NCS000150_COMPLETE FILE - HISTORICAL_20161019

NORTH CAROLINA
Department of Environmental Qual

STORMWATER DIVISION CODING SHEET
RESCISSIONS
PERMIT NO.
AIL50 OO
DOC TYPE
❑COMPLETE FILE -HISTORICAL
DATE OF
RESCISSION
❑ O�� � �-P / � J /
YYYYMMDD

aceAnalytical
www.pac0abs.com
October 03, 2016
David Lorbacher
Arclin-Dynea/Moncure
790 Corinth Road
Chapel Hill, NC 27599
RE: Project: STORMWATER SAMPLING
Pace Project No.: 92312830
RECEIVED
O t 19 2016
CEWRAL FILES
DwR SECTION
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Dear David Lorbacher:
Enclosed are the analytical results for sample(s) received by the laboratory on September 19, 2016.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc: Bowman Harvey, Acrlin-❑ynea/Moncure
Chis Lamm, Arclin-Oynea/Moneure
REPORT OF LABORATORY ANALYSES
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc., Page 7 of 24

I
eAnalytical`
invw.pacselahi.corrr
Project: STORMWATER SAMPLING
Pace Project No_: 92312630
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: PL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Ashoville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37736
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
CERTIFICATIONS
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirgiriiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 2 of 24

I
eAnaljftal
a
www.pncelabs.com
Project: STORMWATFR SAMPLING
Pace Project No_= 92312830
Lab ID Sample ID
92312830001 00291916
J
92312830002 00391916
92312830003 00491916
Pate Analytical Services. Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Anatytes
Reported
Laboratory
SM 2540D
KCE
1
PASI-E
SM 5210E
RAY
1
PASI-E
EPA 1664E
JMS
1
PASI-C
EPA 8315
CRT
1
PASI-O
EPA 9040
ALC
1
PASI-A
EPA 350.1
DMN
1
PASI-A
EPA 351.2
BRJ
1
PAS! -A
EPA 353.2
DMN
1
PASI-A
EPA 365.1
CJH1
1
PASI-A
EPA 420.4
DMN
1
PAS1-A
SM 5220D
MDW
1
PASI-A
SM 2540D
KCE
1
PASI-E
SM 5210B
DWJ
1
PASi-E
EPA 1664E
JMS
1
PASI-C
EPA 8315
CRT
1
PASI-O
EPA 9040
ALC
1
PASI-A
EPA 350.1
DMN
1
PASI-A
EPA 351.2
BRJ
1
PASI-A
EPA 353.2
DMN
1
PASI-A
EPA 365-1
CJH1
1
PASI-A
EPA 420.4
DMN
1
PASI-A
SM 5220D
MOW
1
PASI-A
SM 2540D
KCE
1
PASI-E
SM 5210B
DWJ
1
PASI-E
EPA 1664E
JMS
1
PASI-C
EPA 8315
CRT
1
PASI-O
EPA 9040
ALC
1
PASI-A
EPA 350.1
DMN
1
PASI-A
EPA 351,2
BRJ
1
PASI-A
EPA 353.2
DMN
1
PASI-A
EPA365.1
CJH1
1
PASI-A
EPA 420.4
DMN
i
PASI-A
SM 52200
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„ Page 3 of 24

laneAnalytical"'
wwrvpacel86.xcom
ANALYTICAL RESULTS
Project- STORMWATER SAMPLING
Pace Project No.: 92312830
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: 00291916
Parameters
Lab Ill: 92312830001 Collected: 09/19/16 14:15
Results Units Report Limit OF
Received: 09119116 16:35 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
16.8 mglL
3.3
1
09/21/16 09:27
5210E BOD, 5 day EDN
Analytical Method: SM 52108
BOD, 5 day
9.5 mgll
2.0
1
09/21116 13:57
09/26/16 10:07
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mglL
5.0
1
09/23/16 08:33
8315 W HPLC
Analytical Method: EPA 8315 Preparation
Method: EPA 8315
Formaldehyde
140 ug1L
0.10
1
09/21/16 08:15
09/23/16 03:23
50-00.0
9040 pH
Analytical Method: EPA 9040
pH
6.3 Sid. Units
0.10
1
09/30/16 09:51
H6
360.1 Ammonia, Low Level
Analytical Method: EPA 350.1
Nitrogen, Ammonia
11.4 mglL
0.10
10
09/26/16 19:55
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method; EPA 351.2
Nitrogen, Kjeldahl, Total
21.7 mg1L
2.5
5
09127/16 23:40
7727-37-9
363.2 Nitrogen, NO2/NO3 Ares.
Analytical Method: EPA 353-2
Nitrogen, NO2 plus NO3
53.3 mg1L
0.30
15
09/30/16 20:29
365.1 Phosphorus, Total
Analytical Method: EPA365.1
Phosphorus
0.12 mg1L
0.050
1
09/23/16 04:22
7723.14-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
0.038 mg/L
0.010
1
1010311613:49
M1
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
79.0 mg1L
25.0
1
09/23/16 21:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 24

IeAnayicai
. www4wcrabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)B34-4984
Project_ STORMWATER SAMPLING
Pace Project No.: 92312830
Sample: 00391916 tab ID: 92312030002 Collected: 09/19/16 15:00 Received: 09/19/16 16:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
10.8 mg1L
2.5
1
09/21/16 09:27
52108 BOO, 5 day EDN
Analytical Method: SM 52106
BOD. 5 day
11.6 mg/L
2.0
1
09/20/16 16:49 09125116 14:15
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0
1
09/23/16 08:33
8316 W HPLC
Analytical Method: EPA 8315 Preparation Method: EPA 8315
Formaldehyde
81.4 ug1L
0.10
1
09/21/16 08:15 09/23116 03:43
50-00-0
9040 pH
Analytical Method: EPA9040
pH
6.9 Std. Units
0.10
1
09/30/16 09:51
H6
350.1 Ammonia, Low Level
Ana lylical Method: EPA 350.1
Nitrogen, Ammonia
1.8 mglL
0,010
1
09/26/16 19:17
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
4-1 mg1L
0.50
1
09/27116 23:28
7727.37-9
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
8.1 mg1L
0,060
3
09/30/16 20:30
366.1 Phosphorus, Total
Ana lylical Method: EPA 365.1
Phosphorus
0.088 mglL
0.050
1
09/23/16 04:23
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
0.030 mg/L
0.010
1
1010311613:51
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
62.0 mg1L
25.0
1
09/23/16 21:55
REPORT OF LABORATORY ANALYSIS
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Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 24

aceAnalytical
wwwpacelahs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc-
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: STQRMWATER SAMPLING
Pace Project No.: 92312830
Sample: 00491916 Lab ID: 92312930003 Collected: 09119/16 14:00 Received: 09119116 16:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
17.6 mg1L
1
5.0
1
09/21/16 09:28
5210B BOD, 5 day EON
Analytical Method: SM 5210B
80D, 5 day
17.4 mglL
2.0
1 09120/16 16:49
09/25/16 14:15
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg&
5.0
1
09/23116 08:33
8315 W HPLC
Analytical Method: EPA 8315 Preparation
Method: EPA 8315
Formaldehyde
24.3 ug1L
0.10
1 09/21/16 08:15
09/23/16 04:03
50-00-0
9040 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units
0.10
1
09/30/16 09:51
H6
350.1 Ammonia, Low Level
Analytical Method: EPA 350.1
Nitrogen, Ammonia
0.60 mglL
0.010
1
09/2611619:19
7664-41-7
351.2 Total Kjoldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldaht, Total
6.6 mg1L
0.50
1
09/27/16 23:29
7727-37-9
353.2 Nitrogen, N021NO3 Ares.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
19.6 mg/L
0.20
10
09/30/16 20:31
366.1 Phosphorus, Total
Analytical Method: EPA365.1
Phosphorus
1.1 mg1L
0.050
1
09123/16 04:24
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
0.024 mg1L
0.010
1
1010311613:52
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
126 mg1L
25.0
1
09/23/16 21:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 24

accAnalj cal
WW'Weelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
QC Batch: 329568 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Paco Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 1826189
Matrix:
Water
Associated Lab 9amples: 92312830001, 92312830002, 92312830003
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 09/21/16 09:21
LABORATORY CONTROL SAMPLE:
1826190
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Total Suspended Solids
mg1L
250
252 101 90-110
SAMPLE DUPLICATE: 1826191
92312787001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 131 113 15 D6
SAMPLE DUPLICATE: 1826192
92312945003 Dup
Parameter Units Result Result RPD Oualifiers
Total Suspended Solids mg1L 141 146 3
Results presented on this page are in the units indle3ted by the "Unds" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 1010312016 04:52 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 24

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc-
6701 Conference Drive
Raleigh, NC 27607
(919)834-49B4
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
OC Batch: 329406
Analysis Method:
SM. 5210B
QC Batch Method: SM 52108
Analysis Description:
5210B BOD, 5 day EDN
Associated Lab Samples: 92312830002. 92312830003
METHOD BLANK: 1825466
Matrix: Water
Associated Lab Samples: 92312830002, 92312830003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 09/25/16 i4:15
LABORATORY CONTROL SAMPLE:
1825467
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg1L
198 199
101 84.6-115.4
SAMPLE DUPLICATE: 1825468
92312784002 Dup
Parameter
Units
Result Result
RPD Qualifiers
SOD, 5 day
mg/L
131
131 0
Results presented on this page are In the units indicated by the "Unlis" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 24

aceanafyica!®
"mpacdahs.com
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
QC Batch: 329610
QC Batch Method: SM 5210B
Associated Lab Samples: 92312830001
METHOD BLANK: 1826439
Associated Lab Samples: 92312830001
Parameter
Units
BOD, 5 day
mg1L
LABORATORY CONTROL SAMPLE: 1826440
Parameter
Units
BOD, 5 day
mg1L
SAMPLE DUPLICATE: 1826441
Parameter Units
BOU, 5 day mg1L
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 21607
{919j834-4984
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210E BOD, 5 day EDN
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 09/2611610:07
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 219 111 84.6-115.4
92312975001 Dup
Result Result RPD Qualifiers
672 662 1 B1
Resorts presented on this page are in the units indicated by the-UnRs;- column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/0312016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 24

(�IlacleAnalyticalo
wwwpacula4mm
QUALITY CONTROL DATA
Projecl: STORMWATER SAMPLING
Pace Project No.: 92312830
OC Batch: 330004 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1828435 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 09/23/16 08:28
Pace Analytical Servicas, Inc.
6701 Conference Drive
Raleigh. NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
1828436
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifers
Oil and Grease
mgtL
40 36.5
91
78-114
MATRIX SPIKE SAMPLE:
1828437
92313006001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
34.4
86
78-114
Results presented on this page are in the units Indicated by the `Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 24

(�.Iacmnalyficaf'
W*W.Pacefebtizom
QUALITY CONTROL. DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
QC Batch: 321682 Analysis Method: EPA 8315
QC Batch Method: EPA 8315 Analysis Description: 8318 HPLC
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
1919j834-49B4
METHOD BLANK: 1711792 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Formaldehyde ug/L ND 0.10 09/23/16 02:02
LABORATORY CONTROL SAMPLE: 1711793
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Formaldehyde ug/L 200 123 61-4 39-153
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1712603 1712604
MS MSD
92312830001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Conc, Result Result % Rec % Rec Limits RPD Qual
Formaldehyde ug/L 140 200 200 251 221 55.7 40.5 39-153 12.8
Results presented on this page are In the units indicated by the "rinits" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 1010312016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 24

aceAnalytical
www.pecdabs.com
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No,: 92312830
QC Balch: 331194 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92312830001, 92312830002, 92312830003
SAMPLE DUPLICATE: 1834993
92312947001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 5.8 5.8 0 H6
SAMPLE DUPLICATE: 1834994
92313414001 Dup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 6.6 6.7 1 H6
Pace Analytical Services, Inc.
8701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented an this page are in the units indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10103/2016 04:52 PM without the written consent of Pace Analytical Services, Inc,.
Page 12 of 24

aceAnalyllcal
www,pscelabsmm
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
OC Batch: 330300 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: 350.1 Ammonia, Low Level
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1830085 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.010 09/26/16 18:25
PaceAnalytital Services, Inc.
Vol Conference Drive
Raleigh, NC 27607
1919)834-4984
LABORATORY CONTROL SAMPLE: 1830086
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg1L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1830087 1830088
MS MSD
92312729001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quat
Nitrogen, Ammonia mg1L 0.014 1 1 1.0 1.0 98 98 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1830089 1830090
MS MSD
92312729002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mglL 0,014 1 1 1.0 1.0 99 98 90-110 1
Results presented on this page are In the units and;cased by the "Units" corumn except where an alternate unit Is presented to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
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Date: 1010312016 D4:52 PM without the written consent of Pace Analytical Services, lnc..
Page 13 of 24

laceAnalytical"
wwwpecelat* com
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
QC Batch; 330231 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92$12830001, 92312830002, 92312830003
METHOD BLANK: 1829768 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Nitrogen, Kjeldah[, Total
mg/L
NO 0,50 09127/16 23:19
LABORATORY CONTROL SAMPI.C:
1829769
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/L
10
9.0 90 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1829770 1829771
MS MSD
92313310001 Spike Spike MS MSD MS MSD % Roc
Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 2,4 10 10 12.2 10 98 76 90-110 20 M1,R1
Results presented on this page are In the units Indicated by the'llnils" column except where an alternate unh is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1010312016 04:52 PM without the written consent of Pace Analytical Services, Inc„
Page 14 of 24

15ceAna1j&a1'v
wwpacafabs.com
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No_= 92312830
QC Batch: 331176 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1834910 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0.020 09/30/16 17:03
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1834911
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2A 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1834912 1834913
MS MSD
92313547001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L NO 2.5 2.5 2.5 2.5 101 102 75-125 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1834914 1834915
MS MSD
92313547002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg1L 0.021 2.5 2.5 2.5 2.5 100 98 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the tight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc„
Page 15 of 24

(�..5a'cie Analytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
OC Batch: 329936 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1828215 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mglL ND 0.050 09/23/16 04:05
Race Analytical Services, Inc-
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1628216
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg1L 2.5 2.4 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1828217 1828218
MS MSD
92313012001 Spike Spike MS MSD MS MSD °1° Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Phosphorus rtiglL ND 2.5 2.5 2.5 2.5 97 97 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1828219 1828220
MS MSD
92312729010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quai
Phosphorus mglL 3.1 2.5 2.5 5.7 5.9 103 111 90-110 4 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 24

aceAnalytical
www.pacelaAacom
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
Pace Analytical Services, Inc.
5701 Conference Drive
Raleigh, NC 27607
[phone]
QC Batch: 331472 Analysis Method: EPA 420.4
QC Batch Method: EPA 420A Analysis Description: 420.4
Phenolics
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1836474 Matrix: Water
Associated Lab Samples: 92312830001, 92312830002, 92312830003
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Phenol mglL ND 0.010
10103/1613:37
LABORATORY CONTROL SAMPLE: 1836475
Spike LCS
LCS % Rec
Parameter Units Conc. Result
% Rec Limits
Qualifiers
Phenol mg1L ,05 0.052
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1836476 1836477
MS MSD
92312700004 Spike Spike MS
MSD MS
MSD
% Rec
Parameter Units -- Result Conc. Conc. Result
Result % Rec
% Rec
Limits
RPD Qua]
Phenol mg1L 0.020 .05 .05 0.15
0.14 257
230
90-110
9 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1836478 1836479
MS MSD
92312830001 Spike Spike MS
MSD MS
MSD
% Rec
Parameter Emits Result Conc. Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Phenol mg1L 0,038 .05 .05 0.076
0.076 74
75
90-110
1 M1
0
Results presented on this page are In the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 24

a ce Analytical
wwwpace1ab =n
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No-: 92312830
OC Batch: 329943 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92312830001, 92312830002, 92312830003
METHOD BLANK: 1828247 Matrix; Water
Associated Lab Samples: 9231283000i, g2312830002, 92312830003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 09/23/16 21:55
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh. NC Z7607
(919)B34-4984
LABORATORY CONTROL SAMPLE: 1828248
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mgtL 750 745 99 90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 1828249 1828250
MS MSD
'32312258006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L ND 750 750 639 839 112 112 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1828251 1828252
MS MSD
92312589001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 2310 750 750 2390 2410 10 13 90-110 1 Mt
Results presented an this page are In the units indicated by the "Units' column except where an altemale unit is presented to the right of the recall.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM wilhotlt the written consent of Pace Analytical Services, Inc..
Page 18 of 24

aceAnalytical
www.pacefafu.com
QUALIFIERS
Project: STORMWATER SAMPLING
Pace Project No.: 92312830
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantilation Limit-
RL - Reporting Limit.
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anaiyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values-
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable -
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nilresodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyle is a combined concentration.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PAST-E Pace Analytical Services - Eden
PASI.O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
B1 Less than 1.0 mg11- DO remained for all dilutions set. The reported value is an estimated greater than value and is
calculated for the dilution using the least amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time,
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/03/2016 04:52 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 24

aceAnalytical
wwwpacelaba.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project' STORMWATER SAMPLING
Pace Project No.: 92312830
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92312830001
00291916
SM 2540D
329568
92312830002
00391916
SM 2540D
329568
92312830003
00491916
SM 2540D
329568
92312830001
00291916
SM 5210B
329610
SM 5210B
329634
92312830002
00391916
SM 5210B
329406
SM 5240B
329563
92312830003
00491916
SM 52108
329406
SM 5210B
329563
92312830001
D0291916
EPA1664B
330004
92312830002
00391916
EPA16648
330004
92312830003
00491916
EPA1664B
330004
92312830001
00291916
EPA 8315
321682
EPA 8315
322170
92312830002
00391916
EPA 8315
321682
EPA 8315
322170
92312830003
00491916
EPA 8315
321682
EPA 8315
322170
92312830001
00291916
EPA 9040
331194
92312830002
00391916
EPA 9040
331194
92312830003
00491916
EPA 9040
331194
92312830001
00291916
EPA 350.1
330300
92312830002
00391916
EPA 350.1
330300
92312830003
00491916
EPA 350.1
330300
92312830001
00291916
EPA 351.2
330231
92312830002
00391916
EPA 351.2
330231
92312830003
00491916
EPA 351.2
330231
92312830001
00291916
EPA 353.2
331176
92312830002
00391916
EPA 353.2
331176
92312830003
00491916
EPA 353.2
331176
92312830001
00291916
EPA 365.1
329936
92312830002
00391916
EPA 365.1
329936
92312830003
004S1916
EPA 365.1
329936
92312830001
00291916
EPA 420.4
331472
92312830002
00391916
EPA 420.4
331472
92312830003
00491916
EPA 420.4
331472
92312830001
00291916
SM 5220D
329943
92312830002
00391916
SM 5220D
329943
92312830003
00491916
SM 5220D
329943
Date: 10/03/2016 04:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrilten consent of Pace Analytical Services, Inc..
Page 20 of 24

ff Jocument Revised: May 24, 2016
Sample Condition Upon Receipt(SCUR) I Page 1 of 2
i'dC[?Al]dl lCal Document No.; Issuing Authority:
F•RAL-CS-001-Rev.04 I Pace Raleigh Quality Office
;t4;Saili{ife;tondt`idri {pori j 0
"- r FiCCCiptE::i;a :,'.Gre:Proje
y`
❑fed Ex
❑UPS ❑U5P5]Client
HCourier.
❑ Commercial
[-]Pace
❑other:
92312830
Custody Seal Present?
[]Yes ONO
Seats intact? []Yes Z]No
Packing Material:
❑Bubble Wrap
❑Bubble Bags ONcre ❑Other
Date/Irt[tials Person Txamfnln6 Cantnnn:D,�"t
Thermometer:
T1505
Type or I )nwet ❑slue
Nape EP e ❑ ❑Samples on ice, Coolln process has begun
Correction Factor 0.O'C
Cooler Temp Corrected (•C):
Biological Tissue Frozen? ❑Yes ONO 7N/A
Temp should be above( ezing to 6T
USDA Regulated Soll ( FN/A,
+eater sample}
Didsample originate Ina quarantine Lone within the United States: CA, NY, or SC (check maps)?
nYes Na
Did samples originate from a foreign worts tintemptlonaliy,
iorludinrt liawail and Puerto Ricol? nYes u
Comments/Olscrepa ncy:
Chain of Custody Present?
Yes
❑No
[]N/A
1.
Samples Arrived within Hold Tlme?
Yes
❑"
❑N/A
2.
Short Bold Time Analysfs (<72 hr.)? _
Yes
❑No
❑NJA
3. V
Rusts Turn Around Time Requested?
Elves
No
❑N/A
4.
Sufftclent Volume?
Oyes
❑Na
N/A
S.
Correct Containers Used?
Yes
❑no
❑NIA
6.
-Pace Containers Used?
j es
❑No
❑NJA
Containers lntact?
Yes
❑No
[]N/A
7.
Samples Field Filtered?
[-]Yes
❑No
N/A
8. Note if sedimentls visible In the dissolved container
Sample Labels Match COO
]Yes
[:]No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
All containers needing add/base preservation have been
_
10,
checked?
(es
❑nrra
❑NJA
All containers needing preservation aro found to be in
f/
WJowl
compliance with EPA reeommerdatfcn?
(HNOs, HzSO., HCI<2; HaOH >9 Sulfide, NaOHa12 Cyanide)
I Yes
❑No
❑N/A
e xceptions: VOA, Collform, TOC, OII and Grease,
DRD/8015 (water) DOC,LLH
Yes
ONo
❑N/A
Wi*4/LN°A"IA
Samples checked for dechlorination?
Yes
E]No
❑N/A
11.
Heads ace In VOA Vials >5-6mm)7
" Yes
Nn
/A
12.
Trip Blank Present?
©Yes
[]No
N/A
13.
Trip blank Custody Seals Present?
❑Yes
ONO
N/A
Pace Trip Blank Lot H (If urchased):
CLIENT NDTIFICATiON/RESOLUTION Field Data Required? QYes [:]NO
Person Contacted: Date/Time:
Comments/Sample
Dlscrepancy:
Project Mlanager SCURF Review: R f 1 2) l� Date:
Pro}ect Manager SRF Review: _ _ I l r � 9 �O Date: ! —1
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will to sent to the North Carelina DEHNR Certiflcatlor Offlce (i.e.
Out of hold, Incorrect preservattve, out of temp, incorrect containers)
Page 21 of 24

