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HomeMy WebLinkAboutNCG120056_MONITORING INFO_20190110STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV uc DOC TYPE El HISTORICAL FILE � MONITORING REPORTS DOC DATE ❑ r)UILl DI tO YYYYMMDD Semi-annual Stormwater Discharge Monitories Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted January 4, 2019 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: ENCO / Pace Analytical Lab Cert. # 591 / 67 Comments on sample collection or analysis: Part A: 5tormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2018 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑. Monthly' [month �C�p�-DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA CC ` ED ❑Zero -flow ❑Water Supply ❑SA JAN 10 2019 ®Other: wS-IV, Nsw CENTt�L FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION ❑ No discharge this period:' Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand -_ - Fecal Coliform Total Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 ml 100 mg/L or 50 mg/L 001 12/20/18 0.88 120 360 33 002 12/20/18 0.88 590 96.0 95 003 12/20/18 0.88 17 6.0 3.7 004 12/20/18 0.88 15 14.0 26 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24hour rainfall amount, inches3 Non -polar O&G/TPH by, EPA 1664 (SGT-HEM) ' Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 12/20/18 0.88 <2.70 33 7.4 002 12/20/18 0.88 <2.70 95 7.1 003 12/20/18 0.88 <2.70 3.7 7.6 004 12/20/18 0.88 <230 26 7.0 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Dischar e" reports within 30 days of receipt of the lob results or at end of monitoring eriod in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aw re t t there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permfttee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 NI _ F=JVCO Laboraton*es Accurate. Timely. Responsive. Innoratiue. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, January 2, 2019 Republic Services of NC (RE014) Attn: Christopher Gustin 9650 Oxford Rd Rougemont, NC 27572 RE: Laboratory Results for Project Number: Semi -Annual, Project Name/Desc: Upper Piedmont Stormwater ENCO Workorder(s): CB17202 Dear Christopher Gustin, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, December 20, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, i Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 c, 1 MNES,CO www.encolabs.com SAMPLE SUMMARY/LABORAT0RY CHRONICLE Client ID: Outfall#1 Lab ID: CB17202-01 Sampled: 12/20/18 08.00 Received: 12/20/18 11:14 Parameter Preparation HoigQatCjTlme(9) P= Vate/Time(s) Analysis DatelTime(s) EPA 1664A EPA 1664A 01/17/19 12/26/18 14:14 12/31/18 13:42 Feld NO PREP 12/20/18 08:14 12/20/18 08:00 12/20/18 08:00 SM 254OD•2011 NO PREP 12/27/18 12/27/18 12:39 12/27/18 12:39 SM 5220D-2011 Same 01/17/19 12/26/18 10;10 12/26/18 1120 alentID: Outfall#2 tab ID: C017202-02 Sampled: 12/20/18 08:35 Received: 12/20/18 11:14 Parameter EPA 1664A Preparation EPA 1664A Hol4 Qatelf7ime(s) 01/17/19 ftgg DatelTime(s) 12/26/18 14:14 An ftsis DatelTime(s) 12/31/18 13:42 Feld NO PREP 12/20/18 08:49 12/20/18 08:35 12/20/18 08:35 SM 254OD-2011 NO PREP 12/27/18 12/27/18 12:39 12/27/18 12:39 SM 5220D-2011 Same 01/17/19 12/26/18 10:10 12/26/18 13:20 Client ID: Outfall#3 Lab ID: CB17202-03 Sampled: 12/20/18 08:15 Received: 12/20/18 11:14 e8 meter PMpjratlQn Hold Date/Time(s) PrSR Date/Tlmefsl Anati sis DatelTime(s) EPA 1664A EPA 1664A 01/17/19 12/26/18 14:14 12/31/18 13:42 Feld NO PREP 12/20/18 08:29 12/20/18 08:15 12/20/18 08:15 SM 254OD•2011 NO PREP 12/27/18 12/27/18 12:39 12/27/18 12:39 5M 522OD-2011 Same 01/17/19 12/26/18 10:10 12/26/18 13:20 Client ID: Outfall#4 Lab ID: C817202-04 Sampled: 12/20/18 09:00 Received: 12120/18 11:14 Parameter EPA 1664A Preparation EPA 1664A Hold Date/Ume(sl 01/17/19 Prep Date/Time(s) 12/26/18 14:14 Analysis Date(ijMe(sl 12/31/18 13:42 Feld NO PREP 12./20/18 09:14 12/20/18 09:00 12/20/18 09:00 SM 2540D-2011 NO PREP 12/27/18 12/27/18 12:39 12127/1H 12:39 SM 5220D-2011 Same 01/17/19 12/26/18 10:10 12/26/18 13:20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 0utfaO#1 Lab ID: CB17202-01 Anal ResuILS Elm ma E" Units Holhod NGt Chemical Oxygen Demand 120 10 10 mg/L SM 5220D-2011 PH 7.4 0.0 0.0 PH Units Field Total Suspended Solids 33 10 10 mg/L SM 254OD•2011 Client ID: Outfall#2 Lab ID: CB17202-02 Analyte Results Flag MQL En units Method Notes Chemical Oxygen Demand 590 10 10 mg/L SM 5220D-2011 PH 7.1 0.0 0.0 PH Units Field Total Suspended Solids 95 33 33 mg/L SM 254OD-2011 Client ID: Outfa[1#3 Lab ID: CB17202-03 Anal Results flil9 MDL E" Units Methods Notes Chemical Oxygen Demand 17 10 10 mg/L SM 5220D-2011 PH 7.6 0.0 0.0 PH Units Feld Total Suspended Solids 3.7 3.3 3.3 mg/L SM 254OD-2011 Ghent ID: Outfall#4 Lab ID: CB17202-04 Anal Results E6U H6 M vau Metbod NRLO;i Chemical Oxygen Demand 15 10 10 mg/L SH 5220D-2011 PH 7.0 0.0 0.0 PH Units Feld Total Suspended Solids 26 5.0 5.0 mg/L SM 2540D•2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in tuu• I Page 3 Of 1 O Iwr �co www.encolabs.com ANALYTICAL RESULTS Description: Outfall#1 Lab Sample 1D:CB17202-01 Received: 12/20/18 11:14 Matrix: Surface Water Sampled:12/20118 08:00 Work Order: CB17202 Project: Upper Piedmont Stormwater Sampled By: CLIENT (Classical Chemistry Parameters ' ^ - EACO Cary mt fled arralyte fNC 5911 Analyte ICAS_Numberl Rs,sul Flag Units RE MPIL POL Batch Method Analyzed By NRN2 Chemical Oxygen Demand^ 120 mg/L 1 10 10 BL26012 SM 5220D-2011 12/26/18 13:20 1OC Total Suspended Solids^ 33 mg/L 4 10 10 BL27003 SM 254OD-2011 12/27/18 12:39 OMR Field Parameters Analyte fCAS Numberl j;esul HIS Units DE M1P_L EQL ktrh Method Analyzed By 1Y41l� PH 7.4 pH Units 1 0.0 0.0 BL21007 Feld 12/20/18 08:00 CL1 Classical Chemistry Parameters Analyte rCAS Numberl Results Flag Units PE MDL PQL Batch Method Analyzed 01 Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5.00 8L26014 EPA 1664A 12/31/18 13:42 5MA Description: Outfall#2 tab Sample ID:CB17202-02 Received: 12/20/18 11:14 Matrix: Surface Water Sampled: 12/20/18 08:35 Work Order: C617202 Project: Upper Piedmont Stormwater Sampled By: CLIENT Classical Chemistry Parameters ' ^ - EMCO Cary r[rtilled enalyte W 591J Analyte rCAS Numbed Ress11l;i F122 mom DE HU I'41 Batch Meth Anahraed By N Chemical Oxygen Demand^ 590 mg/L 1 10 10 81-26012 SM 5220D-2011 12/26/18 13:20 ]OC Total Suspended Solids^ 95 mg/L 13.3 33 33 81-27003 SM 254OD-2011 12/27/18 12:39 OMR Field Parameters Analyte rCAS Numbed $PviIYC4 Units DE MDL P patch Method Analyzed 21 Notes PH 7.1 pH Units 1 0.0 0.0 BL21007 Feld 12/20/18 08:35 CLI Classical Chemistry Parameters Analyte rCAS Number] ResulElan llnit;i DE M" EQL @d[th Method Analyzed @y Notes Oil & Grease (HEM-SGT) Non -Polar Material 2,70 U mg/L 1 2.70 5.00 81-26014 EPA 1664A 12/31/18 13:42 SMA FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. I Page 4 of 1 O WNS_00) www.encolabs.com ANALYTICAL RESULTS Description: Outfall#3 Lab Sample ID:CB17202-03 Received: 12/20/18 11:14 Matrix: Surface Water Sampled: 12/20/18 08:15 Work Order: CB17202 Project: Upper Piedmont Stormwater Sampled By: CLIENT Chemistry Parameters ^ - ENCO Cary certified anaAfe (NC 5911 Analvte fCAS Numberl Result Elan mam pF ma p¢b Rates Method Analyzed OX Notes Chemical Oxygen Demand^ 17 mg/L 1 10 10 81-26012 SM 5220D-2011 12/26/18 13:20 ]OC Total Suspended Solids^ 3.7 mg/L 1.33 3.3 3.3 8L27003 SM 254OD-2011 12/27/18 12:39 OMR Field Parameters Results Flas 111111211 PE MIX PQL Batcli Method Ans111a-ed fix dotes PH 7.6 pH Units 1 0.0 0-0 8L21007 Feld 12/20/18 08:15 CU Classical Chemistry Parameters Analyte fCAS Number! Resul am unm DF HU Pa IgGh Method Analyzed jay Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5.00 BL26014 EPA 1664A 12/31/18 13:42 SMA Description: Outfall#4 Lab Sample 10:CB17202-04 Received: 12/20/18 11:14 Matrix: Surface water Sampled: 12/20/18 09= work Order: CB17202 Project: Upper Piedmont Stormwater Sampled By: CLIENT Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] nalyfg_[CAS Number) Resat flag !molts Pf M2l. PQL @dLlh Method Armed $y N� Chemical Oxygen Demand ^ 15 mg/L 1 10 10 8L26012 SM 5220D-2011 12/26/18 13:20 10C Total Suspended Solids^ 26 mg/L 2 5.0 5.0 8L27003 SM 254OD-2011 12/27/18 12:39 OMR Field Parameters Anahrte fCAS Numkrl Results ELOA Units PFF MPA PQL Batch Method Analyzed Ox Nootes PH 7.0 pH Units 1 0.0 0.0 81-21007 Feld 12/20/18 09:00 CLI Classical Chemistry Parameters Anahrte fCAS Numberl Rend4 Ellis Ullitri pE M" E" RAW1 Method Analyzed By No Oil & Grease (HEM-SGT) Nan -Polar Material 2.70 U mg/L 1 2.70 5.00 BL26014 EPA 1664A 12/31/18 13:42 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full I Pager) Of 1 O r 9 �0 a www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SL26012 - Same Blank (81.26012-BLKI) Prepared: 12/26/2018 10: 10 Analyzed: 12/26/2018 13:20 Spike Source %REC RPD .Analvte Result Flag P9L Units Level Result %REC Limits RPD Limit Hates Chemical Oxygen Demand 10 U 10 mg/L LCS (811.26012-BS1) Prepared: 12/26/2018 10: 10 Analyzed: 12/26/2018 13:20 Spike Source %REC RPD Analvte Result Flag P-QL Units Level Result %REC u61i RPD Limit Motes Chemical Oxygen Demand 480 10 mg/L 500 97 90.110 Matrix Spike (8L26012-M51) Prepared: 12/26/2018 10: 10 Analyzed: 12/26/2018 13:20 Source: C516033-03 Spike Source %REC RPD Anaivte Result Flag POL Units Level Result %REC Llm(ts RPO Limit Notes Chemical Oxygen Demand 510 10 mg/L 526 IOU 98 90-110 Matrix Spike Dup (BL26012-MSDl) Prepared: 12/26/2018 10: 10 Analyzed: 12/26/2018 13:20 Source: CB16033-03 Spike Source %REC RPD 1illalYte Result Flag SQL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 520 10 mg/L 526 10 U 99 90.110 0.8 10 Batch OL27003 - NO PREP Blank (BL27003-BLK1) Prepared & Analyzed: 12/27/2018 12:39 Spike Source %REC RPD _Analvte Result Flag ML Units Level Result °/a REC Ldmlts RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (BL27003-BS1) Prepared & Analyzed: 12/27/2018 12:39 Spike Source %REC RPD .Anaivte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 95 7.5 mg/L 100 95 BG-120 Duplicate (BL27003-DUPl) Prepared & Analyzed: 12/27/2018 12:39 Source: CB03710-01 Spike Source %REC RPD -ArWwtc Resul Flag F_QL Units Level Resul %REC ihmltf RPD Limit Notes Total Suspended Solids 420 50 mg1L 400 4 20 Duplicate (8L27003-DUP2) Prepared & Analyzed: 12127/2018 12:39 Source: CB03710-02 Spike Source %REC RPD _Anaivtc Result Flag POL Units Level Result %REC Limltg RPD Limit Notes Total Suspended Solids 280 50 mg/L 290 1 20 Classical Chemistry Parameters - Quality Control Batch OL26014 - EPA 1664E Blank (81.26014-BLKl) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source %REC RPD Analvte Result Flaq ML Units Level Result %REC Llmfts RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 u 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. Page 6 Of 10 �co www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch BL26014 - EPA 1664E - Continued LCS (BL26014-BS1) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source %REC RPD Anallrft RcEult Fld9 POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 80.0 5.00 mg/L 81.6 98 64-132 LCS Dull (BL26014-BS01) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source %REC RPD .Analvt4 Result nag POL Units Level Result %REC Limits RPD Llmlt Notes_ Oil & Grease (HEM-SGT) Non -Polar Material 73.6 5.00 mg/L 80.0 92 64-132 8 34 Matrix Spike (BL26014-114SI) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Source: B505483-01 Spike Source %REC RPD .Analvtc Result Flau POL Units Level Result %REC Limits RPD Unfit W&D Oil & Grease (HEM-SGT) Non -Polar Material 77.9 5.00 mg/L 85.1 2.70 U 92 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. I Page 7 Of 1 O (��Go www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit, The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 1 O PAI C®10775 Central Pon Dr, 4810 Executive Park Court, Suite 111 --- - - --- - t02-A W Orlando. FL 32824 JacksomMa. FL 32216.606E Cary, NC (407)82rr5314 Fax(407)850-6945 (904)296-31'107 Fax(904)296-6210 (9t9)467- Client Nm ae Republic Services of NC (RE014) Prajecl Number Sergi-Annualm R © N u7 L CO O U - u- l-• 0_ ((}.. Y 0 NC G t!3 N H Address_ - 9650 CWord'Rd Protect Nae/Desc ,. Upper Piedmont Stormwater CitylST21p Rougemont. NC 27572 PO N 1 Billing Info' 2418: P07087378- Tel (3.36) 364-3699 Fax ReporWtg Contact Christopher Gustin s, . Samplar(s)Name, Affiliation (Print) Bi8i Contact Christopher Gustin Sampler(s) Signature Sze Location / Time Zone - Preservation item N Sample ID (Fre)d Ideniiricauon) Collection Date Collection Tme Comp 1 Grab Matrix (see codes) Total N of Containers f i L-z.� /�' B:a�A Sw 5 X X X X ni�ll '6 A /z- 7-D Q" .31 A (� Sw 5 X� X ' X- X /1-- 2,4 �. 8. /� A G Sw - 5 X X x X. Sw 5 x x x x- oodwinds Industrial Ct. - 27511 MM Fax (S19) 467-3515 Page •• of O equested Analyaes Requested Turnarou r - Times o rn Note: Rush requests subp acceptance by the fecikS CO d Standard Expedited Due Lab Workarder • G,�B�17�2�02.. Codes) (Comibno as nocesery)" Sample Comments e Ki! Prepered By ime £ielinquished ay - - Dat y Da une CwnrQj9tWSPOw1 Reponang Requirements Retinquished By DaWrove Received By Data/rrme Relinquished By DaI TTane Received By DataTma er N's & Temps an B=eipt Condition upon Receipt tL Acceptable Unacceptable Matrlr : GW-UrOuridwaler SO -SW OW-0nnkang Water SE -Sediment SW -Surface water WW-Wastawatef A-Av O-Other (Keith" in comments) Press on: I -Ice M-MCI N-MN03 5-t12504 NG-NaOM Other (aeraa in comments) Note: All samples submitted to ENCO Lath are in accordance with the terms and conditions listed on the reverse of this Term. unless prior wntten agreementS exist e Ki! Prepered By ime £ielinquished ay - - Dat y Da une CwnrQj9tWSPOw1 Reponang Requirements Retinquished By DaWrove Received By Data/rrme Relinquished By DaI TTane Received By DataTma er N's & Temps an B=eipt Condition upon Receipt tL Acceptable Unacceptable Matrlr : GW-UrOuridwaler SO -SW OW-0nnkang Water SE -Sediment SW -Surface water WW-Wastawatef A-Av O-Other (Keith" in comments) Press on: I -Ice M-MCI N-MN03 5-t12504 NG-NaOM Other (aeraa in comments) Note: All samples submitted to ENCO Lath are in accordance with the terms and conditions listed on the reverse of this Term. unless prior wntten agreementS exist Matrlr : GW-UrOuridwaler SO -SW OW-0nnkang Water SE -Sediment SW -Surface water WW-Wastawatef A-Av O-Other (Keith" in comments) Press on: I -Ice M-MCI N-MN03 5-t12504 NG-NaOM Other (aeraa in comments) Note: All samples submitted to ENCO Lath are in accordance with the terms and conditions listed on the reverse of this Term. unless prior wntten agreementS exist 9 01 Sample Preservation Verification ENCO Cary MM% CG) =eim Work Order: CB17202 Project: Upper Piedmont Stormwater Client: Republic Services of NC (RE014) Project Semi -Annual Logged In: 20-Dec-18 11:20 Logged By: John C King Preservation Check Performed By: Date/Time: 12,2c)-(-F 1 L, C1317202-01 Pres,(pH)V', pH,Checked1 Control., Adjw df'IDal mW,.TY KPH -Adu t Reagent Used/Cm Mets' t IReqUir6a�nt B 250rnLA+H2SO4 <2 Y I N I M-A Y I N C 250rnLA+H2SO4 <2 Y / N I Y / N I& D 250rnLP+H2S0.4 <2 O)l - N NA Y I NA C817202-02 Cont Type We�,(pH) ' Requirement pHChecked Y In Control pH Adjusted ' Dwerllinie, -, - � � � — 7 ' It � - . - , Reagent Used/Cornrnentsi .. oAdiiisted!., 8 250rnLA+H2SO4 <2 Y I N I ^ Y 1 N ICtIA C 250mLA+H2SO4 <2 Y! _N 16A -Y N /0 D 250rnLP+H2SO4 <2 (D)l N / NA Y N1 NA CB17202-03 rC6.nd�,- 7 tv. ;4dPresi(pH),, pH Checked DaterFime, e pl­�djbited,� Adiustdr Re�gent.Usdd/Comrnehts B 250rnLA+H2SO4 <2 Y / N IrA C 250rnLA+H2SO4 <2 Y / N / Y / N D 250rnLP+H2SO4 <2 I N / NA Y! I NA CB17202-04 Cont. Type. pH H Checked 0 Adjusted' usted Reagent:DatelTime e Requirement In Control Adjusted? B 250mLA+H2SO4 <2 Y / N /(N Y I N C 250mLA+H2SO4 <2 Y / N I A Y / N! D 250rnLP+H2SO4 <2 V I N / NA Y I& N Reaqent Name ID 2 pH Strip ID: C: \ELMN-nP rint4ko-Preservation Check. rpt Reagent Name ID 31 4 1 Reagent Name ID F Page 10 of 10 Fage 1 aceAnalytrcal —pacefabs.mn January 02, 2019 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: CB17202 Pace Project No.: 92411625 Dear Ms. Franz: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 1DD Huntersville, NC 28078 (704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2018. The results relate only to the samples included in this report. Results reporte d herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please f eel free to contact me. Sincerely, Qa. qq , `,c,'-,ani Angela Baioni angela.baioni@ pacelabs.com (704) 875-9092 Project Manager Enclosures VAI61Z4&612 W.V-16]:Ti71La].V L1i VWj&i&I This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical. wwwpocelabs.corn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: CB17202 Pace Project No.: 92411625 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certiflcation #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinkino Water Certification #: 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of pace Analytical Services, LLC. Page 2 of 13 aceAnalytrcal wwwpacetabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)87S9D92 Project: Pace Project No.: CB17202 92411625 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92411625001 Outfall #1 SM 9222D-2006 DJB 1 PASI-R 92411626002 Outfall 02 SM 9222D-2006 DJB 1 PASI-R 92411626003 Outfall 03 SM 9222D-2006 DJB 1 PASI-R 92411626004 Outfall 94 SM 9222D-2006 