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HomeMy WebLinkAboutNCG100014_MONITORING INFO_20190612STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V C& 1 Do DOC TYPE ❑HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ a�I9 O�Q Ia YYYYMMDD v 409 Rogers Vicw Court Mid Atlantic fnRaleigh, 19.7 299Ia of nee sIs.250.ssi8 Engineering & Environmentaf Solutions facslMlte 919,2W9950 MAAONLINE.COM ED May 24, 2019 JUN 2 2Q19 DIIy�r'� 'Os' TioN NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — TRUCK YARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on May 13, 2019 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCEO CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 FACILITY NAME Marsh Auto Parts, Inc. - Truckyard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample. Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units TotalSuspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead; Total Recoverable, mg/L TotafToxic Organics3, mg/L Benchmark - - 6.0-9.01 ` 100/50Z is 8,000 (Tiers 2'and 3) 0.03 1.0 Outfall A 05/13/19 1.45 6.8 14 <2.70 0.7 0.00480 J NA Outfall B 05/13/19 1.45 7.2 10 <2.70 <4.7 <0.00310 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit, 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix 0, Table II of Chapter 44 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Manogement Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) jq,t r Title (Print title) 54�� e. Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) s `— �q_ (Date) Form 5W U-251, last revised October 25, 2012 Page 2 of 2 ENCO Laboratones Accurate, Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, May 24, 2019 Marsh Truck Parts (MA035) Attn: Steve Marsh P.Q. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Truck Yard ENCO Workorder(s): CCO2611 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, May 13, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 (9mil 99 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: TruckyardA Lab ID: CCO2611-01 Sampled: 05/13/19 11:00 Received: 05/13/19 14:00 Parameter EPA 1664B Preparation EPA 16648 Hold atelTime(s) 06/10/19 Preo Date/Time(s) 05/13/19 15:43 Analysis DAMITlme(s) 05/17/19 13:56 EPA 6010D EPA 3005A 11/09/19 05/14/19 13:54 05/17/19 10:56 EPA 8015C NA 05/27/19 05/21/19 09:00 05/21/19 14:08 SM 254OD-2011 NO PREP 05/20/19 05/20/19 09:47 05/20/19 09:47 Client ID: Truckyard B Lab ID: CCO2611-02 Sampled: 05/13/19 11:15 Received: 05/13/19 14:00 Parameter RrepAration hold Date/Trme(s) Prep DatelTime(s) Analysis Date/Time(s) EPA 1664B EPA 1664E 06/10/19 05/13/19 15:43 05/17/19 13:56 EPA 60101) EPA 3005A 11/09/19 05/14/19 13:54 05/17/19 10:59 EPA 8015C NA 05/27/19 05/21/19 09:00 05/21/19 14:27 SM 2540D-2011 NO PREP 05/20/19 05/20/19 09:47 05/20/19 09:47 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Truckyard A Lab ID: CCO2611-01 Anelyte Resin E619 Hu EQL Units Method Note Lead - Total 0.00480 3 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 14 3.1 3.1 mg/L SM 2540D-2011 Client ID: Truckyard B Lab ID: CCO2611-02 Total Suspended Solids Results flAg MQL P.QL uoibi 10 4.0 4.0 mg/L Method SM 2540D-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 Description: Truckyard A ANALYTICAL RESULTS Lab Sample ID: CCO2611-01 Matrix: Surface Water Sampled:05/13/19 11:00 Project: Truck Yard Sampled By: CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods CIO) www.encolabs.com Received: 05/13/19 14:00 Work Order: CCO2611 ^ - ENCO Cary cued ana0e [NC 5911 Analyte rCAS Numberl Results figs Units PE M2L M Batch Method Analyzed Jay Notes Lead [7439-92-1]^ 0.00480 1 mg/L 1 0,00310 0.0100 9E14024 EPA 6010D 05/17/19 10:56 JDH Classical Chemistry Parameters ^ - ENCO Cary-Arficd.7-1yte (NC 591] Analyte rCAS Numberl Results Hag unu pf tML EQL Balch Method Ana bEx 1t Notes Total Suspended Sollds^ 14 mg/L 1.25 3.1 3.1 9E20002 SM 2540D-2011 05/20/19 09:47 LG Non -Halogenated Semivolatile Organics by GC Analyte rCAS Numberl g9su]b E[ag units DE Na PQL D trh Method Analyzed 1f1 Dotes Diethylene Glycol[111-46-6] 4.3 U mg/L 1 4.3 10 9E21008 EPA 8015C 05/21/19 14:08 JIB Ethylene Glycol[107-21-1] 4.7 U mg/L 1 4.7 5.0 9E21008 EPA 8015C 05/21/19 14:08 JIB Propylene Glycol[57-55-6] 4.3 U mg/L 1 4.3 5.0 9E21008 EPA 8015C 05/21/19 14:08 JIB Triethylene Glycol [112.27.6] 6.9 U mg/L 1 6.9 10 9E21008 EPA 8015C 05/21/19 14:08 JJB QL-02 S&Mmtes Qf M& l vl % Rec % Rec Limits AR A & Notes 1,3-&Wene Glycol 240 1 200 119 % 61-125 9E21008 EPA 8015C 05/21/1914:08 JJB Classical Chemistry Parameters ^ - ENCO Jad" 711e cerfrfied ana" [NC 442] Analyte FCAS Numberl Results fin S[nm yf MU pUL Batch Method Analyze Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 9E13011 EPA 1664E 05/17/19 13:S6 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CCO2611-02 Received: 05/13/19 14:00 Matrix: Surface Water Sampled:05/13119 11:15 Work Order: CCO2611 Project: Truck Yard Sampled By:CLIENT . Metals (total recoverable) by EPA 6000/7000 Series Methods L3 ^ - ENCO Cary rerirfied analyze iNC 591J Analyte rCAS Numberl Results Bu Units if MU PQ.6 Ankh Method Analyzed By Notes Lead [7439-92.1]^ 0.00310 U mg/L 1 0.00310 0.0100 9E14024 EPA 6010D 05/17/19 10:59 ]DH Classical Chemistry Parameters ^ - EMCO Cary certified analyze (NC 591J Results Flag ab Rf MPl PQL Batch Method Analyzed By Notes Total Suspended Solids^ 10 mg/L 1,61 4.0 4.0 9E20002 SM 254OD-2011 05/20/19 09:47 LG Non -Halogenated Semivolatile Organics by GC Analyte [CAS Numberl RepUlts Elag Units Df MU M Ad= Method Analyzed 01 Notes Diethylene Glycol[111-46-61 4.3 U mg/L 1 4.3 10 9E21008 EPA 8015C 05/21/19 14:27 JIB Ethylene Glycol[107-21-11 4.7 U mg/L 1 4.7 5.0 9E21008 EPA 8015C 05/21/19 14:27 JIB Propylene Glycol[57-55-6] 4.3 U mg/L 1 4.3 5.0 9E21008 EPA 8015C 05/21/19 14:27 JIB Triethylene Glycol[112-27-6] 6.9 U mg/L 1 6.9 10 9E21008 EPA 8015C 05/21/19 14:27 JIB QL-02 Surrogates Results pf Spikevl %Rec %ReCLimlls A= dBy Notes 1,3 Bury/erte Glyml 260 1 200 130 % 61.125 9E21008 EPA 8015C 0512111914:17 JIB OS-03 Classical Chemistry Parameters ^ - ENCO Jacksonville [eviified analyze (NC 442] Analyte rCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material^ Results Elag Vhm PE M2L R" DAWb Method Analyzed ]U Note 2.70 u mg/L 1 2.70 5.00 9E13011 EPA 1664B 05/17/19 13:56 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 �JVC10 www.encolabs.Com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 9E14O24 - EPA 3005A Blank (9E14024-BLK1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:35 Spike Source %REC RPD -Analyte Result Flag POL Units Level Result %REC Limits RPD LlmU Notes Lead 0.00310 U 0.0100 mg/L LCS (9E14024-BS1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:41 Spike Source %REC RPD Anal s Result Flag POL Units Level Be6u °/oREC Limits RPD Limit Notes Lead 0.195 0.0100 mg/L 0.200 98 80-120 Matrix Spike (9E14024-MS1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:46 Source: CCO2610-01 Spike Source a/oREC RPD fijmlvte Result Flag P_OL Units Level Result %REC Limits RPD Like ij Notes Lead 0.197 0.0100 mg/L 0.200 0.00310 U 98 75-125 Matrix Spike Dup (9E14024-MSD1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:49 Source: CCO2610-01 Spike Source %REC RPD -Analyft Result Flap ROL Units Level Resin 9/aREC Limits RPD Limit Notes Lead 0.196 0.0100 mg/L 0.200 0.00310 U 98 75-125 0.2 20 Post Spike (9E14024-PS1) Prepared: 05/14/2019 13:54 Analyzed: 05/17/2019 10:51 Source: CCO2610-01 Spike Source %REC RPD Anal vte Result Flap POL Units Level ResulF °/oREC Limits RPD Limit Notes Lead 0.205 0.0100 mg/L 0.200 0.00139 102 80-120 Classical Chemistry Parameters - Quality Control BBtCh 9E2OOO2 - NO PREP Blank (9E20002-BLK3) Prepared & Analyzed: 05/20/2019 09:47 Spike Source %REC RPD Anal adg Result Fld9 ROL .Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9E20002-651) Prepared & Analyzed: 05/20/2019 09:47 Spike Source %REC RPD .AnAIM Result Flap POL Units Level Result a/oREC Limits RPD imi Notes Total Suspended Solids 96 2.5 mg/L 100 96 80-120 Duplicate (9E20002-DUP3) Prepared & Analyzed: 05/20/2019 09:47 Source: CCO5461-01 Spike Source %REC RPD -Anatvte Result Flap POL units Level Result a/oREC Limits RPD LjMU Notes Total Suspended Solids 220 110 mg/L 200 9 20 Duplicate (9E20002-DUP2) Prepared & Analyzed: 05/20/2019 09:47 Source: CC06600-01 Spike Source °/oREC RPD Analvte Result Ela9 F!" Units Level Result °/oREC Ljml RPD Limit Notes Total Suspended Solids 110 71 mg/L 120 5 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in fu3l. Page 6 of 9 0�14 C 6: __ M19) www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 9E21008 - NA Blank (9E21008-BLK1) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 15:23 Spike Source %REC RPD Anahrte Rwlt Flag PL Uslits Level Result %REC Limits RPD Llmft dotes Diethylene Glycol 4.3 U 10 mg/L Ethylene Glycol 4.7 U 5.0 mg/L Propylene Glycol 4.3 U 5.0 mg/L Triethylene Glycol 6.9 U 10 mg/L 1,3-8u1ylene Glycol 210 m91L 200 106 61-125 LCS (9E21008-BSI) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 13:11 Spike Source 9/*REC RPD -Analvt Result F.iag RQL Units Level Result %REC Limits RPD Motes Diethylene Glycol 250 10 mg/L 200 124 61-127 Ethylene Glycol 240 5.0 mg/L 200 119 73-132 Propylene Glycol 190 5.0 mg/L 200 97 74-123 Triethylene Glycol 310 10 mg/L 200 157 44-137 QL-02 1,3-6utylene Glycol 200 m9/1 200 100 61-125 LCS Dup (9E21008-BSD1) Prepared: 05/21/2019 09:00 Analyzed: 05/21/2019 13:30 Spike Source %REC RPD Anavte Result ElAg P_4.1. Units Level Result %REC Limits RPD Limjt Notes Diethylene Glycol 240 10 mg/L 200 118 61.127 5 11 Ethylene Glycol 200 5.0 mg/L 200 98 73.132 19 10 QR-06 Propylene Glycol 210 5.0 mg/L 200 104 74-123 8 8 Triethylene Glycol 250 10 mg/L 200 124 44-137 23 16 QR-06 1,3-8u[y4ene Glycol 180 m9/L 200 91 61-125 Classical Chemistry Parameters - Quality Control Batch PE13011 - EPA 16640 Blank (9E13011-BLX1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source */*REC RPD -Anal Resu t Flag ROL MtS Level Resu %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (9E13011-BSI) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source %REC RPD Anal Result Ehu P91 YA112 Level Result %REC Limits RPD Ltnnit Notes Oil & Grease (HEM-SGT) Non -Polar Material 71.7 5.00 mg/L 81.0 88 64-132 LCS Dup (9E33011-BSD3) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Spike Source %REC RPD .Analyte Result Elan PQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 67.3 5.00 mg/L 79.7 85 64-132 6 34 Matrix Spike (9E13011-MS1) Prepared: 05/13/2019 15:43 Analyzed: 05/14/2019 15:16 Source: BCO2004-01 Spike Source %REC RPD .AntMe Res"I flan P-9L Units Level Result o/*REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 50.0 5.00 mg/L 74.6 2.70 U 67 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 7 Df 9 0NSC� www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column, The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QR-06 The RPD value for the LCS/LCSD was outside of QC acceptance limits. QS-03 Surrogate recovery outside acceptance limits FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OR -CUSTODY RECORD www.encolabs.com• I0775 Genoa] Poi Dr. 4810 Ememovo Ptlr4 Court- Suta I I I 102-A Woodwmd3 InduSYal CL Orlando. FL 32824 Jedrsrinvile. FL 3Z21GZM Cary. NC ml l (407) 82fr53ra- Fay (407) 850•t M (904) 29E3007 Fax (904) 295-6210 - (919) 4b7.9090 Fax (91914117-3515 Paige OF c4lent Memo . Project Number Rsquaatod Ana"M Requested Turnaround Marsh Truck Parts (MA035) -(none], Times Ar[dre33 - Prorom mmov= - Wen.- Rush requexta suo)ea to P - O. , Box 427 Truck Yard arx:oatanca by Iha radfily ca,rrsrrc�, - PO 0 r rlrInD Ift Siler City . NC 273" ❑ Standard Tel Far P.epaHrig Contact CD (919) 663-1908 Steve'.Marsh A _ Expedited swmdvrts) Name. 4tfilatbn (Prinq esenq u' c Holtman Due — In sarlplttr(s) Slgnsturo Sits Lo=cn I nmo Zenop e tab WOfieordei Goa a� � CCO2f 11 PresemaU (See Codes) (Combine as oecesaery). Gdlwllon Ivlablx 'Towel x of } 4oir, a Simplu ID (Field Idanlikkkki) Collodion Oats 'rmw :Comp l,Giab (sea Codes) canw-le,s Sample Comments TEuiaic yard A t:-A'M° '�? SiN 7. X X' X X e Truckyard B '� % < < i$ A Sw 7 X X X ` X ri aPrAl11 . C <--Total ## oLCantBiner8 Sample Kit Prepared By. ,.r 411 Datol11a18 Reilnquls BV - Da197lme RoWmd By. Datr!?Ime Comm=-JSpacial Reporting Roquircmans j Refinqurhod BY Didammo RacervoB By DallYnrlo Helirpui9hed fay untelrlme Received By Ualcrflmrs Gootnr Ot d Tempi: an Receliet b`.Acceptable Cordon Upon Peceipt Unacceptable Matrix. GW-Groundwolor SO-Soi OW -Drinking Water SESedmera SWSurtacm Water WW-MmIwtater A -Air "Ihw (detail In commentsl Prosarwdan: 1-Iep H-HCI :N.HNO3 &H2SO4 NO-NeGH D-Oltear. (datall In rornmonm) Nato. Ad ramcloz a timWcd to ENGO Lobs are In oworowvo with Me tom1B and corrd,00AS ILMad on the wereo of Wo torn. unless prior wiitton agmOrlontr 0IS1 Sample Preservation Verification ENCO Cary Work Order: CCO2611 Project: Truck Yard Client: Marsh Truck Parts (MA035) Project #: [none] Lagged In: 13-May-19 14:59 Logged By. Rachel Ann YrnIsh , - w Date/Time:Z-5, n I I q 5 Preservation Check Performed By: ' CCO2611 -01 pK' heckedl/.'"'k Pate/Time P 0- Requ refnent. i n C-'6.'n &6' 1'- ,�k B 250rnLA+H2SO4 <2 Y / N (NA Y I N I C 250mLA+H2SO4 <2 Y I N I Y I N I UA I D J2.50mLP+HNO3 1 <2 rY ) N I NA Y (,N) NA CCO2611-02 --l-I 1 Tye 5, Pres',(pl-l) PHCheckedI,; ;5r,,,- 7, 77. F-7-Dateffime!—, O.H ed '�AAUSt6d -` Rea ro '0 - L - !4L� V IS 250MLA+H2SO4 <2 Y f N 16� Y / N CpraA C 250MLA+H2SO4 <2 Y I N I'V&- 'Y / N / UA D 1250mLP+HNO3 1 �2 (M N I NA_J Y QN l NA . Reagent Name ID 2 pH Strip ID: PH Strips C&741 Reagent Name ID 3 4 Reagent Name ID 6 C:\elmnt%PrimkwKv-, --..-... A Page 1 of 1 r 409 Rogers View Court Mid Atlantic Raleigh. NC 2710 office 919.250.9918 Engineering & Environmental Solutions facsimile 919.250.9950 MAAON LINE.COM November 26, 2018 NCDEQ/DWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED Subject: STORMWATER SAMPLING RESULTS DEC 0 4 Z015 MARSH AUTO PARTS, INC. — TRUCK YARD CENTRAL FILES 3700 SILER CITY SNOW CAMP ROAD GWR SECTIO^1 SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on October 26, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report Laboratory Analytical Report a EXPERIENCED CUSTOMER FOCUSED INNOVATIVE Is STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 FACILITY NAME Marsh Auto Parts. Inc.-Truc!9ard PERSON COLLECTING SAMPLE(S) Stephen Marsh _ CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 COUNTY Chatham PHONE NO. 919 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date -Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic 3 Organics , mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 10/26/18 1.30 6.8 14 <2.70 <4.7 0.008471 NA Outfall B 10/26/18 1.30 7.0 7.6 <2.70 <4.7 0.005101 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table It of Chapter 40 Code of Federal Regulations (CFR) Part 122, Form SWU-2S1, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) k% s~ Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) 1-Zq - (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 QP ENCO Laboraton'es Accurate. Timely. Responsive Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, November 8, 2018 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CB06058 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 26, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 CeC0 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C806058-01 Sampled: 10/26/18 09:20 Received: 10/26/18 13:45 Date/Time(s) Parameter EPA 1664B Preparation EPA 1664B Hold DatelTime(s) 11/23/18 Preo QatelTime(s) 11/01/18 12:25 Analysis 11/05/18 11:39 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:23 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:03 5M 25400-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 Client ID: TruckyardA Lab ID: CB06038-02 Sampled: 10/26/18 09:40 Received: 10/26/18 13:45 Parafn ter EPA 1664E Preparation EPA 1664B Hold Date/Time(s) 11/23/18 Prep DatelTime(s) 11/01/18 12:25 Analysis Date/Time(s) 11/05/18 11:39 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:26 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:22 SM 