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NCG100199_MONITORING INFO_20190218
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V OO I �� DOC TYPE ❑HISTORICAL FILE 'MONITORING REPORTS DOC DATE o oe-t YYYYMMDD Mid Atlantic Engineering & Environmental Solutions February 10, 2019 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 Facsimile 919.250.9950 MAAONLINE.COM NCDEQIDWR RECEIVED Attention: Central Files 1617 Mail Service Center FEB 18 2019 Raleigh, North Carolina 27699-1617 CENTRAL FILES D1NR SECTION Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concem: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on December 12, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR:2018 FACILITY NAME G&N Used Auto Parts COUNTY Nash PERSON COLLECTING SAMPLE(S) George VaRnieres PHONE NO. 252 977-3710 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting 'No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 .... 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0-9.03 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 12/12/2019 8.2 <3.9 <4.8 <5.0 <0.005 NA Note- If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title rint title] Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." i 3 - Aq (Signature of Permittee or Designee (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 aceAnalytical W",,Gacalabs.cm December 20, 2018 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N USED AUTO PARTS Pace Project No.: 92410575 Dear Chuck Hoffman: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 (�Ia'ne Analytical' www.pacelabs.com Project: G&N USED AUTO PARTS Pace Project No.: 92410575 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification M C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification #: 80226 Kentucky W W Certification #:98019 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/N E LAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL0065 Oklahoma Certification #: 2018-101 Texas Certification #: T104704355-18-12 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-16-00257 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 2 of 13 aceAnalytical www.pa�ceaBb9.cam SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersvitle, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92410575 Analytes Lab ID Sample 10 Method Analysts Reported Laboratory 92410575001 OUTFALL NO. 1 EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol-G lycol RID 1 PASI-I EPA 601 OD SH1 1 PASI-A SM 254OD-2011 CEH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 13 aceAnalytrcal� *WW.Petef 8.WM ANALYTICAL RESULTS Project: G&N USED AUTO PARTS Pace Project No.: 92410575 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 1 Lab ID: 92410575001 Collected: 12/12/18 10:00 Received; 12/13/18 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Total Petroleum Hydrocarbons 8015M Glycols in water Ethylene glycol 6010 MET ICP Lead 2540D Total Suspended Solids Total Suspended Solids Date: 12/20/2018 02:00 PM Analytical Method: EPA 16645 ND mglL 4.8 1 12/20/18 05:03 Analytical Method: EPA 8015 Alcohol -Glycol ND mglL 5.0 1 1211811816:40 107-21-1 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A NO ug1L 5.0 1 12/15/18 03:35 12/17/18 03:36 7439-92-1 Analytical Method: SM 2540D-2011 ND mg1L 3.9 1 12/15/18 07:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 acmnalytical wtrw.pacefabs.mn QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92410575 QC Batch: 448699 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92410575001 METHOD BLANK: 2457606 Associated Lab Samples: 92410575001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2457607 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersviiie, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 12/20/18 04:42 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 19.2 18.6 98 64-132 MATRIX SPIKE SAMPLE: 2457608 35436943002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU 20 22.8 96 64-132 Results presented on gels page are In the units Indicated by the "Units" column except where an afternale unit Is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/20/2018 02:00 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalyiical www.psceiabs.com QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92410575 QC Batch: 476916 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92410575001 METHOD BLANK: 2201052 Associated Lab Samples: 92410575001 Parameter Units Ethylene glycol mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/18/18 15:36 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2201053 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 32.6 130 55-144 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2202081 2202082 MS MSD 10458901001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 30.7 31.6 117 120 38-154 3 Results presented on this page are In the units Indicated Uy the "Units" column except where an alternate unit IS presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/20/2018 02:00 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalyticale www.pac$Ws.com QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92410575 QC Batch: 447513 Analysis Method: EPA 601 OD QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92410575001 METHOD BLANK: 2452125 Associated Lab Samples: 92410575001 Parameter Units Lead uglL LABORATORY CONTROL SAMPLE: 2452126 Parameter Units Lead uglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/17/18 03:12 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 411 82 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2452127 2452128 MS MSD 92410522027 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result . % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 422 438 84 88 75-125 4 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/20/2018 02:00 PM without the written consent of Pace Analytical Services, LLC. Page 7of13 aceAnalytical www,pecobs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92410575 QC Batch: 447794 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92410575001 METHOD BLANK: 2453565 Matrix: Water Associated Lab Samples: 92410575001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/15/18 07:35 LABORATORY CONTROL SAMPLE: 2453566 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 251 258 103 90-110 SAMPLE DUPLICATE: 2453567 92410531002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 491 485 1 SAMPLE DUPLICATE: 2453568 92410643002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO NO Results presented on this page are in the units indicated by the "hits' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/20/2018 02:00 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalytica! "W.PaC4ft .carry QUALIFIERS Project: G&N USED AUTO PARTS Pace Project No.: 92410575 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up t1 - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services -Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/20/2018 02:00 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 aceAnalytrcal� www.pacelabs.cm QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: G&N USED AUTO PARTS Pace Project No.: 92410575 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92410575001 OUTFALL NO. 1 EPA 1664E 448699 92410575001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol 476916 92410575001 OUTFALL NO. 1 EPA 3010A 447513 EPA 601 OD 447839 92410575001 OUTFALL NO. 1 SM 2540D-2011 447794 Date: 12/20/2018 02:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 • Sample Condition Upon Recei t(SCUR) Page 1 of 2 acekalical Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receivittg samples: Asheville ❑ Eden(] Greenwood ❑ Huntersvillg, f Ralelgh❑ Mechanicsville❑ Client Name: W®# ; 924 1 0575 Project #: — --Courier:— -- ,0Ped'Ex ❑UPS ❑LISPS _ _-❑Clle-nE ❑ Commercial ❑Pace ❑Other:. 92410575 Custody Seal Present? ❑Yes ,ONO Seals Intact? ❑Yes -dNo Packing Material: [JB bu ble Wrap ]Bubble Bags ❑None ❑ Other Thermometer: ❑ Ifl Gun Io: 92TO46 Type of Ice: tjWet []Blue Cooler Temp ('Q: 3 Correction Factor: Add/Subtract (T) 0.0 Cooler temp Corrected ('Cl: USDA Regulated Soil ( N/A, water sample) Did samples originate in a quaranilne zone within the United States: CA, NY, or SC (check maps)? ❑Yes ❑No - pate/Initials Person Examining Contents: �— 0 - 7 ` t ' Biological Tissue Frozen?. ❑Yes [:]No 3k/A ❑None Tempshould be above freezing to VC Samples out of temp criteria. Samples on Ice, cooling process has begun Did samples originate from a foreign source (inter6kbnally, 1-1iidlnoHawaii and Puprtn Ricni7 1`16s nNo Comments/Discrepancy: Chain of Custody Present? es []No N/A 1. Samples Arrived within Hold Time? Yes [-]No []NIA 2. Short Hold TlmeAnalysis (<72 hr.)? ❑yes UN. ❑N/A 3. Rush Turn Around rime Requested? Yes �o ❑N/A 4. SufficientVolum"e7 es No N/A 5. Jr 1 ( cur T Correct Containers Used? -Pace Containers Used? fees []No ❑No []No ❑N/A ❑N/A 6. Containers Intact? 2res ❑No ❑N/A. 7. Dissolvadana Sls:Samples FieldFlltered7 Yes ❑No NIA B. Sample Labels Match COC? -Includes Date/Ti me/ID/Analysis Matrix: 1 es (:]No ❑N/A 4. Headspace In VOA Vials (>5-6mm)7 Yes ❑No ❑N/A S0. Lv Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Des ONO .219/A ❑No N/A 11. COMMENTS/SAM4PtE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Field Data Required? []Yes []No Project Manager SCURF Review: /, Date: A, %f J / 1 Project Manager SRF Review: }'%f r _ Date: �, ��1 /'4l ) Page 11 of 13 N !+ C 1p 00 V Ol lA A w N F+ Items ZZZZZZxAZxZZZ BP4U-125 mL Plastic Unpreserved (N/A) (CI-) BP3U-250 mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) 8P4S-12S mL Plastic H25O4 (pH < 2) (Cl-) 9F314-250 mL plastic HNO5 (pH < 2) BP42-125 mL Plastic 2N Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (C)-) WGFU-Wide-mouthed Glass Jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (CI-) AG1H-1 liter Amber Hd (pH < 2) AG3U-250 mLAmber Unpreserved (N/A) (Cl-) zzzzZZAIAX AGiS-1 liter Amber H2SO4 (pH < 2) AG35-250 mL Amber H2SO4 (pH < 21 AG3A(DG3A)-750 mL Amber NH4Cl'(N/A)(LI-) DG9H-40 mL VOA HCI (N/A) VG9T-40 mL VOA N22S2O3 (N/A) �f VG9U-40 mL VpA Ur•P (N/Ai DG9P-00 ML VOA H3PO4 (N/A) VOAK(6 vials per kit)-5035 kit (NIA) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A— lab} SP2T-2SG mL Sterile Plastic (N/A— lab) BP3A-2SO mL Plastic (NH2)2SO4 (9.3-9.7) AGOU-100 mL Amber Unpreserved vials (N/A) VSGU-20 mL Scintillation vials (N/A) 8G9U-40 mL Amber Unpreserved vials (N/A) N 0 w aceAnalXical ..n:.pa:eraosc:.m CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain•of•Cuslody is a LEGAL DOCUMENT. AS relevant fields mull be completed a=ealely, Section A Section B Section C Page_ eT Reelulred Client InfotrnationRequired Project Iniormalion: invoice Infornuttion; CarToany: Mid -Atlantic Associates, Inc. Report TO'. Chuck Hoffman (choffman@maaonline.corn) Attention: Chuck Hoffman Aodress: 409 Rogers View Court Copy TO: Ron i]avis (rdavis@maeonline.com Company Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, INC 27610 Address, 409 Rogers View Court, Raleigh, NC 1 NPDEs i GROUND WATER r DRINKING WATER F— UST r RCRA � 1— OTHER Emaa To: choffman@maac,niine.com Purchase Cyder NO.: R2037.00 °per Q'A* — Refeferxe: Phone: 919-250-9918 Fax! 919-250-9950 Prow Name: G&N Used Auto Paris P'— P'Wd Tyriek Hooks Site Location rapt 0g.r, STA TE; NC Requested Due DaIdTAT: STandard Project Number. R2037,02 poca Pmfde s', 5921 Requested Anatysis Filtered (YIN) Section D Vaf]d Matrix Ceder aa y z NegMifed caefa tm«m rlan NMTRIX = -_ COLLECTED Preservatives i N Y N Y ORMq —TER OW WT ^ OU = a) WATER WW WASTEWATER P 4 • U COMPOSITE START COMPOSITE O Z PRODUCT $L salUSOUO OL Z 4 ENGfGRAB SAMPLE ID AR Y �? w � `r° ; m ,APE (A-7- D-9 f,-) OTHER Ts Lu c z F o `o Sample IDS MUST BE UNIQUE TISSUE O IL r (.7 m U U x Q o"J.11 _ F CL of O n C a O G 0 W m r Q 0 d m w DATE TIME DATE TIME rn a 7 r Y Y z z O LU m Pace Project NoJ Lab I.O. i-" Cutfall No. 1 WT G 7 4 1 2 1 Xi x x x Rainfall (inches): 2 H: •3 7 { g• , E 9 10 r 12 ADT10NAL COMMENTS " - OI -• • RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BYN ,iAFRLU%T10_ DATE 'TIME 4 SAMPLE CONDITIONS J SAMPLER NAME AND SIGNATURE m PRINT Name OT SAMPLER: e— A _ m t0 CD s m a u z U '��'+ m to E 17 DATE Signed .2— SIGNATURE of SAMPLE 'Ig rjMM10DfYY): /2� r — 0 (✓ 1 -MnPartant Nele; RV sC,^ thisfarm Mee 11e-01kC Putt NET 30dry pt ffl termt.md,6rt Mie lair• thanesof 3.5%VP mensh 101 A"-m— aot p+id w0ie 30dm. F-ALL-Q•02Dr .08, 12.Oct-2007 a•" Mid Atlantic Engineering & Environmental Solutions May 21, 2018 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.2 50.99 18 facsimile 919.250.9950 MAAONLINE.COM RECEIVED MAY 3 0 2018 C �EN = F«1L fifLE D A'R SECTIC , Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on April 24, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 FACILITY NAME G&N Used Auto Parts COUNTY Nash PERSON COLLECTING SAMPLE(S) George Vagnieres PHONE NO. 252) 977-3710 CERTIFIED LABORATORY(S) Pace Analytical Lab #12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units. Total Suspended Solids (TSS), mg/L Non -polar O&G/TP1H (Method 1664 SGT-HEM),, mg/L"" Ethylene Glycol, mg/L ,. Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0-9.01 "106/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 4/24/2018 1.24 7.9 21.4 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 5-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Pr -es . Title (P 'nt title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 5-c'?, 411--.204? (Date) Form SWU-2S1, last revised October25, 2012 Page 2 of 2 ace Analytical wmpacetabs conr May 08, 2018 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N Used Auto Parts Pace Project No.: 92382167 Dear Chuck Hoffman: Pace Analytical Services, LLC 9800 Kincey Ave. suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Ifyou have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 • aceAnalytical www.pacelab&C= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: GSN Used Auto Parts Pace Project No.: 92382167 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification #: CL-0065 Illinois Certification #: 200074 Oklahoma Certification #: 2017-124 Indiana Certification #: C-49-06 Texas Certification #: T104704355-18-12 Kansas/NELAP Certification #:E-10177 West Virginia Certification #: 330 Kentucky UST Certification #: 80226 Wisconsin Certification #: 999788130 Kentucky WW Certification #:98019 USDA Soil Permit #: P330-16-00257 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification M E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification M 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification M E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 ace Analytical " www.paceiabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)B75-9092 SAMPLE ANALYTE COUNT Project: G&N Used Auto Parts Pace Project No.: 92382167 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92382167001 Outfall No. 1 EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol RID 1 PASI-1 EPA6010 SH1 1 PASI-A SM 2540D MVC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalyfrcal. wwwpacawbs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: G&N Used Auto Parts Pace Project No.: 92382167 Sample: Outfall No. 1 Lab ID: 92382167001 Collected: 04/24/18 11:40 Received: 04/25/18 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 05/06/18 23:51 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 04/27/18 17:45 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND uglL 5.0 1 04/27/18 22:45 05/04/18 20:21 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 21.4 mg1L 7.1 1 04/30/18 18:52 Date: 05/08/2018 10:39 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical. wwwpaceiabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92382167 QC Batch: 409546 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92382167001 METHOD BLANK: 2272001 Matrix: Water Associated Lab Samples: 92382167001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 5.0 05/06/18 23:33 LABORATORY CONTROL SAMPLE: 2272002 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 19.2 19.3 100 64-132 MATRIX SPIKE SAMPLE: 2272003 92382291001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 19.5 97 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 s acmnalytical www.pacetebs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )B75-9092 Project: G&N Used Auto Parts Pace Project No.: 92382167 OC Batch: 438816 QC Batch Method EPA 8015 Alcohol -Glycol Associated Lab Samples: 92382167001 METHOD BLANK: 2027761 Associated Lab Samples: 92382167001 Parameter Units Ethylene glycol mg/L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/26/1814:21 LABORATORY CONTROL SAMPLE: 2027762 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 19.5 78 55-144 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2030951 2030952 MS MSD 50195437002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 30.7 29.5 113 108 38-154 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuQ, Date: 05/08/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytircal a www.pacawbs.coom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92382167 QC Batch: 408343 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92382167001 METHOD BLANK: 2265909 Matrix: Water Associated Lab Samples: 92382167001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 05/0411819:47 LABORATORY CONTROL SAMPLE: 2265910 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead uglL 500 483 97 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2265911 2265912 NIS MSD 92382446002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 494 482 99 96 75-125 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05108/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical e www.pacefa6s.tpm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92382167 QC Batch: 408590 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382167001 METHOD BLANK: 2267100 Matrix: Water Associated Lab Samples: 92382167001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/18 18:46 LABORATORY CONTROL SAMPLE: 2267101 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 252 101 90-110 SAMPLE DUPLICATE: 2267102 92382134001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 6.2 7.0 12 D6 SAMPLE DUPLICATE: 2267103 92382161001 Dup Parameter Units Result Result RFD Qualifiers Total Suspended Solids mg/L 15.8 15.8 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalytical WWW..pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: G&N Used Auto Parts Pace Project No.: 92382167 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL- Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PAS1-C Pace Analytical Services - Charlotte PASI-1 Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 aceAnalytical' www.peoekft.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N Used Auto Parts Pace Project No.: 92382167 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92382167001 Outfall No. 1 EPA 1664E 409546 92382167001 Outfall No. 1 EPA 8015 Alcohol -Glycol 438816 92382167001 Outfall No. i EPA 3010A 408343 EPA 6010 408378 92382167001 Outfall No. 1 SM 2540D 408590 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 10:39 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: uocumens nevueu; rout uo,y 0, cuio aceAnalyticalY Sample Condition Upon Rece! t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F•CAR•CS-033•Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [2'�' Raleigh[] Mechanicsville❑ Client Name: ! I, �-[O]Cllpen�t ject Courier el❑UPS USPS ❑ Commercial ❑Pace ' ❑Qther: Custody Seal Present? ❑Yes 124o Seals Intact? ❑Yes Qi oo Packing Material: ❑Bubble Wrap Ueubble Bags []None ❑ Other Thermometer: Type of Ica: Blue ❑ IR Gun 10: 92TO36 � ❑ Cooler Temp ('C): �• ii Correction Factor: Add/Subtract ('C) +p,j Cooler Temp Corrected ( USDA Regulated Soil ( N/A, water sample) Did samples originateln 'a quararitine zone within the United States: CA, NY, or SC (check maps)? MYes F INo W0# 92382167 I Il�ll��lllill 1llill 111 92362167 Datelinitials Person Examining Contents/ Biological Tissue Frozen? ❑None ❑Yes [)No EWA— Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on Ice, cooling process has begun Did samples originate from a foreign source (internationally, inrl•.idlnrr Hawall and Puerto Rica,? Dyes nNo Cam ments/Dlscrepancy: Chain of Custody Present? es No N/A 1. Samples Arrived within Hold Time? No N/A 2. Short Hold Time Analysts (42 hr.)? QYES o ❑NIA 3. Rush Turn Around Time Requested? Yes CWo ❑NIA 4. Sufficient Volume? No ❑N/A 5. t �7 rr {r \ 71 1 )L`t!�' Correct Containers Used? -Pace Containers Used? Wee$ Yes ❑No No ❑N/A ❑N A 6. Containers Intact? No N/A 7. Dissolved analysis. Samples Field Filtered? ❑Yes QKO' ❑N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: [2XW (:]No ❑NIA 9. Heads ace in VOA Vials s5.6mm]? QV6 []NO N/A 10. t �! l G(� j�i6ti'b e Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes EJYCS o Elflo pN/A NIA 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Protect Manager SRF Review: Date/Time: Field Data Required? (]Yes ❑No Date: Z� Date: Page 11 of 13 VVLL111C11L IMOL11C• aceAfta! C8f Sample Condition U on Recei t(SCUR) r Page 1 of 2 Document No.: Issuing Authority: F•CAR-CS•033•Rev.06 Pace Carolinas Quality Offic Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (watet) DOC, LLHg "Bottom half of box Is to list number of bottle Project NW®# 923621.67 i, PM: NMG flue Date: 03/09/1B CLIENT: 82-MID ATLAN j L is m mL n u E v1 •N•1 a L 2 C Dr-c u E /0� N a N es N n u E 0 0 a z u Z uui m 7 m r9 a v x a v ry E N N a N m 0 I E d N A. m m Cu Q z m E � x c Q ro u N a E y� N ro 9 t °' g 3 z d y C = a E v �_ .. N v S n .0 E `m M = VJ u y c 7 n`y E Q E N 3 N S p N ` o E ` .r M V a v1 = v E ¢ E yy'11 1V lh U z `m Q 0 ¢ frn� Q 4 2 '. S 4 O 1 E s Z 1r1 O 2 d O F � Y d Z o j 6 O E � a z v O CL = 4 O a E O d . 1n o i it ,sn y :'�'. sr Z In ro a is n r '3 = ac I Z u N �' y vi 1 E rn N F, _ I Z `- U ^ m :+ 1^ E � 4n Nr "� O in N i 2 u a E yo7 rV d u N m c a E 1 E $ n a 1n m c 21 c n E C ry z I m Z u u n 3 `m a a E 1 - j fl X' I Y N z 3 4 5 fi 7 S 9 10 li 12 —H— \1 N\N pH Adjustment Log for Preserved Samples Sample 10 iype of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot p _ ___ e. wneOeNpr rhrrn is - - the Nartn Carolina Utnlvn Lerarlcau Vn —11L. I.,e, Out Of hold, intarrect preservative, out of temp, incorrect containers. Page 12 of 13 fi 1,.�e.4ria�jfipt� Section A Required Client lnformation: Section B Required Project Information: CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Page: 1 Of t Company: Mid Atlanix Associates, Inc. Report To: Chuck Hoffman Attention:. Address: 409 Rogers View Court Copy To: Company Name: Raleigh, NC 27610 Address: _ ' Regulatory Agency Email: Purchase Order il: Pace Quote: Phone; Fax Project Name: G&N Used Auto Parts Pace Project Manager. nicole,gasiorowski pacelabs_com. State I Location Requested Due Date: Project s, Pare Profilo a: 5921 NC Requeztod Ariaf is Filtemd (YIN - - - a y MATRU CCIM — 0 COLLECTED � Preservatives IN—V W.I. Dw q u w.u. warn vwv n a Z P.—d P SAMPLE ID H m m o• OL �s START END One Character per boa_ ww wP i d s (A-Z, 0-9 r, -) A. Ids be , of m O 4 (7 a m U must unique T c ,�„ „�� oz v m '� S g ~ J L UJIsampla ei a In y a r o ~ y DATE TIME PATE TIME ✓�+ : S = = z z O" r m W a/i 30 vio l(•v I 1 ci I 1 Out1aIl No, 7 uvr x x x x z - /.. 3 4 r 5 `I_ / im4e- t 6_ 7 B 9 10 11 12 1 +1 �. ADOmON.SL COIAMENTS " - RELINQUISHED BY f AFFILIATION DATE TIME ACCEPTEDJ7 f AFFILWTtON - DATE TIME - SAMPLE CONDITIONS L S -!,C 0 0 t . az ,' - SAMPLER NAME AND SIGNATURE c S a C PRINT Name of SAMPLER: _E3 P rfJt .z _0 m Z m o? _ E g? SIGNATURE of SAMPLER t DATE Signed: Ifs STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGlOO199 �� SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 -N (This monitoring report shall be received by the Division no later than 30 days 5 ZV from the date the facility receives the sampling results from the laboratory.) FACILITY NAME G&N Used Auto Parts �JLES COUNTY Nash PERSON COLLECTING SAMPLE(S) George Vagnieres"��'�� `�"v PHONE NO. (252) 977-3710 CERTIFIED LABORATORY(S) Pace Analytical _ Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 s,aoo (Tiers 2 and 3) 0.03 1.0 Outfall001 8/29/2017 2.0 8.1 11.0 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. headings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form 5WU-251, lost revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention UA Pla �i'�li�C�S Name (Print name) Elf Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 T- 00-/' Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge a nd belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or e) Y_06NI (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 aceAnalytical www.pacelabs.= Pace Analytical Services, LLC 9B00 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 September 15, 2017 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N Used Auto Parts Pace Project No.: 92353346 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on August 30, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 13 aceAnalytical wwwpacslabs.C= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersviile, NC 28078 (704)875.9092 Project: G&N Used Auto Parts Pace Project No.: 92353346 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 003971 Indiana Certification #: C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification #: 80226 Kentucky WW Certification #:98019 Charlotte Certification IDs 9800 KinceyAve, Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LAW0028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2016-075 Texas Certification #. T104704355-16-10 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330.16-00257 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical www.pacetabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: G&N Used Auto Parts 92353346 Analytes Lab ID - Sample ID Method Analysts Reported Laboratory 92353346001 Outfall No. 1 EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol BJVV 1 PASI-I EPA6010 SH1 1 PASI-A SM 2540D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, UC Page 3 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 HuntersviRe, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: G&N Used Auto Parts Pace Project No.: 92353346 Sample: Outfall No. 1 Lab lD: 92353346001 Collected: 08/29/17 11:05 Received: 08/30/17 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 5.0 1 08/31/17 06:04 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 09/05/17 14:51 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND uglL 5.0 1 09/12/17 21:25 09/14/17 03:38 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 11.0 mg/L 6.2 1 08/31/17 01:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical® www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92353346 QC Batch: 375861 QC Batch Method: EPA 1664B Associated Lab Samples: 92353346001 METHOD BLANK: 2081960 Associated Lab Samples: 92353346C01 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 08/31/17 05:53 LABORATORY CONTROL SAMPLE & LCSD: 2081961 2081962 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mglL 20 19.3 19.4 96 97 64-132 1 30 Results presented on this page are in the units indicated by the "Units" column except where an altem ate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09115/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical+m www.pacelabs.c m Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92353346 QC Batch: 404158 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92353346001 METHOD BLANK: 1859527 Associated Lab Samples: 92353346001 Parameter Units Ethylene glycol mg1L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 0910511712:46 LABORATORY CONTROL SAMPLE: 1859528 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mglL 25 30.8 123 41-162 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1859529 1859530 MS MSD 30228429001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 33.0 35.3 122 132 20-172 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2017 0& 18 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalyfical wwtvpacefabs.=" Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GIN Used Auto Parts Pace Project No.: 92353346 QC Batch: 377234 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92353346001 METHOD BLANK: 2090151 Matrix: Water Associated Lab Samples: 92353346001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 09/14/17 03:01 LABORATORY CONTROL SAMPLE: 2090152 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 464 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2090153 2090154 MS MSD 92353331001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L 2.5U 500 500 468 459 94 92 75-125 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except it full, Date: 09/15/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical wwwpacalabs.own Pace Analytical Services, LLC 98001 Ave. Suite 100 Huntersville, i 2BO78 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92353346 QC Batch: 375843 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92353346001 METHOD BLANK: 2081914 Matrix: Water Associated Lab Samples: 92353346001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/31/17 01:09 LABORATORY CONTROL SAMPLE: 2081945 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2081916 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2081917 Parameter Units Total Suspended Solids mg/L Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 254 102 90.110 92352892001 Dup Result Result 12.8 15.2 92353332006 Dup Result Result 9.0 9.1 RPD Qualifiers 17 D6 RPD Qualifiers 1 Results presented on this page are in the units indicated by 1he "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, Date: 09/15/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalyticaI www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: G&N Used Auto Parts Pace Project No.: 92353346 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N -N itrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-1 Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 ace Analytical "m..pacalafu.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N Used Auto Parts Pace Project No.: 92353346 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92353346001 Outfall No. 1 EPA 1664E 375861 92353346001 Outfall No. 1 EPA 8015 Alcohol -Glycol 404158 92353346001 Outfall No. i EPA 3010A 377234 EPA 6010 377501 92353346001 Outfall No. 1 SM 2540D 375843 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2017 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: August 4, 201? Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: r BC0ARc?!` ica F•CAR-CS•033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ SamplieXonclitionClient Name: WO# � 9235334fi Project N; .. ��,t.� �t--�1���.t rks�L,•,,4f Courier: ' QFed Ex �]UP$ USPS T []Client 1111111111111111111111 ❑ Commercial ❑Pace ❑Other: 6 Date/Initlals Person Examining Contents: 1, �� I Packing MaterlaI ❑Bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes []No❑N/A ❑ YP IR Gun 10: J Type of Ice: wet [-]Blue ❑none Correction Factor: Cooler Temp Corrected {'CI: Z Temp should be above freezing to VC ❑Samples out of temp criteria.5amples on ice, cooling process has begun USDA Regulated oil I [Q N/A, water sample) Did samples or" mate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter it'onaEly, ❑Yes No including Hawaii and Puerto Rico)? ❑Yes FNa / Comments/Discrepancy: Chain of Custody Present? es Na N/A 1. Samples Arrived within )told Time? Yes QNo N/A 2. Short Hold Time Analysls 02 hr.)? ❑Yes • No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes o N/A 4, Sufficient Volume? Yes ❑No ❑N/A Correct Containers Used? -Pace Containers Used? LT/e es ❑No No ❑N/A N/A 6. Containers Intact? • es No NIA 7. Dissolved analysis: Samples Field Filtered? Des No N/A 9. Sample Labels Match CDC? -Includes Date/Time/ID/Analysis Matrix: / 21es [:]No ❑N/A 9. Heads ace In VOA Vials (>5-6mm)? ❑Yes d' ❑NIA 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes Yes UNG No ❑NI NIA lt. CLIENT NOTIFICATION/RESOLUTION Field Data Required? Des ❑NO r[n+'r ! _ C Person Contacted: ly L �tb "3(4�� Date/Time: Comments/Sample Discrepancy: iv--4 rvv 4/ U\.) l-� 0. f AIIVW A. D r f71 SS Lot ID of Split Containers: Project Manager SCURF Review: )�l¢� Date: Project Manager SRF Review: � Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form vAll be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect cantalners) Page 11 of 13 m 3 v p K a ^ c' d c m 0 a C. C m LA r^ n '~ ro O r► d ^--. r 0 n O m � n � N (it 1 � 3 (b y A n. v tZ C A R � a o' 3 tp N 3 0 w m n n v CL ro b n 8 a :7 0 Re ma zzzzzzzzzzzv SP41.1-125 mL Plastic Unpreserve (N/A) (Cl.) OM-250 ml.Plastic Unpreserve (N/A) 8PZU-500 mL Plastic Unpreservc (NIA) SP1U-1 liter Plastic Unpreserved ( /A) HP45-125 mL Plastic 112504 (pH c ) (CI-) 9P3N-250 mL plastic HNO3 (pH c ) SP4Z-12S mL Plastic ZN Acetate 2 NaOH (>9) BP4C-12S mL Plastic NaOH (pH > 2) (CI-) WGFU-Wide-mouthed Glass jar Lnpreserved AG1U-1 liter Amber Unpreserved N/A) (CI-) AG114-1 liter Amber HO (pH c 2) G3U-250 mi. Amber Unpreserve�d IN/A) (Cl-) E AG15-1 liter Amber 112504 (pH c ) A." ZZ AG3S-250 mL Amber H2504 (pH < 2) z2izz. ZZZA AG3A(DG3AI-250 mt Amber NH4[I II (N/A)ICI-) i l.fJ OG9H-40 mL VOA IIC1 IN/A) VG9T-40 mL VOA Na2S203 {N/A) VG9u-40 mL VOA Unp (N/A) OG9P-40 mL VOA 143PO4 (NIA) VOAK (6 vials per kit]-5035 kit A A) V/GK (3 vials per kit)-VPH/Gas kit IN/A) SPST-175 mL Sterile Plastic (N/A lab) SPZT-250 mL Sterile Plastic (N/A lab) BP3A-250 mL Plastic (NH2)2SO4 ( .3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N A) Fr I I _F1 GN 0 S � O C w- z LA m CL O �, 3 Cr _S CuO X � 0 Cr O N n X O � � � � z M d y � � 1L O Cr tR M CL O M .'► O10 n Vr O 0 a O 7 O e`b n a uti T � 0 )aQ�o n a c 3 o ra c rb ru n -0 ., w p jp 2 p m ro 4 M c ^ n Co ^ A m rn r 3 � 3 rti w o0 © L C N O. D C7 4 C r M c S /A p o :P — a " e>Q 0 33 Z M In a s• to w 4bb r G V e9 t0 A N w ' za::Tr iml I CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information_ equired Project Information: Invoice Information: Page: 1 Of 1 lFagorl To Holtman, Chuck Attention: opy To: Company Name: Company: Mio Atlantic Associates, Inc, Address apg Roqers View C1 Raleigh, NC 27830 Address: Regulatory A Email: urc trio Order a: Pace Ouote. Phone: Fax eroject Name: GSN Used Auto Pans Pace Project Manager: nicole.gasiorowshi ,pacelabs.com. State I Location ' Requested Due Date: fTojeci N. Pace Profile #: 5921 1 NC Request Analysis Filtered M a 2 ,AATR,x coos ° o COLLECTED Z Preservatives } N—es W. DW U Q Wam WT u to ~ U Was�n Way Product SAMPLE ID WW P _ o 2 m 06 OL u START END One Character per boa, W.P WP w a `•; $ `o tA-Z, 0-9 /, -) n. u� O > w F m m = C7 U Sample Ids must be unique U „_ is x w TO, J O m q c C Q, m w a G n �, <a a s ��`?�� m m�a�� o m f2a5 �3�IG DATE TIME O = _ = z z mi O 1 w 1 OuVall No i I VVT Vnin •US 2 3 4 5 6 7 8 9 10 11 12 j ADOlT10NAL COMMENTS REL INQUlSHED BY I AFFILIATION OATS SINE ACCEPTED 9Y I AFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE C e Mi m z w PRINT Name of SAMPLER: t / w _ A$ Z E m z rn'c } SIGNATURE of SAMPLE DATE Signed: a) rn ny d -,_ - � - 11 Glad Atlantic Engineering 8 Environmental Solutions September 18, 2017 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concern: 409 RogC,tVipw Court Ra;aigh, NC . 7h 10 afl,cc 9#925099i8 lsr.s;m"lc 919'150 9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on August 29, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report Laboratory Analytical Report - --- - - - -- - --- ; v RERIENCEr) CUSTOMER FOCUSED INNOVATIVE .75 A. Mid Atlantic Engineering & Environmental Solutions June 14, 2016 NCDEQIDWR RECEIVED Attention: Central Files JON % 0 2016 1617 Mail Service Center FILES Raleigh, North Carolina 27699-1617 owR S C-rtON Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 2761 v office 919.250,9918 facsimile 919.250.9950 MAAONLIN E.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on May 19, 2016 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918, Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment-. Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199� SAMPLES COLLECTED DURING CALENDAR YEAR:2016 9VC,e " (This monitoring report shall be received by the Division no later than 30 days �d16 from the date the facility receives the sampling results from the laboratory.) SUN FACILITY NAME G&N Used Auto Parts V. this RAL. IFtaS COUNTYNash PERSON COLLECTING SAMPLE(S) George Vagnieres `'�wR S PHONE NO. 252) 977-3710 CERTIFIED LABORATORY(S)Pace Analytical Lab #12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring farm noting "No Flow" or "No Discharge' within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (T5S), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50� 15 $,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 5/19/2016 2.5 7.8 5.7 <1.51 <5.0 0.0077 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 15ee If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Date (cy Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (141 (Signature of Permittee or Designee) (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 UeAnaly'tical. W%Wpacerabs.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 May 27, 2016 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N USED AUTO PARTS Pace Project No.: 92298461 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, d� Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. �q pG�REO REPORT OF LABORATORY ANALYSIS TNT ',r This report shall not be reproduced, except in full, !q � without the written consent of Pace Analytical Services, Inc.. Q�RA' Page 1 of 18 ac6Analytical www.pacelabs.=n Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: G&N USED AUTO PARTS Pace Project No.: 92298461 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification M 0042 Kentucky WW Certification #:98019 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2014-148 Texas Certification #: T104704355-15-9 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-10-00128 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 18 UeAnal tical® J www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: G&N USED AUTO PARTS Pace Project No.: 92298461 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92298461001 OUTFALLNO. 1 EPA 8015AIcohol-Glycol BJW 1 PASI-I EPA 6010 CDF 1 PASI-A SM 2540D MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 18 aceAnalytical www,pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 ANALYTICAL RESULTS Project: G&N USED AUTO PARTS Pace Project No.: 92298461 Sample: OUTFALL NO. 1 Lab ID: 92298461001 Collected: 05/19116 11:00 Received: 05/20/16 09:25 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 05/24/16 17:55 107-21-1 6010 MET lCP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead 7.7 ug/t_ 5.0 1 05/23/16 18:30 05/25/16 08:17 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 5.7 mg1L 3.6 1 05/24/16 11:48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/27/2016 04:50 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 aceAnalytical tsww.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92298461 QC Batch: GCSV/19815 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92298461001 METHOD BLANK: 1546255 Associated Lab Samples: Parameter Units Ethylene glycol mg/L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 05/24/1611:57 LABORATORY CONTROL SAMPLE: 1546256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 27.5 110 60-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1546257 1546258 MS MSD 92297987001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Ethylene glycol mg/L ND 25 25 24.9 24.3 100 97 23-157 3 Results presented on this page are in the units indicated by the "Units" column except where an altemale unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/27/2016 04:50 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 18 aceAnalytical www.pwetabs.com Pace Analytical Services, Inc. 9B00 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92298461 QC Batch: IMPRPI21803 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92298461001 METHOD BLANK: 1739865 Matrix: Water Associated Lab Samples: 92298461001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 05/25/16 07:56 LABORATORY CONTROL SAMPLE: 1739866 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug1L 500 441 88 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739867 1739868 MS MSD 92298450001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Lead ug1L ND 500 500 476 455 95 91 75-125 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/27/2016 04:50 PM without the written consent of Pace Analytical Services, Inca Page 6 of 18 aceAnalytical wwwpwWabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92298461 QC Batch: WET145099 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92298461001 METHOD BLANK: 1739744 Associated Lab Samples: 92298461001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: Parameter 1739745 Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1739746 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1739747 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 05124/1611:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 240 96 90-110 92298318001 Dup Result Result 94.0 106 92298447002 Dup Result Result ND 12.0 RPD Qualifiers 12 D6 RPD Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/27/2016 04:50 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 aceAnalytica!