DJB 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 acmnalytical www.pace4bs.cwn ANALYTICAL RESULTS Project: CB17202 Pace Project No.: 92411625 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Outfall #1 Lab ID: 92411625001 Collected: 12/20/18 08:00 Received: 12/20118 12:50 Matrix: Water Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Colifonm RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 360 CFU1100 mL 1.0 1 12/20/18 15:35 12/21/18 14:00 Date. 01/02/2019 09:42 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 (�IaneAnalyficale www.pocelab.cam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: C817202 Pace Project No.: 92411625 Sample: Outfall #2 Lab ID: 92411626002 Collected: 12/20/18 08:35 Received: 12/20118 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 96.0 CFU1100 mL 1.0 1 12/20/18 15:35 12/21/18 14:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2019 09:42 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical oww.pacelabs.aom ANALYTICAL RESULTS Project: CB17202 Pace Project No.: 92411625 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvOle, NC 28078 (704)875�9092 Sample: Outtatl A3 Lab ID: 92411625003 Collected: 12/20118 08:15 Received: 12/20/18 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual MBIO 92220 Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 6.0 CFU1100 mL 1.0 1 12/20/18 15:35 12/21/18 14:00 Date: 01/02/2019 09:42 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 13 0 acmnalytical www.pweAabs.com ANALYTICAL RESULTS Pace Analytical Services. LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875.9092 Project: CB17202 Pace Project No.: 92411625 Sample: Outfall #4 Lab ID: 92411626004 Collected: 12/20/18 09:00 Received: 12/20118 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 14.0 CFU11DO mL 1.0 1 12/20/18 15:35 12/21118 14:00 Date: 01102/2019 09:42 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 7 of 13 (�IacieAnalytical wwwpacefafu.mm QUALITY CONTROL DATA Project: C617202 Pace Project No.: 92411625 QC Batch: 450035 Analysis Method: SM 9222D-2006 OC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - RAL Associated Lab Samples: 92411625001, 92411625002, 92411625003, 92411625004 METHOD BLANK: 2463013 Matrix: Water Associated Lab Samples: 92411625001, 92411625002, 92411625003, 92411625004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFUl100 mL ND 1.0 12/21/18 14:00 SAMPLE DUPLICATE: 2463014 92411625001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 360 390 8 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Results presented on this page are inthe units Indicated by the "units" column except Mere an altemate unit is presented b the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2019 09:42 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 0 aceAnalytical www.pacelabs.rnm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 2BO78 (704)875-9092 QUALIFIERS Project: CB17202 Pace Project No.: 92411625 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 01I0212019 09:42 AM without the written consent of Pace Analytical Services, LLC, Page 9 of 13 aceAnalytical www pacelabs.cnm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: C617202 Pace Project No.: 92411625 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92411625001 Outfall #1 SM 9222D-2006 450035 SM 922213-2006 450048 92411625002 Outfall #2 SM 922213-2006 450035 SM 9222D-2006 450048 92411625003 Outfall #3 SM 9222D-2006 450035 SM 9222D-2006 450048 92411625004 Outfall #4 SM 922213-2006 450035 SM 9222D-2006 450048 Date: 01/02/2019 09:42 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recei t(SCUR) Page 1 of 2 Document No.: issuing Authority: F-CAA-CS-033-Rev.06 Pace Carolinas Quality office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvlfle Client Name:. Project #: EnCti Courlen Fed Ex OUPS USPS Ocilent ❑ commercial ❑Pace []Other:_ Custody Seal Present? []Yes Sfo Seals Intact? []Yes [�Ko Mechanicsville[] WOp:92$11625 92411625 Oats/Inldats Person Eramining Contenb., I L I"l % -a Packing Material: []Bubble Wrap []Bubble Bags QN-one ❑ other Biological -tissue Frozen? Thermometer. []Yes[]NO❑N/A ©IR Gun 10: GA%TW*I Type oflce: jet ❑Blue ❑Nona Cooler Temp (IC): y , 0 Correctlon Factor, Add/Subtract ('C) a tS q Temp should be above freezing to 6'C Cooler Temp Corrected ('Qj 'A []Samples out of temp criteria. Sampler on ico, cooling process his begun USDA Regulated Soli ([ KIN water sample) Did samples odainate In a ouarantine rune within the Unhed Statrs: CA. NY_ er SC fcheck mans)? nid samnlas oddnate from a fareiin source flnternat!onaliv. Yes No Including llswalt and Puerto RlcolY QYas ©Na Comments/Discrepancy: Chain of Custo Present? oNo N/A 1, Samples Arrived within Hold Time? s Na NIA 2. Short Hold Time Am sta 02 hr.? []NO J3NJA 3. Rush Turn Around Time Requested? QY. MNIA 4. Sufficient Volume? QV6 ONO N/A S. Correct Containers Used? -Pace Containers Used? 9<s _ ❑No " No •,.C]N/A • [ NIA 6. Containers Intact? es ONO N/A 7. Dissolved analyst Samples Field Filtered? Yes No /A 8• Sample tabols Match COC? [oyes ❑Na []NIA 9. Heads ace in VOA Vials >S-6mm)7 a No /A ID, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes j]Na No L9 /A /A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLLMON r Lot ID of split containers: Person contacted: Project Manager SCURF Review: i' 11 � b Project Manager SRF Revlaw: 29 Date/Time: Field Oita Required? []Yes ❑No Date: Page 11 of 13 Document Name: Document Revised: February 7, 2018 a an��d Sam ie Coftdltion Upon Receipt SCUR Pole 1 oft Document No.: Issuing Authority: • �^"P'r'aj F-CAR-CS-033-Rov.05 Pace Carolinas Quallty Office *Check mark top half of box If pH and/or dechlorinatlon Is verified and within the acceptance range for preservation samples. Exceptfons: VOA, Collfoim, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project# WO# • 9241 16L5 1` PM: RMB Due Date: 01/02/19 CLIEW: u-•I::Nco Z aCL E o IL 3 z ¢ n M E m Co in ry u E do 4. z v re Y ry IS a E rr c A 7 pi 2 a C E $ 3 Z j >; a� S e t � a1 GCL a N & r�r v fi aEE d V z c� eJ ( < E E i E a } Q if X ` = p. n 9 � t n E A � ti yi `^• m S i b E A E z e t 2 1 3V + 1 4 6 7 9 10 E pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added tot M Nate: Whenever there is a dLtcrepancy affecting North Caroana compliance samples, a copy of this farm vrlll be sent to the North Carolina 0E1tNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 12 of 13 SUBCONTRACT ORDER ENCO Cary CB17202 ! ! SENDING LABORATORY, RECEIVING LABORATORY: ENCO Cary Tri-Test (Raleigh) 102-A Woodwinds Industrial Court 6701 Conference Drive Cary, NC 27511 Raleigh, NC 27607 Phone: 919.467.3090 Phone :(919) 8344984 Fax: 919.467,3515 Fax: Project Manager: Stephanie Franz Project State of Origin: North Carolina Sub Lab ID Orlglnating Lab ID Client Matrix Dale Sampled Sample Comments Outrali#1 Surface Water 20-Dec-18 08:00 D D ( Coliform, Feca19223E 02-Jan-19 I5:00 20-Dec-I8 15:55 Containers Supplied: Sleri1e250mLP+NaThio (E) Sub Lab ID rlg noting Lab ID Client Matrix Dale Sampled Sample Comments Outfe11102 Surface Water 20-Dec-18 08:35 U [} Z- Coliform, Fecal9223B 02-Jan-19 15:00 20-Doc18 16:30 Containers Supplied: Sterile250ml-P+NaThio (E) I u h ID Orig net ng Lob 1D Client Matrix Date Sampled Sample Comments Outfall#3 Surface Water 20-Dec-1808.15 OE) FORM I �/ Coliforrlt, kcut922313. , , 024an-19 15:00 20-Dec-18 16:10 Containers Supplied.• Sterila250mLP+NaTltio (E) Sub Lab ID Originating Lah ID Client Matrix Date Sampled Sample Comments Outfall#4 Surface Water 20-Dec-18 09:00 Li Coliform, 1-ccal9223B 02-Jan-19 15:00 20-Dec-t8 16:55 Containers Supplied: Steri1e250m1..P+NaThio (E) J (plc-t- X-L1.2a11-p1'% 1-;L54 page IP@I1913 of 13 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted July CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: ENCO / Pace Analytical Lab Cert. # S91 / 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �2017 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthlyl (month] DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEIVED ®Other: WS-IV, NSW JUL 07 2017 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTRAL FILES DWR SECTION ❑ No discharge this period:2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks - - 1Z0 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 001 06/19/17 2.1 45 6.0 6.9 002 06/19/17 2.1 64 53.0 40 003 06/19/17 2.1 34 6.0 17 004 06/19/17 2.1 39 900 130 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 06/19/17 2.2 <2.70 6.9 7.87 002 06/19/17 2.1 <2.70 40 8.28 003 06/19/17 2.1 <2.70 17 7.82 004 06/19/17 2.1 <2.70 130 8.1 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 3 Z-,c:;r 7 (Date) Permit Date:11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Nk ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, June 28, 2017 Republic Services of NC (RE014) Attn: Christopher Gustin 9650 Oxford Rd Rougemont, NC 27572 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Upper Piedmont Stormwater ENCO Workorder(s): CA06955 Dear Christopher Gustin, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, June 19, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from - outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only m the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 1 CIE wNCO www.encolabs.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client ID: SW#2 Lab ID: CA06955-01 Sampled: 06/19/17 09:00 Received: 06/19/17 13:00 Pagameter EPA 1664A Hold DatelTime(sl 07/17/17 Prco Date/Time(s) 06/21/17 Analysis Date/lime(s) 11:28 06/21/17 14:17 Feld 06/19/17 D9:14 06/19/17 09:00 06/19/17 09:00 SM 2540D-1997 06/26/17 06/26/17 14:47 06/26/17 14:47 SM 5220D-1997 07/17/17 06/20/17 11:28 06/20/17 15:26 Client 1D: SW#1 Lab ID: CA06955-02 Sampled: 06/19/17 09:30 Received: 06/19/17 13:00 Parameter EPA 1664A Hold Date/Time(s) 07/17/17 prep DatelTime(sl 06/21/17 Analysis DatelTime(s) 11:28 06/21/17 14:17 Feld 06/19/17 09:44 06/19/17 09:30 06/19/17 09:30 SM 2540D-1997 06/26/17 06/26/17 14:47 06/26/17 14;47 SM 5220D-1997 07/17/17 06/20/17 11:28 06/20/17 15:26 Client ID: SW#3 Lab ID: CA06955-03 Sampled: 06/19/17 10:15 Received: 06/19/17 13:00 Parameter EPA 1664A Hold Date/Time(s) 07/17117 Prep DatelTime(s) 06/21/17 Analysis DatelTime(s) 11:28 06/21/17 14:17 Feld 06)19/17 10:29 06/19/17 10:15 D6119/17 10:15 SM 254OD-1997 06/26/17 06/26/17 14:47 06/26/17 14:47 SM 5220D-1997 07J17/17 06/20/17 11:28 06/20/17 15:26 Client I0: SW#4 Lab ID: CA06955-04 Sampled: 06/19/3.7 10:40 Received: 06/19/17 13:00 parameter EPA 1664A Hold oats/Tlme(sl 07J17/17 06/21/17 ) Analysis Date/Time(s) 11:28 06/21/17 14:17 Field 06J19/17 10:54 06119/17 10:40 06/19/17 10:40 SM 254OD-1997 06J26/17 06/26/17 14:47 06/26/]7 14:47 SM 5220D-1997 07J17/17 06/20/17 11:28 06/20/17 15:26 FINAL Thl5 report relates Only to the Sample a5 re[eNed by the laboratory, and may only he reprodu[ed in Full. I Page 2 of 10 ce-1V�C0 www.encolabs.eom SAMPLE DETECTION SUMMARY Client ID: SW#2 Lab ID: CA06955-02 Analld9 Results EWS du E2L Units Mgthod 1Y4I4a Chemical Oxygen Demand 64 10 10 mg/L SM 522OD-1997 PH 8.28 0 0 pH Units Feld Total Suspended Solids 40 12 12 mg/L SM 2S40D-1997 Client ID: SW#1 Lab ID: CA06955-02 Anallds Results flab MPL PQL Unlu Method Ncyte Chemical Oxygen Demand 45 10 10 mg/L SM 522OD-1997 PH 7.87 0 0 pH Units Feld Total Suspended Solids 6.9 2.5 2.5 mg/L SM 254OD-1997 Client ID: SW#3 Lab ID: CA06955-03 Anal ResullGi Flag MPL EEL 1Lab Method Notes Chemical Oxygen Demand 34 10 10 mg/L SM 5220D-1997 PH 7.82 0 0 pH Units Feld Total Suspended Solids 17 8.3 8.3 mg/L SM 254OD-1997 Client ID: SW#4 Lab I0: CA06955-04 Anal ResulL4 Ew M" PQL ymila Mftod IQUM Chemical Oxygen Demand 39 10 10 mg/L SM 5220D-1997 PH 8.1 0 0 pH Units Feld Total Suspended Solids 130 12 12 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. I Page 3 Of 1 Q ENCO www.encolabs.com ANALYTICAL RESULTS Description: SW#2 Lab Sample ID:CA06955-01 Received: 06/19/17 13:00 Matrix; Surface Water Sampled:06119/17 09:00 Work Order: CA06955 Project: Upper Piedmont Stormwater Sampled By:Client JClassical Chemistry Parameters 1 ^ - HKV m y aytllfed arwy- [NC 5911 Analyte rCAS Number] Resul EIA2 Units 2E M21 PZ Batch Method Analyzed By tlRtei Chemical Oxygen Demand^ 64 mg/L 1 10 10 7F20014 SM 5220D-1997 06/20/17 15:26 )OC Total Suspended Solids^ 40 ryl 5 12 12 7F26015 SM 2540D-1997 06/26/17 14:47 OMR Field Parameters Analyte rCAS Numberl Results f1119 MRb QE Mpl, E" Batch Method AnIhMed ft Notes pH 8.28 pH Units 1 0 0 71`20003 Field 06/19/17 09:00 CLI Classical Chemistry Parameters Analyte fCAS Numberl Read*e fibs Units pE HX pQL Both Math AOahaed By Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5,00 7F21007 EPA 1664A 06/21/17 14;17 SMA Description: SW#1 Lab Sample ID:CA06955-02 Received: 06/19/17 13:00 Matrix: Surface Water Sampled: 06/19/17 09:30 Work Order: CA06955 Project: Upper Piedmont Stormwater Sampled Hy:Client (Classical Chemistry Parameters 1 ^ - UliM QVVawbyAeiarRw1w 5YU Anahrte FCAS Number] RMI EId9 y2b pE MU PQL Batch Math Analyzed By Notes Chemical Oxygen Demand^ 45 mg/L 1 10 10 71`20014 SM 5220D-1997 06/20/17 15:26 ]OC Total Suspended Solids^ 6.9 mg/L 1 2.5 2.5 71726015 SM 254OD-1997 06/26/17 14:47 OMR Field Parameters Ana a fCAS Number] Reyu EIw Units 2E MQ6 E21, Batch Meth AliplyzO fly No pH 7.87 pH Units 1 0 0 7F20003 Field 06/19/1709:30 CLI Classical Chemistry Parameters Analyte ICAS Numberl Results MR 5m1lit9 12F M91: PQL Batch Method Analyz By Notes Oil & Grease (HEM-5G17 Nan -Polar Material 2.70 U mcVL 1 2.70 5.00 7F21007 EPA 1664A 06/21/17 14:17 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, I Page 4 of Q 9 �Go www.encolabs.com ANALYTICAL RESULTS Description: SW#3 Lab Sample I0:CA06955-03 Received: 06/19/17 13:00 Matrix: Surface Water Sampled:06/19/17 10:15 Work Order: CA06955 Project: Upper Piedmont Stormwater Sampled By:Cllent Chemistry Parameters ^-B%CVtwyoatA!)iarulyte[AC 5911 Results flag units QE H" M Batch 14gth4d Anallasd ft Notes Chemical Oxygen Demand^ 34 mg/L 1 10 10 7F20014 SM 5220D-1997 06/20/17 15:26 30C Total Suspended Solids^ 17 mg/L 3.33 8.3 B.3 7F26015 SM 254OD-1997 06/26/17 14:47 OMR Field Parameters Analyje [CAS Numberl Result E fin Units PE MQI, EQL A11rh Meth,Anted By lYofac PH 7.82 pH Units 1 0 0 71`20003 Field 06/19/17 10:15 CLI Classical Chemistry Parameters Oil & Grease (HEM-SG1) Non -Polar Material Description: SW#4 Matrix: Surface Water Project: Upper Piedmont Stormwater Results flag units PIE JAK P_QL Batch Method Analyzed ft Not 2.70 U mg/L 1 2.70 5.00 7F21007 EPA 1664A 06/21/17 14A7 SMA Chemistry Parameters Lab Sample ID:CA06955-04 Sa mpled: 06/ 19117 10:40 Sampled By: Client Received: 06/19/17 13:00 Work Order: CA06955 ^ - stun Qwy OaW [AlC 5s11 Analyte FCAS Numberl Results fly Units QF MRL pL Daub lletb Analyzed By No Chemical Oxygen Demand^ 39 mg/L 1 10 10 71`20014 SM 5220D-1997 06/20/17 15:26 10C Total Suspended Solids^ 130 mg/l. 5 12 12 7F26015 SM 254OD-1997 06/26/17 14A7 QMR Field Parameters Besul 11ag Units QE RU PQL Batch Nestled Analyzed By riQLra pH 8.1 pH Units 1 0 0 7F20003 Field 06/19/17 10A0 CLI Classical Chemistry Parameters Analyte [CAS Numbed Results fin MlI a Af M" R L Daub Method Analyzed ft Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5.00 71`21007 EPA 1664A 06/21/17 14:17 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 0f 1 O 0�co www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batd7 7F20014 - Saam Blank (7F20014-BLKI) Prepared: 06/20/2017 11:28 Analyzed: 06/20/2017 15:26 Spike Source %REC RPD Analvte Result Rao POL Units Level Res1lll %REC Umljs RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7F20014-BS1) Prepared:06/2012017 11:28 Analyzed:O6/20/2017 15:26 Spike Source %REC RPD Anal Result Elm PQl unju Level Result %REC ll RPD Limit Notes Chemical Oxygen Demand 510 10 mg/L 500 102 90-110 Matrix Spike (7F20014-14S1) Prepared: 06/20/2017 11:28 Analyzed: 06/20/2017 15:26 Source:CA04561-01 Spike Source %REC RPD Analvte Result Rao POL Units Level Result %REC LlmiRPD Limit Notes Chemical Oxygen Demand 1500 20 mg/L 1000 500 99 90-110 Matrix Spike Dup (7F20014-MSD1) Prepared: 06/20/2017 11:28 Analyzed: 06/20/2017 15:26 Source: CA04561-01 Analvte Chemical Oxygen Demand Bald► 712601S - NO PREP Result Rao POL 1600 20 Spike Source %REC RPD Units Level Result %REC Limits RPD J ill Notes mg/L LOGO 500 109 90-110 6 10 Blank(7F26015-BLKl) Prepared & Analyzed: 06/26/2017 14:47 Spike Source %REC RPD Analldg Res1L(t flask Pot units Level Result %REC LIml RPD It= Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7F26015-BS3) Prepared & Analyzed: 06/26/2017 14:47 Spike Source %REC RPD Anatvte Result Raq POL Units Level Result %REC Limb RPD Llmj! Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (7F26015-DUP1) Prepared & Analyzed: 06/26/2017 14:47 Source: CA09S83-01 Spike Source %REC RPD Analvte Result Raq POL Units Level Sesul %REC Limi RPD um Notr„l Total Suspended Solids 16 8.3 mg/L 22 35 20 QM-12 Duplicate (7F26015-DUP2) Prepared & Analyzed: 06/26/2017 14:47 Source: CAD9S83-02 Spike Source %REC RPD Anal lde Result FIN PQL V111L9 Level Resul %REC Limits RPD Limit Notes Total Suspended Solids 40 12 mg/L 44 10 20 Classical Chemistry Parameters - Quality Control Bated► 7F210107 - EPA 16646 Blank(7F21007-BLKI) Prepared:06/2112017 11:28 Analyzed:06/2112017 14:17 Spike Source %REC RPD Anal YtC Result EIdA EQL units Level gel %REC Umlts RPD Limit Notes Oil & Grease (HEM•SGT) Non -Polar Material 2.70 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In fut. Page 6 Of= www.encolabs.com QUALM CONTROL DATA Classical Chemistry Parameters - Quality Control Oafdl; 7F11007 - EPA 1664E - Continued LCS (7F21007-BSI) Prepared: 06/21/2017 11:28 Analyzed: 06/21/2017 14:17 Spike Source %REC RPD Anallrte Result Flap POL Units Level Result %REC idLlilRPD J11pit (Votes Oil & Grease (HEM-SGT) Non -Polar Material 82.5 5.00 mg/L 76.0 106 64-132 LCS Dup (7F21007-BSD1) Prepared: 06/21/2017 11:28 Analyzed: 06/21/2017 14:17 Spike Source %REC RPD Anal Yt6 B, Sul Flag ML utlits Level Result %REC Lima RPD twit Ng= Oil & Grease (HEM-SGT) Non -Polar Material 74.8 5.00 mg/L 77.5 96 64-132 10 34 Matrix Spike (7F21007-MS1) Prepared: 06/21/2017 11:28 Analyzed: 06/21/2017 14:17 Source: BA0263"1 Spike Source %REC RPD Analvte Result Flaa POL Units Level Resin %REC Lima RPD L1mit Notes Oil & Grease (HEM-SGT) Non -Polar Material 23.2 5.00 mg/L 22.0 2.70 U 106 64-132 FINAL Thls report relates only to the sample as recehred by the laboratory, and may only be reproduced in Full. I Page 7 Qf 1 O www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical cluantitabon limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. FI NAL Thfs report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 of 10 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD Q =) 10775 GO Ual Pon Or, 4810 ExecuBw Park COUM Sulte III t02-A Woodwltrd! industrial Cl. Ovtando. FL 32624 Jacksonville, FL 32216.6009 Cary, NC 27511 (407) 826-5314 Fn. f407t &W-6945 (904)29fr3W7 Fax (9W) 29U-6210 (9191467-3090 Fak 1914) 467.3.515 ,^,Bent Name I Project Nrmrper I Rsqursted Anatvses 41 Billing Info Rouf erriont NC 27572 2016: P0567E209 Tel Fax (336) 3E4-3699 Roportulg Contact Chri3topher Gustin Sampler(s) Name, AffdwLwn (Print) Bi ung Contact Chr�slopher Gustin sarnplegs) sprat , - �1.•-- j sne Lorabort! Tine x(0, . 7- item of Sample ID (Field Identapeation) -__-_ CO�f!xtion Date -. Collection Time Como f Grab - Maui■ (we codes) TOW #or Containers Q,� 1 �7-9-&44,t _ 5 w #"-3�`l��! Ars`� FA CV Q Ln ti f -R O U3 0 Preservation (See Codes) (Combine <-• Total q of Containers www.encolabs. O Page _ _ _ of ° Requested Turnarou rn Times ro CL Nele : Rusn requests SLOW acceptance by the N"r! _ Standard _ Expedited Due _L_ .ab Workorder . CA069 5 Sample Comments 'oil 2 d Sa a Kit Prepared ay . Dar rate Relinquished Datefrime Recen By DatafTime wm I ReponxV Requirements Relnquished By, Datefrime ace ive By I Dam Time Relinquished By Dalerrime cc' .7 BY i1J j DaterTurte Cooler d's & Temps on Receipt 1 ( ICDnditan U- Jn Recami Acceptable _Unacceptable Matrix: GW-Groundwater SO -Sail DW-drinking Water SE-Sedcment SW -Surface Water WW-Wastewater A -Ale O.Otner jdetail in comments) Preservation: t•lca H-HCI N-HNO3 S-H2SO4 140-r'JaO1i O-Other (detail in comments) Note: AN samples submitted to ENCO Laos ale in accordance with tho corms anlo corldd ens, listed on the reverse of this farm, kmtoss pfior written agreements exist Sample Preservation Verification ENCO Cary ;1 l Work Order: CA06955 Project: Upper Piedmont Stormwater Client: Republic Services of NC (RE014) Project #: [none} Logged In, 19-Jun-17 13:02 Logged By John C King CA06955-01 Cont Type Tres (pH)_,. 'Requirement pH Checked/ In Contro! Date/Time 'pH Adjusted i ' Adjusted Reagent UsedJCorriments „ B 250mLA+H2SO4 <2 Y I N 1 N Y I N I C 25OmLA+H2SO4 <2 Y I N/ A Y I N 1 D 250mLP+H2SO4 <2 671 N I NA Y I& I NA CA06955-02 Cont Type Pres (pH) Requirement pH Checked ! In Control, pH Adjusted DateRme ' Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N! Y I N! 6A C 250mLA+H2SO4 <2 Y I N/ tilA Y I N 1 W ' D 250mLP+H2SO4 <2 - I N I NA Y 1 d I NA CA06955-03 Cont Type Pres (pH) - pH Checked / Daieffime • pH Adjusted . Reagent Used/Comments' Requirement In Control Adjusted B 250mLA+H2SO4 <2 Y 1 N/ i(g` YIN C 250mLA+H2SO4 <2 Y I N! ) Y/ N I N D 250mLP+H2SO4 <2 1 N/ NA Y & 1 NA CA06955-04 Cont' Type Pres (pH) Requirerrient . pH Checked /• _ '. In Contr DatelTime pH Adjusted .Reagent Adjusted. Used/Comments B 250mLA+H2SO4 <2 Y/NIV Y 1 N N C 250mLA+H2SO4 <2 YIN 1 Y I N I I I D 250mLP+H2SO4 <2 1 N 1 NA Y I I NA Reagent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID 5 6 Page 10 of 14 Page 1 of 1 aceAnalytical *" paoslabs cw June 21, 2017 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: CA06955 Pace Project No.: 92344723 Dear Ms. Franz: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on June 19, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please f eel free to contact me. Sincerely, (*c +1, +C Lr Q, Angela Baioni angela.baioni@ pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytrcal —pacelabs.mn Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875r9092 CERTIFICATIONS Project: CA06955 Pace Project No.: 92344723 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification M 16 North Carolina Wastewater Certification * 67 North Carolina Drinking Water Certification M. 37731 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the wntten consent of Pace Analytical Services, LLC. Page 2 of 13 Pace Analytical Services, LLC aceAnalytical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpaoelabs.com (704)$75-9092 SAMPLE ANALYTE COUNT Project: CA06955 Pace Project No.: 92344723 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92344723001 SW#2 SM 9222D BWJ 1 PASI-R 92344723002 SW#1 SM 9222D BWJ 1 PASI-R 92344723003 SW#3 SM 9222D BWJ 1 PASI-R 92344723004 SW#4 SM 9222D BWJ 1 PASi-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pare Analytical Services, LLC. Page 3 of 13 (�IacleAnalX cal' www.pacdabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: CA06955 Pace Project No.: 92344723 Sample: SW#2 Lab ID: 92344723001 Collected: 06119117 09:00 Received: 06/19117 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1111310 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 53.0 CFU1100 mL 1.0 1 06/19/17 14:55 Date: 06/2112017 11:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 4 of 13 acmnaVical wwwpacelabscom ANALYTICAL RESULTS Project: CA06955 Pace Project No.: 92344723 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SW#1 Lab ID: 923"723002 Collected: 06/19/17 09:30 Received: 06/19/17 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual MBIQ 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Coliforrns 6.0 CFU1100 mt. 1.0 1 06/19/17 14:55 Date: 06/2112017 11 158 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical wwwpacefabs.com FIMTAWINA1104:1*111%1&1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 Project: CA06955 Pace Project No.: 92344723 Sample: SW#3 Lab ID: 92344723003 Collected: 06/19/17 10:15 Received: 06119117 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 6.0 CFU1100 mL 1.0 1 Date: 06121 /2017 11:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06119/ 17 14:55 Page 6 of 13 m acmnalytical wwwpacelab CM ANALYTICAL RESULTS Project: CA06955 Pace Project No.: 92344723 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SVM Lab ID: 92344723004 Collected: 06/19/17 10:40 Received: 06/19/17 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MB10 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 900 CFU1100 mL 1.0 1 06/19/17 14:55 Date: 06/21 /2017 11:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 13 laneAnalyfical" www.pacelabs.com QUALITY CONTROL DATA Project: CA06955 Pace Project No.: 92344723 QC Batch: 365783 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAIL Associated Lab Samples: 92344723001, 92344723002, 92344723003, 92344723004 METHOD BLANK: 2027749 Matrix: Water Associated Lab Samples: 92344723001, 92344723002, 92344723003, 92344723004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Colifonns CFU1100 mL ND 1.0 06/19/17 14:55 SAMPLE DUPLICATE: 2027750 92344723001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 53.0 53.0 0 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "units" column except More an alternate unitis presented b the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/21/2017 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 acmnalytrcal W"Pacelabs.cam QUALIFIERS Project: CA06955 Pace Project No.: 92344723 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06121 /2017 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 IiMeAnalyticale www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CA06955 Pace Project No.: 92344723 Lab ID Sample ID QC Batch Method QC Batch 92344723001 SW#2 SM 9222D 365783 92344723002 SW91 SM 9222D 365783 92344723003 SW#3 SM 9222D 365783 92344723004 SW#4 SM 9222D 365783 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Analytical Method Analytical Batch This report shall not be reproduced, except in full, Date: 06121/2017 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 I uocumentName: ni lecnapec Sample Condition Upon Receipt(SC' aceAnalytrca� Document No.: r I F-CAR-DA-003-RevA2 uocument Hevisea: lino Page i of 2 tssuing Authority: Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh® Mechanicsville[] Sample Condition Upon Client Name:Receipt project #: WO# : 92344723 Courier: ❑Fed ❑UPS ❑t1SP5 Client I I,II��I III ❑ Commercial ❑Pace []Other; 923444 13 723 Custody Seat Present? ❑Yes VPo Seals Intact? ❑Yes Date/Inldah Pemn Examining Contents: { Packing Material: ❑Bubble wrap ❑Bubble Bags one ❑Other: Thermometer. ® Ili Gun ID: _ IS-3492 _ Type of Ile: et ❑91ue ❑kone ❑Samples on ice, cooling process has begun Correction Factor. sub.ai Cooler Temp Corrected ('C): � Biological Time Frozen? ❑Yes ❑No 0—/A Temp should be above freezing to VC USDA Regulated Soil ( 5N/A, water samplel Did sample originate in a arantine zone within the United States: CA, NY, or K (check maps)? Did samples originato from a foreign source (inte alionaliy, oyes EWO including Hawaii and Puerto Rico I? ❑Yes o Comments/Dtscre an : Chain of Custody Present? ; 1. Samples Arrived within Hold Time? ❑ } 2. Short Hold Time Amato$ (472 hr.)? U U,, U 3. Rush Turn Around Time Requested? ❑ 4, Sufficient Volume? © ❑ ' S. Correct Containers Used? -Pace Containers Used? i 6. I Containers Intact? ❑ ❑ 7. Samples Field Filtered? 9. Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes Date/Time/ID/Analysis 0 9. Headspace in VOA Vials (>5-6mm)? Yes No N/ 10. Trip Blank Present? Trip Blank Custody Seals Present? Yes ❑ Yes No ❑ No Nf N A II. CLIENT NOTIFICATION/RLSOLUBON Person Contacted: I Comments/Sample Discrepancy: F1Nd aata Required? LJYes LJNo 0ate/Time: G-1k- Project Manager SCURF r Review; ,-- Date: 1 + Project Manager SRF Review: I=)-yn �b Date: L(/— i J_irt Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolma DEHNR Certifrcadon Dffiw (i.u. Out of hold, Incorrect preservative, out of temp, Incorrect containers) Page 11 of 13 N a w N 1+ O items zzz4zzz tiKU-125 mL Plastic Unpreserved (N/A) (CH MU-250 mL Plastic Unpreserved (N/A) 9p2U-S00 mL Plastic Unpreserved (NIA) BP1U-1 liter Plastic Unpreserved (N/A) BP35.250 mL Plastic H2SO4 (pH < 2) ICI-) 8P3N-ZSO mL plastic HNO3 {poi <2) 9z BP32-250 mt Plastic ZN Acetate & NaOH (>9) BP30250 ml. Plastic NaCIM (pH a 12) (CH WGW-Wide-mouthed Glass jar Unpreserved AGW-1 liter A nberunpreserved (N/A) (CI-) AG1H-1 liter Amber HCI (pH < 2) AG31.1-250 mLAmber Unpreserved (N/A) (CJ-) - AGIS-1 titer Amber H2SO4 (pH < 21 A635.250 mL Amber M2504 (pH < 2) AG3A(DG3A)-250MLAmber NH4Q (N/A)(CI•) I I DG9H-40 mL VOA HCi (N/A) VG4T-40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unp (NIA) DG9P-40mL VOA H3PO4 IN/A) VQAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit}VPH/Gas k;t (N/A) SPST-125 mL Sterile Plastic (N/A -lab) SPM250 mL Sterile Plastic IN/A- tab) BP3A-250 mL Plastic(NH2)2SO4I9.3-9.7) Cubltainer VSGLM20mLScintilla tionvials INIA) ON V 0 M SUBCONTRACT ORDER ENCO Cary CA06955 SFISIDING LABORATORY: RECEIVING LABORATORY. ENCO Cary Tri-Test (Raleigh) 102-A Woodwinds Industrial Court 6701 Confcrcncc Drivc Cary, NC 27511 Raleigh, NC 27607 Phone: 919-467.3090 Phone :(919) 834-4984 Fax; 919.467.3515 Fax: Project Manager: Stephanie Franz Project State of Origin: North Carolina Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments SW42 Surface Water 19-Jun-1709:00 Coliform, Fecal9223B 28-Jun-17 15M 19-Jun-17 16,55 Courainrrs .Sapplicd: Stcrile250m1_P+Na'l%io (E) Sub Lab 11) Originating Lab ID Client Matrix Date Sampled Sample Comments Surface Water 19-Jun-1709:30 Coliform, Fecal9223B 28-Jun-17 15:00 19-Jun-17 17:25 Containers Supplied: Stcrile250ml,P+NaTltio (E) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 6'}-{SWJ13 Surface Water 19-Jun-1710:15 Colifomn, F=t 92239 28-Jan-17 15:00 19-Jun-17 19:t0 Containers Supplied: Slerile230mLP+NuThio tEJ Sub Lab ID Originating Lab Ill Client Matrix Dale Sampled Sampls Comments SWit4 Surface Water 19-Iun-1710:40 C olifomt, Fecal 9223B 28-Jun-17 15:00 19-Jun-17 19:35 Containers Supplied: Sicrile250mLP+NaThio (E) rC— "'"Palgefi � of 13 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted January 1, 2018 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: ENCO / Pace Analytical Lab Cert. # 591 / 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2017 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA R F=r 1= 11/F_ ® ®Other: WS-IV, NSW .JAN 19 2018 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION INFORMATION PROCESSING UNIT ❑ No discharge this period?' Outfall No. Date Sample Collected' (ma/dd/yr} 24-hour,r6infall amount, ` Inches3 Chemical Oxygen Demand _ -Fecal Coliform Total Suspended Solids Benchrirarks =__> _ - 120 mg/L 2000 count per 100 mU 100 mg/L or 50 mg/0 - 001 12/07/2017 0.05 No Discharge No Discharge No Discharge 002 12/07/2017 0.05 32 <1.0 21 003 22/07/2017 0.05 12 <1.0 6.7 004 12/07/2017 0.05 21 <1.0 3.9 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mglU' where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 5WU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample 24-hour rainfall Collected' amount, Non -polar O&G/TPH by Total Suspended Solids pH (mo/dd/yr) Inches3 - EPA 1664 (SGT-HEM) Benchmarks =-_> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 12/07/2017 0.05 No Discharge No Discharge No Discharge 002 12/07/2017 0.05 9.26 21 7.8 003 12/07/2017 0.05 15.3 6.7 8.3 004 12/07/2017 0.05 4.55 3.9 8.6 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that =ntor submitting false information, including the possibility of fines and imprisonment for knowing violations." 2 AJI r (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 r NIA F CO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, December 18, 2017 Republic Services of NC (RE014) Attn: Christopher Gustin 9650 Oxford Rd Rougemont, NC 27572 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Upper Piedmont 5tormwater ENCO Workorder(s): CA14660 Dear Christopher Gustin, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, December 7, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This repot relates only to the sample as received by the! laboratory, and may only be reproduced In full. I Page 1 Of O f SAMPLE SUMMARY/ LABORATORY CHRONICLE www.encolabs.com Client ID: Outfall #4 Lab ID: CA14660-01 Sampled: 12/07/17 08:30 Received: 12/07/17 13:37 parameter EPA 1664A Preparation EPA 1664A Hold DatelTimefsl O1/04/18 Prep Date/Time(s] 12/13/17 10:55 Analysis DatelTime(sl 12/15/17 1L20 Field NO PREP 12/07/17 08:44 12/07/17 08:30 12/07/17 0,930 SM 2540D-1997 NO PREP 12/14/17 12/13/17 14:45 12/13/17 14:45 SM 5220D-1997 Same 01/04/18 12/08/17 12:19 12/08/17 16t25 Client ID: Outfall #3 Lab ID: CA14660-02 Sampled: 12/07/17 09:00 Received: 12/07/17 13:37 Parameter EPA 1664A Preparation EPA 1664A Hold Date/Time(s] O1/04/18 Prep Date/Time(s] 12/13/17 10:55 Analysis Date/Time(s] 12/15/17 11:20 Feld NO PREP 12/07/17 09:14 12/07/17 09:00 12/07/17 09:00 SM 2540D-1997 NO PREP 12/14/17 12/13/17 14:45 12/13/17 14:45 SM 52200-1997 Same 01/04/18 12/08/17 12:19 12/08/17 16:25 Client ID: Outfall #2 Lab ID: CA14660-03 Sampled: 12/07/17 09:30 Received: 12/07/17 13:37 Parameter EPA 1664A Preparation EPA 1664A Hold Datelrime(s) 01/04/18 Prep DatelTime(s) 12/13/17 10:55 Analysis Date/Time(s] 12/15/17 11:20 Feld NO PREP 12/07/17 09:44 12/07/17 09:30 12/07/17 09:30 SM 2540D-1997 NO PREP 12/14/17 12/13/17 14:45 12/13/17 14:45 SM 52200-1997 Same 01/04/18 12/08/17 12:19 12/08/17 16:25 FINAL This report relates only to the sample as received by She laboratory, and may arty be reproduced in full. Page 2 Of 1 O www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall #4 Lab ID: CA14660-01 Analyt Resin Flag MA P46 Units Method Notes Chemical Oxygen Demand 21 10 10 mg/L SM 5220D-1997 Oil & Grease (HEM-SGT) Non -Polar Material 4.55 7 2.70 5.00 mg/L EPA 1664A pH 8.6 0.0 0.0 pH Units Field Total Suspended Solids 3.9 2.5 2.5 mg/L SM 254OD-1997 Client ID: Outfall #3 Lab ID: CA14660-02 AnalyU Results flu M21 PS?1 Units Method Notes Chemical Oxygen Demand 12 10 10 mg/L SM 5220D•1997 Oil & Grease (HEM-SGT) Non -Polar Material 15.3 2,70 5,00 mg/L EPA 1664A pH 8.3 0.0 0.0 pH Units Feld Total Suspended Solids 6.7 2.5 2.5 mg/L SM 254OD-1997 Client ID: Outfall #2 Lab ID: CA14660-03 Analld Results RU du E" 5!n!ta Method Notes Chemical Oxygen Demand 32 10 10 mg/L SM 5220D-1997 Oil & Grease (HEM-SGT) Non -Polar Material 9.26 2.70 5.00 mg/L EPA 1664A pH 7,8 0.0 0.0 pH Units Feld Total Suspended Solids 21 5.0 5.0 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced !n full. I Page 3 Of O li�o) CS NIL www.encolabs.com ANALYTICAL RESULTS Description: OutFall #4 Lab Sample ID:CA14660.01 Received: 12/07/17 13:37 Matrix: Surface Water Sampled: 12/07/17 08:30 Work Order: CA14660 Project: Upper Piedmont Stormwater Sampled By:Client (Classical Chemistry Parameters ^-etmCwyctyV#ed"yte[AC 5911 Analyje_[CM Numbed Results Flag Units Of M 1 E" latch Method Analyzed BY Notes Chemical Oxygen DemandA 21 mg/L 1 10 10 7LO8025 SM 5220D-1997 12/08/17 16:25 10C Total Suspended Solid5A 3.9 mg1L 1 2.5 2.5 71-13006 SM 254OD-1997 12/13/17 14:45 OMR Field Parameters Analyte fCAS Numberl Results Flag knits QE Ha M Basch Method Aril gy Notes pH 8.6 pH Units 1 0.0 0.0 7LO8017 Field 12/07/17 08:30 CLI Classical Chemistry Parameters Analyte (CAS Numbed Oil & Grease (HEM-SGT) Non -Polar Resul i Flag Units PE MU EM Batch Meth Analyzed By Notes 4.55 ) mg/L 1 2.70 5.00 71-13008 EPA 1664A 12/15/17 11:20 SMA Description: Qutfail #3 Lab Sample ID:CA14660.02 Received: 12/07/17 13:37 Matrix: Surface Water Sampled: 12/07/17 09:00 Work Order: CA14660 Project: Upper Piedmont Stormwater Sampled By:Client Classical Chemistry Parameters ^-SIC0C-rca%9a "/XeP%C5911 Analyte fCAS Numberl Results Ew Units P-E dU RQL Batch Meth,Alialyzed By Notes Chemical Oxygen Demand' 12 mg/L 1 10 10 7L08025 SM 5220D-1997 12/08/17 16:25 )OC Total Suspended Solids' 6.7 mg/L 1 2.5 2.5 71-13006 SM 254OD-1997 12/13/17 14:45 OMR Field Parameters Analyze FCAS Numberl Results EU-19 units RE BPI M Batch Meth Analyzed BY NaMs pH 8.3 pH Units 1 0.0 0.0 7LO8017 Feld 12/07/17 09:00 CLI Classical Chemistry Parameters Analyte fCAS Numbed Results E149 Units 2E MP!