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NCG100024_MONITORING INFO_20170612
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. �V Cc DOC TYPE El HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ q01 r7 bLQ 1 a YYYYMMDD Md Atlantic Enginuaring 8 Environmental Solutions May 18, 2017 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS FOSS AUTO RECYCLING 1915 RIDDLE ROAD DURHAM, DURHAM COUNTY, NORTH CAROLINA PERMIT NCGIO0024 MID -ATLANTIC JOB NO.00OR2066.00 To Whom It May Concern: 409 Rogers Vic* Court Raleigh. NC 7 76 10 office 919.250 99I a facsim;le 919 250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected on April 26, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were below their respective benchmark values or within their benchmark range. If you have any questions or need additional information, please contact me at 919-250-9918 Sincerely, MID -ATLANTIC ASSOCIATES, INC. ?'� �� k S 7e - - a � Ron J. Davis Stormwater Services Manager Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100024 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Foss Recycling, Inc. Durham NC PERSON COLLECTING SAMPLE(S) Anthony Smith CERTIFIED LABORATORY(S) Pace Analytical Lab #12 Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Durham PHONE NO.(800) 672-9722 PLEASE REMEMBER TO SIGN ON THE REVERSE —) For sampling periods with no discharge, you must submit this discharge monitoring farm noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 04/26/17 6.0 8.1 12.3 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons di ctly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware tha re ar"ignificantBenat�s for submitting false information, including the possibility of fines and imprisonment for knowing violations." ;nature o .IPe ttee or (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 e aceAnalytical WW..pacelabs,mm May 10, 2017 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 Dear Chuck Hoffman: Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. e;PCCRFO TNi l9e`RAjp REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical e w�vw,pacelabs.00m Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 Indiana Certification IDs 7726 Moller Road, Indianapolis, 1N 46268 Illinois Certification #: 003971 Indiana Certification #: C-49-06 Kansas/NELAP Certification #:E-10177 Kentucky UST Certification #: 80226 Kentucky WW Certification #:98019 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 20078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL-0065 Oklahoma Certification #: 2016-075 Texas Certification #: T104704355-16-10 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit M P330-16-00257 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 (�IaceAnalytical www.pacelabs.tom Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 Lab ID Sample I❑ 92338561001 Outfall No. 1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol RID 1 PASI-I EPA6010 SH1 1 PASI-A SM 2540D MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 I eAnalytical xnnr.pacelebs.cam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 Sample: Outfall No. 1 Lab ID: 92338561001 Collected: 04/26/17 08:30 Received: 04/27/17 09:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 5.0 1 05/01/17 07:12 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 05/04/17 14:16 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 05/0211711:30 05/09/1716:52 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 12.3 mg/L 8.3 1 05/02/17 10:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05110/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical www.pacelabs.com Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 QC Batch: 358573 QC Batch Method: EPA 1664B Associated Lab Samples: 92338561001 METHOD BLANK: 1988785 Associated Lab Samples: 92338561001 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 05/01/17 06:52 Pace Analytical Services, LLC 9900 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 LABORATORY CONIROL SAMPLE: 1988786 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.2 96 64-132 MATRIX SPIKE SAMPLE: 1988787 92338516002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 21.6 97 64-132 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytical Wow.pawai* com QUALITY CONTROL DATA Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 QC Batch: 385237 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92338561001 METHOD BLANK: 1776642 Matrix: Water Associated Lab Samples: 92338561001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L ND 5.0 05/04/17 12:45 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1776643 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 29.6 118 41-162 r MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1776877 1776878 MS MSD 60243312001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 29.6 30.8 116 120 20-172 4 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 0 IacleAnalyfical (�waw.pacafabs.com QUALITY CONTROL DATA Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 QC Batch: 358609 Analysis Method: EPA6010 OC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92338561001 METHOD BLANK: 1988897 Associated Lab Samples: 92338561001 Parameter Units Lead ug/L LABORATORY CONTROL SAMPLE: 1988898 Parameter Units Lead ug/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 05/09/1716:46 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 455 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1988899 1988900 MS MSD 92338561001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Lead ug/L NO 500 500 465 422 93 84 75-125 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 laceAnalyticalo wwwpacefabs,com QUALITY CONTROL DATA Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 QC Batch: 358767 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92338561001 METHOD BLANK: 1989668 Associated Lab Samples: 92338561001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1989569 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 0510211710:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 248 99 90-110 SAMPLE DUPLICATE: 1989670 92338369003 Dup Parameter Units Result Result Total Suspended Solids mglL 100 104 SAMPLE DUPLICATE: 1989671 92338713004 Dup Parameter Units Result Result Total Suspended Solids mg/L 164 157 RPD Qualifiers 4 RPD Qualifiers 4 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This repon shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 (�IaceAnalyticale WWW.pecelabs.own QUALIFIERS Project: Foss Recycling, Inc- Durham Pace Project No.: 92338561 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 0 aceAnalytical ~. pecelahs ow QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Foss Recycling, Inc- Durham 92338561 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92338561001 Outfall No. 1 EPA 1664E 358573 92338561001 Outfall No. 1 EPA 8015 Alcohol -Glycol 385237 92338561001 Outfall No. 1 EPA 301CIA 358609 FPA6010 358879 92338661001 Outfall No. 1 SM 2540D 358767 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2017 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: Sept. 21, 2016 e �80AMXkal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS•033-Rev.01 Pace Quality Office Laboratory receiving samples: Asheville [] Eden❑ Greenwood Huntersvik±,L Raleigh[] Mechanicsville[] - Sample ++ Client Name: kecelpt{'� , j Protect Courier: ed Ex ❑UPS ❑USPS ❑Client ❑ Commercial ❑Pace ❑Other: Custody Seal Present? Dyes \-4No Seals Intact? []Yes W0#:92338561 1111111111111111 92338561 Date/Initials Person Examining Con, iN' � % I Packing Material: ❑bubble Wrap N:�8ubble Bags [-]None ❑Other: Thermometer: —T f� Gun ID: 1 1� Type of Ice; et []Blue ❑None c /i_.iSamples on Ice, cooling process has begun eF1� r�f�,b N A Correction Fa or; Cooler Temp Corrected ('C}: �- � Biological Tissue Frozen? ❑Yes �" ❑ / Temp should be above f ezing to 6'C USDA Regulated Soil /A, water sample) Did sampl originate in uarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (In�ter�tionaliy, MYesc Eo including Hawaii and Puerto Rico)? ❑Yes ' ]]W Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (02 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers intact? Samples Field Filtered? Sample Labels Match COC? -Includes Date/rime/ID/Analysis Matrix:oAr Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: No ❑N/A 1. ONO ❑N/A 2. N/A 3. }Na fro ❑N/A 4. ONO ❑N/A 5, [:]No No ❑N/A ❑N/A 6. No ❑N/A 7. [:]No 9/A 1 8. Note if sediment is visible in the dissolved container []NO ❑N/A Dyes ❑No /A 14. ©Yes dbN 11. Oyes ONO C ft Field Data Required? ❑Yes ❑No Date/Time: Date: L�� Date: as® Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 11 of 13 m c<Dn N O w 3 m a 0 v rn m m e ra S a 0 a n ro. 2 �> Q v m �- rn � fD A. �• ii O Ott a a c � O � m � d fD N -1 { R w � 0 ro � o_ 0 M u7 D 3 O 3 m 0 G — a M ro � w c 67 a w w Y w o to OC .1 a, N a w N Y Itemp zzzzzzzzzzzz BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) SP3U-250 mL Plastic Unpreserved (N/A) MU-500 mL Plastic Unpreserved (N/A) 8P1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2SO4 (pH < 2) (Cl-) BP3N-250 mL plastic HNO3 (pH < 2) BP32-250 mL Plastic ZN Acetate & NaOH (>9) zzzzzz BP3C-250 mL Plastic NaOH (p H > 12) (Cl-) WGFU-wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) Z, AGSH-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2504 (pH < 2) AG35-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(CI-) D69H-40 mL VOA HCI (N/A) VG9T-40 mLVOA Na2S203 (N/A) (JI VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK 16 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit�VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A — lab) SP2T-250 mt. Sterile Pia stic (N/A —lab) BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) GN 6 N t{b rr O B = C. =- o nl m 7 -" vt CL IN 3. Cr 'O 0 jr _3 X (A r► rD O m Ln s� G lu 3 a rl f6 DJ r o vi r -0 Z x CC1 ID n ace Analytical CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-of-Cusiody is a LEGAL DOCUMENT All relevant fields must be completed accurately. Section A Section 8 Section C Page of f9 Required Clienl Infanm TTalion Required PMMCl Inforalion Invoice m hilolatron, d 11 Company Mid -Atlantic Associates. Inc. Report To: Chuck Hoffman (choffman@maaonline.com) AlienUOn Chuck Hoffman Aodres.S 409 Rogers View Court Copy To Ron Davis (rdavis@rnaaonline.com Company Na-- Mid-Attantic Associates. inc. REGULATORY AGENCY Raleigh, NC 27610 Address 409 Rogers View Court. Raleigh, INC — NPDES r GROUND W I- UST i RCRA TER ^ DRINKING WATER OTHER Email To choffman@maaonline.eom Purchase Order No. R2066.04 Pace Q11ple -- Reference Phone. 919-250-9918 Fax 919-250-9950 Project Name. Foss Recycling, Inc. - Durham Ppce IMojen Nicole GasiorOwski Site Location Menager, STATE: NC Requested Due DatefTAT: standard PmleCl NUTTIDer. R2066.00 Task 40G00 Pace Requested Analysis Filtered (YIN) Section D Valid Matrix Codes z Requtmd Chem Infc—d— MATRIx GORE o a COLLECTED Preservatives 's N Y N Y DR.'tl WAIER OW O z WATER WT WASTE WATER WL'y PRODI/CT P U d! cdvaoSaT!_ START r.OWO&TE Ct1➢VGRA° O C~.1 m SORJSLILID sL J J y _ QI y SAMPLE ID E Wp Q W In `D o AR (A.Z.0-91; ) orr�R UT ¢ IL z a T Sample 3Ds MUST BE UNIQUE TMSUE i5 O 0. FF4 d st L L7 U x j r J Z O U h m C c N ?' ID c p a If O �,5 3V S(v L o w DATE TIME DATE TIME u 7 2? 2 2 i O a- J Pace Project NoJ Lab I.D. 1 Outfall No. 1 11 c I 1 7 a 1 1 z 1 x x x x Rainfall (inches): P61 2 H: 3 4 5 6 7 B 9 10 11 12 ADDITIONAL COMMENTS AFFILIATION RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEP ED BY 1 AFFI TtON DATE ' TIME SAMPLE CONDITIONS `` /7 SAMPLER NAME AND SIGNATURE u -0 a W E vz m` Y PRINT Name of SAMPLER: �. t�j l y� m z V a E A SIGNATURE of SAMPLER; DATE Signed ,yVl 'impenam N°ic. ey sgm..g Iho lore yo„ me ac Wrig Axes NET 30 day paymem 1— one agreeing 10 We Mrgcs or 1.5% per rnmlie rur any,muces ;b Pala .�D,ie �D c, F-A'-Q-02Crev.D8, 12.001-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100024 SAMPLES COLLECTED DURING CALENDAR R: 2014 (This monitoring report shall be received b ivis' later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Foss Recycling, Inc., Durham, INC COUNTY Durham PERSON COLLECTING SAMPLE(S) Anthony Smith PHONE NO. (800) 672-9722 CERTIFIED LABORATORY(S) Pace Analytical Lab # 1.2 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring farm noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic prganics3, mg/L Benchmark i - - 6.0 — 9.01 100/50, 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 11/17/14 0.5 7.8 24.0 <5.0 <10.0 <0.0050 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Monogement Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) -fir Title (Prin ti e) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dire y responsi or gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that t r are sigpirigark penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." or.09'signeej (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 HUM Atlantic Engineering & Environmental Solutions December 9, 2014 +��C��VCU NCDENRIDWQ CU Attention: Central Files AOG 2 4 2015 1617 Mail Service Center CENTRAL FILES Raleigh, North Carolina 27699-1617 DWR SECTION Subject: STORMWATER SAMPLING RESULTS FOSS AUTO RECYCLING 1915 RIDDLE ROAD DURHAM, DURHAM COUNTY, NORTH CAROLINA PERMIT NCGIO0024 MID -ATLANTIC JOB NO. OOOR2066.00 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected on November 17, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were below their respective benchmark values or within their benchmark range. If you have any questions or need additional information, please contact me at 919-250-9918 Sincerely, MID -ATLANTIC ASSOCIATES, INC. c� Q�- Charles B. Hoffman, PG Project Geologist Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report !ceAna1j&a1' www.pacefabsxarn r November 25, 2014 Darin McClure Mid Atlantic Associates, Inc. RE: Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 Dear Darin McClure: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNi standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytical vnnepacelabs.com Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification l0s 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Kentucky UST Certification #: 0042 Louisiana/NELAP Certification #: 04076 Ohio VAP Certification #: CL-0065 West Virginia Certification #: 330 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 Ic eAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Foss Recycling. Inc - Durham Pace Project No.: 92226130 Pace Analytical Services, Inc. 9800 Kincey Ave- Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92226130001 Outfall No. 1 EPA 1664E CLW 1 PASI-C EPA 8015 -Alcohol-Glycol DMT 1 PASI-1 EPA6010 JMW 1 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 ace Analytical —pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 Sample: Outfall No. 1 Lab ID: 92226130001 Collected: 11/17/14 09:00 Received: 11/18/14 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg1L 5.0 1 11/21/14 10:08 8015M Glycols in water Analytical Method: EPA 8015 -Alcohol-Glycol Ethylene glycol ND mg/L 10.0 1 11/20/14 22:31 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug1L 5.0 1 11/19/14 16:10 11/20/14 06:16 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 24.0 mg1L 12.5 1 11/20/14 17A7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalytical ' www.pacelabs.com QUALITY CONTROL DATA Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 QC Batch: GCSV119571 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92226130001 METHOD BLANK: 1335595 Associated Lab Samples: 92226130001 Parameter Units Total Petroleum Hydrocarbons mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/21/14 09:54 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 hunlersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1335596 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL 20 17.8 89 64-132 MATRIX SPIKE SAMPLE: 1335597 92226171001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 16.9 84 64-132 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /25/2014 0316 PM without the written consent of Pace Analytical Services, Inc,. Page 5 of 12 aceAnalytical www.pacelabs.com Project: Foss Recycling, Inc - Ourham Pace Project No.: 92226130 QC Batch: GCSV113524 QC Batch Method: EPA 8015 - Alcohol -Glycol Associated Lab Samples: 92226130001 METHOD BLANK: 1192335 Associated Lab Samples: Parameter Units Ethylene glycol mg/L LABORATORY CONTROL SAMPLE: 1192336 Parameter Units Ethylene glycol mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 8015 - Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result limit Analyzed Qualifiers ND 10.0 11/20/14 21:35 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 256 102 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1192337 1192338 MS MSD 92225933001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L ND 250 250 249 257 99 103 67-133 3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical r www.pacelabs.com Project: Foss Recycling, Inc - Durham Pace Project No.; 92226130 QC Batch: MPRP117384 QC Batch Method: EPA 3010 Associated Lab Samples: 92226130001 METHOD BLANK: 1334135 Associated Lab Samples: 92226130001 Parameter Units uglL Lead LABORATORY CONTROL SAMPLE: 1334136 Parameter Units Lead ug1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/20/14 05:42 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 500 461 92 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1334137 1334138 MS MSD 92225784001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Lead ug1L 24.5 500 500 465 461 88 87 75-125 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 QC Batch: WET134380 Analysis Method: SM 2540D QC Batch Method: SM 25400 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92226130001 METHOD BLANK: 1335352 Associated Lab Samples: 92226130001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: Parameter 1335353 Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1335354 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1336355 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/20/1417:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 230 92 90-110 92225937001 Dup Result Result 2640 2740 92226135013 Dup Result Result ND ND RPD Qualifiers 4 RPD Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical 1 www.pacefabs.com QUALIFIERS Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitalion Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyt ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASW Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytrcal 1r www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Foss Recycling, Inc - Durham Pace Project No.: 92226130 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92226130001 Outfall No. 1 EPA 1664E GCSV119571 92226130001 Outfall No. 1 EPA 8015 - Alcohol -Glycol GCSVl13524 92226130001 Outtall No. 1 EPA3010 MPRP117384 EPA6010 ICPI15666 92226130001 Outfall No. 1 SM 2540D WET134380 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 14/25/2014 03:16 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 •• �l°c�CEftlk7fyflCc71 Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: u fa- ,4fq c, n 4-, Courier: ❑ Fed Ex ❑ LIPS❑ LISPS[] Client❑ Commercial❑ Pace Other Custody Seal on Cooler/Box Present: ❑ yes ❑ono Seals intact: ❑ yes ❑ no f{� �x ' 1,055V ., Packing Material: B Bubble VDp [Bubble Bags ❑ None ❑ Other ,,---,, � Thermometer Used: IR Gun 1 1 Type of Ice: et Blue None LYSamples on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Tern 3 •C p Temp should be above freezing to 6°C Biological Tissue Is Frozen: Yes No NIA Comments: date and Initials of person examining contents: I► lrh% _ Chain of Custody Present: Crres ONO ❑NIA 1. Chain of Custody Filled Out: Dyes Galo ❑NIA 2. JJ a cA.& k HWV Chain of Custody Relinquished: l�res ONO ❑NIA 3. 13�0 f-�� Say n/ 11 "4 (�i°+ Q r+n. Sampler Name & Signature on COC: 2<es ONO ❑NIA 4, Samples Arrived within Hold Time: 13 rea ❑No ❑NIA 5. Short Hold Time Analysis (<72hr): Dyes 29', ❑NIA 6. Rush Turn Around Time Requested: Ono ❑. ❑NIA 7. �Yeses Sufficient Volume: r /ram/+'ilaYes N ❑NIA S, 01111( I`Cu.vt( I 0& 6—a+k-1 - Correct Containers Used: -Pace Containers Used: /Yes ❑No ❑Yes Ono ❑NIA ❑NIA 9. Containers Intact: Yes ONO ❑NIA 10, Filtered volume received for Dissolved tests Dyes ONO 0N'1A 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: s ❑No ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, ooliform, TOG, O&G, wl-DRO (water) Eyes ❑No �es ONO �,�� I.d Yes [IN. ❑NIA ❑NIA 13, Samples checked for dechlorination: 11 Yes ❑No NIA 14. Headspace in VOA Vials >6mm : Ye ©No NIA 15. 1l Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): Dyes ❑No Dyes ONO NIANIA ONA 16. Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: R 0 ((-iVV.t Vj DatelTime: 11 1616 Comments/ Resolution; ^ j/; I: n)i� o(W (7 f1 _l.y� SCURF Review: U'' W jDate: It y W®# ; 9222613- SRF Review: �`i( Date: �' Note: Whenever there Is a discrepancy affecting North Carolina compliance IIfIIlIIl11I11Ifllll samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, 92226130 incorrect containers) Page 11 of 12 aceAnalXical -J.1%ars01C . Ction A quires Client In:armatiors CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant Gelds must be completed aeiaratety. Section B Section C Required Project IMartnation; Invoice Information: N Page: of mpany: Mld-.+Gamic Associates, Inc. Report To; Chuck Hoffman (Choffman ?maaonllne.com) Attenton: Chuck Hoffman dress: 409 Rogers View Court copy Ta Joanna Crow (icrow@maaonline.com) Company Name: Mid -Atlantic Associates, inc. REGULATORY AGENCY Raleigh, NC 27610 Address: 409 Rogers View Court, Raleigh, NC r- NPOES r GROUNDWATER r DRINKING WATER F- UST f RGRA )— OTHER iaa Tv rhoffman@rnaaonline.com Purchase Order Na: R2066.04 PaCe Qj Ke - Reference: 919-250-9918 919-250-9950 project Name: Foss Recycling, Inc. - Durham P-- "eO Kevin Herring Site Location heanaw. STATE: NC Quested Due DatarrAT: Snndard Project Numtler. R2066.00 Task 40000 puce PSO�'O s: — Requested Analysis Fittered (YIN) Section D Valid Matrix Codes a E. a Rvquirad Came Information MATRI COLLECTED Preservatives y N Y N Y DRNW° *WATER OW - F m WATER Wr $ V O WAST£ WATrF Ww to COLO-O&TE COMPOSITE PROOLICT P START FNOIGRAe softJSOw er. > z v Y Oft m SAMPLE ID +� W° p o rn I rn c° p U (A-z 0-9i OTHER or 4 w a ,.y Sample tOs MUST BE UNIQUE TISSUE TS U a F y t C0 u x W ,�,� d O g c F a �t222r ti3 a CL IL L ° o L _ e H DATE TIME DATE TIME a 2 = i Z O Q 0. tx Pace Project Nol Lab I.D. f Outfall No. 1 wr G 7 4 1 1 t 1 21 x I x x I x I I Rainfall (inches): 2 H: 3 4 5 5 7 8 9 ID E1 2 ADDtT1ONAL COMMENTS RELINQUISHED BY AFRUATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 4 -7 L-" I -l5- t (1 .: [(.Uv 3.Y !J Y SAMPLER NAME AND SIGNATURE r� 8z v m m� PRINT Name of SAMPLER: n SIGNATURE of $AMPEER: r Igned~IX �/�.� TM� O - - _ �v-gn' — 4�1 v r Important Note: By algning Wa forth you are wopt++g Paee'a NET 30 day payment tams and agraeinp to We charges d 1.5% per momh fu any Invoices not paid "WA 30 a F-ALL-0-020rev,08, t 2-Oct-2907 slid Atlantic Engineering & Environmental Solutions March 11, 2014 NCDENR/DWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS FOSS AUTO RECYCLING 1915 RIDDLE ROAD DURHAM, DURHAM COUNTY, NORTH CAROLINA PERMIT NCGl00024 MID -ATLANTIC JOB NO. OOOR2066.00 To Whom It May Concern: REECEIVF® Nov 10 2014 CENTRAL FILES DWR SECTION 409 Rogers View Court Raleigh, NC 27610 office 919.250,9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected on February 18, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. All parameters were below their respective benchmark values or within their benchmark range. If you have any questions or need additional information, please contact me at 919-250-9918 Sincerely, MID -ATLANTIC ASSOCIATES, INC. et. I - Charles B. Hoffman, PG Project Geologist Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGIO0024 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Foss Recycling, Inc. Durham, NC COUNTY Durham PERSON COLLECTING SAMPLE(S) Anthony Smith PHONE NO. (800) 672-9722 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE �l Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall . No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023`" 01051 78141 pH, Standard Units Total'Sdspended' Solids (TSS), mg/L -..,. Non=polar,,., O&G/TPH (Method 1664 SGT-H.EM)mg/:L . Ethylene..Glycol, mg/L :Lead, Total. Recoverable,^ mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.o 100/502 15 8 000.. ` (Tiers 2 and.3). 0.03` 1.0 Outfall001 02/18/14 1.5 7.6 6.2 <5.0 <10.0 <0.0050 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." I t �t *UY iw�� Name (Print name) Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel props gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons re ctly responsihl o athering the information, the information submitted is, to the hest of my knowledge and belief, true, accurate, and complete. i am aware th there are signipfarXpenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature/off ermittee or v �O r / (Date} Form SW U-251, last revised October 25, 2012 Page 2 of 2 aceAnalytical wwwpacelahs.com February 26, 2014 Beverly Oglesby Mid Atlantic Associates, Inc. 409 Rogers View Court Raleigh, NC 27610 RE: Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Dear Beverly Oglesby: Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Jon D Bradley jon.bradley@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Darin McClure, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 acmnalytical +w+w.pacOahs.com Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Kentucky UST Certification #: 0042 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Louisiana/NELAP Certification #: 04076 Ohio VAP Certification #: CL-0065 Pennsylvania Certification #: 68-04991 West Virginia Certification #: 330 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 aceAnalyticaI WW..pacefabs.com Project FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 Lab ID Sample 1D 92190076001 OUTFALL Net SAMPLE ANALYTE COUNT Method EPA 1664B EPA 8015 - Alcohol -Glycol EPA 6010 SM 2540D REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Anatytrcal Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Analysts Reported Laboratory CLW 1 PASI-C CEM 1 PASI-I JMW 1 PASI-A WRC 1 PASI-A Page 3 of 13 aceAnaIXical wmepscelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc, 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875.9092 Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 Sample: OUTFALL N01 Lab ID: 92190076001 Collected: 02/18/14 12:00 Received: =19114 09:40 Matrix: water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 1664 SGT-HEM, TPH Analytical Method: EPA 1684E Total Petroleum Hydrocarbons ND mg1L 5.0 1 02/21/14 09:30 8015M Glycols In water Analytical Method: EPA 8015 -Alcohol-Glycol Ethylene glycol ND mg1L 10.0 1 02/21/14 19.40 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug1L 5.0 1 02l20114 10:40 02/21/14 20:18 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 6.2 mg/L 2.6 1 02/25/14 15:08 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/26/2014 03:37 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 aceAnalXical wwwpacefabs.com Project: FOSSAUTO RECYCLING DURHAM Pace Project No.: 92190076 QC Batch: GCSV116720 QC Batch Method: EPA 16648 Associated Lab Samples: 92190076001 METHOD BLANK: 1141757 Associated Lab Samples: 92190076001 Parameter Units Total Petroleum Hydrocarbons mg1L LABORATORY CONTROL SAMPLE: 1141758 Parameter Units Total Petroleum Hydrocarbons mg/L Date: 02/26/2014 03:37 PM QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 02/21/14 09:29 Spike LCS Cone. Result 20 16.9 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 84 64-132 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 13 acmnalytical wwwpacdahs.com QUALITY CONTROL DATA Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 Pace Analytical Services, Inc. 9800 Kincey Avo. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: GCSV112145 Analysis Method: EPA 8015 - Alcohol -Glycol QC Batch Method: EPA 8015 - Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92190076001 METHOD BLANK: 1051466 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg1L NO 10.0 02/22/14 13:54 LABORATORY CONTROL SAMPLE: 1051467 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg1L 250 255 102 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1051468 1051469 MS MSD 92190076001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L NO 250 250 247 247 97 97 67-133 0 Date: 02/26/2014 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 aceAnalytical —pacelahs.=n I Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 QC Batch: MPRPI15271 QC Batch Method: EPA 3010 Associated Lab Samples: 92190076001 METHOD BLANK: 1141178 Associated Lab Samples: 92190076001 Parameter Units ugfL Lead QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 02121/1419:08 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE:: 1141179 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 484 97 80-120 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE; 1141180 1141181 MS MSD 92190006008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug1L 35.7 500 500 510 508 95 94 75-125 0 Date: 02/26/2014 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 aceAnalytical www.pacelaDs.cam 1 Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA Project: FOSS AUTO RECYCLING DURHAM Pace Project No.: 92190076 QC Batch: WETl29688 QC Batch Method: SM 2540D Associated Lab Samples: 92190076001 METHOD BLANK: 1144769 Associated Lab Samples: 92190076001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1144770 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 1144771 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1144772 Parameter Total Suspended Solids Date: 02/26/2014 03:37 PM Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 02/25/1415:01 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 268 107 80-120 92190015002 Dup Units Result Result mglL 18.0 19.0 92190047001 Dup Units Result Result mglL ND ND RPD Qualifiers 5 RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8of13 aceAnaIXical www.pecelabs.=n QUALIFIERS Project: FOSSAUTO RECYCLING DURHAM Pace Project No.: 92190076 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28070 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2- Dip henylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TN I accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte PAST -I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/26/2014 03:37 PM without the written consent of Pace Analyticat Services, Inc.. Page 9 of 13 aceAnalytical www.pacefabs.= QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: FOSS AUTO RECYCLING DURHAM 92190076 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92190076001 OUTFALL N01 EPA 1664E GCSV116720 92190076001 OUTFALL N09 EPA 8015 - Alcohol -Glycol GCSV112145 92190076001 OUTFALL N01 EPA3010 MPRP115271 EPA6010 ICP113856 92190076001 OUTFALL N01 SM 2540D WET129688 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/26/2014 03:37 PM without the written consent of Pace Analytical Services, Inc.. Pagel 0 of 13 �• ��rf l?1ceAr�aly�lcar le Condition Upon Receipt (SCU Document Number: F-C H R-C S-03-rev.13 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Client Name:-Wlb Courier: Fed Ex ❑ ups[]USPS❑ Client❑ m❑ Pace Other Comercial "' ? Ofianal'. Duebate , Custody Seal on Cooler/Box Present: ❑ yes Q/no Seals intact: El yes ❑ no g Packing Material: ❑ Bubble Wrap ❑ Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 13 1 Type of lee: L"e Blue None E-8amples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T1301: No Correction Corrected Cooler Temp.:___ �j� C Biological Tissue is Frozen: Yes No NIA Date an tit o examining conten Temp should be above freezing to VC Comments: Chain of Custody Present: es ONO ❑NIA 1. Ye Chain of Custodv Filled Out: lds ONO ❑NIA 12. Sampler Name & Signature on COC: tans ❑No ❑NIA 4. Samples Arrived within Hold Time: eyes ONO ❑NIA 5. Short Hold Time Analysis (<72hr): ❑Yes /dNo ❑NIA 6. Rush Turn Around Time Requested: ❑Yes Ptro ❑NIA 7, Sufficient Volume: OYees ONO ❑NIA 8. Correct Containers Used: -Pace Containers Used: Yes ONO Ores ONO ❑NIA ❑NIA 9. Containers Intact: ❑Yes ON ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ONO 11'NIA 11. Sample Labels match COC: -Inc3udes date/time/ID/Analysis Matrix: o ❑NIA 12. � �`- 15[�ll� DA All containers needing preservation have been checked. yes ONO 1JN1A 1 13. All containers needing preservation are found to be in EPA ❑ s ONO ❑NIA comp)€ance with recommendation. exceptions: VOA, colirorm, TOC, O&G, WI-DRO (water) ❑Yes ❑No Samples checked for dechlorination: Oyes ONO NIA 14, Headspace in VOA Vials (>6mm): ❑Yes IWo ❑NIA 15, Trip Blank Present: ❑Yes ONO EWiA 16. Trip Blank Custody Seals Present ❑Yes ONO C]'NIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: --N)kj I Date: SRF Review: I —�vb I Date: 1 A 14I1 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) I.t Field Data Required? Y 1 N Page 11 of 13 N O W ace Analytical Section A R—imd Gent lrsomratidn: CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields musl be completed accurately. Section R Section C Required Project Infovmacion'. Invoice Information Page: of company- Mid -Atlantic Associates, Inc. Report To: ChUCx Hoffman (choffman@maaonline.com) Atlefltiorl: Chuck Hoffman Address: 409 Rogers View Court COPYTO: Joanna Crow Qerow@maaonline.eom) company Name: Mid -Atlantic Associa,as, inc. REGULATORY AGENCY Raleigh, NC 27610 Address: 409 Rogers View Court, Raleigh, NC r- NPDES r- GROUNDWATER r- DRINKING WATER i UST r RCRR [- OTHER Ernay TO: choffman@maaonlifte.com Purchase Order No.: R2066.04 Pace Quote -- Refaren Ce: Phone. 919-250-991$ Fax: 919-250-9950 Projecl Name: Foss Recycling, Inc. - Durham P00ePmieet Kevin Herring Site Location Manager STA TE: NC Requested Due Data/TAT: Stindard Project Number. R2066.00 Task 40000 Pau Profle a, _ Requested Analysis Filtered (YIN) Section D valid Maki: codes o z Requlred client IAformalion MATRIX CODE o o COLLECTED Preservatives > N Y N Y DRVWRd WATER DW �- U 0dl WATFR WT WASTE WATER WW u v U COMPOSITE ODrapOSITE U Q Z PRODUCT P m START ENDGRAa ul 2 SOdr-Ot4 SL OR. OL of U ee► too Q1 Y } SAMPLE 1D "� _ �? z C An AR (A-Z, 0-9 IA i oTKR os O w < a ¢ Sample [Ds MUST BE UNIQUE TISSUE TS O w z C7 N U x J w u p m T c H 7 72 r d o c�z U� m='Q W a a z A C) a L m DATE TIME DATE TIME U) x z x z z F r. w J Pace Pro]eet NoJ Lab I.D. 1: Outfall 140. 1 111 G - - 7 4 1 21 1 1 x x X1 X1 I I I I I Rainfall (inches): 2 H: 4 5 6 7 8 9 10 ' 11, 12 ADprtIONAL�IAENT9 RELINQUISHED BTlAFFtLIATION DATTc, TIME - ACCEPTED lay!AFFILIATION _ DATE ..,nms -' SAMPLE CONDMONS SAMPLER NAME AND SIGNATURE _ PRINT Name of SAMPLER: Eg I, SIGNATURE of SAMPLER; flATESlel.d a Impw s Neta: lay sjw" v a norm yw we soeeptirgl Pace's NET 30 day Payment terms and agreeing to Iota charges off.$% per mash for"imoius rnt paid etthln 30 days. F-ALL-G-020rev.08, 12-Oct-2007 "�ace Anavicai vnm.parslahs.com Section A Required Client Information; CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fiords must be completed accurately. Section B Section C Required Project Information: Invoice Information: Page: of C-Arlag Report To: Attention; 1bb0311 AAkLin-k'iC Address:,,,, w COPY TO: Company Name: REGULATORY, - -Svc t Cr 2-7 10 Address, NPIDES F- GROUND WATER F- DRINKING WATER F- UST 1- RCRA OTHER Email To: lo Purchase Order No.: Pam Cluote Reference: 4W.- Fax: Project Name: Pa Pa� Project L - c�A zso- Requested Due DaterrAT: Project Number Pace Profile 0: Section D matrix Codes Z COLLECTED Preservatives z T11 RequiredCbent Information MATRIX I CODE Drinking Water DW water WT je 0 C) z Waste Water WW P Product COMPOSITE START COMPOSITE ENO)GKAH U UJ SL soilisolid 0 SAMPLE ID Oij OL Wipe VVP 0 LLr — (A-Z. 0-9 1, Air AR w 0 w - z -0 CD Sample IDS MUST BE UNIQUE Tissue TS Other OT 0 V L< CL LU LU M uJ uJ < 0 U 0) (L LL 2! C% :2 < M M C) CL 0 0 DATE TIME DATE TIME it M M z z 2 ) I . of Project NoJ Lab LD, 1-fuw M I I I I I 2' 3 �P, -4 fir 7) is V710 91 i2 LC mmms'. 'RE NQUtSHEDBYIAFFILIATION'.: D� -i �EPTED2YIAFFiikhdi' f""ADDMON '7- SAMPLE CONDITIONS ' - . ORIGINAL SAMPLER NAME AND SIGNATURE' S PRINT Name of SAMPLER: Akywle e E F- ix E a SIGNATURE of SAMPLER'. (AA-� CATE Signed '�%" (MWDDfYY); 0 U) *Imponant Note: By signIng This form you are accepting Paces NET 30 day payment larms and agreeing to late charges or 1-5% per month for any I* not Paw -ft)p days. F-ALL-Q-020rev.07, 15-May-2007