® www,pacelabs.c= Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28076 (704)875-9092 QUALIFIERS Project: G&N USED AUTO PARTS Pace Project No.: 92298461 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-N itrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-I Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/27/2016 04:50 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 18 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N USED AUTO PARTS Pace Project No.: 92298461 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92298461001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol GCSV119815 92298461001 OUTFALL NO. 1 EPA 3010A MPRP121803 EPA6010 ICP119562 92298461001 OUTFALL NO. 1 SM 2540D WET145099 Date: 05/27/2016 04:50 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 18 ��al Analytical. Client Name: Sample Condition Upon Recei t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CHR-CS-003-rev.19 Pace Fluntersville Quality Office jL •�t !r � �C -' 1 ��� Page 2of2forinternalUse ONLY Project: ail®# • 92296461 Courier: ©Fed Ex CUPS ❑USPS ❑Client 11111111111111111111111 ❑ Commercial ❑Pace ❑Other: 92298462 Custody Seal Present? ❑Yes NNo Seals Intact? [—]Yes [PNo 2 hG )f Date/Initials Person Examining Contents: L (M Packing Material: []Bubble Wrap [Bubble Bags []None ❑Other: Thermometer: T1505 Type of ice: 141pet ❑Blue ❑None ❑Samples on ice, coaling process has begun Correction Factor: OVC Cooler Temp Corrected (°C): 2.' CW Biological Tissue Frozen? []Yes [ qNo []N/A Temp should be above freezing to VC USDA Regulated Sbil (❑ N/A, water sample) Did samples originate Ina quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a foreign source (internationally, rlYes fulNa Includlna Hawaii and Puerto Rico)? ❑Yes ®No Comments/Discrepancy: Chalri of Custody Present? WYes []No N/A 1. Sam pies Arrived within Hold Time? QYes ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes PQNo ❑N/A 3. Rush Turn Around Time Requested? ❑Yes No N/A 4. Sufficient Volume? PYes []No ❑N/A 5. Correct Containers Used? Ayes []No ❑N/A 6. -Pace Containers Used? WYes []No N/A Containers Intact? Yes []No []N/A 7. Samples Field Filtered? ❑Yes MNo ❑N/A 8. Note If sediment is visible in the dissolved container Sample Labels Match COC? 1 �-•� Ql-LI✓L/ Yes [:]No ❑N/A 9. -Includes Date/'rime/ID/Analysis Matrix: All containers needing acid/base preservation have been 10. HII0 PH42 checked? ENS ❑No []N/A All containers needing preservation are found to be In Na IM2 compliance with EPA recommendation? HZS019H41 (HNO3, H2SO4, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) ®Yes ❑No []N/A HcOH P11.12 Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC,LLHg WYes QNo ❑N/A N10HJZ.GAcpH,9 Samples checked for dechlorination? byes 1gNo ❑N/A 11. Heads ace In VOA Vials >5-6mm)? MYes No ❑N/A 12. Trip Blank Present? ❑Yes [ ❑N/A 13. Trip Blank Custody Seals Present? ❑Yes .�No �No ❑N/A Pace Trip Blank Lot q(if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Date/Time: Field Data Required? []Yes [:]No Project Manager SCURF Review: lSl Date: `� � ,0 Project Manager SRF Review: �J �-, Date: 5 Z-d I 0 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, Incorrect preservative, out of temp, incorrect containers) Page 10 of 18 !�aceAnalyfical CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accuralely. m 0 Section A Section B Section C Page- of 8, Required Cfsent Information: Required Project Informationt: InvOX;e Informauom company: Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman@maaonline.com) Atlention: Chuck Hoffman Address: 409 Rogers View Court Capy To: Ron Davis (rdavis@maaonline.com Company Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 Address. 409 Rogers View Court, Raleigh, NC NPDES r- GROUND WATER ; DRINKING WATER i UST i- RCRA r- OTHER Ema l Tv: choffman@maaonline.com Purchase order No.: R2037.00 Pace Ovate - Reference: Phone: 919-250-9918 Fax: 919-250-9950 Project Name: G&N Used Auto Parts Pace Praject Nicole Gasiorowski Site Location Manager. STATE: NC Requested Due Date/TAT: standard Project Number. R2037.00 Pau prate it. -- q , 1- Requested Analysis Filtered (YIN) Section D Valid Matrix Codas ~ I Requlmd Cgenl Information MATRIX CODE o COLLECTED Preservatives i N Y N Y oawxwc wA: ER Dw v U WATER WT WASTEWATER Ww 'e' u U COMPOSITE OOseM51TE I- L) 17 PRODUCT P m START EN=P a _ Z SORI-•OUD SL m a SAMPLE ID E = i? s CO m to m t I C` (A-z 0-9! •-I OTHER OT d a = H O ?. _= Sample IDS MUST BE UNIQUE Tt=E is p w CL F m y -C (ry m U a a o 0) n O Q S O N o `m C T n ul ~ y DATE TIME DATE TIME H # 7 S S 2 Z Z O F F to Pace Project Nod Lab I.D. 1 Outfall No. 1' wr G y G�"' 7 4 1 2 X. x x x Rainfall inches : '{ 2 H: 7 r f 4 S 0 6 T 1 1 1 5 S 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY r AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS F=rc SAMPLER NAME AND SIGNATURE ' o w m � z ; PRINT Name of SAMPLER: -_ �; ' fi IL�1 � n oZ .-' } o} o e m } " z DATEMDSIIYn1'jed e C/ / SIGNATURE of SAMPLER: : j 2 `�L4 m ~ o y ; e v E y .g (MM c� -tmportamt NOW Sy signing this ram you am accepting Pace's NET 30 nay paMem terms Ono agmmng 10 Late ehafgCS Of 1 5% per month (Of any InvoiCe3 not paid within 30 days. FALL-Q-020rev08. 12-0e1-2007 �bA EN-1CO Laboratoli'leRs Aceerrate. Tir»elf, Responsive. Innovative. 4810 Executive Park Court, suite 111 Jacksonville FL, 32216-6069 Phone: 904.296.3007 FAX: 904.296.6210 Friday, May 27, 2016 Pace Analytical (PA007) Attn: Nicole Gasiorowski 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 RE: Laboratory Results for Project Number: Charlotte Pipe, Project Name/Desc: 92298461 ENCO Workorder(s): BZ02254 Dear Nicole Gasiorowski, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, May 24, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chris Tompkins Project Manager Enclosure(s) Page 12 of 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7 (� �Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OutfallNO. 1 Lab ID: 6Z02254-01 Sampled: 05/19/16 11:00 Received: 05/24/16 11:00 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664E 06/16j16 05/25/16 17:00 05/26/16 14:36 Page 13 of 18 FINAL This report relates onty to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7 cerluca www.encolabs.com SAMPLE DETECTION SUMMARY No positive results detected. Page 14 of 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7 ENCO www.encolabs.com ANALYTICAL RESULTS Description: Outfall NO. 1 Lab Sample I0:BZ02254-01 Received: 05/24/16 11:00 Matrix: Water Sampled.,05/19/16 11:00 Work Order: BZ02254 Project: 92298461 Sampled By: Classical Chemistry Parameters ^ - ENCO Jacksoakile certified awlXe [NC 442] Analytee [CAS Numberl Results fin Units RE EML pQ,L Batch Method Analyzed By Notes Oil & Grease (ITEM-SGT) Non -Polar 1.51 U mg/L 0.558 1.51 2.79 6E25003 EPA 1664E 05/26/16 14:36 SMA Material^ Page 15 of 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7 0PVC www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5E25003 - EPA 1664A Blank (6E25003-BLK3) Prepared: 05/25/2016 17:00 Analyzed: 05/26/2016 14:36 Spike Source %REC RPD .AnDlyte Result Fl0g PPOL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 0.685 U 1.27 mg/L LCS (6E25003-BS1) Prepared: 05/25/2016 17:00 Analyzed: 05/26/2016 14:36 Spike Source %REC RPD -Anal ]de Pesult Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGf) Non -Polar Material 82.6 5.00 mg/L 75.8 109 6+132 LCS Dup (6E25003-65131) Prepared: 05/25/2016 17:00 Analyzed: 05/26/2016 14:36 Spike Source %REC RPD -Ar101yte Rmit Flag K-1 Units Level Result %REC Limits RPD IImi Notes Oil & Grease (HEM-SGT) Non -Polar Material 63.4 5.00 mg/L 74.6 85 64-132 26 34 Matrix Spike (6US003-101SI) Prepared: 05/25/2016 17:00 Analyzed: 05/26/2016 14:36 Source: BZ02254-01 Spike Source Q/oREC RPD .AMIYW Result Flan PS?L tlnit5 Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material silo 3.59 mg/L 57.5 1.94 U 141 64-132 QM-07 Page 16 of 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7 CIEJVCa www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. Page 17 of 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7 Chain of Custody -ZZ,�=l ace Analytical I� •� rxw Y��:''JUS.u.xer Wurkufdur: 922984cl VVOrk>VdP-r Narng: G&W 05,FD A!JTO PANTS I Rosuits Requested By: 611Me Report.I 131;00ice to 'Subcontract Ta:::.. R�rluer.'.ecf Ai�aEysis Nicole Gasia(miis:i F'c= ATIvI}'[ICc11 :r'%Iri4rC !! P.d._'l r 800 Kinc:ey Ax-. Suite 100 Hume.5ville, NC 28078 F'-nna (7: 4)i75 9f)92 �.'nail: niccle.gasi�•rowski�:.;acul�k�s.currr ,��;{.� �,t l � State of Sample Orlgii : NC P--rvad.Cuntaifiers r ii,ni S mrla FD • DBt.hime Lob,10, �MatTiicv 1 OUTFALLN4-1_µ �l1�nn�r,11-nn F229"14rOMI Ylalr:r ....... _.. 1 --- — - - -. 5 Transfers i rleased Dy Datell'ime Fic/c'civcd By D2tefTim/c l 372 2 v 3' niiiieirts LAB USE ONLY .. ............... ... i Cooler Terri erature on Receipt 4), L{ °C Custody Seal Y OF N Received on Ice ZY- or N Sam l'es Intactj'(,or N v • v UD � Fr,daY. Amy 2ti. �-1•t6 r1;07:G s,4Fa - co o FNIT-A I-C-t102rcw,00 . AWO12003 "i 0 • CD ace Analytical www.pacalabs.c= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 October 10, 2016 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N Used Auto Parts Pace Project No.: 92314316 /, c. f�r10`D I91 RECEIVE® NOV o 9 2016 CENTRAL FILES DWR SECTION Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on September 30, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. pc�o TNI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 aceAnalyircal »ww.pa&ab&conr Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92314316 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification #: 0042 Kentucky WW Certification #:98019 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersvilie, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2014-148 Texas Certification #: T104704355-15-9 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit M P330-10-00128 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 acaAnalytrcal www.pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: G&N Used Auto Parts Pace Project No.: 92314316 Analytes Lab ID Sample 1D Method Analysts Reported Laboratory 92314316001 Outfall No. 1 EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASI-I EPA6010 SH1 1 PASI-A SM 2540D CJH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 acmnalyircal wwwpacefabs-wn Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: G&N Used Auto Parts Pace Project No.: 92314316 Sample: Outfall No. 1 Lab ID: 92314316001 Collected: 09/29/16 11:00 Received: 09130/16 10:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mglL 5.0 1 10/05/16 05:59 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 10/03/1615:34 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND uglL 5.0 1 10/03/16 20:15 10/07/16 02:54 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mglL 3.8 1 10/04/16 03:03 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalyiicalm www.pacelabs.com Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92314316 QC Batch: 331845 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92314316001 METHOD BLANK: 1838622 Associated Lab Samples: 92314316001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE. 1838623 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/05/16 05:50 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 17.8 89 64-132 MATRIX SPIKE SAMPLE: 1838624 92314258001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 20 15.0 75 64-132 MATRIX SPIKE SAMPLE: 1838625 35268166001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 58.0 40 97.2 98 64-132 MATRIX SPIKE SAMPLE: 1838626 35268166007 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 5.OU 20 15.3 76 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10110f2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 acaAnalyiical wW..paWahs.c= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875.9092 Project: G&N Used Auto Parts Pace Project No.: 92314316 QC Batch: 354368 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92314316001 METHOD BLANK: 1639957 Associated Lab Samples: 92314316001 Parameter Units Ethylene glycol mg/L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: , EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/03/16 15:15 LABORATORY CONTROL SAMPLE: 1639958 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 21.4 86 60-129 MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 1639959 1639960 MS MSD 92314316001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L ND 25 25 29.0 24.0 116 96 23-157 19 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 aceAnalytica!' wt"wpacefabs.trom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92314316 QC Batch: 331362 QC Batch Method: EPA 3010A Associated Lab Samples: 92314316001 METHOD BLANK: 1836096 Associated Lab Samples: 92314316001 Parameter Units Lead ug/L LABORATORY CONTROL SAMPLE: 1836097 Parameter Units Lead ug/L QUALITY CONTROL DATA Analysis Method: EPA6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/07/16 02:41 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 500 492 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1836098 1836099 MS MSD 92314155005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 488 491 98 98 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 accAnalytical www.pewabs'= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92314316 QC Batch: 331607 QC Batch Method: SM 2540D Associated Lab Samples: 92314316001 METHOD BLANK: 1837355 Associated Lab Samples: 92314316001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1837356 Parameter Units Total Suspended Solids mg1L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 10/04/16 02:58 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 230 92 90-110 SAMPLE DUPLICATE: 1837357 92314300015 Dup Parameter Units Result Result Total Suspended Solids mg/L 81.4 45.7 SAMPLE DUPLICATE: 1837358 Parameter Units Total Suspended Solids mg/L 92314312007 Dup Result Result ND ND RPD Qualifiers 56 D6 RPD Qualifiers Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnalytical www.pacelabs.c= Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersvilte, NC 28078 (704)875-9092 QUALIFIERS Project: G&N Used Auto Parts Pace Project No.: 92314316 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/10/2016 12:27 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 aceAnalytrcal e www.pacalabs.cam Pace Analytical Services, LLC 9800 Kncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N Used Auto Parts Pace Project No.: 92314316 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92314316001 Outtall No. 1 EPA 1664B 331845 92314316001 Outfall No. 1 EPA 8015 Alcohol -Glycol 354368 92314316001 Outfall No. 1 EPA 3010A 331362 EPA 6010 92314316001 Outfall No. 1 SM 2540D 331607 Date: 10/10/2016 12:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 331635 Page 10 of 12 / ceRnalyticalo Sample Condition Upon Receiptl[SCUR) Page 1 of 2 Document No.: Issuing Authority: ! F-CAR-CS-033-Rev.00 Pace Quality Office Page 2 of 2 for Internal Use ONLY .