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HomeMy WebLinkAboutNCG100015_MONITORING INFO_20190612STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V DOC TYPE ❑HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ go) q b 4d I ai YYYYMMDD a id Atlantic Enginaaring6 Environmental Solutions RECEIVED 409 Rogen View Court Raleigh, NC 77510 amce 919,750,9910 lacsimNa 919230.9950 Jib"_J4L207 MAAONLINE.COM CCA,'TR AL FILES May 24, 2019 0Vvn� , I, T1 A) NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11TH STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on May 13, 2019 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 FACILITY NAME Marsh Auto Parts, Inc. - Caryard PERSON COLLECTING SAMPLE(S) Stephen Marsh _ CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023,; 01051, 78141 pH, Standard Units Total Suspended Solids'(TSS), mg/L Non -polar O&G/TPH (Method:1664 SGT-HEM)„mg/L Ethylene Glycol, mg/L head, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 .15 . 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 5/13/19 1.45 6.9 4.8 <2.70 <4.7 <0.00310 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled Stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Sign ure Date Mail Original and one copy to: 'Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee or Designee) (Date) Form SW U-251, lost revised October 25, 2012 Page 2 of 2 ENCO Laboratones Accurate. Timer. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, May 24, 2019 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Car Yard ENCO Workorder(s): CCO2610 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, May 13, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page t of 8 �uco www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ED: Caryard Lab ID: CCO2610-01 Sampled: 05/13/19 11:30 Received: 05/13/19 14:00 Parameter EPA 1664E Preparation EPA 1664E Hold DatelTime(s] 06/10/19 Prep Date/Time(s) 05/13/19 15:43 Analysis Date1T1me(5) 05/17/19 13:56 EPA 6010D EPA 3005A 11/09/19 05/14/19 13:54 05/17/19 10:38 EPA 8015C NA 05/27/19 05/21/19 09:00 05/21/19 13:49 SM 254OD-2011 NO PREP 05/20/19 05/20/19 09:47 05/20/19 09:47 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 �JVCO www.encolabs.com SAMPLE DETECTION SUMMARY :1 Client ID: Caryard Lab ID: CCO2610-01 Anatrte Besuf Flag MU PALL Units Method Mstes Total Suspended Solids 4.8 2.5 2.5 mg/L SM 254UD-20I I FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 0NS�� www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID: CCO2610-01 Received: 05/13/19 14:00 Matrix: Surface Water Sampled:05/13/19 11:30 Work Order: CCO2610 Project: Car Yard Sampled By: Client (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - £NCO Cary cerhfred analyze (NC 591) Analyte rCAS Numberl Results PLIL9 Units 2E K" pQL Difth mrth431 Analyzed ft Notes Lead [7439-92-1]1 0.00310 U mg/L 1 0.00310 0.0100 9E14024 EPA 60101) 05/17/19 1038 7DH Classical Chemistry Parameters ^ - ENCO Cary CL-Itfred analyte (NC 5911 Analyte rCAS Numberl Results Flag Un;ts of Hu E91 "kb Method Analyzed Notes Total Suspended Solids^ 4.8 mg/L 1 2.5 2.5 9E20002 SM 2540D-2011 05/20/19 09:17 LG Non -Halogenated Semivolatile Organics by GC Anahrte 1CAS Numberl Resents E[ag Units pf H" EQL lakh Method Analyzed f[ Notes Diethylene Glycol [ 111-46-6] 4.3 U mg/L 1 4.3 10 9E21008 EPA 8015C 05/21/19 13:49 1]8 Ethylene Glycol[107-21-1] 4.7 U mg/L 1 1.7 5.0 9E21008 EPA 8015C 05/21/19 13:49 318 Propylene Glycol[57-55-6] 4.3 U mg/L 1 4.3 5.0 9E21008 EPA 8015C 05/21/19 13:49 JIB Triethylene Glycol [112-27-6] 6.9 U mg/L 1 6.9 10 9E21008 EPA 8015C 05/21/19 13:49 1]B QL-02 su►rPootes BgiNL Q,E YSA&E Lv! R/o Rec % Rec limits filtm Method An fr Notes 1,3-Butylene Gf -1 200 1 200 99 % 61-125 9E21008 EPA 8015C 0512111913:49 ll8 Classical Chemistry Parameters ^ - ENCO Jacksonville Cer&&d anatyte (NC 4421 Analyte (CAS Numberl Results Elag Qab of M" E91 DA= Method Analyzed $y Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2,70 5.00 9E13011 EPA 1664B 05/17/19 13:56 SMA MaterialA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 CENN www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 5000/7000 Series Methods - Quality Control Balch 9EI4024 - EPA 3005A Blank (9E14024-BLKI) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:35 Spike Source %REC RPD -Anallde Result Flag P-4L Units Level Result %REC Limits RPD Lima Notes Lead 0.00310 U 0.0100 mg/L LCS (9E14024-BS1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:41 Spike Source %REC RPD ,ADaIYIl: Result Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0195 0.0100 mg/L 0.200 98 80-120 Matrix Spike (9E14024-MS1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:46 Source: CCO2610-01 Spike Source %REC RPD Analyte Result Flag POL U its Level Result %REC Limits RPD Limit Notes Lead 0.197 0.0100 mg/L 0.200 0,00310 U 98 75-125 Matrix Spike Dup (9E14024-MSD1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:49 Source:0002610-01 Spike Source "/oREC RPD -Analyte Result flag M Units Level Result °/a REC Limits RPD Limit Notes Lead 0,196 0.0100 mg/L 0,200 0,00310 U 98 75-125 0.2 20 Post Spike (9E14024-PSI) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:51 Source: CCO2610-01 Spike Source %REC RPD .Anal Sde Result flag NX Units Level gRjul %REC Limits RPD LIMA Notes Lead 0.205 0.0100 mg/L 0.200 0.00139 102 80-120 Classical Chemistry Parameters - Quality Control Batch 9E20002 - NO PREP Blank (9E20002-BLK3) Prepared & Analyzed: 05/20/2019 09:47 Spike Source %REC RPD Anal 1t Result F109 FQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2,5 mg/L LCS (9E20002-BS1) Prepared & Analyzed: 05/20/2019 09:47 Spike Source %REC RPD Analyte Result Flag POL units Level Result a/nREC Limits RPD MMA Notes Total Suspended Solids 96 2.5 mg/L 100 96 80-120 Duplicate (9E20002-DUP3) Prepared & Analyzed: 05/20/2019 09:47 Source: CCO5481-01 Spike Source %REC RPD -Analyte Result flag POL Units Level Result °/GREC Limits RPD limit Notes Total Suspended Solids 220 110 mg/L 200 9 20 Duplicate (9E20002-DUP2) Prepared & Analyzed: O5/20/2019 09:47 Source:0006600-01 Spike Source %REC RPD Anal lds Result Elu EQL Units Level Rgsul %REC Limits RPD Limit Notes Total Suspended Solids 110 71 mg/L 120 5 20 Non-Nalogenated Serinivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control LJ Batch 9E21008 - NA Blank (9E21006-BLK1) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 15:23 Spike Source %REC RPD -Anatvte Result Flag P-OL Units Level Result o/nREC Limits RPD Limit Notes Diethylene Glycol 1.3 U 10 mg/L Ethylene Glycol 4.7 U 5.0 mg/L Propylene Glycol 4.3 U 5.0 mg/L Triethylene Glycol 6.9 U 10 mg/L 1,3-SLWene Glycol 110 m9/L 100 i06 61-125 LCS (9E21008-BS3) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 13:11 Spike Source %REC RPD -Analvte Result Flan PQL Units Level Result %REC Limits RPD 1113011 Notes Diethylene Glycol 250 10 mg/L 200 124 61-127 Ethylene Glycol 240 5.0 mg/L 200 119 73-132 Propylene Glycol 190 5.0 mg/L 200 97 74-123 Triethylene Glycol 310 10 mg/L 200 157 44-137 QL-02 1,3-Butylene Glycol 200 mg/L 200 100 61-125 LCS Dup (9E21008-BSD1) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 13:30 Spike Source %REC RPD Anal lde Result E1119 Q91 l nits Level Result %REC Limps RPD LiB1it Notes Diethylene Glycol 240 10 mg/L 200 118 61-127 5 11 Ethylene Glycol 200 5.0 mg/L 200 98 73-132 19 10 QR-06 Propylene Glycol 210 5.0 mg/L 200 104 74-123 8 8 Triethylene Glycol 250 10 mg/L 200 124 44-137 23 16 QR-06 i,3-Butylene Glycol 180 m9/L 100 91 51-125 Classical Chemistry Parameters - Quality Control Batch 9E13011 - EPA 16648 Blank (9E13011-BLK1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source %REC RPD .Analvte Result Flag PQL UNU Level Result %REC Limits RPD 9mit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (9E13011-BS1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source %REC RPO Anal YtS: Result Elag E91 Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 71.7 5.00 mg/L 81.0 88 64-132 LCS Dup (9E13011-BSD1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source %REC RPD .Analvte Result Flag P-QL units Level Result %REC Limy RPD Limp Notes Oil & Grease (HEM-SGT) Non -Polar Material 67.3 5.00 mg/L 79.7 85 64-132 6 34 Matrix Spike (9E13011-MS1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Source: BCO2004-01 Spike Source %REC RPD .Analvte Result Flag POL Units Level quit %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 50.0 5.00 mg/L 74.6 2.70 U 67 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 0�14W www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample. preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25%concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALL] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QR-016 The RPD value for the LCS/LCSD was outside of QC acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-07-CUSTODY RECORD www.encolabs.com ® 10775 Celural Port Dr. 4810 EnecuOve Park Court; Sulto.111 102-A yJoodwtrlda InduotAal Ct. OrlaWm Fl 3024 Jacl=rm.lo. FL 32218 wm Gary•. NC 275.1 (407) 82sr•5914 Fax (407) a5G-E9a5 (904) e95-3oa7, Fox (904) 206-6210 (91U)4s7-31M Fer (s19)+sr-351ti Page of Crwrd Name Proieet Nurirber Requested Analyses Requested Turnaround March Truck Parts (MA035) [none] Times Addr06! PFO;40 N=64) cC r race : Rush reWosw oubrW, to P.O_. Bo.c 427 Car Yard ar£dp!'snco b1 the laadtr C ry151'fLia PO a 1 BIG ng Into 1- Siler City. NC 27344 Standard Tel Fay Repcatarp Canted CIO CD(919) 663-1908 Steve Marsh m�• ' N Expedited �p SaruplM(s) Names. Afrdisliui (Prird) eCFe mta[ � � t u k Hoffman r - Due Uj (� _ sa rows) slgn=m site Locat'an J Time Zono tabWorkorder go o; CCO2610 �. Preservation (Sea Codas) ((;embire9 as rtcC4 8fir) CdArctidrr Matrix Total M of Item a '-Sample lie (Fled lden:5-nrion) C Wd:on nale Time comp loath• (.vre cedes) •r rjunem - - tti Sample Comments Ca and f3A SW -7 X X X. X l w � - t-- Total of Containers Sarsp'o !{il Prtepartnl y D'ahJTGra Ru6unluatwd B - Dala/iinee R 9 Qat¢Inme ,, t y CammanlrJSped Roporpnq Rsgtdretnonts " RehnQuahed Daterrime Rwolmd Sy. Dateliima ReGrquktwd W Datornme Rticelvad BY QaUCMw Cooler A5 8 Temps on Receipt Cnr doinn 11pon Rerpipt' Acceptable Unacceptable En Yatrhe :OW-Gradrdwater So.soi BW43rtrd:irg Water SE-Sedment SW$:uiace Water' WW-Waste'watar AWS d-Other (detail in comments) Preanrwdldn: Hea H-NCI "NO3- S-H?SO4 N"AOH O-Other (derail in awenrrna) Note : Al samples su1m7ined to E14CO tabs are in w=rcarce with Un tams ernd curdilirms listed on the iewrw d ttus trim, vnkrss priw writt9n agaements ealsy Simple Preservation Verification ENCO Cary Work Order: CCO2610 Prbject: Car Yard Client: Marsh Truck Parts (MA035) Project #. [none] Logged in: 13-May-19 15:17 Logged By: Rachel Ann Y ni,hI 151 C) Preservation Check Performed By: Date/Tlrne�-5 115 CCO261 0-01 ConFAt�lj t-, jx dw,' nq-v4., -,-T4�,P-res type66rit-Used ',(1pFI)t,!' OH,Gheckedfl ;�r L e;,-k - �'J.A&!50atelTim PH psied 1 -:4 . Co(nments', P-I�eqptre.m.enl.., i.6tontrbl-, . fq-,:4,� �'AdjUsi&dl�," B 250rnLA+H2504 <2 Y I N I (P rA Y I N I C 250ml-A+F!2504 <2 Y I N I EA,, Y I N I NA D 1250mLP+HNO3 e2 CY)f N I NA I Y (7N NA Reaqent Name ID 2 pH Strip ID: PH Strips C8J0741 C:\eIrnnt\Prii,-,..--, iva=iwc3tIVMaIIt!CK.F.Dt Reaqent Name ID 3 4 Rea_qent Name ID 5 6 Page 1 of 1 Mid Atlantic Engineering R Environmental Solutions January 9, 2018 NCDEQ/DWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on December 20, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. vEo CEJgN24 2913 Ron Davis owR cP/tE8 Stormwater Services Manager 7-16N Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 FACILITY NAME Marsh Auto Parts, Inc. - Caryard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. 919) 663-1908 CERTIFIED LABORATORY(S) ENCO Inc. Lab # 592 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample,.Collected, • mo/dd/year Total. Rainfall,. inches 00400, 00530. 77023'. , . 01051 781.41' pH,;, -. Standard Units Total'Sbspendetl <' Solids (TS5), m L g/ Non polar O&G/'fPH [Method.1664 SGT-HEM) ,•mg/L . fEttiylene Glycol;. mg/L Lead; T&M,. Recoverable, mg/L T661 oxic 3 Ofganics , mg/L .Benchmark - - 6.0.-9.01 100/502 :. ... ZS;... F ,. 8;000 `. (Tiers=2:and13) . 0 03 : 1A Outfall001 12/20/17 1.10 7.2 34 <2.70 <4.7 0.0140 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2- STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." A A6yw Name (Print name) Title (Print title) Sig ure Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee or Designee) (Date) Form SW U-251, last revised October 25, 2012 Page 2 of 2 ENCO Laboraton"es, Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, January 5, 2018 Marsh Truck Parts (MA035) Attn: Steve Marsh P.Q. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CA11654 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, December 20, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 10 � t www.encotabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE ClientID: Caryard Lab ID: CA11654-01 Sampled: 12/20/17 11:50 Received: 12/20/17 13:55 Parameter Hold DatelTime/sl Prep DatelTime(s] EPA 1664B 01/17/18 12/30/17 11:57 01/03/18 1234 EPA 6010D 06/18/18 12/29/17 08:26 01/04/18 12:00 EPA 8015C SM 254OD-1997 01/03/1B 12/27/17 01/02/18 12/26/17 10:06 01/02/18 11719 15:20 12/26/17 15:50 Client ID: Truckyard A Lab ID: CA116s4-02 Sampled: 12/20/17 12:00 Received-. 12/20/17 13:55 Parameter EPA 1664B EPA 6010D SM 254OD-1997 Hold Date/Time(s) 01/17/18 06/18/18 12/27/17 Prep Date/Time(sl 12/27/17 12/29/17 12/26/17 Analysis Date/Timefs) 11:32 12/29/17 16:45 08:26 01/04/18 12:12 15:20 12/26/17 15:50 Client ID: Truckyard A Lab ID: CA11654-02RE1 Sampled: 12/20/17 12:00 Received: 12/20/17 13:55 Parameter EPA 8015C Hold Date/Timefsl 01/03/18 Pimp_DatelTime(s) 01/02/18 Analysis Date/Timefsl 10:06 01/02/18 12:15 Client ID: Truckyard 9 Lab ID: CA11654-03 Sampled: 12/20/17 12:15 Received: 12/20/17 13:55 Parameter EPA 1664E EPA 6010D Hold DatelTime(s) 01/17/18 06/18/18 Prep Date/Time(s) 12/27/17 12/29/17 Analysis Date/Timefsl 11:32 12/29/17 16:45 08:26 01/04/18 12:15 EPA 8015C 01/03/18 SM 254OD-1997 12/27/17 01/02/18 10:06 01/02/18 11:56 12/26/17 15:20 12/26/17 15:50 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 2 of 10 6 P'= M ,,,,r _' I� rllr www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: CA11654-01 Anal Results Ela9 MU PAL Units Method Notes Lead - Total 0.0140 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 34 5.0 5.0 mg/L SM 254OD-1997 Client ID: Truckyard A Lab ID: CA11654-02 A06lm Results Eldg MQL PQL Units Method Note Lead - Total 0,00714 3 0.00310 0.0100 mg/L EPA 601OD Oil & Grease (HEM-SGT) Nan -Polar Material 4,35 1 2,70 5.00 mg/L EPA 1664E Total Suspended Solids 23 5.6 5.6 mg/L SM 2540D-1997 Client ID: Truckyard B Lab ID: CA11654-03 AnatvW Results EL19 H" PQL vAb Method Llut�s Lead - Total 0.00718 3 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 38 10 10 mg/L SM 254OD-1997 FINAL This rep6rt relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 10 Description: Caryard Matrix: Surface Water ANALYTICAL RESULTS Lab Sample ID:CA11654-01 Sampled: 12/20/17 11:50 Project: Marsh Truck Parts Sampled By: CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods www.encolabs.com Received: 12/20/ 17 13: 55 Work Order: CA11654 ^ - ENCO Cary certified a -Me [NC 5911 Analyle rCAS Sul tMrl Resulfin M11M PE MIL EQL VAUh , 1iethod Analyzed By 1i9 e Lead [7439-92-1]^ 0.0140 mg/L 1 0.00310 0.0100 71-29004 EPA 6010D 01/04/18 12:00 ]MV Classical Chemistry Parameters ^ - ENCO Cary cer&&d analyze INC 5911 Analvte rCAS Numberl Results fig Units QE Mgt EQL Batch Method Angh=d By Notes Total Suspended Sollds^ 34 mg/L 2 5.0 5.0 71-26007 SM 254OD-1997 12/26/17 15:50 OMR Non -Halogenated Semivolatile Organics by GC Anatvte rCAS Numberl Ethylene Glycol[107.21-1] Results flag Units 17E M12L PQL Batch Method Analyzed By Notes 4.7 U mg/L 1 4.7 5.0 BA02016 EPA 8015C 01/02/18 11:19 JIB Surroaates ResulCr —Of Spike L v1 % Rec ft Rec Limits Awiftb Ana By Notes 1,3-Butylene Glycol 250 1 200 127 % 50-150 8AO2016 EPA 8015C OIIOZ11811.19 JJB Classical Chemistry Parameters ^ - ENCO Jacksonville cerf&ed onalyte (NC 4411 Analyde [M Numberl Results Ela9 !lofts RE MRL EQL Batch Method Anahaed By N9te Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 71-30002 EPA 1664E 01/03/18 12:34 SMA Material^ Description: Truckyard A Lab Sample ID:CA11654-02 Received: 12/20/17 13:55 Matrix: Surface Water Project: Marsh Truck Parts Sampled: 12/ 20/ 17 12 : 0 0 Sampled By: CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods Work Order: CA11654 ^ - ENrV Cary cerfified analyze INC F911 Anal= rCAS Number! Results E]gg Yalu 2E MU pU Bich Method Analyzed By NOW Lead [7439-92-1]^ 0.00714 1 mg/L 1 0,00310 0.0100 71-29004 EPA 6010D 01/04/18 12:12 ]MV Classical Chemistry Parameters ^ - EW O Cary certified enaVe (NC 5911 Anatyte ICAS Numberl Results fig MO& 12E MU FQL Batch Method Analyzed By Notes Total Suspended Solids^ 23 mg/L 2.22 5.6 5.6 71-26007 SM 2540D-1997 12/26/17 15:50 OMR Non -Halogenated Semivolatile Organics by GC :J Analvte rCAS Numberl Resul 4 ) lag Units pE M" ply $=h Method Analyzed BY Notes Ethylene Glycol[107-21-1] 4.7 U mg/L 1 4.7 5.0 8A02016 EPA 8015C 01/02/18 12:15 ]JB &are aces $ QE , Ike Lv! % Xec % Rec LimlCs fiact tjp A By Notes 1,3-1tutylene Glycol 170 1 2W 84 % 50-150 8AW016 EPA 8015C 01102118 11:15 JJB Classical Chemistry Parameters ^ - ENCO Jacksonville Certified analyze [VC 4421 Analyte rCAS Numberl Results E[;g YAM RE MPI EQL Batch shod Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar 4.35 ] mg/L 1 2.70 5.00 71-27004 EPA 16649 12/29/17 16:45 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 10 r � s www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID: CA11654.03 Received: 12/20/17 13:55 Matrix: Surface Water Sampled:12/20/17 12:15 Work Order: CA11654 Project: Marsh Truck Parts Sampled By: CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENC0 Cary -rfaW analyse INC 591] Anahrte 1CA5 Numberl Resu[ Jig Units Of KU P9L Bi&h Method Analyzed Ry Notes Lead [7439-92-1]^ 0.00718 J mg/L 1 0.00310 0.0100 71_29004 EPA 6010D 01/04/18 12:15 JMV Classical Chemistry Parameters ^ - ENW Cary cerdlred analyse (NC 5911 Ana a [CAS Numberl Results frog units QE Mk ML BAtrh Method Analyze By Notes Total Suspended Solids^ 38 mg/L 4 10 10 7L26007 SM 254OD-1997 12/26/17 15:50 OMR Non -Halogenated Semivolatile Organics by GC Analvte ICA-S Numberl Resul flog Units PE MDL p21L Batch Method Atlawzgd fiy Notes Ethylene Glycol [ 107-2 1 - 11 4.7 U mg/L 1 4.7 5.0 BA02016 EPA 801SC 01/02/18 11:56 JIB Surr wtes 6,is11LCE —Of Spike L vl % Rec % Rec [imps fiff" l Med €d BJl Notes 1,3-BoVene Glycol 160 1 100 129 % 50.150 &401016 EPA 8015C 01102118 11,56 JJB Classical Chemistry Parameters ^ - ENCO Jack" vrlle C&bfkv Anahrte ICAS N mglberl Oil & Grease (HEM-SGT) Non -Polar Material^ R4u1L4 flag Units PE MU FQL Batch Method Analyzed By Notes 2.70 U mg/L 1 2.70 5.00 71-27004 EPA 1664B 12/29/17 16:45 SMA FINAL This report relates onty to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 10 kk www.encolabs.com QUALITY CONTROL DATA Metals {total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7L29004 - EPA 3005A Blank (7L29004-BLK3) Prepared: 12/29/2017 06:26 Analyzed: 01/04/2018 11:52 Spike Source %REC RPD Analvte Result Flan POL Unite Level Result %REC Limits RPD Limit Motes Lead 0.00310 U 0.0100 mg/L Blank (7L29004-BLK2) Prepared: 12/29/2017 08:26 Analyzed: 01/04/2018 11:54 Spike Source %REC RPD Anal Yte Result Elan P91 u111b Level ResyI %REC Limits RPD Ljmd Notes Lead 0.00310 U 0.0100 mg/L LCS (7L29004-BS1) Prepared: 12/29/2017 08:26 Analyzed: 01/04/2018 11:57 Spike Source 9/6REC RPD AnalvW Result Flan POL Units Level Result °1oREC Limits RPD ldma Notes Lead 0.214 0.0100 mg/L 0.200 107 80-120 Matrix Spike (711-29004-161S1) Prepared: 12/29/2017 08:26 Analyzed: 01/04/2018 12:02 Source: CA11654-01 Spike source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0.234 0.0100 mg/L 0.200 0.0140 110 75-125 Matrix Spike Dup (7L29004-MSD1) Prepared: 12/29/2017 08:26 Analyzed: 01/04/2018 12:05 Source: CA11654-01 Spike Source %REC RPD Anal Result FIa1 POL Units Level Resul %REC Limits RPD Limit Notes Lead 0.214 0.0100 mg/L 0.200 0.0140 100 75.125 9 20 Post Spike (71-29004-PS1) Prepared: 12/29/2017 08:26 Analyzed: 01/04/2018 12:07 Source: CA11654-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0.240 0.0100 mg/L 0.200 0.0140 113 80-120 Classical Chemistry Parameters - Quality Control Batch 7L26007 - NO PREP Blank (7L26007-BLK1) Prepared: 12/26/2017 15:20 Analyzed: 12/26/2017 15:50 Spike Source %REC RPD .Analvte Result Flee POL Units Level RMft %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (71-26007-BS1) Prepared: 12/26/2017 15:20 Analyzed: 12/26/2017 15:50 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Ljluft Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (7L26007-DUPi) Prepared: 12/26/2017 15:20 Analyzed: 12/26/2017 15:50 Source: CA16599-01 Spike Source %REC RPD Anal vle Result Elaa PS?l tin& Level Result %REC Limits RPD Limit Notes Total Suspended Solids 240 50 mg/L 300 23 20 QM-12 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7L26007 - NO PREP - Continued Duplicate (7L260O7-DUP2) Prepared: 12/26/2017 15:20 Analyzed: 12/26/2017 15:50 Source: CA16624-01 Spike Source %REC RPD .Analyte Result Flag P-QL Units Level Be6u %REC Limns RPD Limit Motes Total Suspended Solids 68 33 mg/L 96 34 20 QM-12 Non -Halogenated Semivolatile Organics by GC - Quality Control 11 Batch 8A02016 - NA Blank (SAO2016-BLKI) Prepared: 01/02/2018 10:06 Analyzed: 01/02/2018 10:21 Spike Source %REC RPD .Anallrte Result Flag PQ Units Level Result %REC Limits RPD Llmlt Notes Ethylene Glycol 4.7 U 5.0 mg/L 1,3-Butylene Glycol 210 mg/L 200 103 50-150 LCS (SA02O16-BSI) Prepared: 01/OZ/7018 10:06 Analyzed: 01/02/2018 10:40 Spike Source %REC RPD .Analyte Result Flag PQL Units Level Result 9/nREC Limits RPD LIMA Notes Ethylene Glycol 200 5.0 mg/L 200 102 70-130 1,3-BuWene Glycol 1.00 mg/L 200 96 50-150 LCS Dup (8AO2016-BSDS) Prepared: O1/02/2018 10:06 Analyzed: O110212018 11:00 Spike Source %REC RPD -Anahte Result Flag PQt Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 200 5.0 mg/L 200 102 70-130 0.7 25 1,3-Butylene Glycol 180 -91L 200 90 50-150 Classical Chemistry Parameters - Quality Control Batch 7L27004 - EPA 1664E Blank (711-27004-1311-11(3) Prepared: 12/27/2017 11:32 Analyzed: 12/29/2017 16:45 Spike Source %REC RPD -AnaNte Result Flag J!" Units level Result %REC Limits RPD Lung Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (7L27004-BSI) Prepared: 12/27/2017 11:32 Analyzed: 12/29/2017 16:45 Spike Source %REC RPD -Anatyk RMIt Flag PQL knits Level Result %REC Limits RPD Limlt Notes Oil & Grease (HEM-SGT) Non -Polar Material 74.6 5.00 mg/L 79.4 94 64-132 LCS Dup (7L27OO4-BSD1) Prepared: 12/27/2017 11:32 Analyzed: 12/29/2017 16:45 Spike Source %REC RPD Analyt Result Flag PQL Units Level Result %REC L(mI RPD himit Notes Oil & Grease (HEM-SGT) Non -Polar Material 62.7 5.00 mg/L 79.4 79 64-132 17 34 Matrix Spike (7L27004-MSI) Prepared: 12/27/2017 11:32 Analyzed: 12/29/2017 16:45 Source: BA05350-01 Spike Source %REC RPD .Analyte Result Flag PQL Units Level Result woREC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 41.4 5.00 mg/L 75.2 4.33 49 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. Page 7 of 10 i N I �Cmaj www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7L30002 - EPA 16540 Blank (700002-181-11(i) Prepared: 12/30/2017 11:57 Analyzed: 01/03/2018 12:34 Spike Source %REC RPD Analyte Result Flag ML Units Level ResulT %REC Limits RPD LImiL Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (7130002-113SI) Prepared: 12/30/2017 11:57 Analyzed: 01/03/2018 12:34 Spike Source %REC RPD Anal a Result Faa PQL unks Level Result %REC Limits RPD UMA Notes Oil & Grease (HEM-SGT) Non -Polar Material 82.3 5.00 mg/L 80.6 102 64-132 LCS Dup (71-30002-i SD1) Prepared: 12/30/2017 11:57 Analyzed: 01/03/2018 12:34 Spike Source %REC RPD _Analvte Result Flag P_QL Units Level Result %REC Limits RPD L= Notes Oil & Grease (HEM-SGT) Non -Polar Material 112 5.00 mg/L 91.7 122 64-132 31 34 Matrix Spike (7L30002-MSI) Prepared: 12/30/2017 11:57 Analyzed, 01/03/2018 12:34 Source: BA05194-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Lkmit Notes Oil & Grease (HEM-SGT) Nan -Polar Material 49.1 5.00 mg/L 88.5 2.70 U 55 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 10 I�X 09 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL; Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 10 _ 1D775 Central Pori Dr. 4810 Executive Park Court, Suite 111 '102-A Woodwinds Industrial Cl. Orland[), FL a2a24 Jacksornille, FL =I6-6M9 Cary. NC 27511 (407) 826.5314 Fax (407) $50.6945 (9041 296-3D07 Fax (9D4) 296.6210 (919) 467.3090 Fax (919) 467.3515. Page __- Of Client Name Marsh Truck PartS I(MAOS5) Project Number - - - Requaated Anatysee Requested Turnaround Times Note: Rust[) regtrest6 Subject to acceptance by me facility _ Standard _ _ Expedited Due _I a+ tD 06 o a O L N M Cn w- ICAI Address P:O. Box 427 Project NameiOesc - Marsh Truck Parts oityfsTrry - -Siler Ci NC 273A4 PO 01 Biltieg into, Tel C-1 663-1908 Far ` Reporting Contact Steve Marsh mpr Saer(S) Nana. Atfiliabon (Print) Biting Contact Chuck Hoffman sampter(sl signature Site Lecabon r Tree zone Lab Workorder 1654 • Preservaton (See Colds) (Combine as nee5s,ary1 lm r Sample 10 (Fled Idontiriwlion) Codaction Data Collection Time ComP I Grua Matrix 95e0 cod(1s) Total k of containers Sampie Comments L ZD-lZ 1j;.% �d Truckwirdz-U -i7 IZN=:. Crr,a SIN 7 X X X X de 7► Z- e a -7, < Total # of Containers ` Sample Kit Prepared By � G U7 7737/ Relinquished By - • c DAN)Mma .� , 1 y �� � .. Daloornme Comments+Speclal Reporting Requirements Relingwshed Ery. Date/ruae Received By, OatelT-ame RelintlUshed By Dalarri me Received By DatuMme Cooler k's d. Temps on Receipt _ - .7� Condiian n Rec"t Acceptable Unacceptable Hatrix:GW.Groundwater SO -Soil OW-Onnking Water SE -Sediment SW-Surtace Water WW-Wastewater A -Air O-Oftr (detatl in comments) Prasaryatlon: I.lea (t-FICI N-HNO3 S-1­12SO4 NO-NaOH O-Otter (detail In commentsl Note: AD Samples submdteb t0 ENCO Lab4 are in accordance N.th the terms and conditions listed on tee reverse o1 this farm, unless prior wmten agreements past 1 Sample Preservation Verification ENCO Ca C� Cary Work Order: CA11654 Project: Marsh Truck Parts Client: Marsh Truck Parts (MA035) Project #: [none] Logged in: 20-Dec-17 15:28 Logged By: John C King Preservation Check Performed By: � DatelTime: /off G //, , CA11654-01 Cont Type Pres (pH) _ Requirement pH Checked I In Control . pH Adjusted Datel> kme, Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N I Y! rN 1 LA , C 260mLA+H2SO4 <2 Y P N I Y I N/ I& D 250mLP+HNO3 <2 I N I NA Y /0I NA CA11654-02 Cont Type Pres (pH) Requirement pH Checked I In Control pH Adjusted Dateffime Adjusted Reagent Used/Comments B 250mtA+H2SO4 <2 Y I N 1 Y I N I C 250mLA+H2SO4 <2 Y I N! Y I N I I D 250mLP+HNO3 <2 I N 1 NA I Y I / NA u CA11654-03 Cont TypepH Pres (pH) Requirement pH Checked 1 in Control Date�me Adjusted Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y I N 1 , Y I N I C 250mLA+H2SO4 <2 Y! N I Q Y I N/ D 250mLP+HNO3 1 <2 YIN 'NA Y ! 1 NA "i P Reacient Name ID 1 . 2 PH Strip ID: CoS2Q A Reagent Name ID 3 4 Reagent Name ID 5 6 C:IELMNT1Printlwko_PreservationCheck. rpt Page 1 id Atlantic Engineering & Environmental Solutions June 19, 2018 NCDEQIDWR RErFIVE® Attention: Central Files JUL 0 3 2018 1617 Mail Service Center,' 'iL FlLEa Raleigh, North Carolina 27699-1617 �rR S� FILE Subject: STORMWATER SAMPLING RE ULTS MARSH AUTO PARTS, INC. — AR YAR 211 EAST 11T" STREET SILER CITY, NORTH CAROLIN NPDES PERMIT NO. NCG10001 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919,250,9918 facsimile 919,250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on May 17, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE 40 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGl00015 FACILITY NAME Marsh Auto Parts, Inc. - Caryard _ PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 592 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample, Collected, _ mo/dd/year. Total Rainfall, inches, 00400 00530 - - - - 77023 .01051 78141 pH Standard Units Total'Suspendi"d Solids (TSS) mg/L Non polar O&G/TPH (Method',1664' SGT-H EM);`r mg/L Ethylene`Glycol, mg/L Lead, Total Recoverable, mg/L.mg/L Total,Toxic Organics3, Benchmark - - 6.0 — 9.01 100/S02 i5 s;aoo (Tiers 2 and 3) 0.03. 1,0 Outfall 001 5/17/18 1.25 6.8 <2.5 Q.70 <4.7 0.00606 J NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Pagel of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." D Name (Print name) JM14r Tit rintU e) r G.► D L C7 Sign V re Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee or (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 ENCO Laboratones Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 31, 2018 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CB06059 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, May 17, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 �co www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CB06059-01 Sampled: 05/17/16 09:00 Received: 05/17/18 11:25 Parameter EPA 1664E Preparation EPA 1664E Hold Date/Time(s) 06/14/1B Prep Date/Time(sl 05/24/18 11:07 A_nnglysis Date/Time(s) 05/25/16 15:50 EPA 6010D EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 10:25 EPA 8015C NA 05/31/18 05/30/18 04:39 05/30/18 07:36 SM 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 OS/23/18 14:05 Client ID: Truckyard A Lab ID: CB06059-02 Sampled: 05/17/18 09.30 Received: 05/17/18 11:25 Parameter Preparation IHgld Date/Time(s) Prep Date/Time(s) Analysis Date/Time(sl EPA 1664D EPA 1664B 06/14/18 05/24/18 11:07 05/25/18 15:50 EPA 6010D EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 10:27 EPA 8015C NA 05/31/18 05/30/18 04:39 05/30/18 07:55 SM 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 05/23/18 14:05 Client ID: Truckyard B Lab ID: CB06059-03 Sampled: 05/17/18 09:40 Received: 05/17/18 11:25 Parameter Preparation Hold Date/Time(s) Prep Date/Tune(:) Analysis Date/Time(:) EPA 1664E EPA 1664E 06/14/18 05/24/18 11:07 05/25/18 15:50 EPA 60101) EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 10:30 EPA 8015C NA 05/31/18 05/30/16 04:39 05/30/18 08:15 SM 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 05/23/18 14:05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 2 of 9 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: CB06059-01 Anal ide Lead - Total Bsiulti Flan 0,00606 3 H" M 0.00310 0.0100 !!nb Method Notes mg/L EPA 6010D Client ID: Truckyard A Lab ID: C606059-02 ABallyte Ethylene Glycol H.alllti Elan 330 H" E" 4.7 5.0 !ln1C4 Mgthad Notes mg/L EPA 8015C Client ID: Truckyard B Lab ID: CB06059-03 Analute Total Suspended Solids Bsaulti Eim 3.9 K E" 2.5 2.5 unm Method Notes mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample I D. C606059-01 Received: 05/17/18 11:25 Matrix: Surface Water Sampled: 05/17/18 09:00 Work Order: CB06059 Project: Marsh Truck Parts Sampled By:CLIENT (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary c&tfred analyze (NC 5911 Analyte (CAS Numberl Resull;4 E[ag knila 2E HU EM Batch Method Analyzed Jly JYltw Lead [7439-92-1]^ 0.00606 J mg/L 1 0.00310 0.0100 BE24015 EPA 6010D 05/29/18 10:25 JDH Classical Chemistry Parameters ^ - ENCO Cary ceftevd analyze [NC 5911 Analyte FW Numberl Results E[dg Units 2E ma M akt&h Method Analyzed @y Notes Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 BE23005 SM 2540D-1997 05/23/18 14:05 OMR Non -Halogenated Semivolatile Organics by GC Analyte rCAS Numberl ResulL4 E119 mom 2E MU PA Batch Method Analyzed ft Note Ethylene Glycol[107-21-1) 4.7 U mg/L 1 4.7 5.0 8E30005 EPA 8015C 05/30/18 07:36 JIB SUM29Ates 2E ,mike Lvl % Rec h &K limits58 meth A & Notes 43-Butylene Glycol 180 1 200 92 % 50-150 8E30005 EPA 8015C 05130118 07..36 J118 Classical Chemistry Parameters ^-rACOJmksronviliecertfiedanalyze[AC 4421 Analyte rCAS Numberl Resul figs Units pE MU PQL Batch Method Analyzed ft dotes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 BE24005 EPA 1664B 05/25/18 15:50 SMA Description: Truckyard A Lab Sample ID:CB06059-02 Received: 05/17/18 11:25 Matrix: Surface Water Sampled: 05/ 17/18 09:30 Work Order: CB06059 Project: Marsh Truck Parts Sampled By:CLIENT LMetals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Lary c"fledan,?VeINC 591] Analyte rCAS Numberl Results Ela mob 2E M2L Pal. Batch Method Analyzed 1�1r lY4It1� Lead [7439.92-1]^ 0.00310 U mg/L 1 0.00310 0.0100 8E24015 EPA 6010D 05/29/18 10:27 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyze (NC 5911 Anatyte rCAS Numberl Results E[sg Units QE MI EQL D=h Method Analyzed Am iiAU Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 8E23005 SM 254OD-1997 05/23/16 14:05 OMR Non -Halogenated Semivolatile Organics by GC Analyte rCAS Numberl ResRIU Flag Units 2E M26 E L Batch Method Analyzed f}Y Note Ethylene Glycol [107-21-11 330 mg/L 1 4.7 5.0 8E30005 EPA 8015C 05/30/18 07:55 JIB uffegates M Spike lv! 219 Rec L1m/ts ad= 9QdGF�� BY d9Is.4 1,3.8utylene Glycol 200 1 200 98 % 50-150 8E304105 EPA 8915C 05130118 07.•55 M Classical Chemistry Parameters ^ - ENCO Jacksonville certified anafyte INC 4421 Analyte fCAS Number] Results Elm Units 2E H" E" A" Method Analyzed D11 Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 8E24005 EPA 1664E 05/25/18 15:50 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Truckyard 8 Lab Sample I D: CB06059-03 Received: 05/17/18 11:25 Matrix. Surface water Sampled:05/17/18 09:40 Work Order: CB06059 Project: Marsh Truck Parts Sampled By:CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary rertrfied a-W (NC 5911 Analyte rCAS Numberl Results E612 Units 2E EDL E" 13BLSh Method Analyzed �1t Notes Lead[7439-92-1]^ 0.00310 U mg/L 1 0,00310 0,0100 8E24015 EPA 6010D 05/29/18 10:30 3DH Classical Chemistry Parameters ^ - ENCO Cary -tbfied analyte [NC 5911 Analyte rCAS Number] $es1l Bag Units QF MU P26 Batch Method Analyze ay Notes Total Suspended Solids^ 3.9 mg/L 1 2.5 2.5 8E23005 SM 2540D-1997 05/23/18 14:05 OMR Non -Halogenated Semivolatile Organics by GC Analyte 1CAS Numberl Results ]_[ag YAM 2E MU EQL Batch Method Analyzed AY Notes Ethylene Glycol(107-21-1] 4.7 U mg/L 1 4.7 5.0 8E30005 EPA 8015C 05/30/18 08:15 33B SMates 2E Spike Lv1 9F, Rec % RecLlmits &dab me By Note 1,3-80)4ene Glycol ISO 1 200 92 % 50.150 900005 EPA 8015C 05/30/18 08:15 JJB Classical Chemistry Parameters ^ - ENCO Jaol_sanvilk Certified.?-W (NC 4421 Analyte rCAS Numberl R esul Fig Units iZE MU E" BA= Method Analxzrd Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 BE24005 EPA 1664E 05/25/18 15:50 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 5 of 9 CS www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch SE24015 - EPA 3005A Blank (8E24015-BLKi) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 09:51 Spike Source "/DREG RPD -Analtite Result Flag POL Units Level Result %REC Limits RPD Limit motes Lead 0.00310 U 0.0100 mg/L LCS (SE24015-B51) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 09:57 Spike Source %REC RPD Analvt Result Flag 1291 Units Level Resul %REC Limits RPD Limit Notes Lead 0.197 0.0100 mg/L 0.200 99 SO-120 Matrix Spike (8E24015-MS1) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:01 Source:CB06833-01 Spike Source %REC RPD Analvte Result Elag QQL units Level Result %REC Limits RPD Limit Notes - Lead 0.190 0.0100 mg/L 0.200 0.00310 U 95 75-125 Matrix Spike Dup (SE24015-MSD1) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:04 Source: C606833-01 Spike Source %REC RPD nalvw Result Flan P0L Units Level Resin %REC Limits RPD Limit Notes Lead 0.193 0.0100 mg/L 0.200 0.00310 U 97 75-125 1 20 Past Spike (SE2401S-PS1) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:06 Source: C806833-01 Spike Source %REC RPD Anal Yte Result Elag PQL Units Level Result %REC Limits RPD Limit Notes Lead 0.199 0.0100 mg/L 0.200 -0.00287 100 80-120 Classical Chemistry Parameters - Quality Control Batch 8E23005 - NO PREP Blank (8E23005-BLK1) Prepared & Analyzed: 05/23/2018 14:05 Spike Source %REC RPD Anal lde Result Elag PQL Units Level Result %REC Limits RPD limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (8E23005-B51) Prepared & Analyzed: 05/23/2018 14:05 Spike Source %REC RPD -Analyte Result Flag POL units Level Result 9ioREC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 101 80-120 Duplicate (SE23005-DUPl) Prepared & Analyzed: 05/23/2018 14:05 Source:CB05042-01 Spike Source MoREC RPD AnaWte Result Flag PQL units Level gem %REC Limits RPD Limit Notes Total Suspended Solids 290 50 mg/L 310 6 20 Duplicate (8E23005-DUP2) Prepared & Analyzed: 05/23/2018 14:05 Source: CB06066-03 Spike Source %REC RPD Anal Result El" ML Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 880 100 mg/L 870 0.9 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 �JVCC-3 www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 8E30005 - NA Blank (8E30005-BLKi) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 06:36 Spike Source %REC RPD -Am tyW Result Flaa P_QL Units Level Result %REC Limits RPD u1njZ Notes Ethylene Glycol 4.7 U 5.0 mg/L 1,3-Buty/ene Gly[a/ 200 m91L 200 101 50-150 LCS (8E30005-BSI) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 06:55 Spike Source %REC RPD An_aUrte Resin Flag PQL Units Level Resin %REC Limits RPD umjj Notes Ethylene Glycol 200 5.0 mg/L 200 101 70.130 1,3-6utyfene Glycd 180 mg/L 200 92 50-150 LCS Dup (8E30005-BSD1) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 07:18 Spike Source %REC RPD AnalA Result Flag M Units Level Result °/uREC Limits RPD Limit Plotes Ethylene Glycol 200 5.0 mg/L 200 100 70-130 0.2 25 i,3-Batj — Glycol 160 m9A 200 78 50-150 Classical Chemistry Parameters - Quality Control Batch 8E24005 - EPA 16648 Blank (8E24005-BLK1) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Spike Source o/aREC RPD Ana)yte Result Flag PQL Units Level gesyl %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (8E24005-BS1) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Spike Source °kREC RPD Analvte ResUl Flau PQL units Level gel 9/aREC Limb RPD Lima Ngtes Oil & Grease (HEM-SGT) Non -Polar Material 78.0 5.00 mg/L 80.0 98 64-132 LCS Dup (8E24005-BSD1) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Spike Source %REC RPD Anal ytE Result Elm PQL units Level Result %REC Limits RPD Limit N2Ns Oil & Grease (HEM-SGT) Non -Polar Material 75.0 5.00 mg/L 80.0 94 64-132 4 34 Matrix Spike (8E24005-M51) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Source: BB02283-01 Spike Source %REC RPD Anal vte R4.s rwlt F.IIM N.I. ni Level Result %REC Limits RPD Lim$ Notes Oil & Grease (HEM-SGT) Non -Polar Material 74.7 5.00 mg/L 8010 2.70 U 93 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 7 of 9 C, Nk'q ; =M) 110 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed For but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (850/16 or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 8 of 9 CO 10775 Central Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Indushial CL Orlando, FL 32924 Jacksor% to, Ft 32216.6369 Cory, NC 27511 U#M_ (407) 826-5314 Fax (407) 650-6945 {9M) 296.3007 Fax (904) 296.6219 (919) 467.3090 Fax (919) 467.3515 Page Of Client Name Mamh Truck Parts (MA036) Project Number [none] Requested Analyses Requested Turnaround Times Note: Rush requests subject to acceptance by the t odity Standard Expedited Due —/--J_ V% 0 r CD CIO W it? Ckd o a p o N Address P.O. Box 427 Projeel Name/Desc Marsh Truck Parts GUY/sT2ip Si ler City . NC 273" PO • r etlting Into Tel (919) 663-1908 Reporting Contact Steve Marsh Samptor(s) Name. AffiEialion (Print) Bi1G Contact Nshuck Hot"en SamDler(s)Stgnalure Site LocationITuneZone LabWorkorder CB 6.0.5.9:. '- ��r�:..� r s�-;+..' Prescry tfon (See Codes) (Combine as necessary) item • Sample ED (Fw1d Identification) Collection Date Coileaon Time Comp! Grab Matrix (see codes) Total Y of Containers Sample Comments —Go—yard - ',. i7- d A R 41►1::, , :. " , - ' - SW 7 X X X ° Truc and A -% '/-1 31% SW 7 X X X X Truc ard'B '7 -ts: _ , SW 7 X X X X At Ile Av ell c q E-T `I — Total H of Containers e K4 Prepared By D e/fft iema,� ReWlgedsne By / 1AeiinqJSed8yiFDatelTune DatdTvne Rece By DatolTcna nwSpeciat Reporting Requirements Received By DaNu Tune Relirquishad By oatolTune, Received By DalefTrme rDlerir's&TeffV��onR ipt o1 Receipt Conry7ACCeptableUnacceptable Matrix; GW-Groundwater SO -Sod OW -prinking Wtuer SE -Sad Got SWSudaCB Water WW-Wastawatar A -Air O-Qlher (dotatl In comments) Preservation: Mice WHCI N-HNO3 S-H2SO4 NO-NaOH Other (detail in comments) Nate : Aft sarnplas submitted to ENCO Labs ate in accordance with the terms and conditions ksteo on the reverse Ot this form, unless poor wntten agreements exist Sample Preservation Verification ENCO Cary Work Order: CB06059 Client: Marsh Truck Parts (MA035) Project: Marsh Truck Parts Project #: [none] Logged In: 17-May-18 14:27 Logged By: John C King Preservation Check Performed By:� DatelTime: 57,,7l� CB06059-01 Cant Type Pres (pH) ;Requirement, pH Checked ! En.Control pH,Adjmt6d DatelTme t: -I , Adjusted t Reagent lJsedlGominents f B 250mLA+H2SO4 <2 Y/ N I Y I N! A C 250mLA+H2SO4 <2 Y/ N /tali Y I N! D 250mLP+HNO3 <2 ky/ N I NA Y /U / NA CB06059-02 Cont Type F?res (P .. } Ftequire'ment p • , hec e / In Control , , 4y ; ateRme pti Adjusted { , _ Adlustid Reagent UsedlCommentsYi ,�.. B 25DmLA+H2SO4 <2 Y I N/ A Y I N! rA C 250mLA+H2SO4 <2 Y/ N I Y I N/ 4A D 250mLP+HNO3 <2 Y I N I NA1 Y 1(J / NA CB06059-03 Cont hype Pres' P ttequirenent : P H Chec e / ln'Cont#bl �, _, ate i",: pH Adtusied m..TegedlComnts Adjusted ,:� N Reaw ent ",Us , me B 250mLA+H2SO4 <2 Y I N! A� Y I N C 250mLA+H2SO4 <2 Y I N/ Y I N I I3 250mLP+HNO3 <2 of N / NA I Y I 1 NA Reagent Name ID Reacient Name ID Rea ent Name ID 1 3 5 2 1 4 6 pH Strip ID: l: �M. F20 C:IELMNTIPrintlwko_PreservationCheck. rpt Page 1 Mid Atlantic Engineering & Environmental Solutions November 26, 2018 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11 T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM RECEIVED DEC 0 4 Z018 CENTRAL FILES CMIR SECTIO ; Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on October 26, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE r,' , STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 FACILITY NAME Marsh Auto Parts, Inc. - Carvard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total`5usperided Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM),,mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total -Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 10/26/18 1.30 7.1 12 <2.10 <4.7 <0.00310 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled Stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122, Form SWU-251, lost revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." S Name (Print name) 8sr Title ( tt title) C A� 3X.-� Signaty" Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter North Carolina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) t-Z�-�� (Date Form SWU-251, last revised October25, 2012 Page 2 of 2 ENCO Laboratones Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, November 8, 2018 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CB06058 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 26, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full, Page 1 of 9 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C606058-01 Sampled: 10/26/18 09:20 Received: 10/25/18 13:45 Parameter EPA 16645 Preparation EPA 1664E Hold DatelTime(sl 11/23/18 Prep DatelTime(sl 11/01/18 12:25 Analysis DaWriime(s) 11/05/18 11:39 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:23 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:03 SM 254OD-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 Client ID: Truckyard A Lab ID: CB06058-02 Sampled: 10/26/18 09:40 Received: 10/26/18 13:45 Parameter EPA 1664B Preparation EPA 1664E Hold DatelTime(s) 11/23/18 Prep Date/Time(s) 11/01/18 12:25 Analysis Date/Time(s) 11/05/18 1139 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:26 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:22 SM 254OD-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 Client ID: Truckyard B Lab ID: CB06058-03 Sampled: 10/26/18 09:50 Received: 10/26/18 13:45 Parameter Preparation Hold DatelTime(sl Prep DateMme(51 Analysis DatelTime(s] EPA 1664E EPA 1664E 11/23/18 11/01/18 12:25 11/05/18 11:39 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:28 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:40 SM 254OD-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: CB06058-01 Anallta Elu MU P91 Units Method Motes Total Suspended Solids 12 2.5 2.5 mg/L SM 2544D-2D11 Client ID: Truckyard A Lab ID: CB06058-02 Ana Elan Hu EU Units Mathsd Notes Lead - Total O.00B47 3 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 14 3.1 3.1 mg/L SM 2544D-2011 Client ID: Truckyard B Lab ID: CB06058-03 Analxte Results flag MR4 E I. liniu Method hew Lead - Total 0.00510 3 0,00310 010100 mg/L EPA 6010D Total Suspended Solids 7.6 2.5 2.5 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 0 E., NS� www.encwlabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C506058-01 Received: 10/26/18 13:45 Matrix: Surface Water Sampled: 10/26/18 09:20 Work Order: CB06058 Project: Marsh Truck Parts Sampled By:CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENQ7 Cary ct10W awl [NC 5911 Analyte ICAS Numberl Results Elan mab 2E MU pQL Batch Method Analyzed by Notes Lead [7439-92-1]A 0.00310 U mg/L 1 0.00310 0,0100 8K06017 EPA 60100 11/07/18 10:23 IDH Classical Chemistry Parameters ^ - ENCO Cary cetifred analyte [NC 5911 Analyte rCAS Numberl Results fw9 l,lalls Di M12L PQL BAlch Method Analyzed Dy Notes Total Suspended SolldsA 12 mg/L 1 2.5 2.5 8130003 SM 2540D-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC nalyte ICAS Numberl RefulLs flag Units Df MQL EQL DAtch Method Analyzed JU Notes Ethylene Glycol[107-21-1] 4.7 U mg/L 1 4.7 5.0 8130004 EPA 8015C 10/31/18 08:03 JIB Sutr ZW= $gig RE Spike jyf % Rec % Rec Limps fidftt fy lza 1,3-81ly/ene Glycol 180 1 200 92 % 50-150 8J30004 EPA 8015C 10131118 08:03 JJ8 Classical Chemistry Parameters ^ - ENCO Aky nralk C&bfied analyte [NC 4421 Analyte rCAS Numberl )Results EW9 mom D.E M" E" zaf&h Method Analyzed By dotes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 81<01008 EPA 1664E 11/05/18 11:39 SMA Description: Truckyard A Lab Sample ID:CB06058-02 Received: 10/26/18 13:45 Matrix: Surface Water Sampled: 10/26/18 09:40 Work Order: CB06058 Project: Marsh Truck Parts Sampled By:CL]ENT Metals (total recoverable) by EPA 6000/7000 Series Methods A - Eft-0 Cory certitk+d analyte Analyte rCAS Numberl Results fig Units 2E HU j:Q6 WO JjrthQd Analyzed &y Note Lead [7439-92-1]A 0.00847 1 mg1L 1 0.00310 0,0100 8K06017 EPA 6010D 11/07/18 10:26 JOH Classical Chemistry Parameters ^ - ENM Cory cerNred analyze [NC 5911 Analyte rCAS Numberl ResuI flag Ua ty 12E mu PQL Batch Method Analyzed ILY h9twi Total Suspended Solids^ 14 mg/L 1.25 3.1 3,1 8130003 SM 254OD-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC Analvte ICAS Numberl Results f[89 Unks 2E lU E" A=b Method Analyzed By boles Ethylene Glycol[107-21-1) 4.7 U mg/L 1 4.7 5.0 0330004 EPA 8015C 10/31/18 08:22 J1B Sumaoates ggfy(g QE Spike Lvl % Rec % Rec A By ly2tu 1,3-Butylene Glycol 190 1 200 94 % 50-150 BJ30004 EPA 8015C 10131118 08:22 M Classical Chemistry Parameters ^ - EACD Jacksonville cer 1W anaVe [NC 4421 Analyte rCAS Numberl $will flag Units 2E M" E9.6 Batch Method Analyzed Ay Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 BK01008 EPA 1664B 11/05/18 11:39 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Ce Ni'S = M1) ko www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CB06058-03 Received: 10/26/18 13:45 Matrix: Surface Water Sampled:10/26/18 09:50 Work Order: CB06058 Project: Marsh Truck Parts Sampled By: CLIENT (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary cerVrred ana4 to [NC 591] Analyte rCAS Numberl Results Ekg MAim Df H2L EQL IlAk]y Meth wed Notes Lead [7439-92-1]^ 0.00510 I mg/L 1 0,00310 0.0100 8KO6017 EPA 6010D 11/07/18 10:28 JDH Classical Chemistry Parameters ^ - ENW Cary —b&d analyse (NC 591] Analvte 1CAS Numberl gesu]E[ag Units QF mu E" Batcb Method gold $y Note� Total Suspended Solids^ 7.6 mg/L 1 2.5 2.5 BJ30003 SM 2540D-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC Analvte fCAS Numberl $esu] Elm MD& 2E M" pQL $iyb Method Analvzed By ARW Ethylene Glycol[107-21-1] 4.7 u mg/L 1 4.7 5.10 8330004 EPA 8015C 10/31/18 08:40 JIB Surrvaab= RE Spike %H,<F %RecLim/ts &11"A Meths dBY Notes 1,3 eurylene Glycol 200 1 200 98 % 50.150 8J30004 EPA 8015C 10131118 08,40 UB Classical Chemistry Parameters ^ - ENCO aadcsanv111e certified analyse [NC 442] Analvte [CAS Numberl Resultc ELU Ulm Qf HRL E" BA= Method i y Noteg Oil & Grease (HEM-SGT) Non -Polar 2.70 Ll mg/L 1 2.70 5.00 8KO1008 EPA 1664B 11/05/18 11:39 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 Ce ' C=0 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batd!il SK06017 - EPA 3005A Blank (8K06017-BLK1) Prepared, 11/06/2018 10:41 Analyzed: 11/07/2018 10:04 Spike Source %REC RPD Anal ldg Result Elag E L Units Level Result %REC Limits RPD Limit Notes Lead 0.00310 U 0,0100 mg/L LCS (8K06017-BSI) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:10 Spike Source %REC RPD Analyt l+ Result flag FQ.L Units Level Result %REC Limits RPD Limit Notes Lead 0.195 0.0100 mg/L 0.200 98 80-120 Matrix Spike (BK06017-MS1) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:13 Source:CB14770-04 Spike Source %REC RPD Anal Yte Result Flag P L Units Level Result %REC Limits RPD Limit Notes Lead 0.191 U100 mg/L 0200 0,00310 U 96 75-125 Matrix Spike Dup (8K06017-MSD1) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:16 Source: CB14770-04 Spike Source %REC RPD Anal tde Result Ela9 QQL 111111t5 Level Result %REC Limits RPD Limit Notes Lead 0.189 0.0100 mg/L 0.200 0.00310 U 94 75.125 1 20 Post Spike (SK06017-PSI) Prepared: 11/061201B 10:41 Analyzed: 11/07/2018 10:18 Source: C614770-04 Spike Source a/oREC RPD Analyt Result E1ag P_ L Units Level Resul %REC Limits RPD Limit Notes Lead 0.205 0.0100 mg/L 0.200-0.000768 102 80-120 Classical Chemistry Parameters - Quality Control Batdi &730003 - NO PREP Blank (8330003-BLKI) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD Analyt e Result E149 P.QL Units Level get %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (8730003-BSI) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD Anal lt Result flag P_QL Units Level Result MoREC Limits RPD Limit Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 Duplicate (6330003-DUPi) Prepared & Analyzed: 10/30/2018 10:02 Source:CB15181-01 Spike Source °/oREC RPD Analyt Result Flag £QL Udts Level Result 0/aREC Limits RPD Limit Dotes Total Suspended Solids 2700 500 mg/L 2200 19 20 Duplicate (8330003-DUP2) Prepared & Analyzed: 10/30/2018 10:02 Source: C816046-01 Spike Source %REC RPD 9nalyte Result El" QQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 220 50 mg/L 230 4 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 8730004 - NA Blank (8730004-8LK1) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 06:59 Spike Source %REC RPD -AQaw" Result Elm RIX Unit5 Level Result %REC Limits RPD Ljmji Notes Ethylene Glycol 4.7 U 5.0 mg/L 1,3-8uty/e7e Glycol 210 mg/L 200 105 50.150 LCS (8330004-BSI) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 07:18 Spike Source °/DREG RPD Anal Yte Result Etas P9S VAM Level gqsug %REC Limits RPD Limit Notes Ethylene Glycol 230 5.0 mg/L 200 117 70-130 1,3-Sid# a Glyral 200 mg/L 200 102 50-150 LCS Dup (8330004-BSDI) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 07:36 Spike Source %REC RPD Anal I Result Et" PQL Units Level Resul %REC Limits RPD umlt Notes Ethylene Glycol 240 5.0 mg/L 200 118 70-130 0.8 25 1,3-Butylene Glycol 190 m91L 200 93 59-150 Classical Chemistry Parameters - Quality Control Batch 8K01008 - EPA 1664B Blank (8K01008-BLK1) Prepared: 11/01/2018 12:25 Analyzed: 11/05/201B 11:39 Spike Source %REC RPD -Aa8h[te Result Flag PM Units Level Result %REC Limits RPD Ljmlt Notes Oil & Grease (HEM-5GT) Non -Polar Material 2.70 U 5.00 mg/L LCS (SK01008-BSI) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2016 11:39 Spike Source %REC RPD Anal lrte Result flag PQL Units Level Result %REC Limits RPD Lmh Notes Oil & Grease (HEM-SGT) Non -Polar Material 78.6 5.00 mg/L 823 96 64-132 LCS Dup (8K01008-BSDI) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Anal Yta Result Flag Pal. SJnits Level Result %REC Limits RPD LW Notes Oil & Grease (HEM-SGT) Non -Polar Material 86.8 5.00 mg/L 80.0 108 64-132 10 34 Matrix Spike (8K01008-MS1) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Source: BB04387-03 Spike Source %REC RPD Anal rte Res eul Elm PQL units Level Result %REC LjmiU RPD Ljm]t Notes Oil & Grease (HEM-SGT) Non -Polar Material 86A 5.00 mg/L 84.4 6.12 95 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 CIFNA mom www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 1 _ O 10775 Ceritral Pon Dr. 4810 Etcecutrve Park Court Suite 1 11 102-A Woodwinds Industrial Ci, Orlanda, FL 32824 Jaticsonvilie. FL 32216.6069 Cary, NC 27511 (407) a26-5314 Fax (407) a50-6945 (904) 296-3007 Fax (904) 296-6210 1919) 467-3090 Fax (919) 467-3515 Page of Clierd Name Marsh Truck Parts (MA435) Pm►«x Number [name] Requested Anatyees Requestied Turnaround Times Note : Rush requasts subieat to acceptance by -the facility _ Standard — Expedited Due _!_/ cg = v7 r - m Cp ❑ t:4 L�� Address P.O. Box 427 Pmoot NamoiDe_sc Marsh Truck Parts Cltyr3T-P Si ler City. NC 273" PO it ! 6e1ing info Tel (919) 663-1908 Fax Reporting Contact Steve Marsh Sampler(s) Name. Affiliation (Print) Bit Contact 18hu ck Hoffman sam"(s) signature Site Location! Time Zone Lab Workordt3r koJ - Preservation {Sae Codes) (Combine as necessary► Item it sample 10 (Field Identilkabon) Collection Pate Collection Time Camp / Grab - Mabbc (eee codes) Total it of Comainers Sample Comments d - - F`3L ,wwSW 7 X X` X. Tlruc and A •Z�-- wt SW 7 X X X X Tic rd B-' �ZL�- s5d. /�7. SVv.R X x x X <-- Total #,of Containers sample Kit Prepared By Dat crime Relinquished By Datefrime By Datarruna ntsrSpecial Reporting Requirements Relirtgwshed Dafarl-vne Received lay V. DatarTime jr Relinquished By DaWriime neceNed By DatelTime or s sf 1 Tamp oror, Receipt Condition pon Receipl 4- ' Acceptable Unacceptable KatnX : GW-GrottrWwatar"SO-SOU DW-Drinfung Water SE -Sediment SW -Surface Water WW-Wastmater.'A-Air 0-0ther (deta9ln comments) Preservation:1-tcie H4iCI. N+W03.5-1­12SO4 NO-NoOH0-Mer (detail in comments) w Note: An samples submrted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist .o Sample Preservation Verification .- �. alp ENCO Cary Work Order: .CB06058 Project; Marsh Truck Parts Client; Marsh Truck Parts (MA035) Project #: [none] Logged In: 27-Oct-18 10:15 Logged By: John C King Preservation Check Performed By: 4 DalelTime: /IX713- //LO CB06058-01 Cont T pe f YRea—gentJ Requ �errte)nt p Iln Control ' pH Adjusted Ad used ` gUsedfcomments i B 1 LA+H2SO4 <2 1 N 1 NA Y 16 1 NA C 1 LA+H2SO4 <2 I N I NA Y /�141 ' 1 NA D 250mLP+HNO3 <2 IN NA Y I 1 NA CB06058-02 Conn Type =Pres p } R6q"uire'rne6t` pH C ecke 1 :In.Control pH Adjusted DatelTme s ; Adiusted ;Reagent UsedlEomments ' B 1 LA+H2SO4 <2 f( j' ! N 1 NA Y ! X1 NA C 1 LA+H2SO4 <2 I N I NA Y I 1 NA D 250mLP+HNO3 <2 I N I NA I Y/ 1 NA CB06058-03 _ Cont T pe y r. Pres H (P. } Requirement H Checked P,. �- Y" in Control pH Adjusted ' Dat ; ime Adjusted - r ,, - . ? " , " ] fieagenttUsedlCamments r B 1 LA+H2SO4 <2 / N I NA Y 1 ^/ NA C 1 LA+H2SO4 <2 69/ N! NA Y I 1 NA D 250mLP+HNO3 <2 Y I N I NA Y I / NA Rea ent Name ID 1 2 pH Strip ID: Reacient Name ID Rea ent Name ID 3 5 4 6 C:IELMNTIPrintlwko_PreservationCheck.rpt Page 1 Mid Atlantic Engineering & Environmental Solutions April 26, 2017 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: 409 Rogersvew Court Ralcie, NC 27610 office 919.250.9918 facsimile 919.250,9950 MAAONLINE.COM RECEIVED MAY 0 4 20f17 CENTRAL FILES D1NR SECTIOA! Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on April 6, 2017 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and'ethylene glycol.- As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 FACILITY NAME Marsh Auto Parts, Inc. - Caryard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh _ PHONE NO. 919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. __Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), : mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 4/6/2017 1.5 6.7 6.1 8.82 <4.0 0.00314 J NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) #J ^o T A - - Title (Print title) O Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 6 � W C`7 Date/ "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �E (Signature of r ittee or Designe( 45 _—Z,,, l (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 'E NiCO Laboraton'es Accurate. Timely. Responsive. Innovative. 102-A Woodwinds industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, April 20, 2017 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CA02359 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, April 6, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduoed in full. Page 1 of 9 (�IJ�Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CA02359-01 Sampled: 04/06/17 08:00 Received: 04/06/17 20:00 Parameter Hold Date/Time(s) Prep DatelTimefsl Analysis DatelTimefsl EPA 1664A 05/04/17 04/07/17 16:35 04/11/17 14:52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:55 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 09:53 SM 2540D-1997 04/13/17 04/11/17 12:4S 04/11/17 12:45 Client ID: Truckyard A Lab ID: CA02359-02 Sampled: 04/06/17 08:15 Received: 04/06/17 10:00 EArameter Hold Date/Time(s) Prep Date/Time(sl Analysis Date/Time(s) EPA 1664A 05/04/17 04/07/17 16:35 04/11/17 14:52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:43 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 10:12 SM 2540D-1997 04/13/17 04/11/17 12:45 04/11/17 12:45 Client ID: Truckyard B Lab ID: CA02359-03 Sampled: 04/06/17 08:30 Received: 04/06/17 10:00 Parameter Hold DatelTimefsl Prep Date/Time(s) Analysis Date/Timefs] EPA 1664A 05/04/17 04/07/17 16:35 04/11/17 i4;52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:58 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 10:31 SM 254OD-1997 04/13/17 04/11/17 12:45 04/11/17 12:45 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 �eo www.encolabs.corn SAMPLE DETECTION SUMMARY :1 Client ID: Caryard Lab ID: CA02359-01 Anal rke Results flag M26 P91 Units Method Notes Lead - Total 0.00314 1 0.00310 0.0100 mg/L EPA 6010D Oil & Grease (HEM-SGT) Non -Polar Material 8.82 2.70 5.00 mgjL EPA 1664A Total Suspended Solids 6.1 2.5 2.5 mg/L SM 2540D-1997 Client ID: Truckyard A Lab ID: CA02359-02 Anal vbe Results flag MDL Poll. Units Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 20.2 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 6.8 2.S 2.5 mg/L SM 254OD-1997 Client ID: Truckyard B Lab ID: CA02359-03 Analvte Results flag MOL POL Units Method Notes Total Suspended Solids 2.8 2.5 2.5 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced 0 tull. Page 3 of 9 Description: Caryard Matrix: Surface Water ANALYTICAL RESULTS Lab Sample I D: CA023 59-01 Sampled: 04/06/17 08:00 Project: Marsh Truck Parts Sampled By: Client Metals (total recoverable) by EPA 6000/7000 Series Methods CE NikC� www.encolabs.com Received: 04/06/17 10:00 Work Order: CA02359 ^ - ENCO Cary certified dnatyte (NC 5911 Iyte_fCAS Numberl Results flag Units PIE MDL POL Batch Method Analyzed Ply Notes Lead [7439-92-1]^ 0.00314 ) mg/L 1 0.00310 0.0100 7DO7010 EPA 6010D 04/11/17 11:55 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified arraW (NC 591J AnalM [CAS Numberl Results fjlg Units pf Mu POL Batch Method Analyzed U Notes Total Suspended Solids^ 6.1 mg/L 1 2.5 2.5 71)11003 SM 254OD-1997 04/11/17 12:45 OMR Non -Halogenated Semivolatile Organics by GC A0alyte [CAS Numberl Results Elm Units RE MDL EJ Batch Method Analyzed Ay Notes Ethylene Glycol(107-21-11 4.0 U mg/L 1 4.0 10 7D10008 EPA 8015C 04/10/17 09:53 )JB Surrogates Results 2E &Jke Lv °rb Rec % Rec Lim 9A Method Analyzed AV Notes 113-Sutylene Glycol 180 1 200 92 % 50-150 7DI0008 EPA 8015C 0411011709:53 338 Classical Chemistry Parameters Analyte rCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Description: Truckyard A Matrix: Surface Water Project: Marsh Truck Parts Results E.i89 Units PIE Mph F_Qk Batch Method Armed A-Y tiote 8.82 mg/L 1 2.70 5,00 7DO7014 EPA 1664A 04/11/17 14:52 SMA I ab Sample ID:CA02359-02 Received: 04/06/17 10:00 Sampled: 04/06/17 08:15 Sampled By: Client Work Order: CA02359 Metals (total recoverable) by EPA 6000/7000 Series Methods I ^ - ENCO Cary certified analyze (NC 5911 Analyte FQS Numberl Results fka Units RE MIDL E" patch Method Analyzed lay Notes Lead [7439-92-11^ 0,00310 U m91L 1 0.00310 0,0100 7007010 EPA 6010D 04/11/17 11:43 JMV Classical Chemistry Parameters ^ - ENCO Cary certired a-0-1[NC 591] Analyte rCAS_Number] Results Elm Ynits PIE MDL POL Batch [Method Analyzed gy Notes Total Suspended Solids^ 6.8 mg/L 1 2.5 2.5 7D11003 SM 2540D-1997 04/11/17 12:45 OMR Non -Halogenated Semivolatile Organics by GC Analyte rCAS_Numberl Results EW9 Units RE MOL pew Batch Method Analyzed gy Ethylene Glycol[107-21-11 4.0 U mg/L 1 4.0 10 7D10008 EPA SG15C D4/10/17 10:12 BB Surrogates Results P_f Spikev! °I°Rec R meth Analyzed By Notes 1,3-6utylene Glycol 170 1 200 87 % 50-150 7DI0008 EPA 8015C 04/1011710:12 338 Classical Chemistry Parameters Analyte rCAS_Numberl Results Elms YLIU RE MDL F_Q1. Batch Method Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar 20.2 mg/L 1 2.70 5.00 7DO7014 EPA 1664A 04/11/17 14:52 SMA Material FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 (E�Cmo www.encolabs.com ANALYTICAL RESULTS' Description: Truckyard B Lab Sample ID:CA02359-03 Received: 04/06/17 10:00 Matrix: Surface Water Sampled:04/06/17 08:30 Work Order: CA02359 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - fNCO Cary ceMfied amlyte [NC 5911 Analvte TCASNumber] Results F1f9 Units PFF MDL P4L aalc�h Method Analyz By Notes Lead [7439-92.1]^ 0.00310 u mg/L 1 0.00310 0,0100 7DO7010 EPA 6010D 04/11/17 11:58 ]MV Classical Chemistry Parameters ^ - FNCO Cary -rh&d analyte (NC 5911 Analvte TCAS Numberl Results fig Units PF PL P_4.6 Batch Method Analyzed 13Y Notes Total Suspended Solids^ 2.8 mg/L 1 2.5 2.5 7D11003 SM 254OD-1997 04/11/17 12:4S OMR Non -Halogenated Semivolatile Organics by GC Analvte TCAS Numbed Results Eft Units Pf Ma PQ1 Batch Method nA alvxed By Notes Ethylene Glycol(107-21.1] 4.0 u mg/L 1 4.0 10 7010008 EPA 8015C 04/10/17 10:31 ]]B 1frr IllaP-f Spike LV G Re % Rec limits Batch Method Anagx Notes 113-8utyleae Glycol 180 1 200 97 % 50-150 7D10008 EPA 8015C 041101171021 JiB Classical Chemistry Parameters AnaMe TCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results Flag Units PE MP6 PQL Batch Method Analyzed By Notes 2.70 Ll mg/L 1 2.70 5.00 7DO7014 EPA 1664A 04/11/17 14:52 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 (��Cmo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7DO7010 - EPA 3003A Blank (7D07010-BLK3) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 10:24 Spike Source %REC RPD -An&Ac Result Ilan P9.L Units Level Result %REC Limits RPD 'mi Notes Lead 0.00310 U 0.0100 mg/L LCS (7D07010-BSI) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:36 Spike Source %REC RPD Anal llZe Result Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0.202 0.0100 mg/L 0.200 101 80-120 Matrix Spike (7D07010-MS1) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:46 Source: CA02359-02 Spike Source %REC RPD AnWA4o Result Flaq PQL Units Level Result %REC Limits RPD Limit Notes Lead 0.199 0.0100 mg/L 0.200 0.00310 U 99 75-125 Matrix Spike Dup (7D07010-MSDI) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:48 Source: CA02359-02 Spike Source %REC RPD Ana]Ae Result Flap POL units Level Result %REC Limits RPD Limit Notes Lead 0.201 0.0100 mg/L 0.200 0.00310 U 101 75-125 1 20 Post Spike (7D07010-PS1) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:50 Source: CA02359-02 Spike Source %REC RPD Anal lde Result Flag POI Units Level Result 0/DREG Limits RPD Limit Notes Lead 0.195 0.0100 mg/L 0.200 0.00145 97 80-120 Classical Chemistry Parameters - Quality Control Batch 7D11003 - NO PREP Blank (7D31003-BLK3) Prepared & Analyzed: 04/11/2017 12:45 Spike Source %REC RPD Anal Yte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7D11003-BSI) Prepared & Analyzed: 04/11/2017 12:45 Spike Source %REC RPD .Analvte Result Mau POL Units Level Result %REC Ornits RPD Limit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80.120 Duplicate (7DI1003-DUPI) Prepared & Analyzed: 04/11/2017 12:45 Source: CA01319-01 Spike Source %REC RPD Anande Result Ftaq POL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 240 50 mg/L 240 2 20 Duplicate (7D11003-DUP2) Prepared & Analyzed: 04/11/2017 12:45 Source: CA03276-01 Spike Source %REC RPD Analyt Result Elag P_Q1 Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2200 250 mg/L 1700 23 20 QM-12 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 (��Cmo www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 7D20008 - NA Blank (711310008-BLKl) Prepared: 04/10/2017 08:40 Analyzed: 04/10/2017 08:56 Spike Source °/uREC RPD Analvte Result Flan 19L units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 4.0 U 10 mg/L 1,3-8utylene Glycol 180 mg/L 200 91 50-150 LCS (7D10008-BS1) Prepared: 04/10/2017 08:40 Analyzed: 04/10/2017 09:15 Spike Source %REC RPD -Analvte Result Flag PQL Una Level �u %REC Limits RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 101 70-130 1,3-8utylene Glycol 170 mg/L 200 84 50-150 LCS Dup (71>10008-BSDi) Prepared: 04/10/2017 08:40 Analyzed: U4110/2017 09:34 Spike Source %REC RPD Analvte Resuk Elag P41 units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 210 10 mg/L 200 103 70-130 2 25 1,3-6utylene Glycol 170 m9/L 200 85 50-150 Classical Chemistry Parameters - Quality Control Batch 7DO7014 - EPA 2664E Blank (7D07014-BLK1) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Spike Source %REC RPD Andlvts Result Flag SQL Una Level Result %REC Liimib RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (7D07014-BS1) Prepared: 04/07/20t7 t6:35 Analyzed: 04/11/2017 14:52 Spike Source %REC RPD Anal lrse Result Flag P91 mrliti Level Result %REC Limits RPD Liml Notes Oil & Grease (HEM-SGT) Non -Polar Material 69.3 5.00 mg/L 73.0 95 64-132 LCS Dup (7D07014-BSDi) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Spike Source %REC RPD -Analvte Result Flag P-0L Units Level Resul %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 79.7 5.00 mg/L 73.8 108 64-132 14 34 Matrix Spike (7D07014-MS1) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Source: BA01428-01 Spike Source %REC RPD .Analvte Result Flag POL Una Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 57.8 5.00 mg/L 74.6 2.70 U 77 64-132 FINAL. This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (�09 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced kn full. Page 8 of 9 PtIVIRONMENTAL•CONSEFlVATION LA9tyRATORIES .CHAIN!'OF;-CUST'OOY; RECORD• www,anc41abi.caon -�'� •+;..:`• qji/.l srifll. 11i •Coan4il�n;ftf,nitl{AAs iill 1!".SAj�#]ivrl�i�liKSYM(o1i`•3 "��! 4{isi►}7,ii'_,^d]c� ,!►c:scnvin�ftin�aat>s� � G.ry�a17Sthrr W17iKmor-4,. vl- mltv6witldy ;�i��M+jai:t ru• FiCrl �,yiitt:r llilu •�1s47;G .raiterH{+rr SRt{i I3EV.? of .� j�•ma1lnIII Im Arrly.F �'idrrr •,rs_3no[�lf iittlaf+,"!iF,nrtu. fl>'r� �ni nnr� lllru V, �5111-.��i11C.l aj'� �:pl7M_ + Fis[r, tv t.: ,7uun, I l� �itiSiliFt !llli[ryl�t.li}'i G+7!1'`�11nN 111IrI.r 111Il.IIA, lumicab '}�. titICCRY:1tjV' EPJ+rlimrl C�: iurla�'4!Iit1 Hi1'1F17t:ir. � �%y •3a;ilr-'i, y11�f�YC'i 1! - - 1 � ! FJl:ll%>f.{jYf rd�indnitnfi�l}:.A.k (14\'�Ottkt�IWII3�i 59k9fFll1IMI .�f11.'�Lit� is IMI41."WW-Y;.S71 .A All (;;QGgll ET.M011 F11 mt,111l rValu aguill Iiwlwt'la�nttrl{Pd':J 1Si:li'I.M73'k�:'!1'•G'al lc klYl i�il�nlelailui'll� rlf if -A1 iri'llm-rlllmiuli! tT 1!6 W 1.1171'i1I111;il11%DX k qmv' +1Ir31la UM II' jTI I DIM 11 iil1.IWAli 931111 n jI Ww4,s itl3, I�7lin, !Fills, f 1 Rr sl7l m pyllIIL'iItCFIIi:rtxLii Sample Pre_ s'ervation'Verification -ENCO Cery w6i'k owe-i". rA02W.9 PI Ktirsh Truckparts client Mamb True # PsA3 (MA0,3351 PTdic,-t fnDricj Lagga.J Irt: 664.rr17 1127 Logged Sy. P a ch c-I Ann :Y6rff s',i dart; R I&NAMfiiiii., JpH-� IIV UREd Pg��-u fin b ;itVrrIAW2SO4 � y I N i NA --Y-!.N I' C 2,E4DrrI.LAtI-r29DA �,Z y M INABj Y W),'��A f) jZ'fAI'"RrHNOI3 N / NA "Y fr � j tjA CAOi959-02 A El ji6bhiLA--412G 0.4 y I N �4. J'Y I N tt2 1,250fr.LA-H.IS04 Y'l h J iLN� pjy .,7& 0 1'2Wir.04-MN03 ;:2. Dy N I "I .; y I M"I pk% Pk Ild 'Wo/TTM5' cagcoc Et �c�lGan,ments� Y N km Y1 N-/�n) ]2'50;0-A'411z -c2 Y N XtjS' y 'I N IIVA). D jZ,-Q'fr.1;P-t-HfK)3 tY 1 hi I fqI- - Y f 14A Reagent Name ID 4 Kr ant NdrnG-. 5. 0 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 21316 FACILITY NAME Marsh Auto Parts Inc. - Ca and COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. 919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 r-Lab #_ PLEASE REMEMBER TO SIGN ON THE REVERSE 4 t1 CEf1Veb Part A: Stormwater Benchmarks and Monitoring Results JAN 0 S 2017 For sampling periods with no discharge, you mUstsubmit this discharge monitoring form noting "No Flow" or "No Discharge" within h,- �. 4 r--,L+-A 30 days of the end oflthda~{periQdjt�o comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 1QQ/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 11/29/2016 1.25 7.1 42 18.1 <4.0 NA NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 %_ r A STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." 12- lw1AI Name (Print name) Title (Print title) lrz,�,4 Sie tore Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 Z, 3- Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ure of Permittee or Designee) [Date) Form SW U-251, last revised October 25, 2012 Page 2 of 2 g E NCO La-boralones Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court RECEIVED Cary NC, 27511 �I n17 Phone: 919.467.3090 FAX: 919.467.3515 JA N 0 � �u k r CENTRAL FILES Friday, December 9, 2016 DWR SECTION Marsh Truck Parts (MA035) Attn: Steve Marsh P.Q. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none), Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CZ12424 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, November 30, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 (J�Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CZ12424-01 Sampled: 11/29/16 15:00 Received: 11/30/16 13:00 Parameter Hold Date/Time(s) Prep DatelTirngU) Analysis Date/Time(sl EPA 1664A 12/27/16 12/07/16 11:31 12/08/16 17:51 EPA 8015C 12/13/16 12/06/16 05:12 12/06/16 09:25 SM 2540D-1997 12/06/16 12/01/16 13:30 12/01/16 13:30 Client ID: Truckyard A Lab ID: CZ12424-02 Sampled: 11/29/16 16:15 Received: 11/30/16 13.00 Parameter Hold Date/Time(sl prep Date/Time(s) Analysis QatelTi[DCUs EPA 1664A 12/27/16 12/07/16 11:31 12/08/16 1T.51 EPA 8015C 12/13/16 12/06/16 05:12 12/06/16 09:44 SM 2540D-1997 12/06/16 12/01/16 13:30 12/01/16 1130 Client ID: Truckyard B Lab ID: CZ12424-03 Sampled: 11/29/16 16:30 Received: 11/30/16 13:00 Parameter Hold DatelTimefs) Prep DatelTime(s) Analysis DatelTime(s) EPA 1664A 12/27/16 12/07/16 11:31 12/08/16 17:51 EPA 8015C 12/13/16 12/06A6 05:12 12/06/16 10:03 SM 25401)-1997 12/06/16 12/01/16 13:30 12/01/16 13:30 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 e NISO-E www.encolabs.com SAMPLE DETEC710N SUMMARY Client ID: Caryard Lab ID: CZ12424-01 Analyte RasuI.Ss El49 MOO M Units Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.1 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 42 5.0 5.0 mg/L SM 2540D-1997 Client ID: Truckyard A Lab ID: CZ12424-02 Anal vte es I Flag M2L POL Units Mdhod Notes Total Suspended Solids 470 33 33 mg/L SM 254OD-1997 Client ID: Truckyard R Lab ID: CZ12424-03 Analyte Results E109 MDL POL Utlits Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 16.8 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 82 5.0 5.0 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced m full. Page 3 of 9 (�J�09 www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:CZ12424-01 Received: 11/30/16 13:00 Matrix: Surface Water Sampled:11/29/16 15:00 Work Order: CZ12424 Project: Marsh Truck Parts Sampled By: Client Classical Chemistry Parameters ^ - ENCO Cary cer* ad anatyfe (NC 5911 Analyte rCAS Numberl Results flag Units PF MDJ EBatch Method Analyzed By Notes Total Suspended Solids^ 42 mg/L 2 5.0 5.0 6LO1002 SM 2540D-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile Organics by GC Analyte rCAS Numbers RPcrrltc Flag unitS PFMDL PQ Batch Method Analyzed Ay Notes Ethylene Glycol[107-21-1] 4.0 U mg/L 1 4.0 10 6LO6001 EPA 8015C 12/06/16 09:25 318 Surrogates Results pf Spike Lv1 % Ret % Rec Limits Batch Method An Rk Notes 1,3-Butylene Glycol 170 1 200 85 % 50-150 6LO6001 EPA 8015C 12106116 09:25 JJe Classical Chemistry Parameters Analyte KAS Numberl Results flag Units 2f MDL EQ1 PAtch Method Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar 18.1 mg/L 1 2.70 5.00 6LO7004 EPA 1664A 12/08/16 17:51 SMA Material Description: Truckyard A Lab Sample ID:CZ12424-02 Received: 11/30/16 13:00 Matrix: Surface Water Sampled:11/29/16 16:15 Work Order: CZ12424 Project; Marsh Truck Parts Sampled By:Client Classical Chemistry Parameters ^ - ENCO Cary certified analyte (NC 5911 Analyte ICAS Numberl Results Flacl Units pf MDL p4J Batch Method Analyzed Ay Notes Total Suspended Solids^ 470 mg/L 13.3 33 33 61-01002 SM 2540D-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile Organics by GC Analyte ICAS Numberl Results fig Units PIE MDL g4 Batch Method Analyzed fty Notes Ethylene Glycol[107-21-1] 4.0 U m9/L 1 4.0 10 6LO6001 EPA 8015C 12/06/16 09:44 138 Surrogates: Results _Df Soike L v1 % Rec % Rec Llmirs Batch Method Analyzed & Notes 1,3-Butylene Glycol 160 1 200 82 % 50-150 CLO6001 EPA 8015C 12106116 09.,44 JJ8 Classical Chemistry Parameters Analyte rCAS Numbers Results f]Pg Units Q MDL POL Batch Method Ana vl zo By Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U mg/L 1 2.70 5.00 6LO7004 EPA 1664A 12/06/16 17:51 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 (�Cmo www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CZ12424-03 Received: 11/30/16 I Matrix: Surface Water Sampled:11129/16 16:30 Work Order: CZ12424 Project: Marsh Truck Parts Sampled By: Client Classical Chemistry Parameters ^ • ENCO Cary cedrfied analyte [NC 5911 bnalM FCAS Number] its ELQ Units Pf MDL POL Batch Method Analyzed ft Notes Total Suspended Solids^ 82 mg/L 2 5.0 5.0 6LO1002 SM 25400-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile organics by GC Analyte rCAS Number] Ethylene Glycol(107-21-11 Resulfa E119 Units PIE MAS PQ Batch Method Analyzed 131t Notes 4.0 U mg/L 1 4.0 10 6LO6001 EPA 8015C 12/06/16 10:03 330 5urroaates Rea pE S"I e L v! 0/o Rec % Rec Limits 8atth Method Analysed $y Notes 1,3-Butylene Glycol 170 1 200 66 % 50-150 6LO6001 EPA 8015C IZ10611610:03 -US Classical Chemistry Parameters Analvte ICAS-NUmber] Oil & Grease (HEM-SGT) Non -Polar Material Results FlA9 PAM QE MPS PQ Batch Method Analyzed PY Notes 16.8 mg/L 1 2.70 5.00 6L07004 EPA 1664A 12/08/16 17:51 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 (E�Cmo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6LO1002 - NO PREP Blank (6L01o02-BLKl) Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD .Analyte Result Flpq P_OL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (6L01002-BS1) Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD Analyte Rwult Flag M Units Level Result %REC Limits RPD Limit Notes. Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (6L01002-DUPI) Prepared & Analyzed: 12/01/2016 13:30 Source: CZ16873-01 Spike Source %REC RPD -Analvte Result Flao POL Units Level Resut °/aREC Limits RPD Limit Notes Total Suspended Solids 330 100 mg/L 340 4 20 Duplicate (6L01002-DUP2) Prepared & Analyzed: 12/01/2016 13:30 Source: CZ07890-01 Spike Source %REC RPD Analvte Result Fla_4 POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 62 25 mg/L 57 8 20 Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 6LO6001 - NA Blank (61-06001-BLK1) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 07:31 Spike Source %REC RPD Analyte Result Flag PQL ILnits Level Result %REC Limits RPD limit Notes Ethylene Glycol 4.0 U 10 mg/L 1,3-8utylene Glycol 190 m9/L 200 95 50-150 LCS (6L06001-BSI) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 07:50 Spike Source %REC RPD _Analyte Result FIa9 POL Units Level Result %REC Limits RPD i i Notes Ethylene Glycol 180 10 mg/L 200 92 70-130 1,3-8utylene Glycol 190 mg/L 200 94 50-150 LCS Dup (6L06001-BSD1) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 08:09 Spike Source %REC RPD .Anplvte R@sult FIa9 PQL Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 180 ID mg/L 200 92 70-130 0.8 25 1,3-8utylene Glycol 180 mg/L 200 88 50-150 Classical Chemistry Parameters - Quality Control Batch 6LO7004 - EPA 1664B Blank (6L07004-BLK1) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Spike Source %REC RPD Anallde Result Flag P-OL Units Level Result '/oREC Limits RPD IL-dit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 (��Cme) www.encOlabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6L07004 - EPA 1664E - Continued LCS (6L07OO4-BS1) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Spike Source %REC RPD Analvfe Result Flaq l°QL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 68.5 5.00 mg/L 78.7 87 64-132 LCS Dup (GLO7004-135131) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Spike Source %REC RPD Anal Yte Result Eau P_QL YALU Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 81.2 5.00 mg/L 80,0 102 64-132 17 34 Matrix Spike (6L070O4-MSI) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Source: BZ05272-01 Spike Source %REC RPD AnaJvte Result Flan POL Units Level Resul o/4REC Limi RPD i!mft Notes Oil & Grease (HEM-SGT) Non -Polar Material 105 5.00 mg/L 83.3 97.9 9 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (��Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 or 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Central Port Dr. 4810 Exocubve Park Court, Suite 111 102-A Woodwinds Industrial Ci. Orlando, FL 32824 Jacksonville, FL 32216.6069 Cary, NC 2.17611 (407) 828.5314 Fax (407) 850.6945 J9o4) 296-3007 Fax (904) 296-6210 (919) 467.3090 Fax (919) 467.3915 Page of Client Name Project Number Requested Analyses Requested Turnaround Times t Ivr1Aa31..5; [none] Addrow Projoct NamaiDenc Note : rlrrh rorrucets subJoci to O, % Marsh Truck Parts acceptance by the taciity Clty/STPZip PO b 1 Billing Info Sher C:it' NC 27344 17 Crt U] d G _ Standard Ter Fax Reporting Contact {91 663-1908 Steve Mars � h Q >• � �I L N _Expedited o"� Sampler(s) Name, Aflilfatien (Prim.) Billing Contact Chuck Hoffman �' LO 0 � (fj --�—�— Satnyrer(s) 5grlature Site Location 1 Time Zane Ub_ftrkorde'r , ••x �- ; r CI obi � ,� („ �, �•�,l 7 00 Q r ;12`, Preservation (See Codes) (Coridlne as r,er essary) COaction Malrix joist k 01 qom b Snmp:o ID (Fleid Identification) Collection Dais Tinto Comp! Grab (we codes) Contnrnnrs Sample Comments 1 ram. s G,ra b ,svi! 7 _ __ _ d ._1r..t' t._ .t i1,- _ -'), y!.i.�.t•'J _ �rru r �l L� � 5 '" t: r« - .f _j h. r:r �7_ _r 4 r t: _ , A ,J- �• i� p I t s ,. t r' t ..I ' :, _..... .I ,.. I•: �. n,r .... i. x,- br ! :;;•-s: -. Total # of Containers e Kit Prepared Hy llqprirrm Relinquished By Datoliime Received By DateXime _ LA-4 y O D temen r "I" irecn:s R :nqul5fiedBy DaieiTime DalorlLmo Re45By Goolei ri's 8, Tenops on Receipt Condition Upai Receipt V, t ' Acceptable unr' Matrix: GW-Grouru%zfer so•s«t DW-Drinking Water SE -Sediment SW-Surace Waler WW-Wastewaser A -Air O.Other (detail in comments) Preservation: I -Ice N-IfGI N-111,103 8.112SO4 NO-NUOri 0-01het (detail'u, comments) Note : All samples submitted to ENCO Labs are in accordance widt tJ* terms and conditions listed on the rcyarso of this tnnn, unless prior writien agreaments extst Sample Preservation Verification ENCO Cary Work Order: CZ12424 Client: Marsh Truck Parts (MA035) Logged In: 30-Nov-16 13:22 CZ1 2424-01 - Project: Marsh Truck Parts Project [none] Logged By: Andrew S Coons Cant T"' We P i, res'(IDH)�'.' pH.Cheeked"/ 4OH'Adi6itid:4, Used/Gb6i4nts,,�4,,--A�v-:,-, rement on Adjusted" aReagent, B 250rnLA+H2SO4 <2 Y NA Y kN NA C 250mLA+H2SO4 <2 Y N NA Y 16) NA D 1250ml-P+HNO3 <2 rY) N / NA Y (N) NA CZ12424-02 Corsi --,#",w 'T' nr Te "J --PresXPW�" 1, 17Q�t L We p H�� Checked 1 0 `-.In'C ntrol�,zEj 'H AdjU stddw. Reag6ptUsed./Comments B 250rnLA+H2SO4 <2 Y N �)N A Y /(N J� NA C 250mLA+H2SO4 <2 Y &N)l NA Y Q4).1 NA D 1250mLP+HNO3 <2 P) I N / NA I Y (N\i NA CZ1 2424-03 -Pres (pH):`. Requirement In-Control-O ' "Date ima0'Cont pHAdjdstedO Ad' §ted,;K� e646t,IjsecVCdftim6nts' ';"M B 250mLA+H2SO4 <2 Y (N"'J NA Y FN I NA C 250mLA+H2SO4 <2 Y I(N) NA Y NA D J250rnLP+HNO3 <2 Y N I NA Y i(—N NA Reagent Name ID 2 Reaqent Name ID 3 4 Reaqent Name ID Page 1 of 1 409 Rogers View Court M*gd Atlantic Raleigh. NC 27610 office 919,250.9918 Engineering &Environmental Solutions facsimile 919.250.99S0 MAAONLINE.COM December 27, 2016 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED Subject: STORMWATER SAMPLING RESULTS JAN 0 9 2017 MARSH AUTO PARTS, INC. — CAR YARD CENTRAL FILES 211 EAST 11T" STREET DWR SECTION SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on November 29, 2016 and analyzed for total suspended solids (TSS), pH, oil and grease and ethylene glycol (please note that the samples were not analyzed in the laboratory for total recoverable lead for the current sampling event): As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values, with the exception of Oil and Grease. Based on the results of the December 2016 sampling event, a Tier One Response has been implemented at the facility. Samples will be collected from each outfall during the January -June 2017 monitoring period and analyzed for TSS, pH, oil and grease, ethylene glycol and total recoverable lead. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE - "- r STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 FACILITY NAME Marsh Auto Parts, Inc. - Caryard _ COUNTYChatham PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. 919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50z i5 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 11/19/2015 1.5 7.1 17 <2.7 <4.0 0.00542 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-2S1, lost revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing ail the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) V"kGLA j Title (Print title) 1:�), --, Q \— tt— u-0 Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature od Permittee or Designee) (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 Mod Atlantic Engineering & Environmental Solutions December 22, 2015 NCDENR/DWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: RECEIVED JAN 0 5 2016 CENTRAL FILES DWR SECTION 109 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 90.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on November 19, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE -�TNI ENCO' Labor e Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, December 8, 2015 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C505861 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, November 19, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 10 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C505861-01 Sampled: 11/19/15 08.00 Received: 11/19/15 12:45 parameter EPA 1664A Hold Datg/Time(s) 12/17/15 Preppate/Timefsl 11/23/15 Analysis Rate/Time(s) 11:38 11/24/15 10:23 EPA 6010C 05/17/16 11/24/15 12:26 11/25/15 10:08 EPA 8015C 12/03/15 12/03/15 10:45 12/03/15 13:27 SM 254OD-1997 11/26/15 11/23/15 13:15 11/23/15 13:15 Client ID: TruckyardA Lab ID: C505861-02 Sampled: 11/19/15 07:00 Received: 11/19/15 12:45 Parameter EPA 1664A Hold Date/Time(s) 12/17/15 Prep Date/Time(s) 11/23/15 Analysis Date/Timg(s) 11:38 11/24/15 10:23 EPA 6010C 05/17/16 11/24/I5 12:26 11/25/15 10:27 EPA 8015C 12/03/15 12/03/15 10:45 12/03/15 14:05 SM 254OD-1997 11/26/15 11/23/15 10:40 11/23/15 10:40 Client ID: Truckyard8 Lab ID: C505861-03 Sampled: 11/19/15 07:15 Received: 11/19/15 12:45 Parameter Hold Date] -Time( s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664A 12/17/15 11/23/15 11:38 11/24/15 10:23 EPA 6010C 05/17/16 11/24/15 12:26 11/25/15 10:36 EPA 8015C 12/03/15 12/03/15 10:45 12/03/15 14:42 SM 254OD-1997 11/26/15 11/23/15 10:40 11/23/15 10:40 FINAL This report relates onfy to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 10 �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C505861-01 An�llde 130,iNl�i Elas MPJ= E91 Units Method Notes Lead - Total 0.00542 J 0.00310 0.0100 mg/L EPA 6010C Total Suspended Solids 17 3.3 3.3 mg/L SM 254OD-1997 Client ID: Truckyard A Lab ID: C505661-02 Anal Results ELM MP..!= F" lA& Method Notes Total Suspended Solids 42 8.3 8.3 mg/L SM 2540D-1997 Client ID: Truckyard B Lab ID: C505661-03 Anal vte Resu to EIM Mph E" Units Method Notes Total Suspended Solids 36 8.3 8.3 mg/L SM 254OD-1997 FINAL This report relates only Lo the sample as received by the laboratory, and may only be repmduced in full. Page 3 of 10 E�Go www.encolabs.itom ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C505861-01 Received: 11/19/15 12:45 Matrix: Surface Water Sampled: 11/19/15 08:00 Work Order. C505861 Project: Marsh Truck Parts Sampled By. -Client `Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary cedrfed analyte (NC 591J Results El4g Ymli l 2E MP.L PQL Batch Method Analyzed Py Notes Lead [7439-92-1]^ 0.00542 J mg/L 1 0.00310 0.0100 5K24026 EPA 6010C 11/25/15 10:08 JDH Classical Chemistry Parameters ^ - ENCO Cary cerbricd ana" [NC 5911 Analyte. fCAS Numberl Results flag Units RE MPA EU Batch Method Analyzed By Notes Total Suspended Solids^ 17 mg/L 1.33 3.3 3.3 51<23002 SM 2540D-1997 11/23/15 13:15 MMR Non -Halogenated Semivolatile Organics by GC Analyte _KASNumberl Results Flag Units pf MDL EQL Batch Method Analyzed Al Notes Ethylene Glycol[107-21-1] 4.0 U mg/L 1 4,0 10 5LO3021 EPA 8015C 12/03/15 13:27 JIB &LM!VtLS PE SQL v1 /o Rec ge i Banit MethodA By Clsi�i 1,3-8u"ne Glycol 210 1 200 103 % 50-150 5L03021 EPA 8015C 12,10311513:27 JIB Classical Chemistry Parameters Analyte KAS Number! Oil & Grease (HEM-SGT) Non -Polar Material Description: Truckyard A Matrix: Surface Water Project: Marsh Truck Parts Results flag Units PE MOL P_QL Batch Meth Anglyged By Note 2.70 U mg/L 1 2.70 5.00 5K23005 EPA 1664A 11/24/15 10:23 SMA Lab Sample ID:C505861-02 Sampled-11/19/15 07:00 Sampled By: Client ]Metals (total recoverable) by EPA 6000/7000 Series Methods Received: 11/19/15 12:45 Work Order: C505861 ^ - ENCO Cary cediried anatyte (NC 5911 An CAS Number Res fl[an maiu DF MDL PQL latch Method Analyzed By Notes Lead[7439-92.1]^ 0.00310 a mg/L 1 0.00310 0.0100 5K24026 EPA 6010C 11/25/15 10:27 JDH Classical Chemistry Parameters ^ - ENCO Cary ceivricd analyte JNC 591J Analyte [CA$ Numberl Results Flan Unit DF MDL PPOL, latch Method Analyzed §1 Notes Total Suspended Solids^ 42 mg/L 3.33 8.3 8.3 5K23001 5M 2540D-1997 11/23/15 10:40 MMR Non -Halogenated Semivolatile Organics by GC Analyte fCAS Numberl Results Flaq Units DF MDL Q Batch Method Analwedd —By Notes Ethylene Glycol[107-21-1) 4.0 U mg/L 1 4.0 10 5LO3021 EPA 8015C 12/03/15 14:05 JIB r tes Rrsju/ Df SpQk lv! 3/6 Rec °/a RetLim its Batch eM fhod Ana /v ed By Notes 1,3-Sufylene Glycol 220 1 200 10996 50-150 5LO3021 EPA 8015C 12/03/1514:05 JJB Classical Chemistry Parameters AnalyU fCASS Number] Oil & Grease (HEM-SGT) Non -Polar Material Results fin Units Pl MDL PQ.L Batch Method Analyz Ry Note 2.70 U mg/L 1 2.70 5.00 SK23005 EPA 1664A 11/24/15 10:23 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 10 Description: Truckyard B ANALYTICAL RESULTS Lab Sample ID:C505861-03 Matrix: Surface Water Sampled:11/19/15 07:15 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ��Go www.encolabs.com Received: 11/19/15 12:45 Work Order: C505861 ^ - ENCO Cary certified analyte (NC 5911 Anallae FCAS Numberl Results fin Units pp MDL pgL Batch Method Analyzed BY Notes Lead [7439-92-1]^ 0,00310 U mg/L 1 0.00310 0.0100 SK24026 EPA 6010C 11/25/15 10:36 ]DH Classical Chemistry Parameters ^ - ENCO Cary cerbNed analyft (NC 591] Resultj Has MrIm PE MDL PQL Batch Method Analyzed ll_1t Note Total Suspended Solids^ 36 mg/L 3.33 8.3 8.3 5K23001 SM 2544D-1997 11/23/15 10:40 MMR Non -Halogenated Semivolatile Organics by GC Results Ela9 Y12�1 PIE MDJ P9" Batch Method Analyz By Notes Ethylene Glycol1107-21-11 4.0 u mg/L 1 4.0 10 5LO3021 EPA 8015C 12/03/15 14:42 3113 &—am tes Results pF Spike 1 v! orb Rec % Rec Limits Batch Method Analvred fiy Notes 1,3-6utylene Glycol 230 1 200 116 % 50-150 5LO3071 EPA 8015C 12103/1514:42 JJ8 Classical Chemistry Parameters Analyte rCA5 Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results Elm Units P-E MU E" Batch Method Analyzed 01 Juntas 2.70 LI mg/L 1 2.70 5.00 5K23005 EPA 1664A 11/24/15 10:23 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 at 10 (� �Go www.encolabs.6rn QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch SK24026 - EPA .3005A Blank (SK24026-BLK1) Prepared: 11/24/2015 12:26 Analyzed: 11/25/2015 10:01 Spike Source %REC RPD Arlalyte RQSUIt Bag POL Units Level Result %REC Limits RPD kkok Notes Lead 0,00310 U 0.0100 mg/L LCS (SK24026-BSI) Prepared: 11/24/2015 12:26 Analyzed: 11/25/2015 10:05 Spike Source %REC RPD Anal vte Result Flag M units Level Result %REC Limits RPD Notes Lead 0.199 0.0100 mg/L 0.200 100 80-120 Matrix Spike (SK24026-MS1) Prepared: 11/24/2015 1 2: 26 Analyzed: 11/25/2015 10:11 Source: CSGSS61-01 Spike Source %REC RPD .Analyte Result Ma POL Units Level Resul %REC Limits RPD kmit Notes Lead 0.206 0.0100 mg/L 0.200 0.00542 100 75-125 Matrix Spike D u p (SK24026-MSD1) Prepared: 11/24/2015 12:26 Analyzed: 11/25/2015 10:14 Source: C505861-01 Spike Source %REC RPD Analyte Result IJa9 POL units Level Result p/oREC Limi RPD Limit Notes Lead 0.205 0.0100 mg/L 0.200 0.00542 100 75-125 0.2 20 Post Spike (5K24026-PS3) Prepared: 11/24/201S 12:26 Analyzed: 11/25/2015 10:16 Source: C505861-01 Spike Source %REC RPD Analvte Resy F1a9 P01 Units Level Result %REC Limits RPD Limit N!2tek Lead 0.192 0.0100 mg/L 0.200 0.00542 93 80-120 Classical Chemistry Parameters - Quality Control Batch 5K23001 - NO PREP Blank (5K23001-BLK3) Prepared & Analyzed: 11/23/2015 10:40 Spike Source %REC RPD _Analyte Result EM P-01 Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5K23001-BS1) Prepared & Analyzed: 11/23/2015 10:40 Spike Source %REC RPD Analvte Result Flag P_OL Units Level Resul %REC Limits RPD Limit Notes Total Suspended SoFds 100 2.5 mg/L 100 103 80.120 Duplicate (5K23001-DUPl) Prepared & Analyzed: 11/23/2015 10:40 Source: C513266-01 Spike Source %REC RPD .Analyte Result Oag F10L units Level Result %REC Limits RPD blpijt Notes Total Suspended Solids 180 50 mg/L 170 7 20 Duplicate (SK23001-DUP2) Prepared & Analyzed: 11/23/2015 10:40 11 Source: C513269-01 _Anal Total Suspended Solids Spike Source %REC Result a" Pool Units Level Result %REC Limits RPD 250 100 mg/L 250 2 RPD Unlit NQtes 20 Batch 5K23002 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SK23002 - NO PREP - Continued Blank (SK23002-BLKI) Prepared & Analyzed: 11/23/2015 13:15 Spike Source %REC RPD .Annalvtg Result Flag PQL Units Level ResuO %REC Limits RPD Limit des Total Suspended Solids 2.5 u 2.5 mg/L LCS (SK23002-BSI) Prepared & Analyzed: 11/23/2015 13:15 Spike Source %REC RPD .ABalAe Result Flag E" Units Level Result "/aREC Limits RPD Limit Notes Total Suspended Solids 91 2.5 mg/L 100 91 80-120 Duplicate (5K23002-DUPi) Prepared & Analyzed: 11/23/2015 13:15 Source: C506128-03 Spike Source %REC RPD .Analvte Result Flag P-QL Units Level Resu %REC Limits RPD iimft Notes Total Suspended Solids 500 120 mg/L 330 42 20 QM-12 Duplicate (5K23002-DUP2) Prepared & Analyzed: 11/23/2015 13:15 Source: C511942-01 Spike Source %REC RPD .Analvtg Result Flag P_L Units Level Result %REC LiMits RPD kjmit Notes Total Suspended Solids 37 17 mg/L 37 0 20 Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 5L03O21 - NA Blank (SL03021-BLK1) Prepared: 12/03/2015 10:45 Analyzed: 12/03/2015 11:35 Spike Source %REC RPD .Analvte Result Flag PQL Units Level Result %REC Limits RPD Limit Noteg Ethylene Glycol 4.0 U 10 mg/L 1,3-Bdtylene Glycol 320 mg/L 200 159 50-150 QS-03 LCS (SL03021-BSI) Prepared: 12/03/2015 10:45 Analyzed: 12/03/2015 11:54 Spike Source %REC RPD _Analvte ReSuft Flag P-QL Units Level Result 0/aREC Limits RPD Limit Notes Ethylene Glycol 150 10 mg/L 200 77 70-130 113-sutylene Glycol 210 m9/L 200 107 50-150 LCS Dup (51.03021-BSDI) Prepared: 12/03/2015 10:45 Analyzed: 12/03/2015 12:12 Spike Source %REC RPD -Annalvte Result Flag PQL Units Level Result a/aREC Limits RPD kiEd Notes Ethylene Glycol 150 10 mg/L 200 77 70-130 0.3 25 1,3-8ulylene Gtycol 210 m9/L 200 106 50-150 Classical Chemistry Parameters - Quality Control Batch SK23005 - EPA 16"A Blank (SK23005-BLK1) Prepared: 11/23/2015 11:38 Analyzed: 11/24/2015 10:23 Spike Source a/aREC RPD Analvte Result Flag P-QL Units Level Result a/aREC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 u 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may Drily be reproduced in full. Page 7 of 10 (��Cmo www.encolabs.4om QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5K23005 - EPA 1664A - Continued LCS (SK23005-BSI) Prepared: 11/23/2015 11:38 Analyzed: 11/24/201S 10:23 Spike Source %REC RPD -Ana]Ag R_esplt Flag P0L UnAiS Level Resuh %REC Limits RPD Limit Oil & Grease (HEM-SGT) Non -Polar Material 74.4 5.00 mg/L 80.0 93 64-132 LCS Dup (5K23005-BSD1) Prepared: 11/23/2015 11:38 Analyzed: 11/24/2015 10:23 Spike Source %REC RPD -Analyte Resu flag P4L Uni Level result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 72.1 5.00 mg/L 77.5 93 64-132 3 34 Matrix Spike (5K230o5-MS3) Prepared: 11/23/2015 11:38 Analyzed: 11/24/2015 10:23 Source: SS04855-01 Spike Source %REC RPD AAnalrte Result Flag P-OL Units Level Resuft %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 71.6 5.00 mg/L 86.2 2,70 U 83 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 10 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there Is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. QS-03 Surrogate recovery outside acceptance limits FINAL This report relates only W the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 10 "'Y_ '(f � a ' `ENVIRONMENTAL -CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs._com 10775 Contra] Pat Dr. 4010 F-$$Wove Perk Court. Stdte 11 i r M-A W000winds Industrial Ct. Orlando, FL =4 Jacksonville, FL 32216.8069 Cary, NC 27511 (407) 826-5314 Fax (407) e50-6945 (904) 2W& W Fax (904)2966210 ,-,.(919)467.9090 Fna (s19) 467-3515 Page of Qenl Name ... .. - - Project Numbei ..-. .. _ - .. .' .Requested Anatysea Requested Turnaround , Mar~;h T_r_klr-k Paft8. i Times Address W arnivDesk ) Note; Rush roquests subject to O. a 27 R.t Marsh luck Pas _ _ •, , ... aocep r" by the fadilty � . ChyiST2ip PO 4 I Bitting Into Siler city, NC 27344 ' - C7 - © .Q• - _ Standard Tot Fax HOPWWVContacl 919 663-1908 Steve Marsh o 7+ u CV - Expedited Due Swnpler(sj Name, Affiliation (Print) e" Contact Chuck Hoffman (!) — Sarr:ptor(s) Signature site Location IT4ne Zone. Lab Workorder °° ° C505861 Codas) noco=ry) . - - Preservatow (See (Cornbine as Collection matrix Total • of hem I Sample ID (Fleld IdenWication) Gogoctton Date -Tree Comp J Grab (sdo oodas) Contatners Sample Comments ►j-lq -�� �M _ r-�b arsl 1�' • y5 �i: SAM -`i R --TDta! # of Containers - Semple ril Prepared BY bat ne Lam/ Relinquished BY DatarFini ; } Received Data T CommermlSpedal Reporting Requirements Rormgsshod Datan, 0 Received &fJ Relinquished 9y' OateJTirno Received 8y — Datefiuna _ Gooier I's 6 Temps Rec�eippt Ganditinn Up�Receipt ,. . ,-�'/onas4ep. . 16 L Unacceptable J MaWx . GW-Ground%vator SO-SWI DW-Drinking Waler SE-Serfimard' SW-SUrface water WW-WastaNmtef A-Air-O-Other (detall in commenls] • . Preservation: ]-Ice, H-HCi N-HNO3 S442SO4 NO-NaOH 0.00mr (dnlall in commorus) Note: AO samples submitted to ENCO Labs are in aaomance with the temts and condiUats rstod on the revorae of this form, unless prior written agreerneM9 exist ' 5/�tojacfc; � STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Marsh Auto Parts, Inc. - Caryard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh _ PHONE NO. (919) 663-1908 CERTIFIED LABORATORY(S) ENCO Inc. Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results V2 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar 0&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 05/01/2015 1.752 6.7 20 <2.60 <8.7 0.00380 J NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Alan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print titl Sign Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 -22 -c5— Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee or Designee) j-�--z z - 70 (Date) Form SWU-251, lost revised October 25, 2012 Page 2 of 2 r Mid Atlantic Engineering & Environmental Solutions May 15, 2015 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. 211 EAST 'I 17H STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: MAY 2 6 Z015 CENTRAL FILES DWR SECTION 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on May 1, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918, Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, P.G. Project Geologist Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE F<CR/ E NCO Laborato p Accurate. Timely. Responsive, Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 14, 2015 Marsh Truck Parts (MA035) Attn: Steve Marsh P.Q. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C414992 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 1, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 ((J�Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE :1 Client ID: Caryard Lab ID: C414992-01 Sampled: 05/01/15 09:30 Received: 05/O1/15 11:05 Parameter Hold DatelTimefs) Prep Date/Time(s) Analysis DatelTmme(s) EPA 1664A 05/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28/15 05/08/15 12:08 05/11/15 14:29 EPA 8015C 05/15/15 05/12/15 11:10 OS/12115 18:11 SM 2540D-1997 05/08/15 05/05/15 09:09 05/05/1S 09:09 Client ID: Truckyard A Lab ID: C414992-02 Sampled: 05/01/15 09:40 Received: 05/01/15 11:05 Parameter Prep Date/Time(s) Analysis Gate/Time(s) EPA 1664A 05/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28/15 05/08/15 12:08 05/11/15 14:31 EPA 8015C 05/15/15 05/12/15 11:10 05/12/15 18:28 SM 25440-1997 05/08/15 05/05/15 09:09 05/05/15 09:09 Client ID: Truckyard B Lab ID: C414992-03 Sampled: 05/01/15 10.15 Received: 05/01/15 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664A O5/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28/15 05/08/15 12:08 05/11/15 14:34 EPA 8015C O5/15/15 05/12/15 11:10 05/12/15 18:45 SM 2540D-1997 05/08/15 05/05/15 09:09 05/05/15 09:09 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 (� �Go www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C414992-01 Anal vte Results Elag MDL POL Units Method Notes Lead - Total 0.00380 J 0,00310 0.0100 mg/L EPA 6010C Total Suspended Solids 20 3.3 3.3 SM 2540D-1997 Client ID: Truckyard A Lab ID: C414992-02 AnalResults ELA9 MDL PQ6 Units Method Notes Lead - Total 0.00365 7 0.00310 0.0100 mg/L EPA 6010C Total Suspended Solids 19 3.3 3.3 mg/L SM 2540D-1997 Client ID: Truckyard 8 Lab ID: C414992-03 Anal vte Results Elan MDL POL Units Method Notes Lead - Total 0.00483 J 0.00310 0.0100 mg/L EPA 6010C Total Suspended Solids 26 5.0 5.0 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 Description: Caryard Matrix: Surface Water Project: Marsh Truck Parts ANALYTICAL RESULTS Lab Sample ID:C414992-01 Sampled:05/01/15 09:30 Sampled By:Client (Metals (total recoverable) by EPA 6000/7000 Series Methods (� �Cmo www.enco(abs.com Received: 05/01/ 15 11:05 Work Order: C414992 ^ - ENCO Cary certifi9d analyte INC 591] Analdo FCA5 Numtyerl Results F1a9 Units Q MDL PSL6 gatSli Metb4s! Analyz Ry Notes Lead [7439-92-1]^ 0.00380 J mg/L 1 0.00310 0.0100 5EO8014 EPA 6010C 05/11/15 14:29 JDH Classical Chemistry Parameters LJ ^ - ENCO Cary certified analyze INC 591] AnalM [CAS Numberl Resul flag Units PE MDL pgb Batch Method Analyzed gy Notes Total Suspended Solids^ 20 mg/L 1 3.3 3.3 SE05004 SM 254OD-1997 05/05/15 09:09 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENCO JacksonWie certified analyze (NC 4411 Analyte fCAS Numbed Results Flag Units 2E MDL p_Qk Batch Method Analyzed !3y Notes Ethylene Glycol[107-21-1]^ 8.7 U mg/L 1 8.7 10 SE12008 EPA 801SC 05/12/15 18:11 LTS Surrogates Results pF Svike L vI % Rec % Rec Limits Batch Method Analyzed & Notes 1,3-Butylene Glycol 210 1 200 104 % 50-150 5E12008 EPA 8015C 0511211518:11 LTS Classical Chemistry ParametersL.J Analyla [CAS Numberl Results F[fg Units ICE MDL PD4 Batch Method Analyzed fly Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U mg/L 1 2.60 5.00 5E12005 EPA 1664A 05/13/15 14:22 SMA Description: Truckyard A Lab Sample ID:C414992-02 Received: 05/01/15 11:05 Matrix: Surface Water Sampled:05/01/15 09:40 Work Order: C414992 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary cLwfrW analyze (NC 5911 Analyte rCA5 Numberl Results F]Pq Uni DF MDL POLL Batch Method Anaed By Notes Lead [7439-92-1]A 0.00365 3 mg/L 1 0.00310 0.0100 5EO8014 EPA 6010C 05/11/15 14:3t JDH Classical Chemistry Parameters ^ - ENCO Cary certified a-filte (NC 591] Analyte fCAS Numberl Resul Flao Units DF MDL POLL Batch Method Analyzed By Notes Total Suspended Solids^ 19 mg/L 1 3.3 3.3 5EO5004 SM 25401)-1997 05/05/15 09:W MMR Non -Halogenated Semivolatile Organics by GC A - ENCOlack5onville cefVrk-d analyze (NC 4421 Analyze fCAS Numbed Results Flag units DF MDL POLL Batch Method Analyzed By Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/L 1 8.7 10 5E12008 EPA 8015C 05/12/15 1E:28 LTS Surrogates Results DF 5,olke Lvl %ReC 0/0RecIif" Batch Method Analyzed By Notes 1,3-8utylene Glycol 210 1 200 10596 50-150 5E12008 EPA 8015C 05/12/1518:28 LTS Classical Chemistry Parameters Analvte rCAS Numberl Oil & Grease (HEM-SGT} Non -Polar Material Results flag Units PFF MDL POL Batch JJetbQd AUplyied @Y Notes 2.60 U mg/L 1 2.60 5.00 5Ei2005 EPA 1664A 05/13/15 14:22 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C414992-03 Matrix: Surface Water Project: Marsh Truck Parts Sampled:05/01/15 10:15 Sampled By:Client (� �09 www.encolabs.com Received: 05/01/ 15 11:05 Work Order: C414992 IMetals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO Cary certified analyte [NC 5911 Analyte fCASNumberl Results Flag Units )E MPI PSI: Batch Mettiodl Analyzed Notes Lead (7439-92-1]^ 0.00483 3 mg/L 1 0,00310 0.0100 5E08014 EPA 6010C 05/11/15 14:34 ]DH Classical Chemistry Parameters ^ - ENCO Cary ma7fied analyte [NC 5911 AnalAe FCAS Numberl Results EW Units RE bpi pQL Batch Method Analyzed By Notes Total Suspended Solids^ 26 mg/L 1 5.0 5.0 5E05004 SM 2540D-1997 05/05/15 09:09 MMR INon-Halogenated Semivolatile Organics by GC ^ - INCO Jacksom7he certAw ana" [NC 442] Analyte fCAS Numberl Results Flag Units P_F MDL P t &-t[1 Method Analyzed Jay Notes Ethylene Glycol[107-21-1]^ 8.7 U mg/L 1 8.7 10 5E12008 EPA B015C 05/12/15 18:45 LTS SUrM9fffCs Results PF Snike L v1 X Wo Rec limits Method Analyzed §y Notes 1,3-8utylene Glycol 210 1 200 10S % 50-150 5E12008 EPA 8015C 0511211516:45 LTS Classical Chemistry Parameters Analyte rCAS Numberl Oil & Grease (HEM-SGf) Non -Polar Material Results flag Units PE MDL f" Batch Meths Analyzed ft Notes 3.04 U mg/L 1 3.04 5.85 5E12005 EPA 1664A 05/13/15 14:22 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 or 9 (��Cmo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch SE08014 - EPA 3005A Blank (5E08014-BLK1) Prepared: 05/08/2015 12T8 Analyzed: 05/11/2015 13:43 Spike Source %REC RPD _Analyte Result Flag ROL Units Level Result %REC Limits RPD linift Notes Lead 0.00310 U 0.0100 mg/L LCS (SE08014-BSI) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:46 Spike Source %REC RPD AMvte Result flau P0L mts Level Result %REC Limits RPD Limit Notes Lead 0.210 0.0100 mg/L 0.200 105 80-120 Matrix Spike (SE08014-MS1) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:52 Source: C504820-01 Spike Source %REC RPD _Analvte Result Fbq POL Units Level Result %REC Limits RPD iLMA Notes Lead 0.210 0.0100 mg/L 0.200 0.00310 U 105 75-125 Matrix Spike Dup (SE08014-MSD1) Prepared: 05/08/2015 12:06 Analyzed: 05/11/2015 13:55 Source: C504820-01 Spike Source %REC RPD Anaivte Reslalt FLaq PPOL Units Level gar t %REC Limits RPD Limit Notes Lead 0.214 0.0100 mg/L 0.200 0,00310 U 107 75-125 2 20 Post Spike (5E08014-PS1) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:57 Source: C504820-01 Spike Source %REC RPD Analyt Result Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0.197 0.0100 mg/L 0.200-0.003,15 98 80-120 Classical Chemistry Parameters - Quality Control Batch 5E05004 - NO PREP Blank (5E05004-BLKI) Prepared & Analyzed: 05/05/2015 09:09 Spike Source %REC RPD AOalvte Result Flu P-01 Units Level Result %REC limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SE05004-BSI) Prepared & Analyzed: 05/05/2015 09:09 Spike Source %REC RPD _Anande Result Flag P-01 Units Level Result %REC Limits RPD kimft Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (SE05004-1)UP1) Prepared & Analyzed: 05/05/2015 09:09 Source: C504669-02 Spike Source %REC RPD AnalAe Result Flan POL Units Level Result %REC LimiU RPD Limit Notes Total Suspended Solids 390 62 mg/L 380 3 20 Duplicate (SE05004-DUP2) Prepared & Analyzed: 05/05/2015 09:09 Source: C505434-02 Spike Source %REC RPD AnalYte Result Flag M units Level Result %REC Limits RPD Linift Notes Total Suspended Solids 5100 500 mg/L 4500 13 20 Nan -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 (� �Cmo www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 6E12008 - NO PREP Blank (5E12008-BLK3) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 17:54 Spike Source %REC RPD .Analvte Result Flag ROL Units Level Resuk %REC LimlU RPD Limit Notes Ethylene Glycol 8.7 U 10 mg/L 1,3-8ulylene Glycol 220 -91L 200 112 50-150 LCS (SE12008-BSI) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 t4:26 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 95 70-130 1,3-Bulylene Glycol 220 my/L 200 108 50-150 Matrix Spike (SE12008-MSI) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 19:02 Source: C414992-01 Spike Source %REC RPD Aual1ta Result Flag R" Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 8.7 U 94 70-130 1,3-Butylene Glycol 210 mg/L 200 104 50-150 Matrix Spike Dup (5E12008-MSDI) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 19:18 Source: C414992-01 Spike Source %REC RPD Anal mutt Elag PO-L Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 8.7 U 95 70-130 t 25 1,3-8utylene Glycol 210 M91L 200 107 50-150 Classical Chemistry Parameters - Quality Control Batch 5E12005 - Same Blank (SE12005-BLK1) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Spike Source %REC RPD Anialvte Result Fla-g POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-5Gr) Non -Polar Material 2.60 U 5.00 mg/L LCS (SE12005-BS1) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.2 5.00 mg/L 21.7 84 64-132 LCS Dup (SE12005-BSD1) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Spike Source %REC RPD Analrte Result Flag POL Units Level Resu %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 15.9 5.00 mg/L 21.1 75 64-132 13 34 Matrix Spike (SE12005-MSi) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Source: B404894-01 Spike Source 0/aREC RPD Analvte Result Flag PQL Units Level Result "/oREC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 11.0 5.56 mg/L 23.2 2.89 U 47 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (��Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture contentr where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 10775 Contat Port Dr. 4810 Executive Park Court. Suite i 11 102•A Woodwinds Industrial Ct. �Z:3Qrtando, FL 32824 ,IackSon-Ale, FL 32216.6069 Cary, NC 27511 � (407j 826-5314 Fax (407) 850.6945 (904) 296-3007 Far (9p4) 296.8210 (919) 467-3090 Fax (919) 467-3515 Page of Client Name Marsh Truck Parts MA035 Project Number one Requested Anafyses Requested Turnaround Times Note : Hush requests subject to acceptance by the facility _ Standard _ Expedited Due _ chi-6 7'' V11 co 0 < co � ° ° A c_ C � (1) ~ Address P.O. Sox 427 Project NamofDosc Marsh Truck Parts QtyrSTl'Zap Si3er City, NC 27 344 Po 0 / Bining Info lei (G 19) 663-1908 Fax Reporting Contact Sieve Marsh Samptaf(s) Name, ANilialion (Prinl) Ming Contact Chuck Hoi�rrtarr, Sampler(s) Signature Sita Location / Time Zone Lab Workorder C414992 Preservation (See Codes) (Combine as necessary) here N Sample ID {Fuld Identilmation) DAlorg!ion Dole Collection Tim f4 Cramp! Grab Matrix (see ca�ri�e/s) Total P 4A Containers ' -Sample Comments 7 T t-ICk a d\ rJ -1 — 1S S1N 7 X X X X TruCF, and B 5 to"t6p"c4t,_6 SIN 7 X X X X Apq NfLd_7 r ( <-- Total tt of Containers 3mp Q Prepared By to +m �� Z Relfnqulshed By Dalorrione Racetwd 8 �4!! - . DaleMm- �/l/' /G Commentsl5 I Reporting Requirements Relinquished By Date/rune Rec ' By DateMme{ k n RO+n uishOdBy DaiaMme R celvad Y Daloi-rime C tar It's 8 Te/n Receipt rn} ICori:1604 pon ROCeipt y 'r � c�• 1. [, _ Acceptable Unacceptable Matrix: GW.Groundwater SO -Sail DW-Drinking Water SE-Sodimom SW-Surfacd ,haler MI-Waslowater A -Air O-Other (detail in comments) Preservation: I -Ice H-HCI WHNO3 S-H2SO4 NO.NaOH 0-0tner (detail in comments) Note : Al samples submitted to ENCO Labs are in accordance with the terms and conditions fisted on the reverse of this form, unless prior written agreements oxist W NOW Atlantic Engineering & Environmental Solutions December 9, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.99t8 facsimile 919.250.9950 MAAONLINE.COM RECEIVED DEC 18 2014 CENTRAL FILES DVAIR SECTION Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on November 17, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, P.G. Project Geologist Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 FACILITY NAME Marsh Auto Parts. Inc. - Caryard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/Year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), m /L g Non -polar O&G/TPH [Method 1664 SGT-HEM], mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 11/17/14 1.50 7.1 41 <2.60 <8.7 0.0200 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 15ee If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122, Form SWU-251, last revised October 25, 2012 Page 1 of 2 Ik STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. l further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." m Name (Print name) Title (Print title) ] Signature ' Date L Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ignature bt Permittee or �1-1SA4 (Date] Form SWU-251, last revised October25, 2012 Page 2 of 2 ENCO Laboratories Accurate. - Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, December 4, 2014 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C409618 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 18, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 f www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C409618-01 Sampled: 11/17/14 10:45 Received: 11/18/14 11:45 Parameter Hold DatelTime(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664A 12/15/14 11/25/14 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:09 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:12 SM 254OD-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 Client ID: Truckyard A Lab ID: C409618-02 Sampled: 11/17/14 11:15 Received: 11/18/14 11:4S Parameter Hold Date/iime(sl Prep Date/Time(s) Analysis Date/Timefs) EPA 1664A 12/15/14 11/25/14 10:07 11/26/14 16:13 EPA 6OtOC 05/16/15 11/20/14 09:36 11/24/14 11:12 EPA 8015C 12/01/14 11/21/14 1S:41 11/21/14 21:29 SM 2540D-1997 11/24/14 1.1/19/14 14:20 11/19/14 14:20 Client ID: Truckyard B Lab ID: C409618-03 Sampled: 11/17/14 11:20 Received: 11/18/14 11:45 Parameter EPA 1664A Hold Date/Timefs) 12/15/14 PlCo Die/Time(s) 11/25/14 Aiiiilysis Date/Time(s) 10:07 11/26/14 16c13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:22 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:47 SM 254OD-1997 11/24/14 11/19/14 1410 11/19/14 M20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 I��Ildl www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C409618-01 Analvte Lead - Total Total Suspended Solids Results 0.0200 41 Elm M-L 0.00210 1.0 FQL 0.0100 1.0 Units mg/L mg/L Method Notes EPA 6010C SM 25400-1997 Client TO: Truckyard A Lab ID: C409618-02 ADS Lead - Total Total Suspended Solids Besults 0,0102 47 fbs MPL 0.00210 1.0 R2L 0.0100 1.0 Units mg/L mg/L Method Notes EPA 6010C SM 254OD-1997 Client ID: Truckyard B Lab ID: C409618-03 Anal= Lead - Total Total Suspended Solids Results 0.00617 51 EIP9 3 MDL 0.00210 1.0 FQL 0.0100 1.0 Units mg/L mg/L Method Notes EPA 6010C SM 254OD-1997 FINAL This report relates only to the sample as received by the LBW8tDfY, and may only be reproduced In full. Page 3 of 9 Description: Caryard Matrix: Surface Water ANALYTICAL RESULTS Lab Sample ID:C409618-01 Sampled:ll/ 17/14 10:45 Project: Marsh Truck Parts Sampled By: Client Metals (total recoverable) by EPA 6000/7000 Series Methods www.encolabs.com Received: 11/ 18/ 14 11:45 Work Order: C409618 ^ - ENCO Cary certified analyze JAC 5911 ' Analyte ICAS_Numberl Results flag Units PIE Mpb EU Batch Method Analyzed BY Notes Lead [7439-92-1]A 0.0200 mg/L 1 0.00210 0.0100 41<20013 EPA 6010C 11/24/14 11:09 JDH Classical Chemistry Parameters ^ - E%C0 Cary certified analyze JNC 5911 Analyte fCAS Numberl Results Elm U&M PE MDL EQL Batch MethQd Analyzed Ay Notes Total Suspended SolidsA 41 mg/L 1 1.0 1.0 4K19019 SM 254OD-1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile organics by GC ^ - E%C0Jadkamvflle Cetfied analyze (AC 4421 Analyte ICAS Numberl Results Elan llnits RE MDL Egg Batch Meth AnalyZed jay Notes Ethylene Glycol [107-21-1]A 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:12 ]W] Surrogates_ lTesuJts pf it ke 1 v! % % Rec Llm/ts 9atch Method Analyzed & Note1 1,3-Bu44ene GJyrd 220 1 200 110 % 50-150 4K21008 EPA 8015C 1112111421,12 JWJ Classical Chemistry Parameters Analyte FCAS Numberl Results an Units RE MDL EQL Batch Method Analyzed @y N= Oil & Grease (HEM-SGT) Nan -Polar Material 2.60 U mg/L 1 2.60 5.00 4K25008 EPA 1664A 11/26/14 16:13 M]F Description: Trudryard A Lab Sample ID:C409618-02 Received: 11/18/14 11:45 Matrix: Surface Water Sampled.11/17/14 11:15 Work Order: C409618 Project: Marsh Truck Parts Sampled By:Client MMetals (total recoverable) by EPA 6000/7000 Series Methods ^ - EACO CaryCm6'fred analyze (AC 5911 Analvte FCAS Numberl Results Etas Units gE HDL EQ4 Batch Met wdl Anatvred @y Nis Lead [7439-92-1]1 0.0102 mg/L 1 0.00210 0.0100 4K20013 EPA 6010C 11/24/14 11:12 JDH Classical Chemistry Parameters i ^ - ENCO Cary certified analyre [AC 5911 Analyte rCAS Numberl Besults f m units pE MkL EQL Batch Method Analyzed py NQkE Total Suspended Solids- 47 mg/L 1 1.0 1.0 4K19019 SM 25401)1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile organics by GC ^ - EACO JaCksnrtvzlle certrfred an,?Wff C 4421 Analyte fCAS Numberl Results Elm ViA11 DEE MDL E" Batch Method Analyzed U Notes Ethylene Glycol [107.21-1]^ 8.7 U mg/L 1 8.7 10 41<21008 EPA 8015C 11/21/14 21:29 JWJ Sumvgates Results p_F Spikevl °% %RecIJmltS Batch me Analrzed By f(Qtes 1,3-Butylerre G#wl 220 1 200 108 % 50-150 4K21006 EPA 8015C 11121114 21:29 JWJ Classical Chemistry Parameters Oil & Grease (HEM -SG r) Non -Polar Material Results Elm units PE HU l_'QL Batch Method Analyzed Alit Notes 2.60 U mg/L 1 2.60 5.00 4K25008 EPA 1664A 11/26/14 16:13 MJF FINAL Phis report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 www.encDlabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C409618-03 Received: 11/18/14 11:45 Matrix: Surface Water Sampled:11/17/14 11:20 Work order: C409618 Project: Marsh Truck Parts Sampled By: Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary cetbr7ed analyze CAC 5911 Analyte fCAS Number] gills B29 Units pF MDL pQ Batch Method Analyzed lijl Notes Lead [7439-92-111 0.00617 1 mg/L 1 0.00210 0.0100 4K20013 EPA 6010C 11/24/14 11:22 3DH Classical Chemistry Parameters ^ . EACO Cary c&vfled anatyte [AC 591] Analvte NAS Numberl kp „Irc f&9 Units 2E MQL EQL Batch Met AnalyM ft Notes Total Suspended Solids^ 51 mg/L 1 1.0 LO 4K19019 SM 254OD-1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile Organics by GC ^ - EAC'O J� I/e caiFrAed anjlyte [AC 442] Analvte KAS Numberl Results Sps Units pf MQL POL Batch Method Ay Notes Ethylene Glycol [107-21-11^ 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:47 ]W3 Sumvaahes Resu�ts RE SylkeLY1 % Rec Oh Rec Llm3ts Ball± Analyzed PX ti414� 1,3-Butylene Glycol 210 1 200 107 % 50-150 4K21006 EPA 6015C 1112411421:47 JwJ Classical Chemistry Parameters Analog ICAS Numberl Oil & Grease (HEM-SGl) Non -Polar Material Results flan Units R MIX lQ1 hatch Method AOall%sd f[ Notes 2.60 U mg/L 1 2.60 5.aa 4K25008 EPA 1664A 11/26/14 16:13 M]F FINAL This report relates only to the sample as retched by the laboratory, and may only be reprnduced In full. Page 5 or 9 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 4K20013 - EPA 3005A Blank (4K20013-BLKI) Prepared: 11/20/2D14 09:36 Analyzed: 11/24/2014 10:47 Spike Source %REC RPD Analyt Result Elag eQL Units 'Level Result %REC Limits RPD Li-ft Notes Lead 0.00210 U 0.0100 mg/L LCS (4K20013-BSI) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:51 Spike Source %REC RPD Anal lde KC51111; Elm PGL Units Level Result %REC Limits RPD Limit Notes Lead 0.208 0.0100 mg/L 01200 104 80-120 Matrix Spike (4K20013-MS1) Prepared: 11/20/2014 0936 Analyzed: 11/24/2014 10:57 Source.,C414111-01 Spike Source %REC RPD Analvte Resin Elan P.91. Unite Level Result %REC Limits RPD LIMB Notes Lead 0.221 0.0100 mg/L 0.200 0.00210 U 111 75-125 Matrix Spike Dup (4K20013-MSD1) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:59 Source: C414111-01 Spike Source %REC RPD .An&Ae Result Sao P9i Units Level Result %REC Limits RPD L11Dlt Notes Lead 0.212 0,0100 mg/L 0.200 0.00210 U 106 75-125 4 20 Post Spike (4K20013-PSI) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 11:02 Source: C414111-01 Spike Source %REC RPD Anal]VIC Result Elan PAL Units Level Result D&REC Limits RPD Limit Notes Lead 0.193 0.0100 mg/L 0.200 0.00104 96 80-120 Classical Chemistry Parameters - Quality Control Batch 4K19019 - NO PREP Blank (41K19019-BLKI) Prepared & Analyzed: 11/19/2014 14:20 Spike Source %REC RPD Anal lr3C Result flag P_QL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (41(19019-BS1) Prepared & Anayzed: 11/19/2014 14:20 Spike Source %REC RPD Anande Result Esau P9L Units Level Rgs, t %REC Limits RPD LIMA UQW5 Total Suspended Solids 1DD 1.0 mg/L 100 101 80-120 Duplicate (4K19019-DUPi) Prepared & Analyzed: ll/19/2014 14:20 Source:C409618-01 Spike Source %REC RPD Anal 1te Result EIN POL Units Level Resul %REC Limits RPD Limit Notes_ Total Suspended Solids 39 1.0 mg/L 41 5 10 Duplicate (4K19019-DUP2) Prepared & Analyzed: 11/19/2014 14:20 Source: C409618-02 Spike Source %REC RPD Ana hde Result El," PDX unit4 Level Result %REC Limits RPD Limit Notes Total Suspended Solids 50 1.0 mg/L 47 7 10 Hon-Hatogenated Semivolatile Organics by GC - Quality Control FINAL This report relates ordy to the sample as received by the laboratory, and may only be reproduced In full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Hon -Halogenated Semivolatile Organics by GC - Quality Control Batch 4K21008 - NO PREP Blank (4K21008-eLK1) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 17:47 Spike Source %REC RPD Analytic Result Flag PDL units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 8.7 U 10 mg/L 1,3-But kM Glyro! 190 mq/L 200 95 50-150 LCS (4K21008-B51) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:07 Spike Source %REC RPD Anal Resin Rag PQL Units Level Res %REC Limits RPD Unlit Notes Ethylene Glycol 190 10 mg/L 200 95 70-130 1,3-Ba4*-- Glycol 210 mg/L 200 107 50-150 ' Matrix Spike (4K21008-MS1) Prepared: 11/21/2014 10:41 Analyzed: 1 V21/2014 14:19 Source: B405123-01 Spike Source %REC RPD Analvte Result flag EM UnfL4 Level Result %REC Limits RPD Limit Notes Ethylene Glycol 210 10 mg/L 200 8.7 U 107 70-130 113-Bulyle- Glycol 220 m¢L 200 111 50.150 Matrix Spike Dup (4K21008-MSD1) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:36 Source: B405123-01 Spike Source %REC RPD Anal YiC Result Fla4 POL Units Level Result %REC timlts RPD Limit Notes Ethylene Glycol 220 10 mg/L 200 8.7 U 10B 70-130 2 25 1,3-&Okrte GlytnJ 220 M91L 200 110 50-150 Classical Chemistry Parameters - Quality Control Batch 4K25008 - EPA 1664A Blank (4K25008-BLKI) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD AnalResult flan PAL units Level Result %REC Limits RPD hilnt Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U 5.00 mg/L LCS (4K25008-BSI) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD ADa11de Resul Elau P01 Units Level Result %REC Limits RPD t+rmjt Notes_ Oil & Grease (HEM-SGT) Non -Polar Material 21.2 5.00 mg/L 20.8 102 64-132 LCS Dup (4K25008-65DI) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Ana tvte Result Ela9 E" Units Level Res %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 20.9 5.00 mg/L 20.6 101 64-132 1 34 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 7 of 9 L C7 O www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (650/6 or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fug. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs,c'om 1.;1 lh E , ".4"t Poll Dr. .19 10 Exu- ulivv Park CLuti, Such 11 W h W01.17AM-5 lxlu,;ULr - "I Gr I:r:i , . rwil. _ Jadti .scmr!hf FL T^21 ,­M Gd;y. W. 1-5- (.10il 5:6 53 14 =,-,x (1071 °H-t9j!, '96-3()07 F�x (PW1 2911,4210 0,9)4�7.2(m re'xt9,9)-;F7--5lS Piiyu of CAInl Na!n, P.-J,vul 4msd.-! R6c jebled An. �ys" Reques'ec Tina-cund h. T 14f"TA r—sh sib :il 11w 1, CBy:SBc- T'Z c a C' 1 :N4 S;andard T., I Expedited mitm., i[Flulicii ;F fr)l i Ll, I.,(. SIR' LCMt Uil-1. Lab Wcrkoruc�r GO b,)ci rn nt 1_7 sa.nple Cot-, -11clit's _X. 1'.." �iompw� iD �n_kl Dot- V_ _— _...__._i�_.. �__,_---..L.-_— ----.. Ir • jrel 4'.i X x I x oml C.' Coflti�inw!; -t!lhnqo,-rWl 1;y 3 omi 7.1 a,:,. Xb K T",os an Rece I ..... W, v hintrix " GAr-ClowirlwaL_i I.Vater J-ncc'X;tici WW 'Nzgc,,,,mw A -Air O-C-lipw (,J,4.i .,,ccm vtsj PrP-qrrvAtsDA: Hr.; H.HCl lq HNDa 5 H2501 PA0-11-a0-i `JnW 19 wroWs n layv-7,cd to EN_-o Labs ase v, With U.. 4-1 f—Mullt hVeri — 7.V, -0(m. U-�TCt;C pjiorwrr,� LF'j, "_ i- r,x sI STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGIO0015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the'date the facility receives the sampling results from the laboratory.) FACILITY NAME Marsh Auto Parts, Inc. - Caryard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE -) For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 5GT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 - 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 11/17/14 1.50 7.1 41 <2.60 <8.7 0.0200 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT 40 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." 1Y; 4-VI M'L-( mIm-,k Name (Print name) Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pef4jnittee or 2- k ---1 Lt (Date) Form SW U-251, lost revised October 25, 2012 Page 2 of 2 I 1"�ccq ;,4-" ivh' "PAtLabo- rato Accurate. Timely. Responsive. Innovative, 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX; 919.467.3515 Thursday, December 4, 2014 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C409618 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 18, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OLdc-'s-A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In fuN. Page 1 of 9 I SAMPLE SUMMARY/LABORATORY CHRONICLE www.encolabs.com Client ID: Caryard Lab ID: C409618-01 Sampled: 11/17/14 10:45 Received: 11/19/14 11:45 P Cilmot0.[ EPA 1664A Hold Date/Time(s) 12/15/14 prep patefflmg(s) 11/25/14 Analysis Date/Tlme(s) 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:09 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:12 SM 254OD-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 Client ID: Truckyard A Lab ID: C409618-02 Sampled: 11/17/14 11:15 Received: 11/18/14 11:45 Parameter Hold, pate/Timefs) Prep Date/Time(s) Analysis Date/Tlme(s) EPA 1664A 12/15/14 11/25/14 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:12 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:29 SM 2540D-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 Client ID: Truckyard 0 Lab ID: C409618-03 Sampled: 11/17/14 11:20 Received: 11/18/14 11:4571 Parameter EPA 1664A Hold Date/Timefs} 12/15/14 Prep Date/Time(s) 11/25/14 Analysis Date/Time(s) 10:07 11/26/14 16:13 EPA 6010C O5/16/15 11/20/14 09:36 11/24/14 11:22 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:47 SM 2540D-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 of 9 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C409618-01 Ana Results Flan i' DL PQ6 UTW1 Method NotgA Lead - Total 0,0200 0.00210 0.0100 mg/L EPA 601DC Total Suspended Solids 41 1.0 1.0 mg/L SM 2540D-1997 Client ID: Truckyard A Lab ID: C409618-02 Anjl Results Flag MDL POL Units Method Notes Lead -Total 0.0102 0.00210 0.0100 mg/L EPA 6010C Total Suspended Solids 47 1.0 1.0 mg/L SM 2540D-1997 Client ID: Truckyard B Lab ID: C409618-03 Analvte Results flan HA PQ ll0lti Method Notes Lead - Total 0.00617 1 0.00210 0.0100 mg/L EPA 6010C Total Suspended Solids 51 1.0 1.0 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 3 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C409618-01 Received: 11/18/14 11:45 Matrix: Surface Water Sampled:11/17/14 10:45 Work Order: C409618 Project: Marsh Truck Parts Sampled By: Client [Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - EACO Cary —Red analyze (AC 5911 Analyze fCAS Numberl Results ELM Vili11 AE MDL PQL Datcf Method Analyzed Ay Notes Lead [7439-92-1]A 0.0200 mg/L 1 0.00210 0.0100 4K20013 EPA 6010C 11/24/14 11:09 11)H ssical Chemistry Parameters ^ - EACO Cary cerzzlfed analyte [NC 5911 Analyze fCAS Numberl Results fin Units pf MU PQL Batch Method Analyzed ft Notes Total Suspended Sollds^ 41 rng/L 1 1.0 1.0 41<19019 SM 254OD-1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile Organics by GC ^ - EACOJacksmvflle cetified analyze (AC 442] Analyte FCAS Numberl Results f'1g VDAS PIE MDL PQL Batch Method Aullybed ft Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/L 1 8.7 to 4K21008 EPA 8015C 11/21/14 21:12 JWJ .%LamResults p_F iSn ke 1r! % Rec % Rec Llmlts &atch Method Analyzed By Notes I,J-Butyk— Glycol 220 1 200 110 % 50-150 4K21008 EPA 8015C 11121114 21:12 JwJ Classical Chemistry Parameters Analyze fCAS Numberl Results flag Units pf MRL EQL Batch Method Analyzed lilt Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U mg/L 1 2.60 5,00 41<25008 EPA 1664A 11/26/14 16:13 MJF Description: Trudcyard A Lab Sample ID: C409618-02 Received: 11/18/14 11:45 Matrix: Surface Water Sampled:11/17/14 11:15 Work Order: C409618 Project: Marsh Truck Parts Sampled By: Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - EACO Cary [trbTred a-lyte (AC 5911 Analyze [CAS Numberl Results flag Units DE Ku PQL Batch Method AnalvzLl All HQJ:sv4 Lead [7439-92-1]^ 0.0102 mg/L 1 0.00210 0.0100 4K20013 EPA 601DC 11/24/14 11:12 JDH (Classical Chemistry Parameters ' ^ - EACO mryC&DFied analyze (AC 5911 - Analyte rCAS Number] Resylls Elag Units PIE M PQL Batch Method od Analyzed ILY 112to Total Suspended SolidsA 47 mg/L 1 1.0 1.0 41(19019 SM 254OD-1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile Organics by GC ^ - EACO Jacicsb VfJ1e re-afied analyze [AC 442] Analyze fCAS Numberl Results Eln Sj.nM PE ma PQL Batch Meth QQ AnalyXW AY Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:29 ]W] Surnwates Results -Of Svrkelvl aleRec %RecIrmrCs PACI;& iffam A BY Notes 113-8uty10ne Glycol 220 1 100 108 % 50-150 4K21008 EPA 8015C 11121/14 21:19 JWJ Classical Chemistry Parameters Analyze rCAS Numberl Oil & Grease (HEM-SG-0 Non -Polar Material Results f&9 1lnim PF Ma PQL 1321ch Method Analyzed Ay 2.60 U mg/L 1 2.60 5.00 4K25008 EPA 1664A 11/26/14 16:13 MJF FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C409618-03 Received: 11/18/14 11:45 Matrix: Surface Water Sampled:11/17/14 11:20 Work Order: C409618 Project: Marsh Truck Parts Sampled By: Client LMetals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - EACO ary —1W analyze [AC 591) Analyse [CAS Numbed Results EW9 Un;ts P-E HU pQL Batch Method Analyzed @y Notes Lead [7439-92-11^ 0.00617 1 mg/L I 0.00210 0.0100 4K20013 EPA 6010C 11/24/14 11:22 IDH Classical Chemistry Parameters ^ - EAM Cary c'erafied analyze W 591J Analyte rCAS Numberl Besults Elea !!1?m PIE HU pgL Batch Method Analyze( gy Notes Total Suspended Solids^ 51 mglL 1 1.0 1.0 4K19019 SM 2540D-1997 11/19/14 14:20 MMR [Non -Halogenated Semivolatile Organics by GC ^ - ENCOJacksmvrlle C&Vfied analyze CNC 4421 Analyte rCAS Numberl Results Elm V11M PE MDL P4.6 Aatch Method Analyzed @y H= Ethylene Glycol(107-21-11^ 8.7 U mg[L 1 8.7 10 4K21008 EPA 6015C 11/21/14 21:47 1W] wmwaftf Results p� Solke Lv1 % Rec '/e Rec LTmlts 8atcfi Afelrh BY Notes 113-Butyk— 64itd 210 1 200 107 % 50-150 4K21008 EPA 8015C 11121114 21;47 JwJ Classical Chemistry Parameters Analyse rCAS Numberl Results 8329 units PIE 11U R" Patch Method Analyzed Ay Note Oil & Grease (HEM-SG-0 Non -Polar Material 2.60 U mglL 1 2.60 5.00 4K2500B EPA 1664A 11/26/14 16:13 M1F FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 of 9 www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 4K20013 - EPA 3005A Blank (4K20013-BLKI) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:47 Spike Source %REC RPD -ADalvte Result Flag Pal units Level Result MoREC Limits RPD UnI t Notes Lead 0.00210 U 0,0100 mg/L LCS (4K20013-BSI) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:51 Spike Source %REC RPD Anal Ylg Result Flag POL Units Level Result %REC Limits RPD Uimjt Noteji Lead 0.208 0.0100 mg/L 0.200 104 80-120 Matrix Spike (4K20013-MS1) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:57 Source:C414111-01 Spike Source %REC RPD .Anallfle Result Flag POL Units Level Result %REC Limits RPD Uraft Notes Lead 0.221 0.0100 mg/L 0.200 0,00210 U ill 75-125 Matrix Spike Dup (4K20013-MSD1) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:59 Source: C414111-01 Spike Source 0/aREC RPD Anallrte Result Flag P-oL Units Level Result %REC Limits RPD Limit Notes Lead 0,212 0.0100 mg/L 0.200 0.D0210 U 106 75-125 4 20 Post Spike (4K20013-PS1) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 11:02 Source: C414111-01 Spike Source %REC RPD Anal vts Result Flag e41 Units Level Result °/aREC Limits RPD Limit Notes Lead 0.193 0.0100 mg/L 0.200 0.00104 96 8D-120 Classical Chemistry Parameters - Quality Control Batch 4K19019 - NO PREP Blank (4K19019-BLKI) Prepared & Analyzed: 11/19/2014 14:20 Spike Source %REC RPD Anahrte Result Flag eO1 units Level Result %REC Limits RPD uInk Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (41(19019-BSI) Prepared & Analyzed: 11/19/2014 14:20 Spike Source %REC RPD Analite Result flag PD1 units Level Result a/aREC Limits RPD Iftwit Notes Total Suspended Solids 100 1.0 mg/l 100 101 80-120 Duplicate (4K19019-DUPI) Prepared & Analyzed: 11/19/2014 14:20 Source:C409618-01 Spike Source %REC RPD Anal ytA Result Flag e46 Unitf Level Result °/aREC Limits RPD uinift Notes Total Suspended Solids 39 1.0 mg/L 41 5 10 Duplicate (4K19019-DUP2) Prepared & Anayzed: 11/19/2014 14:20 Source:C409618-02 Spike Source %REC RPD Anal Result flag PQL Units Level Result a/aREC Limits RPD Limit Notes Total Suspended Solids 50 1.0 mg/L 47 7 10 Nan -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in M. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 4K21008 - NO PREP Blank (4K21008-BLK1) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 17:47 Spike Source %REC RPD -Anabd9 Result 8413 M Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 8.7 U 10 mg/L 1,3-Bu44ene G1yml 190 m9/L 207 95 50-150 LCS (4K21008-BS1) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:02 Spike Source %REC RPD An;j1Y.iC Result Elay PQ unim Level Result %REC LiMits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 95 70.130 1,3-8ut *l - Glyeal 210 mg/L 200 107 50-150 Matrix Spike (4K21008-MSI) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:19 Source: B405123-01 Spike Source %REC RPD Anal Result Bag Pl2L Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 210 10 mg/L 200 8.7 U 107 70-130 1,3-8u44_, a G" 220 myL 200 111 50-150 Matrix Spike Dup (4K210DB-MSD1) Prepared: I1/21/2014 10:41 Analyzed: 11/21/2014 14:36 Source: B405123-01 Spike Source %REC RPD AnalYte Result Flag P91, units Level Result o/aREC Limits RPD Limit Notes Ethylene Glycol 220 10 mg/L 200 8.7 U 108 70-130 2 25 1,3-Bulylerti Glynn! 220 M91L 200 110 50-150 Classical Chemistry Parameters - Quality Control Batch 4K25O08 - EPA 1664A Blank (4K25008-BLK3) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Ana11de Result Elan QQl units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U 540 mg/L LCS (4K25008-BS1) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Anal.XtC Resul Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 21.2 5.00 mg/L 20.8 102 64.132 LCS Dup (4K25008-BSD1) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Analvte Resul f1w P-Q units Level Result %REC Limits RPD Limit Notes Od & Grease (HEM-SGT) Non -Polar Material 20.9 5.00 mg/L 20.6 101 64-132 1 34 FINAL TNS report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 7 of 9 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 8 or 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.c'om 1';N'�' P'('rs Of. q9 10 Exa--uliva P;i;k CCUll. Seta 111 Ind-;001 Gi. S:rnnfln. = -;!AQ� Jjao.sorwilla FLW215-^Cn W. 075'". (-1j71 5cE 5314 =ax {07T 8�c-2915 t902; f96300' FI-' pll; 17i9)4F7-20W P�lgt: CA Fjimp p K.1 e.1 P, Ti.. r I I IV tA, vpi.hnJ RCA I QUI - t.e] BV klatrix 7 GW,Gro nJmj!_i SO.S:-;l OW-D,iOinq Water WW A -Ail 0-0,11W (tluui H HC! lq 4CA03 5 H2$04 Mfft A "rrjllrs r—r.-JTV7f:d;o r-N�Cl j.nbn,-trc if, p-mFdari._ttv.dh vcon!Ujfl- livcrim I-.-- fc-- N :-,V, 'nrm wd0t;[ POO: mltor jci I IL "L QLA 0 mid Atlantic Engineering & Environmental Solutions May 5, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: m orn cn 409 Rogers View Court Raleigh, NC 27610 office 919,250.991a facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on April 7, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As summarized on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, P.G. Project Geologist Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Marsh Auto Parts, Inc. - Caryard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. (919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 doys of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 1s 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 4/7/2014 1.75 6.8 8.4 <1.60 <8.7 0.00276 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the PH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waive, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) 4�� 2, Si tore Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather. and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." rfe of Permittee or Designee) (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 4 �E NCO Laborato Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, April 22, 2014 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C401660 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, April 6, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page I of 9 �. �co www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C401660-01 Sampled: 04/07/14 10:00 Received: 04/08/14 12:00 Parameter EPA 1664A Hold Date/Time(s) 05/05/14 Prep Date/Time(s) 04/10/14 Analysis Date/Time(s) 11:30 04/15/14 09:35 EPA 6010C 10/04/14 04/09/14 1119 04/10/14 12:47 EPA 8015C 04/21/14 04/21/14 10:10 04/21/14 15:04 SM 2540D-1997 04/14/14 04/09/14 08:56 04/09/14 08:56 Client ID: Truckyard A Lab ID: C401660-02 Sampled: 04/07/14 11:30 Received: 04/08/14 12:00 Parameter EPA 1664A Hold Date/Time(s) 05/05114 Prep Date/Time(s) 04/10/14 Analysis Date/Time(s) 11:30 04/15/14 09:35 EPA 6010C 10/04114 04/09/14 1319 04/10/14 12:59 EPA 8015C 04/21l14 04/21/14 10:10 04/21/14 15:21 SM 2540D-1997 04/14J14 04/09/14 08:56 04/09/14 08:56 Client ID: Truckyard B Lab ID: C401660-03 Sampled: 04/07/14 11:45 Received: 04/08/14 12:00 Parameter EPA 1664A Hold Date/Time(s) 05/05/14 Prep Date/Time(s) 04/10/14 Analysis DatelTime(s) 11:30 04/15/14 09:35 EPA 6010C 10/04J14 04/09/14 13:19 04/10/14 13:02 EPA 8015C 04/21/14 04/21/14 10:10 04/21/14 15:38 SM 2540D-1997 04/14/14 04/09/14 08:56 04/09/14 08:56 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 (��Cmo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C401660-01 Ana Fvte Resuft Elm !:lU EQL yaII& Meth Notes Lead - Total 0.00276 3 0.00210 0.0100 mg/L EPA 6010C Total Suspended Solids 8.4 1.0 1.0 mg/L SM 254OD-1997 Client ID: Truck -yard A Lab ID: C4D1660-02 Ana Fvte Results Eldg MQL EQL Y.DAA MethNotes Lead - Total 0.00538 3 0.00210 0.0100 mg/L EPA 6010C Total Suspended Solids 53 1.0 1.0 mg/L SM 254OD-1997 Client ID: Trutkyard B Lab ID: C401660-03 Anal vte Results ELM MDL PQ.L Units Notes Lead - Total 0.0100 0.00210 0.0100 mg/L EPA 6010C Oil & Grease (HEM-SGT) Non -Polar Material 4.30 1 1.60 5.00 mg/L EPA 1664A Total Suspended Solids 64 1,0 1.0 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 9 �Cme www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C401660-01 Received: 04/08/14 12:00 Matrix: Surface Water Sampled:04/07114 10:00 Work Order: C401660 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary -Wl ed a-" INC 5911 AnalM [CAS Numberl Results fka Units PE MDL PSt6 Batch Method nA alyzed §y Notes Lead[7439-92-1]^ 0.00276 ] mg/L 1 0.00210 0.0100 4DO9027 EPA6010C 04/10/1412:47 3DH (Classical Chemistry Parameters ' ^ - ENCO G�ry Certified an.76 to INC 591) Analvte rCAS Numberl Results Flag Units PE M" E4L Batch Method Anallll NsT&6 Total Suspended Solids [ECL-0169]^ 8.4 mg/L 1 1.0 1.0 4DO9005 SM 254OD-1997 04/09/14 08:56 MMR Non -Halogenated Semivolatile Organics by GC ^-ENCO.ZY&"nwhR cefVficdanalyzeINC 442) Analvte rCAS Numberl Results ElAg units Pf MDL M Batch Method Analyzed By Notes Ethylene Glycol [107-21-1]^ 8,7 U mg/L 1 8.7 10 4D18010 EPA 8015C 04/21/14 15 04 3W3 Surroeates Results pE Soike Lv1 % Rec QbLRecLlmits @afiX Notes 1,3-8ulylene Glycol 210 1 200 10596 50-150 4018010 EPA 8015C 0412111415.-04 JWJ Classical Chemistry Parameters AnalAC rCAS Numberl DI & Grease (HEM-SGT) Non -Polar Material Results Flag Units PIE MPL EU Batch Method Analy& BY N 1.60 U mglL 1 1,60 5.00 41)10003 EPA 1664A 04/15/14 09:35 MY Description: Truckyard A Lab Sample ID:C401660-02 Received: 04/08/14 12:00 Matrix: Surface Water Sampled:04/07/14 11:30 Work Order: C401660 Project: Marsh Truck Parts Sampled By:Chent Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte INC 5911 Analvte [CAS Numbed Results Elm units PE HDL E Batch Method Analyzed By Notes Lead [7439-92-1]^ 0.00538 3 mg/L 1 0.00210 0.0100 4D09027 EPA 6010C 04/10/14 12:59 3DH Classical Chemistry Parameters ^ - ENCO Cary certified ana4te INC 5911 Analvte fCAS Numbed Results ' Flag Units PE MP4 P. L Batch Method Analyzed BY Notes Total Suspended Solids [ECL-0169]^ 53 mg/L 1 1.0 1.0 41309005 SM 25QD-1997 04/09/14 08:56 MMR INon-Halogenated Semivolatile Organics by GC ^ - ENCO Jackson Wle Certllled analyte INC 4421 Results Flao Units P.E MeL EQ.L Ankh Method Anab!zed Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/L 1 8.7 10 4D18010 EPA 8015C D4/21I14 15:21 3W3 Surnooalies B 2E Spike Lrl 0A RfS % Rec Lim Ita MerlrQ� Ana ¢Y Notes 1,3-8utylene Glycol 210 1 200 104 % 50-150 4D18010 EPA 8015C 04/21/1415:21 JWJ Classical Chemistry Parameters Analvte fCAS Numberl Oil & Grease (HEM-SG�) Non -Polar Material [ECL-0104] Resides Elan units 2f MP6 P.Q6 Batch Method Analyzed lilt Notes 1.60 U mg/L 1 1.60 5.00 4D10003 EPA 1664A 04/15/1409:35 MY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 (I�09 www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C401660-03 Received: 04/08/14 12:00 Matrix: Surface Water Sampled:04/07/14 11:45 Work Order: C401660 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte (NC 5911 Analyte rCAS Numberl Results Eta Units PIE MDL EM Batch Method Analyzed Ay Notes Lead [7439-92-1]A 0.0100 mg/L 1 0.00210 0,0100 4DO9027 EPA 6010C 04/10/14 13:02 3DH Classical Chemistry Parameters ^ - ENCO Cary -rty ,d a-4te (NC 5911 Analyte rCAS Numberl Refits Eli$ unm Pf MP-1. E" batch Method gnalvzed Ay Notes Total Suspended Solids [ECL-0169]^ 64 mg/L 1 1.0 1.0 4DO9005 SM 254OD-1997 G4109/14 08:56 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENCO Jacksonville ceMtka analyte INC 442] Anahft [CAS Number] Results Elm units PE MP6 E" batch Method Analyzed Ay Notes Ethylene Glycol [107-21-1]^ 8.7 ll mg/L 1 8.7 10 4D18010 EPA 8015C 04/21/14 15:38 3W3 surrogates Results pf Svj*e L l % Rec % Rec Limits 8adch Method Analy fy Notes 1,3-80tylene Glyml 200 1 200 101 % 50-150 4D18010 EPA 8015C 0412111415:38 JWJ Classical Chemistry Parameters Analyte rCAS Number] Oil & Grease (HEM-SGT) Non -Polar Material [ECL-0104] Results Ells Units PE MU EU AAkh Method Analyzed ft Notes 4.30 3 mg/L 1 1.60 5,00 4D10003 EPA 1664A 04/15/1409:35 M]F FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 5 of 9 (� �Go www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 4DO9027 - EPA 3005A Blank (4D09027-BLK3) Prepared: 04/09/2014 13c19 Analyzed: 04/10/2014 12:33 Spike Source 0/aREC RPD An Resuh Flaq 1Q Units Level Result %REC Limits RPD Limit Notes Lead 0100210 U 0.0100 mg/L LCS (41309027-B51) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:42 Spike Source °/a REC RPD Anal lde Result Elag P4L units Level Result %REC Limits RPD Limit Notes Lead 0.207 0.0100 mg/L 0.200 103 80-120 Matrix Spike (4D09027-MS1) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:49 Source: C401660-01 Spike Source %REC RPD .Analvte Result F.lao PAL Units Level Res %REC Limits RPD itmit Notes Lead 0.217 0.0100 mg/L 0.200 0.00276 107 75-125 Matrix Spike Dup (4D09027-MSD1) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:S2 Source:C401660-01 Spike Source o/aREC RPD __Analyte Resu t Flaq POLL Units Level Result "/oREC Limits RPD Limit (Votes Lead 0.211 0.0100 mg/L 0.200 0.00276 104 75-125 3 20 Post Spike (4D09027-PSI) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:54 Source: C401660-01 Spike Source %REC RPD Anal Resin Elm P9L U11it4 Level Result %REC Limits RPD Limit Notes Lead 0,195 0.0100 mg/L 0.200 0.00276 96 80-120 Classical Chemistry Parameters - Quality Control Batch 4DO9005 - NO PREP Blank (4D09005-BLK1) Prepared & Analyzed: 04/09/2014 08:56 Spike Source %REC RPD Anal vte Result Elaq P QL Units Level Result %REC Limits RPD Limit Notes - Total Suspended Solids 1.0 U 1.0 mg/L LCS (4D09005-BS1) Prepared & Analyzed: 04/09/2014 08:56 Spike Source %REC RPD _Analvte Result Flao 13% Units Level ReSu %REC Limits RPD Limit Notes Total Suspended Solids 100 110 mg/L 100 103 80-120 Duplicate (4D09005-DUPi) Prepared & Analyzed: D4109/2014 08:56 Source: C404629-01 Spike Source %REC RPD Anal vte Result Flaq IQ Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 440 1.0 mg/L 400 10 10 Duplicate (4D09005-DUP2) Prepared & Analyzed: 04/09/2014 08:56 Source: C404629-02 Spike Source %REC RPD Anal ldg Result Flag POL Units Level Rig %REC Limits RPD Limit Notes Total Suspended Solids 26 1.0 mg/L 26 3 10 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. paw 6 of 9 hlCC:] www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semirfolatile Organics by GC - Quality Control Batch 4D18O10 - NO PREP Blank (41D18010-BLK1) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 12:38 Spike Source %REC RPD Anal vte Result Bag POLL Units Level Resin %REC Limits RPD Limit Notes Ethylene Glycol 8.7 U 10 mg/L 43-8utylene Glycol 210 M91L 100 105 50-150 LCS (4D18010-BS1) Prepared: 04/21/2014 10a0 Analyzed: 04/21/2014 10:30 Spike Source 0/oREC RPD Analvte Result Flag POI- Units Level Result 0/aREC Limits RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 102 70-130 1,3-8utylene Glycol 130 mg/L 100 113 50-150 Matrix Spike (41D18010-1451) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 10:56 Source: B401742-01 Spike Source 0/6REC RPD Anal Result Elea POL units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 83 U 102 70-130 43-8utylene Glycol 210 mg/L 100 106 50-150 Matrix Spike Dup (41318010-1V1SD1) Prepared: 04/21/2014 10:10 Analyzed: D4/21/2014 11:13 Source: 8401742-01 Spike Source %REC RPD Anal lde Result Fig P" units Level Result D/aREC Limits RPD Limi Notes Ethylene Glycol 200 10 mg/L 200 8.7 U 99 70-130 3 25 1,3-8utylene Glycol 210 -91L 200 107 50-150 Classical Chemistry Parameters - Quality Control Batch 4DI0003 - EPA 1664A Blank (41)30003-BLKI) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source 0/4REC RPD Anal Result Flag POL U n As Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGF) Non -Polar Material 1.60 U 5100 mg/L LCS (4D10003-BS1) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source %REC RPD Anal lrfe Result Ehm P_LL ShitllS Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Nan -Polar Material 18.4 5.D0 mg/L 21A B7 64-132 LCS Dup (4D10003-BSD1) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source %REC RPD Analvte Result Fiala P91 Units Level Re 0/aREC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.4 5.00 mg/L 21,2 87 64-132 0.2 34 Matrix Spike (4D10003-MS1) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Source: B401565-02 Spike Source %REC RPD -Analvte Result Flag PO.L Units Level ResuR %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 94.4 6.35 mg/L 26.0 34.3 231 64-132 QM-07 FINAL This report relates only to the sample as reodyed by the laboratory, and may only be reproduced in full. Page 7 of 9 (R�Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com w7s Centrai Pon Or. 4810 Fxeculive Park Court, Suite 1 I 1 K12-A WWdwireis InduAriai CL Y Orland0. FL 32824 .iacksondle, FL 32216-6oeq Cary, NC 27511 007)1226-5314 Fax (407) 850-6945 (90-1).296.3007 Fax (9W) 29tidi210 (919) 467-3090 Fax (919) 467-35t5 Page of i.Ilellt Name Project Number Requested Analyses Requested Turnaround - Marsh Trur-k Parts (MA035) _[npne] Times - fJote :Rush requests srrhjnrl in A;kirest; Projact NamerUesc P.O. Box 427 Marsh Truck Parts acceptance by the facility CiySTIZIp PO Of Billing Into Siier Ch , NC 27 344 � � _ Standard Tel Fax Report,ng Contact (919) fi63-1�0,� Steve Marsh 7' C _ Expedited Sarrpler(s) Name. 41.1ladw (r'rin-) Billing Contact Chuck Hof -man Due r � Samplerfs) Signature Site. Ln .Jlinn i Time Zone Lab Worliorder _- � � ..; = F� : 00 1- ad Preservation 40166 _ J (Sea Codes) {Combine as necessaryj Co;lecticu matrix Total N of l Rom 4` Sample Ill (Field Edent,licat;on} Collection Date 71tne Comp; Grab !see codes) ContainerS � Sample Comments TrLlcky'aard ilS1 '-t -1 — tLI 1 I; Sw 7 X X X X TnaG. and EI _it (y ' 1.4 .g f+. SW .- 7 ' X X. : X X I r'k- .�_K t _-Z I 'i Y'= -:•� wl .-fit �' ,� _ 1 < Totat 0 of Containers Same Kt Frepared Cy Date,?ime Reiirmuishhed1Ry r !]ulcTirriy Rrxer:ed y Dot P e CommentslSpecial ReMrting Requirernenls Relinquished y 4aie, rf R eived ate me Relimuisned By I Date,'Time R ed By n:sln/Time r tl's & Tenips on Receipt Conditirn an Aecelpt r � Acceptable Unacceptable Ustrix GW-Groundwater 54Soit DW-Drinking Water SE-Sttdimont SWSwlace Wati:= WW'Naslewafer A -Air 0-01hei (detail in comments) Preservation: 1-Ice R-HU N-HNO3 S-HZSO4 NO-NaOH O-Otherldetail In comments) Note : All samples submitted to ENCO labs are in accordance with the terms and cunditiuns listed on die ieverso of this form, unless prior written agreements exist L NOW Atlantic Engineering & Environmental Solutions May 5, 2014 Mr. Steve Marsh Marsh Auto Parts, Inc. Post Office Box 427 Siler City, NC 27344 Subject: MARSH AUTO PARTS, INC. — CARYARD 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NGG100015 MID -ATLANTIC JOB NO. 00OR2372.02 Dear Mr. Marsh:_- 409 Rogers View Court Raleigh. INC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find three copies of the Stormwater Discharge Monitoring Report (DMR) for the above -referenced site. Please follow the instructions below to complete this sampling event. 1. Sign and date each DMR on page 2; 2. Forward the first two copies of the report along with the attached cover letter to the Division of Water Quality (mailing address is on the first page of the DMR); and 3. Insert the third copy (labeled "FILE") into Appendix C of your Stormwater Pollution Prevention Plan. Please note that the next stormwater sample can be collected on or after July 1, 2014. We will arrange for delivery of the sample coolers prior to this date. If you have any questions, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, P.G. Project Geologist Attachments: Cover Letter Stormwater Discharge Monitoring Reports Laboratory Analytical Reports EXPERIENCED CUSTOMER FOCUSED INNOVATIVE