NCG120045_COMPLETE FILE - HISTORICAL_20161217

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V C� � � bbl.� rj
DOC TYPE
bd HISTORICAL FILE
❑ MONITORING REPORTS
DUC DATE
,-7
❑ c2 0 , 6 / a` 1
YYYYMMDD

jp� ENCO Laboratories
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Saturday, December 17, 2016 NRepublic Services of NC (RE016) /
Attn: Tammy Mitchell
East Carolina Environemntal, 1922 Republican Road
Aulander, NC 27805
RE: Laboratory Results for
Project Number: [none], Project IName/Desc: Stormwater
ENCO Workorder(s): CZ17981
Dear Tammy Mitchell,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, December 6, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Stephanie Franz
Project Manager
Enclosure(s)
CENTRP,L FILES
DWR SECTION
FTNAL This report relates only to the sample as receMed by the laboratory, and may only be reproduced In full. I Page 1 Of O

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Giant ID: Outfall H-1
Lab ID: CZ17981-01
Sampled: 12/06/16 10:30 Received: 12/06/16 15:43
Parameter
EPA 1664A
Hold -Qatafflmefs]
01/03/17
Prep DatelTimofsl
12/13/16
AnalysisDate171me{al
17:20 12/14/16 15:19
Field
12106/16 10:44
12/06/16
10:30 12/06/16 10:30
SM 2540D-1997
12/13/16
12/07/16
09:40 12/07/16 09:40
plant ID: Outfall 1
Lab ID-. CZ17981-02
Sampled: 12/06/16 10:10 Received: 12106/16 15:43
Parameter
EPA 1664A
Hold Date/Tlmefs
01/03/17
12/13/16
AnallWa Datel-nmefsl
17:20 12/14/16 15:19
Field
12/06/16 10:24
12/06/16
10:10 12/06/16 10:10
SM 254OD-1997
12/13/16
12/07/16
09:40 12/07/16 09:40
SM 522OD-1997
01/03/17
12/08/16
14:27 12/08/16 18:30
plant ID: Outfall 2
Lab ID: CZ17981-03
Sampled: 12/06/16 10:20 Received: 12106/16 15:43
Parameter
EPA 1664A
Hold Date/Tlmefs
01/03/17
12/13/16
AnalysisDatelTimefsl
17:20 12/14/16 15A9
Field
12/06/16 10:34
12/06/16
10:20 12/06/26 10:20
SM 254OD-1997
12/13/16
12/07/16
09:40 12/07/16 09:40
SM 522OD-1997
01/03/17
12/08/16
14:27 12/08/16 18:30
FINAL This repot relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 Of 10

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SAMPLE DETECTION SUMMARY
Client ID: Outfall H-1
Lab ID:
CZ17981-01
Analyle
Results
fin
M"
ML
!l011i
Clioih� 111QL�9
Oil & Grease (HEM-SGT) Non -Polar Material
19.3
2,70
5.00
mg/L
EPA 1664A
PH
7.53
0
0
pH Units
Field
Total Suspended Solids
10
510
5.0
mg/L
SM 2540D-1997
client ID: Outfall 1
Lab ID:
CZ17981.02
ADffi]d0
S4sulte
fin
Ml?L
E"
llnlffi
Method l'1=
Chemical Oxygen Demand
60
10
10
mg/L
SM 5220D-1997
Oil & Grease (HEM-SGT) Non -Polar Material
3.63
1
2.70
5.00
mg/L
EPA 1664A
PH
7.69
0
0
PH Units
Field
Client ID: Outfall 2
Lab ID:
CZ17981-03
AOHL1tW
SesulI0
F199
M"
EQL
unib
Method full
Chemical Oxygen Demand
310
10
10
mg/L
SM 52200-1997
Oil & Grease (HEM-SGT) Non -Polar Material
17.4
2.70
5.00
mg/L
EPA 1664A
PH
7.92
0
0
pH Units
Feld
Total Suspended Solids
45
33
33
mg/L
SM 254OD-1997
FINAL This repot relates onty to the sample as receNed by the laboratory, and may Dnly be reproduced in full. Page 3 Of 1 O

CS
N,'k'
9
s
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ANALYTICAL RESULTS
Description: Outfall H-1 Lab Sample ID:CZ17981-01 Received: 12/06/16 15:43
Matrix: Ground Water Sampled: 12/06/16 10:30 Work Order: CZ17981
Project: Stormwater Sampled By: Matt Elnsmann
Chemistry Parameters
A -&JWQVya XaWJAc5911
Analvte rCAS Numbed Results Elm !Malta pF !v U p" Bad Method Analyzed By No
Total Suspended Solids, 10 mg/L 2 , 5.0 5,0 6L07002 SM 25400-1997 12/07/16 M40 MMR
Field Parameters
Analyte rCAS Numberl Result ElAg Mob of KU EU A= Method Analyg By No
PH 7.53 pH Units 1 0 0 6LO7008 Field 12/06/16 10:30 CLI
Classical Chemistry Parameters
Analyte rCAS Numbed
On & Grease (HEM-SGT) Non -Polar
Resu1an knits QE du Ea a= Method Analyze!) By AIRtIlla
19.3 mg/L 1 2.70 5.00 61-13004 EPA 1664A 12/14/16 15:19 SMA
Description: Outfall 1 Lab Sample I0:CZ17981-02 Received: 12/06/16 15:43
Matrix: Ground Water Sampled: 12/06/16 10:10 Work Order: CZ17981
Project: Starmwater Sampled By: Matt Elnsmann
Classical Chemistry Parameters
^- GYM CwyowwadMO&WIx 5941
$esulie Ein knita QE RM E" Batch Method Analyzed BY tL=
Chemical Oxygen Demand ^ 6o mg/L 1 10 10 6LO8030 SM 522OD-1997 12/08/16 18:30 JOC
Total Suspended SolidSA 2,5 U mg/L 1 2.5 2.5 6L07002 SM 254OD-1997 12/07/16 09:40 MMR
Field Parameters
Anabrte rCAS Numberl Raoul Etas ylytg DE ma EM Batch Method Analyzed By k' glm
PH 7.69 pH Units 1 0 0 6L070as Field 12/06/16 10A0 CLI
Classical Chemistry Parameters
Analvte_fCAS Numberl Results fin knlfa 2E HU P26 Batch Method Analyzed Al 1191111
Oil & Grease (HEM-SGT) Non -Polar 3.63 J mg/L 1 2.70 5,00 6L13004 EPA 1664A 12/14/16 15:19 SMA
Material
Frrw, This report relates only to the sample as received by the laboratory, and may only be reproduced In full. IPage 4 Of =

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ANALYTICAL RESULTS
Description: Outfall 2 Lab Sample ID: CZ17981.03 Received: 12/06/16 15A3
Matrix: Ground Water Sampled:12/06/16 10:20 Work Order: CZ17981
Project: 5tormwater Sampled By: Matt E insmann
(Classical Chemistry Parameters
ulta
EWg Naha
2E
HA
Ply
Ali= Moth gd Analyzed
By d"
Chemical Oxygen Demand^ 310
mg/L
1
10
30
6LOB030 SM 5220D-1997 12/08/16 18:30
3OC
Total Suspended SolidsA 45
mg/L
13.3
33
33
6L07002 SM 2540D-1997 12/07/16 09:40
MMR
Field Parameters
Analvte fCAS Numberl Resulig
Eby unu
DP
MDR
ML
aatlh Math !>d Analyzed
ay h=
PH 7.92
pH Units
1
0
0
6L0700B Field 12/06/16 10:20
CU
Classical Chemistry Parameters
Analvte rCAS Numberrl
Oil a Grease (HEM -SO" Non -Polar
Material
Results flag units DE MDL ML half 1 Method Analriad ax No
17.4 mg/L 1 2.70 5.00 61-13004 EPA 1664A 12/14/16 15:19 SMA
FINAL.
This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 5 Of

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Be" 6107W2 - NO PREP
Blank (6L07002-BLK1) Prepared & Analyzed; 12107/2016 09:40
Spike Source %REC RPD
Analyts Result Flaq POL Units Level Result %REC Limits RPD Ljmit Metes
Total Suspended Solids 215 U 2.5 mg/L
LCS (GLD7002-BS1) Prepared & Analyzed: 12/07/2016 09:40
Spike Source %REC
RPD
Anal lde
Remit Hag e"
Liam
Level Result %REC Limits RPD
limit Notes
Total Suspended Solids
98 2.5
mg/L
100 98 80-120
Duplicate (6L07002-DUP1)
Prepared & Analyzed: 12/07/2016 09:40
Source; CZ16355-01
Spike Source %REC
RPD
Analvile
Result Flag POL
Units
Level Result %REC Liml> RPD
Lunn Notes
Total Suspended Solids
3100 830
mg/L
3500 12
20
Duplicate (61.07002-DUP2)
Prepared & Analyzed: 12/07/2016 09:40
Source:CZ16870-01
Analvte
Total Suspended Solids
Batch OLOSWO - Same
Result Flea POL
280
100
Spike Source %REC RPD
Units Lave! Resin %REC Ld111lta RPD M= Notes
mg/L. 280 0 20
Blank (611.080311 l) Prepared: 12/08/2016 14:27 Analyzed: 12/08/2016 18:30
Spike Source %REC RPD
Anal][te ResLdt Elm ML UnI ti Level Result %REC IJmita RPO Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (6L08030-BSI) Prepared: 12/08/2016 14:27 Analyzed: 12/08/2016 18:30
Spike Source %REC
RPD
Anaiyte
Result Flan
POL
Unite
Level Result %REC LlmltB RPD
Limit Metes
Chemical Oxygen Demand
500
10
mg/L.
500 99 90.110
Matrix Spike (6L08030-MSI)
Prepared; 12/08/2016 14:27 Analyzed: 12/08/2016 18:30
Source: CZ15281-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC IJallts RPD
Unit Notes
Chemical Oxygen Demand
7500
100
mg/L.
5000 2900 93 90.110
Matrix Spike Dup (61.08030-MSD1)
Prepared: 12/08/2016 14:27 Analyzed; 12/08/2016 18:30
Source: CZ15281-01
Spike Source %REC
RPD
Anal YRrp
Result EIM
M
Units
Level Result %REC Lim] RPD
Lima Notes
Chemical Oxygen Demand
7500
100
mg/L
5000 2900 93 90-110 0
10
Classlcal Chemistry Parameters - Quality Control
BaAdi 6L13W# - EPA 16MB
Blank (61.13004-011.Kl)
Prepared: 12/13/2016 11:11 Analyzed: 12/14/2016 15:19
Spike Source %REC RPD
Amltda Rtsslllt Hoe EQL Units Level Result %REC UdMb RPD Lltnit notes
Oil & Grease (HEM-SGT) Nan -Polar Material 2.70 U 5.00 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, I Page 6 of

(ONSol-00)
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 6LI30W - EPA 16646 - Giandnued
LCS (61,13004-BSI) Prepared: 12/13/2016 11:11 Analyzed: 12/14/2016 15:19
Spike Source %REC RPD
Anaivte Result Rao POL Units Level gagul %REC Lima RPD Lbit Notes
Oil & Grease (HEM-SGT) Non -Polar Material 68.7 5.00 mg/L 74.6 92 64-132
LCS Dup (6L13004-1111SDI) Prepared: 12/13/2016 11:11 Analyzed: 12/14/2016 15:19
Spike
Source
%REC
RPD
-Anal! to Result Hag
POL
!!nits
Level
gul %REC
uml RPD
L)t )Notes
Oil & Grease {HEM-SG17 Non -Polar Material 82.3
5,00
mgA
76.9
107
64-132 Is
34
Matrix Spike (GL13004-MS3)
Prepared: 12/13/2016 11:11 Analyzed: 12/14/2016 15:19
Source:SZOS480-01
Spike
Source
%REC
RPD
Analvte Result Flat
POL
Units
Leval
Result %REC
Umb RPD
Umft Notes
Oil & Grease (HEM-SGT) Non -Polar Material 67.3
5.00
mg/L
76.9
5.19 81
64-132
FINAL This report relates only to the sample as receiyed by the laboratory, and may only be reproduced In Full. Page 7 Of O

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
FINAL Thls report relates only to the sample as recerved by the laboratory, and may onty be reproduced In full. I Page 8 of 1 O

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Sample Preservation Verification
ENCO Cary (40
Work Order:
CZ17981
Project:
Stormwater
Client:
Republic Services of NC (RE016)
Project #:
(none)
Logged In:
06-Dec-16 15:49
Logged By:
John C King
CZ17981-01
Cont
T` e '
yp
p
p � °C ecke
�� II ate ime
pH Adjusted,
Reagent Used/Comments
a
;_
Requirement,In,Gontro+�
r; w,Adjusted,
,..
B
250mLA+H28O4
<2_
Y I N A
Y I N I A
C
250mLA+H2SO4
<2
Y / N / t&A
Y / N ! 110 `
CZ17981-02
v
Gont„
. d
Type
res- p
w,•�A 4
p , ec a
A -.. ,R.
a#e me;
pH Adjusted - , e .a
Reagent.UsedlComments
Re ulrementz„alnzContro'I�Adiusted
B
250mLA+H2SO4
<2
Y! N I&
Y I N! A
C
250m1A+H2SO4
<2
Y I N I
Y I N I NA
E
250mLP+H2SO4
<2
LY I N 1 NA •
Y/ IC4 I NA
CZ17981-03
Cant
Type,
,. ,
rea
'-
Requirement
H Checked)
p �..a
tn�Gontrol�
' pHAd)usted:,�x ate ma ,Y
d;
, „..• Adiusted;,Y
Reagent�lised/Comments
.�,�z , r
8
250mLA+H2SO4
<2
Y I N!
Y I N
C
250mLA+H2SO4
<2
YINI
Y I N I &A
E
250mLP+H2SO4
<2
6/ N I NA
Y 1 / NA
Reacient Name ID
1
2
Reacient Name ID
3
4
Reacient Name ID
5
6
Page 10 of Pag
1 c

IaceAnalyticale
(�wim paaelab&CM
December 09, 2016
Ms. Stephanie Franz
ENCO Labs
102 A-Woodswinds Industrial Co
Cary, NC 27511
RE: Project: CZ17981
Pace Project No.: 92322171
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunteraville, NC 28078
[phone]
Dear Ms. Franz:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2016.
The results relate only to the samples included in this report. Results reporte d herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please f eel free to contact me.
Sincerely,
WO- qY l +I i &n
Angela Baioni
angela.baioni@ pacelabs.com
Project Manager
Enclosures
b
9BQA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 11

Pace Analytical Services, LLC
lanemapimle 9800 Kiney Ave. Suite 100
HunteraviHe, NC 2a078078
www.paceraDmm (704)e7s9092
CERTIFICATIONS
Project: CZ17981
Pace Project No.: 92322171
Raleigh Certification Ma
6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification #: 67 North Carolina prinking Water Certification #: 37731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 11

aceAnalytical
aww.pacdebacom
SAMPLE ANALYTE COUNT
Project: CZ17981
Pace Project No.: 92322171
Pace Analytical Services, LLC .
9800 Kincay Ave. Suite 100
Huniersville, NC 28078
[phone]
Analytts
Lab ID Sample ID Method Analysts Reported Laboratory
92322171001 OUTFALL 1 SM 9222D BWJ 1 PASI-R
92322171002 OUTFALL 2 SM 9222D BWJ 1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Ll.C. Page 3 of 11

aceMaViol
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ANALYTICAL RESULTS
Project: CZ17981
Pace Project No.: 92322171
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Hunteravllle, NC 28078
[phone]
Sample: OUTFALL 1 Lab ID: 92322171001 Collecled: 12/0611610:10 Received: 12/06/16 1&30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Focal Coliform RAIL Analytical Method: SM 9222D
Fecal Coliforms 7.0 CFU1100 mL 1.0 1 12/06/16 15:55
Date: 12/09/2016 05:43 PM
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
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aceAnaljftal
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ANALYTICAL RESULTS
Project: CZ17981
Pace Project No.: 92322171
Pace Analytical Services, LLC
9800 KlnceyAve, Suite 100
Huntersville, NC 28078
(704)e76-9092
Sample: OUTFALL 2 Lab ID: 92322171002 Collected: 12/06/16 10:20 Received: 12/06/16 16:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D
Fecal Coliforms 6000 CFU1100 mL 1,0 1 12/06/16 15:55
Date: 12/09/2016 05:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 5 of 11

laneAnalyfical"
wwwpaceAftcom
Project: CZ17981
Pace Project No.: 92322171
QC Batch: 339740
QC Batch Method: SM 9222D
Associated Lab Samples: 92322171001, 92322171002
METHOD BLANK: 1884173
Associated Lab Samples: 92322171001, 92322171002
Parameter Units
Fecal Coliforms CFU1100 mL
SAMPLE DUPLICATE: 1884174
Parameter Units
Fecal Coliforms CFU1100 mL
QUALITY CONTROL DATA
Analysis Method: SM 9222D
Analysis Description: 9222D MBIO Fecal Coliform - RAL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 12/06/16 15:55
92322130001 Dup
Result Result RPD Qualifiers
ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are h the units Indicated by the "Units" column except Ahera an alternate unit Is prosonted b the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 05:43 PM without the written consent of Pace Analytical Services, LLC.
Page 6of11

Pace Analytical Services, LLC
9800 KinceY Ave. Sute too
aceMalX caje
Huntersville, NC 28078
wwwPacelahs.mm
(704)8759092
QUALIFIERS
Project: CZ17981
Pace Project No.: 92322171
L1c1V1:Il11161: -9
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MIX - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazino decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte Is
a combined concentration,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamino using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/0912016 05:43 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 11

acaAnalytical
YMWWP0cWgb&c0M
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CZ17981
Pace Project No.: 92322171
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92322171001 OUTFALL 1 SM 9222D 339740
92322171002 OUTFALL 2 SM 9222D 339740
Date-. 12/09/2016 05:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 8 of 11

Laboratory receiving samples:
Asheville [] Eden[]
Document Name:
Cdhditlon Upon Rec
oocumentNo.:
nnCUMeat Revised: Sept. 21, 2016
page 1 of 2
Greenwood Q Huritersville ._
issuing Authority:
Pace Quality office'
Client Name: Project M.• WO# : 923221 i 1
Courfer. Fed dar Dun Dusn
j] Commercial []Pace ❑other: 92322171
Custociy5eal Present? []Yes JJk0 Seals Intact? []Yes " AD
Dale/Initials Parson pransinhg CondMs: �
Packing Material: DBubble Wrap ❑Bubble Bags aN 0 a ❑Other;
Thermometer
/� IR Gun iD S•qV: Wet ❑Blue ❑None kramples an ice, coeBngprocess has begun
correction F'..rjW #r Cooler Temp Corrected ('Q, alp Biological Tissue Frozen? QYes . []NO kN/A
Temp should be above fLWIng to 6T
USDA Regulated Soil ( [A, water sample)
Did samples originate in a quarantine zone within the United States: Ck NY, or SC (check maps}? did samples odginwafrom a foreign source (lntemati rQW,
Clyes tfto indudini Hawaii and Puerto Me)? []Yes ❑No
mm es Arrivea within Hoia lime?
YeLINO
N A
2.
ShpstHofdTime
Yes
13No
N ih
3.
Rush Turn Around Time R ueated?
Yes
21r,
N A
4.
Sufficion tvolume?
es
No
HA
S. '
Correct Containers Used?
1[JYe
❑Ho
❑N/A
6.
-Pace Containers Used?
Y
QNO
ONIA
Containersintact?
Yu
No
7.
Samples Field Filtered?
Y
No
EfNIA
8.
Note if sediment is visible In the dissolved container
Sample labels Match COC?
C:Jas
QNo
©N/A
9.
/
-Includes Dato me/ID/Anal b Matrix:
Heads ace in VDA Vleis >" m 7
ayes
UND
N/A
10.
Trip Blank Present?
❑Yes
©Na
N/A
11.
T Blank Cust Seals Present? .
res
Na
N A
CLIENTwaripiCATi "EROWrM
Field Data Required? QYes ONO
Person Contacted.
Date/Time;
Comments/Sample
Discrepancy, Dzub,
4�
,
Project Manager SWRF Wow: _ ._ �1911d Cate:
Project Manager SRF Review: Date: .0
Note: Wherwm there is a discrepancyatfocbe North Carollrib'e mplianoo samples, a copyof this toms WIN bo sent to the North Carolina DEHN R CertdRcalian Dffke (La
"of hold; k=rmct pre6ervatAre, art of temp, incorrict ccnt�lners)
Pdge 9 of 11 F

5ampta [onditlon U •on lance! t SCUR ., v V y, • •, Page 2 pf2� - --- • . .
CeAn,7 cal' _ .l< _ � !___L_.
Document No.: Issuing Authorlty,
r F•—' R-a-033-Rev.01 Pace Quality Off Ice
*Check mark top half of bob If pH and/or dechlorination Project# W0# ; 92322171
Is verified and within the acceptance range for out Dote: 12/ 15/ lE
preservatlon samples. _ PM: AMB
Bottom -ha If of box is-t{► Hst-r umbewei-botNes -- CLIENT: 92-ENCO
MEMO
gone
man
Monosson
MENEM
MEW
MENOMINEE
11100011
onsommenson
onm§NklLloommo
BELISMINEENSIMENE
MEN
No
'logo
IN
own
an
man
on
IMEMEMmem
I
moons]
pH Adjtlstment Logfor Preserved Samples
Sample 10
Type of PMemtW
pH Upon welpt
Data prrsenraden adjusted
lima presemdon
aquseed
Amount of Pnservathm
added
tot M
Page 10 011

5END1KC E.AAORATORV:
ENCO Cary
102-A Woodwinds Industrial Court
Cary, NC 27511
Phone: [phone]
Fax: 919.467.351 S
SUBCONTRACT ORDER
ENCO Cary
CZ17981
► I)JA Q: MR
Tri-Test (Raleigh)
6701 Conference !?rive
Raleigh, NC 27607
Phone :[phone]
Fax:
Project Manager: Stephanie Franz Project State of Origin: North Carolina
Sub Lab ID Originating Lob ID Client Matrix Date Sampled S;tm la Comments
Qutfall l Ground Water 06•Dee-I610:10
u
Coiiforni, Fecal9223B 13-Dec-16 15:00 06-Dec-16 18:05
Containers Supplied.'
Sterile250mLP+-NaThio (F)
tral12 Ground Water 06-Dec-16 10.20
��v,{•yi ��} ::� �2� drrp it Q";P �'� F,r, ti�ir- �1?: a':I„ l iIH f�..tiC1-, �p r;.;,:r:r �l,�.:;�}i.:�- �.y�u u�t
�!Z'Is�a �;!.�.tiY�:..J1�i4 ���i�.�:l: '�'ri��f! ��:7.��''.1;.I.i.tL'1F91s.N��F�,fi+�RS.;.yi3ii�f�:3- �1r •r_.4' r...-...�!'...ss;; ��9�&1��--'-.WI�
Coliform, Fecal ` I1
Containers Supplied:
SwrileMml
it✓
Ppapeli8t°(11

y�cG 12 ao 4 S
ENCO Laborato, r1les
Accurate. Timely. Respanvve, Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, June 24, 2016
Republic Services of NC (RE016)
Attn: Tammy Mitchell
East Carolina Environemntal, 1922 Republican Road
Aulander, NC 27805
RE: laboratory Results for
Project Number: [none], Project Name/Desc: Stormwater
ENCO Workorder(s): CSIS287
Dear Tammy Mitchell,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, June 16, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed In accordance with the referenced methods/piocedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Stephanie Franz
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as rewK ed by the laboratory, and may Only be reproduced in rub. (Page 1 of 10

www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
GfentID: Outfall H-1
Lab ID: C513297-01
sample": 06/16/10 09132
Received: 06/16/16 14:27
Parmmeter
EPA 1664A
Hold Qate/Tfine(sl
07/14/16
(+reu
06/22/16
mefsl Analv6ts F lTtmafsl
14:47 + 06/23/16 18:27
Field
06/16/16
10:06 06/16116
09:52 06/16/16 09:52
SM 2540D-1997
06/23/16
06/20/16
12:55 06/20/16 12:55
Client ID: Outfall i
Lab ID; C515287-02
Sampled: 06/16/16 09:31
Received: 06/16/16 24:27
Parameft
EPA 1664A
Hold Date/Tfine(s]
07/14/16
r'rco Data/Timefsl
06/22/16
A 4 s Date!
14:47 06/23/16 18:27
s1
Field
06/16/16
09:45 06/16/16
MR 06/16116 09:31
SM 254OD-1997
06/23/16
06/70/16
12:55 06/20/16 12:55
SM 522OD-1997
07/14/16
06/16/16
16:38 06/17/16 11:20
GlentID: Outfa112
Lob ID. C515267-03
Sampled: 06/16/16 09:15
Received: 06/16/16 14:27
parnmete
EPA 1664A
Hold Gate/TlmefeI
07/14/16
eren-Q t%7Lmefs)
06/721M
Analysis Date/Tfine(s)
14:47 06/23/16 18.27
Field
06/16/16
09:29 06/16/16
09:15 06/16/16 09:15
SM 254OD-1997
06/23/16
D6/20/16
12:55 06/20/16 12:55
SM 5220D-1997
07/14/16
06/16/16
M38 06/17/16 11:20
FINAL This FeAnrt relates 0* tv pie sample as reCchwl by the WmratM, and may a+h be rePr*duMe in hA Page 2 of 9 0

www.ancolabs.eom
SAMPLE DETECTION SUMMARY
Ctient ID: outfall WI
Lab ID:
C515287-01
A-LM
Results
E192 HL
Im
H H41$i
Oil & Grease (HEM-SGf) Non -Polar Material
39.7
2.70
5.00
mg/L
EPA 1664A
PH
8.38
0
0
pH Units
Feld
Temperature
29.2
0
0
°C
Field
Client ID: Outfall 1
Lab ID:
C515287-02
Agaly 1a
ma MM
Ell°
Mau
N12um mob"
Chemical Oxygen Demand
18
10
10
mg/L
SM 522OD-1997
Oil & Grease (HEM-SGT) Non -Polar Material
17.8
2.70
5.00
mg/L
EPA 1664A
PH
8.33
0
0
pH Units
Field
Temperature
28.6
0
0
°C
Field
Client ID: Outtall 2
Lab ID:
C515287-03
A.I]BL1d9
Seitz
flop MU
wh
Mob
11101119111W Mgt"
Chemical Oxygen Demand
16
10
10
mg/L
SM S220D-1997
PH
8.16
a
0
pH Units
Field
Temperature
28.4
0
0
°C
Field
i FNAL rt:s rep n rebtn arHy to the sample as received ty the w:aam.y, and may anh oe reproduced N hA. L Page 3 of 10

www.encolabs.com
ANALYTICAL RESULTS ' I
Description: Outfali H-1 Lab Sample ID:C515287.01 Received: 06/16/16 14:27
Matrix: Ground Water Sampled:06/16/16 09:52 Work Order: C515287
Project: 5tormwater Sampled By:Mitch Hoggard
Chemistry Parameters
^ - £NCO Cary n.Htllfed analyw w 5911 -
Anandte frM hJumberl Balru 11 flu ILnb QE = EQL Mi mew Annam h9w
Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 61`20001 SM 254OD-1997 06/20/16 12:55 MMR
Field Parameters
Analyte rQfi Numberl fite f3w Uab ge = EU A=h mAlabnMd BY oft,
PH 8.38 pH Units 1 0 0 61`17010 Field 06/16/16 09:52 CLI
Temperature 19.2 °C 1 0 0 6F17010 Field 06/16/16 09r52 CLI
Classical Chemistry Parameters
Anal= [CAS Numberl
Oil & Grease (HEM-SGT) Non -Polar
Bawts Elm jinn RE MIX E" .liar MGM Anahmed By m2to
39.7 rtg/L 1 2.70 5.00 6F22010 EPA 1664A 06/23/16 18:27 5MA
Description: outfall 1 Lab Sample ID: C515287-02 Received. 06/16/16 14:27
Matrix: Ground Water Sampled:06/16/16 09:31 Work Order: C515287
Project: 5tormwater Sampled By:Mitch Hoggard
Chemistry Parameters
^ - £NCO Gtry mwMd &W44e [NC 591 J
Analybo rfMRumber] Results Flag jinn RE ML EQL li= (mod AnAtMEW By Noon
Chemical Oxygen DemndA 18 mg/L 1 10 10 6F16028 SM 52200-1997 06/17/16 11:20 10C
Total Suspended SolidsA 2.5 U mg/i 1 2.5 2.5 6F20001 SM 25400-1997 06/20/16 12:55 MMR
Field Parameters
Ananda fCAS Numbed Rau Elft 11M 2E MIX EQL IBM l78m.41i AgaIII hot"
PH 8.33 pH Units 1 0 0 6FI7010 Field 06/16/16 09:31 CLI
Temperature 28.6 °C 1 0 0 6F17010 Field 06/16/1609:3I CLI
Classical Chemistry Parameters
ADOW fCASNumbed Reffull8 an Mob RE IU ffiL 13alrh Math ARahfi d IN l!111I8E
Oil 8 Grose (HEM -SC, r) Non -Polar 17.8 mg/L I 2.70 5.00 6FR2010 EPA 1664A 06/23/I6 18:27 SMA
Material
FIRAL This report retats a* to me sanVie as wowed ty the laboratory. And may only be reproduced in frdL Page 4 of 10

M M& �ww�
www.encolabo.com
ANALYTICAL RESULTS
Description: Outfall 2 Lab Sample ID.C515287-03 Received: 06/16/16 14:27
Matrix: Ground Water Sampled: 06/16/16 09:15 Work Order: C515287
Project: Stormwater - Sampled BV:MitM Hoggard
Chemistry Parameters
Anahrta fCAS gumbo[] Fultz
flag slab
PF
KU
PQL
91Uh
Meth gll
Analyzed
ax rigostE
Chemical Oxygen Demand 1e
mg/L
1
10
10
6F160Z8
SM 522OD•1997
06/17/16 11:20
1OC
Total Suspended SoWSA 2.5
U mg/L
1
2,5
2.5
6F20001
SM 25400-1997
06/20/16 12:55
MMR
Field Parameters
Anand:a FCAS Number] ftesulltz
Elan i1ab
QE
M6
EM
1=
H&
Ana
am Nowl
pH 6.16
pH Units
1
0
0
' 6F17010
Field
06/16/16 09:15
CLI
Temperature 28.4
°C
1
0
0
6FI7010
Field
06116/1609:15
CLI
Classical Chemistry Parameters
Oil & Grease (HEM-SGT) Non -Polar Material
Boullo flag Mau of = E26 111=11 Meth Analxzgd Bic how
2.70 U mglL 1 2.70 5.00 GF22010 EPA 1664A 06/23/16 18:27 SMA
FINAL
This report m4aW only to Me wwok as remm!d W the W mWrV, and nW"be mpwdutxd In 0- Page 5 Of 10

www.ancolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 6F16029 - Same
Blank (611`1602111-13LKI) Prepared: 06/16/2016 16:38 Analyzed: 06/17/2016 11:20
Spike Source %REC RPD
Arta lYla Result Elan M UrI tY Level Resu %REC Lim RPD LiMS RQgs
Chemical Oxygen Demand 10 U 10 mg/L
LCS (GF16028-1351) Prepared: 06/16/2016 16:38 Analyzed: 06/17/2016 11:20
Spike
Source
%REC
RPD
.AMIA1
l),asult Mao
PAX
11.1114b
Level
ROM&
%REC
UMjta RPD
LIM Motes.
Chemical Oxygen Demand
490
10
mg/L
500
99
90-110
Matrix Spike (6P16028-MSI)
Prepared: 06/16/2016 16:38 Analyzed: 06/17/2016 11:20
Source: CZ07494-02
Spike
Source
%REC
RPD
-Anak"
Result Flea
MI.
uAlts
Level
%REC
Limits RPD
UaLft Mates
Chemical Oxygen Demand
560
10
mg/L
526
37
too
90-110
Matrix Spike Dup (GF16028-MSDI)
Prepared; 06/16/2016 16:38 Analyzed: 0611712016 11:20
Source: CZ07494-02
Spike
Source
%REC
RPD
An&IY a
Raxult Elan
P91
Unlb
Level
Resul
%REC
Lfmlla RPD
Limit (tom'_
Chemical Oxygen Demand
570
10
mg/L
526
37
101
90-110 0.8
10
iia" 6F20001 - NO PREP
Blank (6F20001-BLK3) Prepared & Analyzed: 06/20/2016 12:55
Spike Source %REC RPD
Anelvw Result Elan PQL Units Level Rgilift %REC L Mjk RPD 9111111; Notes
Total Suspended Solids 2.5 U IS mg/t.
LCS (mom -BSI) Prepared & Analyzed: 06/20/2016 12:55
Spike Source %REC
RPD
_,Arinlvte
Result EMU
PQL
Unl1s
Level Raw %REC Limits
RPD
Llm[t Nam
Total Suspended Solids
95
2.5
mg/L
100 95 80-120
Duplicate (611`20001-DUPI)
Prepared & Analyzed: 06/20/2016 12:55
Source: CZ05954-01
Spike Source %REC
RPD
Ana
Result E109
J!"
VAM
Level Result %REC LJMM
RPD
MIRM doges
Total Suspended Solids
220
100
mg/L
210
2
20
Duplicnte (6F20001-OUPZ)
Prepared & Analyzed: M/20/2016 12;55
Sources CZOB548-01
Spine Source %REC
RPD
9nalvte
Retrull: Elan
PQL
Units
Level ga& %REC 1. a ti
RPD
Limp r4gftl
Total Suspended Solids
230
100
mg/L
230
2
20
Classical Chemistry Parameters - Quality Control
Batt* 6F22010 - EPA 1664A
Blank (6FZ2010-BLK1)
Prepared: 06/22/2016 14:47 Analyzed: 06/23/2016 18:27
Spike Source %REC RPD
.AnalYto Result Flag P4L Units Level ResWt %REC 11ml RPD Lllplt Notes
Olt & Grease (HEM-SGT) Nan -Polar Material 0.678 u 1.26 mg/L
FINAL This report relates only to the sample as received 6y lne la6cramry, and may any W reproduced in Tull Page 6 of 1

sir �69
www.encolabs.com
QUALITY CONTROL DATA 1
Classical Chemistry Parameters - Quality Control
Batch 6122010 - EPA 1 "M - Contlnued
LCS (6F22010-BSI) Prepared: 06/22/2016 14:47 Analyzed: 06/23/2016 18:27
Spike Source %REC RPD
Ana ROil11t Flao P.Dl 111 ib Level %REC Ua& RPD Lla11t Motes
Oil & Grease (HEM-SGT) Non -Polar Material 78.7 5.00 mg/L 76.0 104 6+132
LCS Dup (GF2201O-BSD1) Prepared: 06/21/2OL6 14:47 Analyzed: 06/23/20I6 18:27
Spike
Source
%REC
RPD
Analvto
Result FIVA
p91
GMFa
Level
l S %REC
LLmLU RPD
IJM Notes
Oil & Grease (HEM-S(3i) Non -Polar Material
66.8
5.00
mg/L
76.3
88
6+132 16
34
Matrix Spike (GF22010-MSI)
prepared: 06/2242016 14:47 Analyzed, 06/23/2016 18:27
Source: 82026a7-01
Spike
Seurco
%REC
RPD
.AnalYtde
Result Flaa
POL
W tSa
Level
SZYj %REC
U= RPD
J,jiR[x Notes
Oil & Grease (HEM-SGT) Non -Polar Material
62.7
5.00
mg/L
74.6
2.70 I1 84
64-132
FINAL This report mrrates only tD tee sample as received by the kibma ry, and may only he ngroduced in roll. Page 7 of 10

www.encola bs.carn
FLAGS/NOTES AND DEFINITIONS,
B The analyte was detected In the associated method blank.
D The sample was analyzed at dilution.
] The reported value Is between the laboratory method detection limit (MDQ and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable,
U The ana" was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this anatyte is an estimated value above the calibration range of the
instrument. This valve is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitatlon limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, In the case of soil samples, moisture content.
N The analysis Indicates the presence of an analyte for which there Is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration Is reported.
FINAL. This report relates only to the sample as recelvW by the laboratory, and may only be rep "hied in RN, I Page 8 P 10

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.coi
•377: (. t4w,-. J.".GI, -hot' L,�t Fl�so (:,JIM; I I
Page _ of
FlordWcr Requested
c
A-Mrev;
Standard
tt-, A, ,1 2 1 f'l ?'L
F I tVzz brj Crt il—,
Expedited
I Wo
-7- Due
LAb Workorder
G Vi T.5,287
tun.vmlpArg C60or1ic- IMIn i e. ;,f, sampte commerlm
5A ctss 25,2 c
�i)4J4 R.31 r
Net 2t.Ll V
y X
F
<-- To:,-u h 01 CLWU;1!1.1 -r:.
17�1
C
fry- Acceptive
Urwc-coptibei
U.vt.. GW:
�v,"rJwa!- SO 5r.t MY I bvw '. 1704,r
SYO
......... ..... kvW fl
A -Ai 0-' 1 P ..
F, f llra 4 94Ulf 5 1 Wiu: ffu-N" 1 0 UMP1
f N. 1.
!�!lj 171. it" I L'--'.&" It
til : 97 -:11 um- W!Irin WV1,11ITIA Af

r
MOME
Sample preservation Verification
ENCQ Cary
Jill
,
Wark Order C515287 Project. Stormwater .
Client. Republic Services of NC (RE016) Pio}e,Ct ft: (none?
Lagged In: 18•,lun-16 13:34 Logged By, Andrew 5 Coons
C815287-01
�+
`? .7•y"'' "4..t i'�e Jfe
`� R" r
�, r i' S`�j
�R iFernei<1t
El>q t;antrot
4 ...� �....�..� Ll4 F
pH Ad(us#er1 ,, d :Auslsd`
Re4966t lJsadlCommenls
A - -
^� . s-, s„
11.ATN2SU4
t2
Y ► NA
Y
Y_
L!--PL-AtH2SO4
..� l
`2�
Y NA
C51S287•b2
A ILA-H'?SO4 I 42 Y "'h -i NA Yi
01LP.+Ft2S0�1 <1. Y t WA 7
U 250mLlI'4- i2SO4 s2 Y fii ! ?,)A Y
C315287.03
R*Wsd time Reagoid.Usedlc:ommef is
h}aiustrsa
��' !�}�.�......''` .�. _ .. ,....._....__•__,ram.._-..
tin'. `
pHAdjua#e�int;idfComliienta
a..��..- ....1
-
A
1LA,1-H2SO4
{2
Y N'! NA
Y MAi
f3
E
1 LA+142SCA
250inL.P- 42804
=2
<k
Y ! NA
Y ! NA
Y NA
Y N't, NA
116'a, ttii niattre � fly r Y
Page 10 of 10

/71aceAnalj4ical"
www.peeefebs.tonr
June 21, 2016
Ms. Stephanie Franz
ENCO Labs
102 A-Woodswinds Industrial Co
Cary, NC 27511
RE: Project: ENCO C515287
Pace Project No.: 92301762
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. Franz:
Enclosed are the analytical results for sample(s) received by the laboratory on- June 16, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4'��CA.tw �✓�c_
Liamm Harrison
[e-mail]
Project Manager
Enclosures
A* ,
ff
st4
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page f of 10

/7-15ceAnalytica(
www.pecelaAs.t,Wrr
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: ENCO C515287
Pace Project No.: 92301762
Raleigh Certification lDs
6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification #; 67 North Carolina Drinking Water Certification #: 37731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of PawArialytical Services, Inc.. Page 2 of 10

PaceAnalytical
www pacalabz,=n
SAMPLE ANALYTE COUNT
Project: ENCO C515287
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersvllle, NC 28078
[phone]
Pace Project No., 92301762
Analysts
Lab ID Sample ID Method Analysts Reported Laboratory
92301782001 OUTFALL 1 SM 9222D RC 1 PAS!-R
92301762002 OUTFALL 2 SM 9222D RC 1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in furl,
without the written consent of Pace Analytical Services, Inc,
10
Page 3 of 10

/74ceftlXical
r
wwwpaeelabs.cwm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
i 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ENCO C515287
Pace Project No.: 92301762
Sample: OUTFALL 1 Lab ID: 92301782001 Collected: 06/16/16 09:31 'Received: 06/16/16 15:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qua!
MBIO 92220 Fecal Coliform RAL Analytical Method: SM 9222D
Fecal Coliforms ND CFU/100 mL 4.0 4 06/16/16 15:59
Date: 06/21 /2016 11:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the wrltten consent of Pace Analytical Services, Inc .
Page 4 of 10

/_.
715ceAnalytrcal
! wwwAecelebs.crom
ANALYTICAL RESULTS
Project: ENCO C515267
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunters011e, NC 2807a
[phone]
Pace Project No.: 92301762
Sample: OUTFALL 2 Lab ID: 92301762002 Collected: 06/16/16 09:15 'Deceived: 06/16/16 15:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Colitorm RAL Analytical Method: SM 9222D
Fecal Coliforms ND CFU1100 mL 4.0 4 06/16/16 15:59
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in fuli,
Date: 06121 /2016 11:36 AM without the written consent or Pace Analytical Services, Inc..
Page 5 of 10

S Pace Analytical Servlcos, Inc.
9840 KineyAve, Sute 100
I/ nn/Maly1Cale Muntersville,
NC 28078
www.pacolabs.com [phone]
I
QUALITY CONTROL DATA
Project: ENCO C515287
Pace Project No,: 92301762
OC Batch: RB1016213
Analysis Method:
SM 9222D
OC Batch Method: SM 9222D
Analysis Description:
9222D M810 Fecal Coliform - RAL
Associated Lab Samples, 92301762001, 92301762002
I
METHOD BLANK. 1758081
Matrix: Water
Associated Lab Samples: 92301762001, 92301762002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Fecal Coiforms CFU1100 mL
ND
1.0 06/16/16 15:59
SAMPLE DUPLICATE: 1758082
92301697001 Dup
Parameter Units
Result Result
RPD Qualifiers
Fecal Coliforms CFU1100 mL
3.0
2.0 40 D6
Results presented on this page are In the units Indicated by d» "Unite" ealumn except where an alternate unit is presented to the rightor the resuft
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/2112016 11:36 AM without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

Paco9800 ICirttcey Ave�Suite 100
ices. Inc.
1,"'715ceAnalytal a Huntersville, NC 28078
www,pacefabs.com
[phone]
QUALIFIERS
Project: ENCO C515287
Pace Project No.: 92301762
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended In SVV846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes.
TN -The NELAC Institute.
LABORATORIES
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21/2016 11:36 AM without the wripen consent of Pace Analytical Services, Inc.. Page 7 of 10

,PaceAMIXical
www.pscelahs.cnm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: ENCO C515287
Pace Project No.: 92301762
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92301762001 OUTFALL 1 SM 9222D R61016213
92301762002 OUTFALL 2 SM 9222D R81016213
Date: 06121 /2016 11:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 10

/�-aceAnalolcal'
Document Name:
ndition Upon ReceiptlSCURI
Document No.:
Document Revised: May 24, 2016
Page 1 of 2
Issuing Authority:
!I Client Name: Protect q: ; WO# : 92301 1 62
raw La bs A I I!
Courier: jFed Ex UPS U5P5 Client II� II� III II III I II �II
❑ Commercial ace Other: # III 11 I!
�/ 92302762
CustodySeal Present? (� []Yes l�`lo Seals Intact? ❑Yes Nq
' Data/InRlals Person Examining Contents:�
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑No,.nn.,e,,�� []other:Thermometer: T1505 Type of Ice; tkiY1fdt ❑Blue ❑None []Samples an ke, cooling process has begun
Correction Factor: GVC Cooler Temp Corrected ('C): Biological Tlasue Frozen? []Yes [:]No [3V/A
Temp should be above frepe Ing to 5T
USDA Regulated Sall (&rN/A, water sample)
Did sampl.DA� e�s -o/riginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Bid samples odalnate from a foreign source {interne lonaly,
MYes [ inciudar¢ Hawaii and Puerto RIcoN 1—IYes o
' Comments/Disae n
Chain of Custody Present?
943
ONO
N/A
1. i
Samples Arrived within Hold Time?
es
ONo
N/A
2.
Short Hold Time Mal as e72 hr.)?
es
No
N A
1
3. ' l 2
Rush Tum Around Time Requested?
Dns
EKI
N A
4.
Sufficlent Volume?
yes
No
N A
5,
Correct Containers Used?
Ves
[I No
❑N/A
6.
-Pace Containers Used?
es
No
ORIA
Containers Intact?
as
Do
N/A
?.
Samples Field Flltered?
Des
No
/A
8. Note if sed6nent Is visible In the dissolved container
Sample labels Match COC?
EJes
❑No
❑N/A
9.
-Includes DateMrne%ID/Mal is Matrix:
All containers needing acid/base preservation have been
IO.
checked?
Yes
ONO
❑N/A
All containers needing preservation are found to be In
compliance with EPA recommendation?
hawo x
(HNOs, H,504, HCk2; WON 4 Sulfide, NaOH>12 Cyanide)
D(.$
❑No
❑hVA
w.au OW
Exceptions: VOA, Conform, 70C, Oil and Grease,
_K12 8o15 water DOCALff
ea
No
N/A
x■wvb.owrx.r
Samples checked for dechlorinatlon7
QYes
ONo
N '
11.
Headspace In VOA Vials ()-5-6mm 1
OYes
ONo
13�,LA
12.
Trip Blank Present?
[:]Yes
❑No
/
13,
Trip Blank Custody Seals Present?
❑Yes
ON o
pN/A
Pace Trlp Blank Lot p (if urchased):
WENT NOTIFICATION/RESOLUTION Fled Dab Required? ❑Yes ONO
Person Contacted:
Comments/Sample
Discrepancy:
Datefrime:
Project Manager SCURF Review: _ _ `, _....- —.. ...._ Date: i (�, ' .� `•r'
Project Manager SRF Review: l -� Rate: t ! 1, + A t
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form w1( be sent to the North Carolina DEHNR Certification office (Le.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 9 of 10

SUBCONTRACT ORDER
ENCO Care
C515x87
LABORATORY,RE(:EII'1NG I.,t00RATQRJ',
ENCO Care
Tri-Test (Raleigh)
102-A Woodwinds Industrial Court 6701 Cutilirence UriJr
Cary, NC 27511 Raleigh, NCc 7607 '
Phone, 919,467.3090 Phone :[phone]
Fax; 919A67.3515 Fax:
Project Mltnager: Stephmie Franz Prgjccl !-4a?e to 00-4o, r`orlh Curoiinn
Ground Water 16-,fun-M 0901
C:otiform, Fecal92238 23-Jun-16 15:00 16-Jun•16 17:26
Contuiners Supphe&
Stcrllc250mlY+-NaThio (F)
Crcund Water 16-Jnn-16 09:I3
CcIiform, Fecal9223B 23-Jun-16 15:00 164un•16 17:Ia
t" opflainers supplied:
Sterile250mLp+NuThiu (F)
ile—G-913Y Dote R—C4c—IVUT1—Y 1531C
Wage I of I
Page 10 of 10

4l
rcGI aWY5
$A CO Laboratories
Accurate. Time4 Responsive. Innovative.
lot -A woodvAnds Industrial Court
I Cary NC, 27511 i
Phone. [phone] FAX: 919.467.351E i
Friday, November 13, 2015
Republic Services of NC (RE016)
Attn: Tammy Mitchell
East Carolina Environemntal, 1922 Republican Road
Aulander, NC 27805
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Stormwater
ENCO Workorder(s): C506722
Dear Tammy Mitchell,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 3, 2015.
Unless otherwise noted in an attached project narrative, all samples were received In
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further Information, please do not hesitate to contact me.
Sincerely,
Stephanie Franz
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reprodumd in fsA . I Page �I of 1 0

www.encolabo.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
alert ID: H-1
tab 10: C506722-01
Sampled: 11/D3/15 09:06 Remlved: 11/03/15 12:15
+.routfa8
Pj1Ii111CfC[
EPA 1664A
HddDRREfTltne(sl
12JO1115
11/09/15
Analysis ate/Tlmefsl
16:14 1 11/11/15 11:51
Field
11/03/15 09:20
11/03/15
09:06 11/03/15 09:06
SM 254OD-1997
11/10/19
11/04/15
10:00 ll/04/IS 10:00
anent to- Outfan 1
Lab ID: C506722-02
Sampled: 12/03/15 08.40 ReCeived: 11/03/15 12 15
P
EPA 1664A
F�dd,Dn[e� rrre[sl
12Jp1J15
Prep Date/TFffldsl
11/09/15
Anah%lr DaIA1110b"
16:I4 11111/15 11:51
Field
11/03/15 08:54
11/03/15
08:40 11/03/15 08:40
SM 254OD-1997
11/10/15
11/04/15
MD0 11/04/15 10:00
SM 5220D-1997
12/01/15
11/07/15
12:55 11/07/15 15:51
alert 10: Outfall 2
Lab ID: C506722-03
Samlped: 11/03/15 08:21 Recelved: 11/03/15 12:15
Parameter
EPA 1664A
Hold Data/Timeftl
12/01/15
p,iney-paMMme(8]
11/09/15
AnalyslsDataffimefsl
16:14 11/11/15 11:51
Field
11/03/15 08:35
11/03/15
08:21 11/03/15 0811
SM 2WD-1997
11/10/15
11/04/15
10:00 11/04/15 10:00
SM 5220D-1997
12/01/15
11/07/15
12:55 11/07/15 15:51
FINAL This report reutes only to the sample as received by the iabaratory, and may only be:eomduced in fill. Page 2 Of 9 0

VYW W.onWab0.00111
SAMPLE DETECTION SUMMARY
Chant 10: Outfall H-1
Lab ID.
C506722-0t
A0ii11l
S wta
Eon
M"
ML
il0lu
LlCIIIl10 dttSCi
PH
7.53
0
0
PH Units
Field
Temperature
17.9
0
0
°C
Field
alert ID: Outfa111
Lab ID:
C506722-02
ADffi]dta
BoldtlE
on
mu
Ea
unu
method�
Chemical oxygen Demand
14
10
10
mg/L
SM 522OD-1997
PH
7.64
0
a
PH Units
Field
Tempereture
17.8
0
0
°C
Field
aient ID: Outfall 2
tab ID:
C506722-03
Ana
acmdu
In
MA
EQL
villu
(� �
PH
7.16
0
0
PH Units
Field
Temperature
19.8
0
0
PC
Field
F1w Thti report mates only to the sample as received by the laboratory, ana may onty be mprwL and in U. Pa ge 3 of 10

�� lessaa.
www.encolabs.com
ANALYTICAL RESULTS
Description: Outfall H-1
Lab Sample 10:C506722.01
Received: 11/03/15 12:15
Matrix: Ground Water
Sampled:11/03/15 09:06
Work Order: C506722
Project: Stormwater
Sampled By:Mitch Haggard
Classical Chemistry Parameters
^ - 60C17 Gry Ch177W AM&E [AC S911
Ante fCAS tiuMberl gesuJg
!in
jln& pF HU M Batch
matho An@bz a Man
Total Suspended Solids^ 2S
U
mg/L 1 2,5 2.5 5KO4003
SM ZWD•1997 11/D4/15 10:00 MMR
Field Parameters
Mum
Flan
!!nits QE 11" PQ1 Batch
tleGta; wl= BY Now
PH 7.53
pH Units 1 0 0 51<04D07
Field 11/03/15 09:06 CLI
Temperature 17.9
°C 1 0 0 5KD4D07
Field 11103/1509:06 CLI
Classical Chemistry Parameters
Analft I[CAS Numberl i1ead1$
an
Multi QE Hu ER A=
Method BY "S=
Oil & Grease (HEM•SG f) Non -Polar MaterW 2,70
U
mWL 1 2.70 5.00 SKOW12
EPA 1664A 11/11/15 11:51 SMA
Description: Ouftl I
Lab Sample ID:C506722.02
Received: 11/03/15 12:15
Matrix: Ground Water
Sampled :!!/03/15 08:40
Work Order: C506722
Project: Stormwater
Sampled By: Mitch Haggard
Classical Chemistry Parameters
^ - EXV ary certr/IW ana yte [AC 5911
Anahma fCAS Numbed $ems tin units 12f "a EQL Batch Plethod Anahzed RK %QteA
Chemical OxyW DemandA 14 mg/L 1 10 10 5KO7002 SM 5220D•1997 11107AS 15:51 IOC
Total Suspended Solids^ 2.5 U mg/i. 1 2.5 2.5 5KD4003 SM 254OD-1997 I I/D4/15 10:00 MMR
Field Parameters
Analyte rCAS Number! Results HiM unit& Of NBL E" Balch leg Angie By MCI
PH 7.64 pH Units 1 0 0 5K040W Field 11/03115 08:40 CLI
Temperature 17.8 °C 1 0 0 SK04007 Field 11/03/15 08:40 CLI
Classical Chemistry Parameters
Annlyte ICAS Number! Reful a Flan gab RE NA Ea Batch "ethRd ArillBy NOUN
Oil & Grease (HEM-5GI) Hon -Polar Material 2.70 U mg/L 1 2.70 5.00 51<09M2 EPA 1664A 11/11/15 11;51 SMA
FINAL This report relates only to tha sample as received by the laboratory, and may only be reproduced fn full Page 4 Of 1771

www.encolabs.com
ANALYTICAL RESULTS
Description: Outfall 2 Lab Sample ID:C506722.03 Received: 11/03/15 12:15
Matrix: Ground Water Sampled:11103/15 08:21 Work Order: C506722
Protect: Stdrmwater Sampled By:Mitch Hoggard I
I
Classical Chemistry Parameters
Aviator., tcJl"Vl bffJ Result:
an
Hafts
Pf
11"
Em
fiatiGh
HOW
hanhad
Al ato
Chemical Oxygen Demand^
10
U
mg/L
1
10
10
5K07002
SM 5220D-1997
11/07/15 15:51
JOC
Total Suspended Solids^
2.5
u
mgll
1
2.5
2.5
SK04003
SM 25400-1997
11/04/15 10:00
MMR
Field Parameters
flips
Un€ta
BE
JIM
E L
atEh
M
An
@u rile
PH
7.16
pH Units
1
0
0
- SK04007
Field
11103/1508:21
CU
Temperature
19.8
"C
1
0
0
5KO4007
Field
11/03AS 08:21
Cli
Classical Chemistry Parameters
Amthrte tCA5 Numberl Ral4ts
EIN
yAft
Qf
Hu
EQL
Dam
tied] d
i
Ilat Alltka
Oil & Grease (HEM-SCM Nan -Polar Material
2.70
U
mg/L
1
2.70
5.00
5K09012
EPA 1664A
t1/11/15 L1:51
SMA
FINAL This report relates only to the sample as retCived W the laboratory, and may only be reproduCod in fuq. I Page 5 Of Q

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch SK0 aw - NO PREP
Blank (SK04003-11ILKI)
Prepared & Analyzed: 11/04/2015 10:00
I
Spike Source %REC
RPD
A, DAiM
IL2sA
flag
MI.
unite
Level ResuJj %REC LLMUS RPD
Licht mows
Total Suspended Solids
2.5
U
2.5
my/L
LCS (SK04003-BS1)
Prepared & Analyzed: 11/04/2015 10:00
Spike Source %REC
RPD
ADsildie
needs
Dap
POL
Motu
Level Rid! %REC Limits RPO
Limit !�q
Total Suspended Solids
96
2.5
mg/L
100 96 80-120
Duplicate (5K04003-OUPS)
Prepared & Analyzed-. I1/04/201510110
Source: C500393-02
Spike Source %REC
RPD
Analvte
Result
Finn
P.QL
Units
Level R4ddt %REC Llmita RPD
Ljmit Notes
Total Suspended Solids
140
25
mg/L
140 0.7
20
Duplicate (51(04003-11UP2)
Prepared & Analyzed: I V0412015 10:00
Source: C500393-01
Spike Source %REC
RPD
Analvte
Result
MCI
POL
Units
Level %REC Limits RPO
Limit Notes
Total Suspended Solids
72
25
mg/L
66 9
20
Batch 5KO7OO2 -✓lame
Blank (SK07002-BLKL)
Prepared: 11/07/201512:55 Analyzed: 11/07/2015 15:51
Spike Source %REC
RPD
Analyta
Result
Han
POL
URIN
Level g %REC Limits RPD
Limit lilacs.
Chemical Oxygen Demand
10
U
10
mg/L
LCS (SK07002-BSI)
Prepared: 11/07/2015 12:55 Analyzed: 11/07/2015 15:51
Spike Source %REC
RPD
Artal
Bawd
Elan
EQL
Units
Level get %REC Limits RPD
LM li4t0L
Chemical Oxygen Demand
490
10
mglL
500 97 90.110
Matrix Spike (5K07002-MS3)
Prepared: 11/07/2015 12:55 Analyzed: 1110712015 15:51
Source: C500393-01
Spike Source %REC
RPD
Autdo
Result
Elaa
PAL
Units
Level Ream" %REC Limltll RPD
Unit Hum
Chemical Oxygen Demand
610
t0
mg/L
526 44 108 90.110
Matrix Spike Dup (SK01002-MSDI)
Prepared: 11/07/2015 12:55 Analyzed: 11/07/2015 15:51
Source: C500393-01
Spike Source %REC
RPD
Anal
laesolt
Elan
MI.
Units
Level Result %REC LimUa RPD
WWI Notes
Chemical Oxygen Demand
580
10
mg/l.
526 44 102 90.110 5
10
Classical Chemistry Parameters - Quality Control
Bitch 5K09O12 - EPA 1664A
Blank (SK09012-BLK3)
Prepared: 11/09/2015 16:14 Analyzed: 11/11/2015 11:51
Spike Source %REC
RPO
ARalyte
Result
Flap
P4L
Units
Level gggy[t %REC UM18 APO
Limit Note4-
Cil & Grease (HEM-SGT) Non -Polar Material
2.70
U
5.00
mg/L
FINAI This report relates only to the !amok as received by the laboratory, and may only be reyraduced fn rues. Page 6 0( 1 Q

www.oncolab&com
QUALITY CONTROL DATA
Classical Chamistty Paramaters - Quality Control
Batch SK09012 - EPA 16"A - Continued
LCS (5K09012-BSI) ! Prepared: 11/09/2015 16,14 Analyzed: 11/11/2015 11:51
Spike Source %REC RPD
Analy" RwWt EIaR PAL Units Levd gaWt %REC LlMJU RPD MM11 fttl
Oil & Grease (HEM-SGT) Non -Polar Material 59.9 5.00 mg/L 79.4 76 64.132
LCS Dup (5K09012-5SD3) Prepared: 11/09/2015 16:14 Analyzed: 111$112015 11:51
Spike
Source
%ItEC
RPD
A1H1 ft
ReSuit Ein
E4L
Units
Level
Recult %REC
t✓MUR RPD
Lim$ Moto
Oil & Grease (HEM-SGT) Non -Polar Material
64.5
5.00
mg/L
78.1
83
64-132 7
34
Matrix Spike (SK09012-M51)
Prepared: 11/09/2015 16:14 Analyzed: 11/11/2015 11:51
Source: 0504602-02
Spike
Source
%REC
RPD
.Analrte
Result Hag
PM
Units
Level
RCUR %REC
limits RPD
wit mates
Oil & Grease (HEM-SGT) Nan -Polar Material
57.2
5.00
mg1L
75.8
19.2 50
64.132
QM•07
F[NAL This report relates only to the sample as r=rved by the laboratory, and may only be repmdomd in full. I Page 7 Of = O

99 —.
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FLAGS/NOTES AND DEFINITIONS
8 The analyte was detected in the associated method blank.
D The sample was analyzed at dilution. 1
!] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of loll samples, moisture content.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
Greater than 250k concentration difference was observed between the primary and secondary GC column.
The lower concentration Is reported.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
FfNAL This report relates only to the sample as received by the laboratory, and may only Dc reproduced In full. Page 8 of 107

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RFntrti': GW-Gro,mdwatet SO-Soe DW-Orv>Mmg Water SE.Saorranl SW.Suetam Water WW-Wamewawr A.Aw O-Other(detau in mrrrMrrt) Prtserrarlon: trice H-HCf N-HP403 S-H2SO4 NO-NaOH OlOefer(Aetaa In ettmmentst
Note : AN aamoss 9-Or red io ENCO Lam are in accordance wah the rerm and ConUlo.G Nslea on fie revvr5. w this tOrm. ulUeU Df" wtd:er agreements ex.sf

Sample Preservation Verification
ENCO Cary
Work Order:
C506722
Project:
Stormwater
Client:
Republic Services of NC (RE016)
Project #:
(none) .
Logged In:
03-Nov-15 12;56
Logged By:
John C King
C506722-01 r
C506722-02
A
ILA+H2SO4
<2 Y l N l OA)Y/ N 1
B
1 LA+H2504
<2 Y/ N 1.3 Y 1 N 1 li
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250MLP+H2SO4
<2 / N 1 NA Y l I NA
C606722-03
A
1 LA+H2SO4
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Y/ N I
Y i N 1 N
1
B
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<2
Y 1 N/
Y 1 N 1
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<2
1 N 1 NA
Y/ N NA
.
Rea ent Name ID
1
2
Reagent Name ID
3
4
Reagent Name I
5
6
Page 10 of 10
Page 1

�;a'ce'
Analytrca!`
wwwpttcefabs.com
November 13, 2015
Ms. Stephanie Franz
ENCO Labs
102 A-Woodswinds Industrial Co
Cary, NC 27511
RE: Project: C506722
Pace Project No.: 92274424
Paco Analytical Services, Inc,
0800 Kincey Ave, Suite 100
Muntersvitle, NC 28078
[phone]
Dear Ms. Franz:
Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
jam, n—„_,
Liamm Harrison
[e-mail]
Project Manager
Enclosures
A-Ccip,
}
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Tull,
9 without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
"
wawpscefa6S.o=
Project: C506722
Pace Project No.: 92274424
Raleigh Certification Ids i
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvi9e, NC 28078
[phone]
CERTIFICATIONS
North Carolina Bioassay Certification #: 18
North Carolina Drinking Water Certification * 37731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc., Page 2 of 10

aceAnaVical
wwwpacebbs.carri
SAMPLE ANALYTE COUNT
Project: C506722
Pace Project No.: 92274424
Pace Analytical Services, Inc,
9900 Kincey Ave. Suite 100
Nuntersville, NC 28078
1704)875-9992
i Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92274424001 OUTFALL 1 SM 9222D RC f PASI-R
92274424002 OUTFALL 2 SM 9222D RC 1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, I nc..
Page 3 of 10

1�;a'aeAnafytical a
www.paceMbs.com
r
ANALYTICAL RESULTS
Paco Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
(704)e75.9092
Project: C506722
Pace Project No.: 92274424 t
Sample: OUTFALL 1 Lab ID: 92274424001 Collected; 11103t15 08:40 Received: 11/03/15 13:00 Matrix: Water
s
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Collfonm RAL Analytical Method: SM 92220
Fecal Coliforms 172 CFUI100 mL 1.0 1 11/03/15 15:24
Date: 11/13/2015 04:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not pe reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

aceAnalwical
www.psnfsba.mm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 29079
[phone]
Project: C506722
Pace Project No.: 92274424 1
Sample: OUTFALL 2 Lah ID: 92274424002 Collected: 11/03/15 08:21 Received: 11/03115 13:35 Matrix: Water
Parameters Results Units Report Limit OF • Prepared Analyzed CAS No. Qua]
MBIO 9222D Fecal Coliform RAL
Fecal Colifarms
Date: 11/13/2015 04A5 PM
Analytical Method: SM 9222❑
4.0 CFU1100 mL 1.0 1 11103115 15:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrihen consent of Puce Analytical Services, Inc..
1g
Page 5of10

;aceAnalytical'
1 wwwpeceleba.com
QUALITY CONTROL DATA
Project: C506722
Pace Project No.: 92274424
Pace Analytical Services, Inc.
9800KInceyAve. Suite100
Huntersville NC 28078
[phone]
QC Balch: 1 RBIO15670 Analysis Method: t SM 92220 '
OC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAIL
Associated Lab Samples: 92274424001. 92274424002
METHOD BLANK: 1598247 Matrix: Water
Associated Lab Samples: 92274424001, 92274424002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU1100 mL ND 1.0 11/03115 15:24
SAMPLE DUPLICATE: 1598248
92274424001 Dup
Parameter Units Result Result RP❑ Qualifiers
Fecal Coliforms CFU/100 mL 172 91.0 62
Result* presented on this pope are in the unite Indicated by the" Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/13/2015 04:45 PM without the written consent of Pace Analytical services, Inc.. Page 6 of 10

Pace Analytical Services, Inc.
�+ m
�UG al ical 8$00KinceyAve. Suite 78
f G�1 111/`I N r Ftunteravilfe. NC 28078
wwwFsceraba.wrrr
(71141a75-9092
f
1
QUALIFIERS
Project: C506722
Pace Project No.: 92274424
DEFINITIONS
DF - Dilution Factor. if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for. but not detected.
Acid preservation may not be appropriate for 2 ChloroathyMnyl ether, Styrene. and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acroiain and Acrylonitriie by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PAST-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1 g This is a less than value
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In cull,
Date: 1111312015 04:45 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

Pace Analytical Services, Inc,
a 9800 ltinceyAve. Suite 100
al
Muntersville, NC 28078
I www.welabs.com [phone]
r
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: C506722
Pace Project No.: 92274424
r r
i Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92274424001 OUTFALL 1 SM 92220 R131015670
92274424002 OUTFALL 2 Slid 92220 RB1015670
REPORT OF LABORATORY ANALYSIS
This reporl shall not be reproduced, except in full,
Date: 1111312015 04:45 PM without the written consent of Pace Analytical Services, Inc„ Page 8 of 10

Document Name: Sample Condition Upon
Document R vleed: May 15, 2015
+ aaeAnalytical f
Recel t SCUR
P cte 1 of 2'
Document No.:
Issul B Authorities:
F-RAL-CS-001-rev.03
Pace Ral ! h Quality Office
,� 'Page 2 of I
Is for Internal Use Only
Client Name:
Courier (Circle): Fed Ex UPS LISPS Client Commercial Pace Other t
I Custody Beal on CoolerlBax Present: 0yea no goals intact: yes no i
1
Pecking Material: Bubble Wrap ags None Other
Circle 7hermomoter Used: IR Gun 9 •122063387T Sallow Wet Blue None D Samptes an lco tooting process has begun
IR Gun Ba 71
Tamp Correction Factor: Add I htract
Corrected Cooler Tamp,:��� C
Tamp should be above freezing to e'C
C
Biological Tissue is Frozen: Yw N NfA
Comments:
Date and In
co
check•
t a s o ps on tumining
s P p
1
Chain of Custody Present:
Yee ❑Na
0NIA
1.
Chain of Cust2d Filled Out
Yes ON.
ONiA
2.
Chain of Custody Relin uished:
yes ONO
❑Nu
3.
Sampler Name & 5 nalure on COC:
Yea ON.
OwA
4.
Samples Arrived wfthln Hold lime:
Yes ONO
OVA
5.
Short Hold Time Analysis <72hr :
Yes ON.
❑wA
6.
Rush Turn Around Time R uested:
❑Yes No
❑wrA
7.
Sufficlent Valume:
6YOS ONO
ONrA
8.
Correct Containers lased:
-Pace Containers Used:
Yes ONO
Yea ONO
❑N/A
❑NIA
$.
Containers Intact:
Yes ONO
❑NIA
10.
Flltered volume received for Olssolved tests
Yee ON.
VfNIA
11.
Sample Labels match COC:
-Inciudes dateltimaJID/Anal is Matrix:
Y ❑No
Ow
12.
E
All containers needing preservellon have been checked.
All containers needing preservation are found to be In
compliance with EPA reeommendadon.
excaoonr VOA. coirorm, TOC. OSO, WWRq weter
Ytl ❑Na
so ONO
as ONO
ONIA
❑wA
13.
Samples checked for dechiorination;
ee ONO
ONIA
14.
Heads ace in VOA Vials >8mm :
byes ONO
NIA
15,
Trip Blank Present'.
Trip Blank Custody Seals Present
Pace Trip Blank Lot # Hpurchased):.._...
❑Yes ONO NIA
❑Yea ONO }C.lNIA
16,
Client NotHicatlonl Resolution:
Person Contacted:
Comments/ Resolution:
Datomme:
Field Dote Requlred7 Y J N
sReRewRF � Data; 1111%,031S
"3iS WO# : 92274424
Note: Whenever there is a discrepancy affacting North Carolina Compliance
samples, a copy of this form will be sent to the North Carolina DEHNR {1 flf{
Certificatlnn Office I Le out of hold, Incorrect preservalive, out of lamp, 74
Incorrect containers) 9227
Page 9 of 10

SUBCONTRACT ORDER
ENCO Cary
C506722 g2:20 �{
SFNgINC LABORATORY: R CEMINGLABORATORY:
ENCO Cary Tri-Test (Raleigh)
102-A Woodwinds Industrial Court , 6701 Conference Mvo t
Cary, NC 27311 ; Raleigh, NC 27607 i
Phone: [phone] Phone :[phone]
Fax: 919,467.3515 Fax:
Project Manager: Stephanie Franz Project State of Origin: North Carolina
{�i) j Qutfall l Ground Water 03-Nov-I508:40
Collform, Fecal9223H ID-Nov-15 15:00 03-Nov-15 14:40
Containers Supplied.-
Steri1c250mLP+Nd7hio (F)
Qutfall 2 Ground Water 03-Nov-1508:21
Coliform, Fxal 922313 10-Nav-15 15:00 03-Nov-15 14:21
Containers Supplied:
Ster11c250mLP+NaThiu (F)
(' 01
1113
--U-3-ta
!I 3 r�
l.• �'7 1. Sf
Y 1 !
Inn E �!.
ate
U
``
�I i5 t33S
Page I of I

hcG laooy � ��15�
ENCO Laboratories
Accurate. Timely. .Responsive. .Innovative.
102-A woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: 919."7.3515
Thursday, June 11, 2015
Republic Services of NC (RE016)
Attn: Tammy Mitchell
East Carolina Environemntal, 1922 Republican Road
Aulander, NC 27805
RE: Laboratory Results: for
Project Number: [none), Project Name/Desc: Stormwater
ENCO Workorder(s): C500078
Dear Tammy Mitchell,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, June 3, 2015.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed In accordance with the referenced methods/ procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OLLSAAA
Chuck Smith
Project Manager
Enclosure(s)
FINAL. This report rdates Cdy to the sample as roMhmd by Ne ta"'Ataty, ar4 may D* bL neproftmmo in ". Page 1 of 9

r
www.encolabo.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Sampled: 06/03/19 11:01 Received: 06/03/13 14.14
Client ID: Outtall H-1
Lab ID: C500076-01
parameter
EPA 1664A
Hold DatelTimefsl
07101)15
prep,Qalm/-Timeffil
06/09/15
Analvsls DatefTimefsl
15:00 06/10/15 15:05
SM 2540bd997
; 06/10/15
06/04/15
14:00 E 06/04/15 14:00 i
Client ID: OutFOR 1
Lab In: C500076-01
Sampled: 06/03/13 10:43 Received: 06/03/15 L4:14
ParandeHold
Colilert 18
DatelTimefsl
06/03/15
pia DaM1Tlmefsl
16:43 06/04/15 13:22 06/03/15
Anahrsls Date/Timefsl
15:18 06/04/15 09:39
EPA 1664A
0/101115
06/09/15
15:00 06/10/15 15:05
SM 254011-1997
06/10/15
06/04/15
14:00 06/04/15 14:00
SM 52200•1997
07/01/15
06/04/15
10:44 06/04/15 15:50
FINAL This report relates only to the sample as necelved by the laboratory, and may only be reproduced in full. Page 2 of 9

www.encolaba.cem
SAMPLE DETECTION SUMMARY
glent ID: outfall 1 Lab ID: C900078 002
Ana8etulla EW9 Ha ML Unb Method Note
Collfarm, Fecal
110 1,0 MPN/100 mL Colilert 18
FINAL This report relates only to the sample as recehed by the laboratory, and may only be reproduced In full. Page 3 or 9

vrww.encolabs.com
ANALYTICAL RESULTS
Description: Outfall H-1 Lab Sample ID:C500078.01 Received; 06/03/15 14;14
Matrix: Ground Water Sampled.06/03/15 11:01 work Order: C500078
Project: 5tormwater Sampled By:Mitch Hoggard
Classical Chemistry Parameters
----very mn enegro lm ereJ
Analvte MAS-Numbed Resul b
fjw
Vow
pIE HU iL fial
Malho Analyzed 11 K=
Total Suspended Solids^ 2.5
U
mg/L
1 2.5 2.5 5F04025
SM 254OD-1997 05/134/15 14:00 MMR
Classical Chemistry Parameters
Aeahtte MAS-Number] Results
El=
unia
PE M" M HOOIh
Math 4d BDaly Its Note
Oil & Grease {HEM-SGTi Non -Polar Material 2,60
U
mg/L
1 2,60 5.00 SF09012
EPA 1664A 06/10/15 15:05 SMA
Description: Outfall 1
Lab Sample ID:C500078-02
Received: 06/03/15 14:14
Matrix: Ground Water
sampled: 06/03/15 i0:43
Work Order: C500078
Project: 5tormwater
Sampled BV:Mitch Hoggard
I Chemistry Parameters
^ - EWV Qfy r "fieean" JAC 5911
Analvte IG15 Numbed lets
BAR
Ogi11
pE
Mi26
E"
11=1
Math
AnalYAe�
@y
Cherrrkal Oxygen Demand^
10
U
rl
1
i0
10
5F04011
SM 522OD-1997
06/04/15 15:50
]OC
Total Suspended Solids^
2.5
U
mall
1
2.5
IS
51`04025
SM 25400-1997
D6/04/15 14:DD
MMR
Microbiological Parameters
^ - &fro Cary aarmiadan W(nr 5911
Analvte [CAS Humberl glSylb
flag
knh
of
BELL
Bate
MPS
Anal
eg
Colltiorm, FeMIA
33
MPN/100 mL
1
1.0
SFD4018
Calilert 18
D6/04/15 09:39
MKS
Classical Chemistry Parameters
Analng WAS Numberl Restill
fkg
gnu
Rf
MW,
EQL
!latch
Metho
Analyzed
AN Notes
Oil & Grease (HEM-SG17 Non -Polar Material
2.60
U
mg/L
1
2,60
5.00
5FO9012
EPA 1664A
06/10/15 15:05
SMA
FINAL This mport relates only to the sample as recelved by the laboratory, and may only be reproquced In full. Page 4 of 9
4

www.encelabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch SF04011 - Same
Blank (SF04011-BLK3) Prepared: 0610,1/2015 10:44 Analyzed: 06/D4/2015 15:50
Spike Source %REC RPD
.Analld'D Result Flay P!L units Level RlsYlt %REC Lilab RPD Ljptlt yp
Chemical Oxygen Demand 10 U 10 mg/L
LCS (SF04011-BSI.) Prepared: 06IG412015 10:44 Analyzed: 06/04/2015 15:50
Spike Source %REC
RPD
Analift
Res It Effie
ML
Units
Level Ry[ult %REC LL89M RPD
L)m)t (Votes
Chemical Oxygen Demand
480
10
molt
500 97 90.110
Matrix Spike (SF04011-I4B1)
Prepared: 06/04/201510:44 Analyzed: 06/04/2015 15!5e
Source: C40GS93-01
Spike Source %REC
RPD
.AnalwU
Result Flay
P,LL
UnBs
level Result %REC Limits RPD
UMt jy
Chemical Oxygen Demand
580
10
mg1L
526 63 98 90.110
Matrix Spike Dup (SF04011-MSD1)
Prepared: 06/04/2015 10:44 Analyzed: 06/04/2015 15:50
Source: C406393-01
Spike SDUMB %REC
RPD
.Analy.w
RcW t Flay
PM
!(nit!
Level Rmtlt %REC Ljmitt RPD
Limit Notes
Chemical Oxygen Demand
590
10
mg/L
526 63 100 9D•110 1
10
Batch SF04025 - NO PREP
Blank (SF04025-BLK1)
Prepared & Analyzed: W04/201514:00
Spike Sauces %REC RPD
Analirte Result Flay POL Units Level RMI %REC Limits RPD Limp )Motes
Total Suspended Solids 45 U 2.5 m911.
LCS (SF04025-BSI) Prepared & Analyzed: 06/04/2015 14'.00
Spike Source %REC
RPD
.Analrte Hatdt Effie
QQL
UOILS
Level Result %REC Limits
RPD
Lbu Notes
Total Suspended Solids 90
2.5
mg/L
100 90 80-120
Duplicate CSF04025-DUPl)
Prepared & Analyzed: 06/04/2015 14:00
Source,C505435-01
Spike Source %REC
RPD
MINIM Result flay
M
units
Lewd Rat %REC UMJM
RPD
tuna H=%
Total Suspended Solids 4700
500
mg/L
5300
12
20
Duplicate (SF04025-DUP2)
Prepared & Analyzed: 06/04/2015 MOD
Source: C506230-01
Spike Source %REC
RPD
.Analm Result Flay
FILL
W tTi
Level Result %REC Limps
RPD
LLMR Notes
Total Suspended Solids 40000
2500
mg1L
43000
7
20
Microbiological Parameters - Quality Control
Batch 5FO4018 - NO PREP
Blank (SF04016-BLK1)
Prepared: OCVO312015 1130 Analyzed: 06/04/2015 09:39
Analwto
Coliform, Fecal
Spike Source %REC RPD
Result Elm POL units Level RUA %REC Limits MPD Llal)t
1.0 U 1.0 MPN/100
mL
MAL This report rNrtes only to the sample as received by the labaratary, and may orgy be reproduced In ruL Page 5 or 9

www.encolabs.cem
QUALITY CONTROL DATA
Microbiological Parameters - Quality Control
Batch 57o4O18 - NO PREP - Continued
j Duplicate (SF04018-DUPi)
Prepared: 06/03/2015 13:30 Analyzed: 06/04/2015 09:39
i
Source: C305849-01
$Pike Source %REC
RPD
-AnahtO Result
Flaa
PQL
Unns
Level gerul %REC LLMjjg RPD
i,JM11; Notes
Collform, Fecal 3.1
1.0
MPN/100
2.0 43
25 QR-04
mL
Classical Chemistry Parameters - Quality Control
Baeich SAW12 - Some
Blank (SF09012-111ILKI)
Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05
Spike Source %REC
RPO
Anallre BLUE
Flag
POL
Units
Level Result %REC UMIM RPD
Limp Notes
Oil IN Grease (HEM•5GT) Non -Polar Materiel 2.60
U
5.00
mg1L
LCS (SF09012-BSI)
Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05
Spike Source %REC
RPD
-Anallde Rmdt
Ra0
@41
11BIts
Level Result %REC L1ml RPD
Limit Notes
Oil & Crease (HEM-SGT) Non -Polar Material 17.1
5.00
mg/L
2115 79 64-132
LCS Dap (SF09012-BSDI)
Prepared: W09/2015 15:00 Analyzed: 06/10/2015 15:05
Spike Source %REC
RPD
Analvte Result
Flae
POL
Units
Level RffiIR %REC Limlks RPD
Lllliit Notes
Oil & Grease (HEM-SGr) Non -Polar Material 17.1
50
mg1L
21.5 79 64-132 0
34
Matrix Spike (SF09012-MSI)
Prepared: 06/09/2015 15:00 Analyzed: 05/101201515:05
Source:B302322-02
Spike Source %REC
RPD
Analrtn Result
EIaR
Poll,
Units
Level Resin %REC Limits RPO
Limit Notes
Oil & Grease (HEM-SGO Non -Polar Material 30.3
5.00
mg/L
23.0 341 NR 64-132
QM-07
FINAL This report relates only to tha sample as reco.Vd by ft laboratory, an0 may orty be reproduced In frAl. Pape 6 of 9

www.eneciabi.com
FLAGS/NOTES AND DEFINITIONS
0 The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between` the laboratory method detection limit (MDQ and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate,
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and Is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
N The analysis Indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QR-04 Duplicate precision outside acceptance limits due to low analyte concentration.
FIN& Mis repot mW= ant to the sample as mmhed by fhe labomtmy, And may orgy be mpmduced in hall. Page 7 of 9

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NCDETIR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P. E, Dee Freeman
Governor Director Secretary
December 4, 2012
Drew Isenhour
Republic Services of North Carolina LLC
1220 Commerce St S W
Conover, NC 28613
Subject: NPDES Stormwater Permit Coverage Renewal
Republic Services Of NC LLC - Aulander
COC Number NCG120045
Bertie County
Dear Permittee:
In response to your renewal application for continued coverage under stormwater General Permit NCG120000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage (COC)
• A copy of General Permit NCG120000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater,'and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January land July 1 of every year (or, if applicable,
report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your
permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last COC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (htt ortal.ncdenr.or web w ws su current -
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit
http://Portal.ncdenr.ors/web/wq/ws/su/npdessw (click on 'General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Ralel North Carolina 27604
Phone: 919-8V-63001 FAX: [phone]
Internet: www--materguali .a
An Equal Oppnr' ni!, 1 AffmnaGve Anion Empio.dr
Nort
h na
Wura#;1

Drew Isenhour
December 4, 2012
Page 2 of 2
Some of the changes include:
Part II:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C: A lower TSS benchmark of 50 mg1l for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections B, C. The monitoring parameter Oil & Grease (0&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Also note that existing
permittees do not need to submit a renewal reguest prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone].
Sincerely,
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Washington Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG120000
CERTIFICATE OF COVERAGE No. NCG120045
STORMWATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Republic Services of North Carolina LLC
is hereby authorized to discharge stormwater from a facility located at:
Republic Services Of NC LLC - Aulander
1922 Republican Rd
Aulander
Bertie County
to receiving waters designated as Cashie River, a class C;Sw waterbody in the Roanoke River
Basin in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts VII, III, and IV of General Permit No. NCG120000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 41h day of December, 2012.
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
May 22, 2006
Mr. Tom Flannagan
Republic Services of NC LLC - Aulander
1922 Republican Road
Aulander, NC 27805
Subject: Stormwater General Permit NCG120000
Operations and Maintenance Reminder
Republic Services of NC LLC - Aulander
COC Number NCG120045
Bertie County
Dear Permittee:
Our records indicate that you have been issued a Stormwater General Permit and a Certificate
of Coverage for your facility. These permits have specific conditions that must be met in order for you
to be in compliance with your permit. It is your responsibility, as the permit holder, to read and
comply with the conditions contained in the permit. '
. It is our responsibility, as the issuing authority, to make sure that the operation and
maintenance of your facility complies with the conditions contained in your permit. To assist you in
complying with these conditions, we are attaching a Technical Bulletin specific to your permit
requirements. We are currently in the process of developing our inspection schedule. Therefore, you
should have all of your records up to date as we may be contacting you in the near future to set up
an inspection of your facility.
If you have any questions, please do not hesitate to contact Samir Dumpor, Pat Durrett or
myself at [phone].
Sincerely
AI 4 od4agq, up rrvis0r
Surface Water Protection Unit
Encl.
CC: WaRO files
North Carolina Division of Water. Quality Internet h2o.encstate,nc.us
943 Washington Square Mall Phone, 252-946-6481 teWashington, NC 27889 FAX [phone] Carob;
An Equal OpportunitylAffirmative Action Employer— 50% Recycledll0% Post Consumer Paper ura!!

�OF W A Michael F. Easley
`Q G Governor
AUG 2003 William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
0 Alan W. Klimek, P.E. Director
MA10-WAR0 Division of Water Quality
July 31, 2003
Tom Flannagan
Republic Services Of NC LLC
1922 Republican Rd
Aulander, NC 27805
Subject: NPDES COC # NCG120045
Republic Services Of NC LLC - Aulander
Compliance Schedule Correction
Bertie
Dear Tom Flannagan:
It recently came to the Division's attention that the compliance schedule in the NCG120000 permit is
incorrect. The compliance refers to requiring a Stormwater Pollution Prevention Plan which is not a
requirement of this permit. The corrected compliance language that should go under Part III, Section A: 1. is
shown below. We have also attached a new page reflecting this change for your permit file (Part III page 1 of
11). This new page should replace the current page in your permit.
SECTION A: COMPLIANCE AND LIABILITY
I. Compliance_ Schedule
The permittee shall comply with the permit in accordance with the following schedule:
Existing Facilities: Upon the effective date of the Certificate of Coverage the permittee shall comply
with all of the conditions detailed in Part II, Section A: Final Limitations and Controls for Stormwater
Discharges.
New Facilities: Upon the beginning of discharges from the operation of the industrial activity the
permittee shall comply with all conditions detailed in Part H, Section A: Final Limitations and Controls
for Stormwater Discharges.
If you have any questions concerning this matter please contact Aisha Lau at
[phone], ext. 578.
Sincerely,
fnrAlan W. Klimek, P.E.
cc; Stormwater and General Permits Unit
Washington Regional Office
Central Files
NCDE:NR
Customer Service Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone]
1 800 623-7748

State of North Carolina
Department of Environment f
and Natural Resources
Division of Water Quality OEM
Michael F. Easley, Governor NCDENR
William G. Ross Jr., Secretary NORTH CAROLINA DEP^RTmENIT OF -
Alan W. Klimek, P.E., Director ENVIRONMENT AND NATuFhwL REscuRCEs
RECEIVED
October 31, 2002
NOV 0 7 2002
Mr. Tom Flannagan
East Carolina Regional MSW Landfill DWQ_�p�I'1f[pt DO
1922 Republican Road YY
Aulander, North Carolina 27805
t. Subject: NOV Rescission request
Permit No. NCG120000
COC No. NCG 120045
Mr. Flannagan:
This letter is in:response to your correspondence of October!16, 2002 concerning a Notice of Violation,
(NOV) issued for failure to submit a renewal application.- A review of our records indicates your
renewal application was received and renewal process has,been completed. The Notice of Violation has
been rescinded and the Division apologizes for any inconvenience this matter may have camsed.
If you have any questions concerning the contents of this letter, please feel free to contact tme at 919-733-
5083 ext. 525.
Sincerely,
344k4m�#-
Bradley Bennett
Stormwater & General Permits Undt
cc: Stormwater and General Permits File
Washington Regional Office
Central Files
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-cortrsumer paper

W A
_co r
0 `C
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
August 23, 2002
TOM FLANNAGAN
REPUBLIC SERVICES OF NC LLC - AULANDER
1922 REPUBLICAN RD
AULANDER, NC 27805
Dear Permittee:
Alan W. i 3
Divisisio
AUG 2 9 2002
DWQ-WARQ
Subject: NPDES Stormwater Permit Renewal
REPUBLIC SERVICES OF NC LLC - AULANDER
COC Number NCG120045
Bertie County
In response to your renewal application for continued coverage under general permit NCG 120000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
A new Certificate of Coverage
* A copy of General Stormwater Permit NCG120000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Washington Regional Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699.1617 [phone]
®��
NCDENR
Customer Service
1- 800-623-7748

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Alan W. Klimek, P.E. Director
06/06/2002
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Iffl?WA
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
RECLa W EDI
ATTN: TOM FLANNAGAN JUIN 2 J 2002
"EAST CAROLINA ENVIRONMENTAL, EAST CAROLINA REG. LANDFILL"
1922 REPUBLICAN RD
AULANDER, NC 27805 D V V Q-WARO
Subject: NOTICE OF VIOLATION
FAILURE TO SUBMIT RENEWAL APPLICATION
"EAST CAROLINA ENVIRONMENTAL, EAST CAROLINA REC
NCG 120000
COC NUMBER NCG 120045
BERTIE COUNTY
Dear Permittee:
This letter is to inform you that, as of the date of this letter, the Division of Water Quality has not received a
renewal request for the subject permit certificate of coverage. This is a violation of NCGS §143.215.1 (c)(1) which
states "All applications shall be filed with the commission at least 180 days in advance of the date on which it is
desired to commence the discharge of wastes or the date on which an existing permit expires, as the case may be".
Any permittee that has not requested renewal at least 180 days prior to expiration or permittee that does not have a
permit after the expiration and has not requested renewal at least 180 days prior to expiration, will be subjected to
enforcement procedures as provided in NCGS § 143-215.6 and 33 USC 1251 et. seq.
In order to prevent continued, escalated action, including the assessment of civil penalties you must submit a
completed permit coverage renewal application to the attention of the "Stormwater and General Permits Unit" at
the letterhead address within ten (10) days of your receipt of this letter (renewal application enclosed). If the
subject discharge has been terminated, please complete the enclosed rescission request form. Mailing instructions
are listed on the bottom of the form. You will be notified when the rescission process has been completed.
Thank you for your prompt attention to this situation. If you have any questions regarding this matter, please
contact Aisha Lau of the central office Stormwater and General Permits Unit at 919-733-5083, ext. 578.
Sincerely,
for Alan W. Klimek, P.E.
Director, Division of Water Quality
cc: Stormwater and General Permits Unit Files
Central Files
Washington Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
D ~<
December 27, 2001
TOM FLANNAGAN
REPUBLIC SERVICES OF NC LLC
1922 REPUBLICAN RD
AULANDER, NC 27805
Gregory J. Thorpe, Ph.D.
Acting Director
RECEpVEDsion of Water Quality
MAR -- 8 2002
DWQ-WARO
Suhject: NPDES Stormwater Permit Renewal
REPUBLIC SERVICES OF NC L1-C
COC Number NCC 120045
Bcrtie County
Dear Permiltee:
Your facility is currently covered for stormwater discharge under General Permit NCC 120000, This permit expires
on August 31, 2002. The Division slal'f is currently in the process of rewriling this permit and is scheduled to have
the permit reissued by late summer ol'2002. Once the permit is reissued, your facility would he eligible for
continued coverage under the reissued permil.
In order to assure your conlinucd coverage under the general perinit, you must apply to the Division of Water
Quality (DWQ) for renewal ol'your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. Theapplication must he completed tmd relurnesl by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge ol'storrnwater frorn your facility
without coverage under a valid stortnwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could resell in assessments ol' civil penalties of up to $10,000 pet- day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the I 1 categories of "storm water discharges associated with industrial activity," (except
construction activities). ]f you feel your lacility can cerfify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stortnwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff niernher listed below or check the Stormwater & General
Permits Unit Web Site at littp:Hti2o.enr.state.nc.us/sti/stormw tter.Iilml
II'the Subject stormwater discharge to waters of the stale has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will he notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Robert Tankard of the
Washington Regional Off icc at 252-946-6481 or Aisha Lau of the Central Office Stormwater Unit at (919)
733-5083, cxt, 578
Sincerely,
.l
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Washington Regional Office
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NCDENit
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
Kerr T. Stevens, Director
Mr. Tom Flannagan
Republic Services of North Carolina, LLC
1922 Republican Road
Aulander, North Carolina 27805
Dear Mr. Flannagan:
P_T_ 1 F?W'A •
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL ResouRCE5
March 26, 2001
I
} I°an- P 28 2001
i t1 L
I I
Subject: NPDES Permit Modification — Name Change
Permit NCG120045
Republic Services of NC, LLC
(Formerly East Carolina Environmental, Inc.)
Bertie County
In accordance with your request received March 20, 2001, the Division is forwarding the°subject permit
modification. This modification documents the change in name at the subject facility. All.othcr,terms and conditions in the
original permit remain unchanged, and. in full. effect. This permit modification is:issued under the 'requirements of North
Carolina General Statute •1437215.1 and the Memorandum of Agreement between North Carolina and the U.-S. Environmental
Protection Agency dated December`6, 1983. , ' • . ' ' I . 11. I °' r ', ' '
If any parts, measurement frequencies or'sampling requirements contained in this, p6rmit:modification are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days ,following
receipt of this letter, This request must be a written petition conforming to Chapter 150B of the North Carolina General
Statutes, filed with the Office of Administrative Hearings, Post Office Drawer,27447, Raleigh, North Carolina 27611-7447.
Unless such demand is made, this decision shall be final and binding.
This permit does not affect the legal requirement to obtain other permits which may be required by the Division of
Water Quality, the Division of Land Resources, Coastal Area Management Act, or any other Federal or Local government
permit that may be required. If you have any questions concerning this permit, please contact Valery Stephens at the
telephone number or address listed below.
cc: Central Files
Washington Regional Office, Water Quality Section
NPDES Unit
Point Source Compliance Enforcement Unit
1617 Mail Service Center, Raleigh, North Carolina 27699.1617
Sincerely,
UA�'&ftA�
Kerr T. Stevens
919 733.5083, extension 520 (fax) 919 733.0719
VISIT US ON THE INTERNET @ httpJlh20.enr.S1ate.nc.us/ [e-mail]

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG120000
CERTIFICATE OF COVERAGE No. NCG120045
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations
promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution
Control Act, as amended,
,.Republic Services of -North Carolina;..LLC <„
is hereby authorized to discharge stormwater from a facility located at
Republic. Services of North Carolina, LLC
NC 1225 — Republican Road
Aulander.
Bertie County
to receiving waters designated as unnamed tributary to Cashie River, in the Roanoke River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, III, IV, V,
and VI of General Permit No. NCG120000 as attached.
This certificate of coverage shall become effective March 26, 2001.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day March 26, 2001,
I u'L� -
err T. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

State of North Carolina
Department of Environment,
.Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Stephen Addington
East Carolina Environmental
771 Corporate Dr. , Suite 1000
Lexington, KY 40503
Dear Mr. Addington:
WASHINGTON OFFICE IF
UtU 0 9 1993 A4
• •
aEM.
SEW N --
November 29, 1993
Subject.
General Permit No. NCG120000
East Carolina Environmental
COC NCG 120045
Bertie County
In accordance with your application for discharge permit received on August 18, 1993, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 A and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6,1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 919/733-
5083.
Sincerely,
Original Signed BY
Coleen H. Sullins
A. Preston Howard, Jr., P. E.
cc: washington_Regional=office
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
Telephone [phone] FAX [phone]
50% recycled/ 10% post -consumer paper
r.

STATE OF NORTH CAROLINA
WASH1'fNGTONE0FFICi
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DMSION OF ENVIRONMENTAL MANAGEMENT ULU 0 9 1993
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
East Carolina Environmental, Inc.
is hereby authorized to discharge st.ortnwater from a facility located at
East Carolina Regional Landfill
NC 1225 - Republican Road
Aulander
Bertie County
to receiving waters designated as an unnamed tributary to Cashie River in the Roanoke River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, and
III of General Permit No, NCG 120000 as attached.
This Certificate of Coverage shall become effective November 29, 1993.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day November 29, 1993.
Original Signed 13y-
Coleen H. Sullins
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

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