��mpI6..iCopditi on Pon. Client Name: W® . 923/4316 eipProject t►: if�Il� II III IIIII II I III Courier: ❑Fed Ex Flups ❑USPS ❑Client ❑ Commercial ❑Pace ❑Other: � 82314316 Custody Seal Present? Dyes ❑No/ Seals Intact? ©Yes ❑No G �, �^ J Date/Initials Person Examining Contents: ` r :2i •�, Packing Material: []Bubble Wrap [�Buhble Bags ❑None []Other: Thermometer: i wet []Blue []None 0 a5 mples on ice, cooling process has begun 11iR Gun ID: 1505 _ _ Type of Ice: Correction Factor: Cooler Temp Corrected (•C): "l•A Biological Tissue Frozen? ❑Yes [-]No QN/A Temp should be above free 'ng'to 6'C USDA Regulated Sall ( N/A, water sample) Did samples iginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internatipnaliy, nywc U n includine Hawaii and Puerto Rico)? MYes 11rf Comments/Discrepant : Chain of Custody Present? 0.4 ONO ❑N/A I. Samples Arrived within Hold Time? QYes ONO [-]N/A 2. Short Hold Time Analysis 1<72 hr.)? ❑Yes IDN ❑N/A 3. Rush Turn Around Time Requested? ❑Yes • No ❑N/A 4. Sufficient Volume? ❑YYees Nio ❑NIA 5. .a, ) Correct Containers Used? ©Yes ONO ❑N/A 6. -Pace Containers Used? Yes ON, ❑N/A Containers Intact? © es (:IN. ❑NIA 7. Samples Field Filtered? ❑Yews ONO INN/A B. Note if sediment is visible in the dissolved container Sample Labels Match COC? [3fes ❑No ❑N/A 9. t -Includes Date/Time/ID/Analysis Matrix: All containers needing acid/base preservation have been / 10 checked and documented on page twoof SCURF? ❑.yrs ❑No ❑N/A , Exceptions: VOA, Coliform, TOC COHdd Grease DRO/8015 (water) DOC, LLHg Samples checked for dechlorination? ❑Yes ❑No J2 N A 11. Heads ace in VOA Vials (>5-6mm)? DY6 ONO ❑N/A 12. Trip Blank Present? [--]Yes ONO QN/A 13. Trip Blank Custody Seals Present? ❑Yes ❑No gNIX� Pace Trip_Blank Lot q ifpurchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: _ Date/Time: Comments/Sample Discrepancy: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: Lj1f��'ry Date: Project Manager SRF Review: NWw Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Page 11 of 12 ,_Face Analytical CHAIN -OF -CUSTODY t Analytical Request Document N The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accclratety. O N Section A Section B Section C `c Page: of Q Required Clwnl InlorTTlation Required Pm 1 infdrmatron. Invoice Information Company: Mid-Atlantc Associates. Inc. Report To'. Chuck Hoffman (choffman@maaonline.com) Attention Chuck Hoffman Address: 409 Rogers View Court copy To: Ron Davis (rdavis@niaaonline.com Company Name, Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 Address. 409 Rogers View Court. Raleigh, NC NPDES I GROUND WATER t- DRINKING WATER i LIST f RCRA r OTHER Email To choffmart@maaonline,com Purchase Order No.: R2037.00 Pace o�1e -- Reletenee; Phone 919-250-9918 Fax 919.250-9950 Project name. G&N Used Auto Parts Pace Project Nicole Gasiorowski Site location Mmwger. STATE. NC Requested Due QaterTAT: Standard Project Numtter. R2037.00 Pace Profile d Requested Analysis Filtered (YIN) Section D Valid Matrl>, Codes c^ a r z Required Grcm InromAnlien UATRIX CODE COLLECTED Preservatives } N Y N Y DRINA.'NG WAtER OW WATER WT WASTE WATER WIN 'n U Lo1.1POSIlE COMPOTE 0 Z PRODUCT P t9 sTART ENMRAB 1 SOILISOLIO SL on. oL O O rq CD j 0 dI SAMPLE ID WPE WT, ... �; I, �, tou ; o aR AR fA-2.0.91,-) GTHER oT p �' >- a to ? m F- p a m C G Sample IDs MUST BE t1NI0UE TISSUE IS p asy < tD m t_ (j �p V U X F- J 1- J Z lu N O O U) = ill df C O ¢ O c C5 1 U O C v d7 Q t � a O DATE TIME DATE. TIME a � 2IC5 = = Z Z $ O .,� 0(L d w !Y Pace Project No.! Lab I.D. t Otrtfall No. 1 vVT c } {�• .,. 7 4 1 2 1 1 x x x X1 I I I I Rainfall inches 2 H: 3 4 s 6 7 8 9 10 11 12 ADDITIONAL COMMENTS AlcLINQUISHED BY I AFFILIATION DATE TI/MEN BY f AFFILIATION DATE SAMPLE CONDITIONS -�(ACCEPTED rTI�M}Er� SAMPLER NAME AND SIGNATURE w q n PRINT Name of SAMPLER: r •`C/rC"S E o ~ V m - o gm @ T j ^1 DATE Signed - SIGNATUREoTSAMPLER: pl -� /AC2 (MMIODlYYJ• - tsiu CA •Imponnnl Note: By %igning Ih,s farm you are acccOng Pace's NET 30 day payment In— and agm—g to We charges of 1.5% per molnh In( any rnvolCcS not pond w!hn 30 days. F-ALL-0-020rev.08, 12.Oct-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR:2016 FACILITY NAME G&N Used Auto Parts COUNTY Nash PERSON COLLECTING SAMPLE(S) George Vagnieres _ PHONE NO. 252) 977-3710 CERTIFIED LABORATORY(S) Pace Analytical Lab #12 RECEIVED Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 NOV 09 2016 Part A: Stormwater Benchmarks and Monitoring Results CENTRAL FILES DWR SECTION For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TS5), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50Z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 9/29/2016 2.5 7.7 <3.8 <5.0 <5.0 <0.005 NA �l1 r11}� j�1�!jM1 yg� U LF� i�•W� � ► E] M U. R Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier i &o Tier:2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is im plementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) 101.-i ,61n — Title (Print title) R 17- ol?016 Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge a nd belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designees (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 Mid Atlantic Engineering & Environmental Solutions February 1, 2016 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919,250.9918 facsimile 919.2S0.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on December 8, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report T M �z rn 0 U) r rn z a M EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR:2015 FACILITY NAME G&N Used Auto Parts PERSON COLLECTING SAMPLE(S) George Vagnieres CERTIFIED LABORATORY(S)Pace Analytical _ Lab #12 Lab # Part A: Stormwater Benchmarks and Monitoring Results (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COU NTYNash PHONE NO. 252) 977-3710 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/50z 1s 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 12/08/2015 2.0 8.2 8.2 <5.0 <5.0 < 0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent - management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) &f-og�� Title (P int title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Design (Date) Form SWU-251, lost revised October25, 2012 Page 2 of 2 aceAnalytrcal www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 22, 2015 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: G&N Used Auto Parts Pace Project No.: 92278991 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on December 09, 2015, The results relate only to the samples included in this report. Results reported herein conform to the most current TNl standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. pCCR�r0 TNi gQoR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 • aceAnalytical www.pecalabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: G&N Used Auto Parts Pace Project No.: 92278991 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification M C-49-06 Kansas Certification #:E-10177 Kentucky UST Certification M 0042 Kentucky WW Certification #:98019 Louisiana Certification #: 04076 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification' #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #; E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 � �] �:klil�I•l8liE-y Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2014-148 Texas Certification M T104704355-15-9 West Virginia Certification #: 330 Wisconsin Certification M 999788130 USDA Soil Permit #: P330-10-00128 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #; 40 South Carolina Certification #: 99030001 West Virginia Certification M 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 aceAnalytical® www.yacelabs.00m Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: G&N Used Auto Parts 92278991 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92278991001 OUTFALL NO. 1 EPA 1664E JMS t PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASH EPA6010 CDF 1 PASI-A SM 2540D MJP 1 PASI-A' REPORT OF LABORATORY ANALYSIS This report shaft not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAnalyilcal. wwwpacslabsmn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: G&N Used Auto Parts Pace Project No.: 92278991 Sample: OUTFALL NO. 1 Lab ID: 92278991001 Collected: 12/08/15 09:25 Received: 12/09/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 11664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 12/16/15 06:17 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 12/14/15 10:47 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND uglL 5.0 1 12/11/15 20:00 12/14/15 16:56 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.2 mglL 5.2 1 12/10/15 10:13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 acepnalytrcal www.paWabs.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92278991 QC Batch: GCSV123560 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Associated Lab Samples: 92278991001 METHOD BLANK: 1629953 Matrix: Water Associated Lab Samples: 92278991001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L NO 5.0 12/16/15 05:56 LABORATORY CONTROL SAMPLE: 1629954 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 20 16.3 82 64-132 MATRIX SPIKE SAMPLE: 1629955 92278676001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L NO 20 14.7 73 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc- Page 5 of 12 aceanalyticals ' wwlw.paolabs-com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92278991 QC Batch: GCSV117829 Analysis Method: EPA 8015AIcohol-Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92278991001 METHOD BLANK: 1444505 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L ND 5.0 12/14/15 10:19 LABORATORY CONTROL SAMPLE: 1444506 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg1L 25 26.5 106 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1444507 1444508 MS MSD 92278991001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L ND 25 25 23.9 28.0 95 112 67-133 16 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 t1 ace Analytical wwwpacewmoom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92278991 QC Batch: MPRP120257 Analysis Method: EPA6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92278991001 METHOD BLANK: 1627193 Matrix: Water Associated Lab Samples: 92278991001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead uglL ND 5.0 1211411516:12 LABORATORY CONTROL SAMPLE: 1627194 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead uglL 500 470 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1627195 1627196 MS MSD 92279212003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Lead uglL ND 500 500 481 434 96 86 75-125 10 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical® wwwpacefabs.mr; Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92278991 QC Batch: WET141880 Analysis Method: SM 2540D QC Batch Method: SM 25400 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92278991001 METHOD BLANK: 1624921 Associated Lab Samples: 92278991001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1624922 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/10/15 10:07 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 244 98 90-110 SAMPLE DUPLICATE: 1624923 92279154021 Dup Parameter Units Result Result Total Suspended Solids mglL ND ND SAMPLE DUPLICATE: 1624924 92278946005 Dup Parameter Units Result Result Total Suspended Solids mglL ND ND RPD Qualifiers RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalXical" " www.paoefabs.tan Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: G&N Used Auto Parts Pace Project No.: 92278991 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitalion Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chioroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. , Pace Analytical is TNI accredited Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, inc.. Page 9 of 12 acetinalytical" W*WPacalab&C= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N Used Auto Parts Pace Project No.: 92278991 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92278991001 OUTFALL NO. 1 EPA 1664E GCSV123560 92278991001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol GCSVJ17829 92278991001 OUTFALL NO. 1 EPA 3010A MPRPI20257 EPA 6010 ICP118280 92278991001 OUTFALL NO. 1 SM 2540D WET141880 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/22/2015 11:37 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 i ace/lnalytrcal' _ uocument ivame: Sample Condition Upon Rece1 Document Number: F-C H R-C S-003-rev.16.1 uocument mevisea: Novemoer, l , Lu i o Page 1 of 2* Issuing Authority: Pace Huntersviile Quality Office Client Name. c� I� '_i Page 2 of 2 is for Internal Use Only Courier: ❑ Fed E)❑ UPC] USP❑ Clier❑ CommerciC Pace Other Q tional " a CustodySeal on Cooler/Box Present: ❑ yes ' Jo. Prod .Dtae Date ❑ no Seals intact: El yes ❑ no Narrie;:.; ;.: Packing Material: ❑ Bubble Wrap ❑ B' ubbie Bags ❑ None ❑ Other Thermometer Used: I Gun T1505 Type of Ice: t Blue None ❑-Same es on ice, cooling process has begun Temp Correction Factor No Correction Date and initials of person examining Corrected Cooler Temp.: -C Biological Tissue Is Frozen: Yes No WA contents: AP / • f Temp should be above freezing to 6°C _ Comments: i Chain of Custody Present: ❑Yes ❑No ❑NIA 1. Chain of Custody Filled Out: 1-1 ❑Yes ❑No ❑NIA 2. Chain of Custody Relinquished: Yeses❑No ❑NIA ISampler Name & Signature on COC: Oyes ❑No ❑N/A 4, Samples Arrived within Hold Time: ❑Ye ❑No ❑NIA 5, Short Hold Time Analysis <72hr : Dyes ©No ❑NIA 6. Rush Turn Around Time Requested: Dyes ❑No ❑NIA 7, Sufficient Volume: Dyes ❑No ❑NIA $. Correct Containers Used: ❑Y e/ONo 0N1A g, — , C jl �� r�; i f f(CG ✓ ::I -Pace Containers Used: ❑4ea No ❑NIA Containers Intact: Yes ❑No ❑NIA Filtered volume received for Dissolved tests ❑Yes`❑No ❑NIA 11. Sample Labels match COC: ❑i Yes ❑No ❑NIA 12. -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. / DYes ❑No ❑NIA 13. All containers needing preservation are found to be in ❑Ye E!No ❑NIA compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI-DRO (water), EIYes •]No Samples checked for dechlorination: ❑Yes ❑No ❑N1A 14. Headspace in VOA Vials >6mm : ❑Yes ❑No NIA 15. Trip Blank Present: ❑Yes ❑No ON A 16, Trip Blank Custody Seals Present ❑Yes ❑No ❑NIA di lent. Notification/ Resolution: Field Data Required? Y I N Person Contacted: C L jA Cjl F)7a lfV(a lDatefTime: IZ,-q..i 2�- Comments/Resolution: Aimp L- w. v i ea e ve e" tZ)L ,r 14 CfWWU "G )t- tug\� V6\XX ant 6CI cnkr� �.nrr�t�rcr.rd� r�:ra1S 4nra tl151S SCURF Review: IV V V" Date: (L- `i -fi plora InK. l "--- SRF Review: -1 Date: . (i — S IAA®# : 92278991 Note: Whenever there Isa discrepancy affecting North Carolina compliance �� ��' �I �I���■� �� �`■ samples, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers) 92278991 Page-ttof 12 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR:2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME G&N Used Auto Parts COUNTYNash PERSON COLLECTING SAMPLES) George Vagnieres PHONE NO. (252) 977-3710 CERTIFIED LAB 0RATORY(S)Pace Analytical _Lab #12 `'5FU Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE r'21�3 Part A: Stormwater Benchmarks and Monitoring Results ry�a For sampling periods with no discharge, you must submit this discharge monitoring farm noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics, mg/L Benchmark - - 6.0 — 9.01 100/502 i5 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 2-3 7.8 19.2 <5.0 <10.0 0.0051 ND Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122 Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) pIn' Oeo Title (P int title) gallnz," nature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) (Date) Form SW U-251, last revised October 25, 2012 Page 2 of 2 M'od Atlantic Engineering & Environmental Solutions July 7, 2015 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NORTH CAROLINA 27803 NPDES PERMIT NO. NCG100199 To Whom It May Concern: REemva) JUL, 15 2015 CENTRAL FILES DWR SECTION 409 Rogers View Court Raleigh, NC 27610 office 919.2 50.99 18 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on June 4, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized an the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. ,rot Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE aceAnalytical www.Pacelabs.C= June 16, 2015 Chuck Hoffman Mid Atlantic Associates RE: Project: G&N USED AUTO PARTS Pace Project No.: 92253072 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on June 05, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 lacieAnalyfical" www. pacelabs.com Project: G&N USED AUTO PARTS Pace Project No.: 92253072 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #:E-101771 E-10247 Kentucky UST Certification #: 0042 Kentucky WW Certification #:98019 Louisiana/NELAP Certification #: 04076 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #; 5342 North Carolina wastewater Certification #: 12 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2014-148 Pennsylvania Certification #: 68-05340 Texas Certification #: T1 04704 355-15-8 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-10-00128 FloridalNELAP Certification #; E87627 Kentucky UST Certification #: 84 West Virginia Certification #; 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnalyticals wwwpacelatrs.com SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 Project: Pace Project No.: G&N USED AUTO PARTS 92253072 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92253072001 OUTFALL NOA EPA 1664B CLW 1 PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASI-I EPA 6010 JMW i PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 (�IaceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704y875-9092 Project: GIN USED AUTO PARTS Pace Project No.: 92253072 Sample: OUTFALL NO.1 Lab ID: 92253072001 Collected: 06/04/15 11:30 Received: 06/05/15 10:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 06/15/15 08:45 801 SM Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 06111/15 18:28 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 5.3 ug1L 5.0 1 06/08/15 17:10 06109/15 20:49 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 12.0 mg1L 4.2 1 06111/15 14:50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 lacieAnalytical www.pacelobs.rum Project: G&N USED AUTO PARTS Pace Project No.: 92253072 QC Batch: GCSV/21643 QC Batch Method: EPA 1664B Associated Lab Samples: 92253072001 METHOD BLANK: 1484604 Associated Lab Samples: 92253072001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 1484605 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 06/15/15 08:44 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 20 17.9 90 64-132 MATRIX SPIKE SAMPLE; 1484606 92253927001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 17.9 87 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 aceAnalytical wwwpacelabs.com QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92253072 QC Batch: GCSVli 5669 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92253072001 METHOD BLANK: 1315435 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L ND 5.0 06/11/15 16:13 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1315436 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 22,9 92 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1315990 1315991 MS MSD 92252710002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 20.0 20.3 80 81 67-133 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 ace Analytical www.pacelabs.cnm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92253072 QC Batch: MPRP118643 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92253072001 METHOD BLANK: 1478701 Matrix: Water Associated Lab Samples: 92253072001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead uglL ND 5.0 06109/1519:54 LABORATORY CONTROL SAMPLE: 1478702 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Lead ug1L 500 477 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478703 1478704 MS MSD 92253110004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 477 516 95 103 75-125 8 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 laceAnalyfical" www.pacefabs.=n QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 HuntersviRe, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92253072 QC Batch: WET138051 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92253072001 METHOD BLANK: 1482385 Matrix: Water Associated Lab Samples: 92253072001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 06111/15 14747 LABORATORY CONTROL SAMPLE: 1482386 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 238 95 90-110 SAMPLE DUPLICATE: 1482387 92253050001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 10 22.0 75 D6 SAMPLE DUPLICATE: 1482388 92253245001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 06116/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 laceAnalytical www.pacelaes.com QUALIFIERS Project: G&N USED AUTO PARTS Pace Project No.: 92253072 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Get - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. �_1=ICI :L•� fa7:71 �� PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:24 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 laceAnalytical Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.WM (744)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N USED AUTO PARTS Pace Project No.: 92253072 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92253072001 OUTFALL NO.1 EPA 1664E GCSVl21643 92253072001 OUTFALLNO.1 EPA 8015 Alcohol -Glycol GCSVI15669 92253072001 OUTFALL NO.1 EPA 3010 MPRP118643 EPA 6010 ICP116724 92253072001 OUTFALL NO.1 SM 2540D WET138051 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06I16I2015 06:24 PM without the written can sent of Pace Analytical Services, Inc.. Page 10 of 14 vvuuI IV( I IVdl lie: �cea�7lytrr�r' Sample Condition Upon Recei Document Number: F-CHR-CS-003-rev.16 Client Name: Al.� Courier: Le x UPS❑ USPS❑ client[ --]Custody ooterlBox Present: ❑ yes/2 Packing Material: ❑ Bubble Bubb e Thermometer Used: [R I�fi T1401T\ Temp Correction Factory T14 1 No Correction UVUU31 ICI I I\CYIOVU. IVIGY IV, Page 1 of 2* Issuing Authority: Pace Huntersville Quality Office ' Page 2 of 2 is for Internal Use Only dommercial❑ Pace Other Q'° p� �r f —tj a�J' f. ,raja � �� n� Seals Intact: ❑ yes ❑ no rnr�:,.,i tt3 t a �icNSher o�-'�Wetiue None Samples on ice, cooling p cess has begun �' •C Biological Tissue is Frozen: Yes No Nr Date and Initi of perspri. examining Corrected Cooler Terri �" contents: Temp should be above freezing to 6°C Comments: Chain of Custody Present: Yes 11 No ONIA 1. Chain of Custody Filled Out: Yes ©No ❑NIA 2. Chain of Custody Relinquished: Yes ONO DNA 3. Sampler Name & Signature on COC: Y 6 ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 5. Short Hold Time Analysis <72hr : ❑Yes No ❑NIA 6, Rush Turn Around Time Requested: Oyes No ❑NIA 7. Sufficient Volume: ❑Yes No ❑NIA 8. 112414 Correct Containers Used: s ONO ONIA 9. -Pace Containers Used: Y s ONO ❑NIA Containers Intact: Yes ONO ONIA ,10. Filtered volume received for Dissolved tests ❑Y C ON, NIA 11. Sample Labels match COC: Yes ONO ONIA 12. -Includes date/timellD/Anal sis Matrix: All containers needing preservation have been checked. Yes No ©N/A 13, All containers needing preservation are found to be in Y s PNo ❑NIA compliance with EPA recommendation. exceptions: VOA, coliforrn, TOC, O&G, VN•0R0 (water] Yes ONO Samples checked for dechlorination: OYZ ONO ONIA 14. Heads ace in VOA Vials >6mm : Yes ❑No ❑NIA {{ 15. Trip Blank Present: OYes ❑No Nr 16. Trip Blank Custody Seals Present Oyes ONO IANIA Pace -Trip-Blank Lot # if urchased : _ __...w._ W_---- ----____-- .•-_--... ..___.__-__-- - _ •- _ ----.__._ _--- _..__ .---_-__-.-- Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Datefi'ime: Comments/ Resolution: SCURF Review: IMU Date: -5- °1^" SRF Review: Date: T5 W® : 92G53®72 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( I.e out of hold, incorrect preservative, out of temp, I Incorrect containers) 92253072 Page 11 of 14 Ir aceAnalytical ' � wrn. wcnuos ccm CHAIN -OF -CUSTODY 1 Analytical Request Document o The Chain -&-Custody is a LEGAL DOCUMENT. All re evant fields must be completed accurately. N Section A Section B Section C Page: of Required Client Information; Required Pmjm information: Irmam InfoarkVion: Oompany: Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (Choffman@maaonline.Com) Attention: Chuck Hoffman Address: 409 Rogers View Court Copy TO[ Joanna Crow 0crow a@maaonline.com) Comparty Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 Address' 409 Rogers View Court, Raleigh, NC i NPDES r- GROUND WATER i DRINKING WATER usT l— RCRA 7 OTHER Email To: choffman@maaonline.eom Purenase oraer No.: R2037.00 Pate °UIX0 -- Refereme: Pr>«re: 919-250-9918 Fax 919-250-4950 Proiea Name: GBrN Used Auto Parts Pie Prahoa Nicole Gasiorowski Sire Location M�e'er STATE: INC Requested Due Date/TAT: Stanaam ProiW Numter. R2037.G0 Pace Profile r, _ 'J j l (� E Requested Analysis Filtered (YIN) _ dM Section D Valid Matrix Codes n a z f"bvd Chat infomLalion MAMhx CODE e M COLLECTED Preservatives 'r N Y N 'Y D"MNG WATER ow WATER wr g 1 o m WASTE WATER vwAr a cow o=TE cpwos U 1] MODUCT P m siAAT EMYGAAB R Z 50r -os� w ok AP SAMPLE ID ? w W v to y _ 2, (A-0-91.