= RM Batch Method Analyzed b No Oil & Grease (HEM-SGT) Non -Polar 15.3 mg/L 1 2.70 5.00 71-13008 EPA 1664A 12/15/17 11:20 SMA Material FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 4 Of 1 O r MMS0100) www.encolabs.com ANALYTICAL RESULTS Description: Outfall #2 Lab Sample ID: CA14660-03 Received: 12/07/17 13:37 Matrix: Surface Water Sampled: 12/07/17 09:30 Work Order: CA14660 Project: Upper Piedmont Stormwater Sampled By:Client Classical Chemistry Parameters 1 Analyte rCAS Numbed Results ElaS UnM 2f Hu RQL Batch Method Analyzed gy Notes Chemical Oxygen Demand^ 32 mg/L 1 10 10 7LO8025 SM 522OD-1997 12/08/17 16:25 JOC Total Suspended Solids^ 21 mg/L 2 5.0 5.0 7L13006 SM 2540D-1997 12/13/17 14:45 OMR 1. Field Parameters Analyze ICAS Numberl Results figs Units PE M" R" Batch Method Analyzed gy N PH 7.8 pH Units 1 0.0 0.0 7LO8017 Feld 12/07/17 09:30 CLI Classical Chemistry Parameters Analyte ICAS Numbed Oil & Grease (HEM-SGT) Non -Polar Material Resin C flag Units PE MU R% Batch Method Analyzed BY X,otes 9.26 mg/L. 1 2.70 5.00 7L13008 EPA 1664A 12/15/17 11:20 SMA FINAL This report relates only to the sample as recelyed by the laboratory, and may only be reproduced in full. Page 5 Of E Q CSNC0 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control 5addt 7L00025 - Same Blank (7L08025-BLK1) Prepared: 12/08/2017 12:19 Analyzed: 12/08/2017 16:25 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limit4 RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7L08025-851) Prepared: IZ/08/2017 12:19 Analyzed; 12/08/2017 16:25 Spike Source %REC RPD Anal Re.81lt Elm P91 units Level Result %REC LimiRPD Limit Notes Chemical Oxygen Demand 510 10 mg/L 500 102 90-110 Matrix Spike (71-08025-1611Si) Prepared: 12/08/2017 12:19 Analyzed: 12/08/2017 16:25 Source: CA08178.02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limit4 RPD Limi! Notes Chemical Oxygen Demand 540 10 mg/L 526 10 U 103 90-110 Matrix Spike Dup (7LOS025-MSDI) Prepared: 12/08/2017 12:19 Analyzed: 12/08/2017 16:25 Source: CA08178-02 Spike Source %REC RPD Analvte Result Flea POL Units Level Result %REC Limits RPD Ljmil Notes Chemical Oxygen Demand 530 10 mg/L 526 10 U 102 90-110 1 10 Batch 7LI3WO - NO PREP Blank (71-33006-Ill Prepared & Analyzed: 12/13/2017 14:45 Spike Source %REC RPD Analvte Result flag PQL Units Level Result %REC Ljmi RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7L13006-BS1) Prepared & Analyzed: 12/13/2017 14;45 Spike Source %REC RPD Analyte Result Ran POL Units Level Result %REC LI11tlti RPD Limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (7L13006-DUPI) Prepared & Analyzed: 12/13/2017 14;45 Source: CA15913-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Lim! L4 RPD Limit Notes Total Suspended Solids 240 50 mg/L 260 9 20 Duplicate (7L33006-DUP2) Prepared & Analyzed; 12/13/2017 11:45 Source: CA16603-01 Spike Source 016REC RPD -ADalyta Resin flag SQL units Level Result %REC Umi( RPD Limit Note Total Suspended Solids 230 50 mg/L 250 8 20 Classical Chemistry Parameters - Quality Control Band! 7L13008 - EPA 1"408 Blank (7L13008-BLK1) Prepared: 12/13/2017 10:55 Analyzed: 12/15/2017 11:20 Spike Source %REC RPD -Anabft Result flag POL Units Level Result %REC Limits RPO limit Notes Oil & Grease (HEM-SGr) Non -Polar Material 2.70 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In fun. I Page 6 of 1 O www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Bateh 7L13008 - EPA 16648 - Continued LCS (71-13008-OS1) Prepared: 12/13/2017 10:55 Analyzed: 12/15/2017 11:20 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Urnil RPD j nfa Notes Oil & Grease (HEM-SGT) Non -Polar Material 82.0 5.00 mg/L 81.6 100 64-132 LCS Dup (71.13008-11SDi) Prepared: 12/13/2017 10:55 Analyzed: 12/15/2017 11:20 Spike Source %REC RPD -Analvw Read flag QOL Units Level Result a/aREC Limit: RPD Wlit Notes Oil & Grease (HEM-SGT) Nan -Polar Material 85.7 5.00 mg/L 82.0 104 64.132 4 34 Matrix Spike (71.13008-MSi) Prepared: 12/13/2017 10:55 Analyzed: 12/15/2017 11:20 Source: BAG4296-01 Spike Source %REC RPD Analvte Result Flao POL Units Level Result 9/aREC Limi RPD Limit Notesz Oil & Grease (HEM-SGY Non -Polar Material 72.6 5.00 mg/L 79.4 2.70 U 92 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fuV. Page 7 Of 1 O @�N www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This repot relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 8 of 1 O �.,.................,...vr.v�..----w.,.....v.,...,....w v.......-.r.-vv.a.vvI r.ww.v www.ce�wioun.avrn Ca 10775 Central Port or, 4810 Exom:ive Park Court, Suite t 1 t 102-A Woodwinds industrial Cl. Orlando, FL 32824 Jacksorrrille. FL 32216.6069 Cory. NC 27511 (407) sn-5314 rax (407) 650-6945 (904(2%-3007 Fax (90a) 296.6210 (919) 467.3090 Fax (9191467-3515 Page Of Client Name - ProjW Number Requested Anatyees Requested Turnarour — Times Note: Rush reauesla sub* a) cn aoeaptanw t)y the taawy co Address ' z Project arrwlDefC c t ', r clwsilZep t ?75f PO to I Mirtg tnto 1 T 26850B c '— 1 Lr �- © CDDue . _ Standard Expedited _I_I Tat r-. 3 -:3 9�, Fax Raportmg Contact Christopher Gustin Samplar(sl Name. Affiliation (Prim( _ Furling Contact Christop;ier Gt_stin _ 4 LL L' U) sampler(s) signature site Location /Twee zone Lab Workorder GA14660 ' Prasarvatlon (See See Codes) (GOmpina as rtarassaryl -. itartn % Sample In (riew ldenbficabon) Coaeotton Date ColieCtOn Time Corp! Grab Matrix (hoe coder:) Total 0 of Contamors C I Sample Comments 14 4 A vv I A Y X �14 Up 'q# 5 X1 X1 X 1 Kit Prepares By 7 ernme Ralirp - Yi DetaTma 0.gtaiaed aY netarr, c,offw vwspacial Reportm Rowkemams I RaliMuffied 61 Datornrme Flomwe0 By Dateltlnq . RelincMshad By DaterCime Received By Date rrme Cooler k' 8 Te on Receipt I �. 1COndVUpon Rompt (�/J! , _: Acceptable Unacceptable Matrix: GW-Uroundwator SD -Sol OW.Um" Water sE•sernmera bW-sursace crater Low-wastawatar A -Air u-Umer 10618e as Comments) rreservetton; n-1Co n-nvn n•nnuU 5•n4aua rau.naun winner joema in cornmenrs! Note: All samples submitted W ENCO labs are in accordance MM 01e terms and CortOitiona listed on the r9aerse of this form, unless prior written agreements exist Sample Preservation Verification, ENCO Cary Can9 Work Order: CA14660 Project: Upper,Piedmont Stormwater Client: Republic Services of NC (RE014) Project #: [none] logged In: 07-Dec-17 13:50 Logged By: John C King Preservation Check Performed By: j�-� • __ DatelTinze: CA 14660-01 Type Pres (pH) , Requirement pH Checked I. In Control , Date/TimeCant pH Adjusted Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N 1 &A Y! N' 1 Al C 250mLA+H2SO4 <2 Y I N I A Y I N I D 250mLP+H2SO4 <2 .• ! N / NA Y- / &/ NA CA14660-02 Cont Type Pres (pH) Requirement pH Checked I In Control pti Adjusted DateMme Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N 1 6IA Y/ N I& C 25OmLA+H2SO4 <2 YINI Y 1 N 14A D 250mLP+H2SO4 <2 i'• 1 N I NA Y I )/ NA CA14660-03 Cant Type Pres (pH) Requirement pH Checked / In Control Dateffime pH Adjusted Adjusted Reagent Used/Comments B 25OmLA+H2SO4 <2 Y/ N I Y/ N! pA C 25OmLA+H2SO4 <2 Y/ N !� Y I N/ D 250mLP+H2SO4 <2 10 1 N / NA YIN 1 NA Rea ent Name_ ID 2 pH Strip ID: Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:IELMNT1Printlwko_PreservationCheck. rpt Page 1 0 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted July 9, 2018 CERTIFICATE OF COVERAGE No. NCG120056 SAMPLE COLLECTION YEAR_2018 FACILITY NAME: Upper Piedmont Regional Landfill SAMPLE PERIOD ® Jan -June ❑ July -Dec COUNTY- Person or [:)Monthly' (month) PERSON COLLECTING SAMPLES: C.Gustin DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: ENCO / Pace Analytical Lab Cert. # S91 / 67 ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: RECEIVED ®Other: WS-IV, NSW JUL 13 2018 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTRAL FILES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTIO"' ❑ No discharge this period?' Outfall No. Date Sample Collected1. (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 001 06/18/18 0.96 44 64.0 54 002 06/18/18 0.96 38 1,000 59 003 06/18/18 0.96 23 2.0 20 004 06/18/18 0.96 61 2,700 1,900 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2412-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Date Sample 24-hour rainfall Outfall No. Collected' amount, Non -polar O&G/TPH by Total Suspended Solids pH (mo/dd/yr) Inches3 EPA 1664 (SGT-HEM) Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 06/18/18 0.96 <2.70 54 7.89 002 06/18/18 0.96 <2.70 59 7.51 003 06/18/18 0.96 4.94J 20 8.44 004 06/18/18 0.96 <2.70 1 10900 7.97 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART lI SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am avpre tha re are nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Permit Date: 11/1/2012-10/31/2017 9 aw/,q (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 •_: r.CCIrP ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3525 Thursday, July 5, 2018 Republic Services of NC (RE014) Attn: Christopher Gustin 9650 Oxford Rd Rougeinont, NC 27572 RE: Laboratory Results for Project Number: Semi -Annual, Project Name/Desc: Lipper Piedmont Stormwater ENCO Workorder(s): CB08894 Dear Christopher Gustin, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, June 18, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NEE_AC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, I Page 1 of i 1 www.encolabs.com PROJECT NARRATIVE Date: 05 July 2018 Client: Republic Services of NC (RE014) Project: Upper Piedmont Stormwater Lab ID: CB08894 Overview This report is an amendment to the original report dated 28 June 2018 for this work order. This report was revised, at the client's request, to investigate the reported detections of TSS in samples #3 Outfall and #4 Outfall. Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments At the client's request, the reported TSS results for #3 Outfall and #4 Outfall were investigated. The sample containers were discovered to be labeled incorrectly. A visual inspection of the two affected samples confirmed the labeling error. All other sample containers associated with this project were checked, and no other errors were discovered. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Stephanie Franz Project Manager FINAL This report relates only to the sample as received by the Laboratory, and may any be reprWucW In full. I Page 2 0f 11 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: #10utfall lab ID: C808894-01 Sampled: 06/18/18 09:00 Received: 06/18/18 12:58 Parameter EPA 1664A EPA 1664A Hold Date/Time(s) 07/16/18 Prep DateMmefs] 06/26/18 11:40 Analvsi;DgtefTlmefs] 06/27/18 16:12 SM 254OD•1997 NO PREP ON25/18 05/19/18 11:49 06/19/18 11:49 SM 5220f)1997 Same 07/16/18 06/25/18 10:15 06/25/18 1112 Client ID: #20utfall LabI0: C808894-02 Sampled: 06/18118 08.45 Received: 06/18/19 12:58 Parameter EPA 1664A EPA 1664A Hold DatelTlme(s] 07/16/18 EM DatelTime(s) 06/26/18 11:40 AnaWs Date/Time(s) 06/27/18 16:12 SM 254OD-1997 NO PREP 06/25/18 06/19/18 11:49 06/19/18 11A9 SM 52200-1997 Same D7/16/18 06/25/18 10:15 06/25/18 13:12 ClientIo: #30utfall Lab ID: CB08894-03 Sampled: 06/18/18 09:15 Received: 06/18/18 12:58 Parameter EPA 1664A QD EPA 1664A Hold DatelTlmefsl 07/16/18 Prep Date/Time(s) 06/26/18 11:40 AnahrAs Date/Tlme(s] 06/27/18 16:12 SM 254OD-1997 NO PREP 06125118 06/19/18 11:49 06/19/18 11:49 SM 5220D-1997 Same 07/16/18 06/25/18 10:15 06/25/18 13:12 Client 110: #4 Outfall Lab ID: CBOS894-04 Sampled: 06/18/18 09:30 Received: 06/18/18 12:58 Para EPA 1664A Preparadon EPA 1664A Hold Date/Time(s] 07/16/18 (s) 06/26/18 11:40 Analysis DateMmefs] 06/27/18 16:12 SM 2540f}1997 NO PREP 06/25/18 06/19/18 11:49 06/19/18 11:49 SM 52200-1997 Same 07/16/18 06/25/18 10:15 06/25/18 13:12 FINAL This repot relates only to the sample as retehred by the laboratory, and may only be reproduced in felt. IPage 3 of 11 1�1 iEo) www.eneolabs.com SAMPLE DETECTION SUMMARY Client ID: #1 Outfall Lab ID: C1308894-01 ADabU Resu is la E" unlu HCth4d N Chemical Oxygen Demand 44 10 10 mg/L SM 522OD-1997 Total Suspended Solids 54 8.3 8.3 mg/L SM 254OD•1997 Client ID: #2 Outfall Lab W. CBCS894-02 Artall C ResulL4 EI+Z9 Hu PQL unlu M Not Chemical Oxygen Demand 38 10 10 mg/L SM 5220D-1997 Total Suspended Solids 59 5.2 5.2 mg/L SM 2540D-1997 Client ID: #3 Outfall Lab ID: CB08894-03 Ana hde Resell Ela MDl E" uhm Mediod M9LC5 Chemical Oxygen Demand 23 10 10 mg/L SM 522OD•1997 Oil $ Grease (HEM-SGT) Non -Polar Material 4.94 1 2.70 5.00 mg/L EPA 1664A Total 5tspended Solids 20 3.8 3.8 mg/L SM 2540D-1997 Client ID: #4 Outfall Lab ID: CBOB894-04 6»aUd>: Results EIn9 mm E2L unfta Motw N Chemical Oxygen Demand 61 10 10 mg/L SM 5220D-1997 Total Suspended Solids 1900 96 96 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 1 CS Nk" 0 0) www.encolabs.com ANALYTICAL RESULTS Description: #1Outfall Lab SampleID:CB08894.01 Received: 06/18/1812:58 Matrix: Surface Water Sampled:06/18/18 09:00 Work Order: CB08894 Project: Upper Piedmont Stormwater Sampled By:CLIENT (Classical Chemistry Parameters ^ - ENW Cary mtfied arralyte[NC 591/ Anahrte FCAS_Number] Resulffi flag llpits DE MIL EQL maim Meths4 Artabi ed ft iY4l� Chemical Oxygen Demand ^ 44 mg/L 1 10 10 SF25011 SM 5220D-1997 06/25/18 13:12 30C Total Suspended Solids^ 54 mg/L 3.33 8.3 8.3 BF19019 SM 2WD-1997 06/19/18 11:49 LBG Classical Chemistry Parameters Analvte (CAS Numberl amdu fhu Units IE MIL E!QL Adch MethQd Anahmo Ew flpSei Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5.00 BF26007 EPA 1664A 06/27/18 16:12 SMA Description. #2 Outfall Lab Sample ID:CB08894-02 Received: 06/18/18 12:58 Matrix: Surface Water Sampled,06118/18 08:45 Work Order: CB08894 Project: Upper Piedmont Stormwater Sampled By: CLIENT Classical Chemistry Parameters ^ - ENCO Cary certified 81781yteW 5911 Anahrte (CAS Numberl $esultg Elag Units DE MU EQL A= 13ethod Anahaed Iffyt IYS:IeS Chemical Oxygen Demand^ 38 mg/L 1 10 10 BF25011 SM 52201)-1997 06/25/18 13:12 ]OC Total Suspended Solkds^ 59 mg/L 2.07 5.2 5.2 8F19019 SM 254OD-1997 06/19/18 11:49 LBG Classical Chemistry Parameters Results Elm Units QE MIL EQL Adtdl Method Analraed ft 1!l9ie5 Oil & Grease (HEM-SG-1) Non -Polar Material 2.70 ll mg/L 1 2.70 5.00 8F26007 EPA 1664A 06/27/18 16:12 SMA Description: #3 Outfall lab Sample ID:CB08894-03 Received: 05/18/18 12:58 Matrix: Surface Water Sampled:06/18/18 09:15 Work Order: CB08894 Project: Upper Piedmont Stormwater Sampled By:CLIENT Chemistry Parameters - ENCO Cary mafied --fyte [MC 591] Anahrte r[AS Number! ReSults Has UE111 DE MIL EQL aitch Meth Qd And By h9las Chemical Oxygen Demand^ 23 mg/L 1 10 10 SF25011 SM 5220D-1997 06/25/18 13:12 ]OC Total Suspended Solids^ 20 mg/L 1.52 3.8 3.8 BF19019 SM 25401)-1997 06/19/18 11:49 MG Classical Chemistry Parameters Anahrte rCAS Numberl Resullg Elite Units IE MIL E" Aillcb M ApahGmd BY Notes Oil & Grease (HEM-SGT) Non -Polar 4.94 1 mg/L 1 2.70 5,00 81`26007 EPA 1664A W27/18 16:12 SMA Material FINAL Tars report relates only to the sample as receroed by tt* laboratory, and may only be reproduced in full. I Page 5 Of j ENCis www.encolabs.com ANALYTICAL RESULTS Description: #4 Outfall Lab Sample ID: CB08894-04 Received: 06/18/18 12:58 Matrix: Surface Water Sampled:06/18/18 09:30 Work Order: CB08894 Project: Upper Piedmont Stormwater Sampled By: CLIENT (Classical Chemistry Parameters ^ - EACO Qwy ca afi d &WW [NC 5911 Anahyte rCAS Numberl Resul E&g Units 2E HU EQL Aillub I9CIh12d Anted Ily N Chemical Oxygen Demand 61 mg/L 1 10 to SF25011 SM 522OD-1997 06/25/18 13:12 ]OC Total Suspended SolidsA 1900 mg/L 38.5 96 96 8F19019 SM 2540o-1997 06/19/18 11:49 LK Classical Chemistry Parameters Anatole rCAS Humberl Resllt5 EIN Units 12E MIX E!QL @itch - Method Anabued fit[ Kates Oil & Grease (HEM-SGT) Non -Polar Material 2.70 ll mg/L 1 2,70 5.00 8F26007 EPA 1664A 06/27/18 16:12 SMA FINAL THs report relates only to the sample as received by the Laboratory, and may Only be reproduced In fun. Page 6 of 11 (. Turn www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch Bf16007 - EPA 1664E - Continued LCS (BF26007-B51) Prepared: 06/26/2018 11:40 Analyzed: 06/26/2018 17:04 Spike Source %REC RPD _Ana[M Result Flag POL Units Level Stet %REC Limi Rpb L,jmft Notes Oil & Grease (HEM-SGT) Non -polar Material 88.0 5.DD mg/L 80.0 110 64-132 LCS Dup (SF26007-BSD3) I Prepared: 06/26/2018 11:40 Analyzed: 06/26/2018 17:04 Spike Source %REC RPD Anahft Result Flag POL Units Level ResuB %REC Untl RPD UlEt Notes Oil & Grease (HEM-SGT) Non -Polar Material 85.6 5.00 mg/L 80.0 107 64-132 3 34 Matrix Spike (BF26007-MS3) Prepared: 06/26/2018 11:40 Analyzed: 06/26/2018 17:04 Source: BB02822-01 Spike Source %REC RPD Analvte Result flag POL Units Level Result %REC LIMJO RPD LIMA Notes 00 & Grease (HEM-SGT) Non -Polar Material 78.4 5.00 mg1L 80.0 2.70 U 98 64-132 FINAL This report relates only to the sample as received by the Laboratory, and may only be reproduced in tuii. Page 8 Of 11 0Leo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL TNs report relates a„ y to the same as received by the laboratory, and may only be reproduced tn futi, Page 9 of 11 10775 Central Pori Dr. 4810 --F-xocutm-- Park Court, Suite 11 i 1 02-A Wooervlas trtdustrWl CL 14D71826-5314 Fax (a07J 850-69d5 190a1296-9007 Fa. {90aJ 296-62i0 (919) 467.3090 Fax (919)a67.3515 Page of Client Name Republic Services of NC (RE014) Project Number Semi -Annual gequestad Anahaea Requested TurnaroD Times 0 1401e : Rush reouests subj acceptance by thetaclle C7 to d Standard _Expedited Due 0 N ,n 0 LL Q to T C ° p vJ ~ Address 9650 Oxford Rd Prgec: Name0aw Upper Piedmont Stormwater CrtylST/Lip Rougemont; NC 27572 Po s / Billing Into 2017: 6268508 Tel (336) 364-3699 Fax Reporting Contact Christopher Gustin Samoler(sl Name. Attiiianon IPnntl Min Contact L hristopher Gustln Samolerlsi Signature See LpCahon / Time Zone Lab Workorder CB08894 PresorvatlDn (Sae COOLS) (Combine as neCassary) Item Y Sampte ID (Feld Identification) Collection Date Collection Time comp 1 Grab Matrix {see codes) Total N of ContainersEI]j Sample Comments 6-/ilk "?.66A►, Ca' SW 5 x x x 8 9 -�9 B; `MA. �- SW 5 X � X � X� X � 9.