CHAIN -OF -CUSTODY !Analytical Request Document
The Ctsai "f-Cuswdy Is a LEGAL DOCUMENT. AN relevant fields must he completed accurately.
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chainroi•CLsiody Is a LEGAL DOCUMENT. All relovarst fields must be compieled accurately.
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` aceAnalytrcal
wwwpacefaba.mm
June 03, 2016
David Lorbacher
Arclin-DynealMoncure
790 Corinth Road
Chapel Hill, NC 27599
RE: Project: Semi -Annual Stormwater
Pace Project No.: 92298178
Pace ArtalyCCal Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
CS d6��'a
RECEIVED
JUN Z 3 2016
CENTRAL FILES
DWR SECTION
Dear David Lorbacher:
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2016. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Liamm Harrison
[e-mail]
Project Manager
Enclosures
cc: Bowman Harvey, Acrlin-DynealMoncure
Chis Lamm, Arclin-Dynea/Morcure
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
x ww.pecefabs.mm
CERTIFICATIONS
Project Semi -Annual Stormwater
Pace Project No.: 92298178
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
019)834-4984
Ashovillo Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
rlorida/NELAP Certification #; E87648
South Carolina Certification #: 99D30001
Massachusetts Certification #: M-NC030
VirginialVELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
Edon Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738
Virginia[VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
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aceAnaIXical
www.pacejahs.oam
i
SAMPLE ANALYTE COUNT
Project: Semi -Annual Slormwaier
Pace Project No.: 92298178
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Roported
Laboratory
92298178001
002051716
SM 2540D
MSH
1
PASI-A
EPA 9040
TEP
1
PASI-A
EPA 350.1
AES2
1
PASI-A
EPA 351,2
SRJ
1
PASI-A
EPA 353.2
DMN
1
PASI-A
EPA 365.1
WRC
1
PASI-A
EPA420A
DMN
1
f ASI-A
SM 5220D
WRC
1
PASI-A
92298178002
00351716
SM 52108
DWJ
1
PASI-E
SM 2540D
MSH
1
PASI-A
EPA 9040
TEP
1
PASI-A
EPA 350.1
AES2
1
PASI-A
EPA 351.2
BRJ
1
PASI-A
EPA 353.2
DMN
1
PASI-A
EPA 365.1
WRC
1
PASI-A
EPA 420.4
DMN
1
PASI-A
SM 52200
WRC
1
PASI-A
92298178003
00451716
SM 2540D
MSH
1
PASI-A
EPA 9040
TEP
1
PASI-A
EPA 350.1
AES2
1
PASI-A
EPA 351.2
BRJ
1
PASi-A
EPA 353.2
DMN
1
PASI-A
EPA 365.1
WRC
1
PASi-A
EPA 420.4
DMN
1
PASI-A
SM 5220D
WRC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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(�IaceAnalytical"
"W-MCelsb&OM
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
Sample: 002051716
Lab ID: 92298178001 Collected:
05/17/16 15:15
Received: 05/18/16 12:30 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
36.0 mglL
10.0
1
05/20/16 17:27
9040 pH
Analytical Method: EPA 9040
pH
6.2 Std. Units
0.10
1
05/24/16 12-40
H6
350.1 Ammonia, Low Level
Analytical Method: EPA 350.1
Nitrogen, Ammonia
4.0 mg1L
0.050
5
05/21/16 16:15
7664-41-7
351.2 Total Kjoldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl. Total
403 mg1L
12.5
25
05128116 03:01
7727-37-9
353.2 Nitrogen, N021NO3 Ares.
Analytical Method: EPA 353,2
Nitrogen, NO2 plus NO3
5.0 mglL
0.040
2
05127/16 17:28
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
0.12 m91L
0.050
1
05/3111615:54
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA 420A
Phenol
1.0 mg1L
0.20
20
05/24116 22:15
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
606 mg1L
25.0
1
06/01116 18:30
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02,42 PM without the written consent of Pace Analytical Services, Inc,. Page 4 of 39

aceAnalytical`
wwwpecelsb3 mm
ANALYTICAL RESULTS
Pace Analytical Services, Inc_
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
Sample: 00351716
Lab ID: 92298178002 Collected: 05/17/16 15:15
Received: 0511B116 12:30 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Quaff
52108 BOO, 5 day EDN
Analytical Method: SM 5210B
600, 5 day
23.6 mg1L
2.0
1
05/19/16 15:13 05124/16 09:13
2640D Total Suspended Solids
Anaiytical Method: SM 2540D
Total Suspended Solids
ND mg1L
8 3
1
05/20/16 17:27
9040 pH
Analytical Method: EPA9040
pH
6.8 S1d, Units
0,10
1
05/24/16 12:40
H6
360.1 Ammonia, Low Level
Analytical Method: EPA 350.1
Nitrogen, Ammonia
2.5 mg1L
0 050
5
05121116 16 19
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
5.7 mg1L
0,50
1
05/28/16 02:44
7727-37-9
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
5.3 mglL
0.040
2
05/27/16 17:30
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
0,059 mgfL
0.050
1
05131/1616:00
7723.14-0
420.4 Phenolics, Total
Analytical Melhod: EPA 420.4
Phenol
0.15 mglL
0,020
2
05124/16 22:07
5220D COD
Analytical Method; SM 5220D
Chemical Oxygen Demand
42.0 mglL
25.0
1
06/01/16 18:30
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.pecelabs.cnm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Semi -Annual Stormwater
Pace Project No. 92298178
Sample: 00451716
Lab ID: 92298178003 Collected: 05/17/16 15:15
Received: 06118/16 12:30 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
19.0 mg1L
5.0
1
05120/16 17:27
D6
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units
0,10
1
05/24/16 12:40
H6
350.1 Ammonia, Low Level
Analytical Method: EPA 350.1
Nitrogen. Ammonia
0.54 mg1L
0.010
1
05/21/16 16:07
7664-41-7
351.2 Total Kjoldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
14.2 mg1L
0,50
1
05/28/16 02:45
7727-37.9
353.2 Nitrogen, NO2IN03 prey.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
9.7 M91L
0,080
4
05127116 17.31
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
0.60 mglL
0.050
1
05131/1616:01
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
0.012 mg1L
0.010
1
05/24116 21:55
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
83.0 mglL
25.0
1
06/01/16 18:30
M1
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc,. Page 6 of 39

aceAnalytical";
wwwpacefabs.cam
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919 }834-49B4
QUALITY CONTROL DATA
Project: Semt•Annual Stormwater
Pace Project No.: 92298178
OC Batch: EDEN122874 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day EDN
Associated Lab Samples: 92298178002
METHOD BLANK: 1737901
Associated Lab Samples: 92298178002
Parameter Units
BOD, 5 day mglL
LABORATORY CONTROL SAMPLE: 1737902
Parameter Units
BOD, 5 day mg/L
SAMPLE DUPLICATE: 1737903
Parameter Units
BOD, 5 day mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 05/24/16 09:13
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 205 104 84.6-115.4
92298245002 Dup
Result Result RPD Qualifiers
198 194 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presonted to the right of the result
REPORTOF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 39

aceanapieal
www.pacafabs.com
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WET145073 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK: 1739401 Matrix: Water
Associated Lab Samples: 92298178001 , 92298178002, 92298178003
Blank Repoi ling
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/20/16 17:25
LABORATORY CONTROL SAMPLE: 1739402
Spike LCS
Parameter Units Conc. Result
Total Suspended Solids mg/L 250 248
SAMPLE DUPLICATE: 17$9403
92298251001 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 228 224
SAMPLE DUPLICATE: 1739404
92298178003 Oup
Parameter Units Result Result
Total Suspended Solids mg/L 19.0 14.2
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, HC 27607
1919j834-4984
LCS % Rec
% Rec Limits Qualifiers
99 90-110
RPD Qualifiers
2
RPD Qualifiers
29 D6
Resells presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 39

aceAnalytica!
wwwpecelaba=n
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WET145067 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92298178001, 92298178002, 92298178003
SAMPLE DUPLICATE: 1738993
92298178001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 62 6.2 0 H6
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 276D7
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 39

aceAnalyfical.
wwwptrcuioba.com
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WETA127711 Analysis Method? EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: 350.1 Ammonia, Low Level
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK: 1739612 Matrix: Water
Associated Lab Samples: 92298178001, 92298178002, 92298178003
Blank Repotting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.010 05/21/16 15:32
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, hIC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1739613
Spike LCS LCS °h Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen. Ammonia mg/L 1 1.0 100 90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739614 1739515
MS MSD
92297039001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits I Qual
Nitrogen, Ammonia mgJL 3.9 1 1 8.9 8.9 500 498 90-110 0
Results presented on this page are in the units Indicated by the'Units" column except where an alternate unit is presenter[ to the right of the resun.
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pane Analytical Services, Inc.,
Page 10 of 39

aceAnalytical
www pacelaas.mm
QUALITY CONTROL DATA
Projecl. Semi -Annual Stormwater
Pace Project No.. 92298178
QC Batch: WETA127732 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK: 1741458 Matrix: Water
Associated Lab Samples: 92298178001, 92298178002, 92298178003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L ND 0.50 05128/16 02:37
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE' 1741459
Spike LCS LCS % Rec
Parameter units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kje$dahl, Total mg/L 10 9.9 99 90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1741460 1741461
MS MSD
92298170001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 5.0 10 10 13.2 1IT2 81 121 90-110 26 M1,R1
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date; 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc,.
Pagel 1 of 39

aceAnalytical.
www.pacalsta.com
QUALITY CONTROL DATA
Project Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch; WETA127768 Analysts Method: EPA 353.2
OC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK; 1743775 Matrix: Water
Associated Lab Samples: 92298178001, 92298178002. 92298178003
Blank Reporting
Parameter Units Result Limit Analyzers Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0,020 05/27/16 16:50
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1743776
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 97 ` 90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1743777 1743778
MS MSD
92297842002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Roc Limits RPD Qual
Nitrogen, NO2 plus NO3 mgfL 0.38 2.5 2.5 2.7 2.7 94 94 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1743779 1743780
MS MSD
92298871002 Spike Spike MS MSD MS MSD % Roe
Parameter Units Result Conc, Cone. Result Result % Rec °% Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg1L ND 2.5 2.5 2.2 2.2 89 89 75-125 0
Results presented on this page are in the units indicated by the "Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 39

aceAnalyfical "
wwwpacelab3.corn
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WETA/27765 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92298178001
METHOD BLANK: 1743645 Matrix: Water
Associated Lab Samples: 92298178001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mglL ND 0,050 05/3111615:33
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-49a4
LABORATORY CONTROL SAMPLE: 1743646
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phosphorus mg1L 2-5 2.6 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICA1 E: 1743647 1743648
MS MSD
92297930001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPO Qual
Phosphorus mgiL 4 3 2.5 2.5 7.4 7.3 124 122 90-110 1 Mi
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1743649 1743650
MS MSD
92298038006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg1L 3.8 2.5 2.5 6.3 6.3 103 102 90-110 0
Results presented on this page are in the units Indicated by the "Unil5" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06103/2016 02:42 PM without the written consent of Pace Arelytical Services, Inc,.
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aceAnalytical "
www.pacalabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, 127607
[phone]
Project:
Semi -Annual Stormwater
Pace Project 1
92298178
QC Batch:
WETAl27766 Analysis Method: EPA 365.1
QC Batch Method:
EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92298178002, 92298178003
METHOD BLANK: 1743651 Matrix: Water
Associated Lab Samples: 92298178002,92298178003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg1L N❑ 1 05131/1615:55
LABORATORY CONTROL SAMPLE: 1743652
Spike LCS LC5 % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg1L 2.5 2.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 17431 1743654
MS MSD
92298179001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 1.9 2.5 2,5 4.3 4.3 99 98 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1743655 1743656
MS MSD
92298756001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 16.6 2.5 2.5 19.8 20.0 126 135 90-110 1 M6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06103/2016 02:42 PM without the written consent of pace Analytical Services. Inc..
Page 14 of 39

aceAnalytical`
www'Pacelaba.com
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WETA127719 Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK: 1740398 Matrix: Water
Associated Lab Samples: 922981781)01. 92298178002. 92298178003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg1L ND 0.010 05/24/16 21:55
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1740399
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phenol mgfL .05 0.054 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1740400 1740401
MS MSD
92298132001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Quat
Phenol mglL NO ,05 .05 0.047 0.056 80 98 90-110 17 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1740402 1740403
MS MSD
92298132002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPU Qual
Phenol mglL 0.016 .05 .05 0.060 0.056 89 80 90-110 8 M1
Results presented on this page are in the units Indicated by the'Unrts" column except where an alternate unit is presented to the right of the resuh,
REPORT OF LABORATORY ANALYSIS
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Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 39

aceAnalytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
QC Batch: WETAI27776 Analysis Method: SM 52200
QC Batch Method: SM 5220D Analysis Description: 52200 COD
Associated Lab Samples: 92298178001, 92298178002, 92298178003
METHOD BLANK: 1744792 Matrix: Water
Associated Lab Samples: 92298178001, 92298178002, 92298178003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 06/01/16 18:30
Pace Analytical Services, Inc-
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1744793
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 738 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1744794 1744795
MS MSD
92298871001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result °/a Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 272 3000 3000 2970 2970 90 90 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1744796 1744797
MS MSD
92298178003 Spike Spike MS MSD MS MSO % Rec
Parameter Units Result Cane, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 83.0 750 750 746 746 88 88 90-110 0 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/03/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 39

lacmna,(Xical"
www.powlabs.com
QUALIFIERS
Project, Semi -Annual Stormwater
Pace Project No.: 92298178
DEFINITIONS
Paco Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Ouantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each anaiyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anaiyte is a combined concentration,
LABORATORIES
PASI-A Pace Anatytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 the precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M5 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06103/2016 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 39

ace Analytical
"W pambbs.swn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Semi -Annual Stormwater
Pace Project No.: 92298178
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92298178002
00351716
SM 5210B
EDEN/22874 SM 5210B EDEN/22884
92298178001
002051716
SM 25401D
WET/45073
92298178002
00351716
SM 2540D
WET/45073
92298178003
00461716
SM 2540D
WET/45073
92298178001
002051716
EPA 9040
WET145067
92298178002
00361716
EPA 9040
WET145067
92298178003
00451716
EPA 9040
WET/45067
92298178001
002061716
EPA 350.1
WETA/27711
92298178002
00351716
EPA 350.1
WETA/27711
92298178003
00461716
EPA 350.1
WETA/27711
92298178001
002051716
EPA 351.2
WETA/27732
92298178002
00351716
EPA 351.2
WETA/27732
92298178003
00451716
EPA 351.2
WETA127732
92298178001
002051716
EPA 353.2
WETA/27768
92298178002
003SI716
EPA 353.2
WETA/27768
92298178003
00451716
EPA 353.2
WETA/27768
92298178001
002061716
EPA 365.1
WETA/27765
92298178002
00351716
EPA 365.1
WETA/27766
92298178003
004517116
EPA 365.1
WETA127766
92298178001
002051716
EPA 420.4
WETA/27719
92298178002
00361716
EPA 420.4
WETA127719
92298178003
00451716
EPA 420.4
WETN27719
92298178001
002051716
SM 5220D
WETA/27776
92298178002
00351716
SM 5220D
WETA/27776
92298178003
00451716
SM 5220D
WETA/27776
Date: 06/03/2016 02:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 18 of 39

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Page 20 of 39

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Ridi 22 bf'39 -

ANALY-FICAI_ ENVIRONMENTAL SERVICES, INC.
AES
May 23, 2016
Liamin Harrison
face Analytical Services, Inc.
9800 Kincev Avenue. Suite 100
Fluntersville NC 28078
TEL: [phone]
FAX: [phone]
RE: 92298178
Dear Liamm Harrison: Order No: 1605F12
Analytical Environmental Services, Inc. received 3 samples on 5/19/2016 10:20:00 AM
for the analyses presented in following repoil.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project. Case Narrative. AES' certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/15-06/30/16.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent,
effective until 12131/15.
-South Carolina Environmental Laboratory Certification number 98016003 effective until
6/3 0/ 16. Y
These results relate only to the items tested. This report may only he reproduced in full and with
written permission from the laboratory.
li'you have any questions regarding these test results, please feel tree to call.
Sincerely,
zf "
WA h-,
Tura Westervelt
Project Manager
3080 Presidential Drive • Atlanta, Georgia 30340 - TA 770.457.81 77 • 1'ax.. 77o,467.8188 • Toll Frue: 800.972.4889
www•_-4.Llmt,0.com Page 23 of 39
1 of 8

1 (,00S F1 Z
, ,�ceAnalytical
_ w+lm.pacesao�cx.�
4i'orkorder: 92298178 Semi -Annual Stormwater qvof.ed By: 612/2016
• Qn & 1 i mien T
Liamm Harrison
P2ceAnalytical Charlotte
P.0.
9800 Kincey Ave. Suite 100
!-fun.erse;lle. `C 28078
Phone [phone]
Email: Eamm.harriso n acala com
@P bs.
i
I State of SGmpie Origin: NC
Preserved Ca- :r:nv.;
r,•
`
ff
i
f Cai:ec:
�
,.>1
�
jte^i Sample ID
f ^rre i+s,- Lab ]C Matrif
� 1 i
: y r �
f LF S USE CN'L �
01 D020$1716 1 5r 7126 i 5:15 92298178001 rla:er
1 _
-
.t E
�X
f 2
0035171E
W,712D.615--15
92298:78002
(+dater
)(,
t6'
JSi,7/20i51515
I92228178002
'later
I
f ! X
•
1
I
� Co:nrnerts
Transfers
Released By
loaterrime
Received By
Gad
[[Daterriime
f
�
12
i
'
t
CoolerTemperature on Receipt
°C E Custody Seal Y or N
_ Received on Ice Y or N _Samples Intact Y or N i
r,Wednesdav, May 1S. 2016 5:08:0° ?6.11
CO
w
FMT-ALL-C-002rev.00 24P.4arch2009 :ace ; ;
2of8

Analytical Environmental Services, Inc
DRIC. 23-May-16
Client:
Paco Analytical Services, Inc.
Client Sample ID:
002051716
Project Name-
92298178
Collection Date:
5/1712016 3: E 5:00 I'M
I,ah 11):
16051'12-001
illatrix:
Aqueous
Iteportin�
Analyses Kcsutt Oual Units E3atchli) IlilI)ntct1nB[yzcd Anal).ct
Limit Iutiun -aotur
Carbonyl Compounds by II1'I,C SNV8315A
Formaldehyde 62000 .5(ii)p ag/L 224213 tll 05/20/201612,35 RF
Q1.01irlen; ' %aluu e><ceces nlasimum crmtammam level
BR), Below reporting limit
II IIvIdir¢g limes far 1—pxmtion ur analysis excevaled
N Analvte not NELAC. certified
B Analyle detected in the assodmed mcihod bleat.
> Greater thnu Resuh value
3of8
E Estirnacrd(-4w above tllulmitatum tAriycl
S Spike Recovery outside limits due to matrix
Nero See case narmtivc
NC Not confirmed
< Less than Result value
1 Estimated value detected below Rep-n.% Lirnit
Page 25 of 39

Analytical Environmental Services, Inc
Da1C: 23-Mav-16
Client:
Pace Analytical Services, Inc.
Client Sample 11):
00351716
Project Name:
92298178
Cullec.lion Date:
5/17/2016 3:15:00 1'M
Lab 11);
16051-'12-002
Matrix:
Aqueous
Analyses Result Reporting Dilution
Qual Units Ratcbll) Date r\nahweJ Anah-sl
Limit Factor
Carbonyl Compounds by 111'1,C SW8315A
1 ornmldehydc 140
Qunliliers. • Valle exceeds maxinunn contamir+ant level
HRL 13clow reposing limit
11 I fnl di rig limes for prepaeaI iun or analysis exceeded
N Annlvte not NGLAC cenified
H Anolyte dewae d in the associated method hLmk
> (ire: w than Result value
4 of 8
50 uglt. 224213 1 05l2012011; 11:40 R1,
E lisefmalcd (value ahove quaaeitm ion rung')
S Spike Recovery outside limits due to mami
Narr See eJSe narrative
NC Not confirmed
< Less than Result vat lie
i Estimated value detected bdnw Reporting Limit
Page 26 of 39

Analytical Environmental Services, Inc
MAC: 23-May- 16
Client:
Pace Anal}'tical Services, Inc.
Clique Sample III:
00451716
Project Name:
92298179
Collection Date:
5/17/2016 3:15:00I'M
hate 11):
10051-12-UO3
Malris:
Aqueous
Reporting; Dilution
:lnalyties RCxull QuilliJnils 13;itctlll? Ualc,tnaf)'zc•d allaksl
Lintit Factor
Carbonyl Compounds by I-IPLC SN3'831SA
i'ornlaldehyde RRL 5o ttsn- 224213 1 05/201201611:55 RF
Ipuxlifirrs: ' Value exceeds macimum contaminant level
HRL Below reporting limit
11 nnlding times fir preparation or analysis exceeded
N Analvte not Nk•LAL: certified
It Analyze delected in the associated mrthod hlank
a Greater than Result value
5 of 8
E Fstimated (value above quorttitativa mnge)
5 Spike Racovery outside limits due m rnairm
Nan See case "Mtiw
NC Not w.furncd
< LesslhanResultvalm
1 listienated value detw,d below Rcpwung Limit
Page 27 of 39

y
A11.11)IiC.11 I'AlVil'l)11111011(ill SCI'viCCS, 'I'llC.
Sslmple/Cooler Receipt C:hculd'Ist
Clicni _ /l/'v'� T/// Y%� Work Oi-der Number2—
Checklist completed by _PO4,j A.Dt9'tei��d%
5il;ilaltirc )�+le
Carrier n:amc: l edFr i il'S/_ Courier Client LIS Mail _ Offier
Shipping conlainer/conit:r in good conditio:i? Yes �No _ Not l're'scltt _
Custody seats intact oil shipping; contahiericooler? YCs — No tint Present
Custody seal~ himet On swilple botlics? Yes — No Not Prescut
t
ConlainerOemp l)lank tcmpmature incompliaucc? {(r:56'C')*Yes _ No
a
Cooler 111 Y f Cooler 112 Cooler 113 C onler 11'I Cooler115 Cooler /10
chain of custody prescnl? Yes = '10 _
Chain of custody Signed when relinquished and received? Yes No
Chain of euslody agrees willl sample labels? l Yes No
Samples in proper co►itaincrfboUle? Yes ✓ No
SamplC container, intact?
Liil'licicrlt Sample voltunc tisr iit�ficakci :esl`?
All samples received within holding.; lime?
Was TAT marked oil the COC?
YCs V No
Ycs _V�" No
Yes V Nn
Yes t/ No
Proceed with SUmdard TAT as per project history? Yes _ No _
Dater- VOA vidl, have zero hendspacc? No VOA viah, submitted Yes _
WalCr - pl l UCCP1.1131C U[MI PCCeij)l? Yes V No ,
Adjusted? Checked by
Sample O111dilion; Good ()tlter(t xpl.11n}
(F(y• difi''usive samples or All'lA lend) Is a known blank included? Yes
See Case Mirmilve for resolution of (tie Nato-Coulbi-IMURM
Not Applicable../
No _
Not Applicable_
V _
No t/
' samples do not hove m comply Wilh the given range fag certain pasamcirts.
i
11Acs_seivcrlllSamrrlc Reeeipt\Nly I UCLI111e'S and pi i Adjustment ShecilSample_Coolcr�Rccillt Chceklist_Rcvl,rlt
m
t'.
6of8
Page 28 of 39

Analytical Environmental Services, Inc
Date: 23-May-16
Client: Pace Analytical Services, Inc.
Project Name: 92298178 Dates Report
Lab Order: 16051712
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name TCLP Date
Prep Date
Analysis Date
1605F12-001A
002051716
5/17/2016 3:15:OOPM
Aqueous
Carbonyl Compounds by HPLC SW8315
5/19/2016 1:00:08 PM
0512012016
1605F12-002A
00351716
5/17/2016 3:15:OOPM
Aqueous
Carbonyl Compounds by HPLC SW8315
5/19/2016 1:00:08 PM
0512012016
1605F12-003A
00451716
5/17/2016 3,15:OOPM
Aqueous
Carbonyl Compounds by HPLC SW8315
5/19/2016 1:00:08 PM
05/20/2016
Page 29 of 39
7 of 8

Analytical Environmental Services, Inc
Client: Pace Analytical Services. Inc.
Project Name: 92298178
workorder: 1605F12
Date: 23-May-16
ANALYTICAL QC SUMMARY REPORT
13atchID: 224213
Sample ID: SI13-224213
Client 10:
Units: ug1L
Prep Date: 05/19/2016
Run No: 317238
SampleType: -NIBLK
'I'esiCode: Cnrbonvl Compounds by 11PLC SW8315A
BatchlD: 224213
Analvsis Date: 0S12012016
Seq No: 6834222
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
I ligh limit RPD Ref Val %RPD
RPD Limit Qua]
Formaldchvde BRL 50
Sample 1D: 1,CS-224213
Client ID:
Units: ugll,
Prep Date: 0511912016
Run No: 317238
SampleType: LCS
TestCode: Carbonyl Compounds by HPLC sw83115A
BatchlD: 224213
Analysis Date: 0.512012016
Seq No: 6834223
Analvte
Result RP'I' Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Fonnaldehvde 954.4 50 1000 95.4 70 130
Sample ID: 1605F12-003AMS
Client ID:
00451716
Units: uglL
Prep Date: 05/19/2016
Run No: 317238
Sample'lvpc: MS
TestCode:
Carbonyl Compounds by HP1.0 SR'8315A
Batch]D: 224213
Analysis Date: OS/20/2016
Seq No: 6834726
Analyze
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
I ligh Limit RPD Ref Val %RPD
RPD Limit Qua[
Fonnaldehvde 990.6 50 1000 34.62 95.6 44.7 135
Sample ID: 1605F12-003AMSD
Client fD:
00451716
Units: uglL
Prep Date: 05/19/2016
Run No: 317238
SampleType: �ISD
TCSiCode:
Carbonyl Compounds by HPLC SNA1315A
Batch[D: 224213
Anal sis Date: 0512012016
Seq No: 6834727
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
f figh Limit RPD Ref Val %RPD
RPD Limit Qual
Fonnaldehvde 1081
Qualirw— > Greater thin Result value
BRL Below reporting limit
J Estimated Value detected below- Reponing Limit
Rpt Lim Reporting Limit
$ of 8
50 1000 34.62 105 44.7 135 990.6 8.71 27.3
a Less than Rmult value
E Estimated (Value above quantitation range)
A-1,1e not \FLAC eenified
S Spike Recovery outside limits due to matrix
B Amlyie detected in the associated method blank
It Holding times for preparation or analysis ecceeded
R RPD outside limits due to matrix
Page 30 of 39

Custody
W(-rkorder: 92298178 Workorder Name: Semi -Annual Stormwater Results Requested By: 6/2/2016
1
a
j r4' aceAnaf ical
- �. u6amrn
i Reperi I invoice To .'.' `
Subcontract Tc
Requested Analysis
Liamm Harrison
Pace Analytical Charlotte t)kCc,�, P.O.
U�
1
I"
9800 i incey Ave. Suite 100
Z
i
E Huntersville, NC 28078
Phone [phone]
�j-Gj t��-���� C�
i
I
1
Email: [e-mail]
{
i State of, Sample Origin: NC
preserved Containers.
i
Collect
=
m
Item
Sample ID - `
Datefiime
Lab [D
Matrix
LAB USE
ONLY
i
1
002051715
5/171201615:15
92298178001
Water
I x
1 2
00451716
5117/2016 15:15
92298178003
Water
X
3
4
5
''
-
Comments '.'-
Transfers
Released By
DatelTlme
Received By
DataMme
2
3
Cooler Tem erature on Receipt
°C Custody Seal Y or N
Received on Ice Y or N Samples Intact Y or NI
Thursday. May 19. 2016 2:04:16 PM FMT-ALL-C-002rev.00 24March2009 Pagel 1 of 1

Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville. NC 28078
Receive Date: 05/19/2016
Reported: 05/25/2016
For: 92298178
Comments: Bod's run out of hold time per client's request.
Sample Number Parameter Sample ID Result Unit Method
160519-22-01 BOD 001 145 mglL SM521OB-2001
160519-22-02 BOD 003 10 mg1L SM52106-2001
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Analyzed Analyst
05/1912016 MO
05/19/2016 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Pago 1 page 31 of 39

Condition of Receipt
Sample Number 160519-22-01 Temp on Arrival: 3
Parameter Schedule: BOD
Received on Ice
Sample Number 160519-22-02 Temp on Arrival: 3
Parameter Schedule: BOD
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page e gage 32 or 39

ACA
ct
"A d ENCO Laboratories
Acairate, Timely. Responsive. Innovative.
4820 Executive Park Court, suite 111
Jacksonville FL, 32216-6069
Phone: [phone] FAX: [phone]
Friday, June 3, 2016
Pace Analytical (PA007)
Attn: Liamm Harrison
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
RE: Laboratory Results for
Project Number: Semi -Annual Stormwater, Project Name/Desc: 92298178
ENCO Workorder(s): BZ02198
Dear Liamm Harrison,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, May 20, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville.
Data from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chris Tompkins
Project Manager
Enclosure(s)
Page 33 of 39
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7

(E-o
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
ClientiD: 002DS1716
Lab ID: BZO2199-01
Sampled: 05/17/16 15:15
Received: 05/20/16 11:00
Parameter
Hold Date/Time(s)
Prep Date/Time(s)
Analysis DatelTimefs)
EPA 166,iB
06/14/16
05/27/16
15:18 06/03/16 11.32
Client ID: 00351716
Lab ID: BZ02198-02
Sampled: 05/17/16 15:15
Received: 05/20/16 11:00
Parameter
Hold Date/Time(s)
Prep Date/Time(s)
Analysis DatelTime(s)
EPA 1664B
06/14/16
05/27/16
15:18 06/03/16 11:32
Client ID: OD451716
Lab ID: BZ02198-03
Sampled: 05/17/16 15:15
Received: 05/20/16 11:00
Parameter
Hold Date/Time(s)
Prep Date/Time(s)
Analysis a/Timefsl
EPA 16648
06/14/16
05/27/16
15:18 06/03/16 11:32
Page 34 of 39
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

QEruco
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 00451716 Lab IDt SZ02198.03
Analvte Results Ems MIX P9L Units Method Notes
Oil & Grease (HEM) 0.932 l 0.621 1.29 mg/L EPA 1664B
Page 35 of 39
r1NAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7

(N�0
www.encolabs.com
ANALYTICAL RESULTS
Description: 002051716' Lab Sample ID: BZ02198-01 Received: 05/20/16 11:00
Matrix: Water Sampled:05/17/16 15:15 Work Order: BZ02198
Project: 92298178 Sampled By:
Classical Chemistry Parameters
^ - ENCO Jacksonville certified analyze W 447]
Analyte FCAS Numberl Results Fag
Oil & Grease (HEM) [C-0007]^ 0.622 U
Description: 00351716
Matrix: Water
Project: 92298178
Classical Chemistry Parameters
^ - ENCOJacksonolle certified anaWe [NC 447]
Analyte ICAS Numberl Results Ba
Oil & Grease (HEM) [C-OW7]^ 0.614 U
Description: 00451716
Matrix: Water
Project: 92298178
Classical Chemistry Parameters
A - ENCO JacksonWJ1e cW ffed analyze [NC 4421
Analyte fCASNumberl Results fin
Oil & Grease (HEM) [C-0007]^ 0.932 }
Units DF MDL EQL B.,aLc,h
mg/L 0.259 0.622 1.30 6EZ7007
Lab Sample ID: BZ02198-02
Sam pled: 05/ 17/ 16 15:15
Sampled By:
Units PIE lwl!?6 EU Batch
rini 0.256 0.614 1.28 6E27007
Lab Sample ID: BZ02198-03
Sampled: 05/ 17/ 16 15:15
Sampled By:
Method Analyzed 1y Notes
EPA 1664B 06/03/16 11:32 SMA
Received: 05/20/ 16 11 M
Work Order: BZ02198
Method Analyzed &y Notes
EPA 1661B 06/03/16 1132 SMA
Received: 05/20/ 16 11:00
Work Order: BZ02198
VULU RE Md1 E" Batch Method Analvxed @s Notes
mg/L 0.259 0.621 1.29 6E27007 EPA 166413 06/03/16 11:32 SMA
Page 36 of 39
FINAL This report relates Orly to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7

9 �60
www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 6E27007 - EPA 1664E
Blank (6E27007-BLK1)
Prepared: OS127/2016 15:I8 Analyzed: 06/03/2016 11:32
Spike Source %REC
RPD
.Analyte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Lima Notes
Oil & Grease (HEM)
0,616
Li
1.28
mg/L
LIES (6E27007-BSI)
Prepared: 05/27/2016 15:18 Analyzed: 06/03/2016 11:32
Spike Source %REC
RPD
.Analyte
Result
flaci
POL
Units
Level Result %REC Limits RPD
Limit Notes
Oil & Grease (HEM)
122
5.00
mg/L
153 80 78-114
LCS Dup (6E27007-B5D1)
Prepared: 05/27/2016 15:18 Analyzed: 06/03/2016 11:32
Spike Source OAREC
RPO
.Analyte
Result
Flaa
P01,
Units
Level Result %REC Limits RPD
"I w Notes
Oil &, Grease (HEM)
143
5,00
mg/L
152 94 78-114 16
18
Matrix Spike 16EZ7007-MSI)
Prepared: OS/27/2016 15:18 Analyzed: 06/03/2016 11:32
Source;SZO2193-01
Spike Source %REC
RPD
,Analyte
Result
Flaq
POL
Units
Level Result 0/aREC Limits RPD
Limit Notes
Oil & Grease (HEM)
33.6
1.25
mg/L
39.9 0.599 U 84 78-114
Page 37 of 39
FINAL This report relates only to the sample as received N the laboratory, and may only be reproduced m full. Page 5 of 7

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
I The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
Page 38 of 39
FINAL Thls report retates only to the sample as received by the laboratory, and may only be reproduced In full. Page 6 or 7

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State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Alan W. Klimek, P.E., Director
March 10, 2004
DYNEA USA INC
ATTN: RW 1-1UMP1.IREYS, OR SUCCESSOR
790 CORINTH RD
MONCURE, NC 27559
YIPFA
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RE50URCE5
Subject: NPI)ES Storrnwater Permit Renewal
Dynea USA Inc
Permit Number NCS000150
Chatham County
Dear Permince:
YOUr facility is currently covered for stormwater discharge under NPDI-S Permit NCS000150. This permit expires
on September 30, 2004. North Carolina Administrative Code (15A NCAC 21-1.0105(e)) requires that an
application for permit renewal be riled at least 180 days prior to expiration of the current permit. In order to assure
your continued coverage under your permit, you must apply to the Division of Water Quality (DWQ) for renewal
of your permit. To make This renewal process easier, we are informing you in advance that your permit will be
expiring. Enclosed you will find an individual permit renewal application form, supplemental information request,
and Stormwater Pollution Prevention Plan certification.
Filing the application form along with the requested supplimental information will constitute your application for
renewal of your permit. As stated above, the application form must be completed and returned along with all
requested information by April 3, 2004 in order for the permit to be renewed by September 30, 2004.
Failure to request renewal by April 3, 2004 may result in a civil assessment of at least $500.00. Larger penalties
may be assessed depending on the delinquency of the request. Discharge ol'stormwater from your facility without
coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could
result in assessments of civil penalties of up to $25,000 per day.
if you have any questions regarding the permit renewal procedures please contact Bill Mills of the Storrnwater and
General Permits Unit at [phone], ext. 548.
Sincerely.
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Storrnwater and General Permits Unit Files
Raleigh Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
ENVIRONMENTAL" MANAGEMENT
� 6' , -"r-COMMISSION
"1617 Mail Service Center
Fiateigh, NC 27699-1617
NOTIFICATION OF INTENT
'TO ISSUE A STATE
:.: NPDEs PERMIT_ j
On the basis of thorough staff review and ap-
pficaiion of Article 21 of Chapter 143, General
Statutes of North Catalina, Public Law 92-500
'� other lawful standards aihd iegnlations, the
North Carolina Environmental Management Com-
mission praposes•lo issue a permit to discharge
,to persons flsied balaw on 5eptarmber 13, 1999,
end subject to spedal conddions.
Persons wishing to comment upon or object to
the proposed determinations are invited to submit
same In wrong to the above address no later
than August 29, 1999. All comments received
prior to that date will be considered in the for-.
mutation of anal determinations regarding the 1
proposed permit. -A public meeting may be held
where the Director "of the Division of .Water I
Quality finds a significant degree of public inter
est in a' proposed permit.
A copy of the draft pem:'t is available by writing i
or calling the Division of '.Pater Quality, 1617 Mail
Service_ Cenle►, Raleigh, North Carolina 27699-
1617, [phone]. -
The RpP lica!inn an! ::�'f :^la a1;;,1 � Idyl ua ;o_
spected at these locations during normal office
hours, Ccoes of the infornsation on fife are avail-
able upon request and payment of the costs of
reproduction. "All such comments or requests
regarding a proposed permit should' make
reference to the NFDES permit number listed
below.
Date: 7126/99
t)avid A. Goodrich-
for Kerr T. Stevens, Director
Division of Water Quality
NPDES No. NCS000115, Novo Nordisk'
Biochem, 77 Perry Chapel Church Road,
Franktinton, North Carolina, 27525 has applied
for a permit to discharge slormwater associated
with industrial activities at a facility located at 77
Perry Chapel Church Road, FrankGnton, North
Carolina. The facility discharges to the waters of
the Tar-Pamrco River Basin.
NPOES No. NCS000150, Neste Resins Corp.,
790 Corinth Road, Moncure, North Carolina,
27559 has applied for a permit to discharge
stormwaler associated with industrial activities at
Franklin County's Newspaper [phone]
109 S. Bickett Boulevard P.O. Box 119 Louisburg, N.C. 27549-0119
AFFIDAVIT
North Carolina —Franklin County.
1, ___-C.ar lt___-Cuxiar_d___ , ._L' uhi- -, of
THE FRANKLIN TIMES, a newspaper published at
Louisburg, Franklin County, N. C., hereby eertify that
the advertisement of _S t a-f e _o f
_E av-Lr�=mantP 1 Nananmm�nr,
----------------
a covv of which is hereto attached, appeared in the fol-
8 ractiity !ocated at 790 Corinthh Road, Moncure,
North Carolina. The lacili v discharges to the
orders or the Gape rear River Basin, ;Sues of said publication: —j u l y _g I _19__9;j
---.... --.--------------------__.19---
--- -"---------------•- _------- 19. --- ;
19—.
7
This h.day,of ------ 19 99
Subscribed artd sworn to before me this t•-h--^_day of
....... -------------I--}--19..99
Notary Public.
My Commission Expires ............

AFFIDAVIT OF PUBLICATION
NORTH CAROLINA.
Wake County. Ss.
PUBLIC NdTICE
STATt= OF NORTH CAROLINA
j ENVIRONMENTAL ANAGEMENT. aDMMI551PN M;tt
k1617 Moil Servl® Curler. Aalelgh NC VM9.1617
:.,i:.a,NOnFICATION OF INTENT To ISSUE
A STATE NPDES PERMIT .., . -
onlhebasis•o1.Iharauyhstaffreviawanda0pticafianalArticle2i
of Chapter t43, General Statutes of North Carolina, Public Law
92.500 and other lawful standards and regulations, the North
Carolina Environmental Management Commission Proposes b
Issue a Permit to discharge to persons listed below an September
13, 1999, and subiect to special conditions.,,
Persons wishing to comment upon or obiect to the Proposed
determinations ore invited to submit some in writing to the above
address no later than August 29, 19". All comments received
prior to that date will be considered in the formulation of final
determinations regarding the PraPosed permit. A Public meeting
may be held where the Director of the Division of Water Duality
finds a significant degree of public interest in a Proposed permit.
A'copy-of the draft permit is available by writing or calling the
Division, of Water quality, 1617 Mail Service Center, Raleigh.
North Carolina 27699.1617, (919) 713-50M. - The application and other Information may be inspected at these
locations during narmal office hours. Copies of the information
on file are available upon rcquesf and gaynteal of the costs of
rearodvction. All such comments or recivests regarding a pro-
posed permit should make reference to the NPDES Permit
number listed below. - -
7a6N9
Isl David A_ Goodrich
for Kerr T. Stevens. Director
Division of water Quality
N P D E 5 No. NCS000115. Nova Nardisk Biochem, 77 Perry Chapel
Church Road Fronklintan, North Carolina. 27525 has noolied for
a Permit to discharge stormwater associated with industrial
activities at a facility located at 77 Perry Chapel Church Road,
Franklinton, North Carolina. The facility discharge$ to the
waters of Ina Tar - Pamlico River Basin.
NPDES No. NCSOM150, Neste Resins Corp., 790 Corinth Rolla.
Mohcure, North Carolina. 17559 has applied for a permit to
discharge stormwater associated with industrial activities at a
facility located of 790 Corinth Road, Moncure, North Carolina.
The facility discharges to the waters of the Cape Fear River
l ll J` i Basin.
Nao: July 29, 1999
PAID
Before the undersigned, a Notary Public of said
County and State, duly Commissioned and authorized to
administer oaths, affirmations, etc., personally appeared
Patricia L. Robinson who, being duly swom or affuTned,
according to law, loth depose and say that she is Billing
Manager -Legal Advertising of THE NEWS AND
OBSERVER PUBLISHING COMPANY a corporation
organized and doing business under the Laws of the State of
North Carolina, and publishing a newspaper known as THE
NEWS AND OBSERVER, in the City of Raleigh, County and
State aforesaid, the' said newspaper in which such notice,
paper, document, or legal advertisement was published was, at
the time of each and every such publication, a newspaper
meeting all of the requirements and qualifications of Section
1-597 of the General Statutes of North Carolina and was a
qualified newspaper within the meaning of Section 1-597 of
the General Statutes of North Carolina, and that as such she
makes this affidavit; that she is familiar with the books, files
and business of said corporation and by reference to the files
of said publication the attached advertisement for NC
DIVISION OF W was inserted in the aforesaid newspaper on
dates as follows: 07129/99
Account Number: 73350831
The above is correctly copied from the books and files of the aforesaid Corporation and publication.
t
;LL,1!I - , ll
Billing Manager -Legal Advertising
Sworn or affirmed to, and subscribed before me, this
30 day of JULY , 1999 AD
In Testimony'Whereof, I have hereunto set my hand
and affixed my official seal, the day and year aforesaid.
X`''!� 1
. _ - ------------- Notary Public
My commission expires 2nd day of July 2000.

The C11.11t all) News
fly ciptipill lkuorb
NORTH CAROLINA
CHATHAM COUNTY
AFFIDAVIT OF PUBLICATION
Before the undersigned, A Notary PUTAC of said County and Stale, duly
corrmmissioned. qualified, and authorized by law to ndminisler oalhs, personally
appeared_ -..._
Florence E. Turner who being
first clitly sworn, deposes and says: that lie (she) is
Accounts Receivable Clerk
(ownw, parinor, pubiishur. or oilier olricer or ompioyea au1h01i7?d In makrr lhls zrtidavil)
of The Chalharn News Publishing Co., inc., engaged in the pubicaliolt of a
newspaper known as, The Chatham Newsflhe Chatham record published, is-
sued, and erilered as second class mail in the Towli of Siler City, in said County
and Slate; that he (she) is authorized to rnalce this affidavit and sworn state-
ment; illat the police or legal adverlisement, 7 trim, ropy of which is allached
hereto, was published in The Chatham News/The Chatham Record on the fol-
lowing dales:
and that the said newspaper in which such nolice, paper, document, or legal
advertisement was published was, at the time of each and every such publica-
tion, a newspaper meeting all of the requirements and qualifications of Section
1-597 of the General Statutes of North Carolina and was a qualified newspaper
within the meaning of Section 1-597 of [he Geneval Statutes of North Carolina.
This lay of
(Sigrralsire of parson nmP.irih lffirlavit)
Sworn to and subscribed before me, this _ -� 2
day
Notary r,rnrr.
My Commission expires: II G? - •-� c
19 '7 2
---IPCI30CWUTCE
STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT
COMMISSION
1617 Mail Service Center, Raleigh,
NC 27699-1617
NOTIFICATION OF INTENT,TO ISSUE
A. STATE NPDES PERMIT
On the basis of thorough staff review
and application of Article 21 of Chapter
143, General Statutes of North Caro
lina, Public Law 92-500 and other lawful
standards and regulations, the North
Carolina Environmental Management
Commission proposes to issue a permit
to discharge to persons listed below on
September 13. 1999, and subject to
special conditions.
Persons wishing to comment upon or
object to the proposed determinations
are invited to submit same in writing to
the above address no later than August
29, 1999. All comments received prior
to that date will be considered in the
formulation of final determinations re-
garding the proposed permit. A public
meeting may be held where the Director
of the Division of Water Duality finds a
significant degree of public interest in a
proposed permit,
A copy of the draft permit is available
by writing or calling the Division of Wa-
fer Quality, 1617 Mail Service Center,
Raleigh, NC 27699.1617, (919) 733-
5093.
The application and other information
may be inspected at these locations
dunng normal office hours. Copies of
the information on file are available
upon request and payment of the costsc
of reproduction. All such comments of
requests regarding a proposed permit
should be make reference to the
NPDES permit number listed below.
Date: July 26, 1999.
David A. Goodrich
Kerr T. Stevens, Director
Division of Water Quality
PDES No. NCS000115, Novo NordisF
Biochem, 77 Perry Chapel Churef
Road, Franklinion, NC 27525 has ap.
plied for a permit to discharge stormwa.
ter associated with industrial activities
at a facility located at 77 Perry Chape
Church Road, Franklinton, NC. The
facility discharges to the waters of the
Tar -Pamlico River Basin, -,
POES No. NCS000150.1 Neste Res
ins Carp., 790 Corinth Road, Moncure
NC 27559 has applied for a permit tc
discharge stormwater associated wits
industrial activities at a facility located E
790 Corinth Road, Moncure, NC. Th,
facility discharges to the waters of the
Cape Fear River Basin.
Jy29-1 t

PUBLIC NOTICE
STATE OF NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
1617 Mail Service Center, Raleigh, NC 27699-1617
NOTIFICATION OF INTENT TO ISSUE A STATE NPDES PERMIT
On the basis of thorough staff review and application of Article 21 of Chapter 143, General Statutes of
North Carolina, Public Law 92-500 and other lawful standards and regulations, the North Carolina
Environmental Management Commission proposes to issue a permit to discharge to persons listed below on
September 13, 1999, and subject to special conditions.
Persons wishing to comment upon or object to the proposed determinations are invited to submit same in
writing to the above address no later than August 29, 1999. All comments received prior to that date will
be considered in the formulation of final determinations regarding the proposed permit. A public meeting
may be held where the Director of the Division of Water Quality finds a significant degree of public
interest in a proposed permit.
A copy of the draft permit is available by writing or calling the Division of Water Quality, 1617 Mail
Service Center, Raleigh, North Carolina 27699-1617, [phone].
The application and other information may be inspected at these locations during normal office hours.
Copies of the information on file are available upon request and payment of the costs of reproduction. All
such comments or requests regarding a proposed permit should be make reference to the NPDES permit
number listed below.
Date 11�C
Kerr T. Stevens, Director
f OY Division of Water Quality
NPDES No. NCS0001 15, Novo Nordisk Biochem, 77 Perry Chapel Church Road, Franklinton, North
Carolina, 27525 has applied for a permit to discharge stormwater associated with industrial activities at a
facility located at 77 Perry Chapel Church Road, Franklinton, North Carolina. The facility discharges to
the waters of the Tar - Pamlico River Basin.
NPDES No. NCS000150, Neste Resins Corp., 790 Corinth Road, Moncure, North Carolina, 27559 has
applied for a permit to discharge stormwater associated with industrial activities at a facility located at 790
Corinth Road, Moncure, North Carolina. The facility discharges to the waters of the Cape Fear River
Basin.

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
April 7, 1999
Neste. Resins Corporation
Attn: R. W. Humphreys
790 Corinth ]toad
Moncure, North Carolina 27559
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Subject: NPDES Permit Renewal Application
Permit Number NCSOOO150
Individual Stormwater Permit
Chatham County
Dear Mr. Humphreys:
The Division of Water Quality's Stormwater and General Permits Unit hereby acknowledges receipt of your renewal
application for coverage under NPDES Permit Number NCS000150 on 3124/99, The submitted renewal package
contained the following items. -
Signed application
Site map
Visual monitoring results summary
:- Best Management Practices summary
i Narrative describing significant changes at the permitted facility
Signed Stormwater Pollution Prevention Plan certification
A preliminary review of the submitted renewal application package has been conducted and it appears to be
complete. No further information is required at this time. If you have any questions about the renewal process or
would like to discuss this letter, please contact me at [phone], extension 584,
in er
Antonio V. Evans, P.E.
cc: Raleigh Regional Office
Stormwater and General Permits Unit
Central Files
SWU-238-032 399
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Neste Resins Corporation
790 Corinth Road Post Office Box 259
Moncure, North Carolina 27559
[phone]
February 25, 1999
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
P.O. Box 29535
Raleigh, NC 27626-0535
Attn: Mr. Bill Mills
-----------
Re: Renewal of Storm Water crniit NCS00015U, N ste Resins Corporation
Dear Mr. Mills_
As we IlaVe discussed on two previous Occasions, I Understand that the Division of Water
Quality is drafting a storm water renewal packet and that there have been delays in its
completion. Once the storm water renewal information is received, Neste Resins
Corporation will complete and submit said information to the Division of Water Quality
within the specified timeframe.
Until the renewal information is received and In complying with the intent of the storm
water permit renewal process, I an't SUbmitting tills notice of continued storm water
operation pursuant to [tic "Expiration of Permil" paragraph of our permit. This notice is
not in lieu of completing Division of Water Quality requirements, but should serve as
documentation that Neste Resins Corporation would like to continue storm water
operations as identified in permit NCS000150.
If you have any questions, please do not hesitate to contact rile at 919-542-2526. 1 look
forward to receiving and completing the renewal information soon.
Respectfully submitted,
Chris D. McKeeman, CSP, CHMM
17-FIS Coordinator
Cc: File

PERMIT COVERAGE RENEWAL APPLICATION
National Pollutant Discharge Elimination System
• Stormwater NPDES Permit NCS000150
00�-_ Neste Resins Corporation
Permit Number NCSOOO 150
NCDENR Chatham County
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
THIS APPLICATION MUST BE SIGNED AND RETURNED ALONG WITH THE REQUESTED
SUPPLEMENTAL INFORMATION TO THE DIVISION OF WATER QUALITY IN ORDER FOR YOUR
FACILITY TO QUALIFY FOR RENEWAL OF YOUR STORMWATER PERMIT NCS000150
PERMIT RENEWAL INFORMATION
The following is the information currently in our database for your facility. Please review this information
Q7)
carefully and make all corrections as necessary in the space provided to the right of the current information.
-r
Facility Name: Neste Resins Corporation
=~'
Mailing Address*: PO BOX 270 7 h Corinth Road
SPRINGFIELD, OR97477 Moncure, NC 27559
.3
—1-
W
Location Address: STATE ROAD 1916 790 Corinth Road
MONCURE, NC 27559 Moncure, .NC 27559
Facility Contact
Phone Number:
Fax Number:
E-mail address:
R.W. HUMPHREYS
No number on file
No address on file
* This is the address to which all permit correspondence will be mailed
CERTIFICATION
91.9-542-2526
919-542-1728
I certify that 1 am familiar with the information contained in the application and that to the best of my
knowledge and belief such information is true, complete and accurate.
Signature Date March 22, 1999
R. W. Humphreys Plant Manager
Print or type name of person signing above Title
Please return this completed renewal form, the information as requested on the next page, and any relevant
documentation to:
Individual Permit Renewal
Division of Water Quality/ WQ Section
Stormwater and General Permits Unit
Post Office Box 29535
Raleigh, North Carolina 27626-0535
Attn: Tony Evans

SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF INDIVIDUAL NPDES
STORMWATER PERMIT
The following should accompany this submittal:
(Do not submit the site Stormwater Pollution Prevention Plan)
Initials
RWH I . A copy of the current Site Map from the Stormwater Pollution Prevention Plan. The
location of industrial activities (including storage of materials, disposal areas, process areas
and loading and unloading areas), drainage structures, drainage areas for each outfall,
building locations and impervious surfaces should be clearly noted. Bee Attached -
N/A 2. A summary of Analytical Monitoring results during the term of the existing permit (if your
permit required analytical sampling). Do not submit individual lab reports. The summary
can consist of a table including such iterns as outfall number, parameters sampled, lab
results, date sampled, and storm event data. *
RWH 3. A summary of the Visual Monitoring results. Do not submit individual lab reports. The
summary can consist of a table including such items as outfall number, parameters
surveyed, observations, and date monitoring conducted. see Attched .
RWH 4. A summary of the Best Management Practices utilized at the permitted facility. Summary
should consist of a short narrative description of each BMP's in place at the facility. if the
implementation of any BMP's is planned, please include information on these BMP's.
See Attached.
RWH S. A short narrative describing any significant changes in industrial activities at the permitted
facility. Significant changes could include the addition or deletion of work processes,
changes in material handling practices, changes in material storage practices, and/or
changes in the raw materials used by the facility. See Attached.
RWH 6. Certification of the development and implementation of a Stormwater Pollution Prevention
Plan for the permitted facility (Sign and return attached form).
* If the final year analytical monitoring of the existing permit term has not been completed
prior to filing the renewal submittal, then the last years monitoring results should be
submitted within 30 days of receipt of the laboratory reports. (i.e. do not withhold renewal
submittal waiting on lab results)
Representative storm sampling may now be conducted anytime during the year (the April to
November window has been eliminated) and the representative rainfall event is now
defined as a storm event that measures greater than 0.1 inches and is preceded by at least
72 hours in which no storm event measuring greater than 0.1 inches has occurred.

SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF
STORM WATER PERM 1T #: NCS000150
1. See attached Site Map and Property Map.
2. No analytical monitoring is required of the Neste Resins Corporation, Moncure, NC
plant.
3. The visual monitoring summary is presented below. Parameters surveyed include
erosion, vegetation, standing water, and evidence of pollution for the stormwater
ditches; silt build-up, structure condition and evidence of pollution for each
stormwater dike; and leaks or spills, evidence of run-off, and housekeeping for
material storage process areas.
Monitoring
Outfall 002 Observations
Outfall 003 Observations
General Observations
Date
10/10/94
Light yellow tint to water
_
Light yellow tint to water with
None.
with no observed odors,
no observed odors.
519195
Colorless with minor
Colorless with minor
None.
sus pendcd solids. No odor.
Suspended solids. No odor.
6/14/96
Colorless with minor
Colorless with minor
Sonic standing water in
suspended solids. No odor.
suspended solids. No odor.
various locations.
Vegetation needs cut
back in and around
ditches.
12/23/96
Colorless Willi minor
Colorless with minor
North dike erosion has
suspended solids. No odor.
suspended solids. No odor.
occurred. Some standing
water in south ditch. Silt
buildup near Outfall 002.
5/21/97
Colorless with minor
Colorless with minor
Heavy vegetation
suspended solids. No odor.
suspended solids. No odor.
buildup in north ditch.
Some standing water
near Outfall 003.
12/12/97
No evidence of staining or
No evidence of staining or
Some erosion near RR
Pollution.
pollution.
tracks in north ditch.
Some standing water but
clean.
5/6/98
No evidence of staining or
No evidence of staining or
Slight erosion behind
Pollution.
pollution.
warehouse in north ditch.
Minor standing water.
1 1/5/98
No evidence of staining or
No evidence of staining or
Short section (50') of
Pollution.
pollution.
standing water in north
ditch.
4. Current Best Management Practices implemented to reduce or eliminate stormwater
runoff from hazardous material storage and process areas include:
Oil and Grease
Maintenance activities during which lubricants might be spilled will not be
performed on trucks or trailers oil the plant site.

Neste Resins Corporation
Stormwater Renewal Permit #: NCSOOO150
03/22/99
Maintenance on forklifts will be performed inside the covered maintenance
shop where spills can be easily cleaned up and prevented from contacting
stormwater.
• Special care will be taken when changing oil in process equipment (pumps, gear
boxes, etc.). Any spills will be cleaned up immediately, including removal of
any contaminated soil.
• All waste oil is accumulated in the waste oil tank at the maintenance shop
before recycling off -site.
Materials Stora e
• All liquid materials will be stored in closed top tanks or closed top drums.
Tanks will be curbed to contain spills. Drums will be stored in areas where
stormwater runoff is directed to the wastewater treatment plant.
• Empty raw materials drums will be treated in the same manner as full drums.
Dry materials in bags will be stored in covered areas out of contact with rainfall.
Only the amount of material needed for a batch process will be removed front
storage and staged in the manufacturing area. All such materials will be
returned to storage or covered if rain starts.
Solid Waste
Separate containers are provided for trash and process waste. These dumpsters
are located in a diked concrete surfaced area. Runoff From this area flows to the
wastewater treatment plant.
• Any waste debris generated as result of maintenance or production will be
collected immediately and disposed of into the proper waste dumpster.
Stormwater System Pollution
• All storage and process areas consist of impervious surfaces designed to drain
into the facility's concrete process drainage ditch. This drainage ditch flows
through the plant and to the onsite wastewater treatment plant.
• The current practice of disposing of all rainfall in process areas in the
wastewater treatment plant will be continued, where practical, in all new
construction. Where not practical, a feasibility study will be conducted on
alternate methods to prevent runoff into the stormwater system.
• Any time contamination of the stormwater system is SLlspected, all stormwater
will be collected at the stormwater ditch dikes and tested before being released.
This procedure will continue Lentil the suspected source of contamination is
corrected and there is 110 evidence of pollution in the water.

Neste Resins Corporation
Stormwater Renewal Permia #: NCS000150
03/22/99
• Any spills on open ground will be contained to prevent flow into the stormwater
system. Steps will be taken to prevent rain runoff from coming in contact with
the contaminated area (cover, berm around area, etc.). Stormwater in the
surrounding area will be tested before releasing. This procedure will continue
until corrective action is completed.
future Projects
• Provide secondary containment for all future storage and process tanks, as well
as solid waste storage areas, to contain incidental process spills or releases.
• Cover all solid waste storage areas with secondary cover (e.g., building) to
prevent contact with precipitation and stormwater.
There have been no significant changes in industrial activities at the Neste Resins
Corporation, Moncure, NC plant.
Neste Resins Corporation has recently installed a third outfall (004) to improve
drainage in a non -process area of the plant (See attached map). This substantially
identical outfall will be monitored semi-annually according to the current permit
requirements. Tile engineering of this outfall is identical to outfalls 002 and 003 and
includes a concrete weir and dual manual valve design. The drainage ditch is earthen
with natural vegetation.
6. See attached Sioi-nmufer Pollution Prevention Plan Development and Implementation
Certification.

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a W10" ial
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a Wee llelaadr%
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SCALE 1' •30' -0'

STORMWATER POLLUTION PREVENTION PLAN
DEVELOPMENT AND IMPLEMENTATION
- CERTIFICATION
N. C. Division of Water Quality, Stormwater and General Permits Unit
Facility Name: NESTE RESINS CORPORATION
Permit Number: NCSOOO150
Location Address: STATE. ROAD 1916
MONCURE, NC 27559
County: CHATHAM
"I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all
attachments were developed and implemented under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information required by the SPPP.
Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information gathered is, to the best of my knowledge and belief, true, accurate, and
complete"
"I certify that the SPPP has been developed, signed and retained at the facility location and the SPPP has been fully
implemented at the named facility location in accordance with the terms and conditions of the stormwater general
permit."
"I am aware that there are significant penalties for falsifying information, including the possibility of fines and
imprisonment for knowing violations"
Sign (according to permit signatory requirements) and return this Certification. DO NOT SEND THE
STORMWATER POLLUTION PREVENTION PLAN WITH THE CERTIFICATION.
Signature Date March 22, 1999
R. W. Humphreys Plant Mana er
Print or type name of person signing above Title
SPPP CertiEcation 2199
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
February 19, 1999
R.W. HUMPHREYS
NESTE RESINS CORPORATION
PO BOX 270
SPRINGFIELD, OR 97477
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Subject: NPDES Stormwater Permit Renewal
Neste Resins Corporation
Permit Number NCS000150
Chatham County
Dear Pennittee:
Your facility is currently covered for stormwater discharge under NPDES Permit NCS000150. This permit
expires on August 31, 1999. In order to assure your continued coverage under your permit, you must apply to the
Division of Water Quality (DWQ) for renewal of your permit. To make this renewal process easier, we are
informing you in advance that your permit will be expiring. Enclosed you will find an individual permit renewal
application form, supplemental information request, and Stormwater Pollution Prevention Plan certification.
Filing the application form along with the requested supplimental information will constitute your application for
renewal of your permit. The application form must be completed and returned along with all requested
information within thirty days of receipt of this letter in order to constitute a timely renewal fling.
Recent legislation modified the fee structure for DWQ permits. Renewal fees have been eliminated and annual
fees have been changed. The new annual fee for your permit is now $715.00 (you will be invoiced later this year
for your annual fee.) A copy of the new fee schedule is enclosed in this package.
Failure to request renewal within the time period indicated may result in a civil assessment of at least $250,00,
Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from
your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS
143-215.1 and could result in assessments of civil penalties of up to $10,000 per day.
If you have any questions regarding the permit renewal procedures please contact Tony Evans of the Stormwater
and General Permits Unit at [phone], ext. 584.
Sincerely,
f�
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Raleigh Regional Office
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
September 17, 1999
Mr. R. W. Humphreys
Neste Resins Corporation
790 Corinth Road
Moncure, North Carolina 27559
1 • •
1-0-%
WW-%
NCDENR
NORTH CAROLINA DEPARTMENT- OF
ENVIRONMENT ANo NATURAL RESOURCES
Subject: Permit No. NCS000150
Neste Resins Corporation
Chatham County
Dear Mr. 'l ybaert:
In response to your renewal application for continued coverage under NPDES stormwater permit
NCS000150, the Division of Water Quality (DWQ) is forwarding herewith the subject state - NPDES permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of
Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1981
Please note that the enclosed permit may differ from the draft permit that was previously sent. Based on a
review of the permit monitoring data received to date, the Division has revised the monitoring strategy for individual
stormwater permits. The measurement frequency has been changed and cut-off concentrations have been removed.
'I'hese changes will he implemented for all second term individual stormwater permits with analytical monitoring
requirements. For those permits with analytical monitoring requirements, Part II - Monitoring, Controls, and
Limitations for Permitted Discharges has been modified to reflect the change in monitoring strategy.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to
YOU, you have the right to an adjudicatory hearing upon written request within thirty (30) clays following receipt of
this letter. This request must he in the form of a written petition, conforming to Chapter 150B of the North Carolina
General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North
Carolina 27611 -7447. Unless such demand is made, this decision shall he final and binding.
Please take notice this permit is not transferable. Part III, B.2. addresses the requirements to he followed in
case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may he required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may he required.
If you have any questions concerning this permit, please contact Tony Evans at telephone number 919/733-
5083 ext. 594.
Sincerely,
ORIGINAL SIGNED BY
WILLIAM C. MILLS
for Kerr T. Stevens
cc: Mr. Roger O. Pfaff, EPA
Raleigh Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Permit No. NCS000150
i
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
►� 1
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Neste Resins Corporation
is hereby authorized to discharge stormwater from a facility located at
Neste Resins Corporation
790 Corinth Road
Moncure, NC
Chatham County
to receiving waters designated as the Haw River, a class WS IV stream, in the Cape Fear River
Basin
in accordance with the discharge limitations, monitoring requirements, and other conditions set
forth in Parts 1, 11, III, IV, V and VI hereof.
This permit shall become effective October 1, 1999.
This permit and the authorization to discharge shall expire at midnight on March 31, 2001.
Signed this day September 13, 1999.
oRw�u �ISc M�� BY
for Kerr T. Stevens, Director
Division of Water Quality
By the Authority of the Environmental Management Commission

r
Permit No. NCS000150
r
TABLE OF CONTENTS
PART I INTRODUCTION
Section A: Individual Permit Coverage
Section B: Permitted Activities
Section C: Location Map
PART 11 MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
Section A: Stormwater Pollution Prevention Plan
Section B: Qualitative Monitoring Requirements
Section C: On -Site Vehicle Maintenance Monitoring Requirements
PART III STANDARD CONDITIONS
Section A: Compliance
and Liability
1.
Compliance Schedule
2.
Duty to Comply
3.
Duty to Mitigate
4.
Civil and Criminal Liability
5.
Oil and Hazardous Substance Liability
6.
Property Rights
7.
Severability
S.
Duty to Provide Information
9.
Penalties for Tampering
10.
Penalties for Falsification of Reports
Section B: General
Conditions
I.
Individual Permit Expiration
2.
Transfers
3.
Signatory Requirements

Permit No. NCS000150
,i
4. Individual Permit Modification, Revocation and Reissuance, or
Termination
5. Permit Actions
Section C: Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D: Monitoring and Records
I.
Representative Sampling
2.
Recording Results
3.
Flow Measurements
4.
Test Procedures
5.
Representative Outfall
6.
Records Retention
7.
Inspection and Entry
Section E: Reporting
Requirements
1,
Discharge Monitoring Reports
2,
Submitting Reports
3.
Availability of Reports
4.
Non-Stormwater Discharges
5.
Planned Changes
6.
Anticipated Noncompliance
7.
Bypass
S.'
Twenty-four Hour Reporting
9.
Other Noncompliance
10.
Other Information '
PART IV LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
PART V I DEFINITIONS
IE

Permit No, NCS000150
PART I INTRODUCTION
SECTION A: INDIVIDUAL, PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified in this permit.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge
stormwater to the surface waters of North Carolina or separate storm sewer system which has
been adequately treated and managed in accordance with the terms and conditions of this
individual permit. All discharges shall be in accordance with the conditions of this permit.
Any other point source discharge to surface waters of the state is prohibited unless it is an
allowable non-stormwater discharge or is covered by another permit, authorization or approval.
This permit does not relieve the permittee from responsibility for compliance with any other
applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree.
Part I Page 1 of 2

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Permit No. NCSOOO 150
PART 11 MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
SECTION A: STORMWATER POLLUTION PREVENTION PLAN
The permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as
the Plan. This Plan shall be considered public information in accordance with Part III, Standard
Conditions, Section E, Paragraph 3 of this individual permit. The Plan shall include, at a
minimum, the following items:
Site Plan. The site plan shall provide a description of the physical facility and the
potential pollutant sources which may be expected to contribute to contamination of
stormwater discharges, The site plan shall contain the following
(a) A general location map (USGS quadrangle map or appropriately drafted
equivalent map), showing the facility's location in relation to transportation
routes and surface waters, the name of the receiving water(s) to which the
stormwater outfall(s) discharges, or if the discharge is to a municipal separate
storm sewer system, the name of the municipality and the ultimate receiving
waters; and accurate latitude and longitude of the point(s) of discharge.
(b) A narrative description of storage practices, loading and unloading activities,
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices.
(c) A site map drawn to scale with the distance legend indicating location of
industrial activities (including storage of materials, disposal areas, process areas
and loading and unloading areas), drainage structures, drainage areas for each
outfall and activities occurring in the drainage area, building locations, existing
BMPs and impervious surfaces, and the percentage of each drainage area that is
impervious. For each outfall, a narrative description of the potential pollutants
which could be expected to be present in the stormwater discharge.
(d) A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part III, Standard Conditions, Section
B, Paragraph 3.
2. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed which control or
minimize the exposure of significant materials to stormwater, including structural and
nonstructural measures. The stormwater management plan, at a minimum, shall
incorporate the following:
Part 11 Page I of 5

Permit No. NCS000150
(a) Feasibility Study. A review of the technical and economic feasibility of changing
the methods of operations and/or storage practices to eliminate or reduce exposure
of materials and processes to stormwater. Wherever practical, the permittee shall
prevent exposure of all storage areas, material handling operations, and
manufacturing or fueling operations. In areas where elimination of exposure is
not practical, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from areas of potential contamination.
(b) Secondary Containment Schedule. A schedule to provide secondary containment
for bulk storage of liquid materials, storage of Section 313 of Title III of the
Superfund Amendments and Reauthorization Act (SARA) water priority
chemicals, or storage of hazardous substances to prevent leaks and spills from
contaminating stormwater runoff. If the secondary containment devices are
connected directly to stormwater conveyance systems, the connection shall be
controlled by manually activated valves or other similar devices [which shall be
secured with a locking mechanism] and any stormwater that accumulates in the
containment area shall be at a minimum visually observed for color, foam, outfall
staining, visible sheens and dry weather flow, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated by the material stored within the containment area. Records
documenting the individual making the observation, the description of the
accumulated stormwater and the date and time of the release shall be kept for a
period of five years.
(c) BMP Summary. A narrative description shall be provided of Best Management
Practices (BMPs) to be considered such as, but not limited to, oil and grease
separation, debris control, vegetative filter strips, infiltration and stormwater
detention or retention, where necessary. The need for structural BMPs shall be
based on the assessment of potential of sources to contribute significant quantities
of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or team) responsible for implementing the
SPRP shall be identified. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater runoff through spills or
exposure of materials associated with the facility operations. The SPRP must be site
stormwater specific. Therefore, a SPCC plan may be a component of the SPRP, but may
not be sufficient to completely address the stormwater aspects of the SPRP. The common
elements of the SPCC with the SPRP may be incorporated by reference into the SPRP.
4. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance program shall be developed. The program shall document schedules of
inspections and maintenance activities of stormwater control systems, plant equipment
and systems. Inspection of material handling areas and regular cleaning schedules of
these areas shall be incorporated into the program.
Part 11 Page 2 of 5

Permit No. NCS000150
Employee Training. Training schedules shall be developed and training provided at a
minimum on an annual basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
operations that have the potential to contaminate stormwater runoff. Facility personnel
(or team) responsible for implementing the training shall be identified.
6. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position assignments provided.
7. Plan Amendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance which has a significant effect on the
potential for the discharge of pollutants to surface waters. The Stormwater Pollution
Prevention Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requirements of the permit. Within 30 days of such notice, the permittee shall
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with
Part III, Standard Conditions, Section B, Paragraph 3) to the Director that the changes
have been made.
8. Facility Inspection Program. Facilities are required to inspect all stormwater systems on
at least a semiannual schedule, once in the fall (September -November) and once in the
spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date'and time of inspection, individual(s)
making the inspection and a narrative description of the facility's Stormwater control
systems, plant equipment and systems. Records of these inspections shall be
incorporated into the Stormwater Pollution Prevention Plan.
Stormwater discharge characteristic monitoring as required in Part 11 of this permit shall
be performed in addition to facility inspections.
9. Implementation. The permittee shall document all monitoring, measurements,
inspections and maintenance activities and training provided to employees, including the
log of the sampling data and of activities taken to implement $MPs associated with the
industrial activities, including vehicle maintenance activities. Such documentation shall
be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
SECTION B. QUALITATIVE MONITORING REQUIREMENTS
Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified below in Table 1. Qualitative
monitoring is for the purpose of evaluating the effectiveness of the Stormwater Pollution
Part 11 Page 3 of 5

Permit No. NCS000150
Prevention Plan (SPPP) and assessing new sources of stormwater pollution. No analytical tests
are required. Qualitative monitoring of stormwater outfalls does not need to be performed during
a representative storm event.
In the event an atypical condition is noted at a stormwater discharge outfall, the Permittee shall
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the Stormwate€ Pollution Prevention
Plan.
All qualitative monitoring will be performed twice per year, once in the spring (April - June) and
once in the fall (September - November)_
Table 1. Qualitative Monitoring Requirements
"
DtschargeFCltaracter�stics,
_
4- = Frequency Y;,�
o -,.
�M6A6t E;n—lg�
' P5'1Y Y rx
A Yl '�"+ a 4k. k 4 Tlr
!F :• '•' 1 ' S= �' t
�LoC't`lltlo
T . .., e•. x'- r 1ia.. ;`.L ?..• Lys ;f;1•
e, i k Ir, ...c-'+-. ...•�i
°t,
Color
Semi -Annual
SDO
Odor
Semi -Annual
SDO
Clarity
Semi -Annual
SDO
Floating Solids
Semi -Annual
SDO
Suspended Solids
Semi -Annual
SDO
Foam
Semi -Annual
SDO
Oil Sheen
Semi -Annual
SDO
Other obvious indicators
Semi -Annual
SDO
of stormwater pollution
Footnotes:
1 Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO)
regardless of representative outfall status.
SECTION C. ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
Facilities which have any vehicle maintenance activity occurring on -site which uses more than
55 gallons of new motor oil per month when averaged over the calendar year shall perform
analytical monitoring as specified below in Table 2. This monitoring shall be performed at all
outfalls which discharge stormwater runoff from vehicle maintenance areas.
All analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of 4 analytical samplings being conducted over the term of
the permit at each stormwater discharge outfall (SDO) which discharges stormwater runoff from
vehicle maintenance areas. The permittee shall complete the minimum 4 analytical samplings in
accordance with the schedule specified in Table 3 .
Part Il Page 4 of 5

Permit No. NCS000150
Table 2. Analytical Monitoring Requirements for On -Site Vehicle Maintenance
S.Y r
D�schat•ge ,Gltaractertsttcs��
LJnttsMeastirement
� dr - - -
� 6oa"yd. �s3.
ampler t��Sample
�kii
-'�'. Lk ..{`s.
` -:--
^�.+'
:
,1 �•+°'i',�k"`c'aag,..m� -t
Fre
�WdX..r�
_-=3
uency1
H
standard
Quarterly- 41h year
Grab
SDO
Oil and Grease
Mgt]
Quarterly- 4' year
Grab
SDO
Total suspended Solids
MEZI
Quarterly- 41h year
Grab
SDO
New Motor Oil Usagegallons/month
Quarterly- 4"' year
Estimate
-
Total FI0w4
MG
Quarterly- 4'h year
(:grab
SDO
Footnotes:
I Measurement Frequency: Once per quarter during the 4" year of the permit term. A year is defined as the 12
month period beginning on the month and day of issuance of the Permit. See Table 2 for schedule of monitoring
periods.
2 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. If the detention pond discharges only in response
to a storm event exceeding a ten year design storm, then no analytical monitoring is required and only qualitative
monitoring shall be performed.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle maintenance activities occur.
4 Total flow shall be, (a) measured continuously, (b) calculated based on the amount of area draining to the outfall,
the amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the measurement
of flow at 20 minute intervals during the rainfall event. Total precipitation and duration of the rainfall event
measured shall result from the sampled representative storm event.
-M. •,� war;
Table 3 Monitoring schedule (for4Permits.tssuedTlO/0.119 .IW' )
�'Ivlonttor�ng perrcad��`
y;Sample Number�=
� �•Stat;t�..: „'_
�� �:�� ��2End� ;'r'�
Year 4 - 1" quarter
1
October 1, 1999
December 31, 1999
Year 4 - Td quarter
2
January 1, 2000
March 31, 2000
Year 4 - 3" quarter
3
April t, 2000
June 30, 2000
Year 4 - 4'h quarter
4
.luly 1, 2000
September 30, 2000
Part 11 Pace 5 of 5

Permit No. NCS000150
PART Ill STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented within
12 months of the effective date of the initial permit and updated thereafter on an annual basis. Secondary
containment, as specified in Part 11, Section A, Paragraph 2(b) of this permit, shall be accomplished within
12 months of the effective date of the initial permit issuance.
Proposed Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented prior to
the beginning of discharges from the operation of the industrial activity and be updated thereafter on an
annual basis. Secondary containment, as specified in Part II, Section A, Paragraph 2(b) of this permit shall
be accomplished prior to the beginning of discharges from the operation of the industrial activity.
Duty to Comply
The permittee must comply with all conditions of this individual permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit upon renewal application.
a. The permittee shall comply with standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants within the time provided in the regulations that establish these
standards or prohibitions, even if the permit has not yet been modified to incorporate the
requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $25,000 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than I year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed an administrative penalty not to exceed $10,000 per violation with the maximum
amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33 USC 13t9 and 40 CFR
122.41(a). ]
c. Under state law, a daily civil penalty of not more than ten thousand dollars ($10,000) per violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit [Ref: North Carolina General Statutes 143-2 t5.6A]
Any person may be assessed an administrative penally by the Director for violating section 301,
302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing any
of such sections in a permit issued under section 402 of the Act. Administrative penalties for Class
violations are not to exceed $10,000 per violation, with the maximum amount of any Class I
penalty assessed not to exceed $25,000. Penalties for Class II violations are not to exceed $10,000
per day for each day during which the violation continues, with the maximum amount of any Class
11 penalty not to exceed $125,000.
Part llI Page I of 8 Pages

Permit No. NCS000150
Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the environment.
4. Civil and Criminal Liabilit
Except as provided in Part Ill, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6A, 143-215.613, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may be subject to
under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USC 1321.
6, Property Rights
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
7. Severability
The provisions of this individual permit are severable, and if any provision of this individual permit, or the
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall furnish to the Director, within a reasonable time, any information which the Director
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit_ The
permittee shall also furnish to the Director upon request, copies of records required to be kept by this
individual permit.
9. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this individual permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not
more than two years per violation, or by both. If a conviction of a person is for a violation committed after
a first conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per day
of violation, or by imprisonment of not more than 4 years, or both.
Part III Page 2 of 8 Pages

Permit No. NCS000150
10. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this individual
permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years
per violation, or by both.
SEC'rION B: GENERAL CONDITIONS
Individual Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the permittee shall submit forms and Dees as are
required by the agency authorized to issue permits no later than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at least t 80 days prior to expiration, will be
subjected to enforcement procedures as provided in NCGS § 143-215.6A and 33 USC 125 t et. seq.
2. Transfers
This permit is not transferable to any person except after notice to and approval by the Director. The
Director may require modification or revocation and reissuance of the permit to change the name and
incorporate such other requirements as may be necessary under the Clean Water Act.
Signatory Requirements
All applications, reports, or information submitted to the Director shall be signed and certified.
All applications to be covered under this individual permit shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the
manager of one or more manufacturing production or operating facilities employing more
than 250 persons or having gross annual sales or expenditures exceeding 25 million (in
second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official. "
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
Part LH Page 3 of 8 Pages

Permit No. NCS000150
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus he either a named
individual or any individual occupying a named. position.); and
(3) The written authorization is submitted to the Director.
c. Any person signing a document under paragraphs a. or b. of this section shall make the following
certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
property gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief,'true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
4. Individual Permit Modification, Revocation and Reissuance, or Termination
The issuance of this individual permit does not prohibit the Director from reopening and modifying the
individual permit, revoking and reissuing the individual permit, or terminating the individual permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations; Parts 122
and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North Carolina
General Statute 143-215.1 et. a[.
After public notice and opportunity for a hearing, the individual permit may be terminated for cause. The
filing of a request for a individual permit modification, revocation and reissuance, or termination does not
stay any individual permit condition. The permit shall expire when the individual permit is terminated.
Permit Actions
The permit may be modified, revoked and reissued, or terminated for cause_ The notification of planned
changes or anticipated noncompliance does not stay any individual permit condition.
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the permittee to achieve compliance with
the conditions of this individual permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
2. Need to Halt or Reduce Not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this individual permit.
3, Bypassing of Stormwater Control Facilities
Part IT] Page 4 of 8 Pages

Permit No. NCS000150
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless:
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
b. There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
weather. This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
c. The permittee submitted notices as required under, Part III, Section E of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may approve an
anticipated bypass after considering its adverse effects.
SECTION D: MONITORING AND RECORDS
1. Representative Samoline
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and
nature of the permitted discharge. Analytical sampling shall be performed during a representative storm
event. Samples shall be taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of water, or substance.
Monitoring points as specified in this permit shall not be changed without notification to and approval of
the Director.
2. Recording Results
For each measurement, sample, inspection or maintenance activity performed or collected pursuant to the
requirements of this individual permit, the permittee shall record the following information:
a. The date, exact place, and time of sampling, measurements, inspection or maintenance activity;
b. The individual(s) who performed the sampling, measurements, inspection or maintenance activity;
C. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
Part III Page 5 of 8 Pages

Permit No. NCS000150
4. Test Procedures
Test procedures for the analysis of pollutants shall conl'orm to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136,
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower reporting level of the procedure.
5. Representative Qutfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status. If it is
established that the stormwater discharges are substantially identical and the permittee is granted
representative outfall status, then sampling requirements may be performed at a reduced number of outfalls.
6. Records Retention
Visual monitoring shall be documented and records maintained at the facility along with the Stormwater
Pollution Prevention Plan_ Copies of analytical monitoring results shall also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous monitoring instrumentation, and copies of all
reports required by this individual permit for a period of at least 5 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time.
Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director), or in the case of a facility which discharges through a municipal
separate storm sewer system, an authorized representative of a municipal operator or the separate storm
sewer system receiving the discharge, upon the presentation of credentials and other documents as may be
required by law, to;
a. Enter upon the permittee'.s premises where a regulated facility or activity is located or conducted,
or where records must be kept under the conditions of this individual permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of
this individual permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),
practices, or operations regulated or required under this individual permit; and
d_ Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
Part III Page 6 of 8 Pages

Permit No. NCS000150
SECTION E: REPORTING REQUIREMENTS
1. Discharge Monitoring Re cu )rts
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be received by the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
Documentation of the qualitative monitoring associated with the initial analytical monitoring event shall be
included with the required analytical monitoring submittal for the first year of the permit coverage.
Analytical results from sampling during the final year of the permit coverage shall be submitted with the
permit renewal application.
2. Submitting Reports
Duplicate signed copies of all reports required herein, shall be submitted to the following address:
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
3. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection
at the offices of the Division of Water Quality. As required by the Act, analytical data shall not be
considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.613 or in Section 309 of the Federal Act.
4. Non-Stormwater Discharges
If the storm event monitored in accordance with this individual permit coincides with a non-Stormwater
discharge, the permittee shall separately monitor all parameters as required under the non-stormwater
discharge permit and provide this information with the stormwater discharge monitoring report.
Planned Chanizes
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which could significantly alter the nature or quantity of pollutants discharged. This notification
requirement includes pollutants which are not specifically listed in the individual permit or subject to
notification requirements under 40 CFR Part 122.42 (a).
Anticinated Noncompliance
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which may result in noncompliance with the individual permit requirements.
Part HI Page 7 of 8 Pages

Permit No. NCS000150
7. Bypass
a. Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit
prior notice, if possible at least ten days before the date of the bypass; including an evaluation of
the anticipated quality and affect of the bypass.
Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass.
Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been received
within 24 hours.
9, [:)Cher Noncompliance
The permittee shall report ail instances of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
10. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in an application for an
individual permit or in any report to the Director, it shall promptly submit such facts or information.
Part III Page 8 of 8 Pages

Permit No. NCS000150
PART IV LIMITATIONS REOPENFR
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) (c), and (d), 304(b) (2) and
307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or approved:
a. Contains different conditions or is otherwise more stringent than any effluent limitation in the individual
permit; or
b. Controls any pollutant not limited in the individual permit.
The individual permit as modified or reissued under this paragraph shall also contain any other requirements in the
Act then applicable.
PART V ADMINISTERING AND COMPLIANCE MONITORING I:EE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed by
the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the Individual Permit.
PART VI DEFINITIONS
Act
See Clean Water Act.
2. Arithmetic Mean
The arithmetic mean of any set of values is the summation of the individual values divided by the number of
individual values.
3. Allowable Non-Stormwater Discharges
This permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) All other discharges that are authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and lire hydrant
fleshings, water from footing drains, flows from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -fighting training.
4. Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure.
Parts IV, V and VI Page 1 of 5

Permit No. NCS000150
5. By_pass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
6. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
i. Clean Water Act
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, et. seq.
8. Division or DWO
The Division of Water Quality, Department of Environment and Natural Resources.
9, Director
The Director of the Division of Water Quality, the permit issuing authority.
10, EMC
The North Carolina Environmental Management Commission.
11. Grab Sample
An individual samples collected instantaneously. Grab samples that will be directly analyzed or
qualitatively monitored must be taken within the first 30 minutes of discharge.
12. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
13. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility or
a surface storage facility.
14. Municipal Separate Storm Sewer System
A stormwater collection system within an incorporated area of local self-government such as a city or town.
15. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsoil or similar naturally -occurring surface materials that are not disturbed by mining operations.
Part V I Page 2 of 5 Pages

Permit No. NCS000150
16. Pcrmittee
The owner or operator issued a permit pursuant to this individual permit.
17. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch,
channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to waters
of the state.
18. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours in which no
storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive
hours of no precipitation. For example, if it rains for 2 hours without producing any collectable discharge, and then
stops, a sample may be collected if a rain producing a discharge begins again within the next 10 hours.
19. Representative Outfall Status
When it is established that the discharge of stormwater runoff from a single outfall is representative of the
discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall
status allows the permittee to perform analytical monitoring at a reduced number of outfalls.
20. Rinse Water Discharge
The discharge of rinse water from equipment cleaning areas associated with industrial activity. Rinse
waters from vehicle and equipment cleaning areas are process wastewaters and do not include washwaters
utilizing any type of detergent or cleaning agent.
21. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year, 24-hour storm event.
22. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right -
to -Know Act of 1986;
Is present at or above threshold levels at a facility subject to SARA title 111, Section 313 reporting
requirements; and
C. That meet at least one of the following criteria:
(1) Is listed in Appendix D of 40 CFR part 122 on either Table II (organic priority
pollutants), Table 1I1 (certain metals, cyanides, and phenols) or `fable IV (certain toxic
pollutants and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 31 1(b)(2)(A) of the CWA at 40
CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
Part VI Page 3 of 5 Pages

Permit No. NCS000150
23. Severe Property Damage
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production.
24. Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or production;
hazardous.substances designated under section 101(14) of CERCLA; any chemical the facility is required to
report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes,
slag and sludge that have the potential to be released with stormwater discharges.
25. Significant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CFR 11.0.10 and CFR 117.21) or section 102 of
CERCLA (Ref: 40 CFR 302A).
26. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
27, Stormwater Associated with Industrial_Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacturing, processing or raw material storage areas at an industrial site. Facilities
considered to be engaged in "industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include discharges from facilities or activities excluded from the NPDES program.
28. Stormwater Pollution Prevention Plan
A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution and
is based on an evaluation of the pollution potential of the site.
29. Ten Year Design Storm
The maximum 24 hour precipitation event expected to be equaled or exceeded on the average once in ten
years. Design storm information can be found in the State of North Carolina Erosion and Sediment Control
Planning and Design Manual.
30. Total Flow
The flow corresponding to the time period over which the entire storm event occurs. Total flow shall be
either; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event.
31, Toxic Pollutant
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Part VI Page 4 of 5 Pages

Permit No. NCS000150
32. upset
Means an exceptional incident in which there is unintentional and temporary noncompliance with
technology based permit effluent limitations because of factors beyond the reasonable control of the
permittee. An upset does not include noncompliance to the extent caused by operational error, improperly
designed treatment or control facilities, inadequate treatment or control facilities, lack of preventive
maintenance, or careless or improper operation.
33. Vehicle Maintenance Activity
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or
airport deicing operations.
34. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or ice from its site of origin which can be seen with the unaided eye.
35. 25-year, 24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
Part VI Page 5 of 5 Pages

i
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
Mr. R. W. Humphreys
Neste Resins Corporation
790 Corinth Road
Moncure, North Carolina 27559
Dear Mr. Tybaert:
A74
NORTH CAROLtNA DEFARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
September 17, 1999
Subject: Pei'nt]it N�t�0150
Neste Resin's Corporation
Chatham County
In response to your renewal application for continued coverage under NPDES stormtwater permit
NCS000150, the Division of Water Quality (DWQ) is forwarding herewith the subject state - NPDES permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of
Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983.
Plcase note that the enclosed permit may differ from the draft permit that was previously sent. Based on a
review of the permit monitoring data received to date, the Division has revised the monitoring strategy for individual
storntwatcr Permits. The measurement frequency has been changed and cut-off concentrations have been removed.
These changes will be implemenled for all second term individual storanwater permits with analytical monitoring
requirements. For those permits with analytical monitoring requirements, Part If - Monitoring, Controls, and
Limitations for Permitted Discharges has been modified to reflect the change in monitoring; strategy.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to
you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following; receipt of
this letter. This request must he in the form of a written petition, conforming to Chapter 150B of the North Carolina
General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North
Carolina 27011 -7447. Unless such demand is made, this decision shall be final and hinding;.
Please take notice this permit is not transferable. Part I1I, 13.2. addresses the requirements to he followed in
case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain ether permits which may he required by the
Division of Environmettal Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
I' you have any questions concerning this permit, please contact Tony Evans at telephone number 919/733-
5083 ext. 584.
Sincerely,
&4LCol
for Kerr T. Stevens
cc: Mr. Roger O. Pfau', EPA
Raleigh Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone,919-733-5083 FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Permit No. NCS000150
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Neste Resins Corporation
is hereby authorized to discharge stormwater from a facility located at
Neste Resins Corporation
790 Corinth Road
Moncure, NC
Chatham County
to receiving waters designated as the Haw River, a class WS IV stream, in the Cape Fear River
Basin
in accordance with the discharge limitations, monitoring requirements, and other conditions set
forth in Parts I, II, III, IV, V and VI hereof.
This permit shall become effective October 1, 1999.
This permit and the authorization to discharge shall expire at midnight on March 31, 2001.
Signed this day September 13, 1999.
for Kerr T. Stevens, Director
Division of Water Quality
By the Authority of the Environmental Management Commission

Permit No, NCS000150
TABLE OF CONTENTS
PART 1 INTRODUCTION
Section A: Individual Permit Coverage
Section B: Permitted Activities
Section C: Location Map
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
Section A: Stormwater Pollution Prevention Plan
Section B: Qualitative Monitoring Requirements
Section C: On -Site Vehicle Maintenance Monitoring Requirements
PART III STANDARD CONDITIONS
Section A: Compliance and Liability
1.
Compliance Schedule
2.
Duty to Comply
3.
Duty to Mitigate
4.
Civil and Criminal Liability
5.
Oil and Hazardous Substance Liability
6.
Property Rights
7.
Severability
S.
Duty to Provide Information
9.
Penalties for Tampering
10.
Penalties for Falsification of Reports
Section B: GeneraI Conditions
1.
Individual Permit Expiration
2.
Transfers
3.
Signatory Requirements
d3s
_,..
0

Permit No. NCS000150
4. Individual Permit Modification, Revocation and Reissuance, or
Termination
5. Permit Actions
Section C: Operation and Maintenance of Pollution Controls
I. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D: Monitoring and Records
I.
Representative Sampling
2.
Recording Results
3.
Flow Measurements
4.
Test Procedures
5.
Representative Outfall
b.
Records Retention
7.
Inspection and Entry
Section E: Reporting
Requirements
1.
Discharge Monitoring Reports
2.
Submitting Reports
3.
Availability of Reports
4.
Non-Stormwater Discharges
5.
Planned Changes
6,
Anticipated Noncompliance
7.
Bypass
8.
Twenty-four Hour Reporting
9.
Other Noncompliance
10.
Other Information
PART IV LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
PART VI DEFINITIONS
M

Permit No. NCS000I50
PART I INTRODUCTION
SECTION A: INDIVIDUAL PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified in this permit.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge
stormwater to the surface waters of North Carolina or separate storm sewer system which has
been adequately treated and managed in accordance with the terms and conditions of this
individual permit. All discharges shall be in accordance with the conditions of this permit.
Any other point source discharge to surface waters of the state is prohibited unless it is an
allowable non-stormwater discharge or is covered by another permit, authorization or approval.
This permit does not relieve the permittee from responsibility for compliance with any other
applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree.
66
Part I Pap I of 2

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Permit No. NCS000150
PART It MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
SECTION A: STORMWA'CER POLLUTION PREVENTION PLAN
The permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as
the Plan. This Plan shall be considered public information in accordance with Part I11, Standard
Conditions, Section E, Paragraph 3 of this individual permit. The Plan shall include, at a
minimum, the following items:
1. Site Plan. The site plan shall provide a description of the physical facility and the
potential pollutant sources which may be expected to contribute to contamination of
stormwater discharges. The site plan shall contain the following:
(a) A general location map (USGS quadrangle map or appropriately drafted
equivalent map), showing the facility's location in relation to transportation
routes and surface waters, the name of the receiving water(s) to which the
stormwater outfall(s) discharges, or if the discharge is to a municipal separate
storm sewer system, the name of the municipality and the ultimate receiving
waters, and accurate latitude and longitude of the point(s) of discharge.
(b) A narrative description of storage practices, loading and unloading activities,
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices.
(c) A site map drawn to scale with the distance legend indicating location of
industrial activities (including storage of materials, disposal areas, process areas
and loading and unloading areas), drainage structures, drainage areas for each
outfall and activities occurring in the drainage area, building locations, existing
BMPs and impervious surfaces, and the percentage of each drainage area that is
impervious. For each outfall, a narrative description of the potential pollutants
which could be expected to be present in the stormwater discharge.
(d) A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part 111, Standard Conditions, Section
B, Paragraph 3.
2. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed which control or
min�mrze.the7exposure of significant materials to stormwater, including structural and
unonstructu alkmeasures. The stormwater management plan, at a minimum, shall
incorporate the following:
.F..
rC; '
t
Part 11 Page 1 of 5

Permit No. NCS000150
(a) Feasibility Study. A review of the technical and economic feasibility of changing
the methods of operations and/or storage practices to eliminate or reduce exposure
of materials and processes to stormwater. Wherever practical, the permitlee shall
prevent exposure of all storage areas, material handling operations, and
manufacturing or fueling operations. In areas where elimination of exposure is
not practical, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from areas of potential contamination.
(b) Secondary Containment Schedule. A schedule to provide secondary containment
for bulk storage of liquid materials, storage of Section 313 of Title III of the
Superfund Amendments and Reauthorization Act (SARA) water priority
chemicals, or storage of hazardous substances to prevent leaks and spills from
contaminating stormwater runoff. If the secondary containment devices are
connected directly to stormwater conveyance systems, the connection shall be
controlled by manually activated valves or other similar devices [which shall be
secured with a locking mechanism] and any stormwater that accumulates in the
containment area shall be at a minimum visually observed for color, foam, outfall
staining, visible sheens and dry weather flow, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated by the material stored within the containment area. Records
documenting the individual making the observation, the description of the
accumulated stormwater and the date and time of the release shall be kept for a
period of five years.
(c) BMP Summary. A narrative description shall be provided of Best Management
Practices (BMPs) to be considered such as, but not limited to, oil and grease
separation, debris control, vegetative filter strips, infiltration and stormwater
detention or retention, where necessary. The need for structural BMPs shall be
based on the assessment of potential of sources to contribute significant quantities
of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or team) responsible for implementing the
SPRP shall be identified. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater ninoff through spills or
exposure of materials associated with the facility operations. The SPRP must be site
stormwater specific. Therefore, a SPCC plan may be a component of the SPRP, but may
not be sufficient to completely address the stormwater aspects of the SPRP. The common
elements of the SPCC with the SPRP may be incorporated by reference into the SPRP_
4. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance program shall be developed. The program shall document schedules of
inspections and maintenance activities of stormwater control systems, plant equipment
and systems. Inspection of material handling areas and regular cleaning schedules of
these areas shall be incorporated into the program.
Pare 11 Page 2 of 5

Permit No. NC5000150
5. Employee Training. Training schedules shall be developed and training provided at a
minimum on an annual basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
operations that have the potential to contaminate stormwater runoff. Facility personnel
(or team) responsible for implementing the training shall be identified.
6. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position assignments provided.
7. Plan Amendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance which has a significant effect on the
potential for the discharge of pollutants to surface waters. The Stormwater Pollution
Prevention Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requirements of the permit. Within 30 days of such notice, the permittee shall
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with
Part III, Standard Conditions, Section B, Paragraph 3) to the Director that the changes
have been made.
S. Facility Inspection Program. Facilities are required to inspect all stormwater systems on
at least a semiannual schedule, once in the fall (September -November) and once in the
spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date and time of inspection, individual(s)
making the inspection and a narrative description of the facility's stormwater control
systems, plant equipment and systems. Records of these inspections shall be
incorporated into the Stormwater Pollution Prevention Plan.
Stormwater discharge characteristic monitoring as required in Part II of this permit shall
be performed in addition to facility inspections.
9. Implementation. The permittee shall document all monitoring, measurements,
inspections and maintenance activities and training provided to employees, including the
log of the sampling data and of activities taken to implement BMPs associated with the
industrial activities, including vehicle maintenance activities. Such documentation shall
be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
SECTION B: QUALITATIVE MONITORING REQUIREMENTS
Qualitativednonitoring requires a visual inspection of each Stormwater outfall regardless of
representative outfalbstatus and shalt be performed as specified below in Table 1. Qualitative
mon toying is�for➢the purpose of evaluating the effectiveness of the Stormwater Pollution
Part I1 Page 3 of 5

Permit No. NCS000150
Prevention Plan (SPPP) and assessing new sources of stormwater pollution. No analytical tests
are required. Qualitative monitoring of stormwater outfalls does not need to be performed during
a representative storm event.
In the event an atypical condition is noted at a stormwater discharge outfall, the Permittee shall
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the Stormwater Pollution Prevention
Plan.
All qualitative monitoring will be performed twice per year, once in the spring (April - June) and
once in the fall (September - November).
Table 1. Qualitative Monitoring Requirements
Discharge Chard teristics
7- -. 43 # �4r a vs 4 � ,1
=1 .,�� 3: ��
nI ..
;r Fr•e u ncy r
i:. .:..
��� 5N =
0..
Monitoring.
LocahonA
Color
Semi -Annual
SDO
Odor
Semi -Annual
SDO
Clarity
Semi -Annual
SDO
Floating Solids
Semi -Annual
SDO
Sus ended Solids
Semi -Annual
SDO
Foam
Semi -Annual
SDO
Oil Sheen
Semi -Annual
SDO
Other obvious indicators
of stormwater pollution
Semi -Annual
SDO
Footnotes:
1 Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO)
regardless of representative outfall status.
SECTION C: ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
Facilities which have any vehicle maintenance activity occurring on -site which uses more than
55 gallons of new motor oil per month when averaged over the calendar year shall perform
analytical monitoring as specified below in Table 2. This monitoring shall be performed at all
outfalls which discharge stormwater runoff from vehicle maintenance areas.
All analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of 4 analytical samplings being conducted over the term of
the permit at each stormwater discharge outfall (SDO) which discharges stormwater runoff from
vehicle maintenance areas. The permittee shall complete the minimum 4 analytical samplings in
accordance with the schedule specified in Table 3 .
Part I I Page 4 of 5

Permit No. NCS000150
Table 2. Analytical Monitoring Requirements for On -Site Vehicle Maintenance
DtScharge Charactertsttc5
r >
5 Uitttsr'
•• _
yMeas)urement
� N'?"?':,' .-._
�aSample
�
�Sample��=
a 'tc ��r 7
� F
� �:t R�a�—• a,P tl�
F
i%,, i� t�3as ,n �.
T.. 2 �
��^� •a��', �
L 3
= 'o_
; ^�
+,s re uenc -_
y�
,i e 1
Cation�;�
H
standard
Quarterly- 4`h year
Grab
SDO
Oil and Grease
m l
Quarterly- 4b year
Grab
SDO
Total suspended Solids
m 1
Quarterly- 41h year
Grab
SDO
New Motor Oil Usagegallons/month
Quarterly- 4" year
Estimate
-
Total FI0w4
MG
Quarterly- 4" year
Grab
SDO
Footnotes:
1 Measurement Frequency: Once per quarter during the 4' year of the permit term. A year is defined as the 12
month period beginning on the month and day of issuance of the Permit. See Table 2 for schedule of monitoring
periods.
2 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. If the detention pond discharges only in response
to a storm event exceeding a ten year design storm, then no analytical monitoring is required and only qualitative
monitoring shall be performed.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle maintenance activities occur.
4 Total flow shall be; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall,
the amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the measurement
of flow at 20 minute intervals during the rainfall event. Total precipitation and duration of the rainfall event
measured shall result from the sampled representative storm event.
Table 3 Monitoring schedule (foPermitsissut:d10/0,11..9.9son.l;y:)
t,ar4y �{�.�
M_omf ringjpert('d
'YY �`�•.4 T iy�
Sample Number
,z a" �f�' �art
,w� St
�`f =
.XEnds
Year 4 _ 1" quarter
1
October 1, 1999
December 31, 1999
Year 4 - 2"d quarter
2
January 1, 2000
March 31, 2000
Year 4 - 3" quarter
3
April 1, 2000
Jane 30, 2000
Year 4-4 1h quarter
4
July 1, 2000
September 30, 2000
Part II Page 5 of 5

Permit No. NCS000150
PART III STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented within
12 months of the effective date of the initial permit and updated thereafter on an annual basis. Secondary
containment, as specified in Part II, Section A, Paragraph 2(b) of this permit, shall be accomplished within
12 months of the effective date of the initial permit issuance.
Proposed Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented prior to
the beginning of discharges from the operation of the industrial activity and be updated thereafter on an
annual basis. Secondary containment, as specified in Part I1, Section A, Paragraph 2(b) of this permit shall
be accomplished prior to the beginning of discharges from the operation of the industrial activity.
2. Duty to Comply
The permittee must comply with all conditions of this individual permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit upon renewal application.
a. The permittee shall comply with standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants within the time provided in the regulations that establish these
standards or prohibitions, even if the permit has not yet been modified to incorporate the
requirement.
The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $25,000 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than 1 year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed an administrative penalty not to exceed $10,000 per violation with the maximum
amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33 USC 1319 and 40 CFR
122.41(a). ]
C. Under state law, a daily civil penalty of not more than ten thousand dollars ($10,000) per violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General Statutes 143-215.6A]
d. Any person may be assessed an administrative penalty by the Director for violating section 301,
302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing any
of such sections in a permit issued under section 402 of the Act. Administrative penalties for Class
I violations are not to exceed $10,000 per violation, with the maximum amount of any Class I
penalty assessed not to exceed $25,000. Penalties for Gass 11 violations are not to exceed $10,000
per day for each day during which the violation continues, with the maximum amount of any Class
II penalty not to exceed $125,000.
Part III Page I of 8 Pages

Permit No, NCS000150
Dutv to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the environment.
Civil and Criminal Liability
Except as provided in Part III, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6A, 143-215.6B, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may be subject to
under NCGS 143-215.75 et seq. or Section 3 l 1 of the Federal Act, 33 USC 1321.
6. Property Rights
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
7. Severability
The provisions of this individual permit are severable, and if any provision of this individual permit, or the
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall furnish to the Director, within a reasonable time, any information which the Director
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit. The
permittee shall also furnish to the Director upon request, copies of records required to be kept by this
individual permit.
9. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this individual permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not
more than two years per violation, or by both. If a conviction of a person is for a violation committed after
a first conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per day
of violation, or by imprisonment of not more than 4 years, or both.
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Part 1.11 Page 2 of 8 Pages

Permit No. NCS000150
10. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this individual
permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a tine of not more than $10,000 per violation, or by imprisonment for not more than two years
per violation, or by both.
SECTION B: GENERAL CONDITIONS
Individual Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the permittee shall submit forms and fees as are
required by the agency authorized to issue permits no later than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least I80 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at least l80 days prior to expiration, will be
subjected to enforcement procedures as provided in NCGS § 143-2 t5.6A and 33 USC 125 t et. seq.
2. Transfers
This permit is not transferable to any person except after notice to and approval by the Director. The
Director may require modification or revocation and reissuance of the permit to change the name and
incorporate such other requirements as may be necessary under the Clean Water Act.
3. Signatory Requirements
All applications, reports, or information submitted to the Director shall be signed and certified.
All applications to be covered under this individual permit shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the
manager of one or more manufacturing production or operating facilities employing more
than 250 persons or having gross annual sales or expenditures exceeding 25 million (in
second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager. in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
Part LII Page 3 of 8 Pages

Permit No. NCS000150
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
Any person signing a document under paragraphs a. or b. of this section shall IMAkc the following
certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
4. Individual Permit Modification, Revocation and Reissuance, or Termination
The issuance of this individual permit does not prohibit the Director from reopening and modifying the
individual permit, revoking and reissuing the individual permit, or terminating the individual permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122
and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North Carolina
General Statute 143-215.1 et. a[.
After public notice and opportunity for a hearing, the individual permit may be terminated for cause. The
filing of a request for a individual permit modification, revocation and reissuance, or termination does not
stay any individual permit condition. The permit shall expire when the individual permit is terminated.
5. Permit Actions
The permit may be modified, revoked and reissued, or terminated for cause. The notification of planned
changes or anticipated noncompliance does not stay any individual permit condition.
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the permittee to achieve compliance with
the conditions of this individual permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
2. Need to Halt or Reduce Not a Defense
It shall noj)bc,a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted"yctivity in order to maintain compliance with the condition of this individual permit.
3. Bypassin , of Stormwater Control Facilities
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Part III Page 4 of 8 Pages

Permit No. NCS000150
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
b. There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
weather. This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
C. The permittee submitted notices as required under, Part III, Section E of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may approve an
anticipated bypass after considering its adverse effects.
SECTION D: MONITORING AND RECORDS
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and
nature of the permitted discharge. Analytical sampling shall be performed during a representative storm
event. Samples shall be taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of water, or substance.
Monitoring points as specified in this permit shall not be changed without notification to and approval of
the Director.
2. Recording Results
For each measurement, sample, inspection or maintenance activity performed or collected pursuant to the
requirements of this individual permit, the permittee shall record the following information:
a. The date, exact place, and time of sampling, measurements, inspection or maintenance activity;
b. The individual(s) who performed the sampling, measurements, inspection or maintenance activity;
C. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
Part ll] Page 5 of 8 Pages

Permit No. NCS000150
Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136.
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower reporting level of the procedure.
Representative Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status_ If it is
established that the stormwater discharges are substantially identical and the permittee is granted
representative outfall status, then sampling requirements may be performed at a reduced number of outfalls.
6. Records Retention
Visual monitoring shall be documented and records maintained at the facility along with the Stormwater
Pollution Prevention Plan. Copies of analytical monitoring results shall also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous. monitoring instrumentation, and copies of all
reports required by this individual permit for a period of at least 5 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time.
Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director), or in the case of a facility which discharges through a municipal
separate storm sewer system, an authorized representative of a municipal operator or the separate storm
sewer system receiving the discharge, upon the presentation of credentials and other documents as may be
required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or conducted,
or where records must be kept under the conditions of this individual permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of
this individual permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),
practices, or operations regulated or required under this individual permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
660-'-s
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Part III Page 6 of 8 Pages

Permit No. NCS000150
SECTION E: REPORTING REQUIREMENTS
1. Dischar =e Monitoring Rcports
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be received by the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
Documentation of the qualitative monitoring associated with the initial analytical monitoring event shall be
included with the required analytical monitoring submittal for the first year of the permit coverage.
Analytical results from sampling during the final year of the permit coverage shall be submitted with the
permit renewal application.
2. Submitting Reports
Duplicate signed copies of all reports required herein, shall be submitted to the following address:
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
3. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection
at the offices of the Division of Water Quality. As required by the Act, analytical data shall not be
considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.6E or in Section 309 of the Federal Act.
4. Non-Stormwater Discharges
If the storm event monitored in accordance with this individual permit coincides with a non-stormwater
discharge, the permittee shall separately monitor all parameters as required under the non-stormwater
discharge permit and provide this information with the stormwater discharge monitoring report.
5. Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which could significantly alter the nature or quantity of pollutants discharged. This notification
requirement includes pollutants which are not specifically listed in the individual permit or subject to
notification requirements under 40 CFR Part 122.42 (a).
6. Anticipated Noncompliance
"The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which may result in noncompliance with the individual permit requirements.
Part III Page 7 of 8 Pages

Permit No. NCS000150
Bypass
a. Anticipated bypass_ If the permittee knows in advance of the need for a bypass, it shall submit
prior notice, if possible at least ten days before the date of the bypass; including an evaluation of
the anticipated quality and affect of the bypass.
Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass.
8. Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been received
within 24 hours.
Other Noncompliance
The permittee shall report all instances Of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
10. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in an application for an
individual permit or in any report to the Director, it shall promptly submit such facts or information.
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Part M Page 8 of 8 Pages

Permit No. NCS000150
PART IV LIMITATIONS REOPENER
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) (c), and (d), 304(b) (2) and
307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or approved:
a. Contains different conditions or is otherwise more stringent than any effluent limitation in the individual
permit; or
b. Controls any pollutant not limited in the individual permit.
The individual permit as modified or reissued under this paragraph shall also contain any other requirements in the
Act then applicable.
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed by
the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the Individual Permit.
PART VI DEFINITIONS
Act
See Clean Water Act.
2. Arithmetic Mean
The arithmetic mean of any set of values is the summation of the individual values divided by the number of
individual values.
3. Allowable Non-Stormwater Discharges
This permit regulates stormwater discharges. Nan-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) All other discharges that are authorized by a non-stormwater NPD1?S permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant
flushings, water from footing drains, flows from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -fighting training
4. Best Management Practices BMPs
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure.
Parts IV, V and VI Page I of 5

Permit No. NCSOOO ISO
5. Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
6_ Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
7. Clean Water Act
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, et. seq.
8. Division or DWO
The Division of Water Quality, Department of Environment and Natural Resources.
4. Director
The Director of the Division of Water Quality, the permit issuing authority.
10. EMC
The North Carolina Environmental Management Commission.
11. Grab Sample
An individual samples collected instantaneously. Grab samples that will be directly analyzed or
qualitatively monitored must be taken within the first 30 minutes of discharge.
12. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
13. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility or
a surface storage facility.
14. Municipal Separate Storm Sewer System
A stormwater collection system within an incorporated area of local self-government such as a city or town.
15. Overburden
&By material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsol 6rsun}lar naturally -occurring surface materials that are not disturbed by mining operations.
Part VI Page 2 of 5 Pages

Permit No. NCS000150
16. • Permittee
The owner or operator issued a permit pursuant to this individual permit.
17. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch,
channel, tunnel, conduit, well, or discrete fissure from which Stormwater is or may be discharged to waters
of the state.
18. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours in which no
storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive
hours of no precipitation. For example, if it rains for 2 hours without producing any collectable discharge, and then
stops, a sample may be collected if a rain producing a discharge begins again within the next 10 hours.
19. Representative Outfall Status
When it is established that the discharge of stormwater runoff from a single outfall is representative of the
discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall
status allows the permittee to perform analytical monitoring at a reduced number of outfalls.
20. Rinse Water Discharize
The discharge of rinse water from equipment cleaning areas associated with industrial activity. Rinse
waters from vehicle and equipment cleaning areas are process wastewaters and do not include washwaters
utilizing any type of detergent or cleaning agent.
21. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year, 24-hour storm event.
22. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right -
to -Know Act of 1986;
Is present at or above threshold levels at a facility subject to SARA tide III, Section 313 reporting
requirements; and
That meet at least one of the following criteria:
(1) Is listed in Appendix D of 40 CFR part 122 on either Table 1I (organic priority
pollutants), Table HI (cer(ain metals, cyanides, and phenols) or Table IV (certain toxic
pollutants and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40
CFR 116.4; or
(3) Is a pollutant for which El'A has published acute or chronic water quality criteria.
Part VI Page 3 of 5 Pages

Permit No. NCSOOOt5O
23. Severe Property Damage
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production.
24. Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; Finished materials such as metallic products; raw materials used in food processing or production;
hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required to
report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes,
stag and sludge that have the potential to be released with stormwater discharges.
25. Significant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of.
CERCLA (Ref: 40 CFR 302A),
26, Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
27. Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacturing, processing or raw material storage areas at an industrial site. Facilities
considered to be engaged in 'industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include discharges from facilities or activities excluded from the NPDES program.
28. Stormwater Pollution Prevention Plan
A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution and
is based on an evaluation of the pollution potential of the site.
29. Ten Year Design Storm
The maximum 24 hour precipitation event expected to be equaled or exceeded on the average once in ten
years. Design storm information can be found in the State of North Carolina Erosion and Sediment Control
Planning and Design Manual.
30. Total Flow
The now corresponding to the time period over which the entire storm event occurs. Total flow shall be
either; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event.
31. Toxic Pollutant 66
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Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Part VI Page 4 of 5 Pages

Permit No. NCS000150
32. Upset
Means an exceptional incident in which there is unintentional and temporary noncompliance with
technology based permit effluent limitations because of factors beyond the reasonable control of the
permittee. An upset does not include noncompliance to the extent caused by operational error, improperly
designed treatment or control facilities, inadequate treatment or control facilities, lack of preventive
maintenance, or careless or improper operation.
33. Vehicle Maintenance Activity
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or
airport deicing operations.
34. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or ice from its site of origin which can be seen with the unaided eye.
35. 25-Year, 24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
Part VI Page 5 of 5 Pages

m
COPIES OF PERMIT ARE TO BE SENT TO THE:
FOLLOWING:
Y_ SIGNED ORIGINAL TO THE APPLICANT
SIGNED COPY TO CENTRAL FILES
Cop), -r0 REGIONAL OFFICE?
COPY TO EPA
v`1 COPY -ro P & F FILE:
-\I_ COPY To COMPLIANCE (NO BP)
COPY 'r0 WAKE COUNTY
COPY TO MECKLENBURG COUNTY
COPY TO ESB
COPY To TRAINING & CERT. (No BP)

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. R, W. Humphreys
P.O. Box 259
Moncurc, NC 27559
Dear Mr. Humphreys:
4 ° •
A
F=1
August 26, 1994
Subject: Permit No. NCS000150
Neste Resins Corporation
Chatham County
In accordance with your application for a stormwater discharge permit received on October
27, 1992, we are forwarding herewith the subject state - NPDES permit.. This permit is issued
pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum
of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within
thirty (30) days following receipt of this letter. This request most be in the form of a written
petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the
Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina 27611
-7447. Unless such demand is made, this decision shall be final and binding.
Please take notice this permit is not transferable. Part I1, B.2. addresses the requirements to
be followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be
required by the Division of Environmental Management or permits required by the Division of
Land Resources, Coastal Area. Management Act or any other Federal or Local governmental
permit that may be required.
If you have any questions concerning this permit, please contact 13111 Mills at telephone
number 919/733-5083.
Sincerelyy
Qriginal Signed nV
Coleen H. SWIll"Et;
A. Preston Howard, Jr, P. E.
cc: Mr. Jim Patrick, EPA
Raleigh Regional Office
P.O. Box 29535, Raleigh, North Carolina 27626.0535 , Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycieoi 10% post-consumei paper

Permit No. NCS000150
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
111211"i"VIN
TO DISCHARGE STORMWATER UNDER " `t-11E
NATIONAL POLL!jTAN`1' DISCHARGE ,EL,IMI—NALVION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management Commission,
and the Federal Water Pollution Control Act, as amended,
Neste Resins Corporation
'.} is hereby authorized to discharge stormwater from a facility located at
S.R. 1916
Moncure
Chatham County
to receiving waters designated as Haw River, a class WS-IV stream, in the Cape Fear River Basin
in accordance with the discharge limitations, monitoring requirements, and other conditions set forth in
Pans I, 11, 11I, and IV hereof.
This permit shall become effective October 1, 1994.
This permit and the authorization to discharge shall expire at midnight on August 31, 1999.
Signed this day August 26, 1994.
Original Signed By
Coleen H. Sullins
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By the Authority of the Environmental Management Commission

Permit No. NCS000150
PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge
stormwater to the surface waters of North Carolina or separate storm sewer system which has been
adequately treated and managed in accordance with the terms and conditions of this Permit. All
discharges shall be in accordance with the attached schedules as follows:
Part L• Monitoring, Controls, and Limitations for Permitted Discharges
Part IT: Standard Conditions for NPDES Stormwater Permits
Part IR: Limitations Reopener
Part I.V: Administeiing and Compliance Monitoring Fee Requirements
Any other point source discharge to surface waters of the state is prohibited unless covered by
another permit, authorization or approval.
This permit does not relieve the perm Wee from responsibility for compliance with any other
applicable federal, state, or local law, rule, standard, ordinance, order, judgement, or decree.
Page 2

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Permit No. NCS000150
PART I
MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
SECTION A: FINAL LIMITATIONS AND CONTROLS FOR STORMWATER DISCHARGES
During the period beginning on the effective date of the permit and lasting until expiration, the
Permit= is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified below.
1, StQrmwaterP llui n PLQventionPl n
The Permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as the
Plan. This Plan shall be considered public information in accordance with Part IT, Standard
Conditions, Section E.8. of this permit. The Plan shall include, at a minimum, the following
_7 items:
a. Site Plan. The site plan shall provide a description of the physical facility and the potential
pollutant sources which may be expected to contribute to contamination of stormwater
discharges. The site plan shall contain the following:
(1) A general location map (USGS quadrangle map or appropriately drafted equivalent
map), showing the facility's location in relation to transportation routes and surface
waters, the name of the receiving water(s) to which the stotmwater outfall(s)
discharges, or if the discharge is to a municipal separate storm sewer system, the
name of the municipality and the ultimate receiving waters; and accurate latitude
and longitude of the point(s) of discharge.
(2) A narrative description of storage practices, loading and unloading activities,
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices.
(3) A site map drawn to scale with the distance legend indicating location of industrial
activities (including storage of materials, disposal areas, process areas and loading
and unloading areas), drainage structures, drainage areas for each outfall and
activities occurring in the drainage area, building locations and impervious surfaces,
and the percentage of each drainage area that is impervious. For each outfall, a
narrative description of the potential pollutants which could be expected to be
present in the stormwater discharge.
(4) A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
(5) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part Il, Standard Conditions, Section
B.9.
Page 4

Permit No. NCS000150
b. Stonmwater Management Plan. The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and nonstructural
measures. The stormwater management plan, at a minimum, shall incorporate the
following:
(1) A study addressing the technical and economic feasibility of changing the methods
of operations and/or storage practices to eliminate or reduce exposure of materials
and processes to stormwater. Wherever practicable the permittee shall cover all
storage areas, material handling operations, manufacturing or fueling operations to
prevent materials exposure to stormwater. In areas where elimination of exposure
is not practicable, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from areas of potential contamination.
(2) A schedule to provide secondary containment for bulk storage of liquid materials,
storage of Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) water priority chemicals, or storage of hazardous
materials to prevent leaks and spills from contaminating stormwater runoff. If the
secondary containment devices are connected directly to stormwater conveyance
systems, the connection shall be controlled by manually activated valves or other
similar devices [which shall be secured with a locking mechanism] and any
stormwater that accumulates in the containment area shall be at a minimum visually
observed for color, foam, and visible sheens, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated. Records documenting the individual making the observation, the
description of the accumulated stormwater and the date and time of the release shall
be kept for a period of five years.
(3) A narrative description shall be provided of Best Management Practices (BMPs) to
be considered such as, but not limited to, oil and grease separation, debit's control,
vegetative filter strips, infiltration and stormwater detention or retention, where
necessary_ The need for structural BMPs shall be based on the assessment of
potential of sources to contribute significant quantities of pollutants to stormwater
discharges and data collected through monitoring of stormwater discharges.
(4) Inspection schedules of stormwater conveyances and controls and measures to be
taken to limit or prevent erosion associated with the stormwater systems.
Spill Prevention and Response Plan. The Spill Prevention and Response Plan shall
incorporate a risk assessment of potential pollutant sources based on a materials inventory
of the facility. Facility personnel (or team) responsible for implementing the plan shall be
identified in the plan. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater runoff through spills or
exposure of materials associated with the facility operations.
d. Preventative Maintenance and Good Housekeeping Program. A preventative maintenance
program shall be developed. The program shall document schedules of inspections and
maintenance activities of stormwater control systems, plant equipment and systems.
Inspection of material handling areas and regular cleaning schedules of these areas shall be
incorporated into the program.
e. EmpIoyee Training. Training schedules shall be developed and training provided at a
minimum on an annual basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
Page 5

Permit No. NCS000150
operations that have the potential to contaminate stormwater runoff. Facility personnel (or
team) responsible for implementing the training shall be identified in the Plan.
Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position(s) assignments provided.
g. Plan Ammendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance which has a significant effect on the
potential for the discharge of pollutants to surface waters. The Stormwater Pollution
Prevention Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requirements of the permit. Within 30 days of such notice, the permittee shall
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with Part
I.t, Standard Conditions; Section B, #9) to the Director that the changes have been made.
It . Facility Inspections. Inspections of the facility and all stormwater sysyns shall occur at a
minimum on a semiannual schedule, once in the fall (September -November) and once
during the spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date and time of inspection, individual(s)
malting the inspection and a narrative description of the facility's stormwater control
systems, plant equipment and systems. Records of these inspections shall be, incorporated
into the Stormwater Pollution Prevention Plan.
Visual monitoring as required in I.A.2.9.(3) shall be performed in addition to facility
inspections.
i. Implementation. Implementation of the plan shall include documentation of all monitoring,
measurements, inspections and maintenance activities and training provided to employees,
including the log of the sampling data and of activities taken to implement BMPs associated
with the industrial activities, including vehicle maintenance activities. Such documentation
shall be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
Page 6

Permit No. NCS000150
2. Minimum Monitoring and Reporting Requirements
Minimum monitoring and reporting requirements are as follows unless otherwise approved in
writing by the Director of the Division of Environmental Management.
a. If a facility has multiple discharge locations with substantially identical stormwater
discharges that are required to be sampled, the permittee may petition the Director for
representative outfall status. If it is established that the stonnwawr discharges are
substantially identical and the permittee is granted representative outfall status, then
sampling requirements may be performed at a reduced number of outfal.ls.
b. Visual monitoring for color, odor, solids, foam, outfall staining, visible sheens and dry
weather flow shall be performed at all stormwater discharge outfall locations. All visual
monitoring shall be documented and records maintained with the stormwater Pollution
Prevention Plan. The initial visual monitoring event shall be performed simultaneously
with the first analytical monitoring event and documentation of only this initial visual
monitoring event shall be submitted along with the required analytical monitoring submittal.
C. For purposes of the stormwater sampling required in this permit, all samples shall be
collected from a discharge resulting from•ajdpresentative storm event (See fart 11,
Standard Conditions, Section A). Failure to monitor storm events in accordance with the
specified frequency shall constitute a violation of this permit. If the stormwater runoff is
controlled by,a detention pond, the following sampling requirements shall apply:
(1) If the detention pond detains the runoff generated by one inch of rainfall for 24
hours, visual observations for color, foam, outfall staining, visible sheens, and dry
weather flow are required, but analytical sampling shall not be required.
(2) If the detention pond discharges only in response to a storm event exceeding a 25-
year, 24-hour storm (See Part H, Standard Conditions, Section A), the pond shall
be considered a non -discharging stormwater control system and not'subject to
NPDES requirements, unless the discharge causes a violation of water quality
standards.
d . Samples analyzed in accordance with the terms of this permit shall be submitted on forms
provided by the Director no Iater than January 31 for the previous year in which sampling
was required to be performed.
e. Analytical results from sampling during the final year of the permit tenn shall be submitted
with the permit renewal application.
f, This permit regulates stormwater discharges. Non-stormwater discharges which shall be
allowed in the stormwater conveyance system are:
(1) All other discharges that are authorized by a non-stormwater NPDES permit.
(2) Uncontaminated groundwater, foundation drains, air -conditioner condensate
without added chemicals, springs, discharges of uncontaminated potable water,
waterline and fire hydrant flushings, water from footing drains, flows from riparian
habitats and wetlands.
(3) Discharges resulting from fire -fighting.
Page 7

Permit No. NCS000150
If the stone event monitored and reported in accordance with this permit coincides with a
non-stormwater discharge, the permittee shall separately monitor and report all parameters
as requited under the non-stormwater discharge permit and provide this information with
the stormwater discharge monitoring report.
g. Specific Stormwater Monitoring Requirements
The specific stormwater monitoring requirements includes visual monitoring of stormwater
samples. Specific monitoring requirements are defined below.
(1) Visual Monitoring
Visual monitoring requires a qualitative visual inspection of each stormwater outfall, regardless
of representative outfall status, for the purpose of evaluating the effectiveness of. the
Stormwater Pollution Prevention Plan (SPPP) and assessing new sources of stormwater
pollution. No analytical tests are required. Visual monitoring of stormwater outfalls does not
need to be performed during a representative storm event.
Stormwater Discharge
h i' i•
F e n 1
Monitoring
T 2
Monitorbig
Lcx ation3
Color
Semi -Annual
Visual
SDO
Odor
Semi -Annual
Visual
SDO
Clarity
Semi -Annual
Visual
SDO
Floating Solids
Semi -Annual
Visual
SDO
Suspended Solids
Semi -Annual
Visual
SDO
Foam
Semi -Annual
Visual
SDO
Oil Sheen
Semi -Annual
Visual
SEO
Other obvious indicators
of stormwater pollution j
Semi -Annual
Visual
I
SDO
I I
Footno-es:
1 Frequency: The first visual monitoring event during the term of the permit must be
performed during the initial analytical monitoring event. AH subsequent visual
monitoring will be performed twice per year, once in the spring and once in the fall.
2 Monitoring Type: Visual monitoring requires a qualitative visual observation of each
stormwater outfall. No analytical testing or sampling is required.
3 Sample Location: Stormwater Discharge Outfall (SDO)
Page 8

Permit No. NCS000150
(2) Analytical Monitoring Requirements for Vehicle Maintenance Activitiesl
Stormwater Discharge
CharactQristjcanit
Measurement
r n 2
Sample
TYP
Sample
Lox,ation3
H
standard
annually
Grab
SDO
Oil and Grease
mg1I
annually
Grab
SDO
New Motor Oil Usage
7allonVmonth
annually
Estimate;
SDO
Total Flow4
MG
annually
Grab
SDO
Lead, Total Recoverable5
u +
annually
Grab
SDO
Total Suspended Solids
mo
annually
Grab
SDO
Detergents (MBAS)6
m tr11
annually
Grab
SDO
Footnotes:
l Stormwater discharges from any vehicle maintenance activity occurring on -site
which uses more than 55 gallons of new motor oil per month when averaged over
the calendar year shall be monitored by the permittee as specified above.
2 Measurement Frequency. Once per year with samples taken within the sampling
window of April through November,
3 Sample Location: Samples to be taken at each storrnwater discharge
outfall (SDO) than discharges stormwater runoff from area(s) where
vehicle maintenance activities occur.
4 Total flow shall be; (a) measured continuously, (b) calculated based on the amount
of area draining to the outfall, the amount of built -upon (impervious) area, and the
total amount of rainfall, or (c) estimated by the measurement of flow at 20 minute
intervals during the rainfall event. Total Precipitation and duration of the rainfall
event measured shall result from the sampled representative storm event.
5 Total recoverable lead monitoring is required only at facilities where fueling occurs.
6 Detergent monitoring is required only at facilities which conduct vehicle cleaning
operations.
(3) - Cut-off Concentrations for Vehicle Maintenance Activities
The arithmetic mean of all analytical sampling results collected during the term of the permit
shall be calculated for each parameter and compared to the cut-off concentrations listed below.
If the arithmetic mean meets the specified cut-off concentration condition for a given parameter,
then the facility is not required to continue annual analytical monitoring for that parameter
during the term of the pen -nit unless a significant change in facility operations or configuration
occurs. If a cut-off concentration results in discontinued analytical monitoring, the permittee is
Page 9

Permit No. NCS000150
required to maintain facility operations that ensure the continuation of stormwater runoff
duality.
The permittee must perform analytical sampling during the first and last year of the permit term
regardless of cut-off concentration conditions. Analytical results from sampling during the
final year of the permit term must be submitted with the permit renewal application.
Storrnw,itcr Diaghijrharacteristio
Cut-off Concentration
E-11
within range 6.0 - 9.0
Oil and Grease
< 30 m
Lead, Total Recoverable
< 0.033 mFZI
Total Suspended Solids
< 100 m
Detergents (MBAS)
< 0.50 mg/1
Footnotes:
1 pl i cannot be averaged due to the nature of the logarithmic pH scale. The most recent pH
sample result shall be used for cut-off concentration purposes.
Page 10

Permit No. NCS000150
SECTION B: SCHEDULE OF COMPLIANCE
1. The permittee shall comply with Final Limitations and Controls specified for stormwater
discharges in accordance with the following schedule:
The Stormwater Pollution Prevention Plan shall be developed and implemented within 12
months of the effective date of this permit and updated thereafter on an annual basis.
Secondary containment, as specified in Part I, Section A, I. b. 2. of this permit, shall be
accomplished within 12 months of the effective date of this permit.
2. Permittee shall at all times provide the operation and maintenance necessary to operate the
pennitted stormwater controls at optimum efficiency.
palge I 1

Individual Stormwater Page Al
PART II
STANDARD CONDITIONS FOR NPDES STORMWATER PERMITS
r• • _a W II
: • 1' :r,a :
The Federal Water Pollution Control Act, also known as the Clean Water Act, as
amended, 33 USC 1251, et. seq.
►���.� n r ;P. :uP
Schedules of activities, prohibitions of practices, maintenance procedures, and
other management practices to prevent or reduce the pollution of waters of the
United States. BMPs also include treatment requirements, operation procedures,
and practices to control plant site runoff, spillage or leaks, sludge or waste
disposal, or drainage from raw material storage.
Means shall be calculated according to the following definitions:
a. Arithmetic Mean: The arithmetic mean of any set of values is the summation
of the individual values divided by the number of individual values.
b . Geometric Mean: The geometric mean of any set of values is the Nth root
of the product of the individual values where N is equal to the number of
individual values. The geometric mean is equivalent to the antilog of the
arithmetic mean of the Iogarithms of the individual values. For purposes of
calculating the geometric mean, values of zero (0) shall be considered to be
one (1).
C. Weighted by Flow Value. Weighted by flow value means the summation of
each concentration times its respective flow divided by the summation of the
respective flows.
rMTOININT,
Liquid raw materials, manufactured products, waste materials or by-products with a
single above ground storage container having a capacity of greater than 660 gallons
or with multiple above ground storage containers having a total storage capacity of
greater than 1,320 gallons.
5. Calendar Dav
The period from midnight of one day until midnight of the next day. However, for
purposes of this permit, any consecutive 24-hour period that reasonably represents
the calendar day may be used for sampling.
•, k - : iej
The rainfall runoff from or through any coal storage pile.

Individual Stormwater Page A2
anoffs. • •,
The Division of Environmental Management, Department of Environment, Health
and Natural Resources.
The Director of the Division of Environmental Management, the permit issuing
authority.
NNIMPTUR
The North Carolina Environmental Management Commission.
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the
Clean Water Act.
11. Land
A disposal facility or part of a disposal facility where waste is placed in or on land
and which is not a land treatment facility, a surface impoundment, an injection well,
a hazardous waste long-term storage facility or a surface storage facility.
All municipal separate storm sewers that are either:
a. Located in an incorporated place with a population of 100,000 or more as
determined by the Decennial Census by the Bureau of Census; or
b. Located in the counties with unincorporated urbanized populations of
100,000 or more, except municipal separate storm sewers that are located in
the incorporated places, townships or towns within such counties; or
c. Owned or operated by a municipality other than those described in
paragraph (a) or (b) and that are designated by the Director as part of the
large or medium separate storm sewer system.
13. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral
deposit, excluding topsoil or similar naturally -occurring surface materials that are
not disturbed by mining operations.
The owner or operator issued a permit.
Any discernible, confined and discrete conveyance, including but specifically not
limited to, any pipe, ditch, channel, tunnel, conduit, well, discrete fissure,

Individual Stormwater Page A3
container, rolling stock, or concentrated animal feeding operation from which
pollutants are or may be discharged to waters of the state.
A storm event that is between 0.2 and 0.8 inches of rainfall and which has a
duration of greater than 3 hours and that is preceded by at least 72 hours in which
no storm event measuring greater than 0.1 inches has occurred.
The fraction of total rainfall that is not infiltrated into or otherwise retained by the
soil, concrete, asphalt or other surface upon which it falls that will appear at the
conveyance as runoff.
Spill containment for the contents of the single largest tank within the containment
structure plus sufficient freeboard to allow for the 25-year, 24-hour storm event.
A chemical or chemical category which:
Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the
Superfund Amendments and Reauthorization Act (SARA) of 1986, also
titled the Emergency Planning and Community Right -to -Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III,
Section 313 reporting requirements; and
c . That meet at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on either Table n
(organic priority pollutants), Table III (certain metals, cyanides, and
phenols) or Table IV (certain toxic pollutants and hazardous
substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A)
of the CWA at 40 CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water
quality criteria.
Includes, but is not limited to: raw materials; fuels; materials such as solvents,
detergents, and plastic pellets; finished materials such as metallic products; raw
materials used in food processing or production; hazardous substances designated
under section 10104) of CERCLA; any chemical the facility is required to report
pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste
products such as ashes, slag and sludge that have the potential to be released with
stormwater discharges.

Individual Stormwater Page A4
21. Significant 1!U
Includes, but is not limited to: releases of oil or hazardous substances in excess of
reportable quantities under section 311 of the Clean Water Act (Ref: 40 CFR
110.10 and CFR 117.71) brxection"10'Z of CERCLA (Ref: 40 CFR 302.4).
The flow of water which results from precipitation and which occurs immediately
following rainfall or as a result of snowmelt.
The discharge from any point source which is used for collecting and conveying
stormwater and which is directly related to manufacturing, processing or raw
material storage areas at an industrial site. The term does not include discharges
from facilities or activities excluded from the NPDES program.
The following categories of facilities are considered to be engaging in "industrial
activity":
a. Facilities subject to stormwater effluent limitations guidelines, new source
performance standards, or toxic pollutant effluent standards under 40 CFR
Subchapter lei Parts 400 - 471 (except facilities which are exempted under
(k) of this definition);
b . Facilities classified as Standard Industrial Classifications 24 (except 2434),
26 (except 265 and 267), 28, 29, 30, 311, 32, 33, 3441, 373;
C. Facilities classified as Standard Industrial Classifications 10 through 14
(mineral industry) including active or inactive mining operations (except for
areas of coal mining operations meeting the definition of a reclamation area
under 40 CFR 434.11(1)) and oil and gas exploration, production,
processing, or treatment operations, or transmission facilities that discharge
stormwater contaminated by contact with or that has come in contact with,
any overburden, raw material, intermediate products, finished products,
byproducts or waste products located on the site of such operations; inactive
mining operations are mining sites that are not being actively rained, but
which have an identifiable owner/operator;
d. Hazardous waste treatment, storage, or disposal facilities, including those
that are operating under interim status or a permit under Subtitle C of
RCRA;
e. Landfills, land application sites, and open dumps that receive or have
received any industrial wastes (waste that is received from any of the
facilities described under this definition) including those that are subject to
regulation under Subtitle D of RCRA;
f. Facilities involved in the recycling of materials, including metal scrapyards,
battery reclaimers, salvage yards and automobile junkyards, including but
limited to those classified as Standard Industrial Classification 5015 and
5093;

Individual Stormwater Page A5
g. Steam electric power generating facilities, including coal handling sites;
h. Transportation facilities classified as Standard industrial Classifications 40,
41, 42, 44, and 45 which have vehicle maintenance shops, equipment
cleaning operations, or airport deicing operations. Only those portions of
the facility that are either involved in vehicle maintenance (including vehicle
rehabilitation, mechanical repairs, painting, fueling and lubrication),
equipment cleaning operations, airport deicing operations, or which are
otherwise identified under (a)-(g) or (i)-(k) of this definition are associated
with industrial activity;
i. Treatment works treating domestic sewage or any other sewage sludge or
wastewater treatment device or system, used in the storage treatment,
recycling, and reclamation of municipal or domestic sewage, including
lands dedicated to the disposal of sewage sludge that are located within the
confines of the facility, with a design flow of 1.0 mgd or more, or required
to have an approved pretreatment program under 40 CFR part 403. Not
included are farm lands, domestic gardens or lands used for sludge
management where sludge is beneficially reused and which are not
physically located in the confines of the facility, or areas that are in
compliance with section 405 of the CWA;
j. Construction activity including clearing, grading and excavation activities
except: operations that result in the disturbance of less that five acres of total
land area which are not part of a larger common plan of development or
sale;
k. Facilities under Standard Industrial Classifications 20, 21, 22, 23, 2434,
25, 265, 267, 27, 283, 285, 30, 31 (except 311), 323, 34 (except 3441),
35, 36, 37 (except 373), 38, 39, 4221-25, (and which are not otherwise
included within (a)-0) of this definition).
For the categories of industries identified in (a) through 0) of this definition the
term includes, but is not limited to, stormwater discharges from industrial plant
yards; immediate access roads and rail lines used or traveled by carriers of raw
materials, manufactured products, waste material, or by-products used or created
by the facility; material handling sites; refuse sites; sites used for the application or
disposal of process wastewaters; sites used for the storage and maintenance of
material handling equipment; sites used for residual treatment, storage, or disposal;
shipping and receiving areas; manufacturing buildings; storage areas (including tank
farms) for raw materials, and intermediate and finished products; and areas where
industrial activity has taken place in the past and significant materials remain and are
exposed to stormwater. For the categories of industries identified in (k), the term
includes only stormwater discharges from all areas listed in the previous sentence
(except access roads) where material handling equipment or activities, raw material,
intermediate products, final products, waste material, by-products, or industrial
machinery are exposed to stormwater.
Material handling activities include the: storage, loading and unloading,
transportation, or conveyance of any raw material, intermediate product, finished
product, by-product or waste product. The term excludes areas located on plant
lands separated from the plant's industrial activities, such as office buildings and
accompanying parking lots as Iong as the drainage from the excluded areas is not
mixed with stormwater drained from the above described areas.

Individual Stormwater Page A6
Industrial facilities (including industrial facilities that are Federally or municipally
owned or operated that meet the description of the facilities listed in (a)-(k)) include
those facilities designated under 40 CFR 122.26(a)(1)(v).
The precipitation event of a duration which will produce the maximum peak rate of
runoff for the watershed of interest resulting from a rainfall event of an intensity
expected to be equaled or exceeded, on the average, once in ten years.
NUMERMI ._ 2 0
The flow corresponding to the time period over which the sample collection occurs.
The total flow calculated based on the size of the area draining to the outfall, the
amount of the built -upon (impervious) surfaces within the drainage area, and the
total amount of rainfall occurring during the sampling period.
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Grab samples are individual samples collected instantaneously. Grab samples that
will be directly analyzed or visually monitored must be taken within the first 30
minutes of discharge. Grab samples for compositing purposes must be collected at
no greater than 20 minute intervals.
b. Composite Sample. a composite sample shall mean:
(1) A flow -weighted composite sample, which is a mixture of aliquots collected
at a constant time interval, where the volume of each aliquot is proportional
to the flow rate of the discharge at the time the sample is collected; or
(2) A time -weighted composite sample, which is a mixture of equal volume
aliquots collected at a constant interval of time.
A composite sample can be obtained from the collection of a series of grab samples,
taken at intervals of no greater than 20 minutes for the entire storm event or the first
three hours of the storm event. The grab sample to be composited must be of no
less than 100 milliliters.
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle
cleaning operations, or airport deicing operations.
Solid particulate matter, both mineral and organic, that has been or is being
transported by water; air, -gradity;,orkr,from- its site of origin which can be seen
with the unaided eye.

Individual Stormwater Page A7
30. Waste Pile
Any non -containerized accumulation of solid, non -flowing waste that is used for
treatment or storage.
MoMMIe WWt
The maximum 24-hour precipitation event expected to be equaled or exceeded, on
the average, once in'25 years.

Individual Stormwater Page A8
1. Duty to Coma
The permittee must comply with all corrditionrof this permit: Any permit
noncompliance constitutes a violation of the Clean Water Act and is grounds for
enforcement action; for permit termination, revocation and reissuance, or
modification; or denial of a permit renewal application.
a. The permittee shall comply with effluent standards or prohibitions established
under section 307(a) of the Clean Water Act for toxic pollutants within the time
provided in the regulations that establish these standards or prohibitions, even if the
permit has not yet been modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates a permit condition is
subject to a civil penalty not to exceed $25,000 per day for each violation. Any
person who negligently violates any permit condition is subject to criminal penalties
of $2,500 to $25,000 per day of violation, or imprisonment for not more than 1
year, or both. Any person who knowingly violates permit conditions is subject to
criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment for
not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed an administrative penalty not to exceed $10,000 per violation with
the maximum amount not to exceed $125,000. [Ref: Section 309 of the Federal Act
33 U SC 1319 and 40 CFR 122.41(a).]
C. Under state law, a daily civil penalty of not more than ten thousand dollars
(S10,000) per violation may be assessed against any person who violates or fails to
act in accordance with the terms, conditions, or requirements of a permit. [Ref:
North Carolina General Statutes 143-215.6A]
d . Any person may be assessed an administrative penalty by the Administrator for
violating section 301, 302, 306, 307, 308, 318, or 405 of the Act, or any permit
condition or limitation implementing any of such sections in a permit issued under
section 402 of the Act. Administrative penalties for Class I violations are not to
exceed $10,000 per violation, with the maximum amount of any Class I penalty
assessed not to exceed $25,000. Penalties for Class H violations are not to exceed
$10,000 per day for each day during which the violation continues, with the
maximum amount of any Class H penalty not to exceed $125,000.
The permittee shall take all reasonable steps to minimize or prevent any discharge in
violation of this permit which has a reasonable likelihood of adversely affecting
human health or the environment.
e_I o_I! _! • • M M
Except as provided in permit conditions on "Bypassing" (Part H, C.3.), nothing in
this permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3,143-215.6A,
143-215.6B, 143-215.6C or Section 309 of the Federal Act, 33 USC 1319.
Furthermore; the permittee is responsible for -consequential damages, such as fish
kills, even though the responsibility for effective compliance may be temporarily
suspended.

Individual Stormwater Page A9
Nothing in this permit shall be construed to preclude the institution of any legal
action or relieve the permittee from any responsibilities, liabilities, or penalties to
which the permittee is or may be subject to under NCGS 143-215.75 et seq. or
Section 311 of the Federal Act, 33 USC 1321. Furthermore, the permittee is
responsible for consequential damages, such as fish kills, even though the
responsibility for effective compliance may be temporarily suspended.
The issuance of this permit does not convey any properly rights in either real or
personal property, or any exclusive privileges, nor does it authorize any injury to
private property or any invasion of personal rights, nor any infringement of
Federal, State or local laws or regulations.
r-� �1M
The provisions of this permit are severable, and if any provision of this permit, or
the application of any provision of this permit to any circumstances, is held invalid,
the application of such provision to other circumstances, and the remainder of this
permit, shall not be affected thereby.
The permittee shall furnish to the Director, within a reasonable time, any
information which the Director may request to determine whether cause exists for
modifying, revoking and reissuing, or terminating this permit or to determine
compliance with this permit. The permittee shall also furnish to the Director upon
request, copies of 'records required to be kept by this permit.
4 • I
The permittee is not authorized to discharge after the expiration date. In order to
receive automatic authorization to discharge beyond the expiration date, the
permittee shall submit such information, forms, and fees as are required by the
agency authorized to issue permits no later than 180 days prior to the expiration
date. Any permittee that has not requested renewal at least 180 days prior to
expiration, or any permittee that does not have a permit after the expiration and has
not requested renewal at least 180 days prior to expiration, will be subjected to
enforcement procedures as provided in NCGS §143-2153.6 and 33 USC 125I et.
seq.
' -4 We WARM14124111411
All applications, reports, or information submitted to the Director shall be signed
and certified.
a. All applications shall be signed as follows:
{1} For a corporation: by a responsible corporate officer. For the purpose of
this Section, a responsible corporate officer means: (a) a president,
secretary, treasurer or vice president of the corporation in charge of a

Individual Stormwater Page A10
principal business function, or any other person who performs similar
policy or decision making functions for the corporation, or (b) the manager
of one or more manufacturing production or operating facilities employing
more than 250 persons or having gross annual sales or expenditures
exceeding 25 miihon-(in second quarter 1980 dollars), if authority to sign
documents has been assigned or delegated to the manager in accordance
with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the
proprietor, respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a
principal executive officer or ranking elected official.
b. All reports required by the permit and other information requested by the Director
shall be signed by a person described above or by a duly authorized representative
of that person. A person is a duly authorized representative only if:
0) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having
responsibility for the overall operation of the regulated facility or activity,
such as the position of plant manager, operator of a well or well field,
superintendent, a position of equivalent responsibility, or an individual or
position having overall responsibility for environmental matters for the
company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
c. Any person signing a document under paragraphs a. or b. of this section shall make
the following certification:
"i certify, under penalty of law, that this document and all attachments were
prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who
manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
The issuance of this permit does not prohibit the Director from reopening and
modifying the permit, revoking and reissuing the permit, or terminating the permit
as allowed by the laws, rules, and regulations contained in Title 40, Code of
Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code, Subchapter 2H .0100; and North Carolina General Statute
143-215.1 et. al.

Individual Stormwater Page Al
This permit may be modified, revoked and reissued, or terminated for cause. The
notification of planned changes or anticipated noncompliance does not stay any
permit condition.
•»• •• :: r• i �:�.rr� • •• 19r• • Z11111MIM
The permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or
used by the permittee to achieve compliance with the conditions of this permit.
Proper operation and maintenance also includes adequate laboratory controls and
appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee
only when the operation is necessary to achieve compliance with the conditions of
the permit.
It shall not be a defense for a permittee in an enforcement action that it would have
been necessary to halt or reduce the permitted activity in order to maintain
compliance with the condition of this permit_
a. Definitions
(1) "Bypass" means the known diversion of stormwater from any portion of a
stormwater control facility including the collection system, which is not a
designed or established or operating mode for the facility.
(2) "Severe property damage" means substantial physical damage to property,
damage to the control facilities which causes them to become inoperable, or
substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does
not mean economic loss caused by delays in production. -
b. Bypass Not Exceeding Limitations.
The permittee may allow any bypass to occur which does not cause limitations to be
exceeded, but only if it also is for essential maintenance to assure efficient
operation. These bypasses are not subject to the provisions of Paragraphs c. and d.
of this section.
C. Notice
{1} Anticipated bypass. If the permittee knows in advance of the need for a
bypass, it shall submit prior notice, if possible at least ten days before the
date of the bypass; including an evaluation of the anticipated quality and
affect of the bypass.

Individual 5tormwater Page Al2
(2) Unanticipated bypass. The permittee shall submit notice within 24 hours of
an unanticipated bypass as required in Pan II, E. 5. of this permit. (24-
hour notice).
d. Prohibition of Bypass
Bypass is prohibited and the Director may take enforcement action against a
permittee for bypass, unless:
(1) Bypass was unavoidable to prevent loss of life, personal injury or severe
property damage;
(2) There were no feasible alternatives to the bypass, such as the use of
auxiliary control facilities, retention of stormwater or maintenance during
normal periods of equipment downtime or dry weather. This condition is
not satisfied if adequate backup controls should have been installed in the
exercise of reasonable engineering judgment to prevent a bypass which
occurred during normal periods of equipment downtime or preventive
maintenance; and
(3) The permittee submitted notices as required under Paragraph c. of this
section.
The Director may approve an anticipated bypass, after considering its adverse
effects, if the Director determines that it will meet the three conditions listed above
in Paragraph d. of this section.
4. Upsets
a. Definition
"Upset " means an exceptional incident in which there is unintentional and
temporary noncompliance with technology based permit effluent limitations
because of factors beyond the reasonable control of the permittee. An upset does
not include noncompliance to the extent caused by operational error, improperly
designed treatment or control facilities, inadequate treatment or control facilities,
lack of preventive maintenance, or careless or improper operation.
b. Effect of an Upset.
An upset constitutes an affirmative defense to an action brought for noncompliance
with technology based permit effluent limitations if the requirements of paragraph c.
of this condition are met_ No determination made during administrative review of
claims that noncompliance was caused by upset, and before an action for
noncompliance, is final administrative action subject to judicial review.
C. Conditions Necessary for a Demonstration of Upset
A permittee who wishes to establish the affirmative defense of upset shall
demonstrate, through properly signed, contemporaneous operating logs, or other
relevant evidence that:..
{ 1) An upset occurred and that the permittee can identify the cause(s) of the
upset;

Individual Stormwater Page A13
(2) The permitted facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Part H, E. 5. (b)
(B) of this permit.
(4) The permittee complied with any remedial measures required under Part II,
A. 2. of this permit.
d . Burden of Proof
In any enforcement proceeding the permittee seeking to establish the occurrence of
an upset has the burden of proof.
Samples collected and measurements taken, as required herein, shall be
characteristic of the volume and nature of the permitted discharge. Samples shall be
taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of
water, or substance. Monitoring points shall not be changed without notification to
and approval of the Director.
somm ;-•er
Duplicate signed copies of all reports required herein, shall be submitted to the
following address:
Division of Environmental Management
Water Quality Section
ATTENTION; Central Files
Post Office Box 29535
Raleigh, North Carolina 27626-0535
Where required, appropriate flow measurement devices and methods consistent
with accepted scientific practices shall be selected and used to ensure the accuracy
and reliability of measurements of the volume of monitored discharges.
Test procedures for the analysis of pollutants shall conform to the EMC regulations
published pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality
Reporting Acts, and to regulations published pursuant to Section 304(g), 33 USC
1314, of the Federal Water Pollution Control Act, as Amended, and Regulation 40
CFR 136.
To meet the intent of the monitoring required by this permit, all test procedures
must produce minimum detection and reporting levels that are below the permit
discharge requirements and all data generated must be reported down to the
minimum detection or lower reporting level of the procedure. If no approved

Individual Stormwater Page A14
methods are determined capable of achieving minimum detection and reporting
levels below general permit discharge requirements, then the most sensitive
(method with the lowest possible detection and reporting level) approved method
trust be used.
The Clean Water Act provides that any person who falsifies, tampers with, or
knowingly renders inaccurate, any monitoring device or method required to be
maintained under this permit shall, upon conviction, be punished by a fine of not
more than $10,000 per violation, or by imprisonment for not more than two years
per violation, or by both. If a conviction of a person is for a violation committed
after a first conviction of such person under this paragraph, punishment is a fine of
not more that $20,000 per day of violation, or by imprisonment of not more than 4
years, or both.
The permittee shall retain. records of all monitoring information, including all
calibration and maintenance records and all original strip chart recordings for
continuous monitoring instrumentation, copies of all reports required by this
permit, for a period of at least S years from the date of the sample, measurement,
report or application. This period may be extended by request of the Director at any
time.
For each measurement, sample, inspection or maintenance activity performed or
taken pursuant to the requirements of this permit, the permittee shall record the
Mowing information:
a. The date, exact place, and time of sampling, measurements, inspection or
maintenance activity;
b. The individual(s) who performed the sampling, measurements, inspection
or maintenance activity;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
FAMEff Il . e ..1 .
The permittee shall allow the Director, or an authorized representative (including an
authorized contractor acting as a representative of the Director), or in the case of a
facility which discharges through a municipal separate storm sewer system, an
authorized representative of a municipal operator.or the separate storm sewer
system receiving the discharge, upon the presentation of credentials and other
documents as may be required by law, to;

Individual Stormwater Page A15
a. Enter upon the permittee's premises where a regulated facility or activity is
located or conducted, or where records must be kept under the conditions of
this permit;
b . Have access to and copy, at reasonable tunes, any records that must be kept
under the conditions of this permit;
c . Inspect at reasonable times any facilities, equipment (including monitoring
and control equipment), practices, or operations regulated or required under
this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit
compliance or as otherwise authorized by the Clean Water Act, any
substances or parameters at any location.
mwm 201 a Ian: • f!: ul
The permittee shall give notice to the Director as soon as possible of any planned
physical alterations or additions to the permitted facility. Notice is required only
when:
a. The alteration or addition to a permitted facility may meet one of the criteria
for determining whether a facility is a new source in 40 CFR Para 122.29
(b); or
b. The alteration or addition could significantly change the nature or increase
the quantity of pollutants discharged. This notification applies to pollutants
which are subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR Part 122.42 (a) (1).
The permittee shall give advance notice to the Director of any planned changes in
the permitted facility or activity which may result in noncompliance with the permit
requirements.
3. Transfers
This permit is not transferable to any person except after notice to and approval by
the Director. The Director may require modification or revocation and reissuance of
the permit to change the name and incorporate such other requirements as may be
necessary under the Clean Water Act.
Monitoring results shall be reported at the intervals specified elsewhere in this
permit.
v � i'N'iRi:f+m: . r
The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information
shall be provided orally within 24 hours from the time the permittee became aware

Individual Stormwater Page A16
of the circumstances. A written submission shall also be provided within 5 days of
the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its
causes; the period of noncompliance, including exact dates and times, and if the
noncompliance has not been corrected, the anticipated time it is expected to
continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence
of the noncompliance.
b . The following shall be included as information which must be reported within 24
hours under this paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the
permit.
(2) Any upset which exceeds any effluent limitation in the pen -nit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants
listed by the Director in the permit to be reported within 24 hours.
e . The Director may waive the written report on a case -by -case basis for reports under
paragraph b. above of this condition if the oral report has been received within 24
hours.
The permittee shall report all instances of noncompliance not reported under Pan 11.
E. 4. and 5. of this permit at the time monitoring reports are submitted. The reports
shall contain the information listed in Pan U. E. 5. of this permit.
• _ - .-UP !R e_ MO
Where the permittee becomes aware that it failed to submit any relevant facts in a
notice of intent to be covered under this permit or in any report to the Director, it
shall promptly submit such facts or information.
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or
Section 308 of the Federal Act, 33 USC 1318, all reports prepared in accordance
with the terms shall be available for public inspection at the offices of the Division
of Environmental Management As required by the Act, effluent data shall not be
considered confidential. Knowingly making any false statement on any such report
may result in the imposition of criminal penalties as provided for in NCGS 143-
215.6B or in Section 309 of the Federal Act
The Clean Water Act provides that any person who knowingly makes any false
statement, representation, or certification in any record or other document
submitted or required to be maintained under this permit, including monitoring
reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a fine of not more than $10,000 per violation, or by imprisonment for
not more than two years per violation, or by both.

Individual Stormwater Page A17
PART III
LIMITATIONS REOPENER
This permit shau be modified or alternatively, revoked and reissued, to comply with any
applicable effluent guideline or water quality standard issued or approved under Sections
302(b) (2) (c), and (d), 304(b) (2) and 307(a) of the Clean Water Act, if the effluent
guideline or water quality standard so issued or approved:
a. contains different conditions or is otherwise more stringent than any effluent
limitation in the permit; or
b. controls any pollutant not limited in the permit.
The permit as modified or reissued under this paragraph shall also contain any other
requirements in the Act then applicable.
PART IV
ADMINISTERING AND CO'XIPLIANCE MONITORING FEE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty)
days after being billed by the Division. Failure to pay the fee in timely manner in
accordance with 15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit.

Memo To The File
Permit Number: NCG000150
Facility Name: Neste Resins Corporation, Inc.
Location Address: 790 Corinth Road, Fayetteville NC
Point of Contact: Willie Bethea, [phone]
Comments:
1. The permit has no analytical monitoring and visual monitoring does not indicate the
need for analytical monitoring. The permit was issued "as is" except for the inclusion
of quarterly monitoring in the 41h year of the permit term for vehicle maintenance that
may occur at the facility.
2. The visual monitoring was performed for the entire permit term except for the fal l of
' 95.
3. The term of the permit was shortened to have the permit expire simultaneously with
the wastewater permit, NC000892. An email was sent to Dave Goodrich informing
him of this condition. Also, a comment was made on IMS to indicate this permit will
be incorporated into the wastewater permit.