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NCG120051_MONITORING INFO_20180627
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v o 0 5 DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ aoJ�� a 7 YYYYM M DD • r Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality, General Permit No. NCG120000 Date submitted 22 June 2018 CERTIFICATE Of COVERAGE NO. NCG120051 SAMPLE COLLECTION YEAR �2018 FACILITY NAME _Uwharrie Environmental IMPLE PERIOD X Jan -June ❑ July -Dee COUNTY _Montgomery � CFJ\/ F or ❑ MonthW (month) PERSON COLLECTING SAMPLES _Brian Scott Re D SCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY ENCO Labs _ Lab Cert. # _CA18914 3Us 2 ❑Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: CEN-TP'L FILES X Other C DWR SEC_f10N PLEASE REMEMBER TO SIGN ON THE REVERSE � Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?? Outfall No. Date Sample Collected' (mo/ cted 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks 120 mg/L 1000 count per 1W mL 1W mg/L or 50 mg/L 1 No Discharge 2 6/12/19 .1" 19 6 71 513 6/12/18 Ah. 10 400 2.8 613 No Discharge 7A No Discharge 7C No Discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ? For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format,."<XX ma/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 76 6/12/18 .10 9.85 3.6 6.8 Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Trer 1, Trer 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ _ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainol and ane copy of this DMR, includina all "No Discharae" resorts. within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage -the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." nA� G lo25 �� (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 ENCO Labuma.urvC.50 Accurate. Timely, Responsive. Innovative. 102-A woodwinds Industrial Court Cary KC, 27311 Phone: 919.467.3090 PAX: 919.467.3515 Friday, June 22, 2018 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Uwharrie Stormwater ENCO Workorder(s): CA18914 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, June 12, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative If applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL Tbls report relate%Only Uo the Wroe as received by the IaboraDy, and may only be reproduced In Ul. Page 1 of 9 www.encolabo.com SAMPLE SUMMARYMABORATORY CHRONICLE alas ID: Outfall s2 tab ID. CA1691"1 : 05/12/18 00:20 Received: 06/12/18 11:50 parammor SM 2540D•1997 NO PREP bold oasarrlmer,l 06/19/18 06113118 07:44 06/13/18 07:44 SM 522OD•1997 Same 07110/18 06/18/18 14:30 06/18/18 17:15 QlsM ID: Outfall Aso lab 10: CA18S14-02 Sampled: 06/12/10 08:00 Received: 06112118 11:50 Para meMr SM 25OD.1997 NO PREP bold Date11'lmela3 D6119/18 06113/18 07:44 06/13/18 07:44 SM 522OD-1997 Same 07/10/18 06118/18 14,30 06/18/18 17:15 plant ID: Outfall 076 Lab M CA10914-03 Sampled: 06/12/18 08:35 Received: 06112/16 11:S0 P,Jromew EPA 1664A Pregafathm EPA 1664A Hold 111101I>11 07/10/18 Edp.Q11CLI>sIIC[ll 06/19/18 1615 06/21/18 14:25 SM 254OD•1997 NO PREP 06/19118 06/13/18 01:44 06/13/18 07:44 5M 4500H+8.2000 NO PREP 06117J18 00:49 06/18/18 15:45 06/18/18 15:45 SM 5220D•1997 Same 07/10/18 06/18/18 14:10 06/18/18 17:15 FINAL. TNs report rdKft only W the sample as received by the IabwaWry, and mar only be reproduced In fuQ. PB e 2 of 9 www.enmtabo.com SAMPLE DETECTION SUMMARY awt ID: Outfall C2 Lab ID: CA18914-01 ABBhu Beautla He4 Hu Eu unb Llmw Kau Chemical Oxygen Demand 19 to 10 mgJl SM 5220D•1997 Total SApended Solids 71 7.1 7,1 mg/L SM 2540D-1997 Chart ID: Outfall 05B Lab ID: CAIU14-02 ADa110 Balmu no M" W. ilnita t Total Suspended Solids 2.8 2.5 2.5 mg,IL SM 2S40D•1997 CAmtt ID: Outfall 075 Lab ID: CA18914-03 ADet><GO Beealta Bea H L Bh untta Neumd Nau 00 9 Grease (HEM) 9.85 2.40 5.00 mglL EPA 1664A PH 6.8 1.0 1.0 PH SM 45DOH+8.2000 Q-01 Temperature for pH (deg. Q 23 PH SM 4500H+8.2000 Q-01 Total Suspended solids 3.6 2.5 2.5 mgll SM 2540D-1997 flow This report relates only to The sam06a as remlved by the laoara , and may only W rWodured In Wx. Page 3 of 9 www.encolobs.com ANALYTICAL RESULTS Dewiption: Outfall A2 Lab Sample 10:CA18914.01 Received: 06/12/18 11:50 Matrix,, Water Sampled: 06/12118 0810 Work Order: CAI B914 Project: Uwharrie Stormwater Sampled By: Brian Scott Chemistry Parameters we raxrdrta 01AC 53111 MEtlb an Jr111111 DE MDL ML At= At daw ax litotes Chemical Oxygen Demand^ 10 mg/L 1 10 10 8FISM3 SM 5220D-1997 06118/18 17:15 MKS Total SuspurdedSOWS ^ 71 mg/L 2.66 7.1 7.1 8F13001 SM254OD-1997 06/13/1807:44 LBG Description: Outfall #58 Lab Sample ID:CA18914-02 Received: 06/12/18 11:50 Matrix, water Sampled: 06/12/18 08:00 Work Order: CA18914 Project: Uwharrie Stormwater Sampled By:8rlan Scott Classical Chemistry Parameters ^ -a QrVew Auaam"JAC s711 Anahn rCAS Numberl $aka an un"s DE RM ML astb Method Analyzed a>1 tlote>L Chemical Oxygen Demand- 10 u mq/L 1 10 10 BF1BW3 SM 522OD-1997 06/18/18 17:1S MILS Total Suspended Solids^ 2.8 mg/L 1 2.5 2.5 8F13001 SM 254OD-1997 06/13/18 07:44 LBG Description: Outfall :97B Lab Sample ID:CA18914-03 Received: 06/12/18 11:50 Matrix: water Sampled:06/12118 08:35 Work Order: CA18914 Project: Uwha►rie Stormwater Sampled By, Brian Scott Classical Chemistry Parameters J ^ - &= iirYcerorfad+hMss let' 5911 Beattie an 211lb Of Ku EDL Alto 68ahl1,ed act man Chemical Oxygen Demand^ L0 U mg/L 1 10 10 8F18003 SM 522OD-1997 06/18/18 17:15 MKS pH^ 618 pH 1' 1.0 1.0 8F18035 iM 4500H+B•200( 06/18/18 1S45 ASC Q•01 Tunperaturs for pH (deg. C) 23 pH I 8FIB035 W 45WH+O.2000 06/18/18 15:45 ASC W Total Suspended Solids- 3.6 mglL 1 2.5 2.5 SF13001 SM 2540D 1997 06/13/18 07;44 LOG Classical Chemistry Parameters Anatvte FCAS Number, 8lnulb Elab I3111 DE tiQl EQL AAU& Mtthgd Aubmad ax ihibu Oil a Greece (HEM) (C-00071 cas mg/L 1 2.40 5.00 SF19012 EPA 1664A 06/21/18 14:25 SMA FMAL ThIS report rdlilft anN to Uw simple as received W the Wboratm, arO may 0" be reproduced M full. I Page 4 of 9 www.enoolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control SAW) BPLIi I - NO PIREP Blank (BF13001-BLK1) Prepared 8 Analyzed: o6/1312018 07:44 Spike Source %REC RPD ArUdM Result Flea POL UnRa Level B19fL1t %REC i MBA RPD Lm11 Hill= Total Susperxkd Solids 2.5 U 2.5 rnWL US (8F13001-BSI) Prepared 6 Analyzed: 06/13/2018 07:44 Spike Source %REC RPD .Anobft Resat FIN PM WAS Loral giliffig %REC Limb RPD LIMA notes Total Suspended Solids 91 2.5 mg/L 100 91 80.120 Duplks6e (BF13001-DUPl) Prepared 9 Analyzed; 0613312018 07.44 Source: C8063111"I Spike Source %REC RPD Analvte Read Flan POL Units Lave! gpay(t %REC Llmita RPD Limit mates. Total Suspended Solids 1100 120 mg1L 1300 15 20 Duplicate (8F13001-DUP2) Prepared 5 Analyzed: 06113/2018 07:44 Source: CB07171-01 Spike Source %REC RPD AnaWW Result Flap POL unit$ Laval Rams %REC LSm" RPD L18111 Total Suspended Solids 110 100 mg1L 110 4 20 8e1dr SP $OM - Some Blank (BF18003-BLKl) Prepared: 06118)2018 14:30 Analyzed: 06/18/2018 1715 Spike Source %REC RPD ADLhf18 E6wift Film MI. Unibf Level Spay$ %REC Limits RPD U w1 nOLEs- Chemical Oxygen Demand 10 U 10 mg/L LCS (018003-857) Prepared: 06/18/2018 14:30 Analyzed: 06/10/2018 17:15 Spike Source %REC RPD Analvin Resat Flea POL UnRs Larval Result %REC Um(v RPD "M11 112MIL. Chemlcai Oxygen Remand 500 10 mg1L 500 100 90.110 Matrix Spike (BF18003-M51) Prepared: 06/18/2018 14;30 Analyzed: 06/1812018 17:15 Source: C507235.02 Spike Source %REC RPD AnaWN Result Flat POL Units Loved &MM %REC UMIM RPO Limit tlarai Chemicai Oxygen Demand 560 10 mg1L 526 34 100 90-110 Matrix Spike Dup (BF18003-M501) Prepared: 06/18/2016 14:30 Analyzed: 06/18/2018 17:15 Source: CB0723"2 Spike Source %REC RPD .ADabft R=& Elan ROL Unite Level Resu1t 96REC Lbrjm RpD Lim11 SY4tes Chemical Oxygen Demand 560 10 mg1L 526 34 99 90-110 0.8 10 seed$ &$Iowa - NO PRAP LCS (BF18035-BSL) Prepared a Analyzed: 06/18/2018 15:45 Spike Source %REC RPD Analvta Result Fiao POL Units Loved moult %REC UM, RPD Limp n21CL PH 7A 1.0 pH 7,01 100 99.101 FINAL This report relates only to the sample as received W We aooremrv, eon may only ha reproEurcd In M. Page 5 of 9 www.encolobs.com QUALM CONTROL DATA Classical Chemistry Parameters - Quality Control BA" SMASI 3 - NO PIRFP - CDOW raed Duplicate (81`18035-DUP1) Prepared a Analyzed; 06/18/2018 15:45 Sourca-CA18914-03 spike Source %REC RPD ArUdVto RCPM Flee POL Urdu Laval Be" %REC Limju RPD Limit Notai pH 6.7 1.0 pH 6.8 0.7 25 Classical Chemistry Parameters - Quality Control DoWft M0012 - ZPA 11048 Bwank (8F19012-8LK1) Prepared' 0609/2018 16:35 Analyzed: 06/21/2018 14:25 Spike Source %REC RPD Analvta Base no em WAS Laval B= t %REC Limia RPD Limit Notes. Oil 9 Grease (HEM) 2.40 11 5.00 mg1L LCS (8P19012-11Si) Prepared: 06119l2018 16:35 Analyzed: 06/21/2010 14:25 Spike Source %REC RPD emllde Result Elaa Pa units Laval go" %REC Limits RPD am Now Oil d Grease (HEM) 155 5.00 mg1L 159 97 78.114 I.CS Dup (8F19012.BSD1) Prepared: 06/19/2018 16:35 Analyzed: 06/21/2018 14:25 Spike Source %REC RPD Analvte Result FLN POL Unho Ltvai SMUM %REC UMJW RPD Limit Home 011 IN Grease (HEM) 165 5.00 mglL 161 103 78.114 7 18 Matrix Spike (8F19012-1431) Prepared: 06/19/2018 16:35 Analyzed: 06/21/2018 14:25 Source: 600273"1 Spike Sours %REC Apo Anelvia Reeldt Flap POL Units Level gftwft %REC Ljm(ts RPD Limit now Diu & Grease (HEM) 165 5.00 mg/L 177 2.40 U 93 78.114 F1wa TMs nWart relates only to the samda Al recerred by the laboratory, &W nw any W reproduced �n full. IPage 6 of 9 www.encolobs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit, The PQL presented Is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative Identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q-01 Analysis performed outside of method - specified holding time. FINAL Trds report reMtes only to the sample as recehmd by me laboratory, and may oral be rrepeduxed In fug. Page 7 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com D 10775 central sort 0, 4810 E2=mw Pork Coma Siae 111 1@.A 1Yoodorrds UX"nat Cl Orhn6o R 329A4 Juksdsrila, 91 37216.600 Cary. NC 2751 F L 44071 SM5314 Far 4407) E50-6945 19041 2%-3007 Fa. r9O4t 296-W t0 {9191 467.3090 F.- 19i91 467.3515 Page.Of l _� Samsva hA Prr-,. wd Or 0x t Da;B'Tsne ft "K 'w d 9 04 'Vora 1' f iz ..,� ntySper:•x' Pfflxerq Pr m.nrra -.1 '♦ - - - ,nrq P.r -- -- __:tea P1tC I" IkrxemW Rr k arsiirre '13 �r,.y,rs�++nFh — rr.•n:r-r 'q;n, AS. 0] { Gaoler rS 6{{ Tgmp. r 9e[eps �) ,}-�� ` 1 ,, Gflridrtiy, lipen Hefrtlr O � l J w C^ Acceptable UnacceptabEe liGw Cuorm7�arar SO -Sao OW *,-g wur SE,Sodmwt SW.Swtm*waer Ww.Wa*fr m#ar A -A, 0 Omar(irW-n carsrrwft) vrwrwtbn: I�" H-kc; Na04M S.Wsoe N044eOH 00trrm Idoua. conrnwmj We A9 sam0les scoff~ to ENCO Labs are ,n ecco,wnce r,me OW terms and condAmm eslec on Me rawrst o1 mu torm, �niesa pnW *man apreenwMh eras! Sample Preservation Verification _ ENCO Cary Work Order: CA18914 Project: Uwharrie Stormwater Client: Republic Services of NC (RE014) Project it: [none] Logged In: 12-Jun-18 12.00 Logged By. Rachel Ann Yonish Preservation Check Performed By: Uz. DatelTimeA L?k12,1 t Y jZJI] CA18914-01 ���i'`wJ _�. ____—_JIJf'S.'�hs�''.�4.L •.i},�,y.��:.�x.�il_ � _....�_._-..._-�AY�.� 1 `:�-1..."fLY..� V�.�..rY-�_ ' • CA18914-02 gent Use 8 "250MLP+H2SO4 <2 Y N 1 NA I Y I& 1 NA CA18914-03 n Reagent Name ID 1� 21 I I PH Strip ID: p}1Strips C7i4620 C:lelmnt\Priru%wxo PreservationCheck.rpt Reagent Name ID 3 41 1 d Reagent Name ID 5 fi Page 9 of 9 age o 1 1!2C6Ana1jfta1* ewwpam" com June 14, 2018 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: CA18914 Pace Project No.: 92388048 Pace Analytical Services, LLC 9800 Kincey Ave. Surle 100 Huntersvilie. NC 28078 (7041875.8092 Dear Ms. Franz: Enclosed are the analytical results for sample(s) received by the laboratory on June 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please f eel free to contact me. Sincerely, OL ` 1. ►ate Angela Baioni angela.baioni@ pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 11 aceAnalytrcal• wwr.Asesd4s com Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersviile, NC 28078 (7041875.9092 CERTIFICATIONS Project: CA18914 Pace Project No.: 92388048 Raleigh Certification Me 6701 Conference Drive, Raleigh, NC 27807 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #, 67 North Caroline Drinking Water Certificallon #: 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written oorrient of Pace Analytical Services, LLC, Page 2 of 11 aceAnalyticale wwwpaomMDscam SAMPLE ANALYTE COUNT Project: CA18914 Pace Project No.: 92388D48 Pace Analytical Services, LLC 9800 Klncey Ave. Suite 10D Wuntersvitle, NC 28078 (704}875.9092 Analysts Lab ID Sample ID Method Analysts Reported Laboratory 9238804=1 Outtal1 62 SM 9222D DJB 1 PASi-R 92388048002 Duthill /ISB SM 9222D DJB 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in lull, Without the written consent of Pace Analytical Services, I.I.C. Page 3 of 11 aceAnalytical• ANALYTICAL RESULTS Project; CA 18914 Pace Project No.: 92388048 Pace Analytical Services, LLC 9800 KInCey Ave. Suite 100 Huntersvilie, NC 28079 i704je75.9M2 Sample: Outfall /2 Lob ID: 9238SM001 Collected: 06/12/18 08:20 Received: 08112/18 13:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Focal Coliform RAL Analytical Method: SM 9222D Feral Coliforms 6.0 CFU1100 mL 2.0 2 06/12/18 15:59 ul REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 08/14/2018 11:33 AM without the written consent of Pace Analytical Servlcus, LLC. Page 4 of 11 1�;IalceAnaljftal* wawpsab&&CD n ANALYTICAL RESULTS Project: CA18914 Pace Project No.: 92386048 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 2BD78 17041875-WO2 Sample: Outfall 05B Lab ID: 92388048002 Collected: 06/12118 08:00 Received: 06112/1813:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Collform RAL Analytical MethDd: SM 92220 Fecal Coliforms 400 CFU1100 mL 1.0 1 06112/1815:59 u1 Date: 06/1412018 11:33 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, without the written Consent of Pero Analytical Services, I.I.C. Page 5 of 11 aceAnallyticale WWWP cMW .COM Project: CA18914 Pace Project No.: 92388048 OC Batch: 415176 OC Batch Method: SM 9222D Associated Lab Samples: 92388048001, 92388048002 METHOD BLANK: 2302285 Associated Lab Samples: 92388048001, 92388048002 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 92220 Analysis Description: 92220 MBIO Fecal Collform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 06112118 15:59 SAMPLE DUPLICATE: 2302267 92388156001 Dup Parameter Units Result Result RPD Qualifiers Fecal Collforms CFU1100 mL ND 40.0 u1 Pace Analytical Services. LLC 9800 Kincey Ave. Sufte 100 Hunteraville, NC 2BO76 (704►8759092 Results presented on this page are Ir the unfta Indkatad by the "UnKs' column except Wren an aeemate w th presented n the npM d the result, REPORT OF LABORATORY ANALYSIS This report $hall not he reproduced, except In ful, Date: 06H 412018 11:33 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 11 Pace Analytical Services, LLC �p d �� /+f 9800 Kincey Ave. SuAe 100 N�+G /7++ Vita Huntersvllle, NC 28078 WWWpwarabseom (704)875-WW2 QUALIFIERS Project: CA18914 Pace Project No.: 92388048 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit, RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPO values. LCS(D) - Laboratory Control Sample (DupliGate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 ChloroethyhAnyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrytonitrile by EPA Method 8260. N-Nitrosodiphenylemine decomposes and cannot be separated from Diphenylemine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS ut Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/14/2018 1113 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 11 aceAnaVical ~pscslabLoom Project, CA18914 Pecs Project No.: 92388048 Lab iD Sample ID 92388049001 Outfail i2 92388048002 Outfall *58 Date: 06114/2018 11:33 AM Pace Analytical Sorvlces, LLC 9800 Kincey Ave. Sure 100 Huntersville, NC 28078 (704)575.9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE QC Batch Method QC Batch Analytical Method SM 9222D 415176 SM 9222D 415176 REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Anslytical Semicas, LLC. Analytical Batch Page a of 11 t Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersvllle ❑ Raleigh Mechanicsville[] ClientNeme: W0# : 92388048 Project #.. Courier, Pace r G]UPS USPSCflant commercial ��Itter 9238 048 Custody Sad Present? Dyes ffVo Seals Intact? ❑Yes XNn Oate/Innialt Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags [16oie ❑ otner Biological Tissue Frozen? Tharmomelart �1 ❑Yes ❑No �N/A Gun ID: Type of Ice: wet []Blue j,]None Cooler Temp ('C): jL4 Correction Factor: Add btne I'CJ a Cooler Tamp Curetted ('C): a �- Temp should be above freezing to VC ❑Samples out of temp crlterh.5amp1es un fee, cnnlutR process has teen USDA Regulated Sail (A N/A, water sample) Did samples orrjll]ate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a !oraign source [fnternat+nnally, 11Yes indudlnahaxniiand Puerto Rical?f—lYas 12No CammanL/Oiscra an Chain of Custody Present? uElflo N/A I . Sam le$ Arrived within Hold Tirne? Y _QNo ONIA 2- Short Hold TimeAnatysh 42hr.)? Yu Na clatlA 3. Rush Turn Around Time Requested? OY, CIN., 0.1A 4. Sufficient Volume? t Nq CJIVA 5, CorrvoContainarsUsed? ContaloarsUsed? Y ON j„ re, ❑No ON/A ONIA 6, �--Pace �I Containers Intnt? �Y. ar ONO 0,41A 7. lys{s: Samples Field F1itered7 No IA 8, Match COC7 rfatolme/ID/ArialyxisMatrix: es ❑No �d QN/A 9. Heads aco in VOA Vials >S•bmm 7 QYES ONO N/A 10, Trip Blank Present? Trip Blank cLatocy Seals Present? ©Yu C]No DOS ONO N/A N/A 11. COMMENTS/SAMPU: DISCREPANCY Cot ID of split containers; CLIENT NOTIFICATION/RESOLUTION ,Person contacted: Date/Time: Project Manager SCURF Review, Protect Manager SAF Ravlew: M Field Data Required? ❑Yes ❑No yy��' Data: /—( �,]� l QU Data: V •-a ' y U Page 9 of 1 t Document Name: Document Revised: February 7, 2018 Sample Condition Upon Racelpt(SCUR) Page 1 of 2 I ��• i _ _DocumentNo.t ` Issuing Authority_+, *Check mark top half of box If ph and/or dechiorination Is verified and within the acceptance range for preservation samples. Excepdans: VOA, CoRfornt TOC oil and Grease, 0110/9015 (water) DOC LJIS "Bottom half of box Is to list number of bottle Project WOW 92388048 PM., AKB Due Dale: 06/21/18 CLIENT: 92-ENCO rl i ry I N x C G C un p ZZ sL w a Q 2 p I Y p� ? 7 a; r Y j ! a 4 1 I I x 8 I d r.� pb 0.0 IL E rya yry� L 5 uo�7 a CE E > I s E G SEE pC Itll ppE p� .9 m m d i t ` y I,1 _ I i 1 f�� ` _I 4 N\4- I ♦ \ 5 IN 11 I� 8 � I _ f I D I �t 1 12 pH Adjustment Log for Preserved Samples Sample IB Type of Vresrrvativo pH upon receipt oats preservation adjusted Time 9resarvation i amount of Pteservattve lot N adiusted E added Note: Nhanever there is a discrepancy affecting +north Carolina compliance sample, a copy of this form will be sent to t." Narth Carolina DEHHR COMMcaricn Of9ce ;1.e, Out of hold, Incattect preservative, out of Lamp, incorrect cnntarnen. i� Page 10 of 11 SUBCONTRACT ORDER ENCO Cary CA18914 �1`t�mG J.ABOBATORY: ENCO Cary Tri-Test (Raleigh) 102-A Woodwinds Industrial Court 6701 Conference Drive Cary, NC 27511 Raleigh, NC 27607 Phone: 919.467.3090 Phone :(919) 834-4984 Fax: 919.467.3515 Fax: Project Manager: Stephanie Franz Project State of Origin: North Carolina Sub Lab ILD Originating Lab ID client RINME Dots Sampled Sample Comments Outrall 102 Water 124un-t8 o8,10 �r '�J �' (� C CC Caiifonn, Fecal 9223E 19-Jun-18 15:00 12-Jun-18 16:15 Containers Supplied: Sterite250m1.PrN8hio(C) u ID Ori hating Clleat Matrix Date Sampled Sam lecommeats Outrall #58 Water I2-Jun-18 011:00 Colifotm. Focal9223B 19-Jun-18 15.00 12-Jun-18 15:55 Containers Supplied: Steritc250rnLP+Na1'hio (C) (1101 V � � 61,ZI1Y q-)`� Relewal By Datc Melied By Datc Page 1poe9 11 of 11 i Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted W19/17, CERTIFICATE OF COVERAGE NO. NCG120051 FACILrrY NAME _Uwharrie Environmental COUNTY _Montgomery PERSON COLLECTING SAMPLES _Brian Scutt LABORATORY__ENCO Labs _ Lab CerL # _CA08283 Comments an sample collection or analysis: SAMPLE COLLECTION YEAR _2017 SAMPLE PERIOD ❑ Jan -June X July -Dec or ❑ Monthly' month Df ISCFIARGING TO CLASS ❑ORW ❑HQW - ❑Trout ❑PNA E❑zero flow ❑Water supply 0sA VED X JAN a,S 2018 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 8 IM OR D�p4 ETION Part A: Stormwater Benchmarks and Monitoring Results '* OCESSING UNIT n No discharge this neriod?2 Outran No. Date Sample Collected imo/dd/gr) 24-hour rainfall amount, Inches Chemical oxygen Demand Fecal Collform Total Suspended Solids Benchmarks => _ - 120 mg/L 1000 count per 1W mL 1W mg/L or s0 mg/L 1 No Discharge 2 No Discharge 5B 12/6/17 Y 10 56 2.5 68 No Discharge 7A No Discharge 7C No Discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfa11, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PM Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format '<XX mgLV. where )0(is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as'>W. Note: if you report a sample value In excess of the benchmark, you must Implement Tier 1, Tler 4 or Tier 3 responses. See General Permit text. Permit Date: 11/l/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount Inches Non -polar 08G f M by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks -=a _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 - 9.0 SU 7B No Discharge Footnotes from Part A also apply to this Part B Note: 1f you repart a sample value In excess of the benchmark, you roust implement ter 1, Tier Z or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION I • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coav of this DMR indudina all "No Dischame'reoorM witbin 30 days of receipt of the lab results for at end of monitodna period in the case of No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION_ FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that thge are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 4; CO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919,467.3319 Friday, December 15, 2017 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 RE: Laboratory Resullts for Project Number: [none], Project Name/Desc: Uwharrle Stormwater ENCO Workorder(s): CA08283 Dear Brian Scott, Enclosed Is a copy of your laboratory report for test samples received by our laboratory on Wednesday, December 6, 2017. Unless otherwise noted In an attached project narrative, all samples were received in acceptable condltlon and processed In accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith For Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as reoetved by the laboratory, and may only be reproduced in foil. Page 1 of a www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OuM11 # 8B Lab ID: CA08283-01 Sampled: 12/06/17 07.50 Received: 12/06/17 11:30 Param g914 Dabal7imefsl Pin Detelllmefsl Colllert 18 12/06/17 15:45 12/07/17 12:43 12/06/17 14:39 12/07/17 11:16 SM 254OD-1997 W13/17 12/12/17 14:45 12112J17 14:45 SM 522DD-1997 01/03/18 12/08/17 12:19 12/06/17 16:25 FIM This report relates only to the sample as reoelved by the laboratory, and may only be reproduced In full. Pape 2 at 8 www.encolabo.com SAMPLE DETECr1ON SUMMARY Ca vt il): nutlell 4, 88 Lab 901 CA08283-01 ADWM Smlum Flan sm F. L V= m It!!�E Collform, Fetal 56 1.0 1.0 MPN/100 mL Colllert 18 Total Suspended Solids 2.5 2.5 2.5 mg/L SM 254OD-1997 This report relates only to the sample as moaNad by the laboratory, and may only be reproduced In full. Page 3 of 9 rrlur� I � www.encolabs.com ANALYTICAL RESULTS Description: Outfall # 5B Lab Sample ID:CA08283-01 Received: 12/06/17 11:30 Matrbc: Water Sampled:12/06/17 07:50 work Order: CA08283 Project: Uwharrie Stormwater Sampled By: Brian Soott Classlcal Chemistry Parameters ^ • fhW Cary crrrdlyd aralyte [AC SYJJ Angq f LC.0 Number] A11 nu Elsa Mau RE hin E" Batch tlathod Anahmed j{y Notm Chemical Oxygen []errand^ 10 u mg/L 1 10 10 7LO8025 SM 5220p-1997 12/08/17 16:25 30C Total Suspended Solid9A 2.3 mg/L 1 2.5 2.5 71.12010 SM 25400-1997 1412/17 14:45 OMR Microbiological Parameters - SW Cary analyte IAC 39t1 Anelyte FQW Number] Emum Elm yob QE Eu Affl&12 Njptho Anghmad By J!� Cogrortn, Fecal^ 85 MPN/100 mL 1 1.0 7LO7036 Colilert 18 12/07/17 11:16 MKS FINAL Th}e report relate only to the sample as receNed by the laboratory, and may only be reproduced in full. Page 4 of 8 www.eneniabs.com QUALITY CONTROL DATA Classical Chemistry Parameters -Quality Control Batch 7LMO25 - Same Blank (7LOS023-BLK1) Prepared: 12/08/2017 12:19 Analyzed: 12/08/2017 16:25 Spike Source %REC RPD .Analrte Result Flan POL Units Level Boma 9bREC Limits RPD LM Nobas Chemical Oxygen Demand 10 U 10 mg/L LCS (7405025-BS1) Prepared: 12/08/2017 12:19 Analyzed: 12/08/2017 160 Spike Source %REC RPD Aeanda Result Flan POL Units Leval Sit %REC Limits RPD Llmlt doles. Chemical Oxygen Demand 530 10 mg/L 500 102 90.110 Matr4r Spike (7L08025-MSI) Prepared: 12/08/2017 12:19 Anal: 12/08/2017 16:25 Source:CA08178-02 Spike Source %REC RPD Ana hd:e Result EIaY POL Units Level gallk %REC Limits RPD Lich notes Chemical Oxygen Demand 540 10 mg/L 526 10 U 103 90.110 Matrix Spike Dup (7LO8025-10119Di) Prepared: 12/00/2017 12:19 Analyzed: 12/08/2017 16:25 x Source:CA08178-02 Spike Source %REC RPD Anahrte Result Flea POL Units Level Result %REC L" RPD Lllnit notes Chemical Oxygen Demand 530 10 mg/L 526 SOU 102 90-110 1 10 Batab M12010 - NO PREP Blank (7L1201O-BLK1) Prepared dk Analyzed: 12/1212017 14:45 Spike Source %REC RPD .Anat94e Result Flan POL units Level gMMg %REC UMMI RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7L1201O-BS1) Prepared 9 Analyzed: 12/12/2017 14:45 Spike Source %REC RPD Anahlte Result Fiat POL Units Level Result %REC NGUM RPD LLMll Notes_ Total Suspended Solids 110 2.5 mg/L 100 106 80.120 Duplicate (7L12010-11111.01111) Prepared 8. Analyzed: 12/12/2017 14:45 Source: CA16549-01 Spike Source %REC RPD .Anahrto Result FIaO POL Units Level Result %REC Llmlts RPD Limit Mgm Total Suspended Solids 1900 170 mg/L 2300 18 20 Duplicate (7L12010-DU112) Prepared la Analyzed: 12/12/2017 14:45 Source: CA15594-01 Spike Source %REC RPD _Anahrta Result Flee POL units Level Reeuit %REC Llelts RPD Limlt Netea- Total Suspended Solids 280 50 mg/L 260 7 20 mi cmblologlcal Parameters - Quality Control BaAdr 7L07036 - NO PREP Blank (7L07038-BLK3) Prepared: 12/06/2017 16:11 Analyzed: 12/07/2017 11:16 Spike Source %REC RPD AnalM Result Fin POL Units Level ggsy[t %REC Limb RPD LEmg notes_ Colifomm, Fecal 1.0 U 1.0 MPN/100 mL FINAL This report rdates only to the temple as reneWM by era laboratory, and may only be reproduced In full. Page 5 or a www.encolobs.com QUALITY CONTROL DATA l+tlrroblok*glcal Parameters - Quality Control Bald* 7LO7936 - NO PREP - Condnued Duplkatte (71.07036-DUPi) Prepared: 12/06/2017 14:39 Anayzed: 12/07/2017 11:16 Source: CAOBZ83-01 Spike Source %REC RPD Anahts Roult Flan Poll. Units level RW %REC Lkab RPD LIM Ngftj Collfom, Fecal 47 1.0 MPN/100 mL S6 16 2S Duplk M* (71.07036-DUP2) Prepared: 12/06/2017 16:11 Analyzed; 12/07/2017 11:16 Source: CA18464-01 Spike Source %REC RPD Anahte Result Flan POL Unita turret R"M %REC ltd UM RPD 11M !Hate'll Collform, Fecal 1.0 U 1.0 MPN/100 mL 110 U 25 FINAL This report relates only to the sample as mceVed by the laboratory, and may only be reproduced in rull. Pape 6 of 8 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value Is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and molsture content, where applicable. E The concentration Indicated for this analyte Is an estimated value above the calibration range of the Instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL Is roughly equivalent to the practical quantitatlon limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of Boll samples, moisture content. PQL PQL: Practical Quantitation Llmlt N The analysis Indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL ThW report relates only to the sample as reoehed by the laboratory, and may only be reproduced In full. page 7 or 8 -L11 eInV118MI"Is IIIL VVII.JIV "VAftI ffwII 'ILiVIIIS I%OVIIL�.j WII/1111'"VI-"VV.71s,sss r' r7L'VVe'7Y R A W.W1116VIOUZA MVI 16T15 Canllai Port Dr. 4810 Exeallire Park Court Sidle I I 1 tO2•A YVoodesaty ' Ct Orlando, FL 32B24 ,tadawnVllla, R, 322154M Cary. NC 27511 (407) &I&5314 Fax (.4M MD -GM 4904) Z* VV Raz (W4) M*.62tO (919) 467{MW Fax (919) 467-MI5 page of . 1 1 O*M Name - Pmpd Nwnbw .Repotted nnstran Requested.Tumaraund Times Note., Fash requests subod to Standard � Expedited Due J © N � v •Q it 0 O 11 CV U) CO Address 500 Landfil'Roae P Narneroesti Uwharrie St rmwater "ISTOP - W. Gilead MC 273M . PO 01 San info (<7// � b Alf S10 573-3897 Fair Report V C ftO Brian Scott $arrlpferls) . AffMaeon (Priru 6811n0 Carew Brian ScScottU) Samplerts) S' sae LoeabonI Time zone „ Ai --I•."'c C r.'L°� �''�` tab wOftrder CA482€33- - (s.. codes) [Coirdir+e asI>.�tam lfem s sampie ID (FW M k%Wd iMbm) CoRec ion oaaa CO➢GCtlon 'none camp► Grab MWX (see codes) -' Tptdf a Of Coruebren - Sample Comments / ft. % 7 7'PW WA g II # WA I B ©uftil4 ' WA .6 X X X X X OU&JllI WA 6 X X X X X. • I - Total # of Cordairlrars Sample iCit Prepared Br �1.� OafaJ1 me 5•'��-1 Relrrqu_.DW BY r p� i bit % �� �" � /Z Con--na sp-W Reponft Req m-wat yk By Datalrkrrer 1•taca+rrd BY - Coder n e Temps on Flawk-t COaln, Rs n AcceptaWe Unaoceptable MWI : GW-Grauodaoter SO-W UW-DM &g Water SE-S*&.eal SWSurtaca Water W W Wastevater A-11Ir O-MW (d" in comments) Preservation: Wco H-HCI N•HNW 5-H2504 NO-NaOM 04NMr (detail in comments) Has: AN samples Kkm; fad to EP= laW are In acowdance with Ow mmrs and torr25ans Rased an the rwmrse of to farm, urims prior written agreements ftW Sample Preservation Verification ENCo Cary Work Order: CA08283 Project: Uwharrie Stormwater Client: Republic Services of NC (RE014) Project #: (none] " Logged in: 06-Dec-17 11:43 Logged By: John C King Preservation Check Performed By: -" _ Datemme: .12 -(,47 ' 42c&a CA08283-01 Cont Type Pres (p ) • Requirement pH Cheeke I In Control ate ime pH Adjusted; Adiusted Reagent,Used/Comments B 250mLP+H2SO4 a2 I N I NA Y I I NA Reacient Name ID Reacient Name ID i 3 2 4 pH Strip ID: C 1-OT ZtJ CAELMN-RPrintlwko_PreservationCheck. rpt Reacent Name ID 5 _ 6 Page 1 c RECEIVED JUL 0 5 2017 CENTRAL FILES DWR SECTION Semi-annual Stormwater Dlscharse Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted 06/07/2017 CERTIFICATE OF COVERAGE NO. NCG220052 SAMPLE COLLECTION YEAR _2017 FACILITY NAME _Uwharrie Environmental SAMPLE PERIOD X Jan -June ❑ July -Dec COUNTY _Montgomery or ❑Monthly` !month) PERSON COLLECTING SAMPLES _Brian Scott DISCHARGING TO CLASS QORW ❑HQW ❑Trout ❑PNA LABORATORY_ENCO tabs_ Lab Cart.N_[AD8289 ❑Zero -flow ❑Water Supply []SA Comments on sample collection or analysis: X Other C Part A. Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 n No discharge this nerlodt2 Outfall No. Date Sample Collected' mo/dd 24-hour rainfall amount 1, Inches Chemical Oxygen Demand Fecal Coilform Total Suspended Solids Benchmarks 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 5123117 .4" 17 2100 53 2 5/23/17 A" 26 460 90 SB 5/23/17 .4" 10 480 23 6B 5/23/17 A' 24 200 29 7A No Discharge - - - - 7C No Discharge ' Monthly sampling (Instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' 5ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. Eor example. do not report Below Detection Limit, BDL, <PQL, Non -detect, No, or other similar non - numerical format. when results are below the applicable limits, thag Musl be reported In the format, "< " where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value In excess of the benchmark, you must implement Tler 2, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Permit Oate: 11/1/2012.10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 n No dlscharae this AerlodT Outfall No. Date Semple Collected Imo/dd/ r) 24-hour rainfall amount, Inches' Nan -polar O&G/WH by EPA 1664jSGf--HEM TartalSuspendedsolids pH Benchmark$ 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 sU 7B 5 23/17 .4" 2,40 10 7.4S Footnotes from Part A also apply to this Part B Note: If you report a sample value In excess of the benchmark, you roust implement Tier 1, Tier 2, or 77er 3 responses. See General permit tent. FOR PART A ANP PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL7 YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ No 0 REGIONAL OFFICE CONTACT NAME: Aftil an orlainal and one cavy of this QM& Indufta aff "No 01scharoll" Matts. within 30 days of recelar gf Ift iQb resufts for at end ofm0iqi&Waa period w reparts) to; Division of Water Quality Attw DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699.1617 "I certify, under penalty of law, that this document and all attachments were prepared under my diretCon or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am :=a significant penalties Far submitting false information, including the possibility of fines and imprisonment for knowing vialations." 6 a617 {Signature of Permlttee) )Date Permit Date: 11/1/2012-10/31/2027 SWU-24B, last revised 10/25/2012 Page 2 of 2 0 ENCO Laboraton"es Acarrete. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919."7.3515 Wednesday, May 31, 2017 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Uwharrie Stormwater ENCO Workorder(s): CA08289 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, May 23, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained In this report are In compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary, Data from outside organizations will be reported under separate cover. If you have any questions or require further Information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received try the laboratory, and may only be reproduced in full. Page 1 of 9 ' ' NiliM Swj www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall #1 Lab I0: CA08289-01 Sampled: 05123/ 17 08.45 Received: 05/23/17 12:25 page SM 2540D-1997 Hold DatelTlme(s) 05/30/17 Prep Date/Tlmefs) 05/26/17 Analysis Date/Time(s) 15:55 05/26/17 15:55 SM 5220D-1997 06/20/17 05/26/17 10:54 05/26/17 17:12 Client I0: Outfall #2 Lab ID: CA08209-02 Sampled: 05/23/17 09:00 Received: 05/23/17 12:25 parameter SM 2540D-1997 Hold DabalTime(s) 05/30/17 pin DatelTlme(s) 05/26/17 Analysis Date/Time(s) 15:55 05/26/17 15:55 SM 5220D•1997 06/20/17 05/26/17 10:54 05/26/17 17:12 Client ID: Outfall#SB Lab ID: CA08289-03 Sampled: 05/23/17 08:30 Received: 05/23/17 12:25 Parameter SM 254OD-1997 Hold Dateinme(s) 05/30/17 Pr,O Date/Time(s) 05/26/17 Analysis DatelTime(s) 15:55 05/26/17 15:55 SM 5220D-1997 06/20/17 05/26/17 10:54 05/26/17 17:12 CllentID: Outfall#6B Lab ID: CA08289-04 Sampled: 05/23/17 09:10 Received: 05/23/17 12:25 Baramete SM 25OD-1997 ROJd DatelTime(s) 05/30/17 Prep Date/Time(s) 05/26/17 Analvsls DatelTlme(s) 15:55 0$/26/17 15:55 SM 52200-1997 06/20/17 05/26/17 10:54 05/26/17 17:12 CllentID: Outfall#7B Lab ID: CA08289-05 Sampled: 05/23/17 09:20 Received: 05/23/17 12:25 Paramete EPA 1664A Hold Data/Tlme(s) 06120/17 Prep Date/Timefs) 05/24/17 Analvsls DatelTime(s) 18:16 05/26/17 16:31 SM 2540D-1997 05/30/17 05/26/17 15:55 05/26/17 15:55 SM 4500H+B-2000 05/23/17 09:34 05/31/17 14:10 05/31/17 14:10 5M 5220D-1997 06/20/17 05/26/17 10:54 05/26/17 17:12 FINAL This report reWtes only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 0f 9 ' �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 01 lab ID: CA08289-01 AEII!lll� Results EI29 Hu R" llulM Method Notes Chemical Oxygen Demand 17 10 10 mg/L SM 522OD-1997 Total Suspended Solids 53 17 17 mg/L SM 254OD-1997 Client 1D: Outfall #2 Lab ED: CA08289-02 Ana BCilllti an Hu E" Lnita Method Notes Chemical Oxygen Demand 26 10 10 mg/L SM 5220D-1997 Total Suspended Solids 90 21 21 mg/L SM 2540D-1997 Client ED. Outfall *56 Lab ED: CA08289-03 A0 Results Elm 11" E9L 9111ls MNotes Total Sus nded Solids 23 10 10 mg/L SM 254OD-1997 Client 10: Outfall #613 Lab ID: CA08289-04 A11911f170 Roulta EIH9 MQL E" ll0ltri Method Notes Chemical Oxygen Demand 24 10 10 mg/L SM 5220D-1997 Total Suspended Solids 29 510 5.0 mg/L SM 254OD•1997 Client ID: Outfall #7B Lab ID: CA08289-CS Anal YC® BrAults Ela9 Hu E" Mobs Method haul pH 6.4 1.0 1.0 pH SM 4500H+B-2000 Q-01 Total Suspended Solids 10 5.6 5.6 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 0f 9 r www.encolabs.com ANALYTICAL RESULTS Description: Outfall #1 Lab Sample ID:CA08289.01 Received: 05/23/17 12:25 Matrix: Water Sampled:05123/17 08:45 Work Order: CA08289 Project: Uwharrie Stormwater Sampled By: Brian Scott Classical Chemistry Parameters ^ - EMU Cary cartifled am6 to [AC 5911 Analyte fCAS Numberl Hall= flag MOW QF MDL 1 L ARIK i MethAnalysed By 12to Chemical Oxygen Demand^ 17 mg1L 1 10 10 7E26010 SM 5220D-1997 05/26/17 17:12 30C Total Suspended Solids^ 53 mg/L 6.67 17 17 7E26012 SM 254OD-1997 05/26/17 15:55 OMR Description: Outfall #2 Lab Sample IDCA08289-02 Received: 05/23/17 12:25 Matrix: Water Sampled:05/23/17 09:00 Work Order: CA08289 Project: Uwharrle Stormwater Sampled By: Brian Scott Classical Chemistry Parameters ^ - EACO mry [crd81°d anaryra IAC 5911 Analvte rCAS Numberl Results f[02 Units RE MU 241. Aw&h Method Analyzed 1!x 1�4t1&9 Chemical Oxygen Demand^ 26 mg/L 1 10 10 7E26030 SM 522OD-1997 05/26/17 17:12 ]OC Total Suspended Solids^ 90 mg/L 8.33 21 21 7E26012 SM 2540D-1997 05/26/17 15:55 OMR Description: Outfall #56 Lab Sample ID:CADS289-03 Received: 05/23/17 12:25 Matrix: Water Sampled:05/23/17 08:30 Work Order: CA082B9 Project Uwharrie Stormwater Sampled By:Brian Scott (Classical Chemistry Parameters ^- EACOCaryy[AC 5911 Analrte fCAS Numberl gesp1 flag ypltg 2E MQL P4L "Wh Method Analyzed @Y Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7E26010 SM 5220D-1997 05/26/17 17:12 ]OC Total Suspended SolldsA 23 mg/L 4 10 10 7E26012 SM 254OD-1997 05/26/17 15:55 OMR Description: Outfall #6B Lab Sample ID:CAOB289-04 Received: 05/23/17 12:25 Matrix: Water Sampled:05/23/17 09:10 Work Order: CA08289 Project: Uwharrie Stormwater Sampled By: Brian Scott Classical Chemistry Parameters Entiro ca yc"Aed analyte [AC 5911 hailIvte [CAS Numbed 926= flag !nits DE MDL E L llatrh M&Olyz 111 (>1gLC,q Chemical Oxygen Demand^ 24 mg/L 1 10 10 7E26010 SM 522OD-1997 05/26/17 17:12 30C Total Suspended SolldsA 29 mg/L 2 5.0 5.0 7E26012 SM 254OD-1997 05/26/17 15:55 OMR Descrlptlon: Outfall #7B Lab Sample ID:CA08289-05 Received: 05/23/17 12:25 Matrix: Water Sampled:05/23/17 09:20 Work Order: CA08289 Project: Uwharrie Stormwater Sampled By: Brian Scott Classical Chemistry Parameters ^ - EACO Cbry crrMAndh-W (AC 5911 Analyte fCAS Numbed $esu[ja flag ll= ➢E M" 12L Batch Method Analyzed Ill Notes Chemical Oxygen Demand^ 10 U mg/L 1 10 10 7E26010 SM 5220D-1997 05/26/17 17:12 30C pHA 6.4 pH 1 1.0 1.0 7E31011 SM 4500H+8-200C 05/31/17 14:10 ASC Q-01 Total Suspended Solids^ 10 mg/L 2.22 5.6 5.6 7E26012 SM 254OD-1997 05/26/17 15:55 OMR Classical Chemistry Parameters 801.111111 flaa 11n1ts Of MQL PQL atch Method Analaw 91 Butts Oil & Grease (HEM) [C-DD07] 2.40 U mg/L 1 2.40 5.00 7E24013 EPA 1664A 05/26/17 16:31 SMA FINAL This report relates only to the sample as received by the laboratory, and may onN be reproduced In full. Page 4 0f J Ce NSco www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7E26010 - Same Blank (7E26010-BLK1) Prepared: 05/26/2017 10:54 Analyzed: 05/26/2017 17:12 Spike Source %REC RPD Anal Remit Elan POL units Level RCSLIt %REC Llmita RPD 1IM11 Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7E26010-BS3) Prepared: 05/26/2017 10:54 Analyzed: 05/26/2017 17:12 Spike Source %REC RPD .Analvto Result Flao POL Units Level Resu1%REC LimlRPD Limp Hotel Chemical Oxygen Demand 500 10 mg/L 500 100 90.110 Matrix Spike (7E26010-MS3) Prepared: 05/26/2017 10:54 Analyzed: 05/26/2017 17:12 Source: CA00231-01 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result %REC Limits RPD Limit dates Chemical Oxygen Demand 1400 20 mg/L 1000 430 97 90-110 Matrix Spike Dup (7E26010-MSDI) Prepared: 05/26/2017 10:54 Analyzed: 05/26/2017 17:12 Source: CA00231-01 Spike Source %REC RPD .AnalYte Result Flaa POL Units Level Result %REC LiMb RPD Llmlt Notes Chemical Oxygen Demand 1400 20 mg/L 1000 430 97 90-110 0.3 10 Batch 7E26011- NO PREP Blank (7E26012-BLK1) Prepared & Analyzed: 05/26/2017 15:55 Spike Source %REC RPD .Analrte Result Flap POL Units Level Result %REC Limits RPD Limit Noel Total Suspended Solids 2.5 U 2,5 mg/L LCS (7E26012-BSI) Prepared & Analyzed: 05/26/2017 15:55 Spike Source %REC RPD _AnWVte Result Flan POL Units Level Resul! %REC Limits RPD LM Notes Total Suspended Solids 100 2.5 mg/L 100 101 80-120 Duplicate (7E26012-DUP1) Prepared & Analyzed: 05/26/2017 15:55 Source: CA04424-01 Spike Source %REC RPD .AnidYte Result Flan PAL Uq(is Level Result %REC LJMUfi RPD = t Notes Total Suspended Solids 7000 500 mg/L 6400 10 20 Duplicate (7E26012-DUP2) Prepared & Analyzed: 05/2612017 15:55 Source: CA06428-01 Spike Source %REC RPD .AnalYte R" Flan P-01 unite Level Result %REC Llulits RPD Limit dotes Total Suspended Solids 240 31 mg/L 270 9 20 Batch 7E31011 - NO PREP LCS (7E31011-BSI) Prepared & Analyzed: 05/31/2017 14:10 Spike Source %REC RPD _AnalYte Result Elm eon Units Level Result %REC Lima RPD Limp dotes PH 7.0 1.0 pH 6.98 100 99.101 FINAL This report relates only to the sample as recelved by the laboratory, and may only be reproduced In cull. Page 5 0 J Ce www.encolahs.com QUALITY CONTROL DATA NOMINEE Classical Chemistry Parameters - Quality Control Batch 7E31011 - NO PREP - Continued LCS (7E31011-BS2) Prepared & Analyzed: 0513112017 14:10 Spike Source %REC RPD Anal Sf?e Result Flag P_4L Units Level Result %REC Llmlla RPD Nmlt Notes PH 7.0 1.0 pH 6.98 100 99.101 Duplicate (7E31011-OUP1) Prepared & Analyzed: 05/31/2017 14:10 Source: CA05421-01 Spike Source %REC RPD .Analvte Result Flag POL Unite Level gesul %REC Limits RPD Limit Notes_ PH 7.0 110 PH 7.0 0.6 25 Classical Chemistry Parameters - Quality Control Batch 7E24013 - EPA 16648 Blank (7E24013-BLK3) Prepared: 05/24/2017 18:16 Analyzed: 05/26/2017 16:31 Spike Source %REC RPD Anal Result Etas P_Ol. Units Level Resul %REC Llml]s RPD Llmlt Iigtes_ Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7E24013-BS1) Prepared: 05/24/2017 18:16 Analyzed: 05/26/2017 16:31 Spike Source %REC RPD Anal ldE Result Flaa RQL Units Level &AMR %REC L4mill RPD LimIL Notes Oil & Grease (HEM) 146 5.00 mg/L 148 98 78.114 LCS Dup (7E24013-BSD1) Prepared: 05/24/2017 18:16 Analyzed: 05/26/2017 16:31 Spike Source %REC RPD .Analvte Result Flag POL Units Level gout %REC Limits RPD L= JNotes 04 & Grease (HEM) 137 5.00 mg/L 149 92 78.114 6 18 Matrix Spike (7E24013-14S1) Prepared: 05/24/2017 18:16 Analyzed: 05/26/2017 16:31 Source: BA022S1-01 Spike Source %REC RPD .Analvte Result Flea P.OL Unite Level ResulL %REC LbnU RPD Llmlt Notes Oil & Grease (HEM) 134 5.00 mg/L 152 2.40 U 88 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 6 0f 9 �� w■ cow► www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was an for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the Instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence. of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q-01 Analysis performed outside of method - specified holding time. FIN& This report relates only to the sample as recelved by the labo atxy, and may only be reproduced In full. Page 7 of 9 i ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN=OF-CUSTODY• RECORD www.encoiabs.com � � f OTLS find Fort G: i614 � Ptii� CEuri ffudu 8! 7 tta+! �'i+fds kK4gr:hld C1+ iSlurce>,f�>!�D{ axsisru�a.R'ttt!t:.� raa�,.txZt3lT 3 t413t1 f ail t psi Y�Ctt N:O x �tf 1{; t'38 �Cii r F:r'ro4 o%vf4 h, aroWM fxs ifipy 41W3Zs5 pageU1 _� iKr pamu a'som s at`NC =46141 r figa�Tsd �rtrms FtgttfXf • t[17113tOt3fliJ . Will U.40f to Ail" d . 5n�Il� UMf$. ;lf AAtQ ueerussrrsiu.k torlie~j 0 0 - ILL0i O Q _ fv CO: .Stiandiri _.,,,. Expeditad Due �J �kCorvvrftGil�lf, wC�273t18' 06' ilia' ..� liq ntalo) S 64$97 }'d�1 •�Lr Sr an Scam Sbei2dm r 6i iiirF1 ino'!a kCI1 WotlSCfrJ41 I U U, O _.. CL H + - i . ttisu�irfaa`Iltii��isenl[�a w raisi�s�'A traru +r tG.��wgl 1Jr 1: ooloehCR-Drams t.�dlldtNill t-,ML '*Mu r UFsm ua¢i. bars asaaat �brd a � - aamsmu. ' 11 . �7 SN5 Wei 6 -[ X jr a a X —. Ea?CFi�il:.. L' /. 00. WA 8 X X x ` �n>-- t Elm ME 0 ME l3rrf�e flit F' a+oa _ 1 iwra i' a tngb U7ra. k" as nrd taterljr�n ED iAp tp r A R'a Arm on rioc%f r; rY-CceptAW4. Ocm"n U;rr Ahtc n H(of —,,Urla=PV11$9 �w.prown ttcr susap ,m+�arrnvvmar t fi.t3os nvrrt 5w.5utsmtr rrw �rasieratur t&r aRnarltM W%;W" +a�nPl ��ntr�wierruo wry a..nus•wcrw+ uurwiari v art asurspnrtis2 �: �131A?057kra✓1 }sdfaiQWtf YY ET�lC..1 Emx 1pd b[ �"�rS•«'A 4unu trd arxLeianaEa.°eJ On flq +'wm4iF al qty lumi.Itide� jmiriwttthr� �qucrttlatm ral:1, Sample Preservation Veri, ication ENdb`lbary ENCO Work Order. CA08289 Project: Uwi arria Storm -water ,Client: RepUblic:Services of NC (RE014) Project # [none] Logged In: 23rMay-17 12`37 Logged.8y: Rachel Ann Yonish CA08289.01 ` - e Ad�ts d A °gua 8 250mtA+hf2SOA Q Y I N; NA Y IN NA C Ji4OmLP+142SQ.4 250niLA+H2SO4 <2 Y I N I A Y I N 1 NA Q Y' N I NA. YIN NA V CA08289.02 MIA ON Ad 1Iam ' 9 250mtA+H-2SO4 --2 Y I N I A Y I N C 250mL4+HZS04 Q UY I N I —NAl Y I N' E 250mLP+H=4 Y N 1 NA Y N NA CA48289-08 It I 8 25.OMLA+H2S-b4 Q Y( N NA Y I N/ C 2"LA+H2SO4 Q Y 1 N NA Y I N 1 E 25OmLP+H2SO4 Q Y N I NA Y D NA CA08289-04 a i yA° 10,11,011OEM t� Fi gpQtCsHdJ'�Cotn►ttelg B' 25DmLA+H2SO4 --c2 Y I N NA Y I .N N' C 75OinLA+H2S64 'c2 -Y I N NA Y I N I A. E 26dr6t:f'+H2SO4 <ZAY)f N 1 NA Y 1• N 1 NA CA08289-05-- LMrit � �a� W •'� t5 R++3� 1r• OKI Y 4v 8 250mLA+H2SO4 Q YIN: NA' Y I N I ' C 250rnt;A+H2SG4 Q Y I N IM Y 1 N I E i 250mLP+H2SO4 Q LY2 N I NA Y N NA 50 'R ent Name I0. 1 •2 R ent,Narne- ID 3- 4 Rea ent Name ID 5 6 Page 9 of 9 P-dqWf IraAnalytica!' wmpscslahaccm May 24, 2017 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: CA08289 Pace Project No.: 92341572 Dear Ms. Franz: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 13 aceAnalytical www.pecetaftcom Pace Anatydcal Services, LLC 9800 Kincay Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: CA08289 Pace Project No.: 92341572 Raleigh Certification Me 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification #: 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 2 of 13 aceAnalytical' WWWP"Wba.00m SAMPLE ANALYTE COUNT Project: CA08289 Pace Project No.: 92341572 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 20078 (704)875-9092 Lab ID Sample ID Method Analysts Analysts Reported Laboratory 92341572001 OUTFALL #1 SM 92220 BWJ 1 PASI-R 92341572002 OUTFALL #2 SM 9222D 8WJ 1 PASI-R 92341572003 OUTFALL #5B SM 9222D BWJ 1 PASI-R 92341572004 OUTFALL #08 SM 9222D BWJ .1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical" www.pacelalmoom ANALYTICAL RESULTS Project: CA08289 Pace Project No.: 92341572 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunterswifle, NC 28078 (704)875-9092 Sample: OUTFALL #1 Lab ID: 92341672001 Collected: 05/23/17 08:46 Received: 05/23/17 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual M810 9222D Focal Collform RAL Analytical Method: SM 9222D Fecal Coliforms 2100 CFU1100 mL 1.0 1 05/23/17 14:15 Rate: 05/24/2017 01:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 bf 13 ` ceAnalytical ' www.pacelaDa.com ANALYTICAL RESULTS Project: CA08289 Pace Project No,: 92341572 Pace Analytical Services, LLC 9800 Kincey Ave. suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 02 Lab ID: 92341672002 Collected: 05/23/17 09:00 Received; 05/23/17 13:35 Matrix; Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 460 CFU1100 mL 1.0 1 05/23/17 14:15 Date: 05/24/2017 01:40 PM REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13` (�Ia'cmnalyfical' www.pacarabloom ANALYTICAL RESULTS Project: CAOB289 Pace Project No.: 92341572 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL OB Lab ID: 92341572003 Collected: 05123117 08:30 Received: 05/23/17 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual M810 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Coliforms 480 CFUI100 mL 1.0 1 Date: 05/24/2017 01:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/23117 14:15 Page 6 of 13 aceAnalytical www.paaelsbs.com ANALYTICAL RESULTS Project: CA08289 Pace Project No.: 92341572 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Wuntersville, NC 28078 (704)875-9092 Sample: OUTFALL MB Lab ID: 92341572004 Collected: 05/23/17 09:10 Received: 05123/17 13:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Coliforms 200 CFU1100 mL 1.0 1 05/23/17 14:15 Date: 05/24/2017 01:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 13' lacieAnalytical' wwwpacetabs.com QUALITY CONTROL DATA Project: CA08289 Pace Project No.: 92341572 QC Batch: 361990 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAIL Associated Lab Samples: 92341572001, 92341572002, 92341572003, 92341572004 METHOD BLANK: 2007365 Matrix: Water Associated Lab Samples: 92341572001, 92341572002, 92341572003, 92341572004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFUI100 mL ND 1.0 05/23/17 14:15 SAMPLE DUPLICATE: 2007366 Parameter Fecal Coliforms 92341494001 Dup Units Result Result CFU1100 mL 700 800 RPD Qualifiers 13 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Resuhs presented on this page are In the units Indicated by the "Units" column except where an ademate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/24/2017 01:40 PM without the written consent of Pace Analytical Services, LLC. ' , r Page 8 0f 13 acmnalytrcal* wwwAacew lmoom QUALIFIERS Project: CA08289 Pace Project No.: 92341572 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. POL - Practical Quantitation limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report &hall not be reproduced, except in full. Date: 05/24/2017 01 A0 PM without the written consent of Pace Analytical Services, LLC. Page,g of d a ceAnalytical e www.psaele &MM QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CA08289 Pace Project No.: 92341572 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92341672001 OUTFALL #1 SM 9222D 361990 92341572002 OUTFALL #2 SM 9222D 361990 92341672003 OUTFALL 06B SM 9222D 361990 92341572004 OUTFALL #BB SM 9222D 361990 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/24/2017 01:40 PM without the written Consent of Pace Analytical Services, LLC. Page 10 003' uocumenr tvame: cal teen spec UDcurnent rteviseo: Sept. 21, 2016 Sample Condition Upon Recel t SCUR Pa e 1 of 2 8CeAnaViCair Document No.: Issuing Authority: F-CAR-GA-003-Rev D2 Pace Quality Office Laboratory receiving samples: Asheville [] Eden(] Greenwood ❑ Huntersville ❑ Client Narne: n. C'> Projects: Courier: ❑Fed Ex OUPS Cusps Clfent ❑ commercial ❑Pace ❑Other: Custody Seal present? ❑Yes P!o Seals Intact? [—]Yes o Datellnluals person Examining Contents:&r Paddng Material: ❑Bubble Wrap ❑Bubble Bags one ❑Other: Thermometer: et ❑Blue ❑None ®IR Gun ID: _ IS-3492 _ Type of IN: Raleigh® Mechanicsville❑ WO#:92341572 ❑Samples on ice, cooling process has b n Correction Factor: Add0.6 Cooler Temp Corrected j'C): Biological Tissue Frozen? ❑Yes []NO N/A Temp should be aboveJxaqJPj4dVC USDA Regulat N/A, water sampie) Did sampleFionate In a quarantine tone within the United Stales: CA, NY, or SC (check maps)? Did samples originate from a foreign source (lnte Dyes 6N. Including Hawaii and Puerto Rico)? (:]Yes No Cornmams/Olscre an : Chain of Custody Present? 4JJ IJ 1. Samples Arrived within Hold Time? 2. Short Hold Tlme Analysis (a72 hr.)7 3. Rush Turn Around Time Requested? 4. Sufflclent Volume? S. Correct Containers Used? -Pace Containers Used? s. Contalriers Intact? Samples Field Rhered? B, Note If sed4ment Is visible in the dissolved contalner Sample Labels Match CDC? -Includes Date/T1me/ID/Analysi5 9. Heads ace in VIOA Vials (>5-6mrn)? Yes No ITA 1 10, Trip Blank Present? TripBlank Custody Seats Present? Yes No Yes No I�A 11. CLIENT NCITIFICATION/RESOLUTION Person Contacted: I Comments/Sample Discrepancy: Date/Time: Field Pate Required? UYes j, RO Project Manager SCURF (.1 Review: _ Date: Project Manager SRF Review Date: Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DFHNR Certification Office (Le, Out or ho(d, Incorrect preservathm, out of temp, incorrect containers) r+ - ---- -. _ --Pagel 1-of13-- { } p $01 pBPPe anpeM&Md P Wn*WV "nips uagmuessid awl pa;sn[pe uope uss ud rgap I jdjwxu uodn Md I aspen. nwd;o odAl I al old-pS soldweg PAJOSSM -10; god luawasn(ptl Hd 14 -0. W ,ISO RommommomiqLeffloom sommumomms mommommommommmommoMMEMEN ONE 0 Essen 0 m 0 'I 61L 60 0 IN ME M M 0 M 0 a 0 sommummmom Mq V, 0 M ME MR M M klq 0 0 03N3-ZG c1NMID LZ/Z0/90 .a}p0 ono owu :wdd I Z15 Z VEZ6 : #OM # PafWd seluoq }o lagtunu;sll of sl xoq )n W4 w0i;08,,,, ,saldwes Uolaemosaid jo; el3uea e3ue;da]3e 94; U1411M Pue Pel}PaA sl u014BUIJ01438P.10/Pue }Id }I xOq;0 AN doa nimu M390, — 0-3WO /4lleno a)ed rb'Aeit-EOOt/a-tl1/]-d AUZ 8ulnssl VON � JO Z z to i a ed uolop ;tIs17S Iwmtl u � uo[llPuo] el um5 aW 17 -idat :oasinau ivawn3on 2adc woi ica :awanr mawn3on SUBCONTRACT ORDER ENCO Cary CA08289 SENDING LABORATORY: RECIEIV(NQLABOIUI'ORY: ENCO Cary 'lei -Test (Raleigh) 102-A Woodwinds Industrial Court 6701 Conference Drive Cary, NC 27511 Raleigh, NC 27607 Phone: 919.467.3090 Phone :(919) 8344994 Fax: 919.467.3515 Fax: Project Manager: Stephanie Franz Project State of Origin; North Carolina Sub Lab ID Originating Lab ID nt ;Iatrrx Date Sampled Sam le Comments Ouirall#1 Water - Malawi M-May4708:45 Coliform, Fecal 9223E 31-May-17 15:00 Containers Supplied; Slcrilc250mLP+NaThio (F) 23-May-17 16:40 Sub Lab ID Originating Lab ID Client Matrix pate Sampled Sample Commentsz C Outfall 142 Water 23-May-17 09:00 Coliform. Fecal9223B 31-May-17 15:00 23-May-l7 16:55 Containers Supplled.- Sterile25OmLP+Na'Mia (F) Sub Lab FD Originsdag Lab ED Client Matrix Date Sampled Sam le Comments Oatfall #5B Water 23-May-17 08:30 Coliform, Fecal9223B 31-May-17 15:00 23-May-17 16:25 Containers Supplied, Stcrile250mLP+NaThio (F) Sub Lab [D Origlnadn8 Lab 1D Client Matrix (late Sampled Sample Comments G . Outfall HbB Water 23-May-17 09:10 Coliform, Fecal 9223B 31-May-17 15:00 23-May-17 t7:05 Containers Supplied: Stcrilc250mLP+Na Ihio (F) Released 13y Dam Rewived By- Date _..._... _ _ Y._..� Pa�a�eatl3E of-13r c► Im �A RECEIVED DEC 16 2016 CENTRAL FILES DWR SECTION Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted December 13, 2016_ CERTIFICATE OF COVERAGE NO. NCG120051 SAMPLE COLLECTION YEAR_2o18 FACILITY NAME Uwharrie Environmental SAMPLE PERIOD Jon -June X July -Dec COUNTY Montgomery or ❑ Monthly' lmon011 PERSON COLLECTING SAMPLES _Brian Scott DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY___,_ENCO Labs _ Lab Cart. # CZ17645 [3Zerodlow [:]watersupply ❑SA Comments on sample collection or analysis; X Other C PLEASE REMEMBER TO SIGN ON THE REVERSE -+ Part A: Stormwater Benchmarks and Monitoring Results n No discharge this period?' Outfall No. Date Semple Collected' mo/dd/ i 24•hour rainfall amount' Inches Chemical Oxygen Demand Fecal Colllorm Total Suspended Solids Benchmarks - 220 mg/L 1000 count per 100 mL 100 mg/L or SO mg/L 1 No Dkscha e 2 No Discharge 56 11/30 2015 .2" 17 13 3.7 68 No Discharge 7A No Discharge 7C No Discharge ' Monthly sampling (instead of semi-annual I must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requlrement. ' See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. EQ,t example, do notrecort Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported In the format. "<XX ma/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: ifyou report a sample value in excess of the benchmark, you must Implement Tier 1, 77er 2, or Tier 3 responses. See General Permit text. Permit Date: 11/l/2412-10/31/2017 SWU.248, last revised 10/25/2012 Page 1 of 2 }- Part 13; Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this nerlodr7 Outfall No. Date Sample Collected` mo/dd/ ) 24-hour ralnfall amount, Inches' Non polar O&G/TPH by EPA t664 ISGT-HEIY!L Total Suspended Solids pH Benchmarks r-_a> _ 15 mg/L 100 mg/L or 50 mg/L 6.0 - 9.0 SU 713 11 3O/2016 .2 2.4 13 6.93 Footnotes from Part A also apply to this Part B Note: if you report a sample value In excess of the benchmark, you must Implement Tier 2, 77er Y, or 77er 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEOANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL7 YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cook of this AMR. Including all "No Discharae*norts, within 30 days of rerelat of the JQb faults for at end pf monitoring Period In the case of "No Discharae" reggrtsl to: Division of Water Quality Attn: DWQCentraI Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN JUIS C6U1FtCATI0N FOR ANY 10JECOMATION REPORTED; "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervislon In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the Person or persons who manage the system, or those persons dire y rrsponsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that th a are sign ant penalties for submitting false information, including the possibIlity of fines and imprisonment for knowing violations." 41, jSignatureoiPermi eel 1 tel Permit Data: 11/l/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual ormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted dune 7, 2010_ CERTIFICATE OF COVERAGE NO. NCG120051 FACILITY NAME _Uwharde Environmental COUNTY Montgomery PERSON COLLECTING SAMPLES _Brian Scott LABORATORY_ENCO_Labs _ Lab Cart. q CZ07304 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results RECEIVED JUN 17 2016 CENTRAL FILES DWR SECTION SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD X dart.lune ❑ duly --Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ❑PNA ❑Zero -flow ❑Water Supply []SA X Other C PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' mo/dd/ 2"our rainfall amount tnches' Chemical Oxygen Demand Fecal Collform Total Suspended Solids Benchmarks eaza 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 5 18 2016 X 35 132 35 2 No Discharge �.�.� SB 5 18/2016 .7" 44 455 ,/ 6a 5/18/2016 .7" 44 1W' 7A No Discharge A We- 7C No Discharge Jet! 1 Monthly sampling (Instead of semi-annual) must begin with the second consecutive be mark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this disc arse monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge, Unattended sites maybe eligible for a waiver of the rain gauge requirement. `See General Permit text, Table 3, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported In numerical format. For example. do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be recorted in the format. "< " where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Nate.• If you report a sample value In excess of the benchmark, you must Implement Tier 1, 77er Z or Tier 3 responses. See General Permit text. Part Br Vehicle Maintenance Area Monitoring Results: only for facilities averaging > S5 gal of new oil per month. Permit Date: 11/1/2012-10/31/2017 SWU.248, last revised 10/25/2012 Page 1 of 2 n No discharge this Deriod?2 Outfell No. Date Sample Collected' (mo/dd 24-hour rainfall amount Inches Nan -polar O$G/TPH by EPA 1664 SGT-HEM Total Suspended Solids pH Benchmarks L5 ml 100 mg/L or 50 mg/L 6.0 — 9.0 SU 76 5/16/2016 .7" .512 16 7.31 Footnotes from Part A also apply to this Part B Note. if you report a sample value 1n excess of the benchmark you must Implement Ver ], Ver 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORtNG RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS 71ER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall an orlainal and one copy of this DMIT indudloa all "No Discharge" reports withfn90 days afrecelat of the lab results for at end ofmonitodna aeriad In the case of "No Dischorae"_reoortsllo: T Division of Water Quality Attn: DWO Central Files 1617 Mall Service Center Raleigh, North Carolina 27695-1617 XOU MU51 SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am awarethatthe /.renificant penalties for submitting false Information, Including the possibility of fines and imprisonment for knowing violations." (Date) Permit Date: 11/1/2012-10/31/20I7 SWU-248, last revised 10/25/2012 Page 2 of 2 /-Y)C�r l a-C)O 5-/ qt..ENCO Laboratoriesie. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 26, 2016 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 ' RE: Laboratory Results for Project Number: [none], Project Name/Desc: Uwharrle Stormwater ENCO Workorder(s): CZ07304 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, May 18, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are'in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 1 of 9 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: COMM # 1 Lab ID: CZ07304-01 Sampled: 05/ 18116 07:45 Received: 05/16/16 11:40 pammeftI SM 254OD-1997 Hold DamlTime(s) 05/25/16 Prep DateMme(s] 05/19/16 Analysis DateiJIMAW 10:45 05/19/16 10:45 SM 5220D-1997 06/15/16 05/23/16 15:52 05/24/16 10:17 Client ID: Qutfall # 58 Lab ID: CZ07304-02 Sampled: 05/28/16 07:25 Reoelved: 05/18/16 11:40 Paramebe SM 254OD-1997 Hold DateMme(s) 05/25/16 QreQ,Datel.Timefs) 05/19/16 Analysis Date/Time(s) 10:45 05/19/16 10:45 SM 52200-1997 06/15/16 05/23/16 15:52 05/24/16 10:17 Client ID: Outfall # 6B Lab I0: CZ07304-03 Sampled: 05/18►16 08:10 Recelved: 03118/ 16 11:40 PSI SM 254OD-1997 Hold DaWTlme(s) 05/25/16 Prep DatelTlme(s) 05/19/16 Analysis DatelTlmom 10:45 05/19/16 10:45 SM 5220D-1997 06/15/16 05/23/16 15:52 05/24/16 10:17 Client ID:' Outfall # 7B Lab ID: CZ07304-04 Sampled: O5/18/1.6 08:25 Received: 03/18/16 11.40 Paramete EPA 1664A Hold Date/Time(s) 06/15/16 P1pp DatafTlme(s) 05/24/16 Analysls DatelTlme(s) 15:13 05/25/16 18:39 Field 05/18/16 08:39 05/18/16 08:25 05/18/16 08:25 SM 254OD-1997 05/25/16 05/19/16 10:45 05/19/16 10:45 SM 5220D-1997 06/15/16 05/23/16 15:52 OSJ24/16 10:17 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 Of 9 Ce. NS 9 9 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outlall # 1 Lab ID: CZ07304-01 ADalyte Results flag Ha E" U= Method Chemical Oxygen Demand 35 10 10 mg/L SM 522OD-1997 Total Suspended Solids 35 12 12 mg/L SM 25400-1997 Client ID: Outfall # 55 Lab ID: CZ07304-02 ADalftte Resul a ELM nu Em uww Math Notes Chemical Oxygen Demand 44 i0 10 mg/L SM 5220D-1997 Total Suspended Solids 3.6 2,5 2.5 mg/L SM 254OD-1997 Client ZD: Outfall # 60 Lab ID: CZ07304-03 Anal lde Results E612 Hu E L UUM MEIN l'lA3a.9 Chemical Oxygen Demand 44 10 10 mg/L SM 5220D-1997 Total Suspended Solids 77 25 25 mg/L SM 2WD-1997 Client ID: Outfall # 70 Lab ID: CZ07304-04 Anal Res u1l3 E" Hu Em IINIS Miser Hatu Chemical Oxygen Demand 35 10 10 mg/L SM 5220D-1997 pH 7.31 0 0 pH Units Field Total Suspended Solids 16 10 10 mg/L SM 254OD-1997 r FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced !n full. I Page 3 Of 9 www.encolobs.com ANALYTICAL RESULTS Description: Outfall # 1 Lab Sample ID:CZ07304-01 Received: 05/18/16 11:40 Matrix: Water Sampled; 05/18/16 07:45 Work Order: CZ07304 Project: Uwharrie Stormwater Sampled By: Brian Scott ]Classical Chemistry Parameters ^ - EACO Cry ayt#Alederaryte (AC 591] Analvte rCAS Number] $esull$ Elail 1llllta 2E M" 2QL M= Method Analyzed Q1C 1!I9Iea Chemical Oxygen Demand^ 35 mg/L 1 10 10 6E23030 SM 522OD-1997 05/24/16 10:17 JOC Total Suspended SolidsA 35 mg/L 5 12 12 6E19006 SM 2540D-1997 05/19/16 10:45 MMR Description: Outfall # 5B Lab Sample ID:CZ07304-02 Received: 05/18/16 11.40 Matrix: Water Sampled: 05/18/16 07:25 Work Order: CZ07304 Project: Uwharrie Stormwater Sampled By: Brian Scott JClassical Chemistry Parameters ^ - SWO Cry J-" (AC 591] Analda rCAS Numberl Re.4u118 EUg llnlla QF HQ,4 EU g=[l Method wed by 119tu Chemical Oxygen Demand 44 mg/L 1 10 10 6E23030 SM 5220D-1997 05/24/16 10:17 JOC Total Suspended SolldsA 3.6 mg/L 1 2.5 2.5 6EI9006 SM 254OD-1997 05/19/16 10:45 MMR Description: Outfall # 6B Lab Sample ID:CZ07304-03 Received: 05/18/16 11:40 Matrix. Water Sompled:05/18/16 08:10 Work Order: CZ07304 Project: Uwharrie Stormwater Sampled By: Brian Scott Chemistry Parameters Analyte rCAS Number] Resul[a flag ]]nits DE Hu 22L 21=11 Method Analyzed Al Notes Chemical Oxygen DemandA 44 mg/L 1 10 10 6E23030 SM 52200-1997 05/24/16 10:17 30C Total Suspended Solids^ 77 mg/L 10 25 25 6E19006 SM 25400-1997 05/19/16 10:45 MMR Description: Outfall # 7B Lab Sample ID:CZ07304-04 Received: 05/18/16 11:40 Matrix: Water Sampled:05/18116 08:25 Work Order: CZ07304 Project: Uwharrle Stormwater Sampled By: Brian Scott Chemistry Parameters ^ - DKV dry canned are4ft [AC 591] AnalAa rCAS Number] RGIU a Elag galta RE . KU EU w= Mc= Analyzed By n9w Chemical Oxygen Demand- 35 mg/L 1 10 10 6E23030 SM 5220D-1997 05/24/16 10:17 JOC Total Suspended Sollds^ 16 mg/L 4 10 10 6E19006 SM 2540D-1997 05/19/16 10:45 MMR Field Parameters Aajhrte [CAS Numberl Rau] ts fin knits 2E MD1 EQL Batch Methl:d Analysed Sir Notes pH 7.31 pH Units 1 0 0 6E19014 Field 05/18/16 08:25 CLr Classical Chemistry Parameters Oil & Grease (HEM) [C-00073 Resulla Ehtg llnb !?E = EU AWWh Method Analysed IN AQtca 0.612 U mg/L 0.255 0.612 1.28 6E24002 EPA 1664A 05/25/16 18:39 5MA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of g www.encolobs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6E19006 - NO PREP Blank (6E19006-51.Kl) Prepared & Analyzed: 05/19/2016 10:45 Spike Source %REC RPD Anal ltr8 Result EIRG POL Unitas Level Result %REC LlBM RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (6E19006-851) Prepared & Analyzed: 05/19/2016 10:45 Spike Source %REC RPD .Analyte Result Flan POL units Level Result %REC Limits RPD Limit notes Total Suspended Solids 96 2.5 mg/L 100 96 80-120 Duplicate (6E19006-DUPS) Prepared & Analyzed: 05/19/2016 10:45 Source: CZ05115-01 Spike Source %REC RPD -Anahlte Result Flaa POL Units Level Result %REC Llmitt RPD Limit Notes Total Suspended Solids 22 12 mg/L 21 5 20 Duplicate (6E19006-OUP2) Prepared & Analyzed: 05/19/2016 10:45 Source: CZ04520-01 Spike Source %REC RPD .Analvte Result FWa POL Units Level Barm,t %REC Limb RPD Limit Notes Total Suspended Solids 52 25 mg/L 52 0 20 Batch 6E23030 - Same Blank (6E23030-BLK3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD -Analvte Result Flag POL Units Level ROSUIt %REC LimltS RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (6E23030-BSI) Prepared: 05/23/201615:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD .AnallfEa R-ul FIN R" Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg1L 500 98 90.110 Matrix Spike (6E23030-MS1) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-01 Splke Source %REC RPD Anal 1dR Result ElaO M Units Level 8eSult %REC Limits RPD 111311111 bores Chemical Oxygen Demand 550 10 mg1L 526 35 97 90-110 Matrix Spike Dup (6E23030-MSD3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source: C512441-OS Spike Source %REC RPD Anal lda Result Emu P.OL Units Level Result %REC kinu RPD limit Notes Chemical Oxygen Demand 550 10 mg/L 526 35 100 90.110 3 10 Classical Chemistry Parameters - Quality Control Bahth 6E24002 - EPA 1664A Blank (6E24002-131-I(l) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD .Analyte Result Flay POL Units Level Result %REC Limits RPD Llmlt Notes Oil & Grease (HEM) 0.613 U 1,28 mg/L FINAL This repot relates only to the sample as recelyed by the labaratory, and may only be reproduced in full. I Page 5 Of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Bm'rh 6E24Od2 - EPA 16641A - Conflnued LCS (GE24002-BS'L) Prepared: 05/24/2016 15A3 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD Anal ldn Result Flan E" units Level Result %REC UmJjq RPD Limit Notes Oil & Grease (HEM) 154 5.00 mg/L 159 97 78-114 LCS Dup (GE24002-BSD3) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Spike Source %REC RPD .Anallfte Result Flaa POL units Level Resin %REC LiNlt& RPD Lwa !Notes Oil & Grease (HEM) 156 5.00 mg/L 160 98 78-114 2 18 Matrix Spike (GE24002-MS1) Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39 Source: BZ02144-01 Spike Source %REC RPD .Analvto Result Flao POL units Level Resul %REC LW11W RPD LID1lt Notes Oil & Grease (HEM) 155 5.00 mg/L 148 2.40 u 104 78-114 FINAL This report relates only to the sample as reomad by the laboratory, and may only be reprndutad In full. Page 6 Of 9 Cem90�j www.encolabs.corn FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyze was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the Instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates onty to the sample as reodved by the laboratory, and may only be reproduced In full. IPage 7 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-OF-CUSTODY`RECOAD. V! am w:encolabs:c ,OTTSCoedalPu5th- 481¢6x aPmkQx tSWM211 ifs-AW".00dwftwi& iffiC_i: - - -- O� i Orlarr00.';iL82a L7U�sarruJ�a. Et 3�z;5-@7 Csy. T1c xr5t, o . (a07j'B2&53ia Fax 1�71 BSt1•a4i5.19p4j 29fr3007' Fnn s+i F98•fi214 iEfi>Tjr=3690 Fax49191 fii7.lii5; I?dg8=. i co . .. ... Repiubii. SelvfC.r~.siot NC (RE014) nel Ae4u�tedTgsrnarortnd o IL Aad ass 50P 1 lndlil! i oad Pro' . 06frocow �vkiatri� Stci"4 o6f ? moo,Fiush,sr�ioe accoylet;co 0ii4% CRY, IVI . +viieatl; hJG 273,06 7.<-" 0 0. Sizindaid iV- Q o Q' .. .. . Tm: g:1C1) :576-36s' 7 Faa Aeecrtn9Ca4tid- :.Bri; rt.Scatt 1 E itetl Sa+4¢Msi : A�ilitKinii jPrvrtj `: rM1_ 'i=0 218t1 .SCOt[ (!a- U} DUB_% 3ne LaraGon /.Tme7ane U _ LH WOiQ[d8« p s Caftoc, u t. Totm of Rerp •' 5sd r iD (Flan dlArtilliiU0 i): -�Go ami Daia•. 7*i . cw- t Gmb ..tsao ioduti Coirairgr' Suvie Comments outhill #. WA. - 6_ x x X ,c Is tip-- T i 3 =;- 1 Ri!F,111: 77" Ti� �_ REWqushBd ,� C10eTarTlme � p�7prt'inq ! i J Rtlk kad By . Dalvlf ime . By Ga?p/! faaalr as 6 oa Recatipl ���.0 ,L Cor ditk s UPW `�ACCepteble: _ 1filaceepta�te Ad41s: avrs�r 9o-Soi1 ow.rxi�hl�p water aFrseamau � swsau�ace wmor- aw 4vp�,osra. aJ11: • aoogr �oetad m ow>u�xas� Prasn.o>lgn. i ioo : M,N� p�k�? s rasiK'!�o•r�gH o.oC4r io¢4n kt coti?r;�ptrsi . EWO Lade ere a aomraaxrn'm.1h tie Ierm�'end'o'aa��loar� a'Wad an tie Aweiso of uiis k�rm �ir*m pikw waM ap� atm .. .. . - — - - . _ _.. - _ - _......�... ��� ...._ _ - . �...+e.+�-.e.•-� z^�„-�-=�- --�.•+.� :-:.�... ,. �� _ � - _- _ _ Lam.,,.-�— � -� . r 0U��� pm��o�� 'Jnmol . --_-'--'_- - —' '-'- `^ ' ---------------r---'---`-- --- -'^— '` ' — - 25 gy 41 v M, & 0 a� - ztl ITT. 11 @��ffi I'M, - r?CIBAfialllCc?I e Kww.pacelabe.Gorrr May 24, 2016 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Ms. Franz: Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm. harrison@pacelabs.com Project Manager Enclosures A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pagel of 11 aceAnalytical a sww.paoefebacom Pace Analytical Services, Inc. 9800 KlnceyAve. Suite 100 Huntensville, NC 28078 (704)875.9092 CERTIFICATIONS Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Raleigh Certification Me 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification #: 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 CeAnalytical www.pecelabs.com SAMPLE ANALYTE COUNT Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92298129001 OUTFALL M SM 9222D RC 1 PASI-R 92298129002 OUTFALL #58 SM 9222D RC 1 PASI-R 92298129003 OUTFALL M SM 9222D RC 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical www.peoelaUMM ANALYTICAL RESULTS Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntereville, NC 28078 (704)875-9092 Sample: OUTFALL #1 Lab ID: 92298129001 Collected: 05/18/16 07:45 Received: 05/18/16 13:06 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 132 CFUl100 mL 1.0 1 05/18/16 14:10 Date: 05/24/2016 03:03 PM REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytical s www,paeelaba.mm ANALYTICAL RESULTS Project: , ENCO CARY CZ07304 Pace Project No.: 92298129 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: OUTI=ALL #5B LabID: 92298129002 Collected: 05/18/16 07:45 Received: 05/18/16 13:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual MBIO 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Colifonns 456 CFU1100 mL 1.0 1 05/18/16 14:10 Date: 05/24/2016 03:03 PM REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 IceArralytr"cal wwwPowabs.cam ANALYTICAL RESULTS Pace Analytical Services, fnc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Sample: OUTFALL #6B Lad lD: 92298129003 Collected: 05/18/16 08:10 Received: 05/18/16 13:05 Matrix: Water Parameters Results Units MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 160 CFU1100 mL Date: 05/24/2016 03:03 PM Report Limit OF Prepared Analyzed CAS No. Qual 1.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 05/18/16 14:10 Page 6 of 11 ceAnalytical wwwpacefebs.00m QUALITY CONTROL DATA Project: ENCO CARY CZ07304 Pace Project No.: 92298129 QC Batch: R131016148 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Associated Lab Samples: 92298129001, 92298129002, 92298129003 METHOD BLANK: 1737463 Matrix: Water Associated Lab Samples: 92298129001, 92298129002, 92298129003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Colifo►ms CFU1100 mL ND 1.0 05/18/16 14:10 SAMPLE DUPLICATE: 1737464 92298192001 Dup Parameter Units Result Result RPO Qualifiers Fecal Coliforms CFU1100 mL ND ND Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page ere In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/24/2016 03:03 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 acmnalytical' WWW'Pscotabacom QUALIFIERS Project: ENCO CARY CZ07304 Pace Project No.: 92298129 OEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit, PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(0) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Siiica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylemine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited anatytes. TNI -The NELAC Institute, LABORATORIES PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/24/2016 03:03 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical' www.psoelalrs.eom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: ENCO CARY CZ07304 Pace Project No.: 92298129 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92298129001 OUTFALL #1 SM 9222D RB1016148 92298129002 OUTFALL #8B SM 9222D RB1016148 92298129003 OUTFALL #BB SM 9222D R1311016148 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/24/2016 03:03 PM without the written consent or Pace Analytical Services, Inc., Page 9 of 11 AAY -RAL W®# : 92295129 _ . } t�; ��� ��.�L.i �� /; � li I III � I Il li � I�illll rlll 92298229 Cul t ody 5 0;11 preio ri L? []."e; S"ZA Evi, i:Ojl(,'i L P:icklng Pe. att.-rL:l: t rja,.jbbl--,'Y.'rap is x 0 L, L 1',:, CL I I C.- u ---------- — Old% cvf:,;j x, J- f Chain of Custody RiAinquished? SallIONY thille and/or S! n-1two or) CDC? hitored Volume Received for (A"olved Tests? tlO*if5HilT'(!1;l IS in IMU vc-i ljM- ,L Switple Lnbols t.;3%:h CC)C? I L 3ral DRO/in" I 1,,5ot4r! L�e)(:,Ltflv N.tAel! fur cec!1104.10:n, -Ileac: :ce in VGA Vials (>5-6rnm).o Tr'lp 013r;k Present? a,,, Trip Hit r D.i:3 Acquiro!? .... ............. Pirujecl f4anoSer SCURF IWAL-w: CIS Pridoct rvl,-wjw SRF Review LJV .. ...... Page 10 of 11 di11CON'l 0M)Lk LI ,-L -C., . ....... f-.X',, 0 ' '. ! r- i 02-A W,a.;dwili6s industr4d Colin F-n: 919.4G7.3515 Prticct I'Amiauu: Stephanie Frunz o! ('60iii: III ............. - -- ---- ----- . ...... "Vnivi. -7, �41 Sub 1..1b 11) 11) iv •,5, 11 V, I -w .114Z WN L,T .. ........... ............... . ..CA ni. 17 A "a I NAT Cofit'orvi, Fcol 522311 25-Nlav- 16 15:01, 177 1 7 Siur;f�2-401111-1'i Na I bio I Fj Page 11 of 11 ~V Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted 10/27/2014 1� r~� CERTIFICATE OF COVERAGE NO. NCG120051 SAMPLE COLLECTION YEAR _2015 r� FACILITY NAME Uwharrie Environmental tt f IMPLE PERIOD ❑ Jan -June X July -Dec COUNTY _Montgomery REC t V or ElMonthly' _ (month) PERSON COLLECTING SAMPLES _Brian Scott 5CHARGING TO CLASS ❑ORW ❑HOW [-]Trout ❑PNA C, LABORATORY ENCO_Labs ^ Lab Cert. # C513829 4� ❑Zeraflaw ❑Water Supply [:]SA C...7 Comments on sample collection or analysis: CENTRAL FILES X Other C pWR SECTION rC PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period: outfall No. Date Sample Collectedl (mo/dd/yr) 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmorks - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 10/28/15 1.3" 44 6000 79 2 10/28/15 1.3" 5o 1360 49 56 10/28/15 1.3" 35 5300 42 68 10/28/15 1.3" 44 1000 100 7A 30/28/1S 1.3" 20 83 7C 10/28/15 1.3" 10 12 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGr-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or S0 mg/L 6.0 — 9.0 5U 7B 10/28/1S 1.3" 2.40 20 9.32 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, rer 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION 8. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an ariainal and one coov of this DMR, includina all "No Discharce'v reports, within 30 days of receiat of the lob results for at end of monitorina oeriod in the case of "No Discharue'reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that tf1ere are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date: 11/1/2012-10/31/2017 /Z- /'1,5-- (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 ENCO Laboratories Accurate. Timely. Responsive. b►nansNve. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone; 919.467.3090 FAX: 919.467.3515 Friday, November 6, 2015 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 RE: Laboratory Results for Project Number: [none], Project Namelaesc: Uwharrie Stormwater ENCO Workorder(s): CS13829 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, October 28, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures, Results for these procedures apply only to the samples as submitted. The analytical results contained In this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) " FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 1 of 1 Ce N, co www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE CIIent ID: Outfall # 1 Lab ID: C513829-01 Sampled: 10/28/15 08:50 Received: 10/ 28115 13:10 Parameter SM 254OD-1997 SM 522OD-1997 Hald Date/Timefs) 11/04/15 11/25/15 erep OatelTime[s1 11/03/15 10/30/15 Analysis Date/Time[s) 10:25 11/03/15 10:25 12:15 10/30/15 18:10 Client ID: Outfall # 2 Lab ID: C513829.02 Sampled: 10/28/15 09:05 Received: 10/28/15 13:10 Eimmeter SM 254OD-1997 SM 522OD-1997 Hold Date/Timefs) 11/04/15 11/25/15 Prep Date/-Tlme[sl 11/03/15 10130/tS Analysis Date/Timefs) 10:25 11/03/15 10:25 12:15 10/30/15 18:10 Client ID: Outfall # 5 8 Lab ID: C513829-03 Sampled: 10/28/15 08:35 Received: 10/28/15 13:10 Parameter SM 254OD-1997 SM 5220D-1997 Hold Date/Tlme(s) 11/04/15 11/25/15 Prep OatelTlme(s) 11/03/15 10/30/15 10:25 11/03/15 10:25 12:15 10/30/15 18:10 CllentlD: Outfall # 6 8 Lab ID: C513829-04 Sampled, 10/28/15 09:15 Received: 10/28/15 13.10 parameter SM 254OD-1997 SM 52200-1997 Hold OatelTlmefs) 11/04/15 11/25/15 Prep DatelTimels) 11/03/15 10/30/15 Analysis DateLT7mefs] 10:25 11/03/15 10:25 12:15 10/30/15 18:10 Client ID: Outlall # 7A Lab ID: C313829-05 Sampled: 10/28/15 09:30 Received: 10/28/13 13:10 Parameter SM 2540D-1997 SM 522OD-1997 Hold DatelTime[s) 11/04/15 11/25/15 Prep Data/Timefs) 11/03/15 10/30/15 Analysts DatelTlme(s} 10:25 11/03/15 10:25 12:15 10/30/15 18:10 Client ID: Outfall # 7C Lab TO: C313829-05 Sampled: 10/28/15 09.35 Received: 10/28/15 13:10 parameter SM 254OD-1997 SM 5220D-1997 Hold DatelTEme[s} 11/04/15 11/25/15 Prep Date/Tlme(s) 11/03/15 10/30/15 Analysis DatelTimefs) 10:25 11/03/15 10:25 12:15 10/30/15 18:10 Client ID: Outfall#78 Lab ID: C513829-07 Sampled: 10/29/15 09:25 Received: 10/28/15 13:10 1 Parameter EPA 1664A Hold DatelTimefs) 11/25/15 Prep Date/Time(s) 11/03/15 1532 Analysis Date/Time(s) 11/05/15 17:23 Field 10/28/15 0939 10/28/15 09:25 10/28/15 09:25 SM 254OD-1997 11/04/15 11/03/15 10:25 11/03/15 10:25 SM 52200-1997 11/25/15 10/30/15 12:15 10/30/15 18:10 FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 1 �co www.encolabs.com SAMPLE DETECTION SUMMARY Client 1D: Outfall # 1 Lab ID: C513829-01 Anal 1tIP. Results E10 am E" halls Method lii Chemical Oxygen Demand 44 10 10 mg/L SM 5220D-1997 Total Suspended Solids 79 25 25 mg/L SM 254OD-1997 Client M. Outfall # 2 lab 11): C513829-02 ADailde Results Eft Hu E" halm Msth4d �@ Chemical Oxygen Demand 50 10 10 mg/L SM 522OD-1997 Total Suspended Solids 49 17 17 mg/L SM 254OD-1997 Client 1D: Outfall # 5 B Lab ID: 0513829-03 ADai7tS& Results Elm Hu Z" dolts Mgthod NoteS Chemlcai Oxygen Demand 35 10 10 mg/L SM 5220D•1997 Total Suspended Solids 42 10 10 ma/L SM 254OD-1997 Anal Yffi ResulT6 no Mel ML 1,lwm Method Notes Chemical Oxygen Demand 44 10 10 mg/L SM 522OD-1997 Total Suspended Solids IN 25 25 mg/L SM 254OD-1997 Client 1D: Outfall # 7A Lab ID: C513829-05 ADandO &AWU Flan HA l" Vaal method EL9ter5 Chemical Oxygen Demand 20 10 10 mg/L SM 5220D-1997 Total Suspended Sollds 83 10 10 mg/L SM 254OD-1997 Client ID: Outfall # 7C Lab ID: C913829-06 Anal flesulhl Ela9 Hu P44 !hilts Method Notes Chemical Oxygen Demand 10 10 10 mg/L SM 522OD-1997 Total Suspended Solids 12 4.4 4.4 mg/L SM 2WD-1997 Client 1113: Outfall # 7B Lab ID: CSL3829-07 ADatvte Results EIN Mu M l nim Mid Notes Chemical Oxygen Demand 29 10 10 mg/L SM 522OD-1997 pH 8.32 0 0 pH Units Field Total Suspended Solids 20 20 20 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 1 .■.el M� kc www.encolabs,com ANALYTICAL RESULTS Description: Outfall # 1 Lab Sample ID:C513829-01 Received: 10/28/15 13:10 Matrix: Water Sampled: 10/28/15 08:50 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian ] Scott Classical Chemistry Parameters ^-SCOC�ryc&MfkdanalM[AC 5911 Analvte rCAS Numbed Resultrt Elag Unitrl RE MDl Em @;itch Meth Analyzed AX Notes Chemical Oxygen Demand^ 44 mg/L 1 10 10 5130015 SM 522OD-1997 10/30/15 18:10 10C Total Suspended Solids^ 79 mg/L 10 25 25 5KO3002 SM 2540D-1997 11/03/15 10:25 MMR Description: Outfall # 2 Lab Sample ID:C513829-02 Received: 10/28/15 13:10 Matrix: Water Sampled: 10/28/15 09:05 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian 3 Scott Classical Chemistry Parameters ^ - &KV Cary certr&d analyre [AC $911 Analvie rCAS Number] Results Ein 11111M QE MPl EU @atch Method Analyzed gY No Chemical Oxygen Demand 5o mg/L 1 10 10 030MS SM 5220D-1997 10/30/15 18:10 30C Total Suspended Solids^ 49 mg/L 6.67 17 17 5K03002 SM 25400-1997 11/03/15 10:25 MMR Description: Outfall # 5 B Lab Sample ID:C513829-03 Received: 10/28/15 13:10 Matrix: Water Sampled: 10/28/15 08:35 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian 3 Scott Classical Chemistry Parameters ^ - EACD Cary c"JW analyre [AC $911 Analvte fCAS Numberl gas flog ua1tg QE Hu 921 Batch Method Analyzed MY tuft Chemical Oxygen Demand^ 35 mg/L 1 10 10 5330015 SM 5220D•1997 1013DI15 18:10 ]OC Total Suspended Solids^ 42 mg/L 4 10 10 5KO3002 SM 2540D-1997 11/03/15 10:25 MMR Description: Outfall # 6 B Lab Sample [D:C513829-04 Received: 10/28/15 13:10 Matrix: Water Sampled: 10/28/15 09:15 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian I Scan iClassical Chemistry Parameters ^ - EACO Lary crrt*d analyre [AC V11 Analvte rCAS Number] ResulElsa units DF MU PAL am Method Analyzed ft Notes Chemical Oxygen Demand^ 44 mg/L 1 10 10 5130015 SM 522OD-1997 10/30/15 18:10 30C Total Suspended Solids^ 100 mg/L 10 25 25 5KO3002 SM 2540D-1997 11/03/15 10:25 MMR Description: Outfall # 7A Lab Sample ID:C513829.05 Received: 10/28/15 13:1D Matrix: Water Sampled: 10/28/15 09:50 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian I Scott Classical Chemistry Parameters ^ • EACO Cary c&Vfled anaW [AC 591) Analyte rCAS Numbers Results pig 11gjtg JDf MU EQ1 latch Method Anal M gar 1 = Chemical Oxygen Demand^ 20 mg/L 1 10 10 5330015 SM 522OD-1997 10/30/15 18:10 30C Total Suspended Sol1d6^ 83 mg/L 4 10 10 5KO3002 SM 254OD-1997 11/03/15 10:25 MEYER PENAL This report relates only to the sample as received tay the laboratory, and may only be reproduced In full. I Page 4 Of (�9 o www.encolabs.com ANALYTICAL RESULTS Description: Outfall # X Lab Sample ID:C513829-06 Received: 10/28/15 13:10 Matrix: Water Sampled: 10/28/15 09:35 Work Order, C513829 Project: Uwharrie Stormwater Sampled By: Brian J Scott Classical Chemistry Parameters ^ - EACO Cary Certfl d om ibte (AfC $911 BesulFlag halts I?E 11" E" Hatch Method AnahaBY hws Chemical Oxygen DemandA 10 mg/L 1 10 10 5130015 SM 52200-1997 10/30/15 18:10 JOC Total Suspended SolidsA 12 m91L 1.75 4.4 4.4 5KO3002 SM 254OD-1997 11/03/15 10:25 MMR Description: Outfall # 7B Lab Sample ID:C513829-07 Received: 10/28/15 13:10 Matrix: Water Sampled; 10/28/15 09:25 Work Order: C513829 Project: Uwharrie Stormwater Sampled By: Brian J Scott Classical Chemistry Parameters ^ - EACD Cary cwf/ lea'am W (AC 591) Anpllyte ICAS Numberl Results Eiag unliffi RE HU EM latch Metho AnalMled Alt N Chemical Oxygen Demand 29 mg/L 1 10 10 5330015 SM 5220D-1997 10/30/15 18:10 JOC Total Suspended SolldsA 20 mg/L 8 20 20 5KO3002 SM 254OD-1997 11/03/15 10:25 MMR Field Parameters Analvte_ rCAS_Number] Results Ehu ]]nits Of MQ.L p_QL latch Metho Analllsld ft ]Yogi pH 8.32 pH Units 1 0 0 5K02018 Field 10/28/15 09:25 CLI Classical Chemistry Parameters Analde [CAS Number] Oil & Grease (HEM) [C-0007] ResultA Elag 1lnit a i2E MQL PQL latch Method Analyzed flit >Notes 2.40 U mWL 1 2.40 5.00 5KO3012 EPA 1664A 11/05/15 17:23 SMA FINAL This report relates only to the sample as received by the laboratory, aM5 may only be reproduced In k1l. Page 5 Of ') www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SJ30015 - Same Blank (5330015-BLKi) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Spike Source %REC RPD Analvte Result Finn Eft Units Level Resulj %REC Lll ft RPD Limit Notes - Chemical Oxygen Demand 10 U 10 mg/L LCS (S130OLS-BS1) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Spike Source %REC RPD .Analvte Result Flaa ROL Units Level gesuR %REC Limb RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90.110 Matrix Spike (5330015-MS1) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Source: C500548-01 Spike Source %REC RPD .Analvte Result Flaa ROL Units Level Result %REC Limig RPD Limit NuUM Chemical Oxygen Demand 770 10 mg/L 500 310 93 90.110 Matrix Spike Dup (5330019-MSDI) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Source: C500548-01 Spike Source %REC RPD _Analvte Result Flaa ROL Units Level Result %REC Limits RPD U= Notes Chemical Oxygen Demand 760 10 mg/L 500 310 90 90-110 1 10 Batch SK03002 - NO PREP Blank (5K03002-BLK1) Prepared & Analyzed: 11/03/2015 10:25 Spike Source %REC RPD .Analvte Result Flao ROL Units Level Result %REC jimitr5 RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SK03002-BSI) Prepared & Analyzed: 11/03/2015 10:25 Spike Source %REC RPD Anand® Re.4ult Flag P-QL Units Level Result %REC Limits RPD Limit Not" Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (SK03002-DUPi) Prepared & Analyzed: 11/03/2015 10:25 Source: C504318-01 Spike Source %REC RPD -Amlvte Result Elao e0L Units Level Result %REC Limitli RPD Lim Notes Total Suspended Solids L000 170 mg/L 1100 4 20 Duplicate (5K03002-DUP2) Prepared & Analyzed: 11/03/2015 10:25 Source: CSOB858-01 Spike Source %REC RPD Analvte Result Elaa e0L Units Level Resuf %REC Limits RPD L= Notes Total Suspended Solids 340 100 mg/L 340 1 20 Classical Chemistry Parameters - Quality Control Batch 5KO3012 - EPA 16644 Blank (SK03012-BLKi) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD Analyte Result Flao ROL Units Level Result %REC limits RPD 1knit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates oNy to the sample as received by the Vaboratory, and may only be reproduced In full. IPage 6 Of 11 Ce Cm s —) www.encolubs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5KO3012 - EPA 1664A - Continued LCS (5K03012-BS1) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD Anahft Result Flag PQL units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 40.9 5.00 mg/L 42A 97 78.114 LCS Dup (51K03012-11IS01) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD Analvte Result Flag P.OL Units Level Result %REC LIi1I RPD Llmlt Notes Oil & Grease (HEM) 35.6 5.00 mg/L 41.9 85 78.114 14 18 Matrix Spike (SK03012-MSi) Prepared: 11/03/2015 15:32 Analyzed: 1110512015 17:23 Source: B504527-OL Spike Source %REC RPD .Anahrte Result Flag P.OL Units level Result %REC Lbb RPD Limit notes Oil & Grease (HEM) 754 5.00 mg/L 155 521 151 78-114 QM-07 FINAL This report relates only to the Sample as recelyW by the laboratory, and may Only be reproduced in full. I Page 7 of 1 Ce N rrr www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification°. P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 Of 1 ENVIRONMENTAL�CONSERVATION LABORATORIES` CHAIN-QF.rCIlSTODY FlECORO www.encolabsccain Ce NS C0 1W75GrdraiPartDrs 4Di0 f8i�eeutKei'a�Caurl�$�ssro;�ttIOi-A4Vo�tpltbuislntlui.tia�Gl; ` f�yffiIi iaekeo�iRls, R 3Z21fi , .y_ Cer� kC 2�751 i i+ml ago i� Fu teo e s as, (gni� goo* �u t�oi} ae e? �o � aar7i60 � �ei�� ear 3si5 : Page.. of <. � . _ sDod "Aiwilysee p Ftequested_1'urr5arourfd p IbijG 04kwltq: Of NC.(REE014 ) 1° Ttmes ' M6 Land ilC k6dd w lame-Stormwatei u j ricio t Rsrch raq�ai to c*WGilead; NCf'?306 Po.r� +- _ :40 m p _ Standard (910) 5f8 3597- ant _ TM. — �E' -- - — -- -- _ e — _ � Expedited �Ga Scot E cn. piece_ t]: E7 - o+fe - S;e Caemio� i:Tirm2m�: _ 0 O• {3 U CCU �-- - _ Pi eemativniSeeEatt�a}'(Caebinpasnoemea $. 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Y, $Y. ..1rrm Rertw+ed B]' DataT�ne AeS7q�shedBy - - �aeetiinse - RereiveEBli - .. - - Rptetfeme -� - - - - - - - Coder A17.13?esnps wr:iecalpt ` y � 6� CaW�on Upon ii4telq r3hrmrt : Uw prpts�Q 4btOf sP 6a7 [nn pprswtq tivamr SF 9er$nef ? 61NtiSurCrtln wasac wW7VftS aA"?, w-aa o-amer [metaP In eaeem±nsb) R San sate !►ilG7' N H++o4 s nzsw NO-NDM' 042ftr JAM -Us fro} lkte 'AS sar?wlse ssabri rnG to EMCO Latra usa 16 riC 4Y!c0 vrlRr Cla lertna A+11! oo!!Q taro toad on iho fcvs+e4 al thh In/m, t�iaAs Prirsr wsgten agrabaiaita saw_ s Page 9 of 11 IN ;sarfi.plo,'Pre.4dr,vation'Ve-'r'lification` 4ry, Old M' brd , rkek W3k§ 0'ea- W�i rffll��t l cli ml'* w�ai6r Client - R ti1i-'dfNC'(RE014) ,Loggeq,!p., '2"ct.;l 513:34 -Log"g'q'd B 'And rew'S'; Coons',1, . . l . _. I - .. y, . 16MA26 1 A, ibA+k LUkO4s, Y fakYNK; E 2 7W N�� (R.4 N A owe A LA+ Y NA Y E ,[25&LP4kitb4" _175�1/ "WY I 1, NA I I Z61382943 A 1 LA+i42SO4 - 1LIA+H.2SO4 .42 NA, ZEE E .1 m pl+Hioo4i NA i J L�� EULI aMM Ll I N. A MEN M a A lLk+H2§d4 <2 i �Y,' -NA 8 1 LA+H 2SO4 <2 -Y: NA I' E 12,%MLP+H2 . SO4 <2 .FY))IN,lyNA,.1 -Y-O<v, NA C513kMd co og rims-PL', ,AL 1 LN+H2SO4 �<2 `Y TNA, �y ' 71i 7NA N yl,_ I WA E '!60_'rn'L'_P+H2'k4 <2 """r ./li"Ty". j, B . . .......... irk I,NA Page lOo -Wk lorfV6dfi,,mitlbft, ,$00'0!e,,Pe-dsoN t ,ENCa'C*r-y Workbrder., C61-629Proj . ed, UWhar4W Siorm'waiter E c0d. In26 LOct, .3 -`34, LO00*:, ' qcIr6w:(SCdcins" '413829-07 -ID: eacen 'Na m e, 0 .11), Resnenchlam Page 11 of 11 aceAnalytical. W1YW'060 03-com October 30, 2015 Ms. Stephanie Franz ENCO Labs 102 A-Woodswinds Industrial Co Cary, NC 27511 RE: Project: C513829 . Pace Project No.: 92273966 Dear Ms. Franz: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntensville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 28, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm.harrison@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. aCG A—a'X!r'+e 9800 Kincey Ave. Suite 100 078 v�i�! lK1r Huntersvills, NC 28078 WWW•PbLC0m (704)875-9092 CERTIFICATIONS Project: C513829 Pace Project No.: 92273966 Raleigh Certification Me 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification* 37731 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 acemapical0 www.Pnoefabt.mm SAMPLE ANALYTE COUNT Project: C513829 Pace Project No.: 92273966 Pace Analytical Services, Inc. 9800 Klncey Ave. Sulfa 100 Huntersville, NC 28078 (704)875-9092 Artalytes Lab ID Sample ID Method Analysts Reported Laboratory 92273966001 OUTFALL #1 SM 92221) RC 1 PASI-R 92273966002 OUTFALL #2 SM 9222D RC 1 PASI-R 92273966003 OUTFALL #8B SM 9222D RC 1 PASI-R 92273966004 OUTFALL #613 SM 9222D RC 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 (�55'cmnalyfical" wwwowebbmm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunteraville, NC 20078 (704)875-9092 Project: C513829 Pace Project No.: 92273966 Sample: OUTFALL #1 Lab tD: 92273966001 Collected: 10/28/15 08:50 Received: 10/28/15 14:50 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual MBIO 9222D fecal Coilform RAL Analytical Method: SM 92220 Fecal Coliforms 6000 CFUI100 mL 1.0 1 10128/15 16:31 Date: 10/30/2015 01:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalXical e www,pe wob8.mm ANALYTICAL RESULTS Project: C513829 Pace Project No.: 92273966 Pace Analytical Services, Inc. 9860 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL #2 Lab iD: 92273966002 Collected: 10128/15 09:05 Received: 10128115 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Collform RAL Analytical Method: SM 9222D Fecal Coliforms 1360 CFU1100 mL 1.0 1 10/28/15 16:31 Date: 10/3012015 01:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalytical WW'W eteba.= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-sa92 Project: C513829 Pace Project No.: 92273966 Sample: OUTFALL #5B Lab ID: 92273966003 Collected: 10/28/15 08:35 Received: 10/28/15 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 5300 CFU1100 mL 1.0 1 10/28/15 16:31 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 10/30/2015 01:58 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 (�IaceAnalytkala www.pgowabs.com ANALYTICAL RESULTS Project: C513829 Pace Project No.: 92273966 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunteraville, NC 28078 (704)875.9092 Sample: OUTFALL #6B Lab ID: 92273966004 Collected: 10128/15 09:15 Received: 10/28/15 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MRIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 1000 CFU1100 mL 1.0 1 10/28/15 16:31 Date: 10/3012015 01:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 CeAnalygcal" trww.ptroelatu.com QUALITY CONTROL DATA Project: C513829 Pace Project No.: 92273966 QC Batch: RBIOI5652 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Associated Lab Samples: 92273966001, 92273966002, 92273966003, 92273966004 METHOD BLANK: 1595390 Matrix: Water Associated Lab Samples: 92273966001, 92273966002, 92273966003, 92273966004 Blank Reporting Parameter Units Result Limit Analyzed Fecal Coliforms CFUl100 mL ND 1.0 10/28/15 16:31 SAMPLE DUPLICATE: 1595391 Qualifiers 92273691002 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFUl100 mL 2.0 2.0 0 1g Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2015 01:58 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical WWWOCsleL W" QUALIFIERS Project: C513829 Pace Project No.: 92273966 DEFINITIONS ❑F - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical services, Inc. 9800 Kinsey Ave. Suits 100 HunteraWle, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS 1g This is a less than value REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2015 01:58 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalyticals www.psoeleb e m QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: C513829 Pace Project No.: 92273966 Pace Analytical Services, Inc. 9800 Kinoey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92273966001 0UTFALL#1 SM 9222D RB1015652 92273966002 OUTFALL 02 SM 9222D RBI015652 92273966003 OUTFALL #5B SM 9222D RBI015652 92273966004 OUTFALL #6B SM 9222D RB1015652 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Gate: 10/30/2015 01:58 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 Documont Nam©: Sample Condition Upon Document Revised: May 15.20l5 ,��•�p CeRnalytia7l - Ret:ei t (SCUR) Pace 1 of 2' Document No.: ! Suf:ig Autharlt ss: F-RAL-CS-001-rev,03 Pa-eIRaloif h Quali~• Of ,mot Client Name: U CouriLr(Clrclu): Fod Ex UPS LISPS Client Commercial Pac: CustotlySaa) qri Cooler/Rex Present; ❑ yes no Seals Intact; yes Packing Material: ❑ Bubble Wrap $ags �]`t None 01hor Circlo Tharmornater Used: IR Gun�1122220665� 3$T�oYYo--f'' Ice: Bt Blue Norio IR Gun l5a N� 22R53711 'Page 2 of 2 is for fnbirnai'Jso Only I Other ❑ no { ❑ $a� npW onti co, ccoling [YOCegs It:]3 Ue;uri Tornp Correction Factor: Add / Subtract 1L C Dato an Inklats of person examining Garrotted Ceoter Tamp,:_ C Biological Tissue is Frozen: vas :tc NA ° f Pr r a r Chuck.. i„mp sl•,cutd Lc.• u!)ovo freezing to TC Comments: Chain of Cuslr,dy Present: Yes ❑No ❑NIA 1. C}vfln of Cuutod� Filled Out: es QNo ❑NIA 2, _ Chain of Custody Relinquished: J&as ONO ❑NIA 3. 18„Inpler Name S Signature on COC: Yea ❑No ❑NIA 4, Sum fes F.rrlvud_within Hold Time: Yes ONO ❑NIA 5, Short Hold Tinto Anal sf5 <72hr): 1-as ❑rio ❑N/A 6. Rush Turn Around Time Requested: ❑Yos ONO ❑NIA 7, SIlffcient Volume: Yon ❑tNo ❑NrA 8. Correct ConlAners Used: 1p(as ONO ❑NIA S. -Pace Co•ntnlners Usad: f1 Yea ❑No ❑NIA t I Con:einc:rs Intact: Yob ONO' ❑NIA 10. 1 Rl,ored wlume received for Dissolv0d tests ❑Yea ONO N/A 11. : nmpfo I,aacls match COC: Y . ONO ❑N/A 12. -Includes dste114me/ID/Anal sis i4latrix. A!i watalnrrs nvuoin;t preservallon have Mann checked, tCNo ❑NLt 13, p Alt .onta'tter, hoc-jinrg proServalion are found to be In ��]//Yas L�(as ❑No ONIA I` ccmpilanca %N10 EPA rocornmenda0art. I/T a�Cc«a'Gs s. VCA r-tib:nt, TOC, O$G, WI-DRO (wr,tor) Yos i INo Samples e:c:;k,:d for dech%Mnation: Yes ONO ❑NIA 14, I Hanospac6 in VOA Vials( >6mm),. Oyes ONO NIA 15. Trier lllnmk Prasent: ❑yes ❑Na 16, Tri;3 Blanl, Custociv Seals Present ❑Yes ©No /NIA rDNfA I Palce Trip B3 3nk Lot f1(it purchased): s Client Noblicatlow Resolution: F101d [)are Rettulrer)? Y 1 N Person Con;acted:� Dalemme: Comments/ Resolution: SCURF/SRF ��, Data; {I1ti WO!! 92273966 Rovl(?w:: 5 II ! r :,Inv 41 t,6,.ati'er thr, ra It, a discrepancy alfec'ing North Carolina compliance sa:l:ples, a ,-ol)y of this form wi11 be sent to the North Carolina 0 HNR j r Cerli3calion WiiC,T (La out of hold, incorrect proservallve, out of lomp, 9227 966 Incorrect containers) I i Page 11 of 12 SURCON'TRACT ORDER ENCO Cary C513829 tit{tYt1M; L, VOR TORY• RECEIVING I.ABOILV7'ORY: C. NICO Car), Tti-Test (Raleigh) 102-A Woodwinds Ludustrial Court 6701 Conference Drive C;try. NC 27511 'Raleigh, NC 27607 I I flume: 919.467.3090 Phone :(919) $34-4984 Fsx: g 10.467,3515 Fax: Proieet Man.igat: Stephanie Frantz project State of Origin: North Carolirinl uh L. Lb it) La Water Colitbrni. Fixnl 9223B 06-Nov-15 15:00 211.Oct-15 16:45 C'c�uipintrs Supplied: �itC1'l IC'? illm! ,I'+1dti !'Iuu (F) 28-Oct-15 08:50 .iample Commeirts I Sul} I.uls III Originating IAb 10 (Alent Matrix Rate SuutplLd ;ample Cemincnts Ourfall02 Water 28-00-1509:05 Colirurnr. Fcattl922311 06-Nov-15 15:00 28-00-15 17:00 5ierilc250mI.P+NaFhiu (F) I Fcal 622311 06-Nov-15 13:00 28.Oct-15 16:30 !:lrt: : finer.,• ;,imf�f ic,l: S.e.ik+250ot:JI+tie CLiu (F) ub 1.:16 11) Originating Lab it) Outfull li 6I3 C:alifnrm, Fecal9223B 06-Nos-15 15:00 C"anrwirers Supplied: ilr25GmIJ' I-Ni Mo (1') Water 28.Oct-15 17:10 Fate Sampled 5u 28-Act-I5 09:15 Comme'siis Received By ; Dice I 1 I'a;a I uF I Page 12 of 12 Invoice To: Republic Services of NC Brian Scott 500 Landfill Road Mt, Gilead, NC 27306 Client Code: RE014 Client ID: Republic Services of NC Client PM: Brian Scott PO#: 4399332 ENCO Cary 102-A Woodwinds Industrial Court Cary, KC 27511 919.467,3090 INVOICE NwICO Invoice Number: C5KO636 Invoice Date: 06-Nov-15 Project: Project Number: Date Received: Uwharrie Stormwater [none] 28-Oct-15 Invoiced by: SPF Remit To: Work Order(s): C513829 Environmental Conservation Laboratories, Inc. 10775 Central Port Drive Orlando, FL 32824 Terms: NET 30 Quantity Analysis/Description Matrix Unit Cost Extended Cost 7 COD SM5220D Water $30,00 $210.00 7 TSS SM2540D Water $12.00 S84,00 l O&G 1664A Water $55.00 $55.00 4 Coliform, Fecal 9223B Water $35.00 $140.00 Invoice'lbtal: S489.00 Page 1 of 1 Pursuant to ENCO Standard Terms and Conditions, a fee of 1.5% per month may be applied for late payment. ♦ I Page 1 of 1 ;' . Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted CERTIFICATE OF COVERAGE NO. NCG120051 FACILITY NAME _Uwharrie Environmental COUNTY _Montgomery PERSON COLLECTING SAMPLES Brian Scott LABORATORY ENCO_Labs = Lab Cert. t# Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR�2025 SAMPLE PERIOD X Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA REC� ❑Zero -flow ❑Water Supply ❑SA L� X Other C JON'] 1 2015 MMMAORWRN T" momnp i UW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 X No discharge this period?z Qutfall No. Date Sample Collected {mo/dd/yrl 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 2 513 6B 7A 7C 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report_ Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General permit text Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 }-. :P'dFt B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. X No discharge this period?Z Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 7B Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO X IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an odainal and one covv of this DMR. including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitorine Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted 10/27/2014 CERTIFICATE OF COVERAGE NO. NCG120051 MPLE COLLECTION YEAR __2014 RECE1 V ]PERIOD ElJan-JuneX July -Dee FACILITY NAME _Uwharrie Environmental AMPLE or ❑ Monthly'_ (month) COUNTY —Montgomery OCT 2 9 2014 DISCHARGING TO CLASS ❑ ❑ []Trout HQW Trout iPNA PERSON COLLECTING SAMPLES _Brian Scott ❑❑ CENTRAL FILES Zero- ❑ flow Water Supply []SA LABORATORY ENCO_Labs _ Lab Cent. #_C406774 pWR SECTION x Other c Comments on sample collection or analysis: Part A: 5tormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE ,l ❑ No discharge this period?' Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, inches3mtcal Oxygen Demand Fecal Goliform Total Suspended Sands Benchmarks => _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 No Discharge 2 No Discharge 58 10/14/14 IN 10 >4.0 1.6 613 10/14/14 .1" 25 727 36 7A No Discharge 7C No Discharge k Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example. do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">)W. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Permit Date:11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 F-1 1Vo discharge this period?' Outfaii No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, IncheS3 Nowpolar 0&G/TPH by EPA 1664 (SGT HEM) Total Suspended Solids pH Benchmarks => _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 7B No Discharge Footnotes from Part A also apply to this Part 8 Note. If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one coaicofthis AMR including all " Vo Discha_rrge:p rft within 30 days of recelnt of the lab results for at end of monitoring period in the case o 'Wo Aischa e" re its to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." lt,4-z G (Signature W Permittee) Permit Date:11/1/2012-10/31/2017 —Z7— iy (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 0 .ENCO Laboratories Accurate. Timely. Responsive Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, October 21, 2014 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt, Gilead, NC 27306 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Uwharrle Stormwater ENCO Workorder(s): C406774 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, October 14, 2014. Unless otherwise noted In an attached project narrative, all samples were received In acceptable condition and processed In accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received b/ the laboratory, and may only be reproduced In full. Page t of 7 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE talent [D: Outrall # S B Lah ID: C406774-01 Sampled- 10/14/14 02:00 Received: 10/14/14 12:10 Paramate[ SM 254OD-1997 Hold Dam/Tune[ 10/21/14 Prep DaWTIme(s) 10/15/14 AnalNmis Date/33MC a] 09:35 10/15/14 09:35 SM 5220D-1997 11/11/14 10/17/14 15:19 10/17/14 18:47 Cllent [D: Outtall # 6 B Lab [Di C406774-02 Sampled: 10/14/14 08:20 Received: 10/14/14 12:10 Parameter SM 254OD-1997 aQJd DataCTlme[s] 10/21/14 Prelp 10/15/14 Analvsle Dace/Tlme[sl 09:35 10/15/14 09:35 SM 5220D-1997 11/11/14 10/17/14 15:19 10/17/14 18:47 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 2 of 7 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall # 5 B Lab M. C406774-01 ADande Chemical Oxygen Demand Total Suspended Solids Results 10 1.6 Ella HM 10 1.0 Ea 10 1.0 1lnits mg/L mg/L Me91211 1ynt�s SM 5220D-1997 SM 2540D-1997 Client 10. Oumll # 6 B Lab 1D: C406774-02 ADalde Chemical Oxygen Demand Total Suspended Solids Eesuft 25 36 Flag a" 10 1.0 Em 10 1.0 1Wxs mg/L mg/L � ile1SS SM S220D-1997 SM 254OD-1997 FINAL This report relates only to the sample as received b/ the laboratory, and may only t1a repmduced In full. Page 3 of 7 www.encolabs.com ANALYTICAL RESULTS Description: Outfall # 5 B Lab Sample IDC406774-01 Received: 10/14/14 12:10 Matrix: Water Sampled: 10/14/14 08:00 Wart Order: C406774 Project: Uwharrie Stormwater Sampled By: Brian I Scott Classical Chemistry Parameters ^ - SWO Lary aWbW areWfAC 591j Analvte rCAS Number] Ji=Lfts ELM iiflit6 1E Hu 1L 1111211 memo 19130lltzed Chemical Oxygen Demand 10 mg/L 1 10 10 4117016 SM 5220D-1997 10/17/14 18:47 30C Total Suspended Soiids 1.6 mg/L 1 1.0 1.0 431SO04 SM 2540D-1997 10/15/14 09:35 MMR Description: Outfall # 6 B Lab Sample ID:C406774-02 Received: 10/14/14 12:10 Matrix: Water Sampled* 10/14/14 08:20 Work Order: C406774 Project: Uwharrie Stormwater Sampled By: Brian ] Scott Classical Chemistry Parameters ^ .,gVC0 Lary aeitlf d Analyta(CAS Number] Chemical Oxygen Demand Total Suspended Solids Resu fla ilnm DE Hu Ml. atch Method Analyzes MX Notes 25 mg/L 1 10 10 4117016 SM 52200-1997 10/17/14 18:47 30C 36 mg/L 1 1.0 1.0 4115004 SM 2540D-1997 10/15/14 09:35 MMR FINAL This report relates only to the Sample as received by the laboratory, and may only be reprodww In Aril. Page 4 of 7 4t1f � www.enc0labs.cam QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Balkh Q715004 - NO PREP blank (43 15004-BLK1) Prepared & Analyzed: 10/ 15/2014 09:35 Spike Source %REC RPD AnaResult Elm POL Units Level Emit %REC LIMI RPD Lima Notes Total Suspended Solids 1.0 U 1,0 mg/L LCS (4115004-BSI) Prepared & Analyzed: 10/15/2014 09:35 Spike Source %REC RPD .Anahfis Result Flaa POL Units level Result %REC Limits RPD 161611t Notes - Total Suspended Solids 96 1.0 mg/L 100 96 80-120 Duplicate (4315004-OUP1) Prepared & Analyzed: 10115/2014 M35 Source: C406774.01 Spike Source %REC RPD .Anah to Result Flag POL Units Level R %REC 1,jM' RPD Limit Notes - Total Suspended Solids 1.2 1.0 mg/L 1.6 29 10 QR-04 Duplicate (4315004-DUP2) Prepared & Analyzed; 10/15/2014 09:35 Source: C406774-02 Spike Source %REC RPD .AnalyM Result Elaa POL Units Level Rat %REC Lb= RPD Lim Notes Total Suspended Solids 37 1.0 mg/L 36 2 10 Ator" Q717O16 - Same Blank (4)17016-BLKI) Prepared: 10/17/2014 15:19 Analyzed: 10/17/2014 18;47 Spike Source %REC RPD .Analvte Result Elan POL Units Level Resul %REC Liml RPD Ljmjt Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (4317016-BSI) Prepared; 10/17/2014 15:19 Analyzed: 10/17/2014 18:47 Spike Source %REC RPD Anal 1fte Result Elm POL Units Level RpyAf %REC Lh= RPD UMIL Norte Chemical Oxygen Demand 510 10 mg/L S00 103 90-110 Matrix Spike (4317016-MSC) Prepared: 10/17/2014 15:19 Analyzed: 10/17/2014 18:47 Source: C401834-01 Spike Source %REC RPD Anal Result Elm P-Ol. Unite Level Befit %REC LIm1M RPD Llglit 021110 Chemical Oxygen Demand 690 10 mg/L 500 200 97 90-110 Matrix Spike Dup (4317016-MSD1) Prepared: 10/17/2014 15:19 Analyzed: 10/17/2014 18:47 Source: C401834-01 Anallde Chemical Oxygen Demand Spike Source %REC Result Elaa POL Units Level Rauh %REC Limits RPD 670 10 mg/L 500 200 94 90-110 2 RPD Limit New 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 of 7 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (850k or greater confidence) to make a "tentative identification". QR-04 Duplicate precision outside acceptance limits due to low analyte concentration. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 6 of 7 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Cenlral Port Dr. 4810 E.uxllti-,ra Park Court, Suite I 1 302-A WDod Antl=_ Industrial Cf. Odarda, FL 32024 Jaeksannrte. F, 3118-G0(Ei9 ' Cary. PFC 27511 (407) 826-531A Fax i LIF) [964) 296-3007 Fdx [9Ca) 295#i2W ;a193 s67-3D% Fax 19191 46: -3E F5 Page of 1_ Client Name Prom Nu,.ber Requested Analyses Requested Turnaround ___-- - — limes — r�} ��4-+ r'� Projectt Address L=are- sc Nall Rush rerur-_Mt �,hr. - w � .) '4r1 i:I-r ar-. _ ._..__ - - �PO U:lt�8'rir�_�,iC, lTjjy��a�?I- _ I .vc�,+ancx 3n meraci!i� t 1 Bit!ng Into Csiy'ST17rp M,. Giiea+dr_ JC 2 -�6 -- - —� 207 "':-02&5w-1046 --- -- .�. Ci I i -- Standard T6 Far Rel7onsrr C<Xtacs [-tii :it 7-3Er SFa,= Sr.^1 �r C r} 1 _-- expedited -------__ Samplers) Nan16. Af}r on (Pn:rr) t° _ __--- —----__--_ I g:Ilin3 C«:tar.:. 1 \i I Due f ✓`r �� �ii�ii�----�- B.ian `.3c,�tS Jt � � � J- - -- --- Sanwivrls) SVnalurC ---- -- --- — -- - 5de LaCari ✓r. r I lm,) Zon? r -- Lao t 6iiSOrdeF Preservation ! Ssi GOd'2 =7 IC.in i bii:e a5 r i'r%:t-_ sal : Itml a sa,:.0ID (Fie!d Crdlecdor De:e ' Cr.ledrm — scvm Cat- Mar x See cotes) rota, P of Cona;=l: �, _ Sample Comments e {{{ _ 11 f1311_____ __._ fr', -. 6 ii I X _ i .I 1._.X_ 1.tttf�3114 1P!A X A IX X % r I f 1 '—. 1 1 i 4 of conlaifiefs 1 Sa%gc Kr. Pr -pared df By f i D.mn: ri , ; (',ry. r1r7;PRl�: $['Prla! R[:SRirinr) f"v+((t�Fr B?Tr_i115 r�SRt�'SChC(,' �V --•! Y r, Ddierc r^H SPr�,: �: $j' — J _--_' _ D:itC/7rNM? Re1-�*_uF ha0 Ey Dta -:lf`u r ii!CLirvc3 Datetrrre Code:• a'. 3 Tinrpls ,0eceipt rs grtln r7r�:ei;;1 Acceotab[e Unarceptadte !Z atrix . Gw-Gto.md^alar SO-SC,n DW-U nkirc dater SE -Sediment SW-SJrLI._e Waler WW-4Ja51a-AQ1cr A -Air O-O'her tdelas i•! tw...,mwn) Preservation: I Irr 'r--=cr W ihi ,03 S I-QSrLI N".--tH D-G!her .rteiei in W,.!renic) . dole Ad wrrk.R s subm :led to E,1CO _atx� ere in nt.rrndaele:e vr'h trte IPfr115 hrrd c(�+li•if6 !r5tad r: t^>n SC Lr3i` cr !tip 7f-n- urir.5s gr.U+ e:+,•tt�l .g•te-ne:rls ex�sl Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted June 10, 2014, CERTIFICATE OF COVERAGE No. NCG120051 FACILITY NAME _Uwharrie Environmental COUNTY _Montgomery PERSON COLLECTING SAMPLES _Brian Scott LABORATORY ENCO_Labs _ Lab Cert. # C313049 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 RECEIVED" PERIOD X Jan -June El July -Dec V or ❑ Monthly month ,SUN 17 2014ASCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA CENTRAL FILES X Other C DWQIBOG PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?' OutFall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 1 5/30/24 .7 31 27 32 2 No Discharge --- --- --- --- 5B 5/30/14 .7 23 27 36 613 5/30/14 .7 23 364 42 7A No Discharge' --- — -- --- 7C 5/30/14 .7 10 <4.0 1.6 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me1L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement rer 1, 7ier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Permit Date: 11/1/2012-10/31/2017 SWU-24$, last revised 10/25/2012 Page 1 of 2 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches} Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU 713 5/30114 .7 2.40 24 6.19 Footnotes from Part A also apply to this Part B Note. If you report a sample value in excess of the benchmark, you must implement Tier 1, Trer 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DMR. includina all allo Dischame" renorts. within 30 days of receipt of the lab results for at end of monitorina period in the case of ®No Dischame'°'rei Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of & —1 (Date) Permit Date. 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 ENFIM�N- CO Laboratories Accurate. Timely. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, June 6, 2014 Republic Services of NC (RE014) Attn: Brian Scott 500 Landfill Road Mt. Gilead, NC 27306 RE: Laboratory Results for Project Number: [none], Project Name/Oesc: lJwhar ie Starmwater ENCO Workorder(s): C313049 Dear Brian Scott, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 30, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained In this report are in compliance with NELAC standards, except as noted In the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCQ Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith For Stephanie Franz Project Manager Enclosure(s) RM This report relates only to the sample as received by the taborarury, and may onM be reproduced in hull, page 1 of 9 www.encolabo.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall # i Lab ID: C313049-01 Sampled: 05/30/14 08:00 Received: 05/30/14 11:17 Parameter SM 254OD-1997 Hold Date(]p W 06/06/14 Peen DataITlmelal 06/03/14 Anelvsfs Date/Time(a) 08:22 D6/03/14 08:22 SM 522OD-1997 06/27/14 06/05/14 16:17 06/05/14 18:52 Client ID: Outfall # SB Lab ID: C313049-0I Sampled. 05/30/14 07.40 Received: 05/30/14 11:17 Paranwfla SM 254OD-1997 Hold Date/Time(al 06/06/14 Prep Date/T1me(e) 06/03/14 0812 06/03/14 08:22 SM 5220D-1997 06/27/14 06/05/14 14:10 06/05/14 18:52 Client ID: Outtall # as Lab ID: C313049-03 Sampled: 05/30/14 08:20 Received: 05/30/14 11:17 Parameter SM 254OD-1997 Hold Date/Timelal 06/06/14 06/03/14 te/Timelal 0B:22 06/03/14 08:22 SM 52201)-1997 06/27/14 06/05/14 14:10 06/05/14 18:52 Client ID: Outfell # 78 Lab ID: C313049-04 Sampled: 05/30/24 08:40 Received: 03/30/14 11:17 PAMMater EPA 1664A Hold DatelTime(el 06/27/14 P 06/05/14 Anelysla Datel7lme(sl 12:30 06/06/14 11:06 SM 254OD-1997 06/06/14 06/03/14 08:22 06/03/14 08:22 SM 4500H+B-2000 05/30/14 08:54 05/30/14 15:10 05/30/14 15:10 SM 5220D-1997 06/27/14 06/05/14 14:10 06/05/14 18:52 Client ID: Outfail # 7C Lab ID: C313049-05 Sampled- 05/30►14 00.50 Received: DS/30/14 11:17 paramateir SM 254OD-1997 HolQQgtefflme(sl 06/06/14 Prep Data/Tlma(al 06/03/14 08:22 06/03/14 08:22 SM 5220D-1"7 06/27/14 06/05/14 14:10 06/05/14 18:52 FINAL This report relates only to the sample as recetved by the laboratory, and may only be reproduced In full. Pape 2 of 9 wwww.encolabs.com SAMPLE DETECTION SUMMARY Chant ID: Outfall # 1 Lab M. C31304"1 Anahrm Bomb Flea MQL EQL vam Meth9d N Chemical Oxygen Demand 31 10 10 mg/L SM 5220D-1997 Total Suspended Solids 32 1.0 1,0 mg/L SM ZWD-1997 Ghent ID: Outfall # SB Lab ID: C313049-02 Analyte Saslllta Ele9 MIL EQL gnu Method atl= Chemical Oxygen Demand 23 10 10 mg/L SM 5220D-1997 Total Suspended Solids 36 1,0 1.0 mg/L SM 254OD-1997 dlent ID: Outfall # 68 Lab ID: C313049-03 Anabu Route Fle4 MQL EQL ihtita Mathsld Chemical Oxygen Demand 23 10 10 mg/L SM 5220D-1997 Total SuspendedSoltds 42 1.0 1.0 mg/L SM 254OD-1997 Ghent ID: Outfall # 76 Lab ID: C313049-04 BOellde B06YEti an Hu ML Nnite Method l� Chemical Oxygen Demand 31 10 10 mg/L SM 5220D-1997 pH 6.7 1.0 1.0 pH SM 4500H+9.2000 Q Total Suspended Solids 24 1.0 1.0 mg/L SM 254OD-1997 awn ID: Outfall # 7C Lab ID: C313049-03 Anabu ROMRS an Hu EQL Unite Method H91e5 Total Suspended Solids 1.6 1.0 1.0 mg/L SM 254OD-1997 FINAL TMs report relates any to the sample as reoeNed by the laborstnry, and may only be reproduced in full. Page 3 of 9 � wir www.encolabs.com ANALYTICAL RESULTS Description: Outfall # 1 Lab Semple ID:C3I3049-01 Received: 05/30/14 11:17 Matrix: Wafter Sampled. 05/30/14 08:00 Work Order: C313049 Project: Uwhanie Stormwater Sampled By: Brian 3 Scott jClassical Chemistry Parameters j Ana[ya[CASNumbed Resul6 En unita RE MQL EQL Batch Method Anabized a 184t89 Chemical Oxygen Demand 31 mg/L 1 10 10 4FOS022 SM 5220D-1997 06/05/14 18:52 JOC [ECL-0035] ^ Total Suspended Solids [ECL-0169]^ 32 mg/L 1 1.0 1.0 4FO3001 SM 2549D-1997 06/03/14 08:22 MMR Description: Outfall # 5B Lab Sample ID:C313049-02 Received: 05/30/14 11:17 Matrix: Water Sampled: 05/30/14 07:40 Work Order: C313049 Project: Uwharrie Stormwater Sampled By: Brian 3 Scott Classical Chemistry Parameters ^ - 6=Cary mVAud arw6ft (AC 5411 Anah te_fCAS Nurntwl Raffidw Eft Chemical Oxygen Demand 23 [ECL-0035]^ Total Suspended Salida [ECL-0169]^ 36 Oma4ption: Outfalt # 6B Matrix: Water Project: Uwharrle Stormwater MwI6 DE En EQL Batch Method Analyzed BY !dam mg/L 1 10 10 4FOS022 SM 5220D-1997 06/05/14 18:52 JOC m9/1. 1 1.0 1.0 4FO3001 SM 254OD-1997 06/03/14 08:22 MMR Lab Sample ID:C313049.03 Received: 05/30/14 11:17 Sampled: 05/30/14 08:20 Work Order: C313049 Sampled By: Brian 3 Scott Classical Chemistry Parameters ^ - ewx Cwy ceartld~ (AC 011 AnaMte rCAS Numberl Rundu la U" Df Hu EQL Aillub Method Ana ft fi= Chemical Oxygen Demand 23 mg/L 1 10 10 4F05022 SM 5220D-1997 06/05/14 16:52 JOC [ECL-0035]^ Total Suspended Solids [ECL-0169]^ 42 mg/L 1 1.0 1.0 4FO3001 SM 2540D-1997 06/03/14 08:22 MMR 7P"'Dn, Outfall # 7B Lab Sample ID:C313049-04 Received: 05/30/14 11:17 trTx:Wader Sampled:05/30/14 08:40 Work Order: C313049 ect: Uwharrle Stormwater Sampled By: Brian 3 Scott Chemistry Parameters ^ - scm C&Ya Lrdad-440/AC s1l Aneivte rQ5 Numtasrl gpl = EAg yg[[g of - K" Mi. ankh mound AnalX&Qd a 0= Chemical Oxygen Demand 31 mg/L 1 10 10 4FOS022 SM 5220D-1997 06/05/14 18:52 JOC [ECL-0035]^ pH [ECL-0062]^ 6.7 pH 1 1.0 1.0 4E30026 SM 4500H+6-200C 05/30/14 15:10 MMR Q Total Suspended Solids [ECL-0169]^ 24 mg/L 1 1,0 1,0 4F03001 SM 254010-1997 06/03/14 08:22 MMR Classical Chemistry Parameters Anaivte rCAS Numberl AM&I EAS UUM DE HU EQL ankh 901111111111 snb=d a Nl= Oil & Grease (HEM) [C-0007] 2.40 U mg/L 1 2.40 5.00 4FOS006 EPA 1664A 06/D6/14 11:06 MJF FINAL This report relates only to the sample as reoeMed by the laboratory, and may only be reproduood In full. Pape 4 of 9 www.enoolabs.com ANALYTICAL RESULTS Description: Outfall # 7C Lab Sample ID: C313049-05 Received: 05/30/14 11:17 Matrix: Water Sampled, 05/30/14 08:50 Work Order:C313049 Project: Uwharrie Stormwater Sampled By: Brian ) Scott Classical Chemistry Parameters ^- MM C2ry mKlAlea' nsyta CAC 59i] Anahrtn rraS NuM&W Results an unb DE t!' u PQL @HUU MmMpd Anahmed a Now Onmiml Oxygen Demand [ECL-0035]^ 10 u mg/L 1 10 10 4FO5022 SM 522OD-1997 06/05/14 18:52 ]OC Total Suspended Solids [ECL-0169]A 1.6 mg/L 1 1.0 1.0 4FO3001 SM 254OD-1997 06/03/14 08:22 MMR FINAL This report relates only to the sample as rcoehred by the laboratory, and may only be reproduced In full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batialr 41530=6 - NO PREP LCS (4E3(026-B51) Prepared & Analyzed: 05/30/2014 15:10 Spike Source %REC RPD Analvta Result Flaq POL Unite Level BOOR %REC )iMfa Rpb Limit Notals PH 6.9 1,0 PH 7.01 99 99-101 Duplicate (4E30026-DUPi) Prepared & Analyzed: 05/30/2014 IS: 10 Source,C313049-04 Spike Source %REC RPD �oande R110111 an eal. Units Leval Emma %REC Llmtla RPD Limit PH 6.6 1.0 pH 6.7 0.3 25 Bartell 4F0300S - NO PREP Blank (4F03001-ELKS) Prepared & Analyzed: 06/03/2014 08:22 Spike Source %REC RPD AnWvto Result Raq POL Unite Level BMA& %REC Llmlts RPD amlt Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (4F03001-BSI) Prepared & Analyzed: 06/0312014 08:22 Spike Source %REC RPD Analvte Result 19M POL Units Level 609Ytt %REC Limbs RPD Jet Note8. Total Suspended Solids 98 1.0 mg/L 100 98 80-120 Duplicate (4F03001-DUPi) Prepared & Analyzed: 06103/2014 08:22 Source:C313049-01 Spike Source %REC RPD �nandn Result Hat POL Units Laval BCj %REC "Mb RPD Limit JOWL Total Suspended Solids 28 1.0 mg/L 32 11 10 QM-12 Duplicate (4F03001-DUP2) Prepared & Analyzed: 06/03/2014 08:22 SourcetC313049-02 Spike Source %REC RPD Anaivte Result Fiat POL UnRa Level BMW %REC Limits RPD Limit Il=L Total Suspended Solids 24 110 mg/L 36 37 10 QM-12 94rfdh 4 FOSM - Mme Blank (4FOS022-BLK1) Prepared: 06J05/2014 14:10 Analyzed: 0610512014 18:52 Spike SOUR* %REC RPD Analvte Reetdt Flaq POL Units Leval Basch %REC LIMIts RPD Lmit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (4F05022-BSI) Prepared: D6/05/2014 14: W Analyzed: 06/05/2014 18:52 Spike Source %REC RPD Anatvtn Milli ELM PAL units Level Butt %REC j MM RPD u[mlt t!Qffit Chemical Oxygen Demand Sw 10 mg/L Sw 100 90-I10 Matrix Spike (41FOS022-MSI) Prepared: 06/65/2014 16:17 Analyzed: 06/05/2014 18:52 Source:C313049-01 Analrle Chemical Oxygen Demand Spike Source %REC Result Ft" POL Units Laval 821111111 %REC 1Jmlbt RPD 520 10 mg/L 500 31 99 90.110 RPD Limit Now FINAL This report relates only W the sample as reoeMad by the laboratory, and may only be reproduced In full. Page 6 of 9 www.encolabs-com QUALITy CONTROL DATA Classlcal Chemistry Parameters - Quality Control BadaA 4 FOSM - aims - QoW67000 Matrix Spike Dup (4F05022-MSDi) Prepared: 06/05/2014 16:17 Analyzed; 06/05/2014 18:52 Source:C313049-01 Spike Source %REC RPD JAnafwft Result Fiaq POL Unlb Level Rena %REC LlMIU RPD Umit Notes Chemical Oxygen Demand 510 10 mg/L 500 31 97 90.110 2 10 Classical Chemistry Parameters - Quality Control Batch 4fDFM - SMA 1"M Blank (4FDS006-BLKi) Prepared: 06/05/2014 12:30 Analyzed: 06/06/2014 11:06 Spike Source %REC RPD Aoallma Spelt Elea Pfll. Ualt Level Read %REC JJnfiW RPD Umft tiotes 00 & Grease (HEM) 2.40 U 5.00 mg/L LCS (41FC5006-11Si) Prepared: W0512014 12:30 Analyzed: 06/06/20m 11:06 Spike Source %REC RPD Anal lAe news EiN OIL ualta Level BfSYIt %REC UMUg RPD U� hones Oil & Grease (HEM) 41.6 5.00 mg/L 41.3 101 78-114 LCS Dup (4F05006-BWI) Prepared: 06/05/2014 12:30 Analyzed: 06/06/2014 11:06 Spike Source cVbREC RPD Anrdvte Result RM POL Unks Level Bend %REC JIMb RPD Ljpljt Notes Oil & Grease (HEM) 40.6 5.00 mg/L 41.1 99 78-114 2 18 Matrix Spike (4F05006-MS1) Prepared: 06/05/2014 12:30 Analyzed: 06/06/2014 11:06 Source: B402501-01 Spike Source %REC RPD Analvte Result Flag POL UnRs Level agad %REC Lialft RPD LIMIS Natal Oil& Grease (HEM) 47.1 5.76 mg/L 46.2 2,76 U 102 78.114 FINAL. This report relates only to the sample as receNed by the laboratory, and may only be reproduced In full. Page 7 of 9 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The anaW was detected In the associated method blank. O The sample was analyzed at dilution. a The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the Instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quandtatlon limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, In the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Q Analysis performed outside of method - specified holding time, QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relahes only, to the sample as renewed by the laboratory, and may only be reproduced In full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.c�n • .:.� c '} "i -� 10775 Central Purl Dr. 4610 Executive Para. Court, Suite Ill 102-A Woedwtnds Indu5wl Ct. a •, '� ti- _ _ _ Odarotlo_ FL 32824 jadC,anv4le. FL 32215-60G9 Cary. NC 27511 ._...,...'Gi'F,, - ,u 3. ,. - .'R . +.� (407) 626-5314 Fax J407} 650-69&5 f904} 2953007 Fax t90a1296�210 19191487-3Q90 Fax (Si91457-35t5 Page Of Cuero Name P-rNA Number Bequestad Analyses Requested Turnaround Times Nutt' . Rush requests Subpa 6 acceptance oy ttw tac ldy Standard Expedited _I 1 Due - - - _ _ ` -- j F E _ Ii Address Profect Nameuesc CaylSrlZp _ PO . 1 Bilking htlo , Tel Fax _ Reporting Contact Sar+r FAtii6atiog (Prvt1) �✓/h�77/1 &lr.ng Ca+tacl s.,A Locabw r Tme tome Lab Worlcorder r Preservation (See Codes) (Gorabine as necessary) Urn tr Sampte 10 (r-field Wernibcatmn) coaedwm Dale Cd'Pcmon Time Camp r Grab MaD- )see codes) Total 6 of Contwoors Sample Comments L. x 5 7 - JII .=:t Q _ i 1� t - - t < Total # of Containers M By a R rid By Dater{ime Re 61 Dat01T Repotting Recluiremants ` [ �• l RaAnquished By DateTme Rece co _ , Datelrime Relirquished By DaterTrme Received By Date-?ime Cooler s's & Temps ran - n (',amdition Upon Receflx AcceptaUe _ Unacceptatke Yavix - GW-Groundw4der SO -Sal OW-Orw& ng Water SE -Sediment SW -Surface Water W W-Wastewalcu A -Air O-Ocher #detall in comments] Presom lom 1-ice H-FICI N-HNO3 SR2SO4 NO-Na0H O.Other (detail in commerts) Note : AN sa:rples subirmted to ENCO Labe are in acc urdax,° with the terms and cergdtions ))sled on the rtxrse of this Wm. unless prior written agrasments exibt