2540D-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 Client ID: Truckyard B Lab ID: CB06058-03 Sampled: 10/26/18 09:50 Received: 10/26/18 13:45 Analysis DateMme(s) Parameter EPA 1664B Preparation EPA 1664E Hold Date/Time(s) 11/23/18 Prep_Date/TimeW 11/01/18 12:25 11/05/18 11:39 EPA 6010D EPA 3005A 04/24/19 11/06/18 10:41 11/07/18 10:28 EPA 8015C NA 11/09/18 10/31/18 05:37 10/31/18 08:40 SM 254OD-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 �uco www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Ca ryard Lab ID: CB06058-01 Analyze Results EIM Ma E" !!nits Method tl= Total Suspended Solids 12 2.5 2.5 mg/L SM 254OD-2011 Client ID: Truckyard A Lab ID: CB06058-02 Auslyte Re%iul s Ela9 MU M llnits Method rL41e5 Lead - Total 0.00847 J 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 14 3A 3.1 mg/L SM 2540D-201 t Client ID: Truckyard B Lab ID: CB06058-03 Analyte Results fida Mil EM !!nits Meth9d Notes Lead - Total 0.00510 3 0.00310 0.0100 mg/L EPA 6010D Total Suspended Solids 7.6 2.5 2.5 mg/L SM 2540D-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 CS www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID: CB06058-01 Received: 10/26/18 13:45 Matrix: Surface Water Sampled:10/26/18 09:20 Work Order: CB06058 Project: Marsh Truck Parts Sampled By: CLIENT (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENC17 CWry certified a-aty (NC 5911 Analvte rCAS Numberl gel Elm Vilm 2E MIL pQL Batch Metho Analyzed ft Note6 Lead [7439-92-1]^ 0.00310 U mg/L 1 0.00310 0.0100 8KO6017 EPA 601UD 11/07/18 10:23 JDH lClassical Chemistry Parameters i ^ - EMCO Cary cerMW analyte [NC VI] Analvte rCAS Numberl Results Flag YJAM DE MU M Batch Method Analyzed Ay Note Total Suspended Solids^ 12 mg/L 1 2.5 2.5 8330003 SM 2WD-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC Analvte rCAS Numberl Results ELdg Units 2E Mph EM litrh Method Analyzed ft Note Ethylene Glycol[107-21-11 4.7 U mg/L 1 4.7 5,0 8330004 EPA 8015C 10/31/18 08:03 I38 & mrra[es Results RE 5eike Lv! % Rec % Rec LA By Notes 1,3•Buty4ene Qw-/ 1&0 1 200 92 % 50-150 MOW4 FPA 801SC ID131118 08:03 JJB Classical Chemistry Parameters ^ - ENCO Jacksonville certified analyze [NC 442] BesulLf fin Units PE MU EQL 111=h Method Analyzed It1[ Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2,70 5,00 8KO1008 EPA 1664B 11/05/18 11:39 SMA .� Ae lA Description: Truckyard A Lab Sample ID:CB06058-02 Received: 10/26/18 13:45 Matrix: Surface Water Sampled:10/26/18 09:40 Work Order: CB06058 Project: Marsh Truck Parts Sampled By:CLIENT Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certthed anaiyte [NC 5911 Analvte rCAS Numberl Results Flag Mau 2E M12L E" Batch Method Analyzed lty M= Lead [7439-92-1]^ 0.00847 J mg/L 1 0.00310 0.0100 8K06017 EPA 6010D 11/07/18 10:26 JDH Classical Chemistry Parameters ^ ENCV Cary c"6ed analyte (NC 5911 Analvte rCAS Numberl Results Elan Units 2E MPS E2L Batch Method Analyzed gy Notes Total Suspended Solids^ 14 mg/L 1.25 3.1 3.1 8130003 SM 2540D-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC Analvte rCAS Numberl Results Elan Units 2E MIL EM film Method Ana lyzed ft BOW Ethylene Glycol[107-21-1] 4.7 U mglL 1 4.7 5.0 8330004 EPA 8015C 10/31/18 08:22 JIB Surrogates g pf Spike L v1 % Rec a/o Rec L/mitr Ak= Meth A By Notes 1,347uty4ene Glycol 190 1 200 94 % 50-150 8J30004 EPA 8015C 10131118 08.•22 JJ8 Classical Chemistry Parameters ^ - EAsCO JacksanvrlM C"fied analyte [NC 442] Analvte rCAS Numberl Results EL>t.lr MAM DE M" E" Batch Method Analyze Q Ily Kau Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 8KO1008 EPA 16643 11/05/18 11:39 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 CIE.00 www.encolabs.com 1. ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CB06058-03 Received: 10/26/18 13:45 Matrix: Surface Water Sampled:10/26/18 09:50 Work Order: CB06058 Project: Marsh Truck Parts Sampled By:CUENT Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary c-trmd analyte (NC S911 Analvte rCAS Numberl Results Elan Units QE MIL ML Batch Method Analyze By dote: Lead[7439-92-1]^ 0.00510 ] mg/L 1 0.00310 0.0100 8KO6017 EPA6010D 11107/1810:28 ]DH JClassical Chemistry Parameters ^ • EACO C-y crrtlBed aaalyte (NC 5911 Ana [CAS Numberl Results E[as Units gE M12L E" Bah Mid Analyzed Ry Note Total Suspended Solids^ 7.6 mg/L 1 2.5 2.5 BJ30003 SM 2540D-2011 10/30/18 10:02 OMR Non -Halogenated Semivolatile Organics by GC Analvte rCAS Numberl Result Elm Units pE MU E2L Aaf&h Method Analyzed By Note Ethylene Glycol[107-21-1] 4.7 U mg/L 1 4.7 5.0 8130004 EPA 8015C 10/31/18 08:40 33B Surrmahes PI Salke 1 vl % Rec % Rec Llmlls A= Keth Analvred fir Notes 1,3-Sutylerte GIX01 200 1 200 98 % 50-150 W30004 EPA 8015C 10131118 08.40 _77B Classical Chemistry Parameters ^ - EAKt7 Jackranvllle certified analyte JAC 4421 Analvte rCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material^ Resul BA9 thllts Ai N" E" Blkh Metho Anallzed By Notes 2.70 U mg/L 1 2.70 5.00 BK01008 EPA 1664B 11/05/18 11:39 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 5 of 9 0 9 1 Em F. F. , s www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 8KO6017 - EPA 3005A Blank (SK06017-BLKI) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:04 Spike Source %REC RPD Anal Yte Result ila9 P-41. Units Level Result °/nREC Limits RPD Limit Notes Lead 0.00310 U 010100 mg/L LCS (SK06017-BSI) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:10 Spike Source %REC RPD Anilil1dl" ReiLllt flag QQL Units Level Resin %REC Limits RPD Llmft Notes Lead 0.195 0.0100 mg/L 0.200 98 80-120 Matrix Spike (8K06017-MS1) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:13 Source: CB14770-04 Spike Source %REC RPD Anal lde Result flag PQL units Level Result %REC Limits RPD Notes Lead 0.191 0.0100 mg/L 0.200 0.00310 U 96 75-125 Matrix Spike Dup (8K06017-MSDS) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:16 Source: CB14770-04 Spike Source %REC RPD Anal vte Result Ela9 R4L Units Level Result %REC Limits RPD Limit Notes Lead 0.189 0.0100 mg/L 0.200 0.00310 U 94 75-125 1 20 Post Spike (8K06017-PS1) Prepared: 11/06/2018 10:41 Analyzed: 11/07/2018 10:18 Source: C614770-04 Spike Source %REC RPD Anal Result Elan P-01 Wilits Level Result %REC Limits RPD Limit Notes Lead 0.205 010100 mg/L 0,200-0.000768 102 80-120 Classical Chemistry Parameters - Quality Control Batch W-70003 - NO PREP Blank (B)30D03-BLK1) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD Anal ltlS Result Hag R l Units Level Remit %REC Limits RPD Limit Notes Total Suspended Soiids 2,5 U 2.5 mg/L LCS (8)30003-BSI) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD -Anahite Result E1s74 e41 unim Level Result %REC Urrift RPD Litt Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 Duplicate (8330003-DUPl) Prepared & Analyzed: 10/30/2018 10:02 Source: CB15181-01 Spike Source %REC RPD Analyt Result Flag POL units Level Result °/aREC Limits RPD Limit Notes Total Suspended Solids 2700 500 mg/L 2200 19 20 Duplicate (8330003-DUP2) Prepared & Analyzed: 10/30/2018 10:02 Source: C616046-01 Spike Source %REC RPD Ana RCsulfin e4L units Level Resin %REC Limits RPD Lim$ Notes Total Suspended Solids 220 50 mg/L 230 4 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 Ce�� www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch W30004 - NA Blank (6130004-BLKI) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 06:59 Spike Source %REC RPD Anal vte R95It Elag QQL Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 4.7 u 5.0 mg/L 1,3-&Wene G/Arn/ 210 m9AL 200 105 50-150 LCS (8130004-BS1) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 07:18 Spike Source %REC RPD Anal vte Result Elan PQL Units Level Result %REC LIM116 RPD Limit Notes Ethylene Glycol 230 5.0 mg/L 200 117 70-130 1,3-841)4ene G/ycol 200 nV11 200 102 50-150 LCS Dup (8130004-BSD3) Prepared: 10/30/2018 05:39 Analyzed: 10/30/2018 07:36 Spike Source %REC RPD Analyte Result EIAO EQL units Level l exult %REC Limits RPD Limit Notes Ethylene Glycol 240 5.0 mg/L 200 118 70-130 0.8 25 1,3-Sutylene Glycol 190 m91L 200 93 50-150 Classical Chemistry Parameters - Quality Control Batch 8KO1008 - EPA 