• _ Q SW 5 X X X X b /� �� SW 5 X x x X _/�. �• LI — Total # of Containers Sample Kit Prepared By Date/rhme CommenWSpecial Reporting Raquirements Relinquished By Rehrlquishod B - Datarrime Received [)at Datemme Cal ( Date. ;me Relintquishad By DatoMme Ramiaed By DateMme Cooler is S Tamps on Receipt jCdo67A n Receipt1 ceptable Unacceptabie Matnx : GIN-Grounomicir SO -Soli DW-Dnnkmg Water SE-Seoiment SW-Surtace Water WW Wastewater A-Ah 0-0ther (detail in comments) Preservation: Hco H-NCI N-HNO3 S-H2SO4 NO-NaoH O-Other (delae in Commenisl Note: All samples submitted to ENCO Labs are in accordance with the torms and conditions listed on the reverse of this farm, unless prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CB08694 Project; Client: Republic Services of NC (RE014) Project #: Logged In: 18-Jun-18 13:21 Logged By: Preservation Check Performed By: CB08894-01 } eP� Upper Piedmont Stormwater Semi -Annual John C King DatetTime:. ��- ( 4&ID Cont Type Pres (pH) Requirement . pH Checked / , jn Control DateMme,.. ' pH Adjusted ," '` ' Aojusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N! IK6 Y I N! C 25OmLA+H2SO4 <2 Y 1 N/ Y I N I D 250mLP+H2SO4 <2 N I NA I Y I b/ NA C B08894-02 Cont Type Pres (pH) Requirement . pH Checked/ In Control pH Adjusted Datelrme Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N! Y I N I C 250mLA+H2SO4 <2 Y I N I Y I N/ rW D 250mLP+H2SO4 <2 / N 1 NA Y ! / NA C B 08894-03 Cont Type Pres (pH) Requirement' phi Checked 1 A In Control DateMme, pH Adjusted. Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N I Y! N 1 C 250mLA+H2SO4 <2 Y I N I Y! N I N61 D 25omLP+H2SO4 <2 I N I NA Y I 1 NA If CB08894-04 Cont Type'. Pres (pH) Requirement pH Checked 1 In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N 1 0 Y I N! C 250mLA+H2SO4 <2 Y 1 N 1 A Y 1 N I A D 250mLP+H2SO4 <2 I N 1 NA Y 1�9 NA Reagent Name ID 1 2 pH Strip ID: U 26 Rea ent Name ID 3 4 Rea ent Name ID 5 6 CaELMNTIPrintlwko_PreservationCheck. rpt Page 11 of 11 age 1 c laceAnalytical w»w.pacalab&com June 20, 2018 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: C808894 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Ms. Franz: Enclosed are the analytical results for sample(s) received by the laboratory on June 18, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please f eel free to contact me. Sincerely, Angela Baioni angela.baioni@ pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Tull, without the written consent of Pace Analytical Services, LLC. Page 1 o(13 (�5a'neAnalyfica( www.pacelab&com Project: CB08894 Pace Project No.: 92388788 Raleigh Certification lDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 13 lacieAnapical" xmwpacelabs cam SAMPLE ANALYTE COUNT Project: CBOBB94 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704y875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92388788001 #1 Outfall SM 9222D DJB 1 PASI-R 92388788002 #2 Outfall SM 9222D DJB 1 PASI-R 92388788003 #3 Outfall SM 9222D DJB 1 PASI-R 92388788004 04 Outfall SM 9222D DJB 1 PASI-R REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical w" pacefabacom ANALYTICAL RESULTS Project: CB08894 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: #1 Oulfall Lab ID: 92388788001 Collected: 06/18/18 09:00 Received: 06118/18 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 64.0 CFU1100 mL 1.0 1 06/18/18 15:50 Date: 06120/2018 06:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalyttcalm www.pacelabs.com ANALYTICAL RESULTS Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Project: CB08894 Pace Project No.: 92388788 Sample: #2 Outfall Lab ID: 92388788002 Collected: 06118/18 08:45 Received: 06/18/18 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 92220 Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 1000 CFU1100 mL 1.0 1 Date: 06/20/2018 06:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06118/18 15:50 Page 5 of 13 laneAnayical" wwwpacelab&Mn ANALYTICAL RESULTS Project: CB08894 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kincey Ave. Su'de 500 Huntersville, NC 28078 (704)875-9092 Sample: #3 Outfall Lab ID: 92388788003 Collected: 06118118 09:15 Received: 06118/18 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Coliforms 2.0 CFU1100 mL 1.0 1 06/18/18 15:50 u1 Date: 06/20/2018 06:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 13 leAnalyfcal wwwpacafats.mm ANALYTICAL RESULTS Project: C808894 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 10D Hunlersville, NC 28078 (704)875-9092 Sample: #4 Outfall Lab ID: 92388788004 Collected: 06/18/18 09:30 Received: 06/18/18 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 2700 CFU1100 mL 1.0 1 06/18/18 15:50 L��-3f�irI:lY�rIF�rL[ I+b��l,u REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuH, without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical www.p aa8Scarn QUALITY CONTROL DATA Project: CB08894 Pace Project No.: 92388788 QC Batch: 415678 Analysis Method: SM. 9222D QC Batch Method: SM 92220 Analysis Description: 9222D MBIO Fecal Coliform - RAL Associated Lab Samples: 9238878B001, 92388788002, 92388788003, 92388788004 METHOD BLANK: 2304985 Matrix: Water Associated Lab Samples: 923887B8001, 92388768002, 92388788003, 92388788004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 06/18/18 15:50 SAMPLE DUPLICATE: 2304986 92388788001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFUl100 mL 64.0 80.0 22 u1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Results presented on this page are In the units Indicated by the "units" column except Mere an alternate unitis presented to the right of the reauh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/20/2018 06:22 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 laneAnalyfical" ~n pacelab&cw Pace Analytical Servlces, LLC 9800 Kincey Ave, Suite 100 Huntersville. NC 28078 (704)875-9092 QUALIFIERS Project: CB08894 Pace Project No.: 92388788 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS u1 Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/20/2018 06:22 PM without the written consent of Pace Analytical Services, L.L.C. Page 9 of 13 aceAnalytical" www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CB08894 Pace Project No.: 92388788 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875r9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92388788001 #1 Outtall SM 9222D 415678 92388788002 #2 Outfall SM 92220 415678 92388788003 #3 Outfall SM 9222D 415678 92388788004 #4 Outfall SM 9222D 415678 Date: 06/20/2018 06:22 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Analytical Batch Page 10 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition upon ReceiptlSCUR) Page 1 of 2 Document No.: Issuing Authority: - CcAnaiytre�r F-CAR-CS-033-Rev,06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville [] Eden[—] Greenwood ❑ Huntersville ❑ Raleigh Mechanicsville❑ '�Sinnple condition Client Name: WO 923 V V d V V Upon Receipt' Project #: ��'G° II�IID I I1�III�� III �I1 Courier: ❑fed Ex []UPS ❑LISPS Client ❑ Commercial ❑Pace ❑Other.___-_ 92388788 Custody Seal Present? ❑Yes No Seals Intact? ❑Yes AN0 Packing Material: 09uhble Wrap ❑Bubble Bags 1�one ❑ Other Thermom er. t✓ Type of ice: wet ❑Rlue R Gun ID; CoolerTemp('C), �?,r�� Correction Factor: Add ubtrac ('C) Cooler Temp Corrected ('C): USDA Regulated Soll (R�N/A, water sample) Did samples arriiglnjw in a quarantine zone within the United States: CA, NY, or SC (check maps)? 11Yes 1w1Ro� Date/Initials Person Examining Contents: Biological Tissu Frozen? ❑None ❑Yes ❑NoN/A Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a Foreign source {inteerrnationally, indudine Hawaii and Puerto Rico)? F lYes P No Comments/Discrepancy: Chain of Custody Present? Yes NO ❑N/A 1. Samples Arrived wlthin Hold Time? es ❑No ❑N/A 2. Short Hold Time Analysis (t72 hr.)? Yes [:IN.. ❑N/A 3. Rush Turn Around Time Requested? Elyes RC N/A 4, Sufficient Volume? EIC, ❑No -/A 5. Correct Containers Used? -Pace Containers Used? Y Yes ❑No []No ❑NJA N/A 6. Containers Intact? 05C❑No N/A 7. Dissolved analysis: Samples Field Filtered? Yrs ❑No N/A B. i Sample Labels Match COO -Includes DateMme/lb/Analysis Matrix: Eves' ❑No ❑NJA 9. Headspace in VOA Vials (>S-6mm17 [yes QNn N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑Nn ❑Na N/A f.N/A it. 0 COMMFNTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Tlme: Project Manager SCURF Review: Project Manager 5RF Review: i /� ? Field Data Required? ❑Yes []No Date: 1 T Date: Page 11 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Receipl(SCUR) Page 1 of 2 Document No.: Issuing Authority: 1. r BCEAf&9Vka1- F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office "Check mark top half of box if pH and/or dechlorination is Project 9 verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle W0 ' 92388 [ 88 PM: AMB Due Date: 06/27/18 CLIENT: 92-ENCO U 2 u 3 Zi x 2' Y II d 13 Z N n, X ptl .N-e C 0 z C y N 4 Z N tYl Q Y yVys f1 p V n y A L V Z N M L a p e4i a 2 n y w v n `a ? y Vnp O ? .a _ ¢ ? M z i rN v .'S4 tr 7 z 2 N Z p C x Z Q ? O n u 7 .=, a l 2 j o m c ro a 2 e� 1 i N p n p w a A B ¢ a E V E d 0 4 O z < Q a < < Y 4 G " d _ _u '� _m a E a C_ < 'E a S c G eV y0 6 ,n I I Si E w E E E E v `u u v01 `y _ C O �7 E C E •J E 0 s A •S if1 f Q C O g o 0 ♦ f�J E a 4m a N a a a S7 W t7 m l7 t7 ell CJ 1a�1 l7 IT u C7 Q1 a O �> N I T a T l7 m so gom m m m d d d ¢ d d ? > a vt 9i m O 1 1 i 3 I 4 f � 6 NN N— Ss I 7 ) B 9 i YO 11 Y2 pH Adjustment Log for Preserved Samples Sample ID Type of Preservatwe PH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note: Whenever there is a discrepancy arrectln8 North Carolina com Pliance samples, a copy of MIS form will be sent to the North Carolina DEHNR CCrtiIIW tion Otrice (i e. Out of hold, inrArrect presCNative, out or temp, incorrect containers. Page 12 of 13 SUBCONTRACT ORDER ENCO Cary CH08894 SENDING LABORATQRY: RECEIVING LABQRATORY- ENCO Cary Tri-Test (Raleigh) 102-A Woodwinds Industrial Court 6701 Conference Drive Cary, NC 27511 Raleigh, NC 27607 Phone: 919.467.3090 Phone :(919) 8344994 Fax: 919.467.3515 Fax: Project Manager: Stephanie Franz Project State of Origin: North Carolina Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments I gi3?jCjt ' -U)f l Outfall Surface Water 18-Jun-1809:00 Coliform, Fecal 9223B 27-Jun-18 15:00 18-Jun-18 16:55 Containers Supplied: Stcri le250mLP+N aTh i o (E) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments �Z��QjUZ Outfall Surface Water 18-Jun-1808:45 Coliform, Fecal 9223E 27-Jun-18 15:00 18-tun-18 16:40 Containers Supplied: Steri1c250m1.P+NaThio (E) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments _JXj:, 3 Outfall Surface Water 18-Jun-l8 09:15 Culifurm, Fecal 9223B 27-Jun-18 15:00 18-tun-18 IT.IO Containers Supplied: Sterilc250m1-P+%Thio (E) q 2-1%51-;S,�- VA #4 Outfall Surface Water 18-Jun-18 09:30 Coliform, Fecal 9223B 27-1un-18 15:00 18-Jun-18 17:25 Containers Supplied, Sterile25GmLP+NaThio (F,) Page I of Page 13 of 13 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted November 30, 2016 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: ENCO / Pace Analytical Lab Cert. # 591 / 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec REclzm /c�r ❑Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA DEC 05 ,1 ❑Zero -flow ❑Water Supply ❑SA CENTRAL WS-IV, NSW RAL FILES DW,R SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches; Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 001 11/14/16 0.55 24 1000 6.8 002 11/14/16 0.55 26 10.0 11 003 11/14/16 0.55 No Discharge No Discharge No Discharge 004 11/14/16 0.55 22 460 34 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 .Wte: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfafl No. Date Sample 24-hour rainfall Collected" amount, Non -polar O&G/TPH by (mo/dd/yr) Inche53 EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 11/14/16 0.55 <2.70 6.8 7.41 002 11/14/16 0.55 <2.70 11 8.02 003 11/14/16 0.55 No Discharge No Discharge No Discharge 004 11/14/16 0.55 <2.70 34 8.29 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lob results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) ?d Al" ZIV (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted June 28, 2016 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: ENCO / Pace Analytical Lab Cert. # 591 / 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑water Supply ❑SA RECEIVED VED ❑Other: WS-IV, NSW JUL 9 12016 CENTRAL 1: PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTIO No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 001 06/16/16 0.14 No Discharge No Discharge No Discharge 002 06/16/16 0.14 35 3.0 11 003 06/16/16 0.14 27 6.0 24 004 06/16/16 0.14 31 96.0 16 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period: Date Sample 24-hour rainfall Outfall No. Collected' amount, Non -polar O&G/TPH by (mo/dd/yr) Inches3 EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 06/16/16 0.14 No Discharge No Discharge No Discharge 002 06/16/16 0.14 <2.70 11 7.6 003 06/16/16 0.14 <2.70 24 7.82 004 06/16/16 0.14 <2.70 16 7.78 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER -AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DM6 including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge"" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." nature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report • for North Carolina Division of Water Quality General Permit No. NCG120000l Date submitted April 11 2016 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results 00PV SAMPLE COLLECTION YEAR �2016 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' March (month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA R7.eel ,r � ®Other: WS-IV. NSW APR f 5 2016 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTP,AL pjLSS DWR SECTION ❑ No discharge this period?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform '- Total Suspended Solids Benchmarks - 120 mg/L 1000'count per 100 mL 100 mg/L or 50 mg/L 004 03/25/16 0.01 44.0 10.0 10.5 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format,"<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 5WU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B:- Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample f Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L4 6.0 - 9.0 SU 004 03/25/2016 0.01 <5.0 10.5 6.7 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coov of this DMR. includina all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monkorinq period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / / 141?