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NCG100070_MONITORING INFO_20190131
r STORMWATER DIVISION CODING SHEET II NCG PERMITS PEkMIT NO. li IV C& Do-o `7d DO TYPE �I ❑ HISTORICAL FILE -MONITORING REPORTS II DO DATE I! li ❑ M � D 18 I YYYYM M DD f r 409 Rogers View Court Mod Atlantic Raleigh,M1 office 915.250.99 18 Engineering & Environmental Solutions facsimile 919.250.9950 MAAONLINE.COM January 31, 2019 NCDEQ/DWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: NOTIFICATION OF NON -SAMPLING EASTERN AUTOMOTIVE, INC. 1551 LEE'S UNION CHURCH ROAD FOUR OAKS, JOHNSTON COUNTY, NORTH CAROLINA PERMIT NCG100070 MID -ATLANTIC JOB NO. 000112057.00 To Whom It May Concern: On behalf of Eastern Automotive, Inc. this letter serves as notification that a stormwater sample was not collected during the second half of 2018. It is our understanding that during this timeframe, a representative storm event did not occur at a time when a stormwater sample could be safely collected (i.e. during daylight when the facility was occupied). If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, R EC F-, I E MID -ATLANTIC ASSOCIATES, INC. FEB 19 2019 CFNTR�A1L FIt.CZ C'�rifl r4CTIOIN Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100070 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 FACILITY NAME Eastern Automotive Four Oaks NC COUNTY Johnston PERSON COLLECTING SAMPLE(S) Kealy Parker PHONE NO. 800-949-4101 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flaw" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfali No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - 77023 01051 78141 pH, Standard Units Total'Suspended SolEds`(TSS), mg/L Non=polar O&G/TPH (Method 1664 SGT-HEM),,mg/L Ethylene. Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0.— 9.01 S00/50? 15 '8;000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 0 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Aauz�� jgqx�e lae-e��z Name (Print name) Title (Print title) _ Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sign ificaniLpenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or 0�—/3-1 c7 (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 Mid Atlantic Engineering & Environmental Solutions February 10, 2019 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS EASTERN AUTOMOTIVE 1551 LEE'S UNION CHURCH ROAD FOUR OAKS, NORTH CAROLINA 27524 NPDES PERMIT NO. NCG100070 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 90,250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on January 15, 2019 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters, with the exception of Ethylene Glycol, were reported below or within their respective benchmark values. Based on these results, a Tier One Response has been implemented at the facility. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. RECEIVED FEB 19 2019 Ron J. Davis CENTRAL FILES Stormwater Services Manager DVJR SECTION Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100070 FACILITY NAME Eastern Automotive, Inc., Four Oaks, NC PERSON COLLECTING SAMPLE(S) Kealy Parker CERTIFIED LABORATORY(S) Pace Analytical Lab ff 12 Lab d Part A. Starmwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Johnston PHONE NO. 919 934-4101 PLEASE REMEMBER TO SIGN ON THE REVERSE --> For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530, -- '77023' 02051 78141 pH, Standard Units Totaf Suspended Solids (TSS), ..mg/L Non --?Polar O&G/i`PH (Method 1664 SGT-HEM); mg/L`` Ethylene'Glycol, mg/L LeadJotal . Recoverable, mg/L Total Toxic 3' Organics , mg/L Benchmark - - 6.0 = 9.01 100/502 15 8,000 (Tiers 2 and.3) 0:03 1.0 Outfall 001 1/15/19 6.9 <2.9 <4.8 7.0 < 0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition, of Total Toxic Organics is that fist as stated in Appendix D, Table it of Chaptei 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Nament name) P < re Sj Title {print title GL/L. Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ;L i5-r1 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Sign of Pefmittee or Designee) (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 (�55'ceAnalj6cal W"r.pacaws,cw January 29, 2019 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 Dear Chuck Hoffman: Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 17, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, l-r Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analocal Services, LLC. Page 1 of 13 (�Ia'cmnaljdical www.pecelabs.oam CERTIFICATIONS Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification #: CL0065 Illinois Certification #: 200074 Oklahoma Certification #: 2018-101 Indiana Certification #: C-49-06 Texas Certification #: T104704355-18-12 KansaslNELAP Certification #:E-10177 West Virginia Certification #: 330 Kentucky UST Certification #: 80226 Wisconsin Certification #: 999788130 Kentucky WW Certification #:98019 USDA Soil Permit #: P330-16-00257 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NEL4P Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiafVELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytcal Services, LLC. Page 2 of 13 Pace Analytical Services, LLC Kincey Ave. te 100 �ceMal 11cale 9800Nuntersville, NC128078 V WWW. i{P h .0DM (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: EASTERN AUTOMOTIVE 92414421 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92414421001 OUTFALL NO. 1 EPA 1664E JMS 1 PASI-C EPA 8015 Alcohol -Glycol RID 1 PASH EPA 601 OD DS 1 PASI-A SM 2540D-2011 MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceftlOcal wN++cPacftftcvm ANALYTICAL RESULTS Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 1 Lab ID: 92414421001 Collected: 01/16/19 12:00 Received: 01/17/19 09:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 01/29/1905:50 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol 7.0 mg/L 5.0 1 0112V19 11:15 107-21-1 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Lead ND ugI 5.0 1 01/18/19 04:40 01/21/19 03:02 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids ND mglL 2.9 1 01/22/19 10:21 Date: 01/29/2019 01A2 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical. www.pacOW3.com QUALITY CONTROL DATA Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 QC Batch: 455010 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92414421001 METHOD BLANK: 2484111 Associated Lab Samples: 92414421001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 01/29/19 05:38 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 LABORATORY CONTROL SAMPLE: 2484112 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.3 101 64.132 MATRIX SPIKE SAMPLE: 2484113 35442756001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU 20 19.2 94 64-132 Results presented on this page are In the unite indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2019 01:42 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical e "ff.pacefts.cam QUALITY CONTROL DATA Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 QC Batch: 481362 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92414421001 METHOD BLANK: 2220878 Matrix: Water Associated Lab Samples: 92414421001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L NO 5.0 01/21/19 10:08 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2220879 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 31.3 125 55-144 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futt, Date: 01/29/2019 01:42 PM without the written consent of Pane Analytical Services, L.L.C. Page 6 of 13 aceAnal0cale www,papwabs.com QUALITY CONTROL DATA Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 QC Batch: 453167 Analysis Method: EPA 601 OD QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92414421001 METHOD BLANK: 2476428 Matrix: Water Associated Lacs Samples: 92414421001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 01/21/19 02:26 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2476429 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Lead ug/L 500 451 90 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2476430 2476431 MS MSD 92414337021 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 460 460 92 92 75-125 0 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2019 01:42 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 13 aceAwliftal o wwwpeoafe6a.com QUALITY CONTROL DATA Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 QC Batch: 453605 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92414421001 METHOD BLANK: 2478512 Matrix: Water Associated Lab Samples: 92414421001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01/22/19 10:18 LABORATORY CONTROL SAMPLE: 2478513 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 256 102 90-110 SAMPLE DUPLICATE: 2478514 92414499001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 193 19B 3 SAMPLE DUPLICATE: 2478515 92414230003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 218 368 51 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2019 01:42 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 laneAnalyfical" www.pacefabs.wm QUALIFIERS Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analyticai Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-i Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2019 01:42 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 13 (�Ia'cmnaljftale www..wcWabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: EASTERN AUTOMOTIVE Pace Project No.: 92414421 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92414421001 OUTFALL NO. 1 EPA 1664B 455010 92414421001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol 481362 92414421001 OUTFALL NO.1 EPA 3010A 453167 EPA 601OD 453186 92414421001 OUTFALL NO. 1 SM 2540D-2011 453605 Date: 01/29/2019 01:42 PM REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: ( Document February 7, 2018 Loft Document No.: office Laboratory receiving samples: Asheville ❑ Eden[-] Greenwood ❑ Huntersville 3--___'Ra1e1gh❑ Mechanicsville❑ • _ Client Name: Wo# ; 92414421 1�1 + j Project h Courier: Fed_4 ❑UPS ❑USPS ❑Client El Commercial ❑Pace ❑Other:_ II Il 11111 (1111 IIII 92414421 Custody Seal Present? ❑Yes No Seals intact? []Yes DNo Data/InlUels Person Examining Contents: Packing Mated al: ❑Bubble wrap ❑9ubble Bags ❑None ❑ Other BloiogicaVissue Frozen?. Thermometter� []Yes [3No ❑N/A L�TR bun lD, 92TO46 Type of Ices Wet ❑Blue Done Cooler Temp ('Cj: f. U Correction Factor: Add/Subtract ('C) p,O r� � Tempshould he above freezing to VC Cooler Temp Corrected CC): ❑Samples out of temp criteria. Samples on Ice, cooling process has6egun USDA Regulated Soil (dN/A, water sample) Old samples originate [n a quarantine zone within the United States; CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally, F1v�. u , in,a,..u w-11 anti Gunrro Ricol? nYes r1N0 Comments/Discrep anty. Chain Df Custody Present? Yes 014o NIA 1. samples Arrived within Hold Time? PYes ONo, -UNIA 2. Short Hold Time Analysis (<72 hr.)? []yes No. NIA 3. Rush Turn Around Time Requested? ❑Yea, ❑No ❑N/A 4. SuffidentVolume? i --Y s ONO N/A 5. Correct Con talnersUsed? 0Yos ❑No []NIA 6. -Pace Containers Used? j]Yes []No ❑NIA /11 Contalners Intact? (Dyes []No ❑N/A r 7. Dissolved anal sis:SamplesFWdFiltered? Yes, No 0NIA B. Sample Labels Match CO C7 es []No []NIA 9. -Includes Datefnme/ID/Analysis Matrix: V V I Heads ace in VOA vials >5.6mm)i Q Yes d No []N/A 10. Trip Ilan k Present7 ❑Yes oNo ❑N//A 11. Trip Ilan kCustody Seals Present? oYes [:]No A/A COMMENTS/SAMPLI DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATSON/RESOLUTION Person contacted: Date%Time: Field Data Required? ❑Yes [-]No Project lMana ge r SCUR F Review: 4'7� Date: / A Project Ntanager SRF Review: q �// _ Date: f ! q Page 11 of 13 u 3 a n -1 0 b n m � . T 0 n 2 9 n 0 w H 9 n � n .-r r O n c 0 -a A a � CD ro m v a CL G � N o N � D � v, 0 n n v �a c b_ { A w N 0 w G e m o w w ti r Itemq zzzzzzzzzzzz BP4U-125 mL Plastic Unpreserved (NIA) (CI-) BP3U-250 mL Ptaatic Unpreserved (NIA) BP2U-S00 mL Plastic Unpreserved (N/A) " BP1U-1 liter Plastic Unpreserved (NIA) BP45.125 ml Plastic H2SO4 (pH < 2) (CI-) SM-250 mL plastic HNO3 (pH < 2) B 42-125 ml Plastic 2N Acetate & NaOH (>9) . BP4tm125 mL Plastic NaOH (PH > 12) (CH WGFU-wide-mouthed Glass Jar Unpreserved AG1U-1 fiter Amber Unpreserved (NIA) (CI-) AG1H-1 liter Amber HCI (pH < 21 AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG15.1 titer Amber 142504 (pH < 2) AG35-250 mt.Amber H2SO4 (pH <2) AG3A(UG3A)-250 mL Amber NH4C1 (N/A)(Cl-) Q-4 L)G9H-40 mL VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unp (N/A) CPGSP-90 mt. VOA tt3PO4 (N/A) VOAK (9 vials per kit)-S035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-12S mL Sterile Plastic (N/A— lab) SPIT-2S0 ml-StedleP3aS%IC.(N/A—lab) MA-250 mL Plastic (NH2}2SO4 (9.3-9-7) AGOU-100 ml, Amber Unpreserved vials (NIA) VSGU-20 mL Scintillation vials (N/A) - R69U•40 mL Amber Unpreserved vials (NIA) YJCERfldlj?+(3l Section A Required Client Information: Section 6 Required Project Information: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately- ,Cetion C Inwice trdormation: Company; Mio Atlantic Associates. Inc- Report To: Chuck Hoffman Attention_ — - - AddresS: 409 Rogers View Court Copy To: Company Name: Raleigh- NC 27610 Address: - Requla!= Agency Email: Purchase Order i!: Pace Ouole: Phone: jFax Project Name: Eastern Automotive Pax Protect Manager nicdle.nasior lw i@pacelabs.com. State! Location Requested Due Dater Project e: Pace Profile a: 5921 NC Re uested Anal sis FtEYcred rN c i 2 4ATRIA coo" `o COLLECTED a Preservatives >- Dl-' g W.rtn bw U 2 Wtlr wT e U w-t' wm- M P `" } a15"" a SAMPLE ID _ " c7 - START END ¢ One Character per box- Ww m s # IA�s-9! -) tiAR OINer OT 00 U } `w W a u Z °°. T Ca v V Sample Ids must be unique Tasty Ts x w o ' v � � m � 1 Al 4 O .���� L Q m m �Zq W C H DATE TIME DATE T1ME H O C D N x 2 x 2 z z o O t W p 0 111 " 7 OuttaM{ No. t VYr X X X X f z 1 [r Arl 1141Y) 2 4. 5 ' S .g. 40 11. 12 ADDITIONAL COMMENTS ,, — -RELINQUt5HE0 BY lAFF{LIATTONDATE TIME _ = - ACO£PYEp BYr AFF�UAT{OiV' D1TE,' -TIME= _ 'SAMPLE GONp1710N5 Al i 1 '�:, / ' r3 .7-0 y ✓V tl SAMPLER NAME AND SIGNATURE- c ca = m m PRINT Name of SAMPLER: ' - � N m SIGNATURE of SAMPLER: / DATE Signed: t ' Y act Atlantic Enginaering & Environmental Solutions January 4, 2018 NCDEQIDWR Attention: Central Files 1617 Mail Service Center RF:r:1 1/FD Raleigh, North Carolina 27699-1617 JAN 19.2018 Subject: STORMWATER SAMPLING RESULTS DWR SECTION EASTERN AUTOMOTIVE INFORMA77ON PROCESSING UNIT 1551 LEE'S UNION CHURCH ROAD FOUR OAKS, NORTH CAROLINA 27524 NPDES PERMIT NO. NCG100070 To Whom It May Concern: 409 Rogcrs View Court Raleigh, NC 77610 GITICe 919 250.991 a iatsimda 919 250.9950 MAAONLINE_COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on December 12, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGIO0070 FACILITY NAME Eastern Automotive, Inc., Four Oaks, NC PERSON COLLECTING SAMPLE(S) Kealy Parker _ CERTIFIED LABORATORY(S) Pace Analytical _ Lab # 12 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Johnston PHONE NO. (919) 934-4101 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics, mg/L Benchmark - - 6.0 — 9.01 100/50� 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 12/12/17 0.14 6.8 <5.0 <5.0 <5.0 < 0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTEALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) �i (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 aceAnalytical wwwpacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 26, 2017 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: Eastern Automotive Pace Project No.: 92366871 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosunn cc: Ron Davis, Mid AtlanticAssociatees, Inc. KCR�C� \Qp�p�p REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical wwwpacdaM.00m Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92366871 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 003971 Indiana Certification #: C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification #: 80226 Kentucky WW Certification #:98019 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2017-124 Texas Certification #: T104704355-17-11 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-16-00257 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification * 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical www.pacefabs.wm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 Project: Eastern Automotive Pace Project No.: 92366871 Lab ID Sample ID 92366871001 Outfall No. 1 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol BJVV 1 PASI-I EPA6010 SH1 1 PASI-A SM 25400 SLB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical www.pecabbs.mm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 ANALYTICAL RESULTS Project: Eastern Automotive Pace Project No.: 92366871 Sample: butfall No. 1 Lab ID: 92366871001 Collected: 12112117 09:45 Received: 12/13/17 10:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 12/15/17 05:03 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 12/18/17 15:06 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 12/17/17 11:55 12/22/17 04:20 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 3.1 1 12/17/17 1114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/26/2017 02:41 PM without the written consent of Pace Analytical Services, LLC, Page 4 o0 13 aceAnalytical ~pacefabs.mn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92366871 QC Batch: 391029 QC Batch Method: EPA 1664B Associated Lab Samples: 92366871001 METHOD BLANK: 2169661 Associated Lab Samples: 92366871001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE. 2169662 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/15/17 04:55 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 19.0 95 64-132 MATRIX SPIKE SAMPLE: 2169663 92366601002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 19.6 96 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12l2612017 02:41 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 �aceftlyfical" W*W..paaafabs.carn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvWe, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92366871 QC Batch: 420518 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015Alcohol-Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92366871001 METHOD BLANK: 1938888 Associated Lab Samples: 92366871001 Parameter Units Ethylene glycol mg1L LABORATORY CONTROL SAMPLE: 1938889 Parameter Units Ethylene glycol mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/18/17 11:51 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 22.3 89 41-162 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1938890 1938891 MS MSD 50186654001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua) Ethylene glycol mg/L ND 25 25 25.1 26.4 99 105 20-172 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/26/2017 02:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 • aceAnalyfical www.pacel2bs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92366871 QC Batch: 391258 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92366871001 METHOD BLANK: 2170937 Associated Lab Samples: 92366871001 Parameter Units Lead uglL LABORATORY CONTROL SAMPLE: 2170938 Parameter Units Lead uglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/23/17 00:33 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers S00 470 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2170939 2170940 MS MSD 92366747001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug1L ND 500 500 453 494 90 99 75-125 9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/26/2017 02:41 PM without the written consent of Pace Analyticai Services, LLC. Page 7 of 13 aceAnalytical www.pacelabs.c m Pace Analytical Services, I t-C 9800 Kincey Ave. Suite 100 fiuntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92366871 QC Batch: 391252 QC Batch Method: SM 2540D Associated Lab Samples: 92366871001 METHOD BLANK: 2170911 Associated Lab Samples: 92366871001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2170912 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2170913 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2170914 Parameter Total Suspended Solids QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/17/17 11:20 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 248 99 90-110 Units 92366775008 Result Dup Result mg/L ND ND Units 92366775018 Result Dug Result mg1L 43.6 65.9 RPD Qualifiers RPD Qualifiers 41 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1212612017 02:41 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalytical www.pacelalss.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704)875-9092 QUALIFIERS Project: Eastern Automotive Pace Project No.: 92366871 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/26/2017 02:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 aceAnalytical Ww.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Eastern Automotive Pace Project No.: 92366871 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92366871001 Outfall No. 1 EPA 1664E 391029 92366871001 Outfall No. 1 EPA 8015 Alcohol -Glycol 420518 92366871001 Outfall No. 1 EPA 3010A 391258 EPA 6010 391451 92366871001 Outfall No. 1 SM 2540D 391252 Date: 12/26/2017 02:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised. August 4, 2017 Sample Condition Upon RecelptiSCURj Page 1 of 2 Document No.: Issuing Authority: aceArralytical F-CAR-CS-033-Rev.04 Pace Qu ali ty Office Laboratory receiving samples: Asheville? ❑ Eden[] Greenwood HuntersvillQ_ Raleigh[] Mechanicsville[] • Client Name; � WO : 92366671 Courier: F d Ex ❑UPS ❑U5 S [—]Client ❑ Commercial ace ❑Other: 92366871 { Custody Seal Present? []Yes o Seals intact? ❑Yes {� Date/Initlats Person Examin{n ont V_1'zJ 1�� Packing Material: ❑Bubble Wrap 46bble Bags ❑None ❑ Other Blatoglca TiIssue Frozen? Thermom er: - r t ❑ [)None None ❑YesN ❑N/A ,IR Gun ID: _7� type of Ice: Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to 6'C []samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil r{&A, water sample] Did samples a i�ln}}ate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, 1IYes Nh including Hawaii and PUenD Rico I? rlYes f r'1WJ Comm ents/Discrepancy: Chain of Custody Present? 15es ONci N/A 1. Samples Arrived within Hold Time? es No N/A 2, Shaft Hold Time Analysis c72 hr.)? Yes ❑N/A 3. Rush Turn Around Time Requested? Qyes ONIA 4. Sufficient Volume? Y ❑No N/A 5. Correct Containers Used? -Pace Containers Used? .- s s ❑No No ❑N/A N/A 6. Containers Intact? cs ND N/A 7, Dissolved analysis: Samples Field Filtered? MYes MNO /A B. Sample labels Match CDC? -Includes Date/Time/ID/Analysis Matrix: I J. \ v\�k ON. N/A 9. Heads ace in VOA Vials {>5-6mm)? s No N/A 10.2. t I Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes ❑N I No ❑N/A ❑N/A 11. CLIENT' NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot If] of Split containers: Project Manager SCURF Review: Project Manager SRF Review: ON Field Data Required? []Yes ❑NO Date/Time: Date: I t3 Date: Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this Form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 11 of 13 Document Name: Document Revised: August 4, 2017 ace�nalytica!" 5ampte Condition Upon ReceiptRSCURI Page 2 of 2 Document No.: Issuing Authority: F•CAR-CS-033•Rev.04 Pace Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and.within the acceptance range for preservation samples. **Bottom half of box is to list number of bottles r q _ Project q,�W • 923.V�� 1 - PM: NMG Due Date: 12/28/17 CLIENT: 92-MID ATLAN It E a! Z Cy1 n E u, a a m 2 to o IA o7 6 a7 2 a is O N 6 m ¢ d ll .y d •• r+ 6 m O N '^ E LA 6R a 6 m t7 N m n E M 6 m O Z '^ a E V a m y x Oq a E O 6 m w L O E Y u. m C d A E iu tP d n _ U m a E v w Q u Z a g' E a of MI U Q N o a a m nl U ¢ O T a E E LA m U 6 u z Q E Lon6 Z 1y 19 Q 2 = 0 E 0 m 0 t] 0 z q p E 0 (n w > z 4 O E 0 m 0 > v O 4 O 0 m U D o `I n ;d Q Q 7 ;� R s l7 A ar E n 6 vl a �v tv E 6 N of 2 E Vf 6 m C 7 U Z 13 E H > Z l7 1 ^� 2 3 4 5 N i i 1 N\ I I 7 —7 8 N I 9 10 N \N\ I N 11 -M. 11 N NN\� I H. 12 pH Adjustment Log for Preserved Samples Sample IQ Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot it Page 12 of 13 -�' CHAIN[ -OF -CUSTODY / Analytical Request Document Fie :r.;1;4k:if The Chain -of -Custody is a LEGAL DOCUMEKT_ All relevant fields must be completed accurately. Section A Section B Section C 1 Required Client Information: Required Project Information: lnyoice Information: Pacie : ; of I ..� Company; Fas:vrn Aulomnk, Ret.on To Ke,:h Parker AuenGen Adrlruss1551 LC,1'S Union Church Roved Copy ia: Comonny Name. Pa-r Oaks. NC 27524 Addrass, Regulatory Agency Emak$. Pun.hnse Ordem I Pace Oume. Phone: llrai Project Name fsslrfft Aatamalwe Pate Project NIAr•.ager. nieole cussiofcw ki{dtpa raatls, tom, State I Location Requesldd Due pate. Project a: Pace Prolde 0. 5921-7 NC Rc ueSted Analysis Filtered JY1N z cr>tt£ - o COLLECTED _ Preservatives } t1.ne�vrau. tnr � O _ n n Z P,eC�ct P SAMPLE ID l7 p N Y ue Or START END r One Character per box. W.P. v'P _- a m m si _ s A I A-Z. 0-9 f. on" of � � P n Samptc Ids me. must be unique ,-. x u TIAIETf-F eu p P On � _� UJ 2 r (LATE TIME O r Ili >~ 1 Oulfatl No. i WT X X X X 2 F3 ' 2 i 2 �z CIL", 2 - fag- widlov, 4 5 6 7 8 9 10 11 12 f f ADDITIONAL COMMENTS REL,NpUMHED BY I AFFILIATION OATS TIME ^ / ` / ACCEPTED BY f AFFILIA D - OAT TIME SAMPLE CONDITIONS icy) G mLA X.1 U 11 ZI 1 1 V 0 E SAMPLER 14AIAE AND StGNATURE C 4 G PRINT NamC of SAMPLER:'/�^ { �) r d U n d SIGNATURE of SAMPLER: DATE Signed:12 L a v } y m y STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100070 RECEIVED JUL 12 2017 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days CENTRAL FILES from the date the facility receives the sampling results from the laboratory.) DWR SECTION FACILITY NAME A -Bishop Towing and Recovery, Fayetteville, NC PERSON COLLECTING SAMPLE(S) Michael McKethan CERTIFIED LABORATORY(S) Pace Analytical _ Lab # 12 Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Cumberland PHONE NO. (910) 483-5156 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 05/31/17 0.80 8.7 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. for those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee d Designee) (Date) Form SWU-251, last revised October 25, 2012 - Page 2 of 2 • id �+r 409 RogersViewv COsrt M'9d p tlantic H afilce 9 f 9.250 99 f 8 fficigf,•NC2991a Engineering 9 Envlrpnmancal Safutions facsim la 419 250.9950 - MAAONLINE.COM April 4, 2017 NCDEQ/DWR Attention: Central Files RECEIVED 1617 Mail Service Center Raleigh, North Carolina 27699-1617 APR 2 4 2017 CENTRAL FILES Subject: STORMWATER SAMPLING RESULTS DWR SECTION EASTERN AUTOMOTIVE 1551 LEE'S UNION CHURCH ROAD FOUR OAKS, NORTH CAROLINA 27524 NPDES PERMIT NO. NCG100070 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on March 16, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGI000?0 FACILITY NAME Eastern Automotive, Inc., Four Oaks, NC PERSON COLLECTING SAMPLE(S) Kealy Parker CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Johnston PHONE NO. 919) 934-4101 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flaw" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 03/16/17 0.90 7.0 <5.0 <5.0 <5.0 < 0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ vraive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or E 4-- (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 e aceAnalytical wn+rpacelabs.coro Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 March 30, 2017 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: Eastern Automotive Pace Project No.: 92334002 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNi1NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical www.paselahs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Eastern Automotive Pace Project No.: 92334002 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification #: CL-0065 Illinois Certification #i 003971 Oklahoma Certification #: 2016-075 Indiana Certification #: C-49-06 Texas Certification #: T104704355-16-10 Kansas/NELAP Certification #:E-10177 West Virginia Certification #: 330 Kentucky UST Certification #: 80226 Wisconsin Certification #: 999788130 Kentucky WW Certification #:98019 USDA Soil Permit #: P330-16-00257 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvilie, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 ace Analytical www.pacelabs.cam Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Eastern Automotive 92334002 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92334602001 Outfall No. 1 (3-16-2017) EPA 1664B JMS 1 PASI-C EPA 8015AIcohol-Glycol RID 1 PASI-I EPA6010 SH1 1 PASI-A SM 2540D MJSi 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fult, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical www.pacelabs.c= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Eastern Automotive Pace Project No.: 92334002 Sample: Outfall No. 1 (3-16-2017) Lab ID: 92334002001 Collected: 03/16/17 11:00 Received: 03/21/17 09:38 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 03/22/17 06:56 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 03/30/17 12:05 107-21-1 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 03/22/17 19:45 03/28/17 07:04 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 03123/17 00:09 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/30/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 ace Analytical ..pacelabs.oarn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92334002 QC Batch: 353183 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92334002001 METHOD BLANK: 1959071 Associated Lab Samples: 92334002001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 1969072 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 03/22/17 06741 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 19.2 96 64-132 MATRIX SPIKE SAMPLE: 1959073 92333353001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 18.6 93 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OP LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/30/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92334002 QC Batch: 379803 Analysis Method: EPA 8015AIcohol-Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92334002001 METHOD BLANK: 1752087 Associated Lab Samples: 92334002001 Parameter Units Ethylene glycol mg/L LABORATORY CONTROL SAMPLE: 1752088 Parameter Units Ethylene glycol mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 03/3011710:52 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 27,1 108 60-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1752089 1752090 MS MSD 50167213001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L ND 25 25 19.3 23.0 74 88 23-157 17 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03130/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytical" atvw.patelabs.C= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92334002 QC Balch: 353165 QC Batch Method: EPA 3010A Associated Lab Samples: 92334002001 METHOD BLANK: 1959042 Associated Lab Samples: 92334002001 Parameter Units Lead uglL LABORATORY CONTROL SAMPLE: 1959043 Parameter Units Lead uglL QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 03/26/17 05:11 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 458 92 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1959044 1959045 MS MSD 92334068001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead uglL ND 500 500 432 428 86 85 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/30/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAna&tcal Ww.Pacelab&=n Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92334002 QC Batch: 353318 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92334002001 METHOD BLANK: 1959893 Matrix: Water Associated Lab Samples: 92334002001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/23/17 00:06 LABORATORY CONTROL SAMPLE: 1959894 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1959895 92333765003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1959896 92333804001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND NO Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/30/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 Pace Analytical Services, LLC Kincey Ave. te 100 aceAnalytical o 9800Hunte sville, NC128078 wwwp"abs.tw (704)875-9092 QUALIFIERS Project: Eastern Automotive Pace Project No.: 92334002 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitro sod iphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI.-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-1 Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/30/2017 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 laceAnalXical " www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Eastern Automotive Pace Project No.: 92334002 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92334002001 Outfall No. 1 (3-16-2017) 92334002001 Outfall No. 1 (3-16-2017) 92334002001 Outfall No. 1 (3-16-2017) 92334002001 Outfall No. 1 (3-16-2017) Date: 03/30/2017 01:57 PM EPA 1664E EPA 8015 Alcohol -Glycol EPA 3010A SM 2540D 353183 379803 353165 EPA 6010 353318 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analyt(cal Services, LLC. 353366 Page 10 of 13 Laboratory receiving samples: Asheville ❑ Eden❑ Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Recet t(SCURj Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ • Client Name: : 92334002 /f / r etY t/' j �C Project #: Wo# j j I Courier:❑PadE x ❑UPS ❑ UShS ❑Client ❑ Commercial[]Other-,_ ❑ ❑Ot er , 92334002 Custody Seal Present? []Yes QNo Seals Intact? Oyes ❑6-6 Date/Initials Person Examining Contents: J^i Packing Material: ❑Bubble Wrap Bubble Sags ❑None ❑Other: Thermometer: �t, et ❑Blue ❑None amples on ice, cooling process has begun (� iR Gun ID: Correction Factor: ^ y }�� Cooler Temp Corrected ('C): Type of ice: Biological Tissue Frozen? ❑Yes E o ❑N/A Temp should be above freping to 6'C USDA Regulated Soil ( N/A, water sample) Did samples o 'ginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source ❑Yes including Hawaii and Puerto Rico)? []Yes Chain of Custody Present? [3res QNo ❑N/A 1. Samples Arrived within Hold Time? Qks' ❑No ❑N/A 2. Short Hold Time Analysis 02 hr.)? Dyes o� ❑N/A 3. Rush Turn Around Tlme Requested? ❑Yes ,—•," L.c}rro ❑N/A 4. Sufficient Volume?' es []No ❑N/A 5. Correct Containers Used? -Pace Containers Used? es es ❑No [:]No ❑N/A ❑N/A 6. Containers Intact? Elf es ❑No ❑N/A 7. Samples Field FiltereQ? ❑Yes No ON% 8. Note if sediment is visible In the dissolved container Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: es ON. ❑N/A 9. Headspace in VOA Vials (>5-6mm)? Ids No ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ONO (:]No E59/-A PWAr 11. CLIENT NOTIFICATION/RESOLUTION Field Data Required? []Yes FIND Person Contacted: Comments/Sample Discrepancy: Date/Time-, Project Manager SCURF Review: L(!� Date: , (,7' Project Manager SRF Review: S Date: ?> ZI Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR CertifiCation Page 11 of 13 N O W 00 v m Ln a w Item# zzzzzzzzzzzz BP4U-125 ml. Plastic Unpreserved tN/A) (Cl-) 8P3U-250 mL Plastic Unpreserved (N/A) BPZU-500 mL Plastic Unpreserved (N/A) h.} BP1U-1 liter Plastic Unpreserved (NIA) BP3S-250 mL Plastic H2SO4 (pH < 2) (Cl) 8P3N-250 ml. plastic HNO3 (pH < 2) BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) BP3C-250 mL Plastic NaOH (pH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) zzzzzzz z Z AGSH-1 liter Amber HCl (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber HZSO4 (pH < 2) AG3S-250 mL Amber H2SO4 (pH < 2) Zlxz AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(CI-) DG9H-40 mL VOA HCl (N/A) VG9T-40 mL VOA Na25203 (N/A) VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SP5T-125 mL Sterile Plastic (N/A — lab) SP2T-250 mL Sterile Plastic (N/A —lab) zzzz zzz z MA-250 mL Plastic (NH2)2SO4 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) GN n t9 A a zz w n ni m 3 C n _ ro rr fp C f ro AOR A S. m y CD I-D C N Q c S O v O N O ro fD n H a ow 2ceAnaj vtrcal CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain•of-Custody is a LEGAL DOCUMENT. All relevant fields mull be campleled atturatey. >ection A Section a Section C Page: of iequired Cltenl Inlormation. Requlmd PTotea Information tnvoice information :ompany Mid-Atlant c Associates, Inc. Repon To Chuck Hoffman (choffman Q@maaoniine.cA n) Att—Wn. Chuck Hoffman ,ddress. 409 Rogei s View Court Copy To. Ron Davis (rdavis@maaonline.com Company Name: Mid-Atlanlic Associates, inc. REGULATORY AGENCY Raleigh, W 27610 Address 409 Rogers View Court, Raleigh, NC r NPDES i" GROUND WATER DRINKING WATER f"- UST I- RCRA OTHER --mail To choffman maaonline.eom Puresase Cider No. R2057,00 Pace mole Reference, hone, 9 t 9-250-9918 Fax 919-250-9950 Proi6dl Name: Eastern Automotive Pace Protect Nicole Gasiorowski SEW Location Manager: STATE: NC tequested Due Dale/TAT: standard Project Numcer. R2057,00 Pace Pfef.le0 -- Requested Analysis Filtered (YIN) Section D Valid Matrix Codes e a z Required Cheat Infer awnMATRtx CODE c t COLLECTED Preservatives `T N Y N Y DRINKMGWATEN OW a (O.T II z Q v ATER WT WASTE WATER I—v t.l c ovPOSITE COMPOSITE f- in m Z PRODUCT v ¢ START ENMRAB w sOusoLlD sL M y } Oi OL SAM LE ID tiyIPE WP — T c; Q H CO L c (A•Z. 9r,•t OTMER OT Ld 1- Q. W Z a a0 Q T N O Sample IDS Nit ST BE UNIQUE TISSUE is O C F df A X J N q C T C rz 2 11 LL O x U) C C>7 = T 4 Q O cca Z U r9 N r Q a rq N ~ y DATE TIME DATE TIME rn x s 2 z z O cc Pace Project No !Lab I.D. 1 Outfall No. 1 WT G 7 4 1 z x x x x Rainfall (inches): 2 -- o fliffti 3LJqt7 l a H: ) 3 4 5 6 7 B 9 10 it 12 ILI ADDITI )NAL COMMENTS REUNQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS ` 5 -Zi-1 A aY3 Y .y Y SAMPLER NAME AND SIGNATURE „ o _ 4 o z PRINT Name of SAMPLER: z SIGNATURE of SAMPLER: DATE Signed t,a I,& 3 v fMMIDDIYYI: U IF I t -Impnrtarl N I e. By srcgnmg Iles farm you are acceptmg Pace's NET 30 -.fay payment lerms and agreeing 1n Llta charges a1 1.5`>y qn mamh ran any onvmees not paid wrthm 30 days, F-ALL'0-020rev.08, 12-Oa-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGIO0070 FACILITY NAME Young's Auto Center & Salva a U-PULL-IT PERSON COLLECTING SAMPLE(S) Steve Wiggins CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Wayne PHONE NO. (919) 894-3500 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 2.0 Outfall006 11/19/15 1.1 7.1 154 <5.0 <5.0 <0.0050 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If off values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument aecuracy) instead of E S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, lost revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." t (Signature of Permittee or Designee) (Date) Form SWU-251, lost revised October25, 2012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100070 FACILITY NAME Eastern Automotive, Inc., Four Oaks, NC PERSON COLLECTING SAMPLE(S)Kealy Parker CERTIFIED LABORATORY(S) Pace Analytical Lab #12 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR:2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY.Iohnston PHONE NO. (919) 934-4101 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics, mg/L Benchmark - - 6.0 — 9.01 100/50z 15 81000 (Tiers 2 and 3) 0.03 1.0 Outfall001 06/04/2015 1.0 7.0 14.3 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Caralina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." '�7` 5�- :Z::TJ (Date) Form SWU-251, lost revised October 25, 2012 Page 2 of 2 mod Atlantic Engineering & Environmental Solutions July 7, 2015 NCDENR/DWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS EASTERN AUTOMOTIVE 1551 LEE'S UNION CHURCH ROAD FOUR OAKS, NORTH CAROLINA 27524 NPDES PERMIT NO. NCG100070 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 276 10 office 919.250.9918 facsimile 919.2S0.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on June 4, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE • aceAnalytrcal www.pacelabs.corn June 16, 2015 Chuck Hoffman Mid Atlantic Associates RE: Project: Eastern Automotive Pace Project No.: 92253074 Dear Chuck Hoffman: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on June 05, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 laceAnalyticalo wwwpacerabsx" Project: Eastern Automotive Pace Project No.: 92253074 Indiana Certification II)s 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification M 200074 Indiana Certification #: C-49-06 Kansas Certification #:E-101771 E-10247 Kentucky UST Certification #: 0042 Kentucky WW Certification #:98019 Louisiana/NELAP Certification #: 04076 Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2014-148 Pennsylvania Certification #: 68-05340 Texas Certification #: T104704355-15-8 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-10-00128 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #; 99030001 West Virginia Certification #: 356 VirciiniaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 Pace Analytical Services, Inc. aceAnalytical A 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpacvlabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Eastern Automotive Pace Project No.: 92253074 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92253074001 OUTFALL NO.1 EPA 1664B CLW 1 PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASI-I EPA601❑ JMW 1 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 acmnalXical wrvwoacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92253074 Sample: OUTFALL NO.1 Lab ID: 92253074001 Collected: 06/04/15 11:00 Received: 06/05/15 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 06/15/15 08:46 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 06/11/15 18:37 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug1L 5.0 1 06/08/15 17:10 06/09/16 20:52 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 14.3 mg/L 2.7 1 06/11/15 14:50 REPORT OF LABORATORY ANALYSIS This report shatl not be reproduced, except in full, Date: 06116/2015 06:29 PM without the written consent of Pace Analytical Services, Inc._ Page 4 of 14 e aceAnalytrcal ~..pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92253074 QC Batch: GCSV121643 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92253074001 METHOD BLANK: 1484604 Matrix: Water Associated Lab Samples: 92253074001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 06/15/15 08:44 LABORATORY CONTROL SAMPLE: 1484605 Spike LGS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.9 90 64-132 MATRIX SPIKE SAMPLE: 1484606 92253927001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 20 17.9 87 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:29 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 acmnalytical w*wpacalabs.corn QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92253074 QC Batch: GCSV115669 Analysis Method: EPA8015Alcohol-Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples. 92253074001 METHOD BLANK: 1315435 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg1L NO 5.0 06/11/15 16:13 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1315436 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 22.9 92 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1315990 1315991 MS MSD 92252710002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L NO 25 25 20.0 20.3 80 81 67-133 1 Results presented on this page are in the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06116/2015 06:29 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 laceAnallytical www pacelabs.com Project: Eastern Automotive Pace Project No.: 92253074 QC Batch: MPRP118643 QC Batch Method: EPA 3010 Associated Lab Samples: 92253074001 METHOD BLANK: 1478701 Associated Lab Samples: 92253074001 Parameter Units Lead ug1L LABORATORY CONTROL SAMPLE: 1478702 Parameter Units Lead ug1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 06/09/1519:54 Spike LCS LCS % Rec Conc, Result % Rec Limits Qualifiers 500 477 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478703 1478704 MS MSD 92253110004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead uglL ND 500 500 477 516 95 403 75-125 8 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06146/2015 06:29 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 ace Analytical wwwpacefabs.com QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92253074 QC Batch: WETl38051 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92253074001 METHOD BLANK: 1482385 Associated Lab Samples: 92253074001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1482386 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1482387 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1482388 Parameter Units Total Suspended Solids mglL Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06/11/15 14:47 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 238 95 90-110 92253050001 Dup Result Result RPD Qualifiers 10 22.0 75 D6 92253245001 Dup Result Result RPD Qualifiers ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:29 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 lac,6Analytical" wwwpaCelab$'c= QUALIFIERS Project: Eastern Automotive Pace Project No.: 92253074 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-1 Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shalt/ not be reproduced, except in full, Date: 06/16/2015 06:29 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 Pace Analytical Services, Inc. aceAnalytical 9804KinceyAve. SuiteOC Hunlersville, NC 2807878 www.Welabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Eastern Automotive Pace Project No.: 92253074 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92253074001 OUTFALL NO.1 EPA 1664B GCSVl21643 92253074001 OUTFALL NO.1 EPA 8015AIcohol-Glycol GCSVI15669 92253074001 OUTFALL NO.1 EPA 3010 MPRP118643 EPA 6010 ICPI16724 92253074001 OUTFALL NOA SM 2540D V11ETI38051 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 06:29 PM without the written consent of Pace Analytical Services, Inc. Page 10 of 14 V VVN1111..114 [1VY1]VN. IYIUy IV, /-v v r Sample Condition U onuRecei t SCUR Page 1 of 2" Awalyficid'Docum9nt Number: Issuing Authority: F-CHR-0-003-rev.16 I Pace Huntersville Quality Office Client Name:ti - /yi W - r G �[ ASS— Page 2 of 2 is for Internal Use Only Courier: E " x UPS[--] USPS❑ Client❑ CommercialEj Pace Other CustodySeal on CoolerfBox Present: es no no 4L 1 4rt. ❑ y Seals intact: El ❑ pro! '.�leDat:t sl"tl %'° 10i, Q� �sl V a f I I��t•',i;�• 1'A6iiir, �tr•.Ry , Packing Material: ❑ Bubble V❑p tj a s ❑ None ❑ Olher Thermometer Used: IR Gun T1401 Type of Ice: !fit Blue None iJ Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp.: -C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No bl! ZComments- Date and Initial pe son �ar ning contents: Chain , 'of Custody Present: yes No ❑NIA 1. Chain of Custody Filled Out: gi fSffi'es tNo ❑NIA 2• NO OkGf Chain of Custody Relinquished: [:IYVD<o ❑NIA 3. Sampler Name & Signature on COC- 13/wifillo ❑NIA 4. Samples Arrived within Hold Time: ElYes ❑N CINIA 5. Short Hold Time Analysis <72hr : ❑Yes d1ol ❑NrA 6. Rush Turn Around Time Requested: O'YZ No ❑NIA 7. Sufficient Volume: E(YV ONO ❑NIA 8. Correct Containers Used: -Pace Containers Used: RKIV ONO 48 s ONO ❑NIA ❑NIA 9. Containers Intact: 14Yes ©No ❑NI 10. Filtered volume received for Dissolved tests ❑Yes ON/ NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix; ❑Y No ❑NIA 12, CtA-C(- li--, ( l�C l tI'(�r aVt COA�c,tla�-S Co ILL ll:CC) All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptlons: VOA, coliform, TOC, 0&G, W-DRO (water) Ye ONO ❑v ONO Yes ONO ❑NIA ❑NIA 13. Samples checked for dechlorination: OYey ONO NIA 14. Heads ace in VOA Vials >6mm : Yes ❑No ONfA 15. Trip Blank Present: Trip Blank Custody Seals Present PaceTri -Blank Lot# (ifurchased:-----.____._.. Dyes ❑No Oyes ❑Na ._ ZNIA _ _ 16. ._.__.--_-_-.—-----------.___-- _-._-. ---.__-- -------.__—_-- Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review:1 U VV ILI Date: IiP"5"1 SRF Review: Date: Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DFHNR Certification Office ( I.e out of hold, incorrect preservative, out of temp, incorrect containers) WO#:92253074 1111111111111111111111 92253074 Page 11 of 14 _ aceAnalytical ' r•n-.v rsaeaND2 cam CHAIN -OF -CUSTODY I Analytical Request Document o The Chain -of -Custody is a LEGAL DOCUMENT. AD relevant fields must be completed accurately.tm N m to Section A Section B Section C ,.^ago: of Requlrod Client Intortnation: Required Project Intgmat;on: invoice InlatmaWn- ,GoMWY Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman@maaontine.com) Attention; Chuck Hoffman Ads: 409 Rogers View Court CoPy To: Joanna Crow acrow@maaonline.corn) Comwnr Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 ddresa. 409 Rogers View Court, Raleigh, NC r NODES f- GROUND WATER - ORINKING WATER i UST i- RCRA i OTHER Email To: rhoffman@maaonllne.COm Purchase Order No.: R2057.00 Pace Chme - Reference: Phone: 919-250-991 S Fac 919-250-9950 P-ia�t N—: Eastem Automotive Pace PMieR _ Nicole Gasiorowski er Site Location NC Requested Due DatertAT; Standard Project Number, R2057.00 Pars Profile a: — STATJ=: Requested Anatysis Filtered (YIN) SoeTlnn D Valid Matrix Codes — z ReQutred Client lnfomstion MATR 2M o COLLECTED Preservatives r. N Y N Y or+aa�rcvrATER vn V Z WATER W'r 4 r� V 0 W WASTEWATER WN 3 corvai"TE COMP=E r PQCPtXT P son�scuo SL - • START E DROPAe w _ Z 07. OL SAMPLE 1D AR = k7 k? tu 0 � to IX r rn {p � c � � l�y� RR AR (A-z 0.91. ) OTHER or O Lu Sample IDS MUST BE UNIQUE TISSUE TS m U a x m w O 0 m OFO— R f Ut a `E ii f u m G CST N = m tD ~ N DATE TIME DATE TIME N = S T cc Z M 2 O F F LU 3 Pace Project NoJ Lab I.D. t WWI No. 1 wT G - - 7 a 11121 x xi x I x I I Rainfall (inches): It� 2 H: 3 4 5 6 7 8 9 - JD ADDITIONAL COMMENTS • - RELINQUISHED BY r AFFILIATION 'DATE - TIME CCEPTEO Y 1 FI TION DATE TIME ` : SAMPLE CONDITIONS t I J SAMPLER NAME AND SIGNATURE o m A C PRINT Name of SANIPLER: 2S SIGNATURE Of SAMPLER Q DATE Signed (I� �11 L ~ _ ¢ L ` (Mmfo "f 1mfWnar l Note: By signing this form you are accepting Page's NET 30 day payment terms and agreeing to Late charges of 1.5% per month for any invokes not Paid w9m 30 cloys. F-ALL-Q-020rev.08, 12-Oct-2007 � ceAnaf flcal dition Upon Rece Docum t Number: F-CHR-JCS-003-rev.16 ✓VVM1111..11I %I 110- IYIGr IVI •-- I- UR _ - Pagel of 2` Issuing Authority: Pace Huntersville Quality Office Client Narne: M to A„6 Gr'�}C ASS* * Page 2 of 21s for Internal Use Only Courier: yI UPS❑ LISPS❑ Client❑ C mercfal❑ Pace Other °>40oP; �FT3E �fr. Custody Seal on CoolerlBox Present: El yes no Seals intact: ❑ yes ❑ no4j �DIEb2ltt3'xy;f f%E f7ip{VBtYie;�`r Packing Material: ❑ Bubble V❑p �b�a s ❑ None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice: lcR Blue None Ll Samples on ice, cooling process has begun TemD Correction Factor T1401 No Correction Corrected Cooler Temp.: •C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No Wo Comments: Date and Initials pe sonar jning contents:��� Chain of Custody Present: -171y"SAN91 ❑NIA 1. Chain of Custody Filled Out: S es No ❑NIA 2. O ta% Chain of Custody Relinquished: OYV114 ❑NIA 3. Sampler Name & Signature on COC: a No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑N ❑NIA 5. Short Hold Time Analysis <72hr - Dyes I&VIDNIA 6. Rush Turn Around Time Requested: ❑Y No ❑NIA 7. Sufficient Volume: Y ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: zy.y I s ❑No ❑No ❑NIA ❑NIA 9. Containers Intact: Yes ❑No ©NI 10. Filtered volume received for Dissolved tests Dyes ON/ NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: Dye No ©NIA 12, CoILI tt:nO `4w` All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. excepllons: VOA, coliform, TOG, Or%G, WI-DRO {water} ZY Yes ❑No ❑No ONo ❑NIA ❑NIA 13. Samples checked for dechlorination: 0!!Z Ono NIA 14. Headspace in VOA Vials >6mm : Yes ❑No ONIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip -Blank Lot # if purchased): ----- -- ❑Yee ❑No ❑Yes ❑No NI ErNIA 16. Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Date/Time: Comments/ Resolution: 5t;UK1- Keview:j LU I Date: I V-�;? 1 SRF Review: Date: - j Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) wus: y[[bJu/4 1111111111111111111111 Page 13 of 14 CHAIN -OF -CUSTODY 1 Analytical Request Document o _ aceAnalXical The Chain-or-Gustody is a LEGAL DOCUMENT. M relevant fields must be completed acauately. v_ wA-.v pACW, OS COM G) m M Section section B Sc-don C Required IPa>9a: of Clien[ In(oA mmalion: Required Pr4mt Information: Invoice Information: _ company. Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman@maaonline.com) Attention: Chuck Hoffman Address: 409 Rogers View Court copy re: Joanna Crow maaonline.corn Q �bw(� ) company Nam: Mid-AEIanGcAssociates. inc. 409 Rogers View Court, Raleigh, NC REGULATORY AGENCY r NPDES 17- GROUND WATER i DRINKING WATER i UST f— RCRA i OTHER Raleigh, NC 27610Address: Email To: rhoffman@masonline-com Purchase Order No.; R2057.00 Pam o+mre _ ReTerar+ce: Phone: 919-250-9918 Fax 919-250-9950 Prom Nam: Easter Automotive Pam PmOm Nicole Gasiorowski Site Location Marmager. STATE: NC Rdquesled Due DatefrAT: SUnaard Project NWntmer. R2057.00 Pam Prof" d _ z Requested Analysis Filtered (YIN) Valld Matrix Codes E Re ubwCCerxinformation MATFt S V COLLECTED Preservatives >- N Y N Y ORWpNG WATLR aW composme CA MppATE m Q WATER wT` WASTE WATER v9vv n V O f owoucr P m 5 START EN010PAS w to w Z scnr�otm sL a a ti ! /�j+'I-�6 SAMPLE ID Am � �? ui _ 4-0ii (A-M MUST BE or!¢R oT Sample IDS MUST BE UNIQUE TLsstrE Ts O p uu a a Z,JIJ m / i V ZO „� a T y G ur tz a. N O O r« � r C N 2 y y ~ DATE TIME DATE TIME w x 7 = 2 2 2 z 41) O d Pace Project Not Lab I.D. 1 Outfall No. 1 wT G 7 41 1 2 x x X1 X1 I Rainfall (inches): I = H: 3 S 5 6- 7 6 9 10- 1i 12- _ ADDITIONAL COMMENTS - RELINQUISHED BY 1 AFFILIATION - ' DATE TIME CCFPTED Y I Fl TION - DATE TIME. SAMPLE CONDITIONS r N SAMPLER NAME AND SIGNATURE v y_ PRINT Name or SAMPLER: Mu W(� a DATE 9r1cd $ E SIGNATURE of SAMPLER: 001141 15 a MMFD co 'Irpul WA NOW: By $19" Vws tam you are acce0ln9 POCa's NET 30 day payrera terms and agreeing to tau charges of 1.5% per menR for arty awdees ndt paw w9 w 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100070 RECEIVED SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days MAR. 16 Z015 from the date the facility receives the sampling results from the laboratory.) CENTRAL FILES FACILITY NAME Eastern Automotive, Inc., Four Oaks, NCp%41R. cIEcTIGN COUNTY Johnston PERSON COLLECTING SAMPLE(S) Kealy Parker PHONE NO. (919) 934-4101 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 C.D Part A: Stormwater Benchmarks and Monitoring Results LAJ ..,.j For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 60W0=0 30 days of the end of that period to comply with permit reporting requirements. LA. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic prganics3, mg/L Benchmark - - 6.0 — 9.01 100/SOz 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 01/05/15 S.0 6.9 7.5 <5.0 <10.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. zSee General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) (Date Form SWU-251, last revised October 25, 2012 Page 2 of 2 �,aceAnalyticale wwwpacetabs.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 January 30, 2015 Darin McClure Mid Atlantic Associates, Inc. RE: Project: Eastern Automotive Pace Project No.: 92231740 Dear Darin McClure - Enclosed are the analytical results for sample(s) received by the laboratory on January 06, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 laceAnalytical" www.pacefabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92231740 Indiana Certification IDS 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Charlotte Certification IDs 9800 Kincey Ave, Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Kentucky UST Certification #: 0042 Louisiana/NELAP Certification #: 04076 Ohio VAP Certification #: CL-0065 West Virginia Certification #: 330 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VifginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 ll�laceAnalj4ical" www,pacef2bs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 SAMPLE ANALYTE COUNT Project: Eastern Automotive Pace Project No.: 92231740 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92231740001 OUTFALL NO. 1 EPA 1664E CLW 1 PASI-C EPA 80 15 Alcohol -Glycol TMW 1 PASI-I EPA 200.7 JMW 1 PASI-A SM 2540D TEP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 �acviAnalyticale www.pacelabs.com r ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Eastern Automotive Pace Project No.: 92231740 Sample: OUTFALL NO. 1 Lab ID: 92231740001 Collected: 01/05/15 08:30 Received: 01/06/15 10:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 01/07/15 07:29 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 01/08/15 13:49 107-21-1 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead ND ug/L 5.0 1 01/07/15 15:00 01/08/15 16:30 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 7.5 mg/L 3.3 1 01/07/15 06:37 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 4of12 laceAnalyfical" ww..pacWa ls.corn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Project: Eastern Automotive Pace Project No.: 92231740 QC Batch: GCSV119988 OC Batch Method: EPA 1664B Associated Lab Samples: 92231740001 METHOD BLANK: 1364601 Associated Lab Samples: 92231740001 Parameter Units Total Petroleum Hydrocarbons mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 01107l15 07:18 LABORATORY CONTROL SAMPLE 4 LCSt7: 1364602 1364603 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg1L 20 17.4 16.9 87 84 64-132 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 laceAnalytical" www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92231740 QC Batch: GCSV/13983 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92231740001 METHOD BLANK: 1219279 Associated Lab Samples: Parameter Units Ethylene glycol mg/L LABORATORY CONTROL SAMPLE: 1219280 Parameter Units Ethylene glycol mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 01/0811512:54 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 23.3 93 49-139 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 /ace Analytical wwwpacelahs.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92231740 QC Batch: MPRP/17668 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92231740001 METHOD BLANK: 1364956 Associated Lab Samples: 92231740001 Parameter Units Lead ug/L LABORATORY GONTROL SAMPLE: 1364957 Parameter Units Lead ug/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 01/08/1514:48 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 500 486 97 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364958 1364959 MS MSD 92231527001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L 0.0091 500 500 496 504 97 99 70-130 2 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364960 1364961 MS MSD 92231643001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Lead uglL <5.0 500 500 482 475 96 94 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 7of12 /YaceAnalytical r www.pacel,,ibs.com r QUALITY CONTROL DATA Project: Eastern Automotive Pace Project No.: 92231740 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 QC Batch: WET135116 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92231740001 METHOD BLANK: 1364590 Matrix: Water Associated Lab Samples: 92231740001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 01/07/15 06:22 LABORATORY CONTROL SAMPLE: 1364591 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 252 101 90-110 SAMPLE DUPLICATE: 1364592 92231940001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 12.4 12.4 0 SAMPLE DUPLICATE: 1364593 92231965001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL &0 8.6 7 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 1�' aceAnalyfical xnvw.pawl3bs'= Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Eastern Automotive Pace Project No.: 92231740 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylliydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 01 /30/2015 07:01 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytical" .7 www.pacefabs.wrn Pace Analytical Services, Inc. 9800 Kircey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Eastern Automotive Pace Project No.: 92231740 Lab ID Sample 1D QC Batch Method QC Batch Analytical Method 92231740001 OUTFALL NO. 1 EPA 1664E GCSV/19988 92231740001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol GCSV/13983 92231740001 OUTFALL NO. 1 EPA 200.7 MPRP/17668 EPA 200.7 92231740001 OUTFALL NO. 1 SM 2540D WET/35116 Date: 01/30/2015 07:01 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP115907 Page 10 of 12 r ' ., aceAll��lytr'ca!' Document Name: Document Revised: September U. ZU1a Condition Upon Receipt (SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name:;4 - Ei n A 5,)Ut it/ f C5 Courier: Fed Ex ❑ UPS❑ USPS❑ Client❑ Comm 'a Pace Other `- ..�•.:'Y CustodySeal on Cooler/Box Present: Rr, f;49, n t9" ° ❑ �ubble es no Seals intact: ❑ yes [`�'—r��" � ��.��,U�j?,;�;ity�cs Packing Material: ❑ Bubble VDPL❑ None ❑ Other Thermometer Used: IR Gun 401 Type of Ice: et Blue done 4.,�p�1,e,ling process has begun Temp Correction Factor T No Correction Corrected Cooler Temp.:C • Biological Tissue is Frozen: Yes No A Temp should be above freezing to 6'C Comments: pate and Initiais garsoq exa nlritj/ contents: Chain of Custody Present: s ❑No 1. Chain of Custody Filled Out: NI Chain of Custody Relinquished: `f I es NrA 3. Sampler Name & Signature on COC: es ONIA 4. Samples Arrived within Hold Time: es ❑No ❑ 5. Short Hold Time Analysis (<72hr): Dyes QN A 6. Rush Turn Around Time Requested: Dyes C> IA 7. Sufficient Volume: es o lqbwx B. ON l Correct Containers'Used: �101N� -Pace Containers Used: NIA 9. Containers Intact: ❑No ❑NIA 10. Filtered volume received for Dissolved tests Dyes ONO 1. Sample Labels match COC: s ❑No ❑NIA -Includes daleltime/1D/Analysis Matrix: 1 , All containers needing preservation have been checked. es ❑No A Ali containers needing preservation are found to be in Yes ❑No compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) EVes ONO 13. Samples checked for dechlorination: Dyes ❑No • r 14. Headspace in VOA Vials (>6mm): Dyes ❑NIA 15 Trip Blank Present: Dyes ONO 04 A Trip Blank Custody Seals Present Dyes ❑No ❑NIA Pace Trip Blank Lot # (if purchased): Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Comments/ Resolution: SCURF Review: Date: I I " if Date/Time: SRF Review: c I jDate: I Note: Whenever there is a discrepancy a ed ing North Carolina compliance samples, a copy of this form will be sent to the Norlh Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) _.WO# � 922��174yO M" 92231740 Page 11 of 12 �7;alceAnalj4ijoal- W—Pak`I.ascc- tion A Arad Client Information: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately, Section 8 Section C Required Project information: Invoice Information: N N (O Page: of panr. Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman (choffman@maaonline.com) Anemia[ Chuck Hoffman OW 409 Rogers'rew Court -^Qr To Joanna Crow ocrow(mmaaoniine.com) Company Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 Address: 409 Rogers View Court, Raleigh, NC i NPOEs i GROUND WATER r- DRINKING WATER i— UST f-• RCRA I— OTHER t To: choffman@rnaaonline.Com Purchase Omer No.: R2057.00 Pace Ovate — Reference: M7 919-250-9918 F- 919-250-9950 Project Name: Eastern Automotive Panag Project KeveRi +erritsg � She Location STATE: NC jested Due DatolTAT: Standard Project r: J� Numbe2D57,Qfl Pau Pmfde x. � 1: y Requested Analysis Filtered (YIN) Section D Valid Matrix Codes a z RegUlrod client Information MATRIX �Df c 2 COLLECTED Preservatives `a N Y N Y ORwgMG WATER Ow WATER WT e O Q7 WASTEWATER 4VMr PROOIXT P " g V m COMPOSITE START COMPOSITE ENOAGRAS W co Z 500.1SO1Jt5 Si a 7 Z5 r on, at SAMPLED � VIP ,y CO �? U {n w ~ m L) O m i '1 (+•Z OSI,.) oTMFR oT p w a Z ~ O S �� Sample 1Ds MUST eE UNIQUE TIME T5 0 V 1 v� 0 U ` a a 61~ m a }% of �C i! y GATE TIME DATE TIME H 2 Z Z d y F uJ m �' Pace Project NoJ Lab I.D.11 Outfall NO. 1 WT G - 7 41 1 1 2 1 1 1 x x x x Rainfall (inches): 5 p -r . t 5 t5 �3a°rr F S 5 S4ay. H: to Ct ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BYIAFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE � °o w m � m PRINT Name of SAMPLER: d4 V 'EDATE $ n2 w I �J �7 SIGNATURE of SAMPLER: ID1YYy: I � � m _ 8 y {M. 1�1i c� •ImPOAant Note: By Signing this form you are accepting Pace's NET 30 day paymelR terms and agreeing to Isle charges of 1.5% per month for any invokes not paid within 30 days. F-ALL-0-020rev.08, 12-Oct-2007