164.6
33
166.7
98.8
70
130
Surr: Decachlorobiphenyl
17.49
0
16.67
105
70
130
Surr: Tetrachloro-m-xylene
14.06
0
16.67
84.3
70
130
Sample ID: 1407E32-005BMS
I Client ID:
Units: ug/Kg-dry Prep Date: 07/21/2014
Run No: 272161
SampleType: MS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 193342 Analysis Date: 07/22/2014
Seq No: 5743612
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
178.4
38
189.8
94.0
41.8
140
Aroclor 1260
169.6
38
189.8
89.4
39.4
140
Surr: Decachlorobiphenyl
18.59
0
18.98
97.9
35.2
148
Surr: Tetrachloro-in-xylene
14.25
0
18.98
75.1
26.2
120
Qualifiers: , > . Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
Page 5 of 6
< Less than Result value
E Estimated (value above quantitaticn range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix

Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 221626
Workor•der: 1407G58
Date: 23-Jul-14
ANALYTICAL QC SUMMARY REPORT
BatclilD: 193842
Sample ID: 140702-005BMSD
Client ID:
Units: ug/Kg-dry Prep Date: 07/21/2014
Run No: 272161
SampleType: MSD
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchlD: 193842 Analysis Date: 07/22/2014
Seq No: 5743615
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
170.3
38
189.8
89.7
41.8
140
178.4
4.64
32.4
Aroclor 1260
179.7
38
189.8
94.7
39.4
140
169.6
5.76
32.7
Sun•: Decachlorobiphenyl
18.90
0
18.98
99.6
35.2
148 _
18.59
0
0
Surr: Tetrachloro-ni-xylene
14.90
0
18.98
78.5
26.2
120
14.25
0
0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
Page 6 of 6
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
E Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
E. RPD outside limits due to matrix

10/2312014 ~.clemson.edu/agiabresults/COMRLBRTURNER, SHERRY1407281603032.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 71034 Clemson University
TURNER, SHERRY
PO BOX 219
CHERAW SC 29520
ACCOUNT COMRLBR
DATE 07/28/2014
[e-mail]
SAMPLE NO. 07161450 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.02
%
0.40
Organic Nitrogen
0.78
%
15.55
Nitrate Nitrogen
---------------------------------------------------------------
2.57
ppm
0.01
INCORPORATED AVAILABLE NITROGEN
ESTIMATE
9.66
SURFACE AVAILABLE NITROGEN ESTIMATE
9.54
---------------------------------------------------------------
Phosphorus as P205
0.59
%
11.78
Potassium as K20
0.11
%
2.17
Calcium
22.41
%
448.23
Magnesium
0.17
%
3.34
Sulfur
0.17
%
3.34
Zinc
208.30
ppm
0.42
Copper
36.00
ppm
0.07
Manganese
44.36
ppm
0.09
Sodium
176.15
ppm
0.35
Moisture
35.71
%
Calcium Carbonate Equivalency
----------------------------------------------------------------------
44.62
%
892.34
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
htip://www.cl emson.edu/ag labresufts/COMRLBRTU RN ER,%20SHERRY1407281603032htm 1/2

% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
35.71
64.29
1285.8
642900
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.02
200
0.4
0.031109
311.0904
0.622181
Organic Nitrogen
0.7775
7775
15.55
1.209364
12093.64
24.18728
Nitrate Nitrogen
0.000257
2.57
0.00514
0.000400
3.997511
0.007995
Incorporated Available Nitrogen Estimate
0.483
4830
9.66
0.751283
7512.832
15.02566
Surface Available Nitrogen Estimate
0.477
4770
9.54
0.741951
7419.505
14.83901
Phosphorus as P2O5
0.589
5890
11.78
0.916161
9161.611
18.32322
Potassium as K2O
0.1085
1085
2.17
0.168767
1687.665
3.375331
Calcium
22.4115
224115
448.23
34.86001
348600.1
697.2002
Magnesium
0.167
1670
3.34
0.25976
2597.605
5.195209
Sulfur
0.167
1670
3.34
0.25976
2597.605
5.195209
Zinc
0.02083
208.3
0.4166
0.0324
324.0006
0.648001
Copper
0.0026
26
0.052
0.004044
40.44175
0.080883
Manganese
0.004436
44.36
0.08872
0.0069
68.99984
0.138
Sodium
0.017615
176.15
0.3523
0.027399
273.9928
0.547986
Calcium Carbonate Equivalency
44.617
446170
892.34
69.3996
693996
1387.992
July 2014

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
BIOSOLIDS SAMPLE DATE: September 17, 2014
METALS
Biosolids
Metal
Content,
ppm
Maximum
Allowable
Metal
Content, ppm
Maximum Maximum
Allowable Application
App. Rate, Rate,
#/Acre/Yr. DT/Acre/Yr.
Maximum
Application
Rate,
WT/Acre/Yr.
Arsenic, Total
1.12
41.00
1.80
401.50
B03.01
Cadmium, Total
1.41
39.00
1.70
301.17
602.35
Chromium, Total
11.38
1200.00
134.00
2943.21
5886.43
Copper, Total
14.92
1500.00
67.00
1122.32
2244.63
Lead, Total
1.87
300.00
13.00
1738.04
3476.09
Mercury, Total
0.02 '
17.00
0.75
8071.88
16143.75
Molybdenum, Total
5.66
18.00
0.80
35.36
70.72
Nickel, Total
15.39
420.00
18.70
303.79
607.57
Selenium, Total
0.57
36,00
4.50
1988.96
3977.93
Zinc, Total
105.11
1525.00
125.00
297.31
594.61
PCB
BDL
1.60
` Actual metal content less than amount indicated
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre "
DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
0.00
0.00
Organic Nitrogen
5575.49
0.56
Incorporated Available Nitrogen
3466.19
0.35
120.00
8.66
17.31
Surface Available Nitrogen
3466.19
0.35
120.00
8.66
17.31
Phosphorus as P2O5
3894.35
0.39
80.00
5.14
10.27
Potassium as K2O
783.91
0.08
50.00
15.95
31.89
Calcium, Total
145507.49
14.55
Calcium as CaO
203710.49
20.37
Calcium as CaCO3 (CCE)
369818.03
36.98
2000.00
1.35
2.70
Magnesium, Total
1051.50
0.11
Manganese
25.19
0.00
Sulfur
1199.47
0.12
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (843-623-2134) and/or the Soil Conservation Service (843-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. O. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: [phone]
PRODUCT USER NAME
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:

Davis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TURNER
Client #: 168
Sample Date: 17-Sep-14
SDG #: SDG-101455
Lab Sample ID: LSID-224031
Sample ID: BIO SOLIDS 9-17-14-500
Parameter
Acid Digestion (Solids)
Selenium, Total
Percent Moisture
Aluminum, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Copper, Total
Lead, Total
Molybdenum, Total
Nickel, Total
Zinc, Total
Mercury, Total
PCB
South Carolina Certification Number: 21117
Receipt Date: 18-Sep-14
Report Date: 23-Oct-14
Approved By: .=t= F
Van Ward
Lab Director
Result
Reporting
Limit
Unit
Method Flag
Date
Time
Analyst
YES
EPA 200.2
9/22/2014
10:00
JR
<0.974
0.974
mg/kg
EPA 7010 / 6010
9/23/2014
11:23
JR
13.9
0.1
wt%
SW846 3540
9/22/2014
16:42
JVJ
3170
39
mg/kg
SW846 6010C,
9/24/2014
13:48
JR
1.93
0.974
mg/kg
SW846 6010C
9/23/2014
11:23
JR
<2.43
2.43
mg/kg
SW846 6010C
9/29/2014
12:05
JR
19.6
2.43
mg/kg
SW846 6010C
9/29/2014
12:05
JR
25.7
2.43
mg/kg
SW846 6010C
9/29/2014
12:05
JR
3.22
2.43
m&-g
SW846 6010C
9/29/2014
12:05
JR
<9.74
9.74
mg/kg
SW846 6010C
10/21/2014
11:18
JR
26.5
2.43
mg/kg
SW846 6010C
9/29/2014
12:05
JR
181
2.43
mg/kg
SW846 6010C
9/29/2014
12:05
JR
<0.040
0.04
mg/kg
SW846 7470A
9/23/2014
13:15
CG
BRL
mg/kg
SW846 8082A S11A
9/25/2014
22:26
BB
Page 1

r
CHAIN OF CUSTODY RECORD
Page of I
Post Office Box 15038 124 West McIver Road
Gluinby, South Carolina 29506 Florence; South Carolina 29501
Telephone (M) 685-6748
1 DICKS
M$1=VM7M
Use Codes in the boxes to indicate —7
whether sample was filtered or preserved.
Komi "—.1
Code: UN03 =A 4004 " D
L Rif
III
moll
011
MINIM
NONE
mom
I
I
I
mom
milli
INmilli0lin�
i111111111
nn�n
�
;,b —y
0 Program Area: D - Drinking Water / 0 - Groundwater / 3 - Solid / W - Waste Water / N - IVMES / O - Other

4 }
tA c(TMFs-
A.NALYTICAL REPORT
CLIENT
Davis & Brown
P.O. Box 15038
Quinby SC 29506
ATTENTION
Scott Fields
PROJECT 11�
224031
LABORATORY REPORT NUMBER
1409122
DATE
September 26, 2014
L Primary Data Review By Secondary Data Review By
Ashley Amick
Chantelle Kanhai Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCD11EC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243

Analytical EnNiro»mental Services, Inc Date: 30-Sep-14
Client: Davis & Brown
Project: 224031
Case N&I'F'atHTYe
Lab IID: 1409122
PCB Analysis by Method 8082:
Percent recoveries for the surrogate spiking compound Tetrachloro-m-xylene on QC samples NM-196762 and LCS-196762 were
outside control limits biased low. All other surrogate recoveries were within control limits.
.Pane 3 of 7

Analytical Environmental Services, )rFnc Date: 26-Sep-14
Client:
Davis & Brown
Client Sample ID:
224031
Project Name:
224031
Collection bate:
9/17/2014 1:00:00 PM
Lab 1D:
1409122-001
Matrix:
Solid
Analyses
Result
Reporting
Limit Qual
Units
l;ateblD
Dilution
Factor
Date Analyzed Analyst
POLYCHLORINATED EIPHENYLS
SW8082A
(SW3550C)
Aroclor 1016
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1221
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1232
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1242
BRL
98
ug(Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1248
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1254
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Aroclor 1260
BRL
98
ug/Kg-dry
196762
1
09/25/2014 22:26
BB
Surr: Decachlorobiphenyl
156
35.2-148 S
' RFC
196762
1
09/25/2014 22:26
BB
Surr: Tetrachloro-m-xylene
112
26.2-120
°/DREC
196762
1
09/25/2014 22:26
BB
PERCENT MOISTURE D2216
Percent Moisture
31.8
0
wt"/u
R276548
1
09/25/201415:00
SG
Qualifiers: ° Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
Paae 4 of 7
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Notcon&cmed
< Less than Result value
7 Estimated value detected below Reporting Limit

t
Analytical Eni i>i onmental Services, Inc.
Sample/Cooler Receipt Checklist
Client Work Order Number
Checklist cortzpleted by. A �
Si . re Date
Carrier name: FedEx -AS —' Courier — Client _ IIS lvlail Other
Shipping container/cooler in good condition? Yes . No _
Custody seals intact on shipping container/cooler? Yes
k-ustoay seats intact on sample bottles`?
Yes
Container/Temp Blank
—
temperature in compliance? (0°<6°C)* Yes.
Cooler #1 Cooler 42 Cooler 43
Cooler #4
Chain of custody present?
Yes
If
Chain of custody signed when relinquished and received?
Yes
Chain of custody agrees with sample labels?
Yes
a
Samples in proper er container/bottle? -
Yes
_
Sample containers intact?
Yes
Sufficient sample volume for indicated test?
Yes
All samples received within holding time?
Yes
f�
No —
No —
No —
No —
No —
No
No _
No —
No _
Not Present _
Not Present V
Not Present
Cooler#5 Cooler•#6
Was TAT marked on the COC? Yes _ No —
Proceed with Standard TAT as per project history? Yes — No — Not Appi icable _
Water - VOA vials have zero headspace? No VOA vials submitted Yes — No —
Water - pH acceptable upon receiptT Yes No Not Applicable
Adjusted? Checked by
Sample Condition: Good Other(Explain)
(For diffusive samples or AIi3A lead) Is a known blank included? Yes — No
See Case Narrative for resolution of the Non-Conformanee.
Samples do not have to compip with the given range for certain parameters.
11Aes serverkManple Receipt\My DocumentslCOCs and pH Adjustment Sheet%Saniple Cooler_Recipt Checklist Revl_rtf
Panes F of 7

Analytical Environmental Services, Inc
Date: 26-Sep-14
Client: Davis & Brown ANALYTICAL QC SUMMARY SPORT
Project Name: 224031
Workorder: 1409I22 BatchID: 196762
Sample ID: MB-196762 Client ID: Units: ug/Kg Prep Date: 09/24/2014 Run No: 276560
SampleType: MBLK TestCode: POLYCHLORINATED BIPHENYLS SW8082A BatchlD: 196762 Analysis Date: 09/25/2014 Seq No: 5841089
Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual
Aroclor 1016 .
BRL
33
Aroclor 1221
BRL
33
Aroclor 1232
BRL
33
Aroclor 1242
BRL
33
Aroclor 1248
BRL
33
Aroclor 1254
BRL
33
Aroclor 1260
BRL
33
Surr: Decachlorobiphenyl
15.09
0 16.67 90.5 70 130
Surr: Tetrachloro-m-xylene
11.18
0 16.67 67.1 70 130 S
Sample ID: LCS-196762 Client ID: Units: ug/l(g Prep Date: 09/24/2014 Run No: 276560
SampleType: LCS TestCode: POLYCHLORINATED BIPHENYLS SW8082A BatchID: 196762 Analysis Date: 09/25/2014 Seq No: 5841091
I
Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual
Aroclor 1016
131.6
33
166.7
78.9
70
130
Aroclor 1260
145.3
33
166.7
87.2
70
130
Sun: Decachlorobiphenyl
14.35
0
16.67
86.1
70
130.
Surr: Tetrachloro-In-xylene
10.86 _
0
16.67
65.2
70
130 S
Sample ID: 1409L50-001AMS
Client ID:
Units: ug/Kg-dry Prep Date: 09/24/2014
Run No: 276560
SampleType: MS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchlD: 196762 Analysis Date: 09/25/2014
Seq No: 5841096
1
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
162.4
34
169.6
95.8
41.8
140
Aroclor 1260
269.9
34
169.6 120.1
88.3
39.4
140
Surr: Decachlorobiphenyl
14.00
0
16.96
82.5
35.2
148
Sum Tetrachloro-m-xylene
11.08
0
16.96
65.3
26.2
120
Qualiacrs: > Greater than Result value
BRL Below reporting limit
d Estimated value detected below Reporting Limit
Rpt Lim Reporting Litnit
Page 6 of 7
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix

Analytical Environmental Services, Inc
Client: Davis & Brown
Project Name: 224031
Workorder: 1409I22
Date: 26-Sep-14
ANALYTICAL QC SUMMARY REPORT
BatchID: 196762
Sample ID: 1409L50-001AMSD
Client ID:
Units: ug/Kg-dry Prep Date: 09/24/2014
Run No: 276560
SatnpleType: MSD
TestCode: POLYCHLORINATED BIPHENYLS Sw8082A
BatchID: 196762 Analysis Date: 09/25/2014
Seq No: 5841098
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
170.4
34
169.6
100
41.8
140
162.4
4.79
32.4
Aroclor 1260
276.0
34
169.6 120.1
91.9
39.4
140
269.9
2.26
32.7
Surr: Decachlorobiphenyl
20.93
0
16.96
123
35.2
148
14.00
0
0
Surr: Tetrachloro-m-xylene
12.77
0
16.96
75.3
26.2
120
11.08
0
0
QuaBRers: > Greater than Result value
BRL Below reporting limit
I Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
Page 7 of 7
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix

10/3/2014 woN.clerrson.edu/aglabresults/COMRLBRTURNER, SHERRY1409241409571.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 91296 Clemson University
TURNER, SHERRY ACCOUNT COMRLBR
PO BOX 219 DATE 09/24/2014
CHERAW SC 29520 [e-mail]
SAMPLE NO. 09171450 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen 0.00 % 0.00
Organic Nitrogen 0.89 % 17.71
Nitrate Nitrogen 120.71 ppm 0.24
---------------------------------------------------------------
INCORPORATED AVAILABLE NITROGEN ESTIMATE
11.01
SURFACE AVAILABLE
NITROGEN ESTIMATE
11.01
---------------------------------------------------------------
Phosphorus as P205
0.62
%
12.37
Potassium as K20
0.12
%
2.49
Calcium
23.11
%
462.19
Magnesium
0.17
%
3.34
Sulfur
0.19
%
3.81
Zinc
219.98
ppm
0.44
Copper
37.32
ppm
0.07
Manganese
42.09
ppm
0.08
Sodium
246.98
ppm
0.49
Moisture
20.59
%
Calcium Carbonate
------------------------------------------------------------------------------
Equivalency 58.73
%
1174.69
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some .loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste; method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
httpJ/www.cl emson.edu/ag labresults/COM RLBRTU RN ER,%20SH ERRY1409241409571.htm

% moisture
% solids
lbs. solids/ton
lbs. solids/500 tons
20.59
79.41
1588.2
794100
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0
0
0
0
0
0
Organic Nitrogen
0.8855
8855
17.71
1.115099
11150.99
22.30198
Nitrate Nitrogen
0.012071
120.71
0.24142
0.015201
152.0086
0.304017
Incorporated Available Nitrogen Estimate
0.5505
5505
11.01
0.693238
6932.376
13.86475
Surface Available Nitrogen Estimate
0.5505
5505
11.01
0.693238
6932.376
13.86475
Phosphorus as P2O5
0.6185
6185
12.37
0.778869
7788.692
15.57738
Potassium as K2O
0.1245
1245
2.49
0.156781
1567.813
3.135625
Calcium
23.1095
231095
462.19
29.1015
291015
582.03
Magnesium
0.167
1670
3.34
0.210301
2103.01
4.206019
Sulfur
0.1905
1905
3.81
0.239894
2398.942
4.797884
Zinc
0.021998
219.98
0.43996
0.027702
277.018
0.554036
Copper
0.003732
37.32
0.07464
0.0047
46.9966
0.093993
Manganese
0.004209
42.09
0.08418
0.0053
53.0034
0.106007
Sodium
0.024698
246.98
0.49396
0.031102
311.0188
0.622038
Calcium Carbonate Equivalency
58.7345
587345
1174.69
73.96361
739636.1
1479.272
September 2014