- 2-,:51C Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Storm -water Discharge Monitorine Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted Februm 25, 2016 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec RECEIVED or ® Monthiyf February (month) MAR 3 �QiDGISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout❑PNA ❑Zero -flow ❑Water Supply ❑SA CENTRAL FILES ®Other: WS-IV, NSW DWR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 El No discharge this period?z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 004 02/25/2016 0.01 <25.0 273 <7.7 2 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/l/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Salads pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 004 02/25/2016 0.01 <5.0 <7.7 7.6 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one jcopV of this DMR, including all "No Discharge" reports, within 30 do vs of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permit Date:11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 aceAnalyfrcal www.pacelabs.cam I March 07, 2016 Christopher Gustin Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 RE: Project: Semi -Annual Stormwater Pace Project No.: 92287841 Pace Analytical Services, Inc. 6701 Conference Drive Dear Christopher Gustin: Enclosed are the analytical results for sample(s) received by the laboratory on February 25, 2016. The results relate only to the samples included in this report. Raleigh, NC 27607 (919)834-4984 Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm.harrison@pacelabs.com Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shatt not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. IaneAnalXical" 67111 Conference Drive Raleigh, NC 27607 www.pacelabs.corn (919)834-4984 CERTIFICATIONS Project: Semi -Annual Stormwater Pace Project No.: 92287841 Raleigh Certification IDS 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Certification IDS 9800 Kinoey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification A 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification M 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #. E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #; 37738 North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification #: 37731 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification M 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification M 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 aceAnalyttical www.pacelabs,com I SAMPLE ANALYTE COUNT Project: Semi -Annual Stormwater Pace Project No.: 92287841 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92287841001 Outfall #4 SM 2540D CHM 1 PASI-E EPA 1664E JMS 1 PASI-C SM 9222D RC 1 PASI-R SM 5220D 1NRC 1 PASI-A REPORT OF LABORATORY ANALYSES This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAnalytical r �+wwpacalabs.aom ANALYTICAL RESULTS Project: Semi -Annual Stormwater Pace Project No.: 92287841 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Outfall #4 Lab ID: 92287841001 Collected: 02/25/16 09:50 Received: 02/25/16 11:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 4ual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 7.7 1 02/26/16 09:55 1664 SGT-HEM, TPH _ Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg1L 5.0 1 03/07/16 05:29 MBIO 9222D Fecal Colfform RAL Analytical Method: SM 9222D Fecal Colifarms 273 CFU1100 mL 1.0 1 02/25/16 15:30 5220D COD Analytical Method: SM 52200 Chemical Oxygen Demand NO mg1L 25.0 1 03/01/16 14:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written consent of PaceAnalytical Services, Inc.. Page 4 of 12 aceAnalytical wwwpawlabsaom Project: Semi -Annual Slormwater Pace Protect No.: 92287841 QC Batch: EDENl21918 QC Batch Method: SM 2540D Associated Lab Samples: 92287841001 METHOD BLANK: 1673997 Associated Lab Samples: 92287841001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1673998 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1673999 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1674000 Parameter Units Total Suspended Solids mg1L Pace Ana"cat Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 02/26/16 09:50 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 246 98 90-110 92287702001 Dup Result Result RPD Qualifiers 1240 1350 9 06 92287854002 Dup Result Result RPD Qualifiers 52.7 50.0 5 Results preaented on this page are in the units Indicated by We *Units" column except where an attemate unit Is presented to the rigid of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written consent of PaceAnalytical Services, Inc.. Page 5 of 12 acmnalytical W^..pacelabs.= Project: Semi -Annual Stormwater Pace Project No.: 92287841 QC Batch: GCSV/24301 QC Batch Method: EPA 1664E Associated Lab Samples: 92287841001 METHOD BLANK: 1679937 Associated Lab Samples: 92287841001 Parameter Total Petroleum Hydrocarbons QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg/L ND 5.0 03/07/16 05:18 LABORATORY CONTROL SAMPLE: 1679938 Parameter Units Total Petroleum Hydrocarbons mg/L MATRIX SPIKE SAMPLE: 1679939 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 15.3 76 64-132 92288763001 Spike MS MS °/. Rec Result Conc. Result % Rec Limits Qualifiers ND 20 17,0 85 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical www.pacelats.cam Project: Semi -Annual Stormwater Pace Project No.: 92287841 QC Batch: R61015988 QC Batch Method: SM 9222D Associated Lab Samples: 92287841001 METHOD BLANK: 1673863 Associated Lab Samples: 92287841001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1673864 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 92220 Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Result ND 92287841001 Units Result CFU1100 mL 273 Reporting Limit Analyzed Qualifiers 1.0 02/25/16 15:30 Dup Result RPD Qualifiers 727 91 06 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are In the units indicated by the'Units' column except where an alternate unit is presented to the right of &is result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 acmnalytical wwwpacelabs.com Project: Semi -Annual Stormwater Pace Project No.: 92287841 QC Batch: WETA126606 QC Batch Method: SM 5220D Associated Lab Samples: 92287841001 METHOD BLANK: 1675402 Associated Lab Samples: 92287841001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1675403 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 03/0111614:30 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 768 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1675404 1675405 MS MSD 92287702001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 8660 30000 30000 38400 38400 99 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1675406 1675407 MS MSD 92288009001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 10700 30000 30000 41200 41200 102 102 90-110 0 Results presented on thla page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 Pace Analytical Services, Inc. 6701 Conference Drive aceAnalyfical Raleigh, NC 27607 WNW.Pacefabs.com (919)834.4984 QUALIFIERS Project: Semi -Annual Stormwater Pace Project No.: 92287841 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MID L-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitnle by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E PaceAnalytical Services - Eden PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/07/2016 02:28 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 ace Analytical wwwpacefabs.narn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: Semi -Annual Stormwater 92287841 Analytical Lab ID Sample ID QC Batch Method QC Batch Anatytical Method Batch 92287841001 Outfall #4 SM 2540D EDEN121918 92287841001 Outfall #4 EPA 1664B GCSV124301 92287941001 Outfall #4 SM 9222D R131015988 92287841001 Outfall #4 SM 52201) WETA126606 REPORT OF LABORATORY ANALYSIS This report shaSi not be reproduced, except in full, Date: 03/07/2016 02:28 PM without the written Consent of Pace Analytical Services, Inc.. Page 10 of 12 UOCutnent Name,. nc­acu. w­­ aceAnaoical' Sample CondlUon U on Receipt(SCUR) Page 1 of 2 Document No., Issuing Authority: F-RAL-CS-001-rev.03 Pace Huntersville Quality Office Client Name: , Project ft- mil k�VQUA� W0#:92287841 Courian ❑Fed Ex ❑UPS ❑USPS �Ciient IIIII� I I IjI I �II I I II ❑Commercial ❑Pace []Other: 92287841 4 I Custody Seal on Cooler/Box Present? ❑Yes (INO Seals Intact? Dyes [;0o Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑Other; Thermometer IR Gun SN:122065387 Used: 5IR Gun SN: 122065371 Type of ice: [JWet ❑Bsue []None❑Samples an Ice, cooling process has begun Cooler Temp Corrected ('C):. Biological Tissue Frozen? ❑Yes []NO O'N/A Temp should he above fr avng to 6'C Correction Factor: 0.01C Date and Initials of Person Examining Contents: Z ��Q USDA Regulated Sell (( N/A, water sample) Old samples or Inate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a forOgn source (intemationatly, (]Yes No Including Hawaii and Pueno Rico)? []Yesr4o If Yes to either question, fill out a Regulated Soil Checklist and include with SCURICOC paperwork. COMMENTS: Chain of Custody Present? Yes Duo N/A 1. Chain of Custody Filled Out? Yes No ❑NIA 2. Chain ofCustod Rclin uished7 Yes ONO N/A 3. Sampler Name and Or Signature on COC? b4ei No ONJA 4. Samples Arrived within Hold Time? Yes EINo N A 5, Short Hold Time Antr sls 02 hr Z Yes No N A 6. Rush Turn Around Time Requested? Yes Na N A 7. 5ufflcient Volume? Ofes Duo N A 8. Correct Containers Used? -Pace Containers Used? [es lyyes ❑No No ON/A DNJA 9. Contalners intact? Yu C3No N A 10. Filtered Volume Received for Dissolved Tests? QYes Or4c, A 11, Note if sediment is visible In the dissolved container Sample Labels Match COC7 -Includes Date/Time/ID/Analysis Matrix: es ❑No ❑N/A 12. All containers needing acid/base preservation have been checked7 All containers needing preservation are found to be in compliance with EPA recommendatlon? (HNOr. H:SOu HU<2; Na0H >9 Sulfide, Na011>12 Cyanide) Exoeptions: VOA, CoFform, TOC, Oil and Grease, DRO/8015(water DOC,LLH Yes yes Yes ONO ❑No ❑No []N/A QNJA N A 13 Samples checked for dechlorization es Q No N/A 14. Heads ace in VOA Vlals >5.6mm)? tlYes No A 15. Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot q ifpurchased) []Yes []Yes ❑No [.]No /A (�N/A 16. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Resolution; Field Data Required? ❑Yes Do ProjectM.-nagerSCtIRFRevlew:' i,.'i�'� �.1\ Uatdi Note: whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. out of hold, incorrect preservative, out of temp. Incorrect containers). Page 11 of 12 .A PaceAnalytical' CHAIN -OF -CUSTODY 1 Analytical Request Document Tne Charm! -Custody Is a LEGAL DOCUMEN r. All rcievani licks roust be comptnted xwratnly. Page. SmIon A Section 9 Section C Re4-imd Cheat Info.maUow Repufred Promw Ir&mxarr: In�oitb lftkrrrnatbrt. C Report ro: /� e Ammon: 10375774 e %' I e fi (Y 4 Address' TQ f Copy To Company Narnc: REGULATORY AGENCY f� I�4 KG 2 7t72 �r�� i NPDES r GROUND WATER f— DRINKING WATER ( LIST RCRA i OTHER Small T Purchave Qnxv No: Pw 0.,Au PIT !TFI. 3 -3 .ram r Mom: ,rt a w Yace thmte r, s4"u0" StATE. Regv,tsd 0— DW./TAT: Ida NumGer. uestt:d Analysts Flltemd (YIN) S.[tson b Matrix Coop u z Rw.�.wnf�Ntnx.m,rc� I.t&IR . f= y ° COLLECTED Presarvalives i Dnnkirg water OW 6 z water w f wastewalor WLV ., @ t�r,7O5rr! tawv>t:e PTWW P C START krn'r�Ln W J d Z $ei!$plid SL '-` C M SAMPLE ID Op, w h LOLL lA-7.041. ) Aq AR Ips Samoa AtliST OE UNIQUE T&sw TS ether QT U X W W Z g p T, 9 i1 O� O O m c ti m Y r r]/1T[ TIME OATF TTtfE _ z z 20 Ix Paw Project NoJ Lab LD. ¢ • .r .:se x x s z S 8 6 9 ,0 11 ,2 ADD1T1ONAL COMMENTS RHlNQU SY r AFF!LLLTION DATE TIME By AF4 bA TWE SAMPLECONDr17099 ORIGINAL SAAIPLERKANEAND SIGNATURE s { PRINT ?+ante Of aAMPLER: v v " U rn E" RATE Signed SIGNATURE of SAMPLER: {MMrAbrYYI: H -bran.,-?N—By shy ma Imm.m. roc�0-!'.w.::. 14F TM „r p.Jrwm ti.%air}ap^ gra u:- 7 I,tS P— mtn7i•-r r.f in—. rd D:W w.M..W eav; F.ALL,Q-020rev.07, 15-May-2007 Semi-annual Stormwater Discharge Monitoring Report ' - for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted February 5, 2016 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results jjSCv_N F0 CEN��CT ON D SAMPLE COLLECTION YEAR , 2016 . SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' January _mmonth DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other: WS-IV. NSW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?z Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, inches - Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks - - 120 mg/L 1000 count per 100 mL ` 100 mg/L or 50 mg/L 004 01/27/16 0.01 <25.0 636 8S.8 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mp.,/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal Coliform results exceed the dilution upper limit, report the result as ">XX". ^r Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2\ ;fore: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B:�Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - - 15 mg/L 100 mg/L or 50 mg/L 6:0 = 9.0'SU 004 01/27/16 0.01 <5.0 85.8 7.45 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results tar at end of monitoring period in the case of "No Discharge' reports) ta: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permit Date:11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted December 21, 2015 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sam In collection or anal sis• SAMPLE COLLECTION YEAR _2015 SAMPLE PERIOD ❑ Jan -June ® July -Dec �/or ❑ Monthly' _ (month) R v DDISCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ❑PNA DEC 2 9 1.015 ❑Zero -flow ❑Water Supply ❑SA p y CENTRAL FILES ®Other: WS-IV, NSW WR SECTION Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?z Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/0 001 12/02/15 0.02 69.0 2730 11.6 002 12/02/15 0.02 91.0 12000 9.8 003 12/02/15 0.02 27.0 273 85.5 004 12/02/15 0.02 <25.0 1730 11.8 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfail, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX m L", where XX is the -numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period? Date Sample 24-hour rainfall Outfall No. Collected amount,. Non=polar O&G/TPH by ----•- Total Suspended Solids pH (mo/dd/yr) Inches3 EPA 1664 (SGT-HEM) Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 12/02/15 0.02 <5.0 11.6 7.81 002 12/02/15 0.02 <5.0 9.8 6.93 003 12/02/15 0.02 <5.0 85.5 7.31 004 12/02/15 0.02 <5.0 11.8 1 6.96 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that theme are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 Z.i -4 A,- Zvi (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted January 8, 2015 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: C.Gustin LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2015 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' _mmonth eft[DIISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA SUN 7 Zd) ❑Zero -flow ❑Water Supply ❑SA ®Other: WS-IV, NSW CEN7-RAL F! DWR SECDON PLEASE REMEMBER TO SIGN ON THE REVERSE 4 � ❑ No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 001 06/02/15 1.16 48.0 81.0 35.0 002 06/02/15 1.16 34.0 300 7.1 003 06/02/15 1.16 27.0 1,730 33.3 004 06/02/15 1.16 25.0 1,480 323 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX ms/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z - -1 Date Sample 24-hour rainfall - -Ou#fall No.: --Collected' amount, Non -polar O&G/TPH by - Total Suspended Solids pH (mo/dd/yr) Inches3 EPA 1664 (SGT=HEM) Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 06/02/15 1.16 <5.0 35.0 8.93 002 06/02/15 1.16 <5.0 7.1 6.52 003 06/02/15 1.16 <5.0 33.3 6.87 004 06/02/15 1.16 <5.0 323 6.65 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coov of this DMR. includina all "No Discharge" reoorts. within 30 days of receipt of the lab results for at end of monitorina Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/l/2012-10/31/2017 I Z U_- (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 (�Iacmnalytical* wnw.pacelabs.ccm Laboratory Report Christopher Gustin Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 Project: SEMI-ANNUAL STORMWATER 2015 Pace Project No.: 92252436 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 2 i Report Date: 06/11/2015 Date Received: 06/02/2015 Sample: OUTFALL #1 Lab ID: 92252436001 Collected: 06/02115 10:19 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg1L 5.0 06/04/15 08:58 Fecal Coliforms 81.0 CFU1100 mL 1.0 06/02/15 17:40 Total Suspended Solids 35.0 mg1L 25.0 06/04/15 08:22 Chemical Oxygen Demand 98.0 mglL 25.0 06/10/15 12:40 Sample: OUTFALL #2 Lab ID: 92252436002 Collected: 06/02/15 07:50 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mglL 5.0 06/04115 08:59 Fecal Coliforms 300 CFU1100 mL 1.0 06/02/15 15:45 Total Suspended Solids 7.1 mglL 3.1 06/04115 08:23 Chemical Oxygen Demand 34.0 mglL 25.0 06/10/15 12A0 Sample: OUTFALL #3 Lab ID: 92252436003 Collected: 06102/15 10:53 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mglL 5.0 06/04/15 08:59 Fecal Coliforms 1730 CFU1100 mL 1.0 06/02/15 17:40 Total Suspended Solids 33.3 mglL 16.7 06/04/15 08:23 Chemical Oxygen Demand 27.0 mglL 25.0 06/10/15 12:40 Sample: OUTFALL #4 Lab ID: 92262436004 Collected: 06102/15 10:53 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg1L 5.0 06/04/15 09:00 Fecal Coliforms 1980 CFU1100 mL 1.0 06/02/15 17:40 Total Suspended Solids 323 mglL 41.7 06/04/15 08:24 Chemical Oxygen Demand 25.0 mg1L 25.0 06/10/15 12:40 cam"'"" Reviewed by: Liamm Carrubba liamm.carrubba@pacelabs.com Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Certification IDs 9800 Kinsey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginialVELAP Certification #: 460221 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Page 1 of 6 (�IaceAnalytical www.pacalabs,Com Asheville Certification IN West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 2 Page 2 of 6 Document Recelpt (SCUR) Document No.: : AL-CS-001-rev.03 Document Revised: May 15, 2015 Page I of 2* Issuing Authorltles: Pace Ralsioh Qualltv Office Client Name: � 'Page 2 of 2 Is for Internal Use Only Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other Custody Seal on CooterlBox Present: ❑ yes El no Seals Intact: yes no Packing Material: ❑ Bubble Wrapt,:12206538];rTP ubble Bags None ❑ piper Circle Thermometer Used: IR Gun of!ce We Blue Nona Samples on lac, occllnp process has began IR Gun 8 71 Temp Correction Factor: Add / §ah aa--3 Q .1.y �c Oato and Initials of pertwn exom n ng Corrected Cooler Temp.: C Biological Tissue is Frozen: Yas No A cof P ry to Temp should be ahove freezing to 6'C Comman;s: ohack: Chain of Custody Present: Oyas IND ❑Nu 1. Chain of Custoqy Filled Out: OYor Zo ❑WA 2. Chain of Custody Relinquished: 40. ONO ❑NrA 3, 1'r5 CT Sampler Name & Signature on COC: Yes ON. ❑wk 4. (>-N1CD Samples Arrived within Hold Time: PIYes ❑No ❑NIA 5. Short Hold Time Analysis 472hr : as ❑No 13WA 6. bit Gill Kush Turn Around Time Requested: ❑Yes .dNo ❑NIA 7. Sufficient Volume: J2TY68 LINO ❑NIA 8. Correct Containers Used: Yes Na R 0111A 9. ABS -Pace Containers Used: ONO OWA Containers Intact: Yee ONO WA 10. Filtered volume received for Dissolved tests Clyde ONO NIA 11. Sample Labels match CDC: Oyne ❑No 13N1A 12. -includes datellimellDlAnal is Matrix: All Containers needing preservation have been checked. �Koa ONO ❑N!A 13. All contalrers needing preservation are round to be In ZYad ❑No ❑N/A compliance Y41h EPA recommendation, exce s: VOA, colVorm. TOC, C&G. Wl-DRO water TJ ae ONO Samples checked for dechlatination: Yee ONO ❑wA 14. Headspaw in VOA Vials 4mm : Oyes ©No A 15. Trip Blank Present: ❑yes ONO rF.INIA 16. Trip Blank Custcdy Seeis Prasent ❑Yee ❑No Rt WA Pace Trip blank Lot p if pui-chased): Client Notification/ Resolu+.ton: Field Data Required? Y I N Person C;:nWclad: Datemme: Comments/ Rosolutlon: SCURF ISRF -� Data: L: of : 92252436 Review:: (.) 