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HomeMy WebLinkAboutNCG200507_MONITORING INFO_20190314NORTH CARD INA Department of Environmental Quai STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V '� aD 0 5J / DOC TYPE ❑HISTORICAL FILE L� MONITORING REPORTS DOC DATE ❑ )o / % o ,3 YYYYMMDD Semi-annual Stormwater Discharge Monitoring Retort (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted 03/05/2019 CERTIFICATE OF COVERAGE NO. NCG20 0 5 0 7 FACILITY NAME Wesbell Investment Recovery LTD COUNTY Person PERSON COLLECTING SAMPLES Diane Bel LABORATORY Environmental Conservation Laborator Lab Cert. # 37724 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD Q Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA F:/�r�I/�ffN ❑❑Zero -flow [:]water Supply []SA Saltwater Other PLEASE REMEMBER TO SIGN ON THE REVERSE -� No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks ==> - - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L' 0.075 mg/L or 0.210 mg/L' 0.126 mg/L or 0.090 mg/Ls 1 02/21/19 0.7 34 mg/L 36 mg/L 1.50 mg/L 0.013 mg/L 0.003 mg/L 0.062 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." --D i (Signature of Permittee) Permit Date: 02/02/2015-12/31/2019 03/05/19 (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted August 17, 2018 CERTIFICATE OF COVERAGE NO. NCG200507 FACILITY NAME Wesbell Investment Recovery COUNTY Person PERSON COLLECTING SAMPLES Diane Bell LABORATORYENCO Lab Cert. # 591 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 AMPLE PERIOD ❑ Jan -June ® July -Dec c N r,... or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Ai�� ti ZQ�a ❑Zero -flow ❑Water Supply ❑SA CAN i� I�ILE� ❑Saltwater ❑Other L\4�iR SEC r 10; PLEASE REMEMBER TO SIGN ON THE REVERSE —> ❑ No discharge this period?z Outfall No: Date Sample Collected {mo/dd/yr)` 24=hour rainfall amount;. Inches ',Total, Suspended.. ;`;Solids ?:. Chemical Oxygen Demand Non -polar oil &grease EPA -Method 1664 ISGT=HEM) '= Copper, ,Total Lead, Total Zinc, Total Benchmarks =_> _ 100:mg/Gor: :. 50 mg/L4 120 mg/L 15 mg/L 1-0:010 mg/L:or ° .0:065.mg/C5 `mg/LS '0:075'mg/L or 0.126 mg/L or 0.090 mg/L5 1 08/03/18 0.27 18 mg/L 18 mg/L 2.40 mg/L 0.008 mg/L 0.003 mg/L 0.049 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: if You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' OutfallNo• Date Sample 1 Collected (mo/dd/yr) 24 hour rainfall amoun3, Inches.. Non polar O&G'by EPA` "1664:.(SGT.M)'_:: =HE Total Suspended Solids.- Benchmarks===>.. : , _ :'15 mg/L 100 mg/L or,50.mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date: 02/02/2015-12/31/2019 .:� -r,�--r? (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 a ^o �eQfIP��, E NiCO Laborato"'es, Accurate. Timely.. Responsive. I or ve` 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, August 15, 2018 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CB11781 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, August 3, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OUTFALL 1 Lab ID: CB11781-01 Sampled: 08/03/18 08:20 Received: 08/03/18 12:55 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E EPA 1664B 08/31/18 08/09/18 10:36 08/10/18 14:27 EPA 6010D EPA 3005A 01/30/19 08/06/18 08:34 08/10/18 14:04 SM 2540D-2011 NO PREP 08/10/18 08/07/18 07:21 08/07/18 07:21 SM 5220D-2011 Same 08/31/18 08/07/18 08:46 08/07/18 11:27 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: OUTFALL 1 Lab ID: C811781-01 Anallyte Results Flag MDL P L Units Method Notes Chemical Oxygen Demand 19 10 10 mg/L SM 5220D-2011 Copper - Total 8.38 3 1.60 10.0 ug/L EPA 6010D Iron - Total 2630 22.0 50.0 ug/L EPA 6010D Lead - Total 3.36 1 3.10 10.0 ug/L EPA 6010D Total Suspended Solids 18 2.5 2.5 mg/L SM 254OD-2011 Zinc - Total 49.3 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 ce Nk' asr4111111101 www.encolabs.com ANALYTICAL RESULTS Description: OUTFALL 1 Lab Sample ID:CB11781-01 Received: 08/03/18 12:55 Matrix: Surface Water Sampled:08/03/18 08:20 Work Order: CB11781 Project: Stolmwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods I1 ^ - ENCO Cary certified analyte [NC 5911 Analvte rCAS Number! Results Flag Units DF MDL Q Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 8H06006 EPA 6010D 08/10/18 14:04 JDH Copper [7440-50-8]^ 8.38 J ug/L 1 1.60 10.0 8H06006 EPA 6010D 08/10/18 14:04 JDH Iron [7439-89-6]^ 2630 ug/L 1 22.0 50.0 8HO6006 EPA 6010D 08/10/18 14:04 JDH Lead [7439-92-1]^ 3.36 J ug/L 1 3.10 10.0 8HO6006 EPA 6010D 08/10/18 14:04 JDH Zinc[7440-66-6]^ 49.3 ug/L 1 4.40 10.0 8HO6006 EPA 6010D 08/10/18 14:04 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyze [NC 5911 Analyte rCAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed Notes Chemical Oxygen Demand^ 19 mg/L 1 10 10 8H07004 SM 5220D-2011 08/07/18 11:27 JOC Total Suspended Solids^ 18 mg/L 1 2.5 2.5 8H07003 SM 254OD-2011 08/07/18 07:21 LBG Classical Chemistry Parameters ^ - ENCO Jacksonville certified andlyte [NC 442] AnaWe rCAS Numberl Results Flag Units DF MDL PPOL Batch Method Analyzed By Notes Oil& Grease (HEM)[C-0007]^ 2.40 U mg/L 1 2.40 5.00 8HO9005 EPA 16646 08/10/18 14:27 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch SH06006 - EPA 3005A Blank (8H06006-BLK1) Prepared: 08/06/2018 08:34 Analyzed: 08/10/2018 12:08 Spike Source %REC RPD Anal vte Result Flan PQL units Level Re ul %REC Limi RPD Lima Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (8H06006-BS1) Prepared: 08/06/2018 08:34 Analyzed: 08/10/2018 12:24 Spike Source %REC RPD Anal vte Result Rao Q Units Level Result %REC Limits RPD killnis Notes Cadmium 18.5 1.00 ug/L 20.0 93 80-120 Copper 185 10.0 ug/L 200 92 80-120 Iron 963 50.0 ug/L 1000 96 80-120 Lead 188 10.0 ug/L 200 94 80-120 Zinc 192 10.0 ug/L 200 96 80-120 Matrix Spike (8H06006-MS1) Prepared: 08/06/2018 08:34 Analyzed: 08/10/2018 12:26 Source: CB11620-01 Spike Source %REC RPD Anal a Result Flaa P L Units Level Result %REC Limits RPD Limit Notes Cadmium 18.0 1.00 ug/L 20.0 0.360 U 90 75-125 Copper 183 10.0 ug/L 200 1.68 91 75-125 Iron 938 50.0 ug/L 1000 22.0 U 94 75-125 Lead 187 10.0 ug/L 200 3.10 U 94 75-125 Zinc 187 10.0 ug/L 200 4.40 U 94 75-125 Matrix Spike Dup (8H06006-MSD1) Prepared: 08/06/2018 08:34 Analyzed: 08/10/2018 12:29 Source: CB11620-01 Spike Source %REC RPD Anal vte Result FlaFlaci Q2 Unats Level Re u %REC Limits RPD Limit Notes Cadmium 17,7 1.00 ug/L 20.0 0.360 U 88 75-125 2 20 Copper 180 10.0 ug/L 200 1.68 89 75-125 2 20 Iron 917 50.0 ug/L 1000 22.0 U 92 75-125 2 20 Lead 182 10.0 ug/L 200 3.10 U 91 75-125 3 20 Zinc 184 10.0 ug/L 200 4.40 U 92 75-125 1 20 Post Spike (8H06006-PS1) Prepared: 08/06/2018 08:34 Analyzed: 08/10/2018 12:31 Source: CB11620-01 Spike Source %REC RPD -Anal vte Result Jag IQ units Level Re u %REC Limits RPD Limi Notes Cadmium 0.0180 0.00100 mg/L 0.0200 -0.000450 90 80-120 Copper 0.183 0.0100 mg/L 0.200 0.00168 90 80-120 Iron 0.936 0.0500 mg/L 1.00 0.00964 93 80-120 Lead 0.185 0.0100 mg/L 0.200 0.00278 91 80-120 Zinc 0.188 0.0100 mg/L 0.200 -0.000513 94 80-120 Classical Chemistry Parameters - Quality Control Batch SH07003 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SH07003 - NO PREP - Continued Blank (8H07003-BLK3) Prepared & Analyzed: 08/07/2018 07:21 Spike Source %REC RPD Anal vte Re-sOtt Slag PQL units Level Resul %REC Limits RPD Limi Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (8H07003-BSI) Prepared & Analyzed: 08/07/2018 07:21 Spike Source %REC RPD Analvte Result Flag Poll. Units Level Result %REC Limits RPD klnft Notes Total Suspended Solids 99 2.5 mg/L 100 99 80-120 Duplicate (SH07003-DUPl) Prepared & Analyzed: 08/07/2018 07:21 Source: CB09954-01 Spike Source %REC RPD Anal vte Result Flea PQL Uei Level Result %REC LimitsRPD Limit Notes Total Suspended Solids 340 50 mg/L 360 7 20 Duplicate (811-1107003-D11,11122) Prepared & Analyzed: 08/07/2018 07:21 Source: CB11426-01 Spike Source %REC RPD -Anah to Reds Flaa POL Moils Level Re ul %REC Limits RPD u1nit Notes Total Suspended Solids 44 25 mg/L 42 5 20 Batch SH07004 - Same Blank (8H07004-BLK3) Prepared: 08/07/2018 08:46 Analyzed: 08/07/2018 11:27 Spike Source %REC RPD Anal vte Result Elag POL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (8H07004-BS3) Prepared: 08/07/2018 08:46 Analyzed: 08/07/2018 11:27 Spike Source %REC RPD Anal vte Result Flan PPOL Wits Level Re ul %REC Limits RPD klinft Notes Chemical Oxygen Demand 490 10 mg/L 500 99 90-110 Matrix Spike (8H07004-MS1) Prepared: 08/07/2018 08:46 Analyzed: 08/07/2018 11:27 Source: CB07360-01 Spike Source %REC RPD An lvt Result ELiq PL Units Level Resu %REC Limits RPD kLmft Notes Chemical Oxygen Demand 560 10 mg/L 526 27 102 90-110 Matrix Spike Dup (8H07004-MSDI) Prepared: 08/07/2018 08:46 Analyzed: 08/07/2018 11:27 Source: CB07360-01 Spike Source %REC RPD Analvte Result Flag P L 1 its Level Resul %REC Limits RPD LLM9 Notes Chemical Oxygen Demand 560 10 mg/L 526 27 101 90-110 0.8 10 Classical Chemistry Parameters - Quality Control Batch 9HO9OO5 - EPA 1664B Blank (8H09005-BLK3) Prepared: 08/09/2018 10:36 Analyzed: 08/09/2018 15:40 Spike Source %REC RPD Analvte Result IElaa lQ Units Level Result %REC Limits RPD iiinit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SH09005 - EPA 1664B - Continued LCS (SH09005-BS3) Prepared: 08/09/2018 10:36 Analyzed: 08/09/2018 15:40 Spike Source %REC RPD Analvte Result Flaq P L Units Level Res 1 %REC Limits RPD Limit Notes Oil & Grease (HEM) 138 5.00 mg/L 160 86 78-114 LCS Dup (811-1109005-13SD3) Prepared: 08/09/2018 10:36 Analyzed: 08/09/2018 15:40 Spike Source %REC RPD Anal Yte Result Flaq POL Units Level Res o/aREC Limits RPD Lwift Notes Oil & Grease (HEM) 132 5.00 mg/L 160 83 78-114 4 18 Matrix Spike (8H09005-MS1) Prepared: 08/09/2018 10:36 Analyzed: 08/09/2018 15:40 Source: BB03493-01 Spike Source %REC RPD Anal a Result Flao 4 Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM). 175 5.00 mg/L 168 47.0 76 78-114 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (9 �Ell 9�rj=) www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-Of-CUST6DY RECORD www.encolabs.com � 4W 10776 Comral Port Dr. 41310 Executive Park.Court, Suite 111 102-A Woodwinds Industrial'CL Orlando, FL 32624 Jacksonville, FL 32216.6669 Cary, NC 27511 (407) 826-5314 Fax'(407) 850.6945 (904) 296.3007 Fax (904) 29"210 (919) 467-3090' fax (919) 467-3515 Page of �gN `PSClient Name y� �JUf t _TnU_ e t eCOL)"t Project Number. Lr v(�L at�tG O f{ram ;'Ivr'r,e i — Requested Analyses Requested Turnaround Times subject to Note: Rush ce by the acceptance by fha taciliry _ Standard _ Expedited Due _ n �, LL O - tL�: C IV) 6 ,. A V - - Address S S /� ( - JS Luc Ci; r'l',z 4+ .. (--i- .r Project NAme/Desc rM G ^ .. PO 2?Billing Into / City1ST/Zip fi�ci Tof 33 -06,00 Fax 3 - Reporting Contact e-& Samplegs).Nama. Aifilirdion (Print). 1 .h1� Billing Contact tt :Cc+�e fegs) Signature Site Location / Time Zone `` '' Lab W_orkdrder Preservation (See Codes) (Combine as necessary) Item 4 SampleAD.(Field Identification) Date Collection Tinto . Comp'/Grab Matrix (see bodes) Totaltr.of ' Containers I - Sample Comments �Collection tf w I . <--Total Yr Of Containers 1� Sample Kit Prepared By DateRme, _ Relitlqui d By Dal ❑n - Received B Date im /t Comments/Special Reporting Requirements Relinquished By 'D lef 1 into odb Datef ima Relinquished By .DataMme, - Received By. .Dated ime Cooler s's a Temps on Receipt A Condition UponReceipt �- ;K Acceptable Unacceptable Matrix:GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW,Surtace Water WW-Waslewater A -Air O-Other(detail In comments) Preservation: t.Ice-H,HCI. N-HNO3 S-H2SO4'NO•NaOH O:Othar(detail in comments): Note.: All samples submitted to ENCO labs are in accordance wlthithe-terms and'condilions.liisted on the reverse or this form, unless prior written agreements exist Sample Preservation Verification ENCO Cary z; t Work Order: CB11781 Project: Stormwater Client: Wesbell Asset Recovery Center (WEO12) Project #: [none] Logged In: 03-Aug-18 13:49 Logged By: Rachel Ann Yonish Preservation Check.Performed By: Ch J DatelTime: s,/,j) I S 13 U l� CB11781-01 Cont t: _F», Type * 2 $Pres» H .�tp } , , �Re_quirement H Checked ppH In Control, 4=; sY AdJusted x , Date�mey � s' ��Ad�usted tee., , a aReagenttUsed/Comments B 250mLA+H2SO4 <2 Y/ N/ Y/ N/ A C 250mLA+'H2SO4 <2 Y/ N/ Y/ N/ A D 250mLP+H2SO4 <2 N / NA Y / / NA 'A-E 250mLP+HNO3 <2 tY / N / NA Y / NA Rea ent Name ID 1 2 pH Strip IC _ PH Strips C7J0820 C:\elmnt\Pi,i ii%wr,u_r-i CtiCi vauonV necK. rpt Reagent Name ID 3 4 Rea ent Name ID _ 5 6 Page 1 of 1 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted February 12, 2018 CERTIFICATE OF COVERAGE NO. NCG200507 FACILITY NAME Wesbell Investment Recovery COUNTY Person PERSON COLLECTING SAMPLES Diane Bell LABORATORYENCO Lab Cert. # 591 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' (month) � � IV DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA �� ❑Zero -flow [:]Watersupply []SA FEB 15 2013 ❑saltwater ❑Other v`r\I i RAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE -� -L1✓R SEC7lOA, No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> - - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 1 01/29/18 0.13 7.9 mg/L 17 mg/L 2.40 mg/L 0.009 mg/L 0.003 mg/L 0.040 mg/L 2 01/29/18 0.13 7.7 mg/L 17 mg/L 2.40 mg/L 0.008 mg/L 0.003 mg/L 0.060 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/0 Footnotes from Part A also apply to this Part B Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ure of Permittee) Permit Date: 02/02/2015-12/31/2019 cs-�-/1)-/I r (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 F u rta TNI' N,,CO Accurate. elf►, Responsive. InnoratiVe. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, February 12, 2018 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CB01278 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, January 29, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data.from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 (qNkl �GL) www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OUTFALL 1 Lab ID: C801278-01 Sampled: 01/29/18 09:00 Received: 01/29/18 15:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E EPA 1664B 02/26/18 02/02/18 13:49 02/07/18 15:10 EPA 6010D EPA 3005A 07/28/18 02/02/18 09:10 02/09/18 14:38 SM 254OD-1997 NO PREP 02/05/18 02/02/18 14:40 02/02/18 14:40 SM 5220D-1997 Same 02/26/18 01/29/18 16:33 01/30/18 14:10 Client ID: OUTFALL 2 Lab ID: CB01278-02 Sampled: 01/29/18 08:55 Received: 01/29/18 15:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E EPA 1664B 02/26/18 02/02/18 13:49 02/07/18 15:10 EPA 6010D EPA 3005A 07/28/18 02/02/18 09:10 02/09/18 14:40 SM 2540D-1997 NO PREP 02/05/18 02/02/18 14:40 02/02/18 14:40 SM 5220D-1997 Same 02/26/18 01/29/18 16:33 01/30/18 14:10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 I K-G) www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: oUTFALL 1 Lab ID: CB01278-01 1 Analvte Results Flaq MDL POL Units Method Notes Chemical Oxygen Demand 17 10 10 mg/L SM 522OD-1997 Copper- Total 9.42 3 1.60 10.0 ug/L EPA 6010D Iron - Total 1280 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 7.9 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 40.1 4.40 10.0 ug/L EPA 6010D Client ID: OUTFALL 2 Lab ID: CB01278-02 Analyt Results Flag MDL POL Units Method Notes Chemical Oxygen Demand 17 10 10 mg/L SM 522OD-1997 Copper- Total 8.13 3 1.60 10.0 ug/L EPA 6010D Iron - Total 2680 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 7.7 2.5 2.5 mg/L SM 2540D-1997 Zinc - Total 59.8 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 www.encolabs.com ANALYTICAL RESULTS Description: OUTFALL 1 Lab Sample ID:C601278-01 Received: 01/29/18 15:00 Matrix: Surface Water Sampled: 01/29/18 09:00 Work Order: CB01278 Project: Stormwater Sampled By: Diane Bell (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified anayte [NC 591] Analyze rCAS Number] Results Flag Units DF MDL ,POLL Batch Method Analyzed Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 8BO2011 EPA 6010D 02/09/18 14:38 JDH Copper [7440-50-8]^ 9.42 J ug/L 1 1.60 10.0 8BO2011 EPA 6010D 02/09/18 14:38 JDH Iron [7439-89-6]^ 1280 ug/L 1 22.0 50.0 8BO2011 EPA 6010D 02/09/18 14:38 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 8BO2011 EPA 6010D 02/09/18 14:38 JDH Zinc[7440-66-6]^ 40.1 ug/L 1 4.40 10.0 8BO2011 EPA 6010D 02/09/18 14:38 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Number] Results Flag Units J& MDL POLL Batch Method Analyzed Notes Chemical Oxygen Demand^ 17 m9/L 1 10 10 BA29038 SM S220D-1997 01/30/18 14:10 JOC Total Suspended Solids^ 7.9 mg/L 1 2.5 2.5 8BO2018 SM 254OD-1997 02/02/18 14:40 OMR (Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Resul Flaq Units DF L POLL Batch Method Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 8602007 EPA 1664B Description: OUTFALL 2 Matrix: Surface Water Lab Sample ID: CB01278-02 Sampled: 01/29/18 08:55 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods Analyzed AX Notes 02/07/1815:10 SMA Received: 01/29/18 15:00 Work Order: CB01278 ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units PFF MDL POL Batch MethodAnalyzed fiC Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 8BO2011 EPA 6010D 02/09/18 14:40 JDH Copper [7440-50-8]^ 8.13 J ug/L 1 1.60 10.0 8BO2011 EPA 6010D 02/09/18 14:40 JDH Iron [7439-89-6]^ 2680 ug/L 1 22.0 50.0 8BO2011 EPA 6010D 02/09/18 14:40 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3,10 10.0 8BO2011 EPA 6010D 02/09/18 14:40 JDH Zinc [7440-66-6]^ 59.8 ug/L 1 4.40 10.0 8BO2011 EPA 6010D 02/09/18 14:40 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Number] Results Flag Units RE MDL POLL Batch Method Analyzed Notes Chemical Oxygen Demand^ 17 mg/L 1 10 10 8A29038 SM 522OD-1997 01/30/18 14:10 JOC Total Suspended Solids^ 7.7 mg/L 1 2.5 2.5 BB02018 SM 254OD-1997 02/02/18 14:40 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Number] Res I Flag Units PFF MDL POL Batch Method Analyzed Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 BB02007 EPA 1664B 02/07/18 15:10 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 9 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods -Quality Control Batch 8502011 - EPA 3005A Blank (SB02011-BLK1) Prepared: 02/02/2018 09:10 Analyzed: 02/09/2018 13:22 Spike Source %REC RPD Anal tie Result Flaa P L Units Level Res I %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (SB02011-BSI) Prepared: 02/02/2018 09:10 Analyzed: 02/09/2018 13:24 Spike Source %REC RPD Anala Result Flaa rQ Units Level Res I %REC Limits RPD Lima Notes Cadmium 21.5 1.00 ug/L 20.0 107 80-120 Copper 212 10.0 ug/L 200 106 80-120 Iron 1120 50.0 ug/L 1000 112 80-120 Lead 215 10.0 ug/L 200 107 80-120 Zinc 221 10.0 ug/L 200 111. 80-120 Matrix Spike (8B02011-MS1) Prepared: 02/02/2018 09:10 Analyzed: 02/09/2018 13:30 Source: CB01425-01 Spike Source %REC RPD Anal vte Result Flag ROL Uni Level Result %REC Limits RPD Limit Notes Cadmium 20.5 1.00 ug/L 20.0 0.360 U 102 75-125 Copper 217 10.0 ug/L 200 1.60 U 108 75-125 Iron 1960 50.0 ug/L 1000 844 111 75-125 Lead 199 10.0 ug/L 200 3.10 U 100 75-125 Zinc 241 10.0 ug/L 200 33.1 104 75-125 Matrix Spike Dup (8602011-MSD1) Prepared: 02/02/2018 09:10 Analyzed: 02/09/2018 13:33 Source: CB01425-01 Spike Source %REC RPD Analvte Resul Flag POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.1 1.00 ug/L 20.0 0.360 U 101 75-125 2 20 Copper 212 10.0 ug/L 200 1.60 U 106 75-125 2 20 Iron 1950 50.0 ug/L 1000 844 110 75-125 0.6 20 Lead 201 10.0 ug/L 200 3.10 U 100 75-125 0.7 20 Zinc 238 10.0 ug/L 200 33.1 103 75-125 0.9 20 Post Spike (8B02011-PS1) Prepared: 02/02/2018 09:10 Analyzed: 02/09/2018 13:35 Source: CB01425-01 Spike Source %REC RPD Anal a Result Flaa IQ Units Level Result %REC Limits RPD iWift Notes Cadmium 0.0202 0.00100 mg/L 0.0200 4.93E-5 101 80-120 Copper 0.213 0.0100 mg/L 0.200 -0.00405 107 80-120 Iron 1.92 0.0500 mg/L 1.00 0.844 108 80-120 Lead 0.199 0.0100 mg/L 0.200 -0.00437 99 80-120 Zinc 0.238 0.0100 mg/L 0.200 0.0331 103 80-120 Classical Chemistry Parameters - Quality Control Batch 8A29038 - Same FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 8A29038 - Same - Continued Blank (8A29038-BLK1) Prepared: 01/29/2018 16:33 Analyzed: 01/30/2018 14:10 Spike Source %REC RPD Anal r<g Resul Flaa P L Units Level Resul %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (8A29038-BS1) Prepared: 01/29/2018 16:33 Analyzed: 01/30/2018 14:10 Spike Source %REC RPD Anal-Ae ReslI Flan Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (8A29038-MS1) Prepared: 01/29/2018 16:33 Analyzed: 01/30/2018 14:10 Source: CA14318-01 Spike Source %REC RPD Anal a Result Flaa IQ Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 19 101 90-110 Matrix Spike Dup (8A29038-MSD1) Prepared: 01/29/2018 16:33 Analyzed: 01/30/2018 14:10 Source: CA14318-01 Spike Source %REC RPD Anal vte Result Fig PQL MAiU Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 530 10 mg/L 526 19 98 90-110 3 10 Batch SS02018 - NO PREP Blank (8B02018-BLK1) Prepared & Analyzed: 02/02/2018 14:40 Spike Source %REC RPD Anal vte Resin Flan P91 Units Level Resul %REC Limits RPD Limi Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (8B02018-BS3) Prepared & Analyzed: 02/02/2018 14:40 Spike Source %REC RPD Anal a Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (8B02018-DUPi) Prepared & Analyzed: 02/02/2018 14:40 Source: CB00712-02 Spike Source %REC RPD Anal Resul Flaq i OL units Level Res %REC Limits RPD Limit Notes Total Suspended Solids 1100 170 mg/L 1200 14 20 Duplicate (8B02018-DUP2) Prepared & Analyzed: 02/02/2018 14:40 Source: CB00712-03 Spike Source %REC RPD Analvte Result Fig Q U-I its Level Result %REC Limits RPD Limit Notes Total Suspended Solids 450 62 mg/L 470 5 20 Classical Chemistry Parameters - Quality Control Batch 8802007 - EPA 1664E Blank (SB02007-BLK1) Prepared: 02/02/2018 10:53 Analyzed: 02/07/2018 15:10 Spike Source %REC RPD Anal lde Result FlIAg IQ -hits Level Result %REC Limits RPD kmil Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 8801007 - EPA 1664E - Continued LCS (SB02007-BS1) Prepared: 02/02/2018 10:53 Analyzed: 02/07/2018 15:10 Spike Source %REC RPD Analvte Resul Fuca Q Units Level Res I %REC Limits RPD Limit Notes Oil & Grease (HEM) 159 5.00 mg/L 161 99 78-114 LCS Dup (8B02007-BSD1) Prepared: 02/02/2018 10:53 Analyzed: 02/07/2018 15:10 Spike Source %REC RPD Anal a Res Flag PQL ant Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 149 5.00 mg/L 163 91 78-114 7 18 Matrix Spike (8B02007-MS1) Prepared: 02/02/2018 10:53 Analyzed: 02/07/2018 15:10 Source: BB00515-01 Spike Source %REC RPD Anal a Result Flaa Q Units Level Result %REC Limits RPD iimft Notes Oil & Grease (HEM) 162 5.00 mg/L 154 2.73 103 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 10775 Centre) Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Cl. _ Orlando. FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511 (407) 826.5314 Fax (407) 850-6945 (9D4) 296.3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page Of Client N��am4{e- 2?)Q a4-0e > tT ovc Project Number - , l�(l }cl r J?��Gt (1ct cam.. i Requested Analyses Requested Turnaround Times Note: Rush requests subject to acceptance by the facility _ Standard _ Expedited Due ji 7 7Y to - ^�c j Address 5 L c/ (~ r�,r. C( . ! r (X, ` ( _ 1 J� ! Project`NamelDesc ! d{ (nIGC 2. r— Cl !ST/Zip CJK bufO ,tom a S PO N 1 Billing Into Tel 3� -3;) Z _ C)�'��. Fax (3ryC, a-C�(oCl. Reporting Contact cage �� Sampler(s) Name, Affiliation (Print) Billing Contact S ler(sj Signature Site Location I Time Zone Lab. Workorder l �J Preservation (See Codes) (Combine as necessary) Item a • Sample to (Field Identification)' - Collection Date Collection Time Comp I Grab Matrix (see codes) Total It of Containers - Sample Comments 0,0 < - Total It of Containers Sample Kit Propared By Datofime Patin rishod By Datelrme LIZ- Receive By Daterrime Comments/Special Reporting Requirements Relinquished By Datefrime Re jved y Daterrime Relinquished By Date(rime. RiAKV By DateTme r,,r#'s&Tempso Receipt Condition pon Receipt _ Acceptable _ Unacceptable Matrix: GW-Groundwater SO -Soil OW -Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: Mca n-Rcl N-HNvs 5-1­t25v4 Nv-Naut-t v-utner taetau in comments) Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CB01278 Project: Stormwater Client: Wesbell Asset Recovery Center (WE012) Project #: [none] Logged In: 29-Jan-18 15:08 Logged By: John C King Preservation Check Performed By: ht1J Date/Time: CB01278-01 Cont' i Type - Presg(pH).. Requirement;,. pH Checked t --., In;Control ,=: ... 'DateMme pH; Adjusted Adjusted: ` .. Reagent Used/Comments B 250mLA+H2SO4 <2.,, •' / N ! NA Y % ! NA , C 250mLA+H2SO4 <2 0( / N / NA Y / to / NA D 250mLP+H2SO4 <2... 0(, / N ! NA Y / & / NA E 250mLP+HNO3 <2 / N / NA Y la / NA CB01278-02 Cant; ., Type Pres(pH) :Requirement pH Checked/ In.Control = Date�me pH Adtusted _ ' Adjusted Reagent UsedJComments B 250mLA+H2SO4 <2 / N / NA Y ! / NA C 250mLA+H2SO4 <2 (! / N / NA Y NA D 250mLP+H2SO4 <2 / N / NA Y /0 / NA E 250mLP+HNO3 <2 V1 N / NA Y / 44 ! NA Reagent Name ID Reaclent Name ID Reagent Name ID_ 1 r � .3 5 2 4 6 . pH Strip ID:Z Cti C:\ELMNT\Print\wko_PreservationCheck.rpt Page 1 i i 11 "1' Semi-annual Storfiriwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG2000OO — Scrap Metal Recycling Date submitted i4-A !�— / �?-- CERTIFICATE OF COVERAGE NO. NCG2O U"5- o FACILITY NAME GJezN k1L COUNTY Djtf S«\ PERSON COLLECTING SAMPLES����_ IX�� LABORATORY ENCG Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR ( ( J7 SAMPLE PERIOD [] 'Jan -June ❑ July -Dec or ❑ Monthly' (month) p DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA !EC1 ❑Zero -flow ❑Water Supply [:]SA APR 2 g ❑Saltwater ❑Other CEN f, AL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE -� DwR SEA �IflN U No discharge this period?' Outfall No. Date Sample. 24 ,hour rainfall Non polar oil;& grease 1 Collected, amount, ; Total Suspended: Chemical Oxygen ` EPA Method 1664_ Copper, Lead, "Zinc , .. . (mo/dd/yr) .: Inches-.' ., Solids Demand (SGT:HEM),,.., :Total; ;. Total Total.:: -; Benchmarks =_> _. 100 mg/L or_. 0010'.mg/L or 0 075 mg/L or. 0.126 mg/L or. s0 mg/L° 120 mg/L 15 mg/L 0005 mg/LS 0 210; mg/Ls 0:090 mg/l ; ' a 01 03 0.10 31 �►'► It M� U. u�3 L- Cl , Uy3 �3/ p, ��� L /t 5 1_ 51 C� 1 L. G• 1% L ej311 W 1'4- C) . 1 U 5.1t i .._ __ I L I -�; i- -. Z l I o., . &_l a rr.�. I 1 o , u IX r--7/L c) -,^ 44 ,-1 1_ c) . u & -i 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B:• V ehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample 24 hour rainfall , - Collected amount, a No.n polar O&G EPA by Total Suspended Solids (mo/dd/yr) Inches 2664>(SGTHEM) Benchmarks > - 15 mg/L 100 mg/L or 50 mg/L° Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES FiTNO ❑ REGIONAL OFFICE CONTACT NAME: Mve c(6"zi Iq I.-i n 4 Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Imo', TI-lat (Signature of Permittee) Permit Date: 02/02/2015-12/31/2019 Lf-7-2,r—(-- (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 ENW Laboratmies Acawf: Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3SiS Tuesday, May 31, 2016 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): C512441 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, May 19, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Out(all2 Lab ID: C512441-01 Sampled: 05/19/16 11:30 Received: 05/19/16 13:55 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/16/16 05/24/16 15:13 05/25/16 18:39 EPA 6010D 11/15/16 05/23/16 09:12 05/24/16 10:12 SM 254OD-1997 05/26/16 05/23/16 10:30 05/23/16 10:30 SM 5220D-1997 06/16/16 05/23/16 15:52 05/24/16 10:17 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: ES12441-01 Analvte Results flag MDC P L Units Method Notes Chemical Oxygen Demand 35 10 10 mg/L SM 5220D-1997. Copper- Total 17.4 1.60 10.0 ug/L EPA 6010D Iron - Total 6370 22.0 50.0 ug/L EPA 6010D Lead - Total 5.16 1 3.10 10.0 ug/L EPA 6010D Total Suspended Solids 440 33 33 mg/L SM 254OD-1997 Zinc - Total 85.5 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 Lewi =qMN"-- ANALYTICAL RESULTS Description: Outfall 2 Lab Sample ID: C512441-01 Received: 05/19/16 13:55 Matrix: Surface Water Sampled:05/19/16 11:30 Work Order: C512441 Project: Storrnwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] - Analyte [CAS Numberl Results Flaa Units DF MOIL P L Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 6E23009 EPA 6010D 05/24/16 10:12 JDH Copper[7440-50-8]^ 17.4 Ug/L 1 1.60 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Iron [7439-89-6]1 6370 ug/L 1 22.0 50.0 6EZ3009 EPA 6010D 05/24/16 10:12 JDH Lead [7439-92-1]^ S.16 J ug/L 1 3.10 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Zinc [7440-66-6]^ 85.5 ug/L 1 4.40 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Classical Chemistry Parameters ^ - ENCO Cary celVfied analyte [NC 591] Analyte rCAS Numbed Results Flag Units DF DLDI POL 440 Method Analyzed §y Notes Chemical Oxygen Demand^ 35 mg/L 1 10 10 6E23030 SM 5220D-1997 05/24/16 10:17 JOC Total Suspended Solids^ 440 mg/L 13.3 33 33 6E23004 SM 254OD-1997 05/23/16 10:30 MMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified anatyte [NC 4421 Analyte rCAS Numbed Results Fig Units DF L M Batch Me Analyzed By Notes Oil & Grease (HEM)[C-00071^ 0.629 U mg/L 0.262 0.629 1.31 6E24002 EPA 1664E 05/25/16 18:39 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Spike Source %REC RPD Analvte Result Flag PT Units Level Res I %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (6E23009-BS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 09:57 Spike Source %REC RPD -An Faq POL LinitsLevel Resul Limit Notes Cadmium 20.1 1.00 ug/L 20.0 101 80-120 Copper 192 10.0 ug/L 200 96 80-120 Iron 1010 50.0 ug/L 1000 101 80-120 Lead 198 10.0 ug/L 200 99 80-120 Zinc 200 10.0 ug/L 200 100 80-120 Matrix Spike (6E23009-MS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:02 Source: CZ06979-01 Spike Source %REC RPD Anal Resull Flag POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.8 1.00 ug/L 20.0 0.360 U 104 75-125 Copper 192 10.0 ug/L 200 1.60 U 96 75-125 Iron 1150 50.0 ug/L 1000 90.7 106 75-125 Lead 199 10.0 ug/L 200 3.10 U 100 75-125 Zinc 205 10.0 ug/L 200 4.40 U 103 75-125 Matrix Spike Dup (6E23009-MSD1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:05 Source:CZ06979-01 Spike Source %REC RPD Anal vte iResult Fla_q M Units Level Resul %REC Limits RPD Limit Notes Cadmium 20.6 1.00 ug/L 20.0 0.360 U 103 75-125 0.9 20 Copper 193 10.0 ug/L 200 1.60 U 96 75-125 0.2 20 Iron 1150 50.0 ug/L 1000 90.7 106 75-125 0.09 20 Lead 197 10.0 ug/L 200 3.10 U 99 75-125 1 20 Zinc 207 10.0 ug/L 200 4.40 U 104 75-125 1 20 Post Spike (6E23009-PS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:07 Source: CZ06979-01 Spike Source %REC RPD Anaivte Result Flag FQL Units Level Result %REC Limits RPD Limit Notes Cadmium 0.0204 0.00100 mg/L 0.0200 0.000188 101 80-120 Copper 0.188 0.0100 mg/L 0.200 -0.00188 94 80-120 Iron 1.13 0.0500 mg/L 1.00 0.0907 103 80-120 Lead 0.193 0.0100 mg/L 0.200 0.000946 96 80-120 Zinc 0.204 0.0100 mg/L 0.200 0.00204 101 80-120 Classical Chemistry parameters - Quality Control Batch 6E23004 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 �4Y�A9ry � q+wRti. QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E23004 - NO PREP - Continued Blank (6E23004-BLK1) Prepared & Analyzed: 05/23/2016 10:30 Spike Source %REC RPD Arlalvte Result Flag Q(2-L U2t5 Level Res I %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (6E23004-B51) Prepared & Analyzed: 05/23/2016 10:30 Spike Source %REC RPD -An MC ReSNIt ELau PQL units Level Result a/aREC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 103 80-120 Duplicate (6E23004-DUP3) Prepared & Analyzed: 05/23/2016 10:30 Source: C512441-01 Spike Source %REC RPD Analvte Resul Flaa PQL Units Level Resul %REC imi RPD LimitNotes Total Suspended Solids 410 33 mg/L 440 8 20 Duplicate (6E23004-DUP2) Prepared & Analyzed: 05/23/2016 10:30 Source:CZ05961-01 Analtde Total Suspended Solids Batch 6E2303O - Same Result Elan P% 210 100 Spike Source a/oREC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 210 0 20 Blank (6E23030-BLKl) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Analvte Result 1la3 PQL Units Level Result a/oREC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (6E23030-BS1) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Analvte Result Ban P_OL Units Level Result a/aREC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (6E23030-MS3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source:CS12441-01 Spike Source %REC RPD Analvte Result Bag P% Units Level Resul %REC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 35 97 90-110 Matrix Spike Dup (6E23030-MSDi) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Spike Source %REC RPD —Anabde Result Flag POL Wilt$ Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 560 10 mg/L 526 35 100 90-110 3 10 Classical Chemistry Parameters - Quality Control Batch 6E24002 - EPA 1664A Blank (6E24002-BLKl) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Analvte Oil & Grease (HEM) Result F_las POI 0.613 U 1.28 Spike Source %REC RPD Units Level Res %REC Limits RPD Limit mg/L Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E24002 - EPA 1664A - Continued LCS (6E24002-BSI) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Analidg Result Flaci P_0L lJIM Level Result %REC Limits RPD Llflig Notes Oil & Grease (HEM) 154 5.00 mg/L 159 97 78-114 LCS Dup (6E24002-BSDi) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Analvte Rasu t 11as ROL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 156 5.00 mg/L 160 98 78-114 2 18 Matrix Spike (6E24002-MSi) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Source: BZ02144-01 Anal Oil & Grease (HEM) Spike Source %REC RPD ReSul F a4 PL Unite Level Result %REC Limits RPD Limit Notes 155 5.00 mg/L 148 2.40 U 105 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 3. ENViRONMEN* CONSERVATION LABORATC RIES °CHAIN OF-Ct#STODY RECURD; +riiiw encolabs:corrk: F;_ s,,�' � tQT75��nrtif'utj.f°ir - uifi2Gr+.uuval'illx'Cair7�uctl:.s' tC,fi�liotlttrn�y&Irid�i5rrdfCi htA!iofw ifn FL 322 .. .i�0?1 26 ri,'iid � alr l94 }d1Sti ti aE! 59(Pt .?Jti,!UW Fak_t 0+}12L�6-F21Q. (gi91 t•'trt iliil};tx7vil`a15- Pag+; ol. fizr{il•iSitFml.lixc;ifLtj' i�ifii_t`l�tltj' f.�llTat7)L'a;s'�G4tGIAi.i�rz�ti�l?fi RC(ti;�rr.It9Cti1�� lirls'i uiSftaG��/ '=ietilnquKilali riy:: ... .. : iDtirit l>31'dt: i3.lrlhRllrtR:' rt<i:;t�t�,E# IYt fly' ' �ffi :iln rlflli!gUeSleEitl �F>. - 1l�tiNFuttc-= --_ net=Slw,i3 t7Y: �dlafTinig. .. Gcoly W*;, Trmpu tii3.nL�dipl. ,..., _: ,. ... s; Ixlti.Ui?Ytt �CCStt.. - .. —Mcoptable _.Unac eplable r letriii„-G6F ulctuiul•r+Kl+r SO�;uiit p1Ne17Mhiru YYi{I�9t: -SE i.WUSf�?Ii SVJ gi::;t�ica Yt2lsit:{"11V Wa-taiwver"A•htr O-UtftSr tClEifiil tit 401gfnnni5l>PrClteNbt4t7iY 1 ICN IS-f Gl N#1:Y03 5 H25r}t NPTJ� LJii O'lXi:cr_�IKtbli fti rAminanral. . .. .. .. .. , . , - Nta1�R .11d ;impics:sutii �r�:ds ENO F.uhrr_are i:t'icieadans+a w„n�:i+c' a.•ira biiii:�iiyfiliURs IiSIeO-oRblteYr�ratr�air' pn� igrm ,aiie.s Fw,a*w7;t�i a jiae7�enis,l�i� . Sample Prer�erva Lion VerificAtiah ENCO°Cary` 11Uork Order: G512441. Projec.I St 'liter Ghent: Weiis el[Ai t kecovery,C6 ter`{WED1:2j Pro�ecfl* [h6, L9990h 1*May-16 14;41 I_aggi d By; Andrdw,S goons +CM 2441-Oi :Rea 'ent-Name' ID Reagent Name .. 10 ... . 2 4 E Lab, Qmt e d` t; Timely. R o a. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, May 31, 2016 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): C512441 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, May 19, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Ouitfall2 Lab ID: C312441-01 Sampled: 05/19/1611:30 Received: 05/19/16 13:55 Parameter Hold Date/Time(s) Prep Date/Time(sl Analysis Date/Time(s) EPA 1664E 06/16/16 05/24/16 15:13 05/25/16 18:39 EPA 6010D 11/15/16 05/23/16 09:12 05/24/16 10:12 SM 254OD-1997 05/26/16 05/23/16 10:30 05/23/16 10:30 SM 5220D-1997 06/16/16 05/23/16 15:52 05/24/16 10:17 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 of 9 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: C512441-01 AnaUdli Results Fig hMD P4 Units Method Notes Chemical Oxygen Demand 35 10 10 mg/L SM 5220D-1997 Copper - Total 17.4 1.60 10.0 ug/L EPA 6010D Iron - Total 6370 22.0 50.0 ug/L EPA 6010D Lead - Total 5.16 J 3.10 10.0 ug/L EPA 6010D Total Suspended Solids 440 33 33 mg/L SM 254OD-1997 Zinc - Total 85.5 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 ANALYTICAL RESULTS Description: Outfall 2 Lab Sample ID:C512441-01 Received: 05/19/16 13:55 Matrix: Surface Water Sampled:05/19/16 11:30 Work Order: C512441 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - SWO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL PPL Batch Method Analyzed Notes Cadmium [7440 43-9]^ 0.360 U ug/L 1 0.360 1.00 6E23009 EPA 6010D 05/24/16 10:12 JDH Copper[7440-50-8]^ 17.4 ug/L 1 1.60 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Iron [7439-89-6]^ 6370 ug/1- 1 22.0 50.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Lead [7439-92-1]1 5.16 J ug/L 1 3.10 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Zinc[7440-66-6]^ 85.5 ug/L 1 4.40 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH JClassical Chemistry Parameters 1 ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Number] Results FLga UnitsRE MDL E Batch Method A! ft Notes Chemical Oxygen Demand^ 35 mg/L 1 10 10 6E23030 SM 5220D-1997 05/24/16 10:17 JOC Total Suspended Solids^ 440 mg/L 13.3 33 33 6E23004 SM 254OD-1997 05/23/16 10:30 MMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte fCAS Numberl Results flpg Units DF MDL SQL Batch Method Analyze JX Notes Oil & Grease (HEM)[C-0007]^ 0.629 U mg/L 0.262 0.629 1.31 6E24002 EPA 16646 05/25/16 18:39 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 6E23009 - EPA 3005A Blank (6E23009-BLK3) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 09:53 Spike Source %REC RPD .Analvte Result of P-0L Units Level Resul %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (6E23009-BS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 09:57 Spike Source %REC RPD An lute_ Result Flaa PQL LlniU Level Res %REC Limits RPD Limit Notes Cadmium 20.1 1.00 ug/L 20.0 101 80-120 Copper 192 10.0 ug/L 200 96 80-120 Iron 1010 50.0 ug/L 1000 101 80-120 Lead 198 10.0 ug/L 200 99 80-120 Zinc 200 10.0 ug/L 200 100 80-120 Matrix Spike (6E23009-MS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:02 Source:CZ06979-01 Spike Source %REC RPD Analyt R su t F a9 POL Unity Level Resul %REC Limits RPD Limit Notes Cadmium 20.8 1.00 ug/L 20.0 0.360 U 104 75-125 Copper 192 10.0 ug/L 200 1.60 U 96 75-125 Iron 1150 50.0 ug/L 1000 90.7 106 75-125 Lead 199 10.0 ug/L 200 3.10 U 100 75-125 Zinc 205 10.0 ug/L 200 4.40 U 103 75-125 Matrix Spike Dup (6E23009-MSD1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:05 Source: CZ06979-01 Spike Source %REC RPD Anal vte Result ElA9 P96 Units Level Result %REC Limits RPD Limit Notes Cadmium 20.6 1.00 ug/L 20.0 0.360 U 103 75-125 0.9 20 Copper 193 10.0 ug/L 200 1.60 U 96 75-125 0.2 20 Iron 1150 50.0 ug/L 1000 90.7 106 75-12-5 0.09 20 Lead 197 10.0 ug/L 200 3.10 U 99 75-125 1 20 Zinc 207 10.0 ug/L 200 4.40 U 104 75-125 1 20 Post Spike (6E23009-PSI) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:07 Source: CZ06979-01 Spike Source %REC RPD Analvte Result flag PZL Unite Level Result %REC Limits RPD Limit Notes Cadmium 0.0204 0.00100 mg/L 0,0200 0.000188 101 80-120 Copper 0.188 0.0100 mg/L 0.200 -0.00188 94 80-120 Iron 1.13 0.0500 mg/L 1.00 0.0907 103 80-120 Lead 0.193 0.0100 mg/L 0,200 0.000946 96 80-120 Zinc 0.204 0.0100 mg/L 0.200 0.00204 101 80-120 Classical Chemistry Parameters - Quality Control Batch 6E23004 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 I QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E23004 - NO PREP - Continued Spike Source %REC RPD A an AC Result flag POLL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 103 80-120 Duplicate (6E23004-DUPl) Prepared & Analyzed: 05/23/2016 10:30 Source: C512441-01 Spike Source %REC RPD AnajAe Re ul Flaa PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 410 33 mg/L 440 8 20 Duplicate (6E23004-DUP2) Prepared &Analyzed: 05/23/2016 10:30 Source: CZ05961-01 .Anallfsg Total Suspended Solids Batch 6E23030 - Same Result flag POL 210 100 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 210 0 20 Spike Source %REC RPD Anal vte Result Elan P% Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90.110 Matrix Spike (6E23030-MS1) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Spike Source %REC RPD Analvte Result Flaci POL Units Level Resol o/aREC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 35 97 90-110 Matrix Spike Dup (6E23030-MSDi) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Spike Source %REC RPD Anal vte Result Elag P4L Units Level Resul o/.REC Limits RPD Limit Notes Chemical Oxygen Demand 560 10 mg/L 526 35 100 90-110 3 10 Classical Chemistry Parameters - Quality Control Batch 6E24002 - EPA 1664A Blank (6E24002-BLKl) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Anal vte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 0.613 U 1.28 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E24002 - EPA 1664A - Continued LCS (6E24002-B51) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Analvte Result Flag P L Units Level Resul %REC Limits RPD Lima Notes Oil & Grease (HEM) 154 5.00 mg/L 159 97 78-114 LCS Dup (6E24002-BSD1) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Analvte Result fl34 P_0L units Level ggsul %REC Limits RPD Limit Notes Oil & Grease (HEM) 156 5.00 mg/L 160 98 78-114 2 18 Matrix Spike (6E24002-MS1) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Source: BZ02144-01 Spike Source %REC RPD Analyte Result Flan FQ Units Level Re ul %REC Limits RPD Limit Notes Oil & Grease (HEM) 155 5.00 mg/L 148 2.40 U 105 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTTAL.CONSEFiVATllp "k3ORATORIES .CHAIN OF.-C!USTODY RECQRD +w►utirwencnfab5.[onk ,.� rt� '1Q7i5 Gem nl FUt'g 1?e ' ' - FCt 7I) Ge+.ui+� I'c1}ti CtiuH �o�e �t_11 �5F1 A 14U6r•Trr'i �n5_ Intl+(a,++�i Cis %i r• Wlmiidt. F L "f2@:A' i f{t !r?i w tlry FL 32:'.3f i�Ftrli` �ai� Ni �l? t.[ (gOZ1826-53 t ,f<r(aA7j'lUt4ti8 i {9q4 i�s,J667-F&i 0!j2�667i0; {9>9}d&7]+l#i 7ttrtf�/47}.d[iiJ i�IS P�g�.:: Of iril{i# Rmpl c+l L3j' .. (et+;i"T mtj+:. Fir lr+ uta++eti B/ r rt - _- CiEmqu� 116 IR v,>..H .� t:✓'n117147+g�+jeflGi ! lafsc� lux? fGccjsrc+nur+t 4c+ftngt+M;ha+t. Fly',' .. it:t a.'Pi,r,%- - -. +MR fly •. ... - .. - ala Inl+r 17glihcju Bled Pp' L�17+t i+mc". _ neceivt !t th OaIdPFime - S Tenip+t a+a.neceipl - _ jcQlAwon um) iinCD6'K.. - ..... Acce0thble Unn.0 eplable FAsUix.: GW-Gipu+`xJr.�+tr+ SO?tioii pW>f7r;,+xinr VYulr i. o^E S eMlpVa SYf Efr;tar:,fr V�afttr-WIV V gr!Mwzic A Mr;,..0-C7tftpf; iClaia+t fn-CURIrt+(ts+ta�,+. "Pna tYOtian '4•IC{i•_N-YGI N�F+.XO;3 S=M S(i++ NgrNagH OAXImr tnetBR in COM-nent96 Na1n : A� ,+mpie t:sutira6it d it pNirO t utts are in 3, o dartco vv is 7Fte axrn3 sind:iYr , lifit+ listcm_an S±ie rCsyrVq th+z httra s ICag prw xxstte t ag+oenr nts wif Sample Preservation Verification 4 E!NCOJ Cary Work Order. C512441. Proaect; S#arrriwater 'Clisnt 1Nesbe11,Asset keii'' fiery Center'(WEO 2); pF6K #.#:: IMP. : Lagged Im' 19-May-16 14.41 Logged By Andt6 S Coons C512441-Qi b max+ a {of �� iiru $til1�aFk��6i��' ... aiU�ri=%= .. s A 1 LA-+H2SO4 2 „Y a ;N l h7A `Y r! NA 1 LA+H2S O4: <2 Y t N.:; : 1+Ir . ' Y a N :. MA D + 250rriLP+Ff2St34. <2 Y �a N' 7 NA :Y t N E 2'5CrnLP+HN.OS,• <2 Y1a N ! 'NA :Y ti+.rJ" NA :Rea lent Name la Rea ent Name,_ !© 2' 4` 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, April 11, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CA00098 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, March 28, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall2 Lab ID: CA00098-01 Sampled: 03/28/17 09:00 Received: 03/26/17 14;34 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 16648 04/25/17 03/30/17 14:00 03/31/17 15:49 EPA 6010D 09/24/17 04/03/17 09:10 04/04/17 11:01 SM 254OD-1997 04/04/17 03/29/17 11:40 03/29/17 11:40 SM 5220D-1997 04/25/17 04/03/17 12:47 04/03/17 16:15 Client ID: Outfall 1 Lab ID: CA00098-02 Sampled: 03/28/17 09:00 Received: 03/28/17 14:34 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 04/25/17 03/30/17 14:00 03/31/17 15:49 EPA 6010D 09/24/17 04/03/17 09:10 04/04/17 11:03 SM 254OD-1997 04/04/17 03/29/17 11:40 03/29/17 11:40 SM 5220D-1997 04/25/17 04/03/17 12:47 04/03/17 16:15 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: CA00098-01 Analvte Results EWS L L Units Method Notert Cadmium - Total 0.598 1 0.450 2.00 ug/L EPA 6010D Chemical Oxygen Demand 45 10 10 mg/L SM 5220D-1997 Copper- Total 51.3 0.870 10.0 ug/L EPA 6010D Iron - Total 10700 6.00 50.0 ug/L EPA 6010D Lead - Total 12.4 3.80 10.0 ug/L EPA 6010D Oil & Grease (HEM) 3.15 3 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 880 50 50 mg/L SM 2S40D-1997 Zinc - Total 116 6.30 10.0 ug/L EPA 6010D Client ID: Outfall 1 Lab ID: CA00098-02 Analvte Resul Flag IML E" Units Method Notes Cadmium - Total 0.553 J 0.450 2.00 ug/L EPA 6010D Chemical Oxygen Demand 37 10 10 mg/L SM 5220D-1997 Copper- Total 12.2 0.870 10.0 ug/L EPA 6010D Iron -Total 5670 6.00 50.0 ug/L EPA 6010D Total Suspended Solids 520 50 50 mg/L SM 254OD-1997 Zinc - Total 69.0 6.30 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 i (Classical Chemistry Parameters ^ - ENCO Cary certified analyze [NC 5911 Analyte rCAS Numberl Results Flaa Units DF MDL PPOL Batch Method Analyzed By Notes Chemical Oxygen Demand^ 45 mg/L 1 10 10 7DO3022 SM 5220D-1997 04/03/17 16:15 30C Total Suspended Solids^ 880 mg/L 20 50 50 7C29W3 SM 2S40D-1997 03/29/17 11:40 OMR Metals (total recoverable) by EPA 6000/7000 Series Methods - ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Results fin Units RE MDL M Batch Method Analyzed @� Notes Cadmium [7440-43-9]^ 0.598 J ug/L 1 0.450 2.00 7DO3002 EPA 6010D 04/04/17 11:01 ACV Copper[7440-50-8]^ 51.3 ug/L 1 0.870 10.0 7DO3002 EPA 6010D 04/04/17 11:01 ACV Iron [7439-89-6]^ 10700 ug/L 1 6.00 50.0 7DO3002 EPA 6010D 04/04/17 11:01 ACV Lead [7439-92-1]^ 12.4 ug/L 1 3.80 10.0 7DO3002 EPA 6010D 04/04/17 11:01 ACV Zinc [7440-66-6]^ 116 ug/L 1 6.30 10.0 7DO3002 EPA 6010D 04/04/17 11:01 ACV Classical Chemistry Parameters ^ - ENCOJackson ville certified analyze [NC 442] Analyte rCAS Numberl Results Els Units pE MDL P L Batch Method Analned ft Notes Oil & Grease (HEM) [C-0007]^ 3.15 J mg/L 1 2.40 5.00 7C29011 EPA 1664E 03/31/17.15:49 SMA Description: Outfall 1 Lab Sample ID:CA00098-02 Received: 03/28/17 14:34 Matrix: Surface Water Sampled:03/28/17 09:00 !Mork Order: CA00098 Project: Stoanwater Sampled By: Diane Bell Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyze rCAS Numberl Results Flag Units DF MDL POL, Batch Method Analyzed ft Notes Chemical Oxygen Demand^ 37 mg/L 1 10 10 7DO3022 SM 522OD-1997 04/03/17 16:15 JOC Total Suspended Solids^ 520 mg/L 20 50 50 7C29003 SM 254OD-1997 03/29/17 11:40 OMR Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Results FFdg Units DF MDL POLL Batch Method Anahrred Notes Cadmium [7440-43-9]^ 0.553 3 ug/L 1 0.450 2.00 7DO3002 EPA 6010D 04/04/17 11:03 ACV Copper[7440-50-8]^ 12.2 ug/L 1 0.870 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Iron [7439-89-6]^ 5670 ug/L 1 6.00 50.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Lead [7439-92-1]^ 3.80 U ug/L 1 3.80 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Zinc (7440-66-6]1 69.0 ug/L 1 6.30 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 4421 Analyte rCAS Numberl Results Eta Units DF MDL POL Batch Method Analyzed Ay Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7C29011 EPA 1664E 03/31/17 15:49 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7C29003 - NO PREP Blank (7C29003-BLKi) Prepared & Analyzed: 03/29/2017 11:40 Spike Source %REC RPD A talybe Result flag P2 UrLuts Level Result °/a REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7C29003-BS1) Prepared & Analyzed: 03/29/2017 11:40 Spike Source %REC RPD A�t7Jyle Result Flan P-0L ni Level Result %REC LWtits RPD Limit es Total Suspended Solids 94 2.5 mg/L 100 94 80-120 Duplicate (7C29003-DUPl) Prepared & Analyzed: 03/29/2017 11:40 Source: CA01293-01 Spike Source %REC RPD An a L Units REC Limits RPD Notes Total Suspended Solids 120 33 mg/L 120 0 20 Duplicate (7C29003-DUP2) Prepared & Analyzed: 03/29/2017 11:40 Source: CA01316-01 Spike Source %REC RPD -Anal vte Result flag POL Units Level Result %REC Limit. RPD Limit Notes Total Suspended Solids 320 50 mg/L 280 1.3 20 Batch 7DO3022 - Same Blank (7D03022-BLK3) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Spike Source NORK RPD Analvte Resul Flan PQL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7D03022-BS3) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Spike Source %REC RPD Aslahft ft$M t E49 PQL Units Level Resul %REC Limits RPD Limit Notes Chemical Oxygen Demand S10 10 mg/L 500 101 90-110 Matrix Spike (7D03022-MS1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Source: CA00098-01 Spike Source %REC RPD Analvte Result El49 P-" Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 590 10 mg/L 526 45 103 90-110 Matrix Spike Dup (7D03022-MSD1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Source:CA00098-01 Spike Source %REC RPD _AnaNN Result flag POL Units Level Kesul %REC Limits RPD Lim" Notes Chemical Oxygen Demand 590 10 mg/L 526 45 103 90-110 0 10 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7D03002 - EPA 3005A Blank (7D03002-BLK3) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:55 Spike Source %REC RPD Anatyte Result Elan POL Units Level Result %REC Limits RPD Limit otes cadmium 0.717 3 2.00 ug/L Copper 0.870 U 10.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 _ -gym IN 21 Spike Source %REC PPD -Anal Result Flag POL units Level Resul %REC Unnits RPD UMA Notes Iron 6.00 U 50.0 ug/L Lead 3.80 U 10.0 ug/L Zinc 6.30 U 10.0 ug/L LCS (7D03002-BS1) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:57 Spike Source %REC RPD -Anal vte Result Elan POL Units Level Resul %REC ki[IJU RPD Limit Notes Cadmium 51.6 2.00 ug/L 50.0 103 ' 80-120 Copper 507 10.0 ug/L 500 101 80-120 Iron 2530 50.0 ug/L 2500 101 80-120 Lead 511 10.0 ug/1- 500 102 80-120 Zinc 514 10.0 ug/L 500 103 80-120 Matrix Spike (71)03002-MS1) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:58 - Source: BA01391-01 Spike Source %REC RPD AeaivSe.. Result flag PQL Units Level Result %REC LiMits RPD umit Notes Cadmium 51.5 2.00 ug/L 50.0 0,873 101 75-125 Copper 818 10.0 ug/L 500 328 98 75-125 Iron 7490 50.0 ug/L 2500 5050 98 75-125 Lead 602 10.0 ug/L 500 74.1 106 75-25 Zinc 858 10.0 ug/1- 500 382 95 75-125 Matrix Spike Dup (7D03002-MSD1) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 11:00 Source: BA01391-01 Spike Source %REC RPD Anobte Result Rao POL UjIits Level Re %REC Limits RPD limit Notes Cadmium 51.5 2.00 ug/L 50.0 0.873 101 75-125 0.09 20 Copper 829 10.0 ug/L 500 328 100 75-125 1 20 Iron 7590 50.0 ug/L 2500 5050 102 75-125 1 20 Lead 601 10.0 ug/L 500 74.1 105 75-125 0.1 20 Zinc 876 10.0 ug/L 500 382 99 75-125 2 20 Classical Chemistry Parameters - Quality Control Batch 7C29011 - EPA 1664E Blank (7C29011-BLKl) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD Analvie R€ ult Rao P-QL Units Level Resul %REC Limits RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7C29011-BS1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD Anahcte R_esul Flag POL Units Level Result o/aREC Limits RPD limit Notes Oil & Grease (HEM) 138 5.00 mg/L 147 94 78-114 LCS Dup (7C29011-BSD1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD AQalvte Result Elan Pot Hosts Level Resul %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 � s www.encolabs.com Spike Source %REC RPD Aiitp _e Rewdt Flaa P4L Units Level Result %REC Limits RPD Limit Notes Oil& Grease (HEM) 130 5,00 mg/L 148 88 78-114 6 18 Matrix Spike (7C29011-MS1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Source: BA01298-01 Spike Source %REC RPD —Analvte Result Raa P41 Units Level Result %REC Limits RPD Lmil Notes Oil & Grease (HEM) 135 5.00 mg/L 153 2.40 U 89 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 I, � i too Al, Mn .;,, .. . z�m �xt,�p j ! d �3 e� i I'V ENCOLaboratorie-S, Accurate. Timely. Respos .Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, April 11, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CA00098 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, March 28, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 1 SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall2 Lab ID: CA00098-01 Sampled: 03/28/17 09:00 Received: 03/28/17 14:34 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 04/25/17 03/30/17 14:00 03/31/17 15:49 EPA 6010D 09/24/17 04/03/17 09:10 04/04/17 11:01 SM 254OD-1997 04/04/17 03/29/17 11:40 03/29/17 11:40 SM 5220D-1997 04/25/17 04/03/17 12:47 04/03/17 16:15 Client ID. Outfall 1 Lab ID: CA00098-02 Sampled: 03/28/17 09:00 Received: 03/28/17 14:34 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 04/25/17 03/30/17 14:00 03/31/17 15:49 EPA 6010D 09/24/17 04/03/17 09:10 04/04/17 11:03 SM 254OD-1997 04/04/17 03/29/17 11:40 03/29/17 11:40 SM 5220D-1997 04/25/17 04/03/17 12:47 04/03/17 16:15 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: CA00098-01 Anal vte Results Flag MDL P2 Units Method Notes Cadmium - Total 0.598 1 0.450 2.00 ug/L EPA 6010D Chemical Oxygen Demand 45 10 10 mg/L SM 5220D-1997 Copper - Total 51.3 0.870 10.0 ug/L EPA 6010D Iron - Total 10700 6.00 50.0 ug/L EPA 6010D Lead - Total 12.4 3.80 10.0 ug/L EPA 6010D Oil & Grease (HEM) 3.15 3 2.40 5.00 mg/L EPA 1664E Total Suspended Solids 880 50 50 mg/L SM 2540D-1997 Zinc - Total 116 6.30 10.0 ug/L EPA 6010D Client ID: Outfall 1 Lab ID: CA00098-02 Analvte Results Flag MDL fpyl Units Method Notes Cadmium - Total 0.553 3 0.450 2.00 ug/L EPA 6010D Chemical Oxygen Demand 37 10 10 mg/L SM 5220D-1997 Copper- Total 12.2 0.870 10.0 ug/L EPA 6010D Iron - Total 5670 6.00 50.0 ug/L EPA 6010D Total Suspended Solids 520 50 50 mg/L SM 254OD-1997 Zinc - Total 69.0 6.30 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591J Analyte rCAS Numberl Results FLaq Units DF MDL POL, Chemical Oxygen Demand^ 45 mg/L 1 10 10 Total Suspended Solids^ 880 mg/L 20 50 50 Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Jacksonville certified analyte [NC 442] Analyte fCAS Numberl Results fin Units pf MDL E% Cadmium [7440-43-9]1 0.598 J ug/L 1 0.450 2.00 Copper[7440-50-8]^ 51.3 ug/L 1 0.870 10.0 Iron [7439-89-6]^ 10700 ug/L 1 6.00 50.0 Lead [7439-92-1]1 12.4 ug/L 1 3.80 10.0 Zinc[7440-66-6]^ 116 ug/L 1 6.30 10.0 Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 4421 Batch Method . Analyzed —By Notes 7DO3022 SM 5220D-1997 04/03/17 16:15 JOC 7C29003 SM 254OD-1997 03/29/17 11:40 OMR Batch Method Analyzed ft Notes 7DO3002 EPA 6010D 04/04/17 11:01 ACV 7DO3002 EPA 6010D 04/04/17 11:01 ACV 7DO3002 EPA 6010D 04/04/17 11:01 ACV 7DO3002 EPA 6010D 04/04/17 11:01 ACV 7DO3002 EPA 6010D 04/04/17 11:01 ACV Analyte rCAS Numberl Results fI g Units pf MDL POL Batch Oil & Grease (HEM) [C-0007]1 3.15 J mg/L 1 2.40 5.00 7C29011 Description: Outfall 1 Lab Sample ID: CA00098-02 Matrix: Surface Water Sampled:03/28/17 09:00 Project: Stormwater Sampled By: Diane Bell Method Analyzed fL Notes EPA 1664B 03/31/17 15:49 SMA Received: 03/28/ 17 14:34 Work Order: CA00098 Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Vil g Units pE MDL POL Batch Method Analyzed �y Notes Chemical Oxygen Demand^ 37 mg/L 1 10 10 7DO3022 SM 522OD-1997 04/03/17 16:15 JOC Total Suspended Solids^ 520 mg/L 20 50 50 7C29003 SM 254OD-1997 03/29/17 11:40 OMR Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Jacksonville certified analyte [NC 442] Anahrte KAS Numberl Results F_[_ga Units DF MDL POL Batch Method Analyzed Notes Cadmium [7440-43-9]^ 0.553 J ug/L 1 0.450 2.00 7D03002 EPA 6010D 04/04/17 11:03 ACV Copper[7440-50-8]^ 12.2 ug/L 1 0.870' 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Iron [7439-89-6]^ 5670 ug/L 1 6.00 50.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Lead [7439-92-1]^ 3.80 U ug/L 1 3.80 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Zinc[7440-66-6]^ 69.0 ug/L 1 6.30 10.0 7DO3002 EPA 6010D 04/04/17 11:03 ACV Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyze [NC 442] Analyte rCAS Numberl Results Elpg Units RE MDL POL Batch Method Analyzed ly Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7C29011 EPA 1664B 03/31/17 15:49 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Spike Source %REC RPD Analvte Re —suit Flan POL Units Level Resul %REC Limits RPD LLMA Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7C29003-BS1) Prepared & Analyzed: 03/29/2017 11:40 Spike Source %REC RPD A_na_ivte Result Hag M yIlits Level Result %REC Limits RPD Lmft Notes Total Suspended Solids 94 2.5 mg/L 100 94 80-120 Duplicate (7C29003-DUPl) Prepared & Analyzed: 03/29/2017 11:40 — Source: CA01293-01 Spike Source %REC RPD Anaa Result Flaq POL Units Level Result %REC Limits RPD 'mi Notes Total Suspended Solids 120 33 mg/L 120 0 20 Duplicate (7C29003-DUP2) Prepared & Analyzed: 03/29/2017 11:40 Source: CA01316-01 Spike Source %REC RPD A�VAe Result Elm POL Unuits Level Result %REC Limits RPD Limit Notes Total Suspended Solids 320 50 mg/L 280 13 20 Batch 7DO3022 - Same Blank (7D03022-BLK1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Spike Source %REC RPD A_nalyte Result Hag POL Units Level Resin %REC Limits RPD L!Mft Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7D03022-BS1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Spike Source %REC RPD -Analvte Result Elag POL Knits Level Result %REC Limits RPD LMA Notes Chemical Oxygen Demand 510 10 mg/L 50D 101 90-110 Matrix Spike (7D03022-MS1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Source: CA00098-01 Spike Source %REC RPD Analvte Result flag POL Units Level Result %REC 'Limits RPD Limit Notes Chemical Oxygen Demand 590 10 mg/L 526 45 103 90-110 Matrix Spike Dup (7D03022-MSD1) Prepared: 04/03/2017 12:47 Analyzed: 04/03/2017 16:15 Source: CA00098-01 Spike Source %REC RPD A-nWv s Result flag POL Units Level Resul %REC Limits RPD kimft Notes Chemical Oxygen Demand 590 10 mg/L 526 45 103 90-110 0 10 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7DO3002 - EPA 3005A Blank 17D03002-BLK1) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:55 Spike Source %REC RPD Anal vte Result Ea_q P_QL Units Level Result %REC Limits RPD LIMil Notes Cadmium 0.717 3 2.00 ug/L Copper 0.870 U 10.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 IIIAI1�ni6 is �m�� .fib QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7D03002 - EPA 3005A - Continued Blank (7D03002-BLK1) Continued Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:55 Spike Source %REC RPD Analyte Result flag FQL Units Level Result °/aREC Limits RPD Limit Notes Iron 6.00 U 50.0 ug/L Lead 3.80 U 10.0 ug/L Zinc 6.30 U 10.0 ug/L LCS (7D(113002-BSI) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:57 Spike Source %REC RPD AnalAe Result Rag POL Units Level Result %REC Limits RPD Limit Notes Cadmium 51.6 2.00 ug/L 50.0 103 80-i20 Copper 507 10.0 ug/L 500 101 80-120 Iron 2530 50.0 ug/L 2500 101 80-120 Lead 511 10.0 ug/L 500 102 80-120 Zinc 514 10.0 ug/1- 500 103 80-120 Matrix Spike (7D03002-MS1) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 10:58 Source:BA01391-01 Spike Source %REC RPD Anal vte Result Flag P-QL Units Level Result %REC Limits RPD Limit Notes Cadmium 51.5 2.00 ug/L 50.0 0.873 101 75-125 Copper 818 10.0 ug/L 500 328 98 75-125 Iron 7490 50.0 ug/L 2500 5050 98 75-125 Lead 602 10.0 ug/L 500 74.1 106 7 i25 Zinc 858 10.0 ug/L 500 382 95 75-125 Matrix Spike Dup (7D03002-MSDi) Prepared: 04/03/2017 09:10 Analyzed: 04/04/2017 11:00 Source; BA01391-01 Spike Source %REC RPD _Analyse RReSSIit Flag PQL Units Level esul %REC Limits RPD mi es Cadmium 51.5 2.00 ug/L 50.0 0.873 101, 75-125 0.09 20 Copper 829 10.0 ug/L Soo 328 100 75-125 1 20 Iron 7590 50.0 ug/L 2500 5050 102 75-125 1 20 Lead 601 10.0 ug/L 500 74.1 105 75-125 0.1 20 Zinc 876 10.0 ug/1- 500 382 99 75-125 2 20 Classical Chemistry Parameters - Quality Control Batch 7C29011 - EPA 1664B Blank (7C29011-BLK1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD �lnalvte Result Hag POL units Level Res 1 %REC Limits RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7C29011-BS1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD Anal vte Result Ebm PQL U1its Level Result o/aREC Limits RPD Limit Notes Oil & Grease (HEM) 138 5.00 mg/L 147 94 78-114 LCS Dup (7C29011-BSD3) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD Anal vte Result ELeg PF-QL Units Level Result o/aREC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7C29011 - EPA 1664B - Continued LCS Dup (7C29011-BSD1) Continued Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Spike Source %REC RPD Anal vte Result fla4 P_oL Units Level Result %REC Limits RPD LimA Notes Oil & Grease (HEM) 130 5.00 rri 148 88 78-114 6 18 Matrix Spike QC29011-MS1) Prepared: 03/30/2017 14:00 Analyzed: 03/31/2017 15:49 Source: BA01298-01 Spike Source °/uREC RPD -Analvft ResulS flag pot Units Level Result '/oREC Limits RPD Linift Notes Oil & Grease (HEM) 135 5.00 mg/L 153 2.40 U 89 78-114 FINAL - This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 z B D J u E MRL N P FLAGS/NOTES AND DEFINITIONS The analyte was detected in the associated method blank. The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation.. data and moisture content, where applicable. The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC co;umn. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 tic ' ax �:�si8`a9 ��Y��a ? y a ¢� Fu$i7��r'�``-�. � 4'k are✓�PT4Ej�agy�� �i/ �E d 3, D5Y7M 8f ��d� ,F�..��°»i f� "� Vim, � ����� - - #'S 8 #'Yyi - O�P'wX+',+irpf4'. '`qT�"'�.8) ,,L'L 4 V&1,LR:iri `' Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted CERTIFICATE OF COVERAGE NO. NCG200 -5 -9 _� FACILITYNAME (,,.Ie5bell SnU�s�►�.nf /)ecUvc/C./ COUNTY ► & rS 0e\ PERSON C `ULLECTING SAMPLES _J ars .61-( LABORATORY C AJUJ Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR aZ U I SAMPLE PERIOD VOJ n-June ❑ Juiy-Dec _or onthly' (month) IVDISGHARGING TO CLASS ❑ORW HQW [:]Trout ❑PNA a ❑Zero -flow ❑Water supply ❑SA AUG 28 Zt1i% ❑Saltwater ❑Other DI/vR SECT1.11 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L' 0.126 mg/L or 0.090 mg/L' og-� t 3, o CX-) 0.003 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 247hour rainfall amount, Inches Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L4 Footnotes from Part A also apply to this Part B Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Dee IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Permit Date: 02/02/2015-12/31/2019 ( Date) SWU-256, last revised 1/28/2015 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted�— CERTIFICATE OF COVERAGE NO. NCG200 5 -e _-4- FACILITY NAME Wet -belt T.I'lU�si wtrn j- /}eCt�yc /`C./ COUNTY LAC r_SCJe\ PERSON c6LLECTING SAMPLES -At LABORATORY C/l_U Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR oZU I SAMPLE PERIOD VMonthlyl n-June ❑ July -Dec or month DISCHARGING TO CLASS ❑ORW HQW ❑Trout ❑PNA ❑Zero -flow [:]Watersupply [:]SA ❑Saltwater ❑Other PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L' 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 o$-� U .lv I -i•3 o•W - v•uv3 U•v5 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L4 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO LK IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail anoriginal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Permit Date: 02/02/2015-12/31/2019 (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 {/jam► ��-^''...:.:4 H< F i sf _� 7k J F- i777 A � I III: r.' �p PCd - r NCO, , 'Os TNI Accurate. eil . Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, August 18, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CA08431 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, August 8, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 (EJ�Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OUTFALL 1 Lab ID: CA08431-01 Sampled: 08/07/17 08:45 Received: 08/08/17 14:30 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 09/04/17 08/16/17 15:53 08/17/17 16:17 EPA 6010D 02/03/18 08/09/17 08:07 08/14/17 13:38 EPA 6010D 02/03/18 08/14/17 15:04 08/17/17 11:59 SM 2540D-1997 08/14/17 08/10/17 10:50 08/10/17 10:50 SM 5220D-1997 09/04/17 08/14/17 12:17 08/14/17 18:00 FINAi_ This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 2 of 9 (IF www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: OUTFALL 1 Lab ID: CA08431-01 Anal vte Results _FIM MIL POL Ynits Mstiod Note Chemical Oxygen Demand 13 10 10 mg/L SM 5220D-1997 Copper - Total 7.31 3 1.60 10.0 ug/L EPA 6010D Iron - Total 589 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 2.80 1 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 6.6 2.5 2.5 mg/L SM 2540D-1997 Zinc - Total 52.8 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 CIE.Nk'co www.encolabs.com ANALYTICAL RESULTS Description: OUTFALL 1 Lab Sample ID: CA0843 1-01 Received: 08/08/17 14:30 Matrix: Surface Water Sampled:08/07/17 08:45 Work Order: CA08431 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results E[6g Units pf P!Z E" Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7HO9004 EPA 6010D 08/14/17 13:38 JMV Copper[7440-50-8]^ 7.31 J ug/L 1 1.60 10.0 7HO9004 EPA 6010D 08/14/17 13:38 JMV Iron [7439-89-6]^ 589 ug/L 1 22.0 50.0 7HO9004 EPA 6010D 08/14/17 13:38 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7HO9004 EPA 6010D 08/14/17 13:38 JMV Zinc[7440-66-6]^ 52.8 ug/L 1 4.40 10.0 7H14043 EPA 6010D 08/17/17 11:59 )MV Classical Chemistry Parameters ^ - ENCO Cary certified aoalyte [NC 591] Analyte fCAS Numberl Results flag Units PIE MU M Batch Method Analyz By Notes Chemical Oxygen Demand 13 mg/L 1 10 10 71-114027 SM 5220D-1997 08/14/17 18:00 30C Total Suspended Solids^ 6.6 mg/L 1 2.5 2.5 71-110011 SM 254OD-1997 08/10/17 10:50 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Oil & Grease (HEM) [C-0007]^ Results flag Units PIE MU M Batch Method Analx:Cc By Notes 2.80 J mg/L 1 2.40 5.00 7H16013 EPA 1664B 08/17/17 16:17 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 (E�eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7H09004 - EPA 3005A Blank (7H09004-BLK3) Prepared: 08/09/2017 08:07 Analyzed: 08/14/2017 13:03 Spike Source %REC RPD Analyte ResuB Ela9 P_QL Units Level Result %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L LCS (7H09004-BS1) Prepared: 08/09/2017 08:07 Analyzed: 08/14/2017 13:06 Spike Source %REC RPD Anal lde Result Elm P91 Units Level Result %REC Limits RPD Limit Notes Cadmium 20.1 1.00 ug/L 20.0 100 80-120 Copper 216 10.0 ug/L 200 108 80-120 Iron 1070 50.0 ug/L 1000 107 80-120 Lead 220 10.0 ug/L 200 110 80-120 Matrix Spike (7H09004-MS1) Prepared: 08/09/2017 08:07 Analyzed: 08/14/2017 13:19 Source: CA08220-01 Spike Source %REC RPD Anal Resul Flaa POL Units Level Result %REC Limits RPD Limit Notes Cadmium 21.0 1.00 ug/L 20.0 0.360 U 105 75-125 Copper 214 10.0 ug/L 200 2.65 106 75-125 Iron 1300 50.0 ug/L 1000 232 107 75-125 Lead 222 10.0 ug/L 200 3.10 U ill 75-125 Matrix Spike Dup (7H09004-MSD1) Prepared: 08/09/2017 08:07 Analyzed: 08/14/2017 13:21 Source: CA08220-01 Spike Source %REC RPD Anal Result Han P44 Units Level Result %REC Limits RPD iimft Notes Cadmium 19.7 1.00 ug/L 20.0 0.360 U 98 75-125 6 20 Copper 214 10.0 ug/L 200 2.65 106 75-125 0.2 20 Iron 1270 50.0 ug/L 1000 232 104 75-125 2 20 Lead 216 10.0 ug/L 200 3.10 U 108 75-125 3 20 Post Spike (7H09004-PS1) Prepared: 08/09/2017 08:07 Analyzed: 08/14/2017 13:24 Source: CA08220-01 Spike Source %REC RPD Anal vte Result Elm POL Units Level Resu %REC Limits RPD Limit Notes Cadmium 0.0195 0.00100 mg/L 0.0200 2.88E-5 97 80-120 Copper 0.206 0.0100 mg/L 0.200 0.00265 102 80-120 Iron 1.27 0.0500 mg/L 1.00 0.232 103 80-120 Lead 0.204 0.0100 mg/L 0.200 -0.00104 102 80-120 Batch 7H14043 - EPA 3005A Blank (7H14043-BLK3) Prepared: 08/14/2017 15:04 Analyzed: 08/17/2017 11:32 Spike Source %REC RPD Ana 1Lt Result Flag POLL Units Level Result %REC Limits RPD limft Notes Zinc 4.40 U 10.0 ug/L LCS (7H14043-BSI) Prepared: 08/14/2017 15:04 Analyzed: 08/17/2017 11:35 Spike Source %REC RPD Analvte Result Etas P9l Units Level Resu %REC Limits RPD Limit Notes Zinc 197 10.0 ug/L 200 98 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7H14043 - EPA 3005A - Continued Matrix Spike (7H14043-MS1) Prepared: 08/14/2017 15:04 Analyzed: 08/17/2017 11:40 Source: CA11692-01 Spike Source %REC RPD Anal Yte Resin Flag P" units Level Result %REC Limits RPD Limit Notes Zinc 224 10.0 ug/L 200 15.5 104 75-125 Matrix Spike Dup (7H14043-MSD1) Prepared: 08/14/2017 15:04 Analyzed: 08/17/2017 11:43 Source: CA11692-01 Spike Source %REC RPD Analvte Result Flag PQI Units Level Result %REC Limits RPD Lima Notes Zinc 222 10.0 ug/L 200 15.5 103 75-125 0.8 20 Post Spike (7H14043-PSI) Prepared: 08/14/2017 15:04 Analyzed: 08/17/2017 11:46 Source: CA11692-01 Spike Source %REC RPD Ana llttg Resul Flag POL Units Level Result %REC Limits RPD Limit Notes Zinc 0.216 0.0100 mg/L 0.200 0.0155 100 80-120 Classical Chemistry Parameters - Quality Control Batch 7HI0011 - NO PREP Blank (7H10011-BLK3) Prepared & Analyzed: 08/10/2017 10:50 Spike Source %REC RPD Ana Re5ult Flag 14 Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7H10011-BSI) Prepared & Analyzed: 08/10/2017 10:50 Spike Source %REC RPD AnalYte Result Flag POL Units Level Result %REC Limits RPD klnft Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (7H10011-DUPl) Prepared & Analyzed: 08/10/2017 10:50 Source: CA10291-01 Spike Source %REC RPD Anah to Result Haig POL Unite Level Result %REC Limits RPD Limit Notes Total Suspended Solids 130 17 mg/L 140 10 20 Duplicate (7H10011-DUP2) Prepared & Analyzed: 08/10/2017 10:50 11 Source: CA11084-01 Ana Total Suspended Solids Batch 7H14027 - Same Result Flag FOL 45 25 Spike Source %REC RPD units Level ResuR %REC Limits RPD Limit Notes mg/L 48 6 20 Blank (7H14027-BLK3) Prepared: 08/14/2017 12:17 Analyzed: 08/14/2017 18:00 Spike Source %REC RPD AnalResult Flag POI Units Level Resuk %REC Limits RPD Mmft Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7H14027-BS1) Prepared: 08/14/2017 12:17 Analyzed: 08/14/2017 18:00 Spike Source %REC RPD Anale Resuli Flag P4L Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 100 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7H14027 - Same - Continued ENEo www.encolabs.com Matrix Spike (7H14027-MS3) Prepared: 08/14/2017 12:17 Analyzed: 08/14/2017 18:00 Source: CA08165-01 Spike Source %REC RPD Analvte Reesult Flag POL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 7100 100 mg/L 5000 2100 99 90-110 Matrix Spike Dup (7H14027-MSD3) Prepared: 08/14/2017 12:17 Analyzed: 08/14/2017 18:00 Source: CA08165-01 Spike Source %REC RPD Anallfte Result Flag PQL Units Level Result %REC Limits RPD imil; Notes Chemical Oxygen Demand 7200 100 mg/L 5000 2100 101 90-110 2 10 Classical Chemistry Parameters - Quality Control Batch 7H16013 - EPA 1664E Blank (7H36013-BLK3) Prepared: 08/16/2017 15:53 Analyzed: 08/17/2017 16:17 Spike Source %REC RPD Anal vte Result Fig POL Uni Level Result %REC Limits RPD lzimit Notes Oil & Grease (HEM) 2.40 u 5.00 mg/L LCS (7H16013-BSI) Prepared: 08/16/2017 15:53 Analyzed: 08/17/2017 16:17 Spike Source %REC RPD Anal vte Result Flag Pol Units Level Result %REC Limits RPD lialit Notes Oil & Grease (HEM) 154 5.00 mg/L 161 96 78-114 LCS Dup (7H16013-13SDI) Prepared: 08/16/2017 15:53 Analyzed: 08/17/2017 16:17 Spike Source %REC RPD Anal yt0 Result Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 142 5.00 mg/L 160 89 78-114 8 18 Matrix Spike (7H16013-MS1) Prepared: 08/16/2017 15:53 Analyzed: 08/17/2017 16:17 Source: BA03605-01 Spike Source %REC RPD Anallfte Result Flag P121 Units Level Resu %REC Limits RPD Limit Notes Oil & Grease (HEM) 428 5.00 mg/L 152 293 89 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (FJ�Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com — I:}771 collral;Wt rn I111i: t!tanvit'n. Patti sn,n. S1M1P I„ yl ilklm',.iu r,,;u,,,ut c' C dowAle R Istfua Wct!4nr4,slc. f:..l'JJ I64f6B,a '.w y. NC 27511 00) W",,Alt film 14071 RUO 6I141. 0XNl? 2%-.iW7 f W-19041:!NW. -0 'flNt 447' K+ ¢air IYtY1 441-ybrs Page of - CIue,N Nana thmlo :t funntu. MsgnrYld 4_ Ml14Mr Asqueated rUrnorotind Times �AS17u1J.9s�LF;Fu^l�vt;3r)i. C1t1tC1-1,]t.1►tffi �tlt�H� rmtw:I 44nsi41irtit lyul► rluufl (IlyttAlY i,dllprj tfSlounkyatw , w: =r.r.r.. ty 11t4 lo'.-A1Y Rux�n4►. N� �.7� 4�_—__ _- N .. I 0 _Standard i�, F.� wot,t,ltty urttrcr N - [:_►34J i22�i7fia� 336i 322-W9S �,rwDlpne} nuN4N, ArNlwarut rnnnrt - . Diare Ball --- - - - - Ywup utrmrl ,t � Expedited UL 2 ' Due i— tt- CH Diane Bell � --- tY LttCMrK," T"a Int■ �✓ Lett 1M7rirO7tlAf' Koxbow < <-, U _ r ycf4�11Lunrrxwt - ae rnaMOW GAo 3 Wwtnral�n II6ou „ q w ID J 101 :w uu ,m,,.n Cblhnitu,t DroF, N ;,Mn' 'atau samplo Commentc- �L SW 5 X X! X X sw 1� x 1 X x I • Totat a of CDlrtstru:+rs �� Sum{up I(il tkptmtnrrt By [1pNvT mt jWlt nut,r,1 fJy NurNWlshrU !ty LLNtNTun4 CWIdTnr., i'<t�d� y pw� .oua r I Wr7 lior4,Tsiw rtttt4rinrSpaaal R4pnwq{ iiurptu'n„wmu RNGIr VW Ui — - -- -- - — ri4ur," 0r-w — — FVetsupuW�ct py — CIeiw ww Cbdm at M1 YW'tR on FtrrolM L-PC m ttu.� Ut .n tta >rGt ArcWAhte Unacc�iA4atNe 1610ert4 : an-:arc,mIAWIR. W soil Ow rnntYltv /twtn, SE �.eeh;T,rM sw-l.,"M N{Olof wW Wat4lrtrami A All 0.10"41 Iesamall w, :3tir+tN4, ►mtruWlan MWe 1+Wl ► -1U4ry3 11,44PS04 NO r jOH 00"to, WmA ii,:gnAw mil t t_ra All santnAi wJ„enrNct t: ENCO IJb4 wa . strardMtce wllh trite 1*tmv Nittl caldNrvtn =lu— 1 ,.., Ill" I4,n.'no elf MIi4 rorm, tNYa44 {Irtty w,7IHss varvrineiss Mem Sample Preservation Verification ENCO Cary Work Order CA08431 Project Stormwater Client Wesbeil Asset Recovery Center (WE012) Project It (none] Logged Ir. 08-Aug-17 14 37 Lodged By Rachel Ann Yonisn CA08431-01 Coat Type Fres (pH) PH Checked Require"" In Dateffime PH Adjusted Adtusted Reagent UsediCamments 6 25OmLA+H2SO4 <2 Y/ W! Y 1 N! A C 25OmLA+H2SO4 e2 Y i N IA Y/ N/ A - D 250inLP+H2SO4 <2 Y N / NA Y / NA E 250MLP+HNO3 <2 Y N / NA Y / NA Reagent Name ID _ t 2 Rea er4; Name ID 3 4 Reaaent Name ►�, 5 6 Page 1 of 1 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General PermitNo. NCG200000 — Scrap Metal Recycling Date submitted 4I/31 1 1 4- CERTIFICATE OF COVERAGE NO. NCG20L S 0. FACILITY NAME COUNTY 7F�Sc�/1 PERSON COLLECTING SAMPLES ic-.' I LABORATORY IJ/1C 0 Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �,U SAMPLE PERIOD ❑ J n-June El July -Dec �or E Monthly' (month) j " Et.11 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA AUG 03 101/ ❑Zero -flow ❑Water Supply [:]SA ❑Saltwater [-]Other CE'NTRAi FILE;, DWR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 MfIfIVI"o-discharge this period?z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 j P:.*,t B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES -1 NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Permit Date: 02/02/2015-12/31/2019 (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted U-9k)-fl i 1- CERTIFICATE OF COVERAGE NO. NCG20_L) S O FACILITY NAME LiCSht COUNTY Cilv"5vn PERSON COLLECTING SAMPLES I )�,e LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR X0 k SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or F Monthly' �y✓�e' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED �ro-flow ❑Water Supply ❑SA i ❑Saltwater ❑Other JUL 1 0 201? CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ZNo discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Pa; —t B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. IlVo`discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L4 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ure of Permittee) Permit Date: 02/02/2015-12/31/2019 0-:5'/06/(2— (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 W r Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 - Scrap Metal Recycling Date submitted co- =�- - ) CERTIFICATE OF COVERAGE NO. NCG20 0 5 O FACILITY NAME l�Jeal�t�� t5�fv4,n� R�cwer�� COUNTY r5cN PERSON C LLECTING SAMPLES ✓�L �� I LABORATORY rc /JC_0 Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR a0 I SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Mrmonthly' c month DISCHARGING TO CLASS ❑ORW HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ESA ❑Saltwater ❑Other PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount Inches3 Total Suspended Solids Chemical Oxy gen ygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 S L ­5 IL N 8 o IL 0. u0 I O.00 fL U. 0 1, l v5) + Wn IL -j /L U.VU`j )� G.Uv3 r1��- U.oy� �L 0 51 LJ t L 1.Li 1L uv , O-UU31y_ V, v 0 C)• Ll r. L_ U r� L 'd w L O.v0 U w3( '7L 00 �- v 51 15- U . '-i a:. S M L I L U . G U) 1t G . c, �3 / ..J IL_ U . U (o � '7 L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L4 Footnotes from Part A also apply to this Part B Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." gnature of Permittee) Permit Date: 02/02/2015-12/31/2019 G(/o--t /(-y— (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 W Ok V"p Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, June 7, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: (none], Project Name/Desc: Stormwater ENCO Workorder(s): CA06156 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 26, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 11 (e� �Cmo www.encolabs.com v SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OUTFALL1 Lab ID: CA06156-01 Sampled: 05/25/17 13:30 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:01 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: OUTFALL2 Lab ID: CA06156-02 Sampled: 05/25/17 13:35 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:03 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample 3 Lab ID: CA06156-03 Sampled: 05/25/17 13:26 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:06 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample Lab ID: CA06156-04 Sampled: 05/25/17 13:15 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 16648 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:19 SM 2540D-1997 06/01/17 05/31/17 13:10 05/31/17 13:10 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample Lab ID: CA06156-05 Sampled: 05/25/17 13:09 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:21 SM 2540D-1997 06/01/17 05/31/17 13:10 05/31/17 13:10 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 11 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: OUTFALL 1 Lab ID: CA06156-03 Anal vte .Results Eta ML P9l Notes Chemical Oxygen Demand 22 10 10 mg/L SM 5220D-1997 Copper - Total 7.15 1 1.60 10.0 ug/L EPA 6010D Iron - Total 854 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 2.48 1 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 15 6.2 6.2 mg/L SM 254OD-1997 Zinc - Total 32.4 4.40 10.0 ug/L EPA 6010D Client ID: OUTFALL 2 Lab ID: CA06156-02 Anal vte Results EW9 MQL POL Units Method Notes Chemical Oxygen Demand 26 10 10 mg/L SM 5220D-1997 Copper - Total 8.55 3 1.60 10.0 ug/L EPA 6010D Iron - Total 1500 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 2.68 1 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 12 4.2 4.2 mg/L SM 254OD-1997 Zinc - Total 43.6 4.40 10.0 ug/L EPA 6010D I Client ID: Sample 3 Lab ID: CA06156-03 Anal ldg Results HAS[ MPS M Units Method Notes Copper - Total 4.78 3 1.60 10.0 ug/L EPA 6010D Iron - Total 83.9 22.0 50.0 ug/L EPA 6010D Zinc - Total 23.5 4.40 10.0 ug/L EPA 6010D Client ID: Sample 6 Lab ID: CA06156-04 An lyt Resu EIN M26 POL y1lb Method Notes Copper - Total 9.21 3 1.60 10.0 ug/L EPA 6010D Iron - Total 190 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 7.0 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 78.2 4.40 10.0 ug/L EPA 6010D Client ID: Sample 7 Lab ID: CA06156-05 Anal vte esults Flag MDL POL Units Method Notes Zinc - Total 66.0 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 11 www.encolabs.com ANALYTICAL RESULTS Description: OUTFALL 1 Lab Sample ID:CA06156-01 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:30 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified anaVe [NC 591] Analyte rCAS Numberl Results Elm Units Qf M2L ,EQ4 Batch Method A alyz ]sy Notes Cadmium (7440-43-91^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:01 JMV Copper[7440-50-B]^ 7.15 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:01 ]MV Iron [7439-89-6]^ 854 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Lead (7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Zinc[7440-66-6]^ 32.4 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Classical Chemistry Parameters ^ - ENCO Cary certfled analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed ¢y Notes Chemical Oxygen Demand 22 mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 15 mg/L 2.5 6.2 6.2 7FO1010 SM 254OD-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte [CAS Numberl Results Flay Units IL 1]v DL pQl Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ 2.48 J mg/L 1 2.40 5.00 7FO2006 EPA 1664E 06/02/17 15:48 SMA Description: OUTFALL 2 Lab Sample ID:CA06156-02 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:35 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell (Metals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO Cary certified analyte [NC 5911 Analyte fCAS Numberl Results Flag Units OF ]U p2L Batch Method Analyzed §y Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:03 )MV Copper[7440-50-B]^ 8.55 ] ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:03 JMV Iron [7439-89-6]^ 1500 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:03 JMV Lead (7439-92-11^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:03 JMV Zinc[7440-66-6]^ 43.6 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:03 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units Qf MOIL E2L Batch Method Analyzed @y Notes Chemical Oxygen Demand^ 26 mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 12 mg/L 1.67 4.2 4.2 7FO1010 SM 2540D-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analvte rCAS Numberl Results flag Units Qf ]U EQL Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ 2.68 J mg/L 1.12 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 11 (Io) www.encolabs.com ANALYTICAL RESULTS Description: Sample 3 Lab Sample ID:CA06156-03 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:26 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Eim yp& PE MU EQ.L Batch Method Analyzed ¢y Notes Cadmium (7440-43-9]1 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:06 ]MV Copper[7440-50-8]^ 4.78 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Iron [7439-89-6]^ 83.9 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Zinc [7440-66-6]^ 23.5 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results F&q Units F MU p]L Batch Method Analyzed Ay Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 7FO1010 SM 254OD-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 441] Analyte fCAS Numberl Results Flag Units QF MDL QQL Batch Method Analyzed fy Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA Description: Sample 6 Lab Sample ID:CA06156-04 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:15 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary cerh'fied analyte [NC 5911 Analyte rCAS Numberl Results Flag Units PF MDL P91 Batch Method wed ¢y Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:19 ]MV Copper (7440-50-8]^ 9.21 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:19 ]MV Iron [7439-89-6]^ 190 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:19 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Zinc[7440-66-6]^ 78.2 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte FCAS Numberl Results E122 Units PFF MDL POL Batch Method Analyzed RX Notes Chemical Oxygen Demand 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 7.0 mg/L 1 2.5 2.5 7E31008 SM 2540D-1997 05/31/17 13:10 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 441] Analyte rCAS Numbed Results Flag units QF MQy Batch Method Analyzed ¢y Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664E 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 11 (� �Go www.encolabs.com ANALYTICAL RESULTS Description: Sample 7 Lab Sample ID:CA06156-05 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:09 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary retified —0e [NC 591] Analvte fCAS Numberl Results fin Units Qf MDL EQL Batch Method Analyzed Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:21 ]MV Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:21 ]MV Iron [7439-89-6]^ 22.0 U ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:21 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:21 JMV Zinc [7440-66-6]^ 66.0 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:21 ]MV Classical Chemistry Parameters ^ - ENCO Cary cerofied analyte [NC 591] Analvte fCAS Numberl Results flag Units DF MDL EQL Batch Method Analyzed ]iy Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 ]OC Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 7E31008 SM 2540D-1997 05/31/17 13:10 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 4421 AnaMe fCAS Numberl Results Flag Units QF ]YJ2L M Aatch Method Analyzed @y Notes Oil & Grease (HEM) [C-0007]1 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 11 (� �Go www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7E30023 - EPA 3005A Blank (7E30023-BLK1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 10:58 Spike Source %REC RPD Anal vte Result Hag PQL Units Level Result %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (7E30023-BS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:01 Spike Source %REC RPD Analyt Result Flag _POL m Level Result %REC Limits RPD kmft Notes Cadmium 20.6 1.00 ug/L 20.0 103 80-120 Copper 196 10.0 ug/L 200 98 80-120 Iron 1050 50.0 ug/L 1000 105 80-120 Lead 202 10.0 ug/L 200 101 80-120 Zinc 209 10.0 ug/L 200 104 80-120 Matrix Spike (7E30023-MS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:07 Source: CA05761-21 Spike Source %REC RPD Analvte Result Flaa P52L m Level Result %REC Limits RPD Limit Notes Cadmium 21.1 1.00 ug/L 20.0 0.360 U 105 75-125 Copper 207 10.0 ug/L 200 1.85 103 75-125 Iron 22100 50.0 ug/L 1000 22200 NR 75-125 QM-07 Lead 208 10.0 ug/L 200 3.10 U 104 75-125 Zinc 229 10.0 ug/L 200 26.4 101 75-125 Matrix Spike Dup (7E30023-MSD1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:10 Source: CA05761-21 Spike Source %REC RPD Anal vte Result Flao PQL Units Level Result %REC Limits RPD kmft Notes Cadmium 21.1 1.00 ug/L 20.0 0.360 U 105 75-125 0.2 20 Copper 208 10.0 ug/L 200 1.85 103 75-125 0.6 20 Iron 22000 50.0 ug/L 1000 22200 NR 75-125 0.5 20 QM-07 Lead 210 10.0 ug/L 200 3.10 U 105 75-125 0.9 20 Zinc 231 10.0 ug/L 200 26.4 102 75-125 0.8 20 Post Spike (7E30023-PS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:13 Source: CA05761-21 Spike Source %REC RPD Anal Result Flaa PQ Units Level Result %REC Limits RPD Limit Notes Cadmium 0.0213 0.00100 mg/L 0.0200 0.000279 105 80-120 Copper 0.210 0.0100 mg/L 0.200 0.00185 104 80-120 Iron 23.2 0.0500 mg/L 1.00 22.2 95 80-120 Lead 0.209 0.0100 mg/L 0.200 0.00196 103 80-120 Zinc 0.250 0.0100 mg/L 0.200 0.0264 112 80-120 Classical Chemistry Parameters - Quality Control Batch 7E31008 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 11 cf=:= � www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7E31008 - NO PREP - Continued Blank (7E33008-BLK1) Prepared & Analyzed: 05/31/2017 13:10 Spike Source %REC RPD Anal vte Result Flag lQ Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7E33008-BS3) Prepared & Analyzed: 05/31/2017 13:10 Spike Source %REC RPD Anal vte Result Flaq ROL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (7E33008-DUPI) Prepared & Analyzed: 05/31/2017 13:10 Source: CA04447-01 Spike Source %REC RPD Anal Result Flag PQL Unite Level Resuk %REC Limits RPD i i Notes Total Suspended Solids 95 25 mg/L 98 3 20 Duplicate (7E31008-DUP2) Prepared & Analyzed: 05/31/2017 13:10 Source: CA06430-01 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 260 50 mg/L 270 5 20 Batch 7FO1010 - NO PREP Blank (7F01010-BLK1) Prepared & Analyzed: 06/01/2017 16:30 Spike Source %REC RPD Analvte Result Flag PQL Units Level Result %REC Limi RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7F01010-BSI) Prepared & Analyzed: 06/01/2017 16:30 Spike Source %REC RPD Analvte Result FEag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (71`01010-DUP3) Prepared & Analyzed: 06/01/2017 16:30 Source: CA04423-01 Spike Source %REC RPD Anal vte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 6500 500 mg/L 8600 28 20 QM-12 Duplicate (7F03030-DUP2) Prepared & Analyzed: 06/01/2017 16:30 Source: CA06427-01 Spike Source %REC RPD Anal Yte Result Flag POL Unitt Level Result %REC Limits RPD Limit Notes Total Suspended Solids 230 50 mg/L 240 3 20 Batch 7FO2008 - Same Blank (7F02008-BLK3) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Spike Source %REC RPD Anal Re usullt Flan POL Units Level Resul1 %REC Limits RPD limft Notes Chemical Oxygen Demand 10 U 10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 11 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7FO2008 - Same - Continued www.encolabs.com LCS (7F02008-BS1) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Spike Source %REC RPD Anal vte Result Fig POL Units Level Resuk %REC Limits RPD kinift Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (7F02008-MS3) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Source: CA06156-01 Spike Source %REC RPD Anab to Result Flag RQL U nits Level Result %REC Limits RPD im' Notes Chemical Oxygen Demand 550 10 mg/L 526 22 101 90-110 Matrix Spike Dup (7F02008-MSD1) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Source: CA06156-01 Spike Source %REC RPD Anal Resul Fta9 PQL Units Level Result %REC Limits RPD Mmit Notes Chemical Oxygen Demand 570 10 mg/L 526 22 104 90-110 2 10 Classical Chemistry Parameters - Quality Control Batch 7FO2006 - EPA 16648 Blank (7F02006-BLK3) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Anal Result FIa9 Q m Level Result %REC Limits RPD 11mg Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7F02006-BS1) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Anal vte Result Flaa PQL units Level ResuR %REC Limits RPD Limit Notes Oil & Grease (HEM) 146 5.00 mg/L 160 92 78-114 LCS Dup (7F02006-BSD1) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Anal vte Result Eb9 M Units Level Result %REC Limits RPD kmft Notes Oil & Grease (HEM) 135 5.00 mg/L 154 87 78-114 8 18 Matrix Spike (7F02006-MSi) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Source: BA02312-01 Spike Source %REC RPD Analyt ResuR Flag PPOL Units Level Result %REC Limits RPD 11MLt Notes Oil & Grease (HEM) 202 5.00 mg/L 156 2.40 U 129 78-114 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 11 Ce== �Go www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 11 II ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.cotii 110A twwatall PlAt 111 44 to E�Aeuww MUN �.cufl J11110 I I 1 1(9 A W,�w**kls Inkmmmil Ct Cow"o R VU24 (4147S00&lt# PmWVW7ldW4HM& for,.4rwsw cbel hwillo PAqVSSW TjFMIXAA ld Timms Wmbell Awwt Rac)varj G'*rdw- (WEDI 2) (noml 5.4 Licy Gwr*l Rd Skormweler Roitm, NO 2,7574 Standard (3 r2 2 -4iXO (33613?2..0693 ow" wl Expedited , kdo 4z *­r1%44-CA. 3.0k D*W Bell Lbb WCPWO*r —6 CA06 1 TID' X y 004,"" s-- j + 1" 30 -4- 1:5c,,Pie_ 'Ilk It I A fwal # of untAhom ,nv. 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MPH Ott jus ec agent � seiiC r r�.s p G _�_, ,y t kt H:.J°/.'.�>"4g E `'.. s: • �xi.r"1 `�+ .�.: i.. �ps„P+'.. ty r..'Lk�yNy,k 2lL*+4 'Q �� bW c•ip'% E(N NA j E 2* nLP{l NQ3 <2 Y` h e NA V AO NA C A06156-03 C71 � PP (P PH {��� t to Ch i H A _ we C; Ad;ur t � � ,� r Reagent } , ," merit:: i 25nL+iS}4 Y i N I ltitA' M I N I D .25QmL:P+l42SG4 <2 Y N I NA Y N I NA E 2-SOrSLP'+t4J3 <2 Y N I NA Y N NA � CA06156-04 Com .., (P Requeement In HAdjust 5�t eage+lt 3se'dar-c.t" merlf5 t+ iuroS �t % :rr <2 t i NI YINI ' C 25CmLA+ H2Sf.}4 <2 Y I N Y I N I D LP+H SCL4 --2 N I NA Y, I NA 2 L-+,HNO3 <2 ' Y I NA I Y NA CA06156-05 Con" Typo � P(es ( H: O i Dat+�Tim ]Ee�,:ent s r^ ra;* P ju u 8 2SOmLA+H2S(D4 _ Y r Y ; i C 25CmLA+L425O4 Q Y I N I Y Pal -: — D 25CmLP+H2SO4 r2 N I NA Y. N I MA E 25OmLP+HNOr3 <2 Y , N I t4A Page 1 of 2, Sample Preservation Verification ENCO Cary _ Wcwk Order CA06156 Project Stormwater Clint W+esbell Asset Recoyer� Center (WEE312) Prat # (novel Logged tn. 26-May-17 14 39 Logged By; Rachel Ann Yonish Reagent. Nanve CQ t 2 3 Reaqent Nacre --E 6 Page 2 of 2 ENCO Laboratorks Accurate. Thnely. Responsive. Innov, 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, June 7, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CA06156 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 26, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OLLC----�A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 11 (� �Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OUTFALL 1 Lab ID: CA06156-01 Sampled: 05/25/17 13:30 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Preo Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:01 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: OUTFALL 2 Lab ID: CA06156-02 Sampled: 05/25/17 13:35 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Preo Date/Time(s) Analysis Date/Time(s) EPA 1664B 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:03 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample Lab ID: CA06156-03 Sampled: 05/25/17 13:26 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:06 SM 254OD-1997 06/01/17 06/01/17 16:30 06/01/17 16:30 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample Lab ID: CA06156-04 Sampled: 05/25/17 13:15 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:19 SM 254OD-1997 06/01/17 05/31/17 13:10 05/31/17 13:10 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 Client ID: Sample Lab ID: CA06156-05 Sampled: 05/25/17 13:09 Received: 05/26/17 14:08 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 06/22/17 06/02/17 12:24 06/02/17 15:48 EPA 6010D 11/21/17 05/30/17 11:30 06/01/17 12:21 SM 2540D-1997 06/01/17 05/31/17 13:10 05/31/17 13:10 SM 5220D-1997 06/22/17 06/02/17 10:05 06/02/17 17:37 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 11 mm�n www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: OUTFALL 1 Lab ID: CA06156-01 Anal Results Flag MQL POLUnits Method Notes Chemical Oxygen Demand 22 10 10 mg/L SM 5220D-1997 Copper - Total 7.15 3 1.60 10.0 ug/L EPA 6010D Iron - Total 854 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 2.48 1 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 15 6.2 6.2 mg/L SM 254OD-1997 Zinc - Total 32.4 4.40 10.0 ug/L EPA 6010D I Client ID: OUTFALL 2 Lab ID: CA06156-02 Anal lda Results flag la E" Units Method Notes Chemical Oxygen Demand 26 10 10 mg/L SM 5220D-1997 Copper - Total 8.55 1 1.60 10.0 ug/L EPA 6010D Iron - Total 1500 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 2.68 1 2.40 5.00 mg/L EPA 1664E Total Suspended Solids 12 4.2 4.2 mg/L SM 2540D-1997 Zinc - Total 43.6 4.40 10.0 ug/L EPA 6010D Client ID: Sample 3 Lab ID: CA06156-03 Anal vte Results Flag MQL EQL Units Method Notes Copper - Total 4.78 3 1.60 10.0 ug/L EPA 6010D Iron - Total 83.9 22.0 50.0 ug/L EPA 6010D Zinc - Total 23.5 4.40 10.0 uQ/L EPA 6010D Client ID: Sample 6 Lab ID: CA06156-04 Anal vte Results EW9 MQL POL VA& Method Notes Copper - Total 9.21 1 1.60 10.0 ug/L EPA 6010D Iron - Total 190 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 7.0 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 78.2 4.40 10.0 ug/L EPA 6010D Client ID: Sample 7 Lab ID: CA06156-05 Analvte Results flan MDL M Units Method Nst�s Zinc - Total 66.0 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 11 ��60 www.encolabs.com ANALYTICAL RESULTS Description: OUTFALL 1 Lab Sample ID:CA06156-01 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:30 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591J Analyte rCAS Numberl Results flag Units DF HU E L Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:01 ]MV Copper[7440-50-8]^ 7.15 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Iron [7439-89-6]^ 854 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:01 JMV Zinc [7440-66-6]^ 32.4 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:01 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified anaWe [NC 591] Analyte rCAS Numberl Results flag Units pf MDL EQL Batch Method Analyzed By Notes Chemical Oxygen Demand^ 22 mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 15 mg/L 2.5 6.2 6.2 7FO1010 SM 2540D-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified anaWe [NC 442] Analyte rCAS Numberl Results Flag Units DF MD4 E" Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ 2.48 J mg/1- 1 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA Description: OUTFALL 2 Lab Sample ID:CA06156-02 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:35 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte [CAS Numberl Results flag Units 2E MDL E" Batch Method Analyzed gy Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:03 JMV Copper [7440-50-8]^ 8.55 ] ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:03 JMV Iron [7439-89-6]^ 1500 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:03 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:03 ]MV Zinc [7440-66-6]^ 43.6 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:03 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Ellis Units 2E MU E" Batch Meth Analyzed By Notes Chemical Oxygen Demand^ 26 mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids 12 mg/L 1.67 4.2 4.2 7FO1010 SM 254OD-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified ana/yte [NC 4421 Analyte [CAS Numberl Results Flag Units Qf Ifs], EQL Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ 2.68 J mg/L 1.12 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 11 www.encolabs.com ANALYTICAL RESULTS Description: Sample 3 Lab Sample ID:CA06156-03 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:26 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaci Units QF MDL E2L Batch Method Analyzed ly Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:06 JMV Copper[7440-50-8]^ 4.78 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:06 ]MV Iron [7439-89-6]^ 83.9 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:06 JMV Zinc[7440-66-6]^ 23.5 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:06 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results f1m Units QF MDL POL Batch Method Analyzed By Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 7FO1010 SM 2540D-1997 06/01/17 16:30 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyie [NC 442] Analyte fCAS Numberl Results Flag Units PE MDL PQ4 Batch Method Analyzed ¢y Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA Description: Sample 6 Lab Sample ID:CA06156-04 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:15 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results f1m Units PIE RU E4 Batch Method Analyzed Ay Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:19 ]MV Copper[7440-50-8]^ 9.21 J ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Iron [7439-89-6]^ 190 ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Zinc [7440-66-6]^ 78.2 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:19 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units Qf MDL POIPOL Batch Method Analyzed ¢y Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 7.0 mg/L 1 2.5 2.5 7E31008 SM 254OD-1997 05/31/17 13:10 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Results Flag Units QF 1JN D4 EQj Batch Method Analyzed gy Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664E 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 11 (��Go www.encolabs.com ANALYTICAL RESULTS Description: Sample 7 Lab Sample ID:CA06156-05 Received: 05/26/17 14:08 Matrix: Surface Water Sampled:05/25/17 13:09 Work Order: CA06156 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results f164 Units Pf MDL POL Batch Method Analyzed Ay Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7E30023 EPA 6010D 06/01/17 12:21 JMV Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 7E30023 EPA 6010D 06/01/17 12:21 JMV Iron [7439-89-6]^ 22.0 U ug/L 1 22.0 50.0 7E30023 EPA 6010D 06/01/17 12:21 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7E30023 EPA 6010D 06/01/17 12:21 JMV Zinc[7440-66-6]^ 66.0 ug/L 1 4.40 10.0 7E30023 EPA 6010D 06/01/17 12:21 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte (NC 5911 Analyte rCAS Numbed Results fin ynb pF ma M Batch Method Analyzed Notes Chemical Oxygen Demand 10 U mg/L 1 10 10 7FO2008 SM 5220D-1997 06/02/17 17:37 JOC Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 7E31008 SM 254OD-1997 05/31/17 13:10 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Results Fig Units DF MQL POL Batch Method AnalYzed AX Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7FO2006 EPA 1664B 06/02/17 15:48 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 11 (� �Go www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7E30023 - EPA 3005A Blank (7E30023-BLKI) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 10:58 Spike Source %REC RPD Analvte Result Flag PQL units Level Result %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (7E30023-BS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:01 Spike Source %REC RPD Analvte ResuAt Flaa Q Units Level ResuK %REC Limits RPD Limit Notes Cadmium 20.6 1.00 ug/L 20.0 103 80-120 Copper 196 10.0 ug/L 200 98 80-120 Iron 1050 50.0 ug/L 1000 105 80-120 Lead 202 10.0 ug/L 200 101 80-120 Zinc 209 10.0 ug/L 200 104 80-120 Matrix Spike (7E30023-MS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:07 Source: CA05761-21 Spike Source %REC RPD Anal vte Result Elm PQL units Level Result %REC Limits RPD unift Notes Cadmium 21.1 1.00 ug/L 20.0 0.360 U 105 75-125 Copper 207 10.0 ug/L 200 1.85 103 75-125 Iron 22100 50.0 ug/L 1000 22200 NR 75-125 QM-07 Lead 208 10.0 ug/L 200 3.10 U 104 75-125 Zinc 229 10.0 ug/L 200 26.4 101 75-125 Matrix Spike Dup (7E30023-MSDI) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:10 Source: CA05761-21 Spike Source %REC RPD Analyse Result Flaa POL Units Level Result %REC Limits RPD Limi Notes Cadmium 21.1 1.00 ug/L 20.0 0.360 U 105 75-125 0.2 20 Copper 208 10.0 ug/L 200 1.85 103 75-125 0.6 20 Iron 22000 50.0 ug/L 1000 22200 NR 75-125 0.5 20 QM-07 Lead 210 10.0 ug/L 200 3.10 U 105 75-125 0.9 20 Zinc 231 10.0 ug/L 200 26.4 102 75-125 0.8 20 Post Spike (7E30023-PS1) Prepared: 05/30/2017 11:30 Analyzed: 06/01/2017 11:13 Source: CA05761-21 Spike Source %REC RPD Analitt Resul Fag PQL Units Level Result %REC Limits RPD kinft Notes Cadmium 0.0213 0.00100 mg/L 0.0200 0.000279 105 80-120 Copper 0.210 0.0100 mg/L 0.200 0.00185 104 80-120 Iron 23.2 0.0500 mg/L 1.00 22.2 95 80-120 Lead 0.209 0.0100 mg/L 0.200 0.00196 103 80-120 Zinc 0.250 0.0100 mg/L 0.200 0.0264 112 80-120 Classical Chemistry Parameters - Quality Control Batch 7E31008 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 11 (� �Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7E31008 - NO PREP - Continued Blank (7E33008-BLKi) Prepared & Analyzed: 05/31/2017 13:10 Spike Source %REC RPD Anal vte Result Flag P L Units Level Resuk %REC Limits RPD Limit Notes Total Suspended Solids 2.S U 2.5 mg/L LCS (7E31008-BSI) Prepared & Analyzed: 05/31/2017 13:10 Spike Source %REC RPD Anal vte Result FFFlAq POL Uni Level Result %REC Limits RPD limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (7E33008-DUPl) Prepared & Analyzed: 05/31/2017 13:10 Source: CA04447-01 Spike Source %REC RPD Analyt Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 95 25 mg/L 98 3 20 Duplicate (7E31008-DUP2) Prepared & Analyzed: 05/31/2017 13:10 Source: CA06430-01 Spike Source %REC RPD Analvte Result Flag _POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 260 50 mg/L 270 5 20 Batch 7F01010 - NO PREP Blank (7F01010-BLKi) Prepared & Analyzed: 06/01/2017 16:30 Spike Source %REC RPD AnalYte Re u Flaa PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7F01010-BS1) Prepared & Analyzed: 06/01/2017 16:30 Spike Source %REC RPD Ana ty_e Re ul Flaa PQL Units Level Result %REC i i RPD Li i Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (7F01010-DUPl) Prepared & Analyzed: 06/01/2017 16:30 Source: CA04423-01 Spike Source %REC RPD Analvte Result FBI g PQL Units Level Result %REC Limits RPD kimft Notes Total Suspended Solids 6500 500 mg/L 8600 28 20 QM-12 Duplicate (7F01030-DUP2) Prepared & Analyzed: 06/01/2017 16:30 Source: CA06427-01 Spike Source %REC RPD Analvte Rnfylt Fla9 PQL omits Level Result %REC Limits RPD Limit Notes Total Suspended Solids 230 50 mg/L 240 3 20 Batch 7F02008 - Same Blank (7F02008-BLKi) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Spike Source %REC RPD Analyte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 11 (9 �M� www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7F02008 - Same - Continued LCS (7F02008-BS1) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Spike Source %REC RPD Anal ResuR Flag PQL units Level Resu %REC Limits RPD kinit Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (7F02008-MS1) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Source: CA06156-01 Spike Source %REC RPD Analyte Result Flag PQL Units Level Rat %REC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 22 101 90-110 Matrix Spike Dup (7F02008-MSD1) Prepared: 06/02/2017 10:05 Analyzed: 06/02/2017 17:37 Source: CA06156-01 Spike Source %REC RPD Anal Result Flaq PQL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 570 10 mg/L 526 22 104 90-110 2 10 Classical Chemistry Parameters - Quality Control Batch 7F02006 - EPA 1664E Blank (7F02006-BLKI) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Analvte Result Flaq IQ Unib Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7F02006-BS1) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Anal vte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 146 5.00 mg/L 160 92 78-114 LCS Dup (7F02006-BSD1) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Spike Source %REC RPD Analyte Result Flag POL Units Level Result %REC Limits RPD knIA Notes Oil & Grease (HEM) 135 5.00 mg/L 154 87 78-114 8 18 Matrix Spike (7F02006-MS1) Prepared: 06/02/2017 12:24 Analyzed: 06/02/2017 15:48 Source:BA02312-01 Analvte Oil & Grease (HEM) Spike Source %REC Result Flaq PQL Uni Level Result %REC Limits RPD 202 5.00 mg/L 156 2.40 U 129 78-114 RPD Lima Notes QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 11 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 11 0 r11r cr > (-Iotq-zws ss LLM aozzgws Coo, cr. 0 z A 44 I J 4i cr, 1 � A a m Sample Presewation Verification ENCO Cary CfMJ �w Work fir° CA061 'i Prgj : stwMwater Ghent Wesbell Asset Recovery Cerfter (WE012) Project Irwonej Logged tn. 26-May -17 14:39 Logged By, Raciel Ann Ybnlsh CA06166-01 Dort Type Plres tPH) tqChe4edi PH Azdtul5teo Dafel -ff IT Reagerl "ti vet: <2 Y I "d zaijw: C 25&niA+H2S 4 <2 Y t tit kN Y I N f(to 2 +H2 sC4 <2 Y °� to I NA Y N NA E 2HN33 Y IV I! Y i NA CAt615"2 Coat Ty [g y till H -A di v5l'ec F A N is NA Reagent CJ C4 ara rim G` 2+.�Y3 i.s_. T•'�.� a - � ( ,[. i Y f N I tm 250mi*H2S 4 <2 Y INJt YIN tNi D 250m F -H2 SO4 <2 Y NINA Y ° NA 250mLP+HNO3<2 N P l+oA Y f Nth CA06156-03 �g,3"��.� �"s{*C}i£'� tom?-P a -WV C 25 nLA+H2yS€g34� fat I ) <2q IA¢ Yt YI INA �N ¢ ';A 2J0fiinLT +Ht703 -- [ ly I t4lt Y l CA06156-04 p es ��y tPH'a �a� f : �� g � - ime Reapot d,•C t 8 2 L—A++f2SO4 z`�. Y i N W ' •; a N t � ;2`:7tirtF+ �f e/ta V <2 Si.�0 a eLT'�'Pi2S, '� s Y7 f 1'+ N Ny Y f 04 m are• .._ +n ry��yy��.,�,,.. ��f any Lt �p NA CAV61JV-05 +€ Type °� 6ci5? Adiussed fat t'i# !e5e`Ci?"iT Ey9 ts 81 250r,-,LA+H2SC34 Y I N & Y I N C 250nAA+H2W4 Y I N I EA Y I N' 3, Q 250rnLP+H2 O4 N I NA Y l� I NA E 250ntLP+HNO3 Y N I NA Y ,N I NA • of 2. Sample Preservation Verification ENGO Cary Work Order CA06156 Proiect, stormwater Client wesbel! Asset Recovery Ceiftr (WE012) Project [none] Logged In.-. 26-May-11 14-39 Logged By Rachel Ann Yonish Reacent Name tQ i Rea ent Name la 3 �. 4 r Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recvcling Date submitted S' IES - aU( �?- CERTIFICATE OF COVERAGE NO. NCG20-0 S SAMPLE COLLECTION YEAR �O j FACILITY NAME (.JtS6t II _-r_yy)1,�-MR<ccr� SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY RE(' !U or [;?'Monthly' /4p�'i ( (month) PERSON COLLECTING SAMPLES sG '? C or TO CLASS ❑ORW ❑HQW [:]Trout❑PNA LABORATORY C-KJCo Lab Cert. # MAY 1 4 1� '1; []Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: ❑Saltwater [:]Other CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE � Part A: Stormwater Benchmarks and Monitoring Results No discharge this period: Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total lead, Total Zinc, Total Benchmarks ==> - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or _0.005 mg/L5 �.0�5 ' 0.07S mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 Lf U `l ^�Il MIL r~- L O.u0S1 I+. 030} 9 �- U. (o � I -� I L �. '� ,� L U v 3 I L U, u031, L L (• L V, o l l l.i , UU 5 L U u3 (l 1. Lf i4 uv "� L_ 1 3 -)It- 13. 4 5 ,.. L 0 003-1IL O,ou31 L U ,oa4K �.IL L_ v.o Url ►� .vo31. L L)IL 1 1-1 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, id.cluding the possibility of fines and imprisonment for knowing violations." � � I ature of Permittee) o S u 5 �- (Date) Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 2 of 2 X..ENCO Laboratories 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, May 5, 2017 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell 555 Lucy Garrett Rd. Roxboro, NC 27574 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CA04891 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, April 26, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0 L. C---� A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 11 (� � �Go www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outtall 1 Lab ID: CA04891-01 Sampled: 04/25/17 11:00 Received: 04/26/17 14:45 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 05/23/17 05/03/17 11:58 05/04/17 15:09 EPA 6010D 10/22/17 05/02/17 08:09 05/03/17 14:31 SM 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 SM 5220D-1997 05/23/17 05/01/17 11:04 05/01/17 13:50 Client ID: Outfall 2 Lab ID: CA04891-02 Sampled: 04/25/17 11:00 Received: 04/26/17 14:45 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 05/23/17 05/03/17 11:58 05/04/17 15:09 EPA 6010D 10/22/17 05/02/17 08:09 05/03/17 14:34 SM 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 SM 5220D-1997 05/23/17 05/01/17 11:04 05/01/17 13:50 Client ID: Sample 3 Lab ID: CA04891-03 Sampled: 04/25/17 15:50 Received: 04/26/17 14:45 Parameter Hold Date/Time(s) Prep Date/Time(s) 11111 Analysis Date/Time(s) EPA 1664B 05/23/17 05/03/17 11:58 05/04/17 15:09 EPA 6010D 10/22/17 05/02/17 08:09 05/03/17 14:36 SM 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 SM 5220D-1997 05/23/17 05/01/17 11:04 05/01/17 13:50 Client ID: Sample Lab ID: CA04891-04 Sampled: 04/25/17 16:00 Received: 04/26/17 14:45 Parameter EPA 1664E Hold Date/Time(s) 05/23/17 Prep Date/Time(s) 05/03/17 Analysis Date/Time(s) 11:58 05/04/17 15:09 EPA 6010D 10/22/17 05/02/17 08:09 05/03/17 14:47 SM 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 SM 5220D-1997 05/23/17 05/01/17 11:04 05/01/17 13:50 Client ID: Sample 5 Lab ID: CA04891-05 Sampled: 04/25/17 16:00 Received: 04/26/17 14:45 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B 05/23/17 05/03/17 11:58 05/04/17 15:09 EPA 6010D 10/22/17 05/02/17 08:09 05/03/17 14:49 SM 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 SM 5220D-1997 05/23/17 05/01/17 11:04 05/01/17 13:50 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. : Page 2 of I1 Lq&LG.(3j) www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 1 Lab ID: CA04891-01 Ana1ye Results PIa4 MIL EQL Units Method Notes Chemical Oxygen Demand 11 10 10 mg/L SM 5220D-1997 Copper- Total 5.24 3 1.60 10.0 ug/L EPA 6010D Iron - Total 1250 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 17 3.3 3.3 mg/L SM 254OD-1997 Zinc - Total 30.7 4.40 10.0 ug/L EPA 6010D Client ID: Outfall 2 Lab ID: CA04891-02 Anandg Results f Lag fmL E" 5t1llm Method Notes Chemical Oxygen Demand 17 10 10 mg/L SM 5220D-1997 Copper- Total 3.37 3 1.60 10.0 ug/L EPA 6010D Iron - Total 1210 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 24 5.0 5.0 mg/L SM 254OD-1997 Zinc - Total 22.2 4.40 10.0 ug/L EPA 6010D Client ID: Sample 3 Lab ID: CA04891-03 AnalYte Results flan MU E91 Units Method Notes Chemical Oxygen Demand 15 10 10 mg/L SM 5220D-1997 Copper - Total 14.4 1.60 10.0 ug/L EPA 6010D Iron - Total 71.3 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 3.9 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 36.2 4.40 10.0 ug/L EPA 6010D Client ID: Sample 4 Lab ID: CA04891-04 Anahrte Results Flag Hu EQL Units Method Notes Chemical Oxygen Demand 13 10 10 mg/L SM 5220D-1997 Copper- Total 3.11 3 1.60 10.0 ug/L EPA 6010D Iron - Total 211 22.0 50.0 ug/L EPA 6010D Oil & Grease (HEM) 3.45 3 2.40 5.00 mg/L EPA 1664E Total Suspended Solids 2.6 2.5 2.5 mg/L SM 2540D-1997 Zinc - Total 24.4 4.40 10.0 ug/L EPA 6010D Client ID: Sample 5 Lab ID: CA04891-05 Analyte Results Flag Ms EQL !-r& Mel fttM Chemical Oxygen Demand 26 10 10 mg/L SM 5220D-1997 Copper- Total 16.5 1.60 10.0 ug/L EPA 6010D Iron - Total 551 22.0 50.0 ug/L EPA 6010D Total Suspended Solids 3.8 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 88.9 4.40 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 1.1 @9��EOJ www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CA04891-01 Received: 04/26/17 14:45 Matrix: Surface Water Sampled:04/25/17 11:00 Work Order: CA04891 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyze [NC 591] Analyte rCAS Numberl Results Fig Uinits DF MDL P L Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7EO2004 EPA 6010D 05/03/17 14:31 ]MV Copper[7440-50-8]^ 5.24 ] ug/L 1 1.60 10.0 7E02004 EPA 6010D 05/03/17 14:31 ]MV Iron [7439-89-6]^ 1250 ug/L 1 22.0 50.0 7EO2004 EPA 6010D 05/03/17 14:31 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7EO2004 EPA 6010D 05/03/17 14:31 ]MV Zinc[7440-66-6]^ 30.7 ug/L 1 4.40 10.0 7EO2004 EPA 6010D 05/03/17 14:31 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified analyze [NC 591] Analyte rCAS Numberl Results Bag. Units QF 1D[D , p" Batch Method Analyzed By Notes Chemical Oxygen Demand^ 11 mg/L 1 10 10 7EO1015 SM 5220D-1997 05/01/17 13:50 ]OC Total Suspended Solids^ 17 mg/L 1.33 3.3 3.3 7D27005 SM 254OD-1997 04/27/17 13:50 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyze [NC 442] Analyte rCAS Numberl Results Elas Units 2E RDA E" Amh Method Analyzed l;y Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7EO3008 EPA 1664E 05/04/17 15:09 SMA Description: Outfall 2 Lab Sample ID:CA04891-02 Received: 04/26/17 14:45 Matrix: Surface Water Sampled:04/25/17 11:00 Work Order: CA04891 Project: Stormwater Sampled By: Diane Bell tals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyze [NC 5911 Analyte rCAS Numberl Results IF S Units pF 1HL EQL VAlrh Method Analyzed @y Notes Cadmium [7410 43-9]^ 0.360 U ug/L 1 0.360 1.00 7E02004 EPA 6010D 05/03/17 14:34 ]MV Copper[7440-50-8]^ 3.37 ] ug/L 1 1.60 10.0 7EO2004 EPA 6010D 05/03/17 14:34 ]MV Iron [7439-89-6]^ 1230 ug/L 1 22.0 50.0 7E02004 EPA 6010D 05/03/17 14:34 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7EO2004 EPA 6010D 05/03/17 14:34 ]MV Zinc 17440-66-6]^ 22.2 ug/L 1 4.40 10.0 7EO2004 EPA 6010D 05/03/17 14:34 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified analyze [NC 591] Analyte rCAS Numberl Results EL49 Units LSE MDL " @8gti Method Analyzed @y Notes Chemical Oxygen Demand^ 17 mg/L 1 10 10 7EO1015 SM 5220D-1997 05/01/17 13:50 ]OC Total Suspended Solids^ 24 mg/L 2 5.0 5.0 7027005 SM 254OD-1997 04/27/17 13:50 OMR Classical Chemistry Parameters 7-71 ^ - ENCOJacksonv/lle certified analyze [NC 442] Analyte rCAS Number] $esy1S6 Elm Units 2E MU PQL 119t9I Method Analyzed Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7EO3008 EPA 1664E 05/04/17 15:09 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 11 �IWMW�WI www.encolabs.com ANALYTICAL RESULTS Description: Sample 3 Lab Sample ID: CA04891-03 Received: 04/26/17 14:45 Matrix: Surface Water Sampled:04/25/17 15:50 Work Order: CA04891 Project: Stormwater Sampled By: Diane Bell (Metals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO Cary certified ana/yte [NC 591] Analyte rCAS Numberl Results Flag ni U PE MDL P L Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7EO2004 EPA 6010D 05/03/17 14:36 ]MV Copper[7440-50-8]^ 14.4 ug/L 1 1.60 10.0 7EO2004 EPA 6010D 05/03/17 14:36 ]MV Iron [7439-89-6]^ 71.3 ug/L 1 22.0 50.0 7EO2004 EPA 6010D 05/03/17 14:36 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7EO2004 EPA 6010D 05/03/17 14:36 ]MV Zinc[7440-66-6]^ 36.2 ug/L 1 4.40 10.0 7EO2004 EPA 6010D 05/03/17 14:36 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified ana/yte [NC 591] Analyte rCAS Numberl Results Flag Units OF MDL EQk Batch Method Analyzed Ay RQLU Chemical Oxygen Demand^ 15 mg/L 1 10 10 7EO1015 SM 5220D-1997 05/01/17 13:50 JOC Total Suspended Solids^ 3.9 mg/L 1 2.5 2.5 7D27005 SM 254OD-1997 04/27/17 13:50 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analyte rCAS Numberl Results Flag Units pT MQ4 PSI Batch Method Analyzed @y Notes Oil & Grease (HEM)[C-0007]^ 2.40 U mg/L 1 2.40 5.00 7EO3008 EPA 1664E 05/04/17 15:09 SMA Description: Sample 4 Lab Sample ID: CA04891-04 Received: 04/26/17 14:45 Matrix: Surface Water Sampled:04/25/17 16:00 Work Order: CA04891 Project: Stonnwater Sampled By: Diane Bell (Metals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO Cary rerbfied analyte [AK' 5911 Analyte fCAS Numberl Results flag Units PF MU PQL Batch Method Analyzed ft Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7EO2004 EPA 6010D 05/03/17 14:47 JMV Copper[7440-50-8]^ 3.11 J ug/L 1 1.60 10.0 7E02004 EPA 6010D 05/03/17 14:47 ]MV Iron [7439-89-6]^ 211 ug/L 1 22.0 50.0 7EO2004 EPA 6010D 05/03/17 14:47 ]MV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7EO2004 EPA 6010D 05/03/17 14:47 JMV Zinc[7440-66-6]^ 24.4 ug/L 1 4.40 10.0 7EO2004 EPA 6010D 05/03/17 14:47 )MV (Classical Chemistry Parameters ' ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results flag Units RE MDL L% Batch Method Analyzed By Notes Chemical Oxygen Demand 13 mg/L 1 10 10 7EO1015 SM 5220D-1997 05/01/17 13:50 JOC Total Suspended Solids^ 2.6 mg/L 1 2.5 2.5 7D27005 SM 254OD-1997 04/27/17 13:50 OMR (Classical Chemistry Parameters ' ^ - ENCO JackwnWIle certified analyte [AC 442] Analyte rCAS Numberl Oil & Grease (HEM) [C-0007]^ Results Flag Units RE MU POL Batch Method Analyzed ft Notes 3.45 J mg/L 1 2.40 5.00 7EO3008 EPA 1664B 05/04/17 15:09 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 11 www.encolabs.com ANALYTICAL RESULTS Description: Sample 5 Lab Sample ID:CA04891-05 Received: 04/26/17 14:45 Matrix: Surface Water Sampled:04/25/17 16:00 Work Order: CA04891 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods 777771 ^ - ENCO Cary certified a-lyle [NC 5911 Analyte rCAS Numberl Results Flaa Units DF�DL POL Batch Method Analyzed IN Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 7EO2004 EPA 6010D 05/03/17 14:49 ]MV Copper[7440-50-8]^ 16.5 ug/L 1 1.60 10.0 7EO2004 EPA 6010D 05/03/17 14:49 JMV Iron [7439-89-6]^ 551 ug/L 1 22.0 50.0 7EO2004 EPA 6010D 05/03/17 14:49 JMV Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 7EO2004 EPA 6010D 05/03/17 14:49 ]MV Zinc [7440-66-6]^ 88.9 ug/L 1 4.40 10.0 7EO2004 EPA 6010D 05/03/17 14:49 JMV Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results E1.02 Units PE MDL EQL A=h Method Analyzed @y Notes Chemical Oxygen Demand^ 26 mg/L 1 10 10 7EO1015 SM 5220D-1997 05/01/17 13:50 JOC Total Suspended Solids^ 3.8 mg/L 1 2.5 2.5 7D27005 SM 254OD-1997 04/27/17 13:50 OMR Classical Chemistry Parameters ^ - ENCO Jacksonville certfied analyte [NC 442] Analyte rCAS Numberl Results fiq Units pf MDL E" Batch Method Analyzed Ay NoteF Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 7EO3008 EPA 1664B 05/04/17 15:09 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 11 � 1 ��Mr,rG www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7EO2004 - EPA 3005A Blank (7E02004-BLKl) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 10:49 Spike Source %REC RPD Ana Result Flag M Units Level Result %REC Limits RPD limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L Blank (7E02004-BLK2) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 10:52 Spike Source %REC RPD Anal YtO Result Flag IQ UnA s Level Result %REC Limits RPD limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (7E02004-BS3) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 13:50 Spike Source %REC RPD Anal vte Result flag POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.5 1.00 ug/L 20.0 102 80-120 Copper 194 10.0 ug/L 200 97 80-120 Iron 1030 50.0 ug/L 1000 103 80-120 Lead 200 10.0 ug/L 200 100 80-120 Zinc 203 10.0 ug/L 200 101 80-120 Matrix Spike (7E02004-MS1) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 13:55 Source: CA03304-01 Spike Source %REC RPD Anal vtg Result flag PQL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.7 1.00 ug/L 20.0 0.360 U IN 75-125 Copper 196 10.0 ug/L 200 1.70 97 75-125 Iron 1960 50.0 ug/L 1000 1010 96 75-125 Lead 200 10.0 ug/L 200 3.10 U 100 75-125 Zinc 305 10.0 ug/L 200 103 101 75-125 Matrix Spike Dup (7E02004-MSDl) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 13:58 Source: CA03304-01 Spike Source %REC RPD Anal vte Result Flag PPOL Ilnits Level Resul %REC Limits RPD Limit Notes Cadmium 21.2 1.00 ug/L 20.0 0.360 U 106 75-125 2 20 Copper 202 10.0 ug/L 200 1.70 100 75-125 3 20 Iron 2010 50.0 ug/L 1000 1010 101 75-125 3 20 Lead 206 10.0 ug/L 200 3.10 U 103 75-125 3 20 Zinc 311 10.0 ug/L 200 103 104 75-125 2 20 Post Spike (7E02004-PS1) Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 14:00 11 Source: CA03304-01 Spike Source %REC RPD Analvte Result flan P-QL UrI is Level Result %REC Limits RPD Limit Notes Cadmium 0.0215 0,00100 mg/L 0.0200 -7.59E-5 108 80-120 Copper 0.204 0.0100 mg/L 0.200 0.00170 101 80-120 Iron 2.03 0.0500 mg/L 1.00 1.01 103 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 11 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7EO2004 - EPA 3005A - Continued Post Spike (7E02004-PS1) Continued Prepared: 05/02/2017 08:09 Analyzed: 05/03/2017 14:00 Source: CA03304-01 Spike Source %REC RPD Analvte Result flag PDX Units Level Result %REC Limits RPD Limit Notes Lead 0.208 0.0100 mg/L 0.200-0.00262 104 80-120 Zinc 0.317 0.0100 mg/L 0.200 0.103 107 80-120 Classical Chemistry Parameters - Quality Control Batch 7D27005 - NO PREP Blank (7D27005-BLK1) Prepared & Analyzed: 04/27/2017 13:50 Spike Source %REC RPD Anal Yte Result Ewa P(X Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7D27005-BS3) Prepared & Analyzed: 04/27/2017 13:50 Spike Source %REC RPD Anal )de Resin flag P01 Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 90 2.5 mg/L 100 90 80-120 Duplicate (7D27005-DUPl) Prepared & Analyzed: 04/27/2017 13:50 Source: CA04256-02 Spike Source %REC RPD Anal vte Result flag Pal. Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 1900 250 mg/L 2400 20 20 Duplicate (7D27005-DUP2) Prepared & Analyzed: 04/27/2017 13:50 Source: CA04764-01 Spike Source %REC RPD Analvte Result slag PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 74 25 mg/L 160 71 20 QM-12 Batch 7EO1015 - Same Blank (7E03015-BLKl) Prepared: 05/01/2017 11:04 Analyzed: 05/01/2017 13:50 Spike Source %REC RPD Anal vte Result )lag PQL 1lnits Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7E01015-BS3) Prepared: 05/01/2017 11:04 Analyzed: 05/01/2017 13:50 Spike Source %REC RPD .AnalYte Result flag M Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (7E03015-MS1) Prepared: 05/01/2017 11:04 Analyzed: 05/01/2017 13:50 Source: CA04193-02 Spike Source %REC RPD Anal Result Flan POLL Units Level Re ul %REC Limits RPD Limit Notes Chemical Oxygen Demand 5900 80 mg/L 4000 2900 75 90-110 QM-07 Matrix Spike Dup (7E03015-MSD1) Prepared: 05/01/2017 11:04 Analyzed: 05/01/2017 13:50 Source: CA04193-01 Spike Source %REC RPD Anal Yte Resul Hag NX Units Level Result %REC Limits RPD Lima Notes Chemical Oxygen Demand 6100 80 mg/L 4000 2900 80 90-110 3 10 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 11 'Oril.l�7✓ www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7EO3008 - EPA 16648 Blank (7E03008-611.11(l) Prepared: 05/03/2017 11:58 Analyzed: 05/04/2017 15:09 Spike Source %REC RPD Ana ht30 Result Elan PQL units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7E03008-BS3) Prepared: 05/03/2017 11:58 Analyzed: 05/04/2017 15:09 Spike Source %REC RPD Analyse Resin flag P-QL unm Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 134 5.00 mg/L 152 88 78-114 LCS Dup (7E03008-BSD3) Prepared: 05/03/2017 11:58 Analyzed: 05/04/2017 15:09 Spike Source %REC RPD Anal Result IIag P(X units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 135 5.00 mg/L 151 90 78-114 1 18 Matrix Spike (7E03008-101S3) Prepared: 05/03/2017 11:58 Analyzed: 05/04/2017 15:09 Source: BA01885-01 Spike Source %REC RPD Anal Yte Result Ela9 P4L unAls Level Resin %REC Limits RPD Limit Notes Oil & Grease (HEM) 166 5.00 mg/L 189 8.12 84 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 11 www.encolabs.com FLAGS/NOTES AND DEFINITIONS a The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 11 �* ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Gontral Port Dr. 4810 Executive Park Court, Suite 111 102•A Woodwinds Industrial Ct. Orlando, FL 32824 .lackwrivttle, FL 32216.6069 Gary, NC 27511 (407)a26,5314 Fax(407) 650.6945 (904)296.3007 Fax(904) 296-6210 (919)467.3090 Fax(919) 467.3515 Page a -_ of Client Name Project Number ! — _Requested Analyses _T _ Requested Turnaround Address fa�('r� tASrIJAir: 1� Times .__.._---._ L �,r fe. /_I 1?a� Project NamelDeso Note Rush requests &0ect to 7 r� 'f'(� acceptance by the faciity Gty15TIZip PO s r Billing Info ! ` Roxxro. NC i j C — Standard fel — .. _ FF.... ta; ortx q .o„ tag,: - i 0 Q � (33i 372 3600 336) 322 t Dlare Bell it z') m U � Expedited _.._.�.. -� _--' �-- .... - - _.. _........._. 6 N — I� Sampler(s) Name. Affiliation (Prim; Billing Contact LL I Die / Diave Bell 'r` San-pw(s) S+gnature . Site Location T Time Zone Lab Workorder C Preservation (See Codes) tGo'nbrrae as necessary) Goiy orljnn Minx Total x of ,�errampn 1 -e=3 td. tt _frri -Prt o. :'ata T•re rn a'G.'aL` leer Sample Comments , ?u_ ._4--'�-_1_il'fib_ _s'sv 5 x x_ __x__ _, ___ 333-0 fray_ �' _.._. X_ sat L y_ q-as--I y. w , 6 i I I ....... . ......._ _ .. . . .......— __._............ __ ___.. -- �- - ; - --1� . ........ -- --- ----------- I 7 Total # of Containers Sample Kit Prri trod By r^ Date:'rime Rc tr..r�shed By , Date-Mme Reserve v DateRirtw i;terrttrten(gtSpeCWI Raporhny Re-qutremenks Re inµrrshed By DatrrJvne Rec y Uate;T rcre rieamq(aahed By Date/Time R ive By Date.'rane Cooler a's & Temps on Receipt ,l V Condition Receipt Acceptable Unacceptable rdatrix GW Groundwater SO -Sal DW-Drink rig Water SE-Sed+ment SW-Surtace Water WW-Wastewater A -Air O.Other (detail in comments) Preservation: Vice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in commenls) Note � AD samples submitted to ENCO Labs are in accordance with the terms and eondkions listed on the reverse of this form, unless prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CA04891 Project: Stormwater Client Wesbell Asset Recovery Center (WE012) Project #: [none] Logged In 26-Apr-1 7 15 02 Logged By John C King CA04891-01 Cont Type Pres (pH} Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 �rl N/ NA Y I I NA C 250mLA+H2SO4 <2 Y 1 N / NA Y 1 L3 / NA D 250mLP+H2SO4 <2 J/ N/ NA Y/ V i NA E 250mLP+HNO3 <2 Y / N / NA Y / �N / NA CA04891-02 Cant Type Pres (pH) Requirement pH Checked/ In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y/ N/ NA Y I 1 NA C 250mLA+H2SO4 <2 / N I NA Y I �N / NA D 250mLP+H2SO4 <2 / N / NA Y / LN / NA E 250mLP+HNO3 <2 J / N / NA Y ,' �N / NA CA04891-03 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Commenis B 250mLA+H2SO4 <2 iY / N / NA Y / / NA C 250mLA+H2SO4 <2 -Y / N / NA Y I tj / NA D 250mLP+H2SO4 <2 / N / NA Y / 0 / NA E 250mLP+HNO3 <2 / N / NA Y /o 1 NA CA04891-04 Cbnt- Type Pres (pH} Requirement pH Checked / In Control pH Adjusted DateMme Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 N / NA Y /I / NA C 250mLA+H2SO4 <2 1 N / NA Y / / NA D 250mLP+H2SO4 <2 ! N / NA Y / V / NA E 250mLP+HNO3 <2 r I N 1 NA Y 1J l NA CA04891-05 Cont Type Pres (pH) Requirement pH Checked I in Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 i N / NA Y I ill / NA C 250mLA+H2SO4 <2 / N / NA Y / I NA D 250mLP+H2SO4 <2 / N I NA Y 1 / NA E 250mLP+HNO3 <2 1 N/ NA Y J' 1 NA Page 1 of 2 Sample Preservation Verification ENCO CaryMIS c6i 6, C= Work Order: CA04891 Project: Stormwater Client: Wesbel! Asset Recovery Center (WE012) Project #: [none] Logged in: 26-Apr-17 15.02 Logged By: John C King Rea ent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID _ 5 6 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year MUn General Permit No. NCG200000 Certificate of Coverage No. NCG20 () ❑❑o ®❑ This monitoring report summary is due to the DEMLR Regional Office no later than March I" of each calendar year. Facility Name: WkSbtLl 1 n,, t �� Mt(1(' ►`tcG"e cy, County: I)er-aun Phone Number( 33(g) 3)LI - C> PQQ Total no. of SDOs monitored Outfail No. Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ RECEIVED Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ APR 2 4 CENT Outfall Total Rainfall, inches 00530 00340 01119 01114 TSS, mg/1 COD, mg/1 Non -polar oil & grease, m /l Total Copper, m /l Total Lead, mg/1 Total Zinc, mg/1 Benchmarks N/4 100/50 120 15 0.010/0.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr os 111 U. G . v 1 'T-4 0, 00 U . o P. S -11 SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑07 Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, m /l COD, mg/1 Non -polar oil & grease, m /l Copper, m l Lead, m l Zinc, m /1 Benchmark .N/A 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other 701 Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, m /l COD, mg/1 Non -polar oil & grease, mg/1 Copper, mg/1 Lead, mg/1 Zinc, mg/1 Benchmark NIA 100150 120 15 0.0101.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 Fresh/salt Date Sample Collected, mo/dd/yr SW U-250NCG20-01.28.15 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature I JIOYLA Date�- Mail Annual DMR Summary Reports to Your Regional DEMLR Office: DEMLR Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 707-9220 ASHEVILLE REGIONAL OFFICE 2090 US Highway 70 Swannanoa, NC 28778 (828) 296-4500 RALEIGH REGIONAL OFFICE 3800 Barrett Drive Raleigh, NC 27609 (919) 791-4200 WINSTON-SALEM REGIONAL OFFICE 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 FAYETTEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 225 Green Street 610 East Center Avenue/Suite 301 Systel Building Suite 714 Fayetteville, NC 28301-5043 (910) 433-3300 WASHINGTON REGIONAL OFFICE 943 Washington Square Mall Washington, NC 27889 (252) 946-6481 CENTRAL OFFICE 1612 Mail Service Center Raleigh, NC 27699-1612 (919) 707-9220 Mooresville, NC 28115 (704)663-1699 WILMINGTON REGIONAL OFFICE 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910) 796-7215 SW U-250NCG20-01.28.15 *I- Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted CERTIFICATE OF COVERAGE NO. NCG20 O _al U a FACILITY NAME uitn, 61 l) 1.K\U4 A-, e c w*n i COUNTY fSun PERSON COLLECTING SAMPLES LABORATORY [—_ NC U Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �,U 1 SAMPLE PERIOD O Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA REG E-i v i= 6 ❑Zero -flow [:]Watersupply []SA ❑Saltwater ❑Other JAN 17 201i ct.NTFzl�a.L. FILES' PLEASE REMEMBER TO SIGN ON THE REVERSE 4 [,'WR IEC TION n No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks ==> - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/Ls 0.126 mg/L or 0.090 mg/Ls ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 0111 • Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B :1 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO wr IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR, includina all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -111 cN�_k J� l (Signature of Permittee) Permit Date: 02/02/2015-12/31/2019 1 `�- (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report (DMR) oil for North Carolina DEMLR General Permit No. NCG200000 Scrap Metal Recycling Date submitted;ro CERTIFICATE OF COVERAGE NO. NCG20,a �', d;:t SAMPLE COLLECTION YEAR FACILITY NAME (,JesGzi j �y►J•sFr`3.nf (�e��.�p."c� n SAMPLE PERIOD QJan-June ❑ July -Dec COUNTY ��r'�ai1 NECEIUEQ or ❑ Monthly' PERSON COLLECTING SAMPLES ��anC' �Zl/ DISCHARGING TO CLASS ❑ORW ❑HQW ❑Tro NA SUN $ 2016 Zero -flow ater Su I SA LABORATORY G AA-0 Lab Cert. # ❑ ❑ p Comments on sample collection or analysis: CENTRAL FILES ❑Saltwater aOOther I +� DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results itPLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks ==> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/Ls 0.075 mg/L or 0.210 mg/Ls 0.126 mg/L or 0.090 mg/L5 os f `9 j tt. U l L 3 5 M� L L U U L v 0051 t.1 U ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If You report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected, (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 02/02/2015-12/31/2019 U5 - (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 /IcG (Po S�) � 4 ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, May 31, 2016 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): C512441 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, May 19, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"(XLC--�A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 CE �Go www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall2 Lab ID: C512441-01 Sampled: 05/19/16 11:30 Received: 05/19/16 13:55 (Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/16/16 05/24/16 15:13 05/25/16 18:39 EPA 6010D 11/15/16 05/23/16 09:12 05/24/16 10:12 SM 254OD-1997 05/26/16 SM 5220D-1997 06/16/16 05/23/16 10:30 05/23/16 10:30 05/23/16 15:52 05/24/16 10:17 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 (e� �09 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: CS12441-01 Analvte Results an MQL POL ni Method Notes Chemical Oxygen Demand 35 10 10 mg/L SM 5220D-1997 Copper- Total 17.4 1.60 10.0 ug/L EPA 6010D Iron - Total 6370 22.0 50.0 ug/L EPA 6010D Lead - Total 5.16 3 3.10 10.0 ug/L EPA 6010D Total Suspended Solids 440 33 33 mg/L SM 254OD-1997 Zinc - Total 85.5 4.40 10.0 ug/L EPA 6010D This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 Description: Outfall 2 ANALYTICAL RESULTS Lab Sample ID:C512441-01 Matrix: Surface Water Sampled:05/19/16 11:30 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods �co www.encolabs.com Received: 05/ 19/ 16 13:55 Work Order: C512441 ^ - ENCO Cary certified analyze [NC 591] Analyte rCAS Numberl Results Flaa Units DF _K" POL Batdt McUwd Analyzed ly Notes Cadmium (7440 43-9]^ 0.360 U ug/L 1 0.360 1.00 6E23009 EPA 6010D 05/24/16 10:12 JDH Copper [7440-50-8]^ 17.4 ug/L 1 1.60 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Iron [7439-89-6]^ 6370 ug/L 1 22.0 50.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Lead [7439-92-1]^ 5.16 J ug/L 1 3.10 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Zinc [7440-66-6]^ 85.5 ug/L 1 4.40 10.0 6E23009 EPA 6010D 05/24/16 10:12 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte [CAS Numberl Results F[aq Units Rf MU EQL Rauh Method Analyzed Ay Notes Chemical Oxygen Demand^ 35 mg/L 1 10 10 6E23030 SM 522OD-1997 05/24/16 10:17 JOC Total Suspended Solids^ 440 mg/L 13.3 33 33 6E23004 SM 25QD-1997 05/23/16 10:30 MMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 412] Analyte rCAS Numberl Oil & Grease (HEM) [C-0007]^ Results Fla9 Units JP-E ILL EQL =111 Method Anah-zed Al Notes 0.629 U mg/L 0.262 0.629 1.31 6E24002 EPA 1664E 05/25/16 18:39 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Cf== www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 6E23009 - EPA 3005A Blank (6E23009-BLK3) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 09:53 Spike Source %REC RPD Ana hfte Result dart PQL Units Level Result %REC Limits RPD kLmft Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (6E23009-BSI) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 09:57 Spike Source %REC RPD Anal lde Result flag PQL Units Level Result %REC Limits RPD km Notes Cadmium 20.1 1.00 ug/L 20.0 101 80-120 Copper 192 10.0 ug/L 200 96 80-120 Iron 1010 50.0 ug/L 1000 101 80-120 Lead 198 10.0 ug/L 200 99 80-120 Zinc 200 10.0 ug/L 200 100 80-120 Matrix Spike (6E23009-MS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:02 Source: CZ06979-01 Spike Source %REC RPD Anal vte Result Flag PQL Units Level Result %REC Limits RPD L11faii Notes Cadmium 20.8 1.00 ug/L 20.0 0.360 U 104 75-125 Copper 192 10.0 ug/L 200 1.60 U 96 75-125 Iron 1150 50.0 ug/L 1000 90.7 106 75-125 Lead 199 10.0 ug/L 200 3.10 U 100 75-125 Zinc 205 10.0 ug/L 200 4.40 U 103 75-125 Matrix Spike Dup (6E23009-MSD1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:05 Source: CZ06979-01 Spike Source %REC RPD Anal Yte Result Elan POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.6 1.00 ug/L 20.0 0.360 U 103 75-125 0.9 20 Copper 193 10.0 ug/L 200 1.60 U 96 75-125 0.2 20 Iron 1150 50.0 ug/L 1000 90.7 106 75-125 0.09 20 Lead 197 10.0 ug/L 200 3.10 U 99 75-125 1 20 Zinc 207 10.0 ug/L 200 4.40 U 104 75-125 1 20 Post Spike (6E23009-PS1) Prepared: 05/23/2016 09:12 Analyzed: 05/24/2016 10:07 Source: CZ06979-01 Spike Source %REC RPD Anal lde Result flag PM Units Level Result %REC Limits RPD Limit Notes Cadmium 0.0204 0.00100 mg/L 0.0200 0.000188 101 80-120 Copper 0.188 0.0100 mg/L 0.200 -0.00188 94 80-120 Iron 1.13 0.0500 mg/L 1.00 0.0907 103 80-120 Lead 0.193 0.0100 mg/L 0.200 0.000946 96 80-120 Zinc 0.204 0.0100 mg/L 0.200 0.00204 101 80-120 Classical Chemistry Parameters - Quality Control Batch 6E23004 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 (E�Cmo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E23OO4 - NO PREP - Continued Blank (6E23004-BLK3) Prepared & Analyzed: 05/23/2016 10:30 Spike Source %REC RPD Ana hr3e Result flag PQL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (6E23004-BSI) Prepared & Analyzed: 05/23/2016 10:30 Spike Source %REC RPD Anal lde Result flag PQL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 103 80-120 Duplicate (6E23004-DUPI) Prepared & Analyzed: 05/23/2016 10:30 Source: C512441-01 Spike Source %REC RPD Anal Yis Result Flag QL Una Level Result %REC Limits RPD Limit Notes Total Suspended Solids 410 33 mg/L 440 8 20 Duplicate (6E23004-DUP2) Prepared & Analyzed: 05/23/2016 10:30 Source: CZ05961-01 Spike Source %REC RPD Anal Yte Result Elan PQL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 210 100 mg/L 210 0 20 Batch 6E23O30 - Same Blank (6E23030-BLK3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Ana lYte B45ulL flag PQL Units Level Result %REC Limits RPD Limit )Votes Chemical Oxygen Demand 10 U 10 mg/L LCS (6E23030-BS1) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Anal Yte Result Ela3 PQL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (6E23030-MS3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Spike Source %REC RPD Anal ltts R4.suit flag ML Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 35 97 90-110 Matrix Spike Dup (6E23030-MSD3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Spike Source %REC RPD Analvte Result Elan PQL units Level Rat %REC Limits RPD Limit Notes Chemical Oxygen Demand 560 10 mg/L 526 35 100 90-110 3 10 Classical Chemistry Parameters - Quality Control Batch 6E24001- EPA 1664A Blank (6E24002-BLK3) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Anal ldC Result Elan PQL Units Level Result %REC Limits RPD limit Notes Oil & Grease (HEM) 0.613 U 1.28 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 �GO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E24002 - EPA 1664A - Continued LCS (6E24002-BS1) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Anal Result Elea PQL units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 154 5.00 mg/L 159 97 78-114 LCS Dup (6E24002-BSDl) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Anal YSe Result MCI POI. units Level Result %REC Limit, RPD Limit Notes Oil & Grease (HEM) 156 5.00 mg/L 160 98 78-114 2 18 Matrix Spike (6E24002-MSl) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Source: SZ02144-01 Spike Source %REC RPD Asnallde Resul Flag PPO ni Level Result %REC Limits RPD kinit Notes Oil & Grease (HEM) 155 5.00 mg/L 148 2.40 U 105 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 . . i CE== www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year ot(Jc General Permit No. NCG200000 Certificate of Coverage No. NCG20©5 0E❑ This monitoring report summary is due to the DEMLR Regional Office no later than March Is' of each calendar year. Facility Name: (,_)P3 le(l „e;�r►,<4 ecvue County: �A r`�c Phone Number: (33G) Outfall No. Total no. of SDOs monitored Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other Yes ❑ No Yes ❑ NoNN Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, ma/I COD, mg/I Non -polar oil & grease, mg/l Total Copper, ma/l Total Lead, ma/1 Total Zinc, ma/I Bench marks AAA 100150 120 15 0.010/0.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr C, H L > l_ U (4 ,_,,l L j v , ,-V , M c SNP1U-250NCG20-0? .28.15 Wesbell Investment Recovery 555 Lucy Garrett Road Roxboro, NC 27574 January 23, 2017 Division of Water Quality Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 To Whom It May Concern: Quantitative monitoring of Stormwater discharge sampling missed for the second sample in 2016. Wesbell missed the second stormwater sample due to an injury requiring surgery from the employee who completes the sampling. Wesbell's backup sampler resigned during this sampling period. I have submitted a SDO Discharge Monitoring Report for the first measureable storm event January 2017. Wesbell will also submit two more samples during the 2017 calendar following the 60-day minimum samples period. Sincerely, Diane Bell Compliance Manger -STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year ' (-)I General Permit No. NCG200000 Certificate of Coverage No. NCG20❑U ❑❑5 ❑O 0 This monitoring report summary is due to the DEMLR Regional Office no later than March 15, of each calendar year. Facility Name: l JesL�,�-t1�c�� rVl e►'t� �f crime �'� County: �� ('Sc-n Phone Number: aiO 3 ri--y (9C1U Total no. of SDOs monitored Outfall No. K— Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No z Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No Er If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, mg/1 Non -polar oil & grease, mg/1 Total Copper, m /I Total Lead, m /I Total Zinc, mg/1 Benchmarks NIA 100/50 120 15 0.01010.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr 7777 I r 2015 SWU-250NCG20-01.28.15 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date 10 - Owl — Mail Annual DMR Summary Reports to Your Regional DEMLR Office: DEMLR Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office ......... (919) 707-9220 ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE 3800 Barrett Drive Raleigh, NC 27609 (919) 791-4200 WINSTON-SALEM REGIONAL OFFICE 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 WASHINGTON REGIONAL OFFICE 943 Washington Square Mall Washington, NC 27889 (252) 946-6481 CENTRAL OFFICE 1612 Mail Service Center Raleigh, NC 27699-1612 (919) 707-9220 WILMINGTON REGIONAL OFFICE 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910) 796-7215 SW U-250NCG20-01.28.15 Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted 10 Q — 1 CERTIFICATE OF COVERAGE NO. NCG20. 5 U FACILITYNAME (A)e-5ht(I __T_0,V?1, tiMerV1 �7,cC���Zi' COUNTY e f SUn PERSON C LLECTING SAMPLES I ��L 7 ' LABORATORY r-_ %V (—U Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR U 15 SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]Water Supply [:]SAr_ RECEIVED ❑Saltwater ❑Other OCT 132015 n PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTRAL FILES MR SECTION ❑ No discharge this period?' �C Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L5 Q-a;- L5 3..1 iL lt_ yU ^ L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copv of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ?-;-/ � lo-CST-l-5 re of Permittee) (Date) Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 2 of 2 • • • TABLE 3.2 NON-STORMWATER DISCHARGE ASSESSMENT AND CERTIFICATION WESBELL INVESTMENT RECOVERY 555 LUCY GARRETT ROAD ROXBORO, NORTH CAROLINA MID -ATLANTIC JOB NO. 000132579.00 NON-STORMWATER DISCHARGE ASSESSMENT Completed by: ""C"'Oe �ji Title: na��/���nPe ►n' �a�c AND CERTIFICATION Date: LX7f /t.c5 / /_ Time: 0: I Outfall Directly Method Used to Describe Results from Identify Potential Name of Person Date of Test Observed During the Test or Evaluate Test for the Presence of Significant Who Conducted or Evaluation Test (identify as Discharge Non-Stormwater Sources the Test or indicated on site map) Discharge Evaluation lay r� vet CERTIFICATION I, k ((� (responsible corporate official), certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. Name & Official Title (type or print) 1 '�6no B. Area Code and Telephone No. on't 3 3 CkcQ C. Signatur6 \ "--�-� D. Date Signed _ I CJ c( �� Mid Atlantic Engineering & Environmental Solutions • ENCO Laboratories 'OB Accurate. Timely. Responsive. .innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, October 9, 2015 Wesbell Asset Recovery Center (WE012) Attn: Diane Bell P.O. Box 1752 Roxboro, NC 27573-9998 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): C503666 Dear Diane Bell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, September 25, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 CE== �Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall2 Lab ID: C503666-01 Sampled: 09/25/15 11:15 Received: 09/25/15 13:25 Parameter Hold Date/Time(s) Pre[) Date/Time(s) Analysis Date/Time(s) EPA 1664E 10/23/15 10/06/15 14:41 10/08/15 13:00 EPA 6010C 03/23/16 SM 254OD-1997 10/02/15 SM 5220D-1997 10/23/15 09/28/15 14:02 09/30/15 13:12 09/28/15 11:40 10/02/15 11:46 09/30/15 13:12 09/28/15 15:25 F; ria.L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 Cf ==�Go www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab ID: C503666-01 byte Results Him MDL Pf , Units Method Notes Chemical Oxygen Demand 28 10 10 mg/L SM 5220D-1997 Iron - Total 276 22.0 50.0 ug/L EPA 6010C Total Suspended Solids 3.1 2.5 2.5 mg/L SM 254OD-1997 Zinc - Total 19.0 3.80 10.0 ug/L EPA 6010C FINA'- This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 �Go www.encolabs.com ANALYTICAL RESULTS Description: Outfall 2 Lab Sample ID: C503666-01 Received: 09/25/15 13:25 Matrix: Surface Water Sampled:09/25/15 11:15 Work Order: C503666 Project: Stormwater Sampled By: Diane Bell Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified —1a to [NC 591] Afalvte rCAS Numberl Results Raq Units DF MDL P L Batch Method Analyzed By Notes Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 SI28030 EPA 6010C 10/02/15 11:46 VLO Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 5I28030 EPA 6010C 10/02/15 11:46 VLO Iron [7439-89-6]^ 276 ug/L 1 22.0 50.0 5I28030 EPA 6010C 10/02/15 11:46 VLO Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 5I28030 EPA 6010C 10/02/15 11:46 VLO Zinc[7440-66-6]^ 19.0 ug/L 1 3.80 10.0 5I28030 EPA 6010C 10/02/15 11:46 VLO Classical Chemistry Parameters ^ - ENCO Cary certYied a-lyte [NC 591] Analyte rCAS Numberl Results fln Units 2E MU E" Rauh Method Analyzed By R910 Chemical Oxygen Demand^ 28 mg/L 1 10 10 5I28015 SM 5220D-1997 09/28/15 15:25 JOC Total Suspended Solids^ 3.1 mg/L 1 2.5 2.5 5I30025 SM 254OD-1997 09/30/15 13:12 MMR Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyte [NC 442] Analvte rCAS Numberl Results F1ilig Units 2E +MDL EQ4 Batch Method Analyzed@y Notes Oil & Grease (HEM) [C-0007]^ 2.40 U mg/L 1 2.40 5.00 5106009 EPA 1664E 10/08/15 13:00 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 (SNSco www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 5718030 - EPA 3005A Blank (5I28030-BLK1) Prepared: 09/28/2015 14:02 Analyzed: 10/02/2015 11:26 Spike Source %REC RPD Anal Yte Result Dag P91 Units Level Result %REC Limits RPD Limit Notes Cadmium 0.360 U 1.00 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Zinc 3.80 U 10.0 ug/L LCS (SIZ8030-BS1) Prepared: 09/28/2015 14:02 Analyzed: 10/02/2015 11:29 Spike Source %REC RPD Anal Y?S Result t Elm POL Units Level Result %REC Limits RPD Limit Notes Cadmium 19.7 1.00 ug/L 20.0 99 80-120 Copper 184 10.0 ug/L 200 92 80-120 Iron 1000 50.0 ug/L 1000 100 80-120 Lead 196 10.0 ug/L 200 98 80-120 Zinc 202 10.0 ug/L 200 101 80-120 Matrix Spike (5I28030-M51) Prepared: 09/28/2015 14:02 Analyzed: 10/02/2015 11:35 Source: C511540-02 Spike Source %REC RPD Anal vte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.4 1.00 ug/L 20.0 0.627 99 75-125 Copper 196 10.0 ug/L 200 1.60 U 98 75-125 Iron 1110 50.0 ug/L 1000 102 101 75-125 Lead 198 10.0 ug/L 200 3.10 U 99 75-125 Zinc 202 10.0 ug/L 200 3.80 U 101 75-125 Matrix Spike Dup (5I28030-MSD1) Prepared: 09/28/2015 14:02 Analyzed: 10/02/2015 11:38 Source: C511SQ-02 Spike Source %REC RPD Anal lde Result Dag M Units Level Result %REC Limits RPD Limit Notes Cadmium 20.4 1.00 ug/L 20.0 0.627 99 75-125 0.1 20 Copper 198 10.0 ug/L 200 1.60 U 99 75-125 1 20 Iron 1120 50.0 ug/L 1000 102 102 75-125 0.6 20 Lead 197 10.0 ug/L 200 3.10 U 99 75-125 0.3 20 Zinc 203 10.0 ug/L 200 3.80 U 101 75-125 0.5 20 Post Spike (5I28030-PS1) Prepared: 09/28/2015 14:02 Analyzed: 10/02/2015 11:41 Source: C511540-02 Spike Source %REC RPD Anal YSE R45LIL Dag P91 Units Level Result %REC Limits RPD Limit Notes Cadmium 0.0205 0.00100 mg/L 0.0200 0.000627 100 80-120 Copper 0.196 0.0100 mg/L 0.200 -0.00128 98 80-120 Iron 1.06 0.0500 mg/L 1.00 0.102 96 80-120 Lead 0.199 0.0100 mg/L 0.200 0.000775 99 80-120 Zinc 0.204 0.0100 mg/L 0.200 0.000651 102 80-120 Classical Chemistry Parameters - Quality Control Batch 5128015 - Same FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 Cf == �Cmo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5128015 - Same - Continued Blank (SI28015-BLKI) Prepared: 09/28/2015 11:40 Analyzed: 09/28/2015 15:25 Spike Source %REC RPD, Anall[Si[S Result EI_ag POL units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (SI28015-BS3) Prepared: 09/28/2015 11:40 Analyzed: 09/28/2015 15:25 Spike Source %REC RPD Anal lcte Result Flag PSL. Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 520 10 mg/L 500 103 90-110 Matrix Spike (5I28015-MS1) Prepared: 09/28/2015 11:40 Analyzed: 09/28/2015 15:25 Source: C500134-01 Spike Source %REC RPD Anal Result Flaa POL m Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 560 10 mg/L 526 21 102 90-110 Matrix Spike Dup (5I28015-MSD3) Prepared: 09/28/2015 11:40 Analyzed: 09/28/2015 15:25 Source: C500134-01 Spike Source %REC RPD Ana hda Result Rau PQL Units Level Result %REC Limits RPD Limp Notes Chemical Oxygen Demand 560 10 mg/L 526 21 103 90-110 0.8 10 Batch 5130015 - NO PREP Blank (5I30025-BLK3) Prepared & Analyzed: 09/30/2015 13:12 Spike Source %REC RPD Anal Result Flag NX Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5I30025-BS3) Prepared & Analyzed: 09/30/2015 13:12 Spike Source %REC RPD Anal YSe Result Flag M Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 101 80-120 Duplicate (5I30025-DUPI) Prepared & Analyzed: 09/30/2015 13:12 Source: C512202-01 Spike Source %REC RPD Anal lde Result Elm PAL Units Level Result %REC Limits RPD Lim Notes Total Suspended Solids 940 360 mg/L 1000 7 20 Duplicate (5I30025-DUP2) Prepared & Analyzed: 09/30/2015 13:12 Source: C509294-01 Spike Source %REC RPD Anal Result om M Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 11 6.2 mg/L 11 2 20 Classical Chemistry Parameters - Quality Control Batch 5JO6009 - EPA 1664A Blank (SJ06009-BLK3) Prepared: 10/06/2015 14:41 Analyzed: 10/08/2015 13:00 Spike Source %REC RPD Anal Yte Result flag POL units Level gesul %REC Limits RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L . FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 Cfco www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5JO6009 - EPA 1664A - Continued LCS (5706009-BSI) Prepared: 10/06/2015 14:41 Analyzed: 10/08/2015 13:00 Spike Source %REC RPD Anal tde Result flag PQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 38.6 5.00 mg/L 41.2 94 78-114 LCS Dup (5306009-BSD3) Prepared: 10/06/2015 14:41 Analyzed: 10/08/2015 13:00 Spike Source %REC RPD Anal Result Elan pa Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 38.2 5.00 mg/L 42.7 90 78-114 1 18 Matrix Spike (5306009-MS3L) Prepared: 10/06/2015 14:41 Analyzed: 10/08/2015 13:00 Source: B504132-01 Spike Source %REC RPD Anal vte Result Flao PQL Units Level Resul %REC Limits RPD Limit Notes Oil & Grease (HEM) 39.8 5.58 mg/L 44.9 2.68 U 89 78-114 Fir.,;,_ This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 Ce N3 00) www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. H-L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 �..... ........ �.. .. .� ........�...... ........ ...... .�.. ... ...�.. ... ..-.... .... ............ ..�..... ... Will er 10775 Central IN)" Park Court. O Orlando. FL 32824 Or Jacksonville FL 32T166-6069&ti0r 111 7Cary. NC Z751rWs IndustrialCt (407) 826-5314 Fax (407) 850-6945 'Wt 4) 296-3007 Fax 1900 296-6210 (919) 467-3090 Fax (919) 467-3.515 Page ___ of ___ Sample Kit Prepared By DateT" Relinquished By DaWTime Received, DateR L T11 dNi��/�S Comments Special Reporting Pegwrementx Rokngwshed By DateIT(me Rd6pvedSy Dater me Rekrlquished By Dale.Txne Received By — DateXime I Cooler s's & Temps on Receipt Condition Upon Receipt '. / cceptable Unacceptable Matrix - GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW Surface Water WW-Wastewater A -A r 0.0ther idetail in comments) P►oervalion:l-Ice M-HCI N-MM S442SO4 NO-NaOH 60ther {detail -n comments) Note, All samples submitted to ENCO Laos are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist s Sample Preservation Verification ENCO Cary =SN Work Order: C503666 Project: Stormwater Client: Wesbell Asset Recovery Center (WE012) Project #: [none] Logged In 25-Sep-15 14 37 Logged By: John C King C503666-01 Cont Type res (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 1 LA+H2SO4 <2 Y / N / 6A Y / N / VA B 1 LA+H2SO4 <2 Y / N / DNA Y / N / &A D 250mLP+H2SO4 <2 Lr-/ N / NA Y / / NA E 1250mLP+HNO3 <2 Y�/ N / NA Y / & / NA Rea ent Name ID 1 2, — Reaclent Name ID 3 4 Reaclent Name ID 5 6 Page 1 of NCDENR • Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report i� U For guidance on filling out this form, please visit: http://portal.ncdenr.org/web/Ir/npdes-stormwater/­ Permit No.: N/C/-&/j/ or Certificate of Coverage No.: Facility Name: Wesbell Investment Recovery County: Person County Phone No. (336) 322-0600 Inspector: 17ia r» (1 Date of Inspection: Qq/ C&5' Time of Inspection: 11 " 15 Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [Z/Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). _........ _... _..... _._........... _........... __........... _.......... ............................._..........-_..............._._...._....._............._..---.— ._ —..---—..._....._......._..._. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. i A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the i permitted site outfall. The previous measurable storm event must have been at least 72 hours I prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: I ti (Signature of Permittee or Designee) SWU-242, Last modified 7/31/2013 Pagel of 2 1. Outfall Description: Outfall No. Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Stcrac-rt of MOl l (ALA rakme+t > . 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: I ��,>7f- br'cwn l deur- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Ae,-rN-P 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 61 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended • solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 �Z 3 4 5 7. Is there any foam in the stormwater discharge? Yes CNo B. Is there an oil sheen in the stormwater discharge? Yes 6) 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition • may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 • STORMWATER DISCORGE OUTFALL (SDO) GENERAL PERMIT NO. NCG200000 DISCHARGE MONITORING REPORT (DMR) CERTIFICATE OF COVERAGE NO. NCG200© 7 Mail original and one copy to: FACILITY NAME 5 e// n eS� C t�I�4f rC Division of Water Quality PERSON COLLECTING SAMPLES Q.- Attn: Central Files CERTIFIED LABORATORY -- r! d Lab # 1617 Mail Service Center Lab # Raleigh, North Carolina 27699-1617 COUNTY PC iS0 f) PHONE NO. (3 F( ,).3�i9 —C�,gaQ Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: ca?0 / 44 (This monitoring report is due at the Division no later than 30 days from the date the facility .F receives the sampling results from the labora&9" �w Outfall No. Date Sample Collected mo/dd/ r Total Rainfall inches 00530 00340 00556 00400 01113 01119 00980 01114 01 _ Total Suspended Solids m Chemical Oxygen Demand m Oil & Grease m pH S.U. Cadmium m Copper m Iron m Lead m Zinr m Benchmark - - 100 120 30 6.0 — 9.0 0.001 0.007 N/A 0.03 0.067 J� . -.Js' 37 2, "7 0 �� 000 • 2% 1,42 ,1 0, 006,113 ' If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. z Total recoverable. Only complete Part B if this facility uses more than 55 gallons of new motor oil per month. Part B: Vehicle Maintenance Activity Mo itoring Requirements Outfall No. Date Sample Collected mo/dd/ r Total Rainfall inches New Motor Oil Usage allmonth 00530 00400 00556 Total Suspended Solids mgA pH S.U. Oil & Grease Benchmark - I - I - 100 6.0 — 9.0 30 Us/ f�© N �AIs2V015 CENTRgL FILES DWR SECTI YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date) NCG200000 DMR Form SWU-256 Page 1 of 1 Outfall No. j Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No Ej If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWO to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 00556 00400 01113 01119 00980 01114 01094 Tss m COD m Oil & Grease m pH S.U. Cadmium MgA Copper m Iron m Lead m Zinc m Benchmark N/A 100 120 30 6.0 - 9.0 0.001 0.007 N/A* 0.03 0.067 Date Sample Collected, mo/dd/yrAM 6<5 J 'Vo 6 1 1 C103�) AIN/0 /11VJ 6100-2/ 3 *Iron benchmark was removed due to variable ambient in -stream concentrations throughout State. However, 90% of ambient monitoring data collected since 2004 by DWQ show background iron concentrations less than or equal to 2.1 mg/I. Stormwater discharge iron concentrations greater than 2.1 mg/I may be contributing iron above background levels. SW U-250NCG20-11.16.09 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWO to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 00556 00400 01113 01119 00980 01114 01094 TSS m COD m Oil & Grease m pH S.U. Cadmium m Copper m Iron m Lead m Zinc MgA Benchmark N/A 100 120 31) 6.0 — 9.0 0.001 0.007 N/A* 0.03 0.067 Date Sample Collected, mo/dd/yr i "Iron benchmark was removed due to variable ambient in -stream concentrations throughout State. However, 90% of ambient monitoring data collected since 2004 by DWQ show background iron concentrations less than or equal to 2.1 mg1l. Stormwater discharge iron concentrations greater than 2.1 mg1I may be contributing iron above background levels. SW U-250NCG20-11.16.09 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date /i Mail Annual DMR Summary Reports to Your Regional DWQ Office: DWQ Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 807-6300 ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE 3800 Barrett Drive Raleigh, NC 27609 (919) 791-4200 WINSTON-SALEM REGIONAL OFFICE 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 WASHINGTON REGIONAL OFFICE 943 Washington Square Mall Washington, NC 27889 (252) 946-6481 CENTRAL OFFICE 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 807-6300 WILMINGTON REGIONAL OFFICE 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910) 796-7215 "To preserve. protect and enhance North Carolina's water._." SW U-250NCG20-11.16.09 X��Q=� NCDENR • Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. httl2://12ortal.ncdenr.org/web/wq/ws/su/nndessw#tab-4 Permit No.: N/C/_ Facility Name: LL County: Per- c Inspector: Date of Inspection: Time of Inspection : /D .' 25 Total Event Precipitation (inches): () eb Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 12f Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). • Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. E A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall . and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature otPermittee or Desigi4e) SWU-242, Last modified 10/25/2012 Pagel of 2 1. Outfall Description: Outfall No. I Structure • Receiving Stream: rM etc.) L 1 tC h Describe the industrial activities that occur within the outfall drainage area: -P r"l—iAL /AL ) 6ahi'ne4-s 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: I 1 A %1 t R r'Ut, n 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A/ C1 6C�a-r 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (D 2 3 4 5 • 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 U) 3 4 5 7. Is there any foam in the stormwater discharge? Yes N B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe • Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year aUl 4 General Permit No. NCG200000 Certificate of Coverage No. NCG20 U❑ 5❑�®❑ This monitoring report summary is due to the DEMLR Regional Office no later than March 15` of each calendar year. Facility Name: Lies be it :/1V4S4-Meo+ ReccAUt /'c1 County: Derson Phone Number: (334e ) .32 1-04DOU Total no. of SDOs monitored Outfall No. I I Is this outfall currently in Tier 2 (monitored monthly)? Yes , No Z Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes [v" No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency Received approval from DEMEl �LR to reduce monitoring frequency Other #Ai C4 "ie.^ /�„'(- Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, m /l Non -polar oil & grease, mg/1 Total Copper, mg/1 Total Lead, m l Total Zinc, mg/1 Benchmarks A/4 100/50 120 15 0.010/0.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr - - .l O 3 z 0xc U.0 -o-oll - U. 15 o 00 0.00 0, - CS 0 3 ,r DWR SIECTION r� p =� JI VI\wI v-I".,. •- � SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. ol` Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No [� Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No [' If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, mg/1 Non -polar oil & grease, mg/1 Copper, mg/1 Lead, m /l Zinc, m /1 Benchmark N/,9 100/50 120 15 0.010i.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr - 3 I v .v0 3 o. OHS 3-a - I &BO Lj5 1 0.01')- - 5- ;� I .ova 0.W3 5 S - 0. yo G 0, a-) 3 SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No.. -3 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall 3 Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, m COD, mg/1 Non -polar oil & grease, mg/1 Copper, mg/1 Lead, m Zinc, m /1 Benchmark N/A 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 Fresh/salt Date Sample Collected, mo/dd/yr- V5 ;L .ol / 0.003 a. o 5- - v•q cx) o , v SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No.. Ig_ Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No M", Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, mg/1 Non -polar oil & grease, mg/1 Copper, mg/1 Lead, mg/1 Zinc, m /1 Benchmark V'1 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr �1-7� - O• 6 3 3 3 .vo 3 U. o a SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. 5 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other Outfall e5 Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, mg/1 Non -polar oil & grease, m Copper, m /1 Lead, mg/1 Zinc, m /1 Benchmark N14 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr - 5- v.v8 Cr SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. W Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, m /l COD, m /l Non -polar oil & grease, mg/1 Copper, mg/1 Lead, m /l Zinc, in A Benchmark N/A 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr 5- - U.H 0-00 U.UV .0 4fb SW U-250NCG20-01.28.15 Additional Outfall Attachment (make copies as needed for additional outfalls) Outfall No. -4-— Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall Total Rainfall, inches 00530 00340 01119 01114 01094 TSS, mg/1 COD, m /l Non -polar oil & grease, mg/1 Copper, mg/1 Lead, m /l Zinc, m /I Benchmark N/A 100/50 120 15 0.010/.005 fresh/salt 0.075/0.210 fresh/salt 0.126/0.090 fresh/salt Date Sample Collected, mo/dd/yr �- 5- U . 3 U .Cx) 0.001 v . v SW U-250NCG20-01.28.15 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date $ - Mail Annual DMR Summary Reports to Your Regional DEMLR Office: DEMLR Regional Office Contact Information: Asheville Office .. Fayetteville Office Mooresville Office ... (828) 296-4500 ... (910) 433-3300 ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 707-9220 ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE 2090 US Highway 70 225 Green Street Swannanoa, NC 28778 Systel Building Suite 714 (828) 296-4500 Fayetteville, NC 28301-5043 (910) 433-3300 RALEIGH REGIONAL OFFICE WASHINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall Raleigh, NC 27609 Washington, NC 27889 (919)791-4200 (252)946-6481 WINSTON-SALEM REGIONAL OFFICE 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 CENTRAL OFFICE 1612 Mail Service Center Raleigh, NC 27699-1612 (919) 707-9220 MOORESVILLE REGIONAL OFFICE 610 East Center Avenue/Suite 301 Mooresville, NC 28115 (704)663-1699 WILMINGTON REGIONAL OFFICE 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910) 796-7215 SW U-250NCG20-01.28.15