•) to 4 z F o(D 7+ it O � I OTHER OT Sample Sple r6s MUST BE UNIQUE nssuE is p U y2y F z d O L JG V iR J W CO.t d = O P m 03 m r- a a a a 0 O v7 s `m c co a 13 y y DATE TIME DATE TIME in _ = x z z 2 O F Pace Project NoJ Lab I.D. 1 Outfali No. 1 wT G - 7 4 1 1 2 1 x x X1 x I Rainfall inches : �J i6iC Z H: f 3 4 - 5 6 7 8 9 ' 10 11 12 ADDITIONAL COMMENTS - RELINQUISHED BY f AFF[UAT10N DATE TIME C BY ! N _ DATE TIME ' SAMPLE CONDITIONS Ua SAMPLER NAME AND SIGNATURE ct 5 w Z c .. PRINT Namc of SAMPLER: 2 u El�cEx' p, 8 � F z SIGNATURE olSAMPLER: No DATE Slgncd •r _ = g E DN (MMMY): c>, m -impe 4M Note: By signing this form you am accepting Pace i NEET 30 nay payment terms and agmeing to Ike changes of 1.5% par month for arty invoices not paid .Min 30 bays. F-ALL-0-020rev.08, 12-OQ-2007 uvI;UIIIVIII 114allie. VUUU1IIcIrl ncalacu. rviay iv, 4.., aceAlk�iyfical' Sample Condition U on Recei t SCUR Page 1 of 2* Document Number: Issuing Authority: r F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: c JI r- Courier: ed Ex UPS❑ LISPS❑ Client❑ Custody est o oolerlBox Present, ❑ yes Packing Material: ❑ Bubble p--BBubb_e Thermometer Used: IF Gfi T1407 Temn Correction Factor -T14 1 No Correction ' Page 2 of 2 is for Internal Use Only ommercialEl Pace Other10°�,,;�sY Seals intact: ❑ yes ❑ nojf�4u U;�+ �No ee- Other Poo If c Wet lue None Samples on ice, cooling p cess has begun Corrected Cooler Tern p•:�' •C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No NI Comments: Date and Initl of pers9n examining cantenis• Ch aih - 'oi'Cu . stbdy Present: es 13 No ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NrA 2. Chain of Custody Relinquished: Yes ❑No ❑NIA 3. Sampler Name & Signature on COC: r 6 ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ON?,, ❑NIA 5. Short Hold Time Analysis <72hr): Oyes No ❑NIA 6. Rush Turn Around Time Requested: ❑Yes No ❑NIA 7. Sufficient Volume: ❑Yes AO ©NIA B. Correct Containers Used: -Pace Containers Used: s ❑No ts ❑No ❑NIA ❑MIA 9. Containers Intact: Yes ONO ❑NIA 10. Filtered volume received for Dissolved tests ❑Y� ❑No L2NIA 11. Sample Labels match COC: -Inctudes date/tlmeliDlAnal sis Matrix: Yes ❑No ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, coliform, TOO, 0&G, Nft•DRO (water) Yes No Y s PNa Yes ❑No ❑NIA ❑NrA 13. Sam les checked for dechlorination: ❑Ye ©No JdNIA 14. Heads ace in VOA Vials >6mm -. Yes ONO ❑NIA t 15. - pa— 7 ` & al Trip Blank Present: Trip Blank Custody Seals Present PaceTri -Blank-Lot # if purchased):-,- ___ __.------.--___- ❑Yes ONO ❑Yes ONO •--- -- ._- NI NIA _-. _ 16. ..__ . -.... _. _ . _ -._.. _ . _ _ -. _ -- -- _-_.- _--- - .-- _-. ----_.__-- Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: DatelTime: Comments/ Resolution: SCURF Review: Date: SRF Review: Date: 5''t`� "---'-" -' • Wad : 92253072 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR �■ ��� ��� Certification Office (I.e out of hold, incorrect preservative, out of temp, incorrect containers) 92253072 Page 13 of 14 CHAIN -OF -CUSTODY 1 Analytical Request Document o aeeAnalyt/ealThe Chain-ot Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Nr � w.r.� prceuos r 0) Section A Section B Section G page: of Required Client information: Requirem d Proiorl Irnorati= Invoice WorTnabon: compent, Mid -Atlantic Associates, Inc. ROPOrt To: Chuck Hoffman (choffman@maaonline.Gom) Attend= Chuck Hoffman Address: 409 Rogers Mew Court COPY To- Joanna Crow (crow@maaonline.com) COmP" Nye: Mid -Atlantic Associates, inc. REGULATORY.AGENCY Raleigh, NC 27610 Address. 409 Rogers View Court, Raleigh, NC f— NPDES 1— GROUND WATER i DRINKING WATER l— UST i— RCRA OTHER Email To: olToffman@maaonline.com Purrttase Order No.: R2037.00 Paea GLwa — Reference: Prone: 919-250-9918 Far 91 g•250 9950 Preied Nye: G&N Used Auto Parts Pa" "I'll Nicole Gasiorowski Site location i,tarraeer. STATE: NC Requested Due DateriAT: seaneare Praied Number. R2037,00 Pace Pr Ile a-,_ r j t Requested Analysis Filtered (YIN) - Section D Valid Matrix Codes o ii x Required cries info =Uon MATRI coop COLLECTED Preservatives 'r N Y N ' Y oqW NG—T" aW 0 x WATER WT o 2 WASTE WAT(A WW V co.P=TE WrppgTE .D vaooueT P START ENDIGRAB W 2 z sOsLmouo U. SAMPLE ID �_ Cr m 6 _ (A Z D 9 r ,-) orkEq oT AR p a Z 13 o ?• fY Sample IDS MUST BE UNIQUE TmsUE TS O uw il ti a 0 () m V' f 2 ✓ ie X J O c3 = ea m rr 0 �' Nz C> ri r d v 4 4 DATE TIME DATE TIME 7 2 2 S Z Z O Ltl a Pace Project NoJ Lab I.D. 1 Outfall No_ 1 wT G — 7 4 1 2 1 1 x xj xj x I I I I I I Rainfall (inches): e iGx 2 H: I.f 3 .. 4 s 6 7 8 9 10 11 12- ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME - G 6Y1 N DATE TIME SAMPLE CONDITIONS -IS f 3D c4 d: Cra Ad SAMPLER NAME AND SK;NATURE a _ m_ z 4 e PRINT Nance of SAMPLER: u z L ~ —g u y DATE Signed SIGNATURE of SAMPLER r �% — ` �� _ (MILWDMIf) U _ V -Impoearu NOW By signing this form you am arrerIV Pite's NET 30 day ptYMM lams and Sgrwmg to Isla tnasyes of t.S% Par month tar My ift o not paid within 30 nays. F-ALL-0.020rev.08, 12.Oct-2007 M*9d Atlantic Engineering & Environmental Solutions December 15, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED DEC 19 2014 CENTRAL FILES DWR SECTION Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA PERMIT NCGIO0199 MID -ATLANTIC JOB NO. 00OR2037.00 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on November 25, 2014 and analyzed for pH, total suspended solids (TSS), total recoverable lead, ethylene glycol and oil and grease. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. el.. I.., Charles B. Hoffman, P.G. Project Geologist Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME G&N Used Auto Parts COUNTY Nash PERSON COLLECTING SAMPLE(S) George Va nieres PHONE NO. (252) 977-3710 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 11/25/14 2-3 7.8 19.2 <5.0 <10.0 0.0051 ND Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / -9 1711V (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 aceAnalytical wwwpacefahs, cram r December 08, 2014 Darin McClure Mid Atlantic Associates, Inc. RE: Project: G&.N Used Auto Parts Pace Project No.: 92227328 Dear Darin McClure: Pace Analytical Services, Inc. 9800 I(incey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 26, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. pccft A TNI cgeo �� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytical www.pacelabs.com r Project: G&N Used Auto Parts Pace Project No.: 92227328 Indiana Certification IDS 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification iDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 FloddalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Kentucky UST Certification #: 0042 Louisiana/NELAP Certification #: 04076 Ohio VAP Certification #: CL-0065 West Virginia Certification #: 330 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Inc.. Page 2 of 12 aceA'nalytical wwwpacelaes.cw SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: Pace Project No.: G&N Used Auto Parts 92227328 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92227328001 Outfall No. 1 EPA 1664B Cl_W 1 PASI-C EPA 8015 Alcohol -Glycol TMW' 1 PASI-I EPA 6010 JMW 1 PASI-A SM 2540D TEP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAna1ytrca1 wwwpacelabs.cem r ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N Used Auto Parts Pace Project No.: 92227328 Sample: Outfall No, 1 Lab ID: 92227328001 Collected: 11/25/14 10:30 Received: 11126114 10:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 12/03/14 08:54 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 1.0 1 12/06/14 00:18 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 5.1 uglL 5.0 1 12/01/1416:10 12/02/1403:31 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.2 mg1L 4.2 1 12/02/14 06:14 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 ;ac le A na lXical wwwpacefabscorn i i QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92227328 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilfe, NC 28078 (704)875-9092 QC Batch: GCSVl19661 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92227328001 METHOD BLANK: 1341673 Matrix: Water Associated Lab Samples: 92227328001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mglL ND 5.0 12/03/14 08:42 LABORATORY CONTROL SAMPLE: 1341674 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 20 17.5 87 64-132 MATRIX SPIKE SAMPLE: 1341675 35165582001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L <5.0 20 16.6 81 64-132 Results presented on this page are In the units indicated by the "Units- column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 _ aceAnalytical www.pacelahs.crom 1 i QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92227328 QC Batch: GCSW13604 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92227328001 METHOD BLANK: 1198159 Associated Lab Samples: Parameter Units Ethylene glycol mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 12/02/14 19:58 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersvitie, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1198160 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 23.3 93 49-139 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1198161 1198162 MS MSD 50107942002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 18.8 22.8 75 91 49-139 19 Results presented on this page are In the units indicated by the "units" column except where an alternate unit Is presented to the Fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical ' WWpacelabs.com i Project: G&N Used Auto Parts Pace Project No.: 92227328 QC Batch: MPRP117442 QC Batch Method: EPA 3010 Associated Lab Samples: 92227328001 METHOD BLANK: 1340540 Associated Lab Samples: 92227328001 Parameter Units ug1L Lead QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/02/14 02:03 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1340541 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead uglL 500 493 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1340542 1340543 MS MSD 92227372001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Lead uglL ND 500 500 468 475 94 95 75-125 1 Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the resulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc - Page 7 of 12 ;ac,Analytical wwwpacefabs.com t QUALITY CONTROL DATA Project: G&N Used Auto Parts Pace Project No.: 92227328 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704)875-9092 QC Batch: WET134532 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92227328001 METHOD BLANK: 1340812 Matrix: Water Associated Lab Samples: 92227328001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/02/14 14:39 LABORATORY CONTROL SAMPLE: 1340813 Spike LCS I.CS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 244 98 90-110 SAMPLE DUPLICATE: 1340814 92227193001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 71.3 75.3 5 SAMPLE DUPLICATE: 1340815 92227360002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 693 723 4 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 /5a'ce Analytical www.pacelahs. c= QUALIFIERS Project: G&N Used Auto Parts Pace Project No.: 92227328 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosod1phenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2014 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 ;ac e A na ly tica i" wwwpecelabs.cw QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: G&N Used Auto Parts Pace Project No.: 92227328 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92227328001 Outfall No. 1 EPA 1664B GCSV119661 92227328001 Outfall No. 1 EPA 8015 Alcohol -Glycol GCSV113604 92227328001 Outfall No. 1 EPA3010 MPRP117442 EPA6010 92227328001 Outfall No. 1 SM 2540D WET134532 Date: 1210812014 W40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP115720 Page 10 of 12 4 Uocument Name'. ., aeeArk�lytica!' Sample Condition Upon Receipt SCUR Document Number: F-CHR-CS-003-rev.15 Client Name:_ (Vt,tu A-J- "It l._Lf uocUfnerlk McVISeU. 0UIJLt:111 a1 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Courier -'O-Fed Bx ❑ UPS❑ USPS❑ Cilent❑ Commerclal❑ Pace Other Custody Seal on Cooler/Box Present: ❑ yesd Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble V❑p ❑ Bubl; i6ags ❑ None ❑ . Other Thermometer Used: IR Gun 11 Type of Ice: � Vet- glue done . ❑Samples on Ice, cooling process has begun Temp Correction Factor T1401 No Correction i. Corrected Cooler Temp.: J • -C Temp should be above freezing to 6°C Biological Tissue Is Frozen: Yes No NIA Date and Initl Is of person examining g contents:, _t IA, Comments: Chain of Custody Present: ❑No ❑NIA 1, Chain of Custody Filled Out: ___Oyes ❑No DNIA 2. Chain of Custody Relinquished: 0"Y"es 11 No ❑NIA 3, Sampler Name & Signature on COG: _--©Yes ❑No ❑NIAK Sam les Arrived within Hold Time: E1Yris ONO ❑NrA 5, Short Hold Time Anal sls (<721hr : ❑Yes,©No` ❑NIA 6. Rush Turn Around Time Requested: ❑Yes ,12No ❑NIA 7. Sufficient Volume: ; ONO ❑NIA 8. Correct Containers Used: -Pace Containers Used: ,-CI❑No Yes ❑No LINIA ❑NIA 9. Containers Intact: -EI—Yes [IN. ©NIA 10, Filtered volume received for Dissolved tests ❑Yes ❑ NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: Yes ❑No ❑NIA 12. All containers needing pfeservallon have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, coliform, TOC, 0&G, W-DRO (water) Yes ❑No p(es ❑No Yes ❑No 11 NIA ❑NIA 13. Samples checked for dechlorination: ©Yes ONO hurl '14. Heads ace in VOA Vials >6mm : YCs ❑No ❑NIA i5. . Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): ❑Yes ❑No ❑Yes ❑No PNIK ❑Nr 16, Client Notification! Resolution: Field data Required? Y 1 N Person Contacted: Daterrime: Comments/ Resolution: SCURF Review: +'U Dale: Zj� 92AA73na SRF Review: �_t Date: 0..k_ WO# • 2 28 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, 922Z732i3 Incorrect containers) Page 11 of 12 _ ZAnalXical` `..+w yINW a5.eel+ CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. AQ relevant Gelds must be completed a', tely, Section A Section 0 Section C Page: at EL Required Client rmtro Irdoarc Required Project Information: Invoice Information: Company: Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman@maaonline.com) Attention: Chuck Hoffman Address: 409 Rogers View Court Copy To: Joanna Crow Qcrow@maaonline.com) Company Name: Mid -Atlantic Associates, Inc. REGULATORY AGENCY Raleigh, NC 27610 Addrt:ss: 409 Rogers View Court, Raleigh, NC I— NPDES t— GROUND WATER i— DRINKING WATER r UST r RCRA r OTHER Email To: choffman@maaonline.eom Purchase order No.: R2037,00 Pace OL&e — Referenu: Phone: 919-250-9918 Fax 919-250-9950 Project Name; G&N Used Auto Parts Pace P"m Kevin Herring Site Location sAansger, NC Requested Due OiteITAT: Standard Project Number, R2037.00 Pau Pmrde C. -7 I !• 1 Requested Anatysis Filtered (YIN) Section D valid Matrix Codes Z E. z Required Client Inform w w,TRtx CODE COLLECTED Preservatives > N Y N Y dewn.q w.TEA OW 0 2 WATER WT r c7 O m WASTE wA7ED WW PRODUCT P Y to C�rIPpSrrE START camoosme ENpl�e V W a0 r Z_ souU3om 5L _ 7 N Ok a SAMPLED WME WP c7 0 " w •� <a p Q m = A,q AR w-7-"r.-) OTHER OT 0 w Q W — n m F— p U T 0 c G Sample Ips MUST BE UNIQUE TtSguE TS U } r Z G /` /�� !L R X a U ID 'jCF c5 c a !6 G p o`"1 X C rn Z Cl R w DATE TIME DATE TIME w c 2 Z T U 2 m Z t0 Z m 2 L O m CrCL Pace Project NoJ Lab I.D. 1 Outfall No. 1 WT G is 3o qLnj 7 1 4:i 1 21 1 1 x x I x I x s Rainfall (inches): 9_—/i L 2 H: , 3 a s B 7 s 9 10 11 12 ADOt110NAL COMMENTS RELINQUISHED liY! AFFILWTiON DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS f L SAMPLER NAME AND SIGNATURE ry c ? R PRINT Name of SAMPLER: �~ c G2�S//` s o. mz y m " E a m r SIGNATURE of SAMPL DATE signed �iF� 1 ! ~ $ W _. c> N 'imporard Note: By signing this farm you are accepting Pace'z NET 30 dry payment terms and agreeing 10 We charges Of 1.5% Per month for any invoices not paid within 30 days. F-ALL-0-020rev.08, 12-Oct-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100199 RECEIVESAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days APR 11 2014 from the date the facility receives the sampling results from the laboratory.) CENTRAL FILES FACILITY NAME G&N Used Auto Parts MAinir,.,., PERSON COLLECTING SAMPLE(S) George Vagnieres --...� CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Nash PHONE NO. (252) 977-3710 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), m /L g Non -polar O&G/TPH (Method lfifi4 SGT-HEM), rng/L Ethylene Glycol, mg/L Lead, Total Recoverable,, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/50Z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 03/19/14 2.0 - 3.0 8.1 4.0 <5.0 <10.0 <5.0 ND Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, lost revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." 62 � �� C / / 1, �- C Name (Print name) ��fc)eu I Title (P int title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ature of Permittee or Designee) vez� (Dat ) Form SWU-251, last revised October 25, 2012 Page 2 of 2 ace Analytical wYrw.pecefabs.com March 27, 2014 Darin McClure Mid Atlantic Associates, Inc. RE: Project: G&N USED AUTO PARTS Pace Project No.: 92194032 Dear Darin McClure: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report, Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Jon D Bradley jon.bradley@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. N-CCREO 2 TNI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytical www.pacelabs.com I Project: G&N USED AUTO PARTS Pace Project No.: 92194032 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Kentucky UST Certification #: 0042 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #; M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Louisiana/NELAP Certification #: 04076 Ohio VAP Certification * CL-0065 Pennsylvania Certification #: 68-04991 West Virginia Certification #: 330 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not W reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 WeAnalytical Nmw, pacetabs.com I SAMPLE ANALYTE COUNT Project G&N USED AUTO PARTS Pace Project No.: 92194032 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92194032001 OUTFALL NO. 1 EPA 1664B CLW 1 PASI-C EPA 8015-Alcohol-Glycol CEM 1 PASI-1 EPA6010 JMW 1 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 e WeAnalytical www.pacelahs.cam f ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92194032 Sample: OUTFALL NO. 1 Lab ID: 92194032001 Collected: 03/19/14 10:30 Received: 03/20/14 13:40 Matrix: Water . Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease ND mg1L 5.0 1 03/25/14 16:18 8015M Glycols In water Analytical Method: EPA 8015 - Alcohol -Glycol Ethylene glycol ND mg/L 10.0 1 03/26/14 10:04 107-21-1 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3010 Lead ND ug/L 5.0 1 03/22/14 10:05 03/24/14 18:01 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 4.0 mg1L 3.2 1 03/26/14 20:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/27/2014 11:44 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 acmnalytical www.pacelabs.o= QUALITY CONTROL DATA Project: G&N USED AUTO PARTS Pace Project No.: 92194032 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 2B078 (704)875-9092 QC Batch: GCSV117050 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92194032001 METHOD BLANK: 1164204 Matrix: Water Associated Lab Samples: 92194032001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 03/25/14 16:16 LABORATORY CONTROL SAMPLE: 1164205 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 38.4 96 78-114 MATRIX SPIKE SAMPLE: 1164206 92194238001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 35.9 87 78-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/27/2014 11:44 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 A acmnalytical wwwpacelabs.com I Project: G&N USED AUTO PARTS Pace Project No.: 92194032 QC Batch: GCSV112258 QC Batch Method: EPA 8015 - Alcohol -Glycol Associated Lab Samples: 92194032001 METHOD BLANK: 1066833 Associated Lab Samples: Parameter Units Ethylene glycol mg1L QUALITY CONTROL DATA Analysis Method: EPA 8015 - Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 10.0 03/24/1412:43 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2B078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1066834 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 250 259 104 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1066835 1066836 MS MSD 92194166009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 250 250 259 256 104 102 67-133 1 Date: 03/27/2014 11:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytrcal wwwpacefebs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92194032 QC Batch: MPRP115493 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92194032001 METHOD BLANK: 1162929 Associated Lab Samples: 92194032001 Parameter Units Lead ug1L LABORATORY CONTROL SAMPLE: 1162930 Parameter Units Lead ug1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 03/2411417:41 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 489 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1162931 1162932 MS MSD 92193929001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quai Lead ug1L ND 500 500 480 474 96 95 75-125 1 Date: 03/27/2014 11:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical www.pecela6s.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: G&N USED AUTO PARTS Pace Project No.: 92194032 QC Batch: WET130188 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92194032001 METHOD BLANK: 1165725 Matrix: Water Associated Lab Samples: 92194032001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 03/26/14 20:32 LABORATORY CONTROL SAMPLE: 1165726 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 228 91 80-120 SAMPLE DUPLICATE: 1165727 92193908001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND 5.8 SAMPLE DUPLICATE: 1165728 92193989001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 13.8 12.6 9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/27/2014 11:44 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 acmnalytical. wwwpace1ab3,com I QUALIFIERS Project: G&N USED AUTO PARTS Pace Project No.: 92194032 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/27/2014 11:44 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytrcal® www.pacefa6s.com I QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Project: Pace Project No.: G&N USED AUTO PARTS 92194032 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92194032001 OUTFALL NO. 1 EPA 16648 GCSV117050 92194032001 OUTFALL NO. 1 EPA 8015 - Alcohol -Glycol GCSV/12258 92194032001 OUTFALL NO. 1 EPA 3010 MPRP115493 EPA 6010 ICP114047 92194032001 OUTFALL NO. 1 SM 2540D WET130188 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/27/2014 11;44 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 Document Name: Document Revised: December 16, 2013 P�ceArlylrCa! Sample Condition Upon Receipt SCUR Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-03-rev.13 P ce luntersville Quality Office Client Name: (�c1�.IC11k_L (�15�c,14((_' 0��,� "t)tvr 13 Courier: ❑ Fed Ex ❑ b USPS❑ Client❑ Commercial❑ Pace Other Custody Seat on Cooler/Box Present: ❑ yes ❑��1 Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap ❑ Bubbl�gs ❑ None ❑ Other 0 .Clonal , Pro) Due Date_: Pro) ,Nal11e Thermometer Used: IR Gun T1102 �9�1 Type of Ice:r&:0 Blue None %E] Samples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T1301: No Correction Corrected Cooler Temp.: 1,6 -C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No NIA Comments: Date and Initials of person examtning contents5�.�-.•.i_ ��^►% Chain of Custody Present: _-0Yes ❑No ©NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NIA 2. Chain of Custody Relinquished' ___—Ules ❑ffoo—ETWK 3. - Sampler Name & Signature on COC: ClYes ❑No ❑NIA 4. Samples Arrived within Hold Time: _—EWes ❑No ❑NIA 5. Short Hold Time Analysis <72hr): ❑Yes ❑NIA 6. Rush Turn Around Time Requested: ayes o ©NIA 7. Sufficient Volume: _,F]Yes ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: Yes El No BYes bNo 11 NIA ❑NIA 9, Containers Intact: —E]Yes ❑No ❑NIA 10. Filtered volume received for Dissolved tests Dyes ❑No /A 11, Sample Labels match COC: -Includes date/time/10/Analysis Matrix: ❑Yes {'PK6� ❑NIA 12. 4(W c� All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coiiform, TOC, O&G, WI-0RO (water) C]Ye's ❑No /0�. ❑No %6Yes ❑No ❑NIA ❑NIA 13. Samples checked for dechlorinatiom []Yes ❑No Af�N/A 14, Headspace in VOA Vials (>6mm): ,,-BYes ❑No ❑NIA 1 Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased ❑Yes ❑No ❑Yes ❑No NIA QNK 16. Client Notification/ Resolution: Field data Required? Y I N Person Contacted: Datef ime: Comments/ Resolution: SCURF Review: V,12 Date: o SRF Review: 1 3� Date: Zo t Note. Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) I Page 11 of 12 ,' ;aceAnaVical- Section A Required Client Information CHAIN -OF -CUSTODY I Analytical Request Document The Chain-ot-Custady is a LEGAL DOCUMENT. All relevant rrelds must be completed accurately. Section B Section C Required Project Information: Invoice Information. Page: of COMpany: Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman(Mmaaonline.00m) Attention: Chuck Hoffman Address: 409 Rogers View Court copy TO: Joanna Crow acrow@maaonline.com) company Name: Mid -Atlantic Associates, inc. REGU[ATQRY'AGENCY' V . •t - Raleigh. NC 27610 Address: 409 Rogers Yew Court, Raleigh, NC r NPDE5 F GROUND WATER F- DRINKING WATERA r-- UST F- RCRA F OTHER Email To, ehoffman@maaonline.com Purchase Order No.: R2037.00 Pace Quote _ Reference: Phone: 919-250-9918 Fax: 919-250-9950 Project Name: G&N Used Auto Parts Pate Preled Kevin Herring Site Loiatioii Manager,..-. '_ ST;i ATE. NC Requested Qua DatefiAT: Standard Project Number R2037.00 Pace Prpfile s, q Z{ Requested'Analysis FiIt&6d-;(YIN)-1 •; Section D Valid Matrix Codes E.`Z J, Required Client Information MATRIX J CODE - COLLECTED Preservatives N Y N Y =NKNG wATER DVY a O U Z O s Q7 WATER WT WASTEWATER yyw P' U COMPOSITE COMPOSITE f- PRODUCT P = 4 START EN6CRA8 W Co Z SO-USOLC Si ID �E `° LIL SAMPLE to-7- 0-9 r.-a OTHER OT w Lu 0. w z a: r O o ,0 '< Sample IDS MUST BE UNIQUE TISSUE TS O U < co r�J nt X tit � tJ Q U d N 2 O O G m AT N Q7 C Q7 O LL m a O5 O �51q pt0" a Q o z 'a< s m d lt-n DATE TIME DATE TIME n _ = = Z 4 �' r W Pace Project Ne.! La I.D. 1 Outfall No. 1 WT G- - � IC' S!1 7 4 1 1 2 x x x x I I Rainfall InCl1e5 :z- 2 1° H: 3 Sa fi. z 7' 3J 8s� 9 q <� :12 AD6tTI6NAt56 -' MENTS ;}- RELINQUISHED BY I AFFIE66661i r',= f DATE ` _ STiME = _ t' _ ACCEPTED 9Y f AFFI[:IATION x�Yl-t�ft,l -_ -DA TIME 4 SAMPLE CONDITIONS i f��Zc`5 3 /0 sC �.E — l 2�ij`� r 3'' `r' 7 ej 'v SAMPLER NAMEA7. N� SIGNATURE`S `3'a_ - •. -OIlCW PRINT Name of SAMPLER- m CD _ o r a =' ,e g S ~ m SIGNATURE of SAMPLER: // DASlgnatl r I N J (MMfTEOD1YYj: U y -Important Note: By signing this to" you are accepting Pace's NET 30 clay payment terms and agree,rq to lam charges of 1.5% per month Far any invoices not paid within 3C daya. F-ALL-0-020rev.08, 12.00I-2007 Mid Atlantic Engineering & Environmental Solutions April 8, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS G&N USED AUTO PARTS 3850 SOUTH CHURCH STREET ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA PERMIT NCGIO0199 MID -ATLANTIC JOB NO. 00OR2037.00 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.250,9918 facsimile 919,250,9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on March 19, 2014 and analyzed for pH, total suspended solids (TSS), total recoverable lead, ethylene glycol and oil and grease. All parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. el.. I.., Charles B. Hoffman, P.G. Project Geologist Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE