NCG100126_MONITORING INFO_20150306

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V \ a, l
DOC TYPE
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ ao �5 ��
YYYYMMDD

CERTIFICATE OF COVERAGE NO. NCG100126
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
RECEI V EDSAMPLES COLLECTED DURING CALENDAR YEAR: 201S
MAR 0 6 2015 (This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
CENTRAL FILES
FACILITY NAME Johnston Auto Salvage OWR SECTION
PERSON COLLECTING SAMPLE(S) Alex Ahmad
CERTIFIED LABORATORY(S) Pace Analytical Lab # 12
Lab #
Part A: Stormwater Benchmarks and Monitoring Results
COUNTY Nash
PHONE NO. [phone]
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within
30 days of the end of that period to comply with permit reporting requirements.
.M"
Outfall
No.
Date
Sample Collected,
mo/dd/year
Total
Rainfall,
inches
00400
00530
----
77023
01051
78141
PH,
Standard
Units
Total Suspended
Solids (TSS),
mg/L
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), mg/L
Ethylene Glycol,
mg/L
Lead, Total
Recoverable,
mg/L
Total Toxic
Organics3,
mg/L
-49
Benchmark
-
-
6.0 — 9.01
100/502
15
8,000
(Tiers 2 and 3)
0.03
1.0
Outfall 001
01/12/15
7.2
50.3
<5.0
<10.0
0.0459
NA
Note: If you report a sampled value in excess of the
benchmark value. or outside the benchmark ranee for nH.
you must imnlemPnt Tier 1 or Tiar 2 rasnnnsas in the GpnPral
Permit.
1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark
range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented
to demonstrate background concentrations were below the benchmark pH range of 6-9.
2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters.
Form SWU-251, last revised October 25, 2012
Page 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122.
Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
Solvent Management Plan Certification Statement
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent
management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
Signature Date
Mail Original and one copy to:
Division of water Quality
Attn: Central Files
1617 Mail Service
Center
North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee or Designee]
2—q_//-7—
(Datej
Form SWU-251, last revised October 25, 2012
Page 2 of 2

1�-ceA­nalytica(
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hurtersville, NC 28078
[phone]
January 16, 2015
Darin McClure
Mid Atlantic Associates, Inc.
RE: Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
Dear Darin McClure:
Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2015,
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
cc: Joanna Crow, Mid Atlantic Associates, Inc.
Chuck Hoffman, Mid Atlantic Associates
Beverly Oglesby, Mid Atlantic Associates, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

QD
vAna1XJca!
www.pacelabs.com
i
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
Indiana Certification IDs
7726 Moller Road, Indianapolis, IN 46268
Illinois Certification #: 200074
Indiana Certification #: C-49-06
Kansas Certification #: E-10247
Pace Analytical Services, Inc.
9B00 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Kentucky UST Certification #: 0042
LouisianalNELAP Certification M 04076
Ohio VAP Certification #: CL-0065
West Virginia Certification #: 330
Florida1NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not Ge reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 12

aceAnalytrcal®
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kinney Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: JOHNSTON AUTO SALVAGE
Pace Project No.- 92232957
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92232957001 OUTFALL NO. 1 EPA 1664E
CLW
1
PASI-C
EPA 8015 Alcohol -Glycol
TMW
1
PASI-I
EPA6010
JMW
1
PASI-A
SM 2540D
WRC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 12

Analytical
a/c
www.pacefabs.com
Pace Analytical Services, Inc.
9B00 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
Sample: OUTFALL NO. 1
Lab ID: 92232957001 Collected: 01/12/15 12:00 Received:
01/13/15 11:00 Matrix: Water
Parameters
Results Units Report Limit DF Prepared
Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mg1L 5.0 1
01114/15 09:05
8015M Glycols in water
Analytical Method: EPA 8015 Aicohol-Glycol
Ethylene glycol
ND mg1L 5.0 1
01116/1513:19 107-21-1
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead
45.9 uglL 5.0 1 01/1411515:10 01/15/1519:44 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
50.3 mglL 8.3 1
01/14/15 17:04
Date: 01/16/2015 04:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 12

�ceAnalytrcal
www.pacefabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
QC Batch: GCSV/20060
QC Batch Method: EPA 1664B
Associated Lab Samples: 92232957001
METHOD BLANK: 1369687
Associated Lab Samples: 92232957001
Parameter Units
Total Petroleum Hydrocarbons mg/L
LABORATORY CONTROL SAMPLE:
1369688
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
MATRIX SPIKE SAMPLE:
1369589
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/14/15 08:31
Spike LCS LCS
Conc. Result % Rec
20 17.2 86
35170500002 Spike MS
Result Conc. Result
5.01J 23.8 22.9
% Rec
Limits Qualifiers
64-132
MS % Rec
% Rec Limits Qualifiers
88 64-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /1612015 04:11 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 12

_ ace Analytical
www.pacelabs.mm
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
QC Batch; GCSV/14063 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Associated Lab Samples: 92232957001
METHOD BLANK: 1223474
Associated Lab Samples:
Parameter Units
Ethylene glycol mg/L
LABORATORY CONTROL SAMPLE: 1223475
Parameter Units
Ethylene glycol mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/1611512:24
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
25 26.6 107 49-139
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/16/2015 04:11 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 12

1��a�eA'nalytical"
www pacelabs.com
l
I -
QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
QC Batch: MPRP117718 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 92232957001
METHOD BLANK: 1370017
Associated Lab Samples: 92232957001
Parameter Units
Lead
uglL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/15/15 00:24
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hun:ersville, NC 28078
(704)a75-9092
LABORATORY CONTROL SAMPLE: 1370018
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead uglL 500 473 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370019 1370020
MS MSD
92233140001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug1L ND 500 500 448 469 90 94 75-125 5
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /16/2015 04:11 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 12

la6m'nalytical*
www.pwotobs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
QC Batch: WET/35232
QC Batch Method: SM 2540D
Associated Lab Samples: 92232957001
METHOD BLANK: 1370240
Associated Lab Samples: 92232957001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
1370241
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1370242
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1370243
Parameter
Units
Total Suspended Solids
mg/L
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
N❑ 2.5 01/1411516:57
Spike LCS
Conc. Result
250 258
92232877001 Dup
Result Result
ND ND
92232925001 Dup
Result Result
77.3 78.7
LCS % Rec
% Rec Limits Qualifiers
103 90-110
RPD Qualifiers
RPD Qualifiers
2
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /16/2015 04:11 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 12

i
_ ace Analytical
www.Aacelabs.c=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MID L-Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaiyles.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-I Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/16/2015 04:11 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12

_ ace Analytical
www.patefabs.00m
i -
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92232957
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92232957001 OUTFALL NO. 1
92232957001 OUTFALL NO. 1
92232957001 OUTFALL NO. 1
92232957001 OUTFALL NO. 1
Date: 01/16/2015 04:11 PM
EPA 1664E
EPA 8015 Alcohol -Glycol
EPA 3010
SM 2540D
GCSV120060
GCSV114063
MPRP117718 EPA 6010
WET135232
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ICP115949
Page 10 of 12

�KI'CoAtkilytical' Jam ie c.onamon upon Receif
Document Number:
F-CHR-CS-003-rev.15
.Client Name: X,�,�
'I or z
Issuing Authority:
Pace Huntersville Quality Office
Courier j❑ Fed Ex ❑ UPS❑ LISPS❑ Client❑ Commercial❑ Pace Other
Custody Seal on Cooler/Box Present: ❑ yes ❑ ` 11) Seais intact: ❑ yes ❑ no
Packing Material: ❑ Bubble V[}p ❑ Bubbidags ❑ None ❑ Other
Thermometer Used: IR Gun TO Type of Ice _el Blue None ..-.[]'Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp.:t, _. '� •C
Biological Tissue Is Frozen: Yes No NIA
Date and Initials of person examining
C
contents: _J --
Temp should be above freezing to 6'C
Comments:
Chain of Custody Present:
--❑Yes ONO
❑NIA
1.
Chain of Custody_Filled Out:
__-DYes
❑N/A
2.
Chain of Custody Relinquished:
iOmoo
❑NIA
3.
Sampler Name & Signature on COC:
❑Yes N6_
­ ONrA
4.
Sam les Arrived within Hold Time:
I�Yes- ONO
❑NIA
5.
Short Hold Time Anal sis <72hr :
❑Yes N6-_©NIA
6,
Rush Turn Around Time Requested:
❑Yes No ❑NrA
7,
Sufficient Volume:
-E•']Yes ❑No
❑NIA
8.
Correct Containers Used:
---[]Yes ONO
❑NIA
g.
-Pace Containers Used:
", Yes ONO
❑NrA
Containers Intact:
fl3 ❑No
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes ONO
❑Nfk
11.
Sample Labels match COC:
"pY s" ❑No
❑NIA
12.
-Includes dateltime/ID/Anal sis Matrix:
All containers needing preservation have been checked.
I`
,©Yes ❑No
❑MIA
13.
All containers needing preservation are found to be in
.0r ❑No
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
C1Yes ❑No
Samples checked for dechlorination:
Dyes ONO
FINIK
f..
14.
Heads ace in VOA Vials >6mm :
PY61a ONO
❑NIA
15.
Trip Blank Present:
❑Yes ONO
IIINIA
16.
'
Trip Blank Custody Seals Present
Dyes ONO
.fW IA
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution:
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: r_(C Date: 1 11,
SRF Review: Vvl .- Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, Incorrect preservative, out of temp,
incorrect containers)
Field Data Required? Y I N
WO#:92232957
111111111111111111IN
92232957
Page 11 of 12

CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
:lion A Section B Section C
luired Client Information- Required Project Infonnation., tnvoica information: Fpage: 1 Of
nparry- 92-MID ATLAN:Iims92 Report To: 8766:92-MIDATLAN:Iims92 Attention:
ITess: 4095o Qers Vew Court CM To: Company Name:
leigh, NC 27610
Addtess:
ail To:
Purchase Order #:
Pace Quote:
me: Fax
Project Nat": Johnston Auto Salvage
Pace Project Manager nicole.qastorowski@pacelab
uested Due Date:
Project ff: ---
Pace Profile #: t; C1 7Z- 1 73
"'RequestedAnafigis
RItered
(YIN)
MAT" COOE
DmIbM VIWW OW
W21W wr
W.V. W.I. ww
P,0000 P
SAMPLE ID SOIVWd $1,
One Character per boX. wqm VVP
(A,r- G-9 1, -) AR
othff OT
Sample Fds must be unique rs
a
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0
x
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COLLECTED
z
-
0
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21
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0
Preservatives
START
END
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DATE
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DITIONALCOMMEN
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:�=EF!TED 6� i Amb�Ti6k
SAMPLER NAME AND SIGNATURE.
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PRINT Name of SAM PLER;-
SIGNATURE of SAMPLER:
DATE Signed:
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