1- f j j j I Note: Whenevrr that* Is a di;;mpency effecling North Carolina eomptianca aernpies, a copy of this forfr. YAI be sent to the North Carolina OEMNR { Cartlflcation Office ( i.a out of hold, incorrect pressrvauve, out of temp, 92262436 In.axrect containers) S Page 3 of 6 .' ZAWWal' Seetlon A PA4p& d awx 7 CHAIN -OF -CUSTODY / Analytical Request Document Thu C hWn-d-0ustody is a LEGAL OOCWENT. AN televaM Lelds ft td be conpWW w=u=*. Section B SWUM C RNP*WihaJ.G NAonrnSar[ b. 601 h 1a • .s w • a' . •. Nam" ph SAMPLE ID oil wim AW AR e "NO "MmOtrarM■©■■■■■■■■ ■■■■■■■■■■■■■MGM . �. CO 0 0 LM a 'ffvw.mr.k Nuw: ft vft Mk axmym n..dwa¢ P'am's NET 30 Crt pyam bans ash aqr.., 10 W. c1Oga. d 1 57L P.r raw+tl. b.rryYMiaee.. b pY1 .I.hF+ 30 d.ps Document Name: Sample Condition Upon Document Revised: May 15, 2015 08A * ' Recai t SCUR Page 1 of 2' Document No.: Issuing Authorities: F-RAL-CS-001-rev .03 Pace Raleigh Quality Office Client Name: -� 'Page 2 of 2 Is for Internal Use Only Courier (Circle): Fed Ex UPS USPS < Client ` Commercial Pace Other CustodySeal on Ccoter/Box Present: 0 yes E!r no Seals Intact: , 'yes [j no Packlrfg Materiel; it Bubble Wrap Bubble Begs None E' Other Circle Thermometer Used: iR Gun L:12�20653X80n! Ice We Blue Nana Samples on los, ccoiing process has begun IR Gun U 71 Temp Correction Factor: Add 1 Dole and In tiale or person exemtn ng Corrected Cooler Tam p.: � C Biological Tissue Is Frozen: Yes No A g ca I P ry io ..s�_ oheck: Temp should be above freezing to e'C Comments: Chain of Custody Present: OYes ONO ❑N1A 1. Chain of Custo Filled Out: 0Yo2 PAO OWA 2. wQfiA Chain of Custody Reifn ulshed: -9- ON. DIVA 3. Sampler Name & Signature on COC: 460, ON. ❑N1A 4. OAA$ 1Cp §Amphes Anived withln Hold Time: ZrYes ONo D WA 5. Short Hold Time Analysis 02hr : es ONO ❑WA Rush Turn Around Time Requested: L]Yes ZNo ON1A 7. Sufficient Volume: Ye: ONO ❑NIA 8. Correct Containers Used: Yes P(ko OWA Via ius— 9. `` 'i' vY A s % aU � - . -Pace Containers Used: Yes ONO OWA Containers Intact: JdY6. ON. 25A 10. Filtered volume received for Dlssolvsd tests Eves ONo WA 11. Sample Labels match COC: ee ONo OwA 12. -includes datehimehl)/Anal is Matrix: AA COnlalmvs needing pmservauon have been shed cad. ONO OWA 13. All omtairere needing preservation are found to be In twos Zjyes ONO ❑NIA compliance with EPA recommendatlon. 1 exoo s: VOA, colderro, TOC, 080. WI-0RO wafer 'LJ . ONO Samples checked for dechtoiination: Yes ONO ❑WA 14. Heads ecxt in VOA Vials I >6mm : ❑Yea ONO QWA 1 S. OYes ONO ;641A 16. Trip Blank Presaril. ZMA Trip Blank Cuslcdy Seals Present Oyes ONo Paco Trip blank Lot A it Purchased): Client Notlficationl Resolu!lon: Field Date RequlrW? Y 1 N Person C::ntsctad: Datemme: Comments/ Rasolutlnn: SCURF 1SRF Data: Review:: 6G i Note: Whanevt•r there Is a discrepancy affecting North Csrollna compliance samples, a copy of uils fora. will be sent to the North Carolina DEHNR Cerupcalion Office (I.a our of hold, Incorrect preservative, out of temp, I.h.>xrect eont&wrt) WO#:92252436 92252436 IIIIIBIIINIIIIIII lII M Page 5 of 6 ,'a�ayncar CHAIN -OF -CUSTODY / Analytical Request Document The Chairpd-Cu Wy is a LEGAL DOCUMENT. A3 rWvaM Wft must be wff*WWd aszu-4jV. lug Ilr • f+ a f— RCRA OTHER 1 .UST ITIM ®Ii■�■■�����I . e - Mr UMIM— M . MUM■■■■■■■ ■■■E■■E■■■■■i-Men y 7 0 (n 0 a w uam �g hg ova 4em yda an awp+4 u P•pY NEf 7q da pq mr t ea v».n0 •q •• np a tw c{wgw d 1 SY pr r ar4 tar w7 mr yye WM4h 36 days. Semi-annual Stormwater Discharge Monitoring Report for North.Carolina Division of Water Quality General Permit No. NCG120000 Date submitted January 8, 2015 CERTIFICATE OF COVERAGE NO. NCG120056 SAMPLE COLLECTION YEAR_2014 FACILITY NAME: Upper Piedmont Regional Landfill SAMPLE PERIOD ❑ Jan -June ® July -Dec COUNTY: Person RECEIVED or ❑ Monthly' (month) PERSON COLLECTING SAMPLES: G. Duhon DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: Pace Analytical Lab Cert. # 67 JAN 14 2015 ❑Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: CENTRAL FILES ®Other: WS-IV, NSW MAIR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 � CfD Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?' � Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/0 001 12/16/14 0.10 <25.0 <4.0 <5.0 002 12/16/14 0.10 <25.0 <4.0 10 003 12/16/14 0.10 <25.0 23.0 10.5 004 12/16/14 0.10 <25.0 8.0 9.3 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Date Sample 24-hour rainfall Outfall No. - Collected' amount, Non -polar O&G/TPH by - Total Suspended Solids pH - (mo/dd/yr) IncheS3 EPA 1664 (SGT-HEM) Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 12/16/14 0.10 <5.0 <5.0 7.47 002 12/16/14 0.10 <5.0 10 6.58 003 12/16/14 0.10 <5.0 10.5 6.95 004 12/16/14 0.10 <5.0 9.3 7.01 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART it SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR. including all "No Discharae" retorts. within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 aceAnalytical wmvpacefabsxom Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Laboratory Report Mr. Greg Duhon Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 Project: UPPER PIEDMONT SEP 2014 Pace Project No.: 92229858 Page 1 of 2 Report Date: 12/30/2014 Date Received: 12/16/2014 Sample: OUTFALL 1 Lab ID: 92229858001 Collected: 12/16/14 12:55 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg/L 5.0 12/19/14 10:15 Fecal Coliforms NO CFU1100 mL 4.0 12/16/14 17:48 Total Suspended Solids NO mg/L 5.0 12/22/14 06:42 Chemical Oxygen Demand NO mg/L 25.0 12/30/14 08:30 Sample: OUTFALL 2 Lab ID: 92229858002 Collected: 12/16/14 13:25 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg/L 5.0 12/19/14 10:16 Fecal Conforms ND CFU/100 mL 4.0 12/16/14 17:48 Total Suspended Solids 10 mg/L 3.8 12/22/14 06:42 Chemical Oxygen Demand ND mg/L 25.0 12/30/14 08:30 Sample: OUTFALL 3 Lab ID: 92229858003 Collected: 12/16/14 13:40 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg/L 5.0 12/19/14 10:16 Fecal Coliforms 23.0 CFU1100 mL 1.0 12/16/14 17:48 Total Suspended Solids 10.5 mg/L 3.1 12/22/14 06:43 Chemical Oxygen Demand ND mg/L 25.0 12/30/14 08:30 Sample: OUTFALL 4 Lab ID; 92229858004 Collected: 12/16114 13:10 Matrix: Water Parameters Results Units Total Petroleum Hydrocarbons ND mg/L Fecal Coliforms 8.0 CFU1100 mL Total Suspended Solids 9.3 mg/L Chemical Oxygen Demand NO mg/L Reviewed by: Liamm Carrubba liamm.carrubba@pacelabs.com Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Cortification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 Report Limit Analyzed Qualifiers 5.0 12/19/14 10:17 1.0 12/16/14 17:48 4.2 12/22/14 06:43 25.0 12/30/14 08:30 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Page 1 of 4 acmnalyiica! wsna!pacerabs.com Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Asheville Certification IDs West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 Page 2 of 2 Page 2 of 4 Document Name: Sample Condition Upon Document Revised: April 04, 2013 �,. deefinatical. Racal t tqrl ir Pagel of 2 Document No.:. Issuing Authorities: ' wvJ+�corp �M, F-RAL-CS-001-rev-02 Pace Asheville QuaBy Office Client Name: Vo Where Recelved: ❑ Huntersville F As Eden Raleigh Courier (Circle): - Fed Ex UPS USPS Client Commercial Pace .Other _— Custody Seal on CoolerlBox Present: U yes no Seals Intact: yes no Packing Material; n Bubble Wfep [l Bubble Bags j None n Other Circle Thermometer Used; IR Gun 6 �122065 a of leo:�Blue Nono Samples on tcs, cooling process has begun ER Gun Back 22065371 Temp Correction Factor: Add 1iyot + R Bate and Initials of person examining ii Corrected Cooler Temp.: I r C l3iologEcai Yissue Is Frozen: Yos No wA comet reso a io check: Temp. should be above freezing to 8°�C Comments: hain of Custod : Present F � Yos ❑No • ❑WA 1. hain of Custody. FlHed Out: yns ON. ❑wA 2, Chatn of Custody Relinquished: os Dive ONIA 3. Sam for dame & Signature on COC: f4yes ❑No ❑wA 4. Samples Arrived within Hold Time: yw ©No i7wA 5. Short Hold Tltno Analysis <721ir): 16yet ❑No QUA Rush Turn Around Time Requested: ❑Yes a`b 04A 7. Sufficient Volume: Oes ONo DwA S. Correct Containers Used. Yas ❑No EIwA 9. -PaceContainers Used: Yes ON* ❑NIA Containers Intact: Yos ❑No 11WA 10. Flltored volume received for Dissolved tests ❑Yee ❑No AWA 11. Sample Labefs match COC: Ye Q140 I wA 12, •Includes dateltlmcAD1Ana1 sis N4atrix: VT All containers needing pres,-rvolon have been checked. [�No [lwA 13. All containers needing preservation are found to be in p�es dNo CIN1A compliance with EPA recommendation. oxcoptions: VDA. 011ann,70C,060,Wl•GRO(waler) Yea C1No Samplos checked for dectilorinallon: Yos EINo ❑NIA 14, Headspaco in VOA Vitals >6mm : 11 ❑No wA 116, Trip Blank Present: ❑Yes ❑No NIA 16. Trip Blank Custody Seals Prosent ❑yes ❑NoiwA Puce TrIp Blank Lot f (if purchased Client Notification) ReSOMIon: Field Date Required? Y ! N Person Contacted: Date/Time: Commenial Resolullow SCUE3F ISitF LJr% 4i t�. tit +�Q . 92 / I l Date: 229658 Note: Whenever there is a discrepancy affecting North Carolina compllont:e 1111111111111P sampios, a copy of this form will be sent to the North Carolina DEHNR Certirication Office ( Le out of hold. incorrect preservativo, W of temp, 922219858 inoonecl conialnora) Page 3 of 4 0 Q N CD aceAna)ytical Chain of Custody Report Results to: Greg Duhon Republic Services 9650 Oxford Rd Rougemont, NC 27S72 ATM: Greg Duhon Ph one: 336.364.3699 Bill Results to: ❑ Standard Report Delivery Republic Services flush Report Delivery (w/ surcharge) Requested Due Date: Project Reference: Upper Piedmont Sep. 2014 ATTN: Purchase Order p: Sampled By: G. Duhon Sample Description Cam sfte — p° Start Date Stop Date ' , DW, SW, Analysis Requested _ or Grab - Start Time Stop Time GW, etc 1Z1��1 f 12/lAllISW Outfall 1 G 20 7,47 COD, Fecal Coliform, TS5, Non -polar O&G Outfall 2 G _ SW C v COD, Fecal Coliform, TS5, Non-poiar O&G Outfall 3 G SW ' COD, Fecal Coliform, TSS, Non -polar O&G /z. /� 1- Outfall4 G SW Q r OCR COD, Fecal Coliform, TSS, Non -polar O&G Rrlin s (sip, tea. Y iced EyDs; j ( Tim 77< Zk4 For Lab Use Only Temperature at receipt: 9dinquished by (signawre) Received by (signature) Da:e, Time Relinquished by (sigrature) Received by (5igna;urel Date Time Temp: C. Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted May 19, 2014 CERTIFICATE OF COVERAGE NO. NCG 120056 SAMPLE COLLECTION YEAR _2014 FACILITY NAME: Upper Piedmont Regional Landfill Q ECEIVEDAMPLE PERIOD ® Jan -June ❑ July -Dec COUNTY: Person 1 ~. or ❑ Monthly) (month) PERSON COLLECTING SAMPLES: G. Duhon MAY 2 2 Z014 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: Pace Analytical Lab Cert. # 67 []Zero -flaw ❑Water Supply ❑SA Comments on sample collection or analysis: CENTRAL FILES ®Other: WS-IV, NSW DWQIBOG Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks ===> - - 120 mg/L 1000 count per 100 mL 100 mg/L or SO mg/L 001 04/30/14 0.75 113 19.0 31.6 002 04/30/14 0.75 99.0 545 11.8 003 04/30/14 0.75 <25.0 11.0 5.6 004 04/30/14 0.75 <25.0 50.0 54.4 i Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they -must be reported in the format. "<XX_mRIC, where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 +l Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period:2 Qutfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non-polarO&G/TPH by EPA 1664 (SGT-HEM) - Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 001 04/30/14 0.75 <5.0 31.6 7.81 002 04/30/14 0.75 <5.0 11.8 7.28 003 04/30/14 0.75 <5.0 5.6 7.09 004 04/30/14 0.75 <5.0 54.4 7.72 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OLITFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitorina Period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2of2 (�IaneAnalXica( www.pac0abs.com Laboratory Report Mr. Greg Duhon Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 Project: STORMWATER 1 Pace Project No.:92199303 r. Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 ir1 (919)B34-4984 Page 1 of 2 Report Date: 05/12/2014 Date Received: 04/30/2014 Sample: OUTFALL 1 LabID: 92199303001 Collected: 04/30/14 09:25 Matrix; Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg1L 5.0 05102/14 09:48 Fecal Coliforms 19.0 CFU1100 mL 1.0 04/30/14 15:55 Total Suspended Solids 31.6 mg/L 5.0 04/30/14 13:51 Chemical Oxygen Demand 113 mg/L 25.0 05/12/14 14:28 Sample: OUTFALL 2 Lab ID: 92199303002 Collected: 04/30/14 09:15 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg/L 5.0 05/02/14 09:48 Fecal Coliforms 545 CFU1100 mL 1.0 04/30/14 15:55 Total Suspended Solids 11.8 mg/L 5.0 04/30/14 13:52 Chemical Oxygen Demand 99.0 mg/L 25.0 05/12114 14:28 Sample: OUTFALL 3 Lab ID: 92199303003 Collected: 04/30/14 09:45 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum hydrocarbons ND mg1L 5.0 05/02/14 09A8 Fecal Coliforms 11.0 CFU1100 mL 1.0 04/30/14 15;55 Total Suspended Solids 5.6 mg1L 2.9 04/30/14 13:53 Chemical Oxygen Demand ND mg1L 25.0 05/12/14 14:28 Sample: OUTFALL 4 Lab ID: 92199303004 Collected: 04/30/14 09:55 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Petroleum Hydrocarbons ND mg/L 5.0 05/02/14 09:49 Fecal Coliforms 50.0 CFU/100 mL 1.0 04/30/14 15:55 Total Suspended Solids 64.4 mg1L 10.0 04/30114 13:53 Chemical Oxygen Demand ND mg1L 25.0 05/12/14 14:28 11 Reviewed by: J'W' %� ' `-' Tabitha M Dacal tabitha.dar-al@pacelabs.com Raleigh Certification IDs 6701 Conference Drive Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntefsville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #; 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification M M-NC030 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiafVELAP Certification #: 460221 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Page 1 of 4 aceAnalytical www.pacaratrs.cw Asheville Certification IDs West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 �. (919)B34-4984 Page 2 of 2 Page 2 of 4 ,; �Pace�lrlalyfical ' Document Name: Sample Condition Upon Document Revised: April 04, 2013 Receipt (SCUR) Page 1 of 2 Document No.: Issuing Authorities: __F-RAL-CS-001-rev.02 1 Pace Asheville Qualitv Office Client Name:�,�' Where Received: Huntersvilte 0 Asheville C] Eden p" Raleigh Courler (Clrcle): - Fed Ex UPS USPS Clien - Commercial Pace Other_ .. _ Custody Seal on Cooler/Box Present: (3 yes 0no Seats intact: fj yos no Parking Material: 0 Bubb.'e Wiap ❑ Bubble Bags ij None Other_ Circle Thermometer Used: lR Gun SH:12209 Type of Ice: ( Blue None Q Samples on kce, cooling process has bopun IR Gun Back Up 5NA22065371 Temp Correction Factor: Add r 5 btr ct r 6 C r Corrocted Cooter Temp.: .) 1 �'i C Biological Tissue Is Frozen: Yes No Temp should be above freezing to 61C Comments: Date and InftWs of person examining tentento r resery t n check; - O l4 Chain of Custody Present; Yes IJNo . Chain of Custody Filled Out: eyes ONO ❑WA 2. Chain of Custody Rellnquished: AYez GNo 13WA 3. Sam ter Name 8 Si nature on CQC: ZJYas ON. i]NIA 4. Sam los ATrivod within Hold Time: Fly. Lu. ❑WA 5. Short Hold Time Analysis <72hr : Ye9 ❑Ho C1wA 6. Rush Turn Around Time Re uosted: ❑YBs 2Lfo GWA 7. Sufficient volume: es 0tb C.INrA 8. Corrobt Containers Used: -Pace Conte€star? Uscd: _AY. ON. 25Yos IJNo ❑wA ❑W'A 9. Containers Intact: _AY. ❑No ❑wA 10. Filtered volume rece'Ivod for Dissolved tests Dyes ❑No JiKwA 11. Sample Labels match COG: Includes date/UrnelID/Ane4 sis Matrix _. Yes 00o Lj_ ❑WA 12. All contalrtom newi'rg'preserva5'on have been chec*ed. All Contak:ers ttaeding presowation are found to be in compliance with EPA ruwmmendation. "roptbrw ynA, wilform, TOC, dAG, WWRO {water} You ❑No �Yas ON. Yes ONO ❑WA LWA 13. ♦]nin les checked for dechtorination; ❑Yee ❑No AWA .14. Woadspace in VOA Vials >6mm : Dyes ❑No AWA 15. Trip [flank Present; 'trip Blank Custody Seals Present Pico Trip Btank Lot # Llf purohase0�_ . _ Dyes Cl No IPMA laves ONO /IVA 16, Client Notification/ Resolution: Person Contacted; Data[Time: 5 4' n jkj -�'4 SCURF ISRF Dnto• Roviow:: i P�IA Nuto: Whoneves there Is o discrepancy affecting North Carolina compAence aampto:., a copy of this form wilt be sent to tho North Carolina DEHNR Ceitlfication Office ( i.o out of hold, interred preservative, out of temp, inoarf�ci contmtnersj Field Data Required? Y r N Place labs€ here OR Handwrite projWnumber (If no label available) G I } Page 3 of 4 Pace AnalyYcaI' CHAIN -OF -CUSTODY 1 Analytical Request Document T:•e CMirrn[•GrWc>'1y rs u LEGAL D4YCURSEI:7. A[I rel@V81i tCd3 n,[:a1 !ye ucrrNa:ad :oral dfey. Section A Section B Section C Fagr 1793522 RKUIrea Cl "m hoi ' rowU Raaulmd Pp*a lnfomwi=-rvolcE In:orrratW: Ram 7o, Croy To' ConzPAny N.".RE_GUtATORY AGENCY Ale- z s �� Addf"C i'- NPDES GROUND W. T£R - DRINKING WATER 0U�� =n. l ix . ?• :1 OoOer Ud.: `"a•" awmanra: UST RCP.A OTkER UG ?Mrx: Fain 1" 3er u�r:mr: 511e Location STATE: ' rrequeatad Due D 'AWT T: Praect NuTtur: 0 — :J Requested Analysis Filtered (YIN) - section D Malrtia Code* 3 COLLECTED Preservarr�es _ > Paa�lradC�crSk,b,-a1a, o D-1" WRW DW ' U vmtr Y3 vi"ivWa•m 'MV 3 u s+a�sre yocn're pmd": P 5045did Si SAMPLE ID p 0rn z _� in �a eA-I.0,91;) ,k' AR LL < m 1 Sark Ds MUST BE UNCOUE .G$uc O tYher DT X u w (U 61 i µ d mM 61DATE nut DATE TINE x z O IIIPace Project Nod Lair i.D. i W Z 'Z w1i 6; 4 s' a T 8 6 i0 ti 12 ADDRIONAL 0ON521 S RE OWSHED BY I AFFILIATION SATE TIME ACCEPTED BY AFF nOK DATE TIME SAMPLE CO11RlTtOHS .0 j SAMPLER NAME AND SIGNATURE U v PRINT Name of SAMPLER: PATE Signed SIGNATURE of SAMPLER: 0� m ~ Yu ` ¢ v n F % (MMIDR M: [ "� N •npr�farr f *, VY YFifV 7i, w' ra rcm araxanp PaWX CET 30 day Pa7n N ram, a ap-.a„p as t.-a d'arjsa 0 t.57. CN mortr aty nracos rar 1l� W days F -L-O 020mv.01. 15-cloy-2007 v n v d CD rL Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted March 6, 2014 CERTIFICATE OF COVERAGE NO.ACG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: G. Duhon LABORATORY: Pace Analytical Comments on sample collection or analysis: SAMPLE COLLECTION YEAR _2014 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Monthly February (month) Lab Cert. # 67 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]watersupply ❑SA ®Other: WS-IV, NSW Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?Z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 003 02/21/14 0.6 Not Analyzed 34.0 Not Analyzed Dr/Ng- . C VtL) AR I a ?n,h I rXML i LEQ 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". IT Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. 1 ❑ No discharge this period:2 Outfail No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 003 02/21/14 0.6 Not Analyzed Not Analyzed Not Analyzed Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERSTIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that thXe are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) it / / , a. / 4 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2of2 aceAnalytical www,pecafabs.com Laboratory Report Mr. Greg Duhon Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 Project: 02/21/14 UPPER PIEDMONT Pace Project No.: 92190641 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)634-4984 Page 1 of 1 Report Date: 03/03/2014 Date Received: 02/21 /2014 Sample: TANKA Lab ID: 92190641001 Collected: 02121/1412:00 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Cyanide ND mglL 0.0050 03/02/14 13:15 Sample: OUTFALL 3 Lab ID: 92190641002 Collected: 02/21/14 12A5 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Fecal Coliforms 34.0 CFU1100 mL 1.0 02/21/14 14:06 Reviewed by: J"-Ut-o`- i v O"� Tabitha M Dacal tabitha.dacal@pacelabs.com Raleigh Certification IDS 6701 Conference Drive Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IDS 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginialVELAP Certification #: 460222 Page 1 of 3 Document Name: Sample Condition Upon Document Revised: April 04, 2013 ���?C2A17c71ytlC�7!' #2ecoi t SCUR Page 1 of 2 Document No.: Issuing Authorities: F-RAL-CS-001-rev.02 Pace Asheville Quality Office U11ent Name: Where Received: El Huntersville, n Asheville El Eden Raleigh Courier (Circlo): Fed Ex UPS USPS lien Commercial Pace Other Custody Seal on CoolerlBox Present: ❑ yes f"/T no, Seats intact: j7 yos 0 no Packing Material: C11 Bubble Wrap i� Bu i Bogs 4 None F" Other/ Circle Thermometer Used. tR Gun SN 2065387Typ of Ice: Wot Blue None EJ Samples on ice, cooling process has begun iR Gun Be Temp Correction Factor: Add f btract Lo. C Date and lnitlela of person examining Corrected Cooler Temp. ; ' C Biological Tissue Is Frozen: Yes NoG ca tfr t ! rc check: 'Romp shpukf be above freezing to 6°C Comments. Chain of Custody Present: Ycs ON" ❑NIA 1, Chain of Custody Filled Out: Yes ONO 0wA 2. Chain of Custody Relinquished: Yes ONO CINIA 3. Sampler Name & Signature on COG: roe ❑No 13NIA 4. Samples Arrived within Hold Time: Yes Dive ©wA 5. Short Hold Time Anal is <72hr : Yes Ow ©wA 6 Rush Turn Around Time Requested: ❑Yee No ❑WA 7. Sufficient Volume: Yes ON. ❑,%VA 8. Correct Containers Used: Yes ❑No ❑WA 9, -Pace Containers Used: 16y. QNa ❑WA Containers Intact: Yea ONO OWA 10. Filtered volume received for Dissolved tests OYes ❑rso ,wA 11. Sample Labels match COC: VYes ❑No 0wA 12. -includes dateAllnorlDlAnal •sis Matrix: M contah'ibis n:uding proservat;on have boon chocked. Yes ONO ©NIA 13, Atl conlstrnVrs needing pn:80rvvat7on are sound to be in '°S ONO ❑N1A ramplionce. with EPA recornmemIntion. 777��� 0 exculQris: VOA, nolifurrr. TOC, O&G,1,YI.ORQ {watw) l Yes No Samples chocked for dechlorination: Yes LlNo ❑wA 14, loads ace in VOA Vials >Gnim : (Ayes ❑No NIA 15. Tri;3 Plank Proscnl: ❑Yes nNo I�NIA 16. Trip Blank Custody Seals Prosurit ❑Yes ❑No 4NIA Pare Trip Blank Lot ft tlf purchasedL,-__ Client Notification! Resolution: Field Date Required? Y I N Person Contacted: Date/Time: Comments/ Resolution: SCURF lSRF pate: r9ca) 'A' ' Review:. Note: Whonovor there le a discropancy atrecling North Carolina compliance samples, a copy or this form wil$ be sent to the North Carolina DEHNR CartiBCation Office { Lo out of hold, incorroct presorvallo, out of temp, incnfrect containers) Place label here OR Handwrite project number (If no labol Available) Page 2 of 3 .1 2ceAnalyficaf' www,paeelabe.cum 6701 Conforance Drive, Raleigh, NC 27607 ph: (919)834-4984,fax: (919)$34.5197 NCVvW Ced#67, NCDW Certll37731 Chaim. of Custody w.o. # Report Results To: Bill To: Company: Upp— 1-��i71�' �r7 Project Reforence: Project Number: _ Purchase Order A: RollnP-ied by ignalu�) ri inquishod b sign tore) i Re otvad srg re) I Received by (signature) e 10a a 71me Time Rclinquiwwd by (signature) Received by (signature) Date Time, ,�Z- qo (,4) Recelpt Corxlitions (Lab Use Only) ❑ 4+20C ❑ Temp: —°C Res. Chlorine: El Absent 0 Present ❑ rVa Acid preserv. e27 0 Yes ❑ No ❑ rVa Base presum >127 C3 Yes C) No © n!a Page 3 of 3 January 28, 2014 Mr. John Holley, PE �R�PUBLIC ZOA Sent via Electronic Transmission Regional Engineer North Carolina Department of Environment and Natural Resources Division of Energy, Mineral and Land Resources Land Quality Section Raleigh Regional Office 1628 Mail Service Center Raleigh, NC 27699-1628 Re: January 2014 DMR Upper Piedmont Environmental Landfill 9650 Oxford Road, Rougemont, NC 27572 NCG 120056 Dear Mr. Holley, RECEIVED FEB 0 3 2014 CENT RAL TILES DVVQIBOO On behalf of the Upper Piedmont Regional MSW Landfill, Republic Services is transmitting a Discharge Monitoring Report in response to the Tier II activities required for fecal coliform at Outfall 003 at the referenced site. This is the second consecutive monthly sample for fecal coliform at Outfall 003 that is below the benchmark value. Based on the analytical results from the past two months and the information previously provided by letter dated December 27, 2013 (copy attached), Republic Services requests the cessation of monthly sampling for fecal coliform from Outfall 003 on a monthly basis. Thank you in advance for your consideration of this request. I can be reached at (919) 354-3227 with any questions. Sincere y, — / '/� z,%--- ' Matt Einsmann, P.E. C Republic Services of NC, LLC Cc: Mr. Greg Duhon, Upper Piedmont Environmental (electronic copy) Mr. Bradley Bennett, DEMLR Stormwater Permitting (hard copies) 1220 Commerce St SW Conover, NC 28613 828.695-2055 • Fax 828.464.2433 www.republicservices.com Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted December 27 2013 CERTIFICATE OF COVERAGE NO. NCG120056 FACILITY NAME: Upper Piedmont Regional Landfill COUNTY: Person PERSON COLLECTING SAMPLES: G. Duhon LABORATORY: Pace Analytical Lab Cert. # 67 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2014 SAMPLE PERIOD ❑ 1an-June ❑ July -Dec or ® Monthly' January month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other: WS-IV, NSW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 003 01/14/14 0.6 Not Analyzed 99 Not Analyzed 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. 11* Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No disGhorge this period Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 003 01/14/14 0.6 Not Analyzed Not Analyzed Not Analyzed Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one coot+ of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitorina oeriod in the case o "'No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 ace Analytical WW..pacelahs.C= Laboratory Report Mr. Greg Duhon Upper Piedmont Environmental 9650 Oxford Rd. Rougemont, NC 27572 Project: SAMPLING 1114 Pace Project No.: 92186294 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 01/28/2014 Date Received: 01/14/2014 Sample: TANK Lab ID: 92186294001 Collected: 01/14/1412:50 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Cyanide 0.0064 mg1L 0.0050 01/26/14 11:13 M1 Sample: OUTFALL 3 Lab ID: 92186294002 Collected: 01/14/14 13:45 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Fecal Coliforms 99.0 CFU1100 mL 1.0 01/14/14 15:35 ANALYTE QUALIFIERS Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Reviewed by: 'J"�W,' 0 ° 1 Tabitha M Dacal tabitha.dacal@pacelabs.com Raleigh Certification IDs 6701 Conference Drive Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification M 460222 Page 1 of 3 ClientNkme:� �- Where Received. (] t-luntersvilla ' ❑ Asheville Eden Raleigh Corrrlor (Circle): Fed Cx UPS US PS p0ijent CommerciaY FaceCihor CrrstodySeal on C0Q)erit30X Present: ElYes Seals Intact: ?es ❑ no Packiroy Materlal: ❑ Bubble. 1M,,jp ❑ B bl. s ray None Circle Thermometer used: IR Gun SN: 22065387T f Ice: vet Other -- Circle None Snm tes on Ice, vole e4 fi n9 process has b un IR Gan B P Ofi537 Ternp Correction Factor: Add /, ubtract . n. G Corrected CopletTei►ip.:�L_..r C, Temp shot ' . Blofor�ical Tissue is Froxen, Ya IN' Rat a d tt > d pa n rs 9 d be Obove freozing to Vc cariEerits Comment% ' Chain of06StodyResont: - CS es.❑No C7WA 1,' Cliaih of Custody Fiiled Out: es . dNa QNIA 2. Chap bf CUstod Reliacluisticd:.e4 ONG, 00/4. 3. Sampler Name &.Signature on COC, es .L]No ,. ❑NrA, q, Sai,tiP es or ed wilhin Hold Time: yes NO ppyA 5• Sti4tt HOId,Titn©Analysis (<72hr): Yes. qNv OWA #OLLI 7TtCn.Af4U[id TIm4 Reyuesfed: [�Ycs . No blIiA S[tff cient VQ,un a: Ycs C1No • C7NfA B. orreot Gohtainers Used Yes t 1N0 C]WA 9, -face Containers Used: Qy,' CiNo' []NIA . CoEitalliers lritact:.' Yes , CINo .ONIA 10. Filtered Volume received for. Dissolved torts t7Yes GN1 , Sample Labets-match COC: Vos' p No. ❑OVA 12, -Includes date time11Q1Analysis Matrix: Me n alrers needirg preservation have been chooker3. a os 13A ❑NIA 13. All coniahars nee liltg preserva4'o9 aro found to be In p�Y� pNo ❑NfA cgt7epitancs�viUt ! pA recanptendaiiert except ens: VOA, co1lfarm, TpG, O�G, LYb0R0 (wa sr) Yes • ONo Initial when complete Saii)le cheokedfoC dectltorinatlon: Yes C1No ONIA 14. Fleadsp'ac©hi V0A w!ts. >Gmm : ❑Yec E714o VNIk 45. 1•rip Blank:Present: 13Yeo pxo WA_ 16. Trip Blank. Cusfpay Seals Pre§ nt ❑Yes ONo C NIA Pace l•rip.ekank Lot ff if pilrohased}:_^__ Client Notification! Resolution: Field Data Requlred? Y I N Person Contacted: Datemme:- GemmelLts/ Nsoluh'on: SCURF Review: SRF Review; Mote: Whenever there 1s a a1feeli1v North Carolina compltanca ant to the North Carollria DEHNR incorrect containers) gate late-i nere Handwrite project number Page 2 of 3 aceAnalytical www.patelabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (319) 8,M-4984. lax: (910) 834-6497 NCIM7 CertxG7• NCDW Cenk37731 Chain of Custody w.O.# Report Results To: Compafly: L%�% ' 1'JE7�it.1pN Alin: ('2 1 A pit) AJ Phone: _fz_3y, _15� Fax: �[.--i / Sampled by (signature): Bill To: - -__ _5i Projecl Reference: Project Number; Purchase Order Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects ere subject to prior approval by the laboratory Requested Due Dale; Sample Descnprton Ll, a �fiNK fa c:era, Start Daie "�$End Daie g[ut8trix 'c i'soc isAnyseslRequegtedtL;" i? i ., ''a$ k a -Start Timesw �' s f itEndtTirne ".. I /Z J J)14- tt��.R ♦ -yti' w. t� EZ t � i�r ROWQQ.. le y signature ece yl(signature) tnNa uses F at Res. Chlorine- Ilinquishpd•t2y, nature) i Rer:eiveri b SK�rlahlfe) Date Tima C_] Absent Dt Present Acid preserv. <27 riehnquished by (stgnature) Received by isgnalure) Dale Tlme ❑Yes ❑ No C3 rva Base preserv. >12? I O Yes ❑ No iJ WE n nla J Page 3 of 3 TRW REPUBLIC Zk*A SERVICES December 27, 2013 Mr. John Holley, PE Regional Engineer North Carolina Department of Environment and Natural .Resources Division of Energy, Mineral and Land Resources Land Quality Section Raleigh Regional Office .1628 Mail Service Center Raleigh, NC 27699-1628 Re:. Request to Cease Sampling under Tier Ih'Requirements Upper. Piedmont Environmental Landfill 9650 Oxford Road, Rougemont, NC 27572 NCG 120056 Dear Mr. Holley, On behalf of the Upper. Piedmont Regional MSW Landfill, Republic Services is 'requesting to cease sampling for fecal coliform from Outfall 003 on a monthly basis in accordance with the Tier I1-requirements under. General Permit NCG12000O. This request is made following an inspection of the site by Mr. David -Parnell- with the Land Quality Section on December 17, 2013. During the site inspection, Mr. Tarnell observed the stormwater basin upstream of.0utfall 003, and eonfirmed.that there was no industrial activity occurring in the drainage area leading to Outfall 003. A summary of the analytical 'results from the site's outfalls from 2010 is attached for reference. In addition, a site map depicting the outfalls is attached. While unconfirmed, the source of the elevated fecal coliform results is likely caused by wildlife activity (both birds and animals) in the area surrounding Outfall 003. It is our opinion that the activities associated with the landfill are not causing the elevated results, and request -that the site be allowed to cease the Tier II requirements. Thank you in advance for your consideration of this request. I can be reached at (919) 354-3227 with any questions. Sincerely, Matt Einsrriann, P.E. Republic Services of NC, LLC Cc: Mr. Greg Duhon, Upper Piedmont Environmental Mr. Bradley Bennett, DEMLR Stormwater Permitting 1220 Commerce St SW Conover, NC 28613 828.695-2055 • Fax 828.464.2433 www.republicservices.com STORMWATER ANALYTICAL RESULTS UPPER PIEDMONT ENVIRONMENTAL LANDFILL NCG120056 Outfall No. Industrial Activity Associated with Drainage Basin Activity Status Date COD (mg/L) Fecal Coliform (CFU/100 mL) ' . TSS :(mg/L) Oil and Grease (mg/L) TPH . {mg/W. 1 Landfill Inactive 6/30/2010 NO NO ND ND NA 5/27/2011 <10 14 111 6A NA'. 9/23/20i1 18.2 . 182: ' . ' 68 5.4 NA _ 5/23/2012 14.9 4 6.7 <5.0 NA 10/29/2012 ND 11 11.1 ND NA 6/3/2013 <25.0 20.0 20.5 NA. <5.0 - • 10/7/2013 <25.0 80.0 19.6 NA <5.0' - 2 Landfill Active 6/30/2010- ND NO NO ND NA 5/27/2011 13.7' 128 63.5 5.8 NA 9/23/2011 54.1. 5,000 99 <5 ' ' NA. '.- 5/23/2012 ND NO - - ND ND NA 10/29/2012 ND 191 9.1 ND NA. 6/3/2013 ', 47,0 6,000 9.5 NA <5.0. 10/7/2013 28.0 SBA 18.1 NA c5.0 3 Borrow Area Inactive. 6/30/2010 ND ND ND ND NA 5/27/2011 11.4 it 11A 1 5.9 NA 9/23/2011 12.6 30 6 <5' NA 5/23/2012 11.8 30 4.1 6.4 NA ' 10/29/2012'- ND . 44' ND ND NA' . 6/3/2013 <25.0.:'. 2,500 5.7 NA <5.0', 10/7/2013 46.0 6,000 25.5 NA <5.0 11/30/2013 No Discharge 12/9/2013 36.0 224.0 14.7 NA <5.0 4 Borrow Area Active .6/30/2010 Outfall Not Constructed 5/27/2011 39.9 100 19.2 <5 NA .9/23/2011 18.2 >6,000 '46.7 5.4 NA '5/23/2012 26.4 ' 95 57.6 6.4 NA. .. 10/29/2012 ND 28 4 ND NA . 6/3/2013 33.0 3,000 5.7 NA <5.0 10/7/2013 <25.0 16.0. 5.8 NA' <5.0 Threshold Value 120 1,000 100 30 15 NO - Not Detected Above Laboratory Reporting Umit NA- Not Analyzed (Note: Sample analysis changed from O&G to TPH with issuance of new General Permit NCG120000, effective November 1, 2012.) Bold Values Indicate result's above'the Threshold Value Page 1 of 1 12/27/2013 Site Map 1 i Upper Piedmont Regional Landfill ZO GRAPHIC iSCALF IN FEET REPUBLIC Date 117i2013 SERVICES