CHERAW ALKALINE BIOSOLIDS SOIL AMENDMENT
CHEMICAL CHARACTERISTICS AND LAND APPLICATION RATES
SIOSOLIDS SAMPLE DATE: November 19, 2014
Biosolids
Maximum
Maximum Maximum
Maximum
Metal
Allowable
Allowable
Application
Application
Content,
Metal
App. Rate,
Rate,
Rate,
METALS
ppm
Content, ppm
#/Acre/Yr. DT/Acre/Yr.
WT/Acre/Yr.
Arsenic, Total
0.55
41.00
1.80
B12.20
1624.39
Cadmium, Total
0.55 `
39.00
1.70
767.07
1534.15
Chromium, Total
0.82
1200.00
134.00
40671.09
81342.19
Copper, Total
0.82
1500.00
67.00
20495.67
40991.34
Lead, Total
0.55
300.00
13.00
5865.85
11731.71
Mercury, Total
0.03 '
17.00
0.75
7284.38
14568.75
Molybdenum, Total
2.22
18.00
0.80
90.09
180.17
Nickel, Total
14.93
420.00
18.70
313.14
626.29
Selenium, Total
0.55
36.00
4.50
2030.49
4060.98
Zinc, Total
5.97
1525.00
125.00
5233.03h 10466.06
PCB
BDL
1.60
Actual metal content less than amount indicated.
Biosolids
Biosolids
Maximum
Maximum
Nutrient
Nutrient
Crop/Soil
Application
Application
Content,
Content,
Requirement,
Rate,
Rate,
ppm
%
#/Acre "
DT/Acre/Yr.
WT/Acre/Yr.
Ammonium Nitrogen
245.73
0.02
Organic Nitrogen
6398.21
0.64
Incorporated Available
Nitrogen
4039.19
0.40
120.00
7.43
14.85
Surface Available Nitrogen
3965.47
0.40
120.00
7.57
15.13
Phosphorus as P205
3664.46
0.37
80.00
5.46
10.92
Potassium as K20
767.91
0.08
50.00
16.28
32.56
Calcium, Total
138724.04
13.87
Calcium as CaO
194213.66
19.42
Calcium as CaCO3 (CCE)
360059.59
36.01
2000.00
1.39
2.78
Magnesium, Total
1001.35
0.10
Manganese
24.57
0.00
Sulfur
1001.35
0.10
Percent Moisture
50.00
" These are typical values and must be adjusted based upon specific site conditions
DT is Dry Tons of Biosolids. WT is Wet Tons of Biosolids.
CERTIFICATION: This biosolid product has been produced by the Town of Cheraw's Wastewater
Treatment Plant by a treatment process that pasteurized plant residual solids using high temperature
and lime (calcium oxide). The Town of Cheraw certifies that this biosolid complies with the
Environmental Protection Agency regulations 40 CFR Part 503 for a "Class A" product and has a metal
and nutrient content as presented above.
DIRECTIONS FOR USE: This biosolid is intneded to be used as a soil amendment. The biosolid
land application rate shall not exceed the most restrictive Maximum Application Rate as indicated in
the table above. The application rate for nitrogen, phosphorus, potassium, and calcium is dependent
upon the crop grown and site soil characteristics. The user should contact the Clemson Extension
Service (B43-623.2134) and/or the Soil Conservation Service (B43-623-2187) for assistance in
determining the proper application rate for each crop and site. In no case shall the land application
rate exceed the agronomic rate for the crop grown. User should also refer to the Clemson Extension
Service Circular #476 titled "Lime and Fertilizer Recommendations."
THIS PRODUCT IS HIGHLY ALKALINE AND SHOULD BE HANDLED ACCORDINGLY.
AVOID PROLONGED CONTACT WITH THE SKIN. AVOID CONTACT WITH THE EYES.
THE TOWN OF CHERAW IS NOT RESPONSIBLE FOR IMPROPER USE OR HANDLING OF THIS
BIOSOLID PRODUCT.
Mr. Ricky D. Ingram, Public Utility Director
P. O. Box 219; Cheraw, SC 29520
Telephone: [phone]
FAX: [phone]
PRODUCT USER NAME:
ADDRESS:
INTENDED USE:
LOCATION OF USE:
QUANTITY RECEIVED:
RECEIVED BY:

Davis & Brown
PO Box 15038
Quinby, SC 29506
[phone] FAX: [phone]
Certificate of Analysis
Client: CHERAW, TOWN OF
P.O.BOX 219
CHERAW, SC 29520
Contact: SHERRY TURNER
Client #: 168
Sample Date: 19-Nov-14
SDG #: SDG-102630
South Carolina Certification Number: 21117
Receipt Date: 20-Nov-14
Report Date: 03-Dec-14
Approved By: — Z/A,.K
Van Ward
Lab Director
Reporting
Parameter Result Limit Unit Method Flag Date Time Analyst
LSID-226570 1007-T
Total Toxic Organics 0.0141 mg/L 8260B\8270D\624 S11A 11/26/2014 18:27 YH
LSID-226571
BIO SOLIDS- 11-19-14-500
Acid Digestion (Solids)
YES
EPA 200.2
11/24/2014
10:00
JR
Selenium, Total
<0.861
0.861
mg/kg
EPA 7010 / 6010C
11/24/2014
11:34
JR
Percent Moisture
22.3
0.1
Wt%
SW846 3540
11/21/2014
16:14
JW
Aluminum, Total
162
3.45
mg/kg
SW846 6010C
11/25/2014
15:00
JR
Arsenic, Total
<0.861
0.861
mg/kg
SW846 6010C
11/24/2014
11:34
JR
Cadmium, Total
<0.861
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Chromium, Total
1.28
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Copper, Total
1.27
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Lead, Total
<0.861
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Molybdenum, Total
<3.45
3.45
mg/kg
SW846 6010C
11/25/2014
15:00
JR
Nickel, Total
23.2
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Zinc, Total
9.28
0.861
mg/kg
SW846 6010C
11/25/2014
10:49
JR
Mercury, Total
<0.040
0.04
mg/kg
SW846 7470A
11/24/2014
12:30
CG
PCB
BRL
mg/kg
SW846 8082A S11A
11/25/2014
' 12:07
BB
Page 1

Analytical Environmental Services, Inc
Date: 2-Dec-14
Client:
Davis & Brown
Client Sample ID:
226571
Project Name:
226571-226570
Collection Date:
11/19/2014 1:00:00 PM
Lab ID:
1411J33-001
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Units
BatchID
Date Analyzed
Analyst
Limit
Factor
POLYCHLORINATED BIPHENYLS
SW8082A
(SW3550C)
Aroclor 1016
BRL
41
ug/Kg-dry
199672
1
I1/25/2014 12:07
BB
Aroclor 1221
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Aroclor 1232
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Aroclor 1242
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Aroclor 1248
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Aroclor 1254
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Aroclor 1260
BRL
41
ug/Kg-dry
199672
1
11/25/2014 12:07
BB
Surr: Decachlorobiphenyl
75.7
36.1-138
%REC
199672
1
11/25/2014 12:07
BB .
Surr: Tetrachloro-m-xylene
106
28.3-116
%REC
199672
1
11/25/2014 12:07
BB
PERCENT MOISTURE D2216
Percent Moisture
18.7
0
Wt%
R280930
1
11/28/2014 09:00
PF
Qualifiers: ` Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Resultvalue
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
J Estimated value detected be Reporting Limit Page 4 of 27

CHAIN F CUSTODYRECORD
Ptdge X of
1E)AVIS & BROWN
Post Office Box 15036 124 West McIver Road
Quinby, South Carolina 29506 Florence, South Carolina 29501
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1/26/2015 , wwvv.clemson.edu/aglabresults/COMRLBRTURNER, SHERRY1412041527595.htm
A N I M A L W A S T E A N A L Y S I S R E P O R T
Agricultural Service Laboratory
LAB No. 121559 Clemson University
TURNER, SHERRY
P 0 BOX 219
CHERAW SC 29520
ACCOUNT COMRLBR
DATE 12/04/2014
[e-mail]
SAMPLE NO. 11191450 MANURE: OTHER STORAGE: COVERED
-----------------RESULTS REPORTED ON AN AS -SAMPLED BASIS----------------------
lbs/ton
Ammonium Nitrogen
0.04
%
0.80
Organic Nitrogen
1.04
%
20.83
Nitrate Nitrogen
---------------------------------------------------------------
3.2'6
ppm
0.01
INCORPORATED AVAILABLE NITROGEN ESTIMATE
13.15
SURFACE AVAILABLE
NITROGEN ESTIMATE
12.91
---------------------------------------------------------------
Phosphorus as P205
0.60
%
11.93
Potassium as K20
0.13
%
2.55
Calcium
22.58
%
451.63
Magnesium
0.16
%
3.26
Sulfur
0.16
%
3.26
Zinc
223.86
ppm
0.45
Copper
40.70
ppm
0.08
Manganese
39.89
ppm
0.08
Sodium
232.81
ppm
0.47
Moisture
18.60
%
Calcium Carbonate
--------------------------------------------------------------------------
Equivalency 58.61
%
1172.21
INCORPORATED PLANT AVAILABLE NITROGEN ESTIMATE - 80% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
incorporated into the soil within hours of application. Assumes some loss of
ammonium-N during application and prior to incorporation.
SURFACE PLANT AVAILABLE NITROGEN ESTIMATE - 50% of ammonium-N, 60% of
organic-N, and 100% of nitrate-N (if determined). Assumes the manure will be
left on the surface of the soil with no incorporation by plowing or irrigation.
Available nitrogen calculations are estimates and if nitrate-N was not re-
quested the amount of available nitrogen may be slightly more than reported.
Also, the actual amount may be more or less than the estimate depending on the
composition of the manure, soil type,, and environmental conditions.
All of the potash in the animal waste should be plant available in the first
year of application. Although not all of the phosphorous is available in the
first year, its availability should be comparable to that in commercial
fertilizers.
The rate of animal waste to apply for crop production is dependent on the
nutrient content of the waste, method of application and incorporation, soil
test, crop to be grown, and previous manure applications. In most cases, the
http://vvNw.clemson.edu/ag labresults/COM RLBRTU RN ER,%20SH ERRY1412041527595.htm 1/2

Olo moisture
solids
lbs. solids/ton
lbs. solids/500 tons
18.6
81.4
1628
814000
%
ppm
lbs/ton
%
ppm
lbs/ton
as -sampled
as -sampled
as -sampled
dry ton
dry ton
dry
Ammonium Nitrogen
0.04
400
0.8
0.04914
491.4005
0.982801
Organic Nitrogen
1.0415
10415
20.83
1.279484
12794.84
25.58968
Nitrate Nitrogen
0.000326
3.26
0.00652
0.000400
4.004914
0.00801
Incorporated Available Nitrogen Estimate
0.6575
6575
13.15
0.80774
8077.396
16.15479
Surface Available Nitrogen Estimate
0.6455
6455
12.91
0.792998
7929.975
15.85995
Phosphorus as P2O5
0.5965
5965
11.93
0.732801
7328.01
14.65602
Potassium as K2O
0.1275
1275
2.55
0.156634
1566.339
3.132678
Calcium
22.5815
225815
451.63
27.7414
277414
554.828
Magnesium
0.163
1630
3.26
0.200246
2002.457
4.004914
Sulfur
0.163
1630
3.26
0.200246
2002.457
4.004914
Zinc
0.022386
223.86
0.44772
0.027501
275.0123
0.550025
Copper
0.00407
40.7
0.0814
0.005
50
0.1
Manganese
0.003989
39.89
0.07978
0.0049
49.00491
0.09801
Sodium
0.023281
232.81
0.46562
0.028601
286.0074
0.572015
Calcium Carbonate Equivalency
58.6105
586105
1172.21
72.00307
720030.7
1440.061
November 2014

Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM MINIMUM
DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT
1 /2/2014
12.87
12.27
165
159
1 /6/2014
12.65
12.35
158
160
1 /10/2014
12.77
12.43
158
159
1 /15/2014
12.80
12.41
159
161
1 /16/2014
12.76
12.41
159
1598
1 /17/2014
12.58
12.29
158
160
1 /22/2014
12.66
12.31
159
160
2/4/2014
12.82
12.55
164
158
2/5/2014
12.55
160
159
2/6/2 014
12.81
12.37
161
159
2/7/2014
12.76
12.31
165
158
2/10/2014
12.90
12.17
160
159
2/17/2014
12:79
12.57
161
159
2/18/2014
12.76
12.55
160
159
2/19/2014
12.85
12.55
159
159
2/20/2014
12.81
12.47
158
159
2/21 /2014
12.87
12.36
173
159
2/24/2014
12.86
12.28
171
158
2/25/2 014
12.85
12.32
162
159
2/26/2014
12.85
12.40
174
159
2/27/2014
12.89
12.28
213
159
2/28/2014
12.71
12.37
212
159
3/3/2014
12.88
12.41
212
159
3/5/2014
12.86
12.41
160
159
3/6/2014
12.59
12.20
161
159
3/21 /2014
12.63
12.36
159
159
3/24/2014
12.93
12.49
159
159
3/26/2014
12.72
12.50
161
159
3/2 6/2 014
12.78
12.43
162
159

I
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM MINIMUM
DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT
4/1 /2014
12.56
12.28
159
159
4/2/2014
12.76
12.31
159
159
4/4/2014
12.51
12.29
159
172
4/7/2 014
12.48
12.21
159
159
4/8/2014
12.59
12.28
159
160
4/9 /2 014
12.51
12.22
159
159
4/10/2014
12.51
12.26
159
159
4/11 /2014
159
159
4/ 14/2014
12.62
12.26
159
159
4/15/2014
12.62
12.28
159
159
4/16/2014
12.68
12.25
159
159
4/ 17/2014
12.36
12.01
159
161
4/ 18/2014
12.51
12.22
159
160
4/22/2014
12.60
12.47
159
159
6/18/2014
12.63
11.84
159
159
6/23/2014
11.92
11.81
161
164
6/24/2014
11.68
11.81
162
173
6/25/2014
11.92
11.99
159
161
6/30/2014
11.84
11.73
159
161

n
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM MINIMUM
DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT
7/1 /2014
12.14
11.88
160
159
7/2/2014
12.08
12.00
166
160
7/3/2014
11.98
11.89
159
160
9/18/2014
12.18
12.02
164
162

t
Pasteurization vessel operates on a constant speed with an in/out
time duration of 30 minutes.
MINIMUM MINIMUM
DATE 2 HOUR pH 24 HOUR pH TEMP IN TEMP OUT
11 /14/2014
12.32
12.08
158
158
11 /17/2014
12.52
12.52
158
163
11 /18/2014
12.56
12.45
162
176
11 /19/2014
12.47
12.29
161
164
12/3/2014
12.33
12.35
159
177
12/4/2014
12.40
12.43
159
158
12/5/2014
12.46
12.16
163
158
12/8/2014
12.46
12.39
197
165
12/10/2014
12.35
12.34
159
168
12/15/2014
12.32
12.32
170
183
12/16/2014
12.30
12.55
158
169
12/23/2014
12.30
12.16
159
172

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town of Cheraw Permit Number: WQ0014248
WWTP Name: Town of Cheraw WWTP NPDES Number: SCO020249
Monitoring Period: From 01 /01 /14 To 12/31 /14
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4❑
Alternative 5 ®
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
1 Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization
Class B:
Alternative 1 ❑
Alternative 2 1-3­7
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Level in
Pathogen Density
um er. o
Excee-
dences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-riique
inimu
Geo. Mean
MaximumUnits
Fecal Coliform
2x 10tothe 91h
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
1000 mpn per
gram of total solid
(dry, weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ 1 Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ®,1 Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑.
No vector attraction reduction options were performed ❑
U Kl'll+' LUA110N SI A'1'L+'MENF (please check the appropriate statement)
Es "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I.certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Ricky Ingram/Public Utility Director
Preparer Name and Title (type or print)
zLS
Signature 9f Prepadr Date_
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
Author Daryl D. Merritt DENR FORM RF.(7/2002)

1. 1
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
I V dilution / 10 ml sample 10-' dilution / 1.0 ml sample
Single Strength Single Strength
10'2.dilution / 1.0 ml sample 10' dilution / 0.1 ml sample
Date/Time Test Set -Up: j- —4"I'l.,'.
40 .n,. Date/ Time Test Read:
Time Placed in Incubator: J : a Sp, y.,, Incubator Temp: 3 Y 6 c
Time Transferred to Water Bath: };ZS' nl Water Bath Temp:
Operator : f �jQ 15��{ �A /�,�J� Media, Lot # 3 A 3 80 S
Solids 3.q, 0 Sample #
MPN Fecal Coliforan = 10 x MPN Index / 100 ml = Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results; - indicates negative -results
Biosolids Collection: Date j - J_f Time Op.

FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
_ (A-B)X100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # :
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish'
Weight of wet sample + dish
% Total Solids
q 7(,4
�q61q--a,0gg7xj64,
3w,;305— �16gq�
ji43g.3q 3`�•��
�,/1

j
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS .
A-1 Medium
Double Strength Single Strength
10` dilution / 10 ml sample 10-1 dilution / 1.0 ml sample
Single Strength
10'z dilution / 1.0-ml sample
Single Strength
10'z dilution / 0.1 ml sample
Date/Time Test Set -Up: a- ? Y-11,'06pqn, ` Bate/ Time Test Read: a Q ' / f - /9,* rk.,
Time Placed in Incubator: ) ::30p. A„ , Incubator Temp: S-5 c-
0
.Time Transferred to Water Bath: q-: 3op n,. Water Bath Temp: C.i
Operator RR1S0 t/i�Media Lot # 3 A 3 84 S'
% Solids 7 /0 Sample #
MPN Fecal Coliform = 10 x MPN Index / 100 ml Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results; -indicates negative results , J
Biosolids Collection: Date Time I'A64 Op. ��/C�2

Where:
CALCULATION FOR TOTAL SOLIDS IN BICSOLIDS SADLE
% Total Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of vet sample + dish (mg)
Sample # :
Weight of dried residue + dish --
Duplicate -weight of dried reside + dish:
Weight of empty dish
Weight of wet sample + dish
% Total Solids 7, q
.�a126ra,d��{
C

FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A 1 Medium
Double Strength Single Strength
10'1 dilution / 10 ml sample 10-' dilution / 1.0 ml sample
Single Strength
10'2 dilution / 1:0 ml sample
Single Strength
10' dilution / 0.1 ml sample
Date/Time Test Set -Up: ,3�/�-/�� :OQ/�=/n• Date/ Time Test Read: 3-A0-1 % �•-3� "^•
Time Placed in Incubator: �:.35�• �- �_ Incubator Temp: 3-s
c
Time Transferred to Water Bath: L' 3S,P•�• Water Bath Temp: �-�• � G
Operator iSON D, Media Lot # 3,23 8'o `} 8
% Solids Sample # 3• J �� J 1 f - SQ p
MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date 3 9- . Time Op.�{��

FORMULA:
'There:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SANPLE
% Totall Solids = (A - B) x 100
C-B
A = IvVeight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # : 3, ]N � — 06
Weight of dried residue + dish:
Duplicate Freight of dried residue + dish:
Weight of empty dish
Weight of wet sample +clash
% Total Solids = ,3 I • /�
1'715-
�f
`3 S 3 S4

I
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10'1 dilution / 10 ml sample
Single Strength
10'1 dilution / 1.0 ml sample
.f
Single Strength
10'2_ dilution / 1.0 ml sample
Single Strength
10'Z dilution / 0.1 ml sample
Date/Time Test Set -Up: Date/ Time Test Read:
Time Placed in Incubator:. Incubator Temp:
Time Transferred to Water Bath:f! SrA.�.. Water Bath Temp:1J�, c
Operator 41) w Media Lot # 32.3 e J qo'
% Solids 3. Sample #:
MPN Fecal Coliform = 10 x WN Index /-100 ml
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: +indicates positive results ; - indicates negative results
Biosolids Collection: Date �-�� �/� Time l�`oo�•�►• '- . Op:

CALCULATION LATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
PLE
FORA:
%Total Solids = (A-B)X100
C-B
VV ere:
A _ Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = VTeight of wet sample + dish (mg)
Sample#:
Weight of dried residue + dish:
Duplicate -weight of dried reside + dish:
Weight of empty dish
Weight of wet sample + dish
% Total solids = : q-3. 4 %
/Q • _• 5,f''l
�4
p��• o TQ-,. "0840 ^
9'Y&.00 - 43,
YaYd.
C

FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A I Medium
Double Strength
10'1 dilution / 10 ml sample
Single Strength
10-' dilution / 1.0 ml sample
r--
Single Strength
10' dilution / 1.0 ml sample
Single Strength
10' dilution / 0.1 ml sample
Date/Time Test Set-Up:.'b0 .m, Date/ Time Test Read: s'•�t ' i o .n�.
a
Time Placed in Incubator: 1: IS-p, rv► . Incubator Temp:
a
Time Transferred to Water Bath: ' 1 Srl� • Water Bath Temp: q4.6 C
Operator LC9 Media Lot # 3 A 3
% Solids Sample #
MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q
per Cram Total Solids Largest Volume x %. Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date �.$~� % — % Time l.`DO ,m .. Op.

C Y
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAWLB
FORMULA.:
% Total Solids = ( A - B) x 100
C-B
VVhere:
A. = Weight of dried residue + dish (mg)
B = Weight of empty dish (Mg)
C = Weight of Bret sample + dish (mg)
Sample # :
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of empty dish
Weight of wet sample + dish
% Total Solids = - 4 G. 17a
�ggo.ao � L(,j�o
c

FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10-1 dilution / 10 ml. sample 10-1 dilution 1.0 ml sample
Single Strength
10' dilution 1.0 ml sample
Single Strength
10' dilution 0.1 ml sample
ftti
Date/Time Test Set -Up: Date/ Time Test Read:
Time Placed in Incubator: Incubator Temp:
Time Transferred to Water Bath: m Water Bath Temp:.
Operator Media Lot 4 :.3,o? cit K+,-A
% Solids Sample#
MPN Fecal Cofform. = 10 xMPN Index/ 100
per G-ram. Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results indicates negative results
Biosolids Collection: Date
00. Y k
f

Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SANTLE
% Total Solids
(A.-B)xl00
. C-B,
A =%7eight of dried residue + dish (mg)
B = Weight of efnpty dish (mg)
C = Weight of wet sample + dish (mg)
Sample # ('P LF -. s-&O
Weight of dried residue + dish:
Duplicate-vveight of dried residue + dish:
Weight of empty dish
Weight of wet sample + dish
% Total Solids, 7"
x too
c
",

C
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
Double Strength Single Strength
10-1 dilution / 10 ml sample 10-1 dilution / 1.0 ml sample
Single Strength
10' dilution / 1.0 ml sample
Single Strength
10'Z dilution / 0.1 ml sample
Date/Time Test Set -Up: -16 -1�' �f,• 60A,,t, Date/ Time Test Read: 7:1 °7-,l 4 l 3 @�, r►
a
Time Placed in Incubator: f: 3@ p.M - Incubator Temp: 3 D G
_ Q
Time Transferred to Water Bath: �,3@P �,, Water Bath Temp: �C
Operator %�, ,� (.� Media Lot # 3Q?
%Solids , e �%a Sample# 7-14-14-S_66 /3AfC.h a�s4S'
MPN Fecal Coliform = 10 x MPN Index / 100 ml = . . C/)
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date Time : Qd Op.

FORMULA:
Vv7here:
CALCUI.,ATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMPLE
% Total Solids
(A.-B)xla0
C-B
A = Weight of dried reside + dish (mg)
B = Weight of empty. dash (mg)
C = NTeight of wat sample + dash (mg)
Weight of dried residue + dish: .
Duplicate Freight of dried residue + dish:
Weight of empty dash
Weight of wet sample + dish
aim Total Solids
SF. 6 M .67,Yc
C
-------------------

FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10` dilution / 10 ml sample 10` dilution / 1.0 ml sample
Single Strength
10` dilution / 1.0 ml sample
Single Strength
10' dilution / 0.1 ml sample
Date/Time Test Set -Up: S 30- 14 1,'t , Date/ Time Test Dead:
Time Placed in Incubator: l : A Incubator Temp: �
Time Transferred to Water Bath: tA'. V-5 Water Bath Temp: � L s a�
Operator Media Lot # 2 , 150 4 �
%Solids �3.3`/� Sample#'a��1Li- ��� �r��ho06
MPN Fecal Coliform 10 x MPN Index / 100 ml =
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date q--a#'-w Atz), Time I = ��p Op. v

A 4
FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BICSOLIDS SAI�QLE
% Total. Solids = (A - B) x 100
C-B
A = Weight of dried residue + dish (mg)
l3 = weight of empty dish (mg)
C = Tei ,ht of wet sample + dish (mg)
Sample A: IiKe D i` 14- �0
Weight of dried reside + dish:
Duplicate -weight of dried residue + dish:
Weight of empty dash
Weigh of wet sample + dish
% Total Solids
ol0
�1 0
100 �, -- R. N3(P )� 10" . ;3 3�1
34..kq c3 r. ),b'63(p
C

FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10-1 dilution / 10 ml sample 10"1 dilution / 1.0 ml sample
Single Strength
10-2 dilution / 1.0 ml sample
Single Strength
10'z dilution / 0.1 ml sample
Date/Time Test Set -Up: �-/ J- J �/: bQ p. Date/ Time Test Dead:rr--
Tinge Placed in Incubator: J � Sd, m . Incubator Temp:
Time Transferred to Water Bath: .rri, Water Bath Temp:
Operator %� �fr} Media Lot # 323 D Ll g
% Solids 1 �f �� 3 i. Sample
MPN Fecal Coliform = 10 x MPN Index / 100 ml
per Gram Total Solids Largest Volume k % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date 9-%`J -% Time - . M ;. Op. h ul/4l

CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAIVTLE
FORMULA:
% Total Solids = (A - B) x 100
C-B
Where:
A = Weight of dried residue + dish (mg)
B = Weight of empty dish (mg)
C = Weeight of -wet sample + dish (mg)
Sample # : 3 - /9— 1, -a ,-a®
Weight of dried residue + dish:
Duplicate weight of dried residue + dish:
Weight of efgty disli
Weigh of wet sample + dish
% Total Solids = �� p • °� ° 3
�g- LP
4L JI -�a-
�,3.
314Y8 4

C .
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength Single Strength
10-1 dilution / 10 ml sample 10'1 dilution / 1.0 ml sample
Single Strength
10' dilution / 1.0 ml sample
Single Strength
10-2 dilution / 0.1 ml sample
Bate/Time Test Set -Up: /D-! I .'00
,,; Date/ Time Test Read:
a
Time Placed in Incubator: Incubator Temp: .34 d �
Time Transferred to Water Bath: =36
Operator Lc7
% Solids, 3�
Water Bath Temp:
Media Lot #
l�
Sample # !C —�S% �- , Q D Lc� �R C% 0 tad
MPN Fecal Coliform = 10 x MPN Index k 100 ml = 0
per Cram Total Solids Largest Volume x. % Dry Sofids .
NOTE: + indicates positive results; -indicates negative results
Biosolids Collection: Date Time Op. �, �(//�, � V.

FORMULA:
Where:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS -SAWLE
% Total Solids = (A - B) x 100
c-B
A = freight of died residue + disk (mg)
B = freight of empty dish (mg)
C _ freight of Bret sample + disk (mg)
Sample # :
Weight of died residue + dish:
Duplicate -vveight of dried. reside + dish:
Weight of empty dish
Weight of vet sample + dish
% Totd So id.s
A
��, �'�oa�a•o8�s
c

,4I 0
�- FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
\ A-1 Medium
Double Strength Single Strength
10-1 dilution / 10 ml sample 10'1 dilution / 1.0 ml sample
Single Strength
10'2 dilution / 1.0 ml sample
Single Strength
10 z dilution / 0.1 ml sample
l Date/Time Test Set -Up: !"%?-4 /�Od
Time Placed in Incubator: /:,3Q,�.,,, :_-
Date/ Time Test Read: Tw /,1` A � ��• ^�
Incubator Temp: ,3 -5 1
Time Transferred to Water Bath: 4!3 0 g. t, , Water Bath Temp: '
Operator G- Media Lot # 3.Z 330 ?
DOD
% Solids I. j;�v Sample # '-,5�aa
MPN Fecal Coliform = 10 x MPN Index / 100 ml * = Q
per Gram Total Solids Largest Volbi ie X. % Diy.,Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date Time : 30 Op.

CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAWLE
FORMLJLA:
% Total Solids = (A - B) x 100
c-B
VVhere:
A = Weight of dried residue + dish (mg)
B =weight of empty dish (mg)
C : '%Teight of wet sample + dish (mg)
Sample # : 1�. �- I q- - 5-6 0
Weight of dried residue + dish:
Duplicate sleight of dried residue + dish
Weight of empty dish
Weight of wet saniple + dish
% Total Solids
a• G sa.�
p4 �4q13-J.0" kib0jr
------------------
cl � es- a.
gig : � � r � �• � �a
a

(VA) 4%
FECAL COLIFORM FOR MUNICIPAL BIOSOLIDS
A-1 Medium
Double Strength
10'1 dilution / 10 ml sample
Single Strength
10-1 dilution / 1.0 ml sample
Single Strength
10' dilution / 1.0 ml sample
Single Strength
10'2 dilution / 0.1 ml sample
Date/Time Test Set -Up: , pt Date/ Time Test Read:
Time Placed in Incubator: 1d .�._pA, nj Incubator Temp: 35, 0 oG17-
Time Transferred to Water Bath: Water Bath Temp:-,�,�t
Operator �I salmi Media Lot #
% Solids 3% �/o Sample #
MPN Fecal Coliform = 10 x MPN Index / 100 ml = Q
per Gram Total Solids Largest Volume x % Dry Solids
NOTE: + indicates positive results ; - indicates negative results
Biosolids Collection: Date �2-I`j-!� Time f0: Op. �ir,4�7e,j S

FG 4ULA:
'�N7here:
CALCULATION FOR TOTAL SOLIDS IN BIOSOLIDS SAMIPLE
% Total Solids = .(A -. B) x l ®O
c-B
A = "Weight of dried residue + dish (mg)
B = iWeight of empty dish (mg)
_Weight of wet sample + dish (mg)
Sample # :/�,�
Weight of dried residue + dish-
Duplicate weight of dried residue + dish:
'VVeight of empty'dish
Weight of wet sample + dish
% Total Solids = q , a
1o.fS6a.
`7
f6.'°.�43?
..,,aa• f83� .