16645 Blank (SK01008-BLK1) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Anal vte Result Elag P_QL Units Level Resin %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 u 5.00 mg/L LCS (8K01008-BSI) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Anal vte Resgli On ROL Units Level Result %REC Lcflib RPD Limit dotes Oil & Grease (HEM-5GT) Non -Polar Material 78.6 5.00 mg/L 82.3 96 64-132 LCS Dup (8K01008-BSD1) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Analvte RrAult Flap QQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-5GT) Non -Polar Material 86.8 5.00 mg/L 80.0 108 64-132 10 34 Matrix Spike (8K01008-MS1) Prepared: 11/1)1/2018 12:25 Analyzed: 11105/201B 11:39 Source: BB04387-03 Spike Source %REC RPD -141a1M Resul Flag POL urlit5 Level Result %REC Limb RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 86.1 5.00 mg/L 84.4 6,12 95 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 0 F. F. NS www.encolabs.com FLAGS/NOTES AND DEFINITIONS :1 B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL; Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 10775 Central Port Or. 4810 E»trre Park Corm, Suite 111 102-A WoodwuWs Industrial Ct. Orlando, FL 32024 Jacksorr ille. FL 32216-6M Cary, NC 27511 w (407) a26.5314 Fax (407) S50-6945 (904) 296-3007 Fax (904) 296.6210 (919) 467-3090 Fax (919) 467-3515 Page of Client Name Marsh Truck Parts (MA035) Project Number [none] Requested Ana"" Requestkd Turnaround Times' Note : Rush requasts subloti to acceptance by the factlity _ Standard Expedited Due —l..�l $ V— o V �.J• m w •' O A a p N c V Address P.O. Box 427 Project NamdDesc Marsh Truck Parts CityrSTrzQ Siler City , NC 27344 PO r! BHlinp Info - Tel (919) 663-1908 Fax ReporLng Contact Stewe Marsh Sampier(sl Name. Affiliation (Print) Btl Contact Lihu do Hoffman Sampler(s) Signature Site Location 1 Time zone Lab Workorder CB:.O60-5$ Preservallion (See Codes) (Combine as necessary) Item A Sample ID (Fietd Identilicadon) Coa amion Date Coaacuon Time Conip 1 Grab Matrix (see'codos) Total 0 d Containers Sample Comments -Camrd 2p Sw 7 X X w x True rd A D rrt Sw 7 X X X X Truckvard B r� 1- - o Sw 7 X X X X j s I 01 .41— .. —boo,- Total tt of Containers Sample Kit Prepared By Dat rrimo Relinquished By DateoMme ' 'ad By Oaternme , nts/Special Reporting Requirenmras Reiingurshtrd B .- .. - ... - ' Dalafr-cne Received By v Datarrime J Relied By DalefTtms Received By DatelTFne er e's 8 Temps on Receipt _ ' . Condition Receipt -• - Acceptable Unacceptable Matrix: GW-Groundwater - SO -SOB DW-Drinking Water SE -Sediment SWSrutace Water W W-Wastewater. A -Air G-Other (detaO In comments) _ PreservaUon: I -Ice liaiCl.-"NO3 S-MSD4 NO-Hal7H 043MCr (datat In commuAts) Note: All sampim submdted to ENCO Labs are in accordance with tote tents and condltlons lisled on the teverso d "s form, urdess prior written agreements exist Sample Preservation Verification ENCO Cary ®rl• . :._ Work Order: ,CB06058 Project: Marsh Truck Parts Client: Marsh Truck Parts (MA035) Project #: (none) Logged In: 27-Oct-18 10:15 Logged By: John C King Preservation Check Performed By: DatelTime: /�%7�/S" //•Y1C� CB06058-01 Copt Type : - Pres (pH) Requirement pH Checke ! ' In Control_ pFi Adjusted = Date�me �Adiusted '. Reagent UsedlComments = B 1 LA+H2SO4 <2 ! N / NA Y 16 1 NA C 1 LA+H2SO4 <2 I N! NA Y 1�11 P! NA D 250mLP+HNO3 <2 I N! NA Y I ! NA CB06058-02 Cora Type '• ' Pres pH) ;Requirement . pH ecke 1 In Control PH AdJusted Date�me ". Adjusted „rt� Reagent Used1. /Comments B 1 LA+H2SO4 <2 S(�r J N! NA Y 1 1 NA C 1LA+H2SO4 12 I N I NA Y! jl NA D 250mLP+HNO3 <2 / N I NA Y I I& I NA CB0605B-03 Copt . - Type ; EL :. Pres (pH) . - Reqquiremenl . pH Checked 1 , In Contr61 e t Dat ime- - pH Adjusted f .: a Adjusted.. - ..... , , , Reagent UsedlComments B 1 LA+H2SO4 <2 l N I NA Y I 1 NA C 1 LA+H2SO4 <2 I N I NA Y! 1 NA D 250ntt_P+HNO3 <2 Y I N I NA I Y I I NA Rea ent Name ID 1 2 pH Strip ID: Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:IPLMNT1Printlwko_PreservationCheck.rpt Page 1 Mid Atlantic Engineering & Environmental Solutions June 19, 2018 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE,COM NCDEQ/DWR RECEIVED Attention- Central Files JUL 0 3 2018 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ultil�TF"��-WR SECTdGT;C, S N Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — TRUCK YARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on May 17, 2018 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values, with the exception of ethylene glycol. Based on these results, a Tier One Response has been implemented at the facility and the results documented in the facility's Stormwater Pollution Prevention Plan (SPPP). If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 FACILITY NAME Marsh Auto Parts, Inc. - Truckyard_ PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 COUNTY Chatham PHONE NO. (919) 663-2908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH {Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 5/17/18 1.25 7.1 <2.5 <2.70 330 <0.00310 NA Outfall B 5/17/18 1.25 7.2 3.9 <2.70 <4.7 <0.00310 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the PH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 25ee General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, lost revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." '5t 4 � C— AAAV— Name (Print name) Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carol ina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submittipg false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permiaee or Designee) (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 4 nes, p ENCO Laborato * Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 2751.1 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 31, 2018 Marsh Truck Parts (MA035) Attn: Steve Marsh P.Q. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): CB06059 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, May 17, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 �co www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CB060S9-01 Sampled: 05/17/18 09.00 Received: 05/17/18 11:25 Parameter EPA 1664E Preparation EPA 1664E Hold DatelTime(s) 06/14/18 Pma Date/Time(s) 05/24/18 11:07 Analysis Date/Time(s) 05/25/18 15:50 EPA 6014D EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 10:25 EPA 8015C NA 05/31/18 05/30/18 04:39 05/30/18 07:36 SM 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 05/23/18 14:05 Client 10: Truckyard A Lab ID: C606059-02 Sampled: 05/17/18 09:30 Received: 05/17/18 11:25 Parameter EPA 1664E Preoaration EPA 1664B Hold DateLTimeW 06/14/18 Pren Date/Time(s) 05/24/18 11:07 Analysis Date/Time(s) 05/25/18 15750 EPA 6010D EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 f0:27 EPA 8015C NA 05/31/18 05/30/18 04:39 05/30/18 07:55 SM 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 05/23/18 14:05 Client ID: Truckyard B Lab ID: CB06059-03 Sampled: 05/17/18 09:40 Received: 05/17/18 11:25 Parameter Preparation Hold Date/Tune( Prep Date/Time(s) Analysis DateMme(s) EPA 1664E EPA 1664E 06/14/18 05/24/18 11707 05/25/18 15:50 EPA 6010D EPA 3005A 11/13/18 05/24/18 08:54 05/29/18 10:30 EPA 8015C NA 05/31/18 05/30/18 04:39 05/30/18 08:15 5M 2540D-1997 NO PREP 05/24/18 05/23/18 14:05 05/23/18 14:05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 rrrlr Om rlirr 6: www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: C506059-01 AnalM Lead - Total Results flim 0.00606 ] mu E" 0.00310 a.UIUU Units Method notes mg/L EPA 601UD Client ID: Truckyard A Lab ID: C606059-02 Analyt€ Ethylene Glycol Results Flis 330 EML m 4.7 5.0 Units Method Notes mg/L EPA 8015C Client ID: Truckyard B Lab ID: CB06059-03 Analyj Total Suspended Solids Elm 3.9 MP6 E" 2.5 2.5 Units Method dsi8s mg/L SM 2546D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 3 of 9 0 Fom m Nqco www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:CB06059-01 Received: 05/17/18 11:25 Matrix: Surface Water Sampled: 05/17/18 09:00 Work Order: CB06059 Project: Marsh Truck Parts Sampled By: CLIENT (Metals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO Cirry ceMfed analyte (NC 5911 Analyte [CAS Numbers Results ELAg S[Bi,U PIE tML PQL Batch Method Analyzed By Notes Lead[7439-92-1)^ 0.00606 J mg/L 1 0.00310 0,0100 BE24015 EPA6010D 05/29/1810:25 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte (NC S9l] Analyte IQW Numberl Results Elaa Units DE I+I.P.L FQL Batch Method Analyzed BIt Notes Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 8E23005 SM 2540D-1997 05/23/18 14:05 OMR Non -Halogenated Semivolatile Organics by GC Anafyte rCA5 Numberl Result fig Units PIE MU ply Batch Method Analyzed By Note Ethylene Glycol[107-21-1] 4.7 U mg/L 1 4.7 5.0 8E30005 EPA 8015C 05/30/18 07:36 JJB Sumnnates p)f Spikevl 96Rec %RecLimfCs match Negh Age Iffy Notes 1,3-Buiylene Glycol 180 1 200 9296 50-150 8E30005 EPA 80JSC 05130118 07:35 JIB Classical Chemistry Parameters ^ - ENCa.lackspnvrlle certfed arralyte (NC 4421 AnatM rCAS Numberl Results Flag unibi PE MU EQL Batch Method Analyzed @y Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 8E24005 EPA 1664E 05/25/18 15:50 SMA Description: Truckyard A Lab Sample ID:CB06059-02 Received: 05/17/18 11:25 Matrix: Surface Water Sampled: 05/17/18 09:30 Work Order: CB06059 Project: Marsh Truck Parts Sampled By: CLIENT iMetals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENC17 Cry tertifit+d e-6 to (NC S91 J Analyte KAS_Numberl Results Flag Vab Df bp,[, PS21r Batch Method Analyzed gy Notes Lead [7439-92.1]^ 0.00310 U mg/L 1 0.00310 0.0100 8E24015 EPA 6010D 05/29/18 10:27 JDH Classical Chemistry Parameters ^ - ENCO CSry certified a-4te (NC 5911 Analyte [CAS Numbed Results E[Og MA& DE MIX E9.L Batch Method Analyzed fix Notes Total Suspended Solids^ 2.5 U mg/t 1 2.5 2.5 BE23005 SM 25QD-1997 05/23/18 14:05 OMR Non -Halogenated Semivolatile Organics by GC Analyte rCA5 Number] Result;t fig Yalu 2E MU E" Batch Method Analyzed $y Notes Ethylene Glycol [107-21-11 330 mg/L 1 4.7 5.0 8E30005 EPA 8015C 05/30/18 07:55 JIB Surrogates 6ezr116f QE Spikevl 5Ret °%Recllmlts fid= Meth e9a&& Notes 1,3-outylene Glycol 200 1 200 9846 50-150 8E30005 EPA 8015C 05130118 07.55 JJB Classical Chemistry Parameters ^ - ENCO JJC*WnH11e CeRrfied analyte (NC 442J ABalrte, rCAS Numberl Results E)ag mom RE MU F2L Batch ftthoo Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/t 1 2.70 5.00 8E24005 EPA 1664E 05/25/18 15:50 SMA Material^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 CeVCO www.encolabs-cam ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CB06059-03 Received: 05/17/18 11:25 Matrix: Surface Water Sampled:05/17/18 09:40 Work Order: CB06059 Project: Marsh Truck Parts Sampled By:CLIENT IMetals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENO Cary cerbfied analyze (NC 5911 Analrte rCAS Numberl Results Fin Units 2E MU p" Batch Method Aid BY Noteg Lead [7439-92-1]^ 0.00310 U mg/L 1 0.00310 0.0100 8E24015 EPA 6010D 05/29/18 10:30 ]DH Classical Chemistry Parameters ^ - ENCO Cary certified analyze (NC S91 J Analvte ICAS_Numberl Re5ults Flag lfn& 2E MU EU ]3atch Method Analyzed $Y Notes Total Suspended Solids^ 3.9 mg/L 1 2.5 2.5 8E23005 SM 254OD-1997 05/23/18 14:05 OMR Non -Halogenated Semivolatile Organics by GC Analyte rCAS Numberl Results flag Units fE M2L M 11tsh Method Analyzed B1 Notes Ethylene Glycol(107-21-1] 43 U mg/L 1 4.7 5.0 SE30005 EPA 8015C 05/30/18 08:15 JIB Surrogates B 2E Spike L vl % Rec % Rec UmiCr Ba Neth Ana fiy Notes 1,3-Butylene Glywl 180 1 200 92 % 50-150 BE30005 EPA 8015C 05130118 M.15 J78 Classical Chemistry Parameters ^ - ENCO Jadmnvilk, terrified analyze INC 442) Analyte rCAS Numberl Results EUg Units 2E M24 E" liD= Method Analyzed B1 !Votes Oil & Grease (HEM-SGT) Non -Polar 2.70 u mg/L 1 2.70 5.00 SE24005 EPA 1664B 05/25/18 15:50 SMA Materia I^ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 EJVC� www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 8E24O15 - EPA .3OO5A Blank (SE24015-8LK3) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 09:51 Spike Source %REC RPD AnaMe Result Flag P" units Level Result %REC Limits RPD limit Notes Lead 0,00310 U 0.0100 mg/L LCS (8E24015-BSI) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 09:57 Spike Source o/aREC RPD Anal vte Result Flag P91 Units Level Re5ul %REC Limits . RPD Limit Notes Lead 0.197 0.0100 mg/L 0.200 99 80-120 Matrix Spike (SE24015-MS1) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:01 Source: C506833-01 Spike Source %REC RPD AnaiYte Result Flag P- L units Level Result %REC limits RPD Limit Notes Lead 0.190 0.0100 mg/L 0.200 0,00310 U 95 75-125 Matrix Spike Dup (BE24015-MSDS) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:04 Source: C006833-01 Spike Source %REC RPD -Analyte Result Mau POL units Level Resin %REC Limits RPD Limit Notes Lead 0.193 0.0100 mg/L 0.200 0.003i0 U 97 75-125 1 20 Post Spike (BE24015-PSI) Prepared: 05/24/2018 08:54 Analyzed: 05/29/2018 10:06 Source:CB06833-01 Spike Source %REC RPD Analvte Result flag P_QL units Level Result %REC Limits RPD Limit Notes Lead 0.199 0.0100 mg/L 0.200-0.00287 100 80-120 Classical Chemistry Parameters - Quality Control Batch SE23005 - NO PREP Blank (SE23005-BLKI) Prepared & Analyzed: 05/23/2018 14:05 Spike Source %REC RPD AnaI)d Result Flag M Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (BE23005-BS1) Prepared & Analyzed: 05/23/2018 14:05 Spike Source %REC RPD Anal]de Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 101 80-120 Duplicate (8E23005-DUPl) Prepared & Analyzed: 05/23/2018 14:05 Source: C605042-01 Spike Source %REC RPD -AnaMe Result Flag POL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 290 50 mg/L 310 6 20 Duplicate (8E23005-DUP2) Prepared & Analyzed: 05/23/2018 14:05 Source: CB06066-03 Spike Source %REC RPD Anelyt Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 880 100 mg/L 870 0.9 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received try the Laboratory, and may only be reproduced'in full. Page 6 of 9 CeJVCO www.encolabs.com QUALITY CONTROL DATA Non -Halogenated 5emivoiatile Organics by GC - Quality Control Batch SE3O005 - NA Blank (SE30005-BLK3) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 06:36 Spike Source %REC RPD Anal vte Res dt Flag P9L U�itS Level Result 016REC Limits RPD LIMB Notes Ethylene Glycol 4.7 U 5.0 mg/L 1,3-8utylene Glycol 200 m9/1 200 101 50-150 LCS (BE30005-BS1) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 06:55 Spike Source 0/aREC RPD Allalyte Restilt E1a9 I'4L tl— j Level Resul %REC Limlb RPD 1,LIn{t Notes Ethylene Glycol 200 5.0 mg/L 200 101 70-130 13-8uty4ene Glycol 180 m9/L 200 92 50-150 LCS Dup (8E30005-BSDi) Prepared: 05/30/2018 04:39 Analyzed: 05/30/2018 07:18 Spike Source %REC RPD Anal lde Result Flag P_QL 1811U Level Resul %REC Limits RPD 1I0111 Notes Ethylene Glycol 200 5.0 mg/L 200 100 70-130 0.2 25 1,3.8utylene GY-1 160 mg/L 200 78 50-150 Classical Chemistry Parameters - Quality Control Batch 8E24OO5 - EPA 1664E Blank (SE24005-BLKi) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2016 15:42 Spike Source 0/aREC RPD Anal Result Flas M tlnit5 Level Result %REC WMI15 RPD Litnit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (8E24005-BSI) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Spike Source %REC RPD Anal lfte Re,Sul Flag PQL U.11M Level R03ul %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 78.0 5.00 mg/L 80.0 98 64-132 LCS Dup (SE24005-BSD1) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Spike Source %REC RPD AnalAe Result Flag P91, Unfts Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 75.0 5.00 mg/L 80.0 94 64-132 4 34 Matrix Spike (SE24005-MSi) Prepared: 05/24/2018 11:07 Analyzed: 05/24/2018 15:42 Source: B002283-01 Spike Source a/oREC RPD Anallrte Result Flag POL units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 74.7 5.00 mg/L 80.0 2.70 U 93 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 0EmN' www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 � 10775 Central Port Dr. eln:lw Drtanrlo, FL 32824 (407)826.5314 Pax (407) 850-6945 4810 Executive Park Court. Suite 111 Jackson iDo, FL 32216-6069 (9D4) 298-3007 Fax (904) 296-6210 102-A Woodwinds Industrial Ct Cary, NC 27511 (919) 467-3090 Fax (9t9) 467-3515 Page of Ci Name Marsh Truck Parts (MA036) Project Number [none] Requested Analyses Requested Turnaround Times Note : Rush requests subject to amuplance by ere facility Standard Expedited Due c� r n M I {D V- v N 2 u� 0) Address P. 4. Box 427 Praject Nare/Desc Marsh Truck Parts Glty/STfzip Siler City , NC 27344 Pot / Billing Into TO (919) 663-1806 Fax Reporting Contact Steve Marsh Sampkn(s) Name, Atliflation (Print) BiIG Contact Zhuck Hoffman SamDler(s) signature Site Location I Tare zone Lab Workorder Preservation it; Codr>y} (Camtrrte as newssary) ltem a Sample ID (Field Ideniilication) Collection Date CcAedtion Time Comp t Grab Matrix (see codes) Total Y of Containers - Sample Comments Cwyard ' �i x- /A'J SW 7 X X X X True and A -!'7�l 3d SW 7 X X X X True and 13 SW. 7 X X X X Aff <--Total # of Containers pia Kit PreDared 6y VIO2� D elrene Rekngrrah By _ Relinq Dat&Tiirne Dele/Time Race 0y E v� w� Received By Dater me 5 -kI- 2 DabwTkne , nWSpecW Reporting Requirements Rofpmquls W By Data/Time RDceivod By DatEdTime Cooler Mbt�Te^�mps�apt CondlUart U Receiq C -, V AIceptable Unacceptable Matrix: GIN -Groundwater SO•Soil DW-Drinking Water SE•Setivnem SW$udacs Water WW Wastewater A-Afr Other (datafl in comments) Preservation: 14ce H-HCI H-HNO3 S•H2SO4 NO-NaOH O-Othec (detail in comments] Note: AD samples submitted to ENCO Labs are in accordance with the terms and oortd bons listed On the reverse of this form, unless pear written agreements exist Sample Preservation Verification ENCO Cary .' �. Work Order: CB06059 Project: Marsh Truck Parts Client: Marsh Truck Parts (MA035) Project At: [none] Logged In: 17-May-18 14:27 Logged By: John C King Preservation Check Performed By: Te DatelTime: C B06059-01 Cont «< Type Pres (pH) . Requirement pH Checked ! Ih Control. P " DatelTime H Adtusted Adjusted.'. Reagent UsedlComments B 250mLA+H2SO4 <2 Y I N/ Y I N/ A C 250mLA+H2SO4 <2 Y I N I Atd Y I N I D 250mLP+HNO3 <2 JY / N I NA Y lU 1 NA CB06059-02 Cont r Type ,,: Pres (PH) s ttequirernent., P . hecke 1 In Control at , amep� pH Adjusted �� Adjusted ,�° x r r� Reagent Used/Comments� �� 5 w ?, B 250mLA+H2SO4 <2 Y I N/ A Y I N I A C 250mLA+H28O4 <2 Y/ N/ 6 1 Y I N/ A D 250mLP+HNO3 <2 Y / N / NA I Y 1 IQ / NA CB06059-03 Cont ,. Type Pres,(P ) , Requirement pHCheck :1, In. Control _ pH Adjusted Date ime Adjusted . . aF r Reagent Used/Comments` " s_ 8 250mLA+H2SO4 <2 Y I N I A' Y I N IIA ` C 250mLA+H2SO4 <2 Y I N! / Y 1 N 1 I7 250mLP+HNO3 <2 QY l N ! NA I Y / 1 NA Rea ent Name ID Reacient Name ID Reagent Name ID 1 3 5 2 4 6 pH Strip ID: 0170Fr2-O C:IELMNT1Printlwko_PreservationCheck.rpt Page 1 1•s s '• 409 Rogers Vic-v Cours Nod Atlantic RatefgNC210 office 91919.350.99 lB Engineering & Environmental Solutions facsimile 919.250.9950 MAAONLINE.COM April 26, 2017 RECENEU MAY 0 4 2017 NCDEQIDWR CENTRAL FILES Attention: Central Files '-)WR SECTION 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — TRUCK YARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on April 6, 2017 and analyzed for total suspended solids (TSS), pH, oil and grease, ethylene glycol and total recoverable lead. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values, with the exception of oil and grease at Outfall A. Based on the results of this sampling event, a Tier One Response has been implemented at the facility. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPEWENCEQ CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 FACILITY NAME Marsh Auto Parts, Inc. - Truckyard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 COUNTY Chatham PHONE NO. (919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 $,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 4/6/2017 1.50 7.1 6.8 20.2 <4.0 <0.00310 NA Outfall B 4/6/2017 1.50 6.8 2.8 <2.70 <4.0 <0.00310 NA Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. ISee If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) j Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." {Signature of Permittee or De (Date) Form SWU-2S1, lost revised October25, 2012 Page 2 of 2 coo I E. N�CO Laborato"'es Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, April 20, 2017 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parks ENCO Workorder(s): CA02359 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, April 6, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page L of 9 E�Cmo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CA02359-01 Sampled: 04/06/17 08:00 Received: 04/06/17 10:00 Parameter Hold Date/Time(s1 Prelz Dala/Timefsl AnAysis Date(Time(s) EPA 1664A 05/04/17 04/07/17 16:35 04/11/17 14:52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:55 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 09:53 SM 254OD-1997 04/13/17 04/11/17 12:45 04/11/17 12:45 Client ID: Truckyard A Lab ID: CA02359-02 Sampled: 04/06/17 08:15 Received: 04/06/17 10:00 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664A 05/04/17 04/07/17 16:35 04/11/17 14:52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:43 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 10:12 SM 254OD-1997 04/13/12 04/11/17 12:45 04/11/17 12:45 Client ID: Truckyard B Lab ID: CA02359-03 Sampled: 04/06/17 08:30 Received: 04/06/17 10:00 Parameter Hold Date/Time(s) Prep_DatelMme(sl AnalysisDatelTime(s) EPA 1664A 05/04/17 D4107117 16:35 04/11/17 14:52 EPA 6010D 10/03/17 04/07/17 08:44 04/11/17 11:58 EPA 8015C 04/20/17 04/10/17 08:40 04/10/17 10:31 SM 254OD-1997 04/13/17 04/11/17 12:45 04/11/17 12:45 FINAL This report relates only to the sample as received by the laboratory, and may onty be reproduced in full. Page 2 of 9 S NIS,: cm:e www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryard Lab ID: CA02359-01 Anal vte Results Elm MpJ, P_.QL Units Method Notes Lead - Total 0.00314 3 0.00310 0.0100 mg/L EPA 6010D Oil & Grease (HEM-SGT) Non -Polar Material 8.82 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 6.1 2.5 2.5 mg/L SM 254OD-1997 Client ID: Truckyard A Lab ID: CA02359-02 Anal 7dg liesults Elm m PQL Units Notes Oil & Grease (HEM-SGT) Non -Polar Material 20.2 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 6.8 2.5 2.5 mg/L SM 2540D-1997 Client ID: Truckyard 8 Lab ID: CA02359-03 Anal Results Elan l DL EQk Units Method Notes Total Suspended Solids 2.8 2.5 2.5 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 (�J�Cmo www.encolabs.corn ANALYTICAL RESULTS Description: Caryard Lab Sample ID:CA02359-01 Received: 04/06/17 W:00 Matrix: Surface Water Sampled:04/06/17 08:00 Work Order: CA02359 Project: Marsh Truck Parts Sampled BV:Client (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certifier!.? —ode (NC 5911 Analyte fCAS Number! Results Flay Units PE IU EQL Batch Method Analyzed by Notes Lead [7439-92-1]^ 0.00314 J mg/L 1 0.00310 0.0100 7007010 EPA 6010D 04/11/17 11:55 JMV Classical Chemistry, Parameters ^ - ENCO Cary certified amw (NC 5911 Analyte fCAS Numberl Results E[ag Units P-E MDL P4.6 Batch Method Analyzed By Notes Total Suspended Solids^ 6,1 mg/L 1 2.5 2.5 7D11003 SM 254OD-1997 04/11/17 12:45 OMR Non -Halogenated Semivolatile Organics by GC Analyte [CAS Numberl Results Flag Units pF MDL pQL Batch Method Analyzed BY Notes Ethylene Glycol[107-21-1] 4.0 U mg/L 1 4.0 10 7D10008 EPA 8015C 04/10/17 09:S3 JIB Surrogates Results -Of && L % Aec % Rec Urn Batch Method AnaBy Notes 1,3-8utylene Glycol 180 1 700 92 % 50.150 7DI0008 EPA 8015C 0411011709:53 JJB Classical Chemistry Parameters Analyle [CAS Numberl Oil & Grease (HEM-SGT) Non -Polar ResUl E&q Units P@ ma EQL match Method Analyz am Note 8.82 mg/L 1 2.70 5.00 7DO7014 EPA 1664A 04/11/17 14:52 SMA Description: Truckyard A Lab Sample ID:CA02359-02 Received: 04/06/17.10:00 Matrix: Surface Water Sampled:04/06/17 08:15 Work Order: CA02359 Project: Marsh Truck Parts Sampled BV:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO dory certified a-V-* (NC 5911 Analyte ICAS Number] Results F[ag Viliu PIE MDL M Batch MethAnalyzed Py Notes Lead [7439-92-1]^ 0.00310 U mg/L 1 0.00310 0,0100 7DO7010 EPA 6010D 04/11/17 11:43 JMV Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte (CAS Numberl Results FI ,g Units PIE MVL E21. Batch Method Analyzed By Notes Total Suspended Solids^ 6.8 mg/L 1 2.5 2.5 7D11003 SM 254OD-1997 04/11/17 12:45 OMR Non -Halogenated Semivolatile Organics by GC Analyte (CAS Numberl Results Flao UWts P-E MpL P-QL Batch Meth¢ Analyzed By Notes Ethylene Glycol [107-21-11 4.0 U mg/L 1 4.0 10 7D10008 EPA 8015C 04/10/17 10:12 JJB Surrogates Results —of Spike 1 v1 % Rec % Rec limits Batch Method Analyzed @y Notes 1,3-8utylene Glycol 170 1 200 81 % 50-150 7DI0008 EPA 6015C 04110117 10:12 JJB Classical Chemistry Parameters analyte [CAS Numberl gesy[tts Flag Units PE MDL EQL Batch Method Analyzed By Note Oil & Grease (HEM-SGT) Non -Polar 20.2 mg/L 1 2.70 5.00 7DO7014 EPA 1664A 04/11/17 14:52 SMA Material FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Ce www.encolabs.com ANALYTICAL RESULTS Description: Truckyard 6 Lab Sample ID:CA02359-03 Received: 04/06/17 10:00 Matrix: Surface Water Sam pled- 04106/17 08:30 Work Order: CA02359 Project: Marsh Truck Parts Sampled By: Client IMetals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - ENCO ary cethfied anaVe [NC 5911 Analyte IFCAS Number S nag units PE HU E46 @-th Method Analyzed lax Notes Lead [7439-92-1]A 0.00310 U mg/L 1 0.00310 0,0100 7DO7010 EPA 6010D 04/11/17 11:58 ]MV Classical Chemistry Parameters ^ - ENCO Cary certified analyte (NC 591] Analyte [CAS Numbed Results slag Units PE MPL EP.L Batch Method Analyzed BY Notes Total Suspended Solids^ 2.8 mg/L 1 2.5 2.5 7D11003 SM 2540D-1997 04/11/17 12:45 OMR Non -Halogenated Semivolatile Organics by GC Nuaftrl Ress1lxs f&g Units PE MGL E26 fAtkh Method Analyzed ft Notes Ethylene Glycol[107-21-1] 4.0 U mg/L 1 4.0 10 7D10008 EPA 8015C 04/10/17 10:31 JJB Surrogates Results pF Svike L v1 % Rec % Rec Limits Batch Method A9Y Notes 1,3-8utylene Wlycol 180 1 200 94 % 50-150 7010008 EPA 8015C 0411011710:31 JJB Classical Chemistry Parameters Analyte [CAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results BPS! Sinn;: PF MDL POL Batch Methed Analyzed Py Notes 2.70 U mg/L 1 2.70 5.00 7DO7014 EPA 1664A 04/11/17 14:52 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 of 9 �lVCG) www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 7D07010 - EPA 3005A Blank (71307010-BLKl) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 10:24 Spike Source %REC RPD _Analyte R-esult Flag POL Units Level Result %REC Limits RPD Limit Notes Lead 0.00310 U 0.0100 mg/L LCS (71307010-13SI) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:38 Spike Source %REC RPD Anal a Rmvk flag P0L Units Level Result %REC Limits RPD M1119 Notes Lead 0,202 0,0100 mg/L 0.200 101 80-120 Matrix Spike (7D07010-MS1) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:46 Source: CA02359-02 Spike Source %REC RPD Analyte Result Flag ROL Units Level Res %REC Limits RPD MUK Notes Lead 0.199 0.0100 mg/L 0.200 0.00310 U 99 75-125 Matrix Spike Dup (7D07010-MSD1) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11!48 Source: CA02359-02 Spike Source %REC RPD Analyte Result Flag P-OL Units Level Result %REC Limi RPD Limit Notes Lead 0.201 0.0100 mg/L 0.200 0.00310 U 101 75.125 1 20 Post Spike (71307030-PS1) Prepared: 04/07/2017 08:44 Analyzed: 04/11/2017 11:50 Source: CA02359-02 Spike Source %REC RPD Analyte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Lead 0.195 0.0100 mg/L 0.200 0.00145 97 80-120 Classical Chemistry Parameters - Quality Control Batch 7D21003 - NO PREP Blank (7D11003-BLKi) Prepared & Analyzed: 04/11/2017 12:45 Spike Source %REC RPD Anayle Rest!$ Flag P4L Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7D11003-8S1) Prepared & Analyzed: 04/11/2017 12:45 Spike Source %REC RPD -Analyte Result Flag POL Units Level Resu 0/6REC Limits RPD, Limit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (7D11003-DUP1) Prepared & Analyzed: 04/11/2017 12:45 Source: CA01319-01 Spike Source %REC RPD Analyte Result Flag P-0L Units Level Result %REC Limim RPD Iimi MOWS Total Suspended Solids 240 50 mg/L 240 2 20 Duplicate (7D11003-DUP2) Prepared & Analyzed: 04/11/2017 12:45 Source: CA03276-01 Spike Source %REC RPD Anahrte Result Flag N L units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2200 250 mg/L 1700 23 20 QM-12 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 a NkS www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 7D10008 - NA Blank (71D10008-BLKI) Prepared: 04/10/2017 08:40 Analyzed: 04/10/2017 08:56 Spike Source %REC RPD .Analyte Result Flag 1110L Una Level Result 0/aREC Limits RPD Limit Notes Ethylene Glycol 4.0 U 10 mg/L 1,3-8utylene Glycol 180 m9/t 190 91 50-150 LCS (7D10008-BS1) Prepared: 04/10/2017 08:40 Analyzed: 04/10/2017 09:15 Spike Source %REC RPD Artalvte Result Flaq PQL Una Level Result %REC Limits RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 101 70-130 1,3-8utylene Glycol 170 m91L 200 84 50-150 LCS Dup (7D10008-BSDi) Prepared: 04/10/2017 08:40 Analyzed: 04/10/2017 09:34 Spike Source a/aREC RPD Analvte Result Elag PQL Units Level Result %REC Limits RPD LL01it Notes Ethylene Glycol 210 10 mg/L 200 103 70-130 2 25 1, 3-80tylene Glycol 170 m9/L 200 85 50-150 Classical Chemistry Parameters - Quality Control Batch 7DO7014 - EPA 16648 Blank (7D07014-BLK1) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Spike Source %REC RPD .Analyte Result Flag NIL Units Level Result %REC Limi RPD Limit Notes. Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (7D07014-BSI) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 IC52 Spike Source °/aREC RPD Anal vte Result Flag P41 Units Level Result a/oREC LlmlU RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 69.3 5.00 mg/L 73.0 95 64-132 LCS Dup (7D07014-BSD1) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Spike Source %REC RPD .Analvte Result Flag PQL Units Level Resu %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 79.7 5.00 mg/L 73.8 108 64-132 14 34 Matrix Spike (7D07014-MSI) Prepared: 04/07/2017 16:35 Analyzed: 04/11/2017 14:52 Source: BA01428-01 Spike Source %REC RPD Analyte Result Flag POL Units Level Resk a/oREC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 57.8 5.00 mg/L 74.6 2.70 U 77 6+132 FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. Page 7 of 9 (� �Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank, D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 EPIVIRONMENTALtO.NSERVATIONLAOCiRATORIES -CHAIWOF-,CUSTODYr RECORD- www.ancolabt,com rvl,wr,oam-�s wqrojow rjj..ii p o ^z Wool mil"IMNIA lk i >;�ei:3.rprb'il'li�lsm!li�1,1r -_ :���: 8L:!S:Irl6ylr�'IFiw�jN - rI Nial 'Al kul;ij= nuwlmxt U i;6wj Lawatq or, fflWrt I M w"'411 lun %MTFOFI I ml [41 1M.Cm "Itlip. riligm1wimlidoi .Sample Preservation Verification ENCo Cary War` Qides; CA02M.9 K1 rch Tnjrk Parts G1enL Wr h TruC:i Per#3 (MA035) Pra ct r; jnorcj. Lorged:lr: OS-Ar717 17 27 Legged Df: P,ac�elAnn `Y nis'. C�40�58 ;i}1 �+`� 'T4'G� PestifT iri �ii n Lurr%r,71, 14 r A'dIiFstcd -- !i 1:dlM A'6H2 iC13 -zr Y. J N ! Nfl y ! N. l 0 2f41ml.PrHh+M 47 Y„) M I NA I -Y r��� NA CAOb59-02 CaQfi: IIaE iE�CtJfehi�_ 1l1:IQl1lT ICE ' L�3it!�y f►«d l� i! L#hr?Ci1[7z11R1'�i}'a — la G.dVr{�'T.l'L-474130-.Z - iti Ni/f� 111i 1igA c 250fr LA++i2.SO4 — Y.1 N i ivA Y I N'r a 250xrLPEN03 %2 - y'. !, / PkJI X !'J PW Cori; lypcc ,) . p"' n ��t�r� _Infecnir :0} jug#.ed �" � 'itrs#ed �?cagcCt'4t �cr�tirrititt� 8 Mr, LA-;-H2SO4 2 Y 1 N J f4Fj M I N I C- 250irLA+1 <2 Y! N& Y t N f�HAE D7 �!,,n! I.P-tHNOi r? Y� W 11Vt.A Y f bI MA Re*iani Name 1 D 1 2 1=164e t i= fTie It] r3 5 -ri:G are=. Name;- ID. 5 CERTIFICATE OF COVERAGE NO. NCGl00014 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT RECEIVE® JAN 0 6 2017 FACILITY NAME Marsh Auto Parts, Inc. - Truckyard CENTRAI III r-S PERSON COLLECTING SAMPLE(S) Stephen Marsh DWR SECTION CERTIFIED LABORATORY(S) ENCO,Inc. Lab #591 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 COUNTY Chatham PHONE NO. (919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 OutfaII A 11/29/2016 1.25 6.7 470 <2.70 <4.0 NA NA Outfall B 11/29/2016 1.25 7.2 82 16.8 <4.0 NA NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. ISee If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table Il of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics.(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution) Prevention Plan." Name (Print name) Title (Print title) L. r4'J' rz-- 1 Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pdrmittee or Designee) �;)L t b (Date) Form SWU-251, lost revised October 25, 2012 Page 2 of 2 4 `ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, December 9, 2016 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Sox 427 Siler City, NC 27344 1 V E D JAN 0 6 2017 RE: Laboratory Results for CENTRAL FILES Project Number: [none], Project Name/D��cRM*sh-T yck Parts ENCO Workorder(s): CZ12424 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, November 30, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may oMy be reproduced in full. Page 1 of 9 0 Foon., Nik' Cm (D www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: CZ12424-01 Sampled: 11/29/16 15:00 Received: 11/30/16 13:00 Parameter Prep Date/Time(s) Analysis DatelTimefs] EPA 1664A 12/27/16 12/07/16 11:31 12/08/16 1T.51 EPA 8015C 12/13116 12/06/16 05:12 12/06/16 09:25 SM 2540D-1997 12/06J16 12/01/16 13:30 12/01/16 1330 ClientIM Truckyard A Lab ID: CZ12424-02 Sampled: 11/29/16 16:15 Received: 11/30/16 13:00 Parameter Hold Date/Time(s) Prep QatelTimefsl analysis DatelTimefs] EPA 1664A 12/27/16 12/07/16 11:31 12/08/16 17c51 EPA 8015C 12/13116 12/06/16 05:12 12/06/16 09:41 SM 2540D-1997 12/06116 12/01/16 13:30 12/01/16 13:30 Client ID: Truckyard B Lab ID: CZ12424-03 Sampled: 11/29/16 16:30 Received: 11/30/16 13:00 Parameter Hold DatelTime(s] Prep Date/Time(s) Analysis DatelTimefs) EPA 1664A 12/27,116 12/07/16 11:31 12/08/16 17:51 EPA 8015C 12/13,f16 12/06/16 05:12 12/06/16 10:03 SM 2540D-1991 12/06/16 12/01/16 13:30 12/01/16 13:30 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced 0 full. Page 2 of 9 (E�Cmo www.encolabs.com SAMPLE DETEMON SUMMARY Client ID: Caryard Lab ID: CZ12424-01 Analyt Resufts Elm MQ6 P4.6 yDit i Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.1 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 42 5.0 5.0 mg/L SM 254OD-1997 Client 1D: Truckyard A Lab ID: CZ12424-02 Analyte Results Elan MDL P91 !hiss Method Notes Total Suspended Solids 470 33 33 mglL SM 254OD-1997 Client ID: Truckyard B Lab ID: CZ12424-03 Anal vte Results Flag mu E" Units Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 16.8 2.70 5.00 mg/L EPA 1664A Total Suspended Solids 82 5.0 5.0 mg/L SM 2540D-1997 FINAL This repot relates only to the sample as rece"sved by the laboratory, and may only be reproduced in full. Page 3 of 9 (J�09 www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample I D: CZ1 2424-01 Received: 11/30/16 13:00 Matrix: Surface Water Sampled:11129/16 15:00 Work Order: CZ12424 Project: Marsh Truck Parts Sampled By: Client (Classical Chemistry Parameters ' ^ - ENCO Cary certified anayte (NC 591] Results Flag UnAl PE '9DL P44 BCC Method Analyz @Y Note Total Suspended Solids^ 42 mg/L 2 5.0 5.0 6LO1002 SM 254OD-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile Organics by GC Analyte [CAS Numbed Results Elks Units PIE MPI M Batch Method nA alyxed @y Notes Ethylene Glycol[107-21-1] 4.0 it mg/L 1 4.0 10 6LO6001 EPA B015C 12/06/16 09:25 JIB Sumvaates Results pf 5pikeLy/ 0/aRec %Retlimiks Batch Method Analyzed fly Notes 1,3-8utylene Glycol 170 1 200 65 % 50-150 6406001 EPA 8015C 12106116 09:25 JIB Classical Chemistry Parameters Analvte IQ$ Number] Oil & Grease (HEM-SGT) Non -Polar Results Elm Units !DE M E" Batch Method Analyzed By Notes 18.1 mg/L 1 2.70 5.00 6LO7004 EPA 1664A 12/06/16 17:51 SMA Description: Truckyard A Lab Sample iD:CZ12424-02 Received: 11/30/16 13:00 Matrix: Surface Water Sampled:11/29/16 16:15 Work Order: CZ12424 Project: Marsh Truck Parts Sampled By: Client Classical Chemistry Parameters ' ^ - ENCO Cary terrified anaWe (NC 591] Analyte [CAS Numberl Results f1Ag Units pf MOIL pgL Batch Method Analyzed My Notes Total Suspended Solids- 470 mg/L 13.3 33 33 6LO1002 SM 2540D-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile Organics by GC Analyte [CAS Numberl Results Etas Units PIE plpL POL Batch Mel do Anal ysg¢ Py Notes Ethylene Glycol[107-21-1] 4.0 u mg/L 1 4.0 10 6LO6001 EPA 8015C 12/06/16 09:44 ]]B Surrogates Results —Of ilk %n Ret °/a Rec Limits Batch Meth Ana lyzed By Notes 43-Hutylene Glycol 160 1 200 82 % 50-150 6LO6001 EPA 8015C 12/05/16OR44 Jig Classical Chemistry Parameters Analyte [CAS Numberl Results flag Units 12f MDL pQL batch Method Analyzed gy Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 lJ mg/L 1 2.70 5.00 6LO7004 EPA 1664A 12/08/16 17:51 SMA FINAL This report relates only to the sample as received by the laboratory, and may only tie reproduced in full. Page 4 of 9 (� �Cmt www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:CZ12424-03 Received: 11/30/16 I Matrix: Surface Water Sampled:11/29/16 16:30 Work Order: CZ12424 Project: Marsh Truck Parts Sampled By: Client (Classical Chemistry Parameters ^ - ENCO Cary mnMed —Ve [NC 5911 alvte [CAS Numberl Results Ep_g Units pf 1a E" Batch Method Analyzed Jay Notes Total Suspended Solids^ 82 mg/L 2 5.0 5.0 6LO1002 SM 2540D-1997 12/01/16 13:30 MMR Non -Halogenated Semivolatile Organics by GC Analvte ICAS Numberl Ethylene Glycol[107-21-1) Results Flag Units RE MPS PQ.4 Batch Method nail z A-Y Notes 4.0 U mg/I. 1 4.0 10 6LO6001 EPA 8015C 12/06/16 10:03 338 Surrogates Results Rf Snike L v! n Rec % Rec Lim 19a Method Analyxeo< By Notes 1,3-8ulylene Glycol 170 1 200 86 % 50-150 6LO6001 EPA 8015C 12106116 10:03 Jig Classical Chemistry Parameters Analvte ICAS Numberl oil & Grease (HEM-SGT) Non -Polar Material Results Flag Units pE MD6 E" Batch Method Analyzed Jay Notes 16.8 mg/L 1 2.70 5.00 6LO7004 EPA 1664A 12/08/16 17:51 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 QEmQB)S www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6L01O0.2 - NO PREP Blank (6L03002-BLKI) Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD .Analvte Result Flag IQ Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (61L01002-BS1) Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD -Anal Sde Result Flag PSLL Units Level Result D/oREC Limits RPD Lmft Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (6L01002-DUP1) Prepared & Analyzed: 12/01/2016 13:30 Source: CZ16873-01 Spike Source D/oREC RPD .Anatyte Result Flan Ni Units Level Result D/oREC Limits RPD Li�!mit Notes Total Suspended Solids 330 100 mg/L 340 4 20 Duplicate (6L01002-DUP2) Prepared & Analyzed: 12/01/2016 13:30 Source: CZ07890-01 Spike Source a/oREC RPD .Analvte Result Flag PO Units Level Result D/oREC Limits RPD Limit Notes Total Suspended Solids fit 25 mg/L 57 8 20 Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 6LO6001 - NA Blank (61.06001-BLI(i) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 07:31 Spike Source D/oREC RPD -Analvte Result Flag PPL Units Level Result D/oREC Limits RPD Limit Notes Ethylene Glycol 4.0 U 10 mg/L 1,3-8utyleno Glycol 190 mg/L 200 95 50-150 LCS (6L06001-BSI) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 07:50 Spike Source D/aREC RPD -Analvte Result Flag PQ Units Level Ltesulk D/oREC Limits RPD Limit Notes Ethylene Glycol 180 10 mg/L 200 92 70-130 1,3-6utylene Glycol 190 mg/L 200 94 50-150 LCS Dup (6L06001-BSD1) Prepared: 12/06/2016 05:12 Analyzed: 12/06/2016 08:09 Spike Source %REC RPD .Ar%Ayte Result Flag IQ Units Level Result D/oREC Limits RPD Limit Notes Ethylene Glycol 180 10 mg/L 200 92 70-130 0.8 25 1,3-Butylene G1yc01 160 mg/L 200 88 50-150 Classical Chemistry Parameters - Quality Control Batch 6L07O04 - EPA 1664E Blank (6L07004-BLK1) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Spike Source a/oREC RPD Anahae Result Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGf) Non -Polar Material 2.70 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 (� �Cmo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5LO7004 - EPA 16645 - Continued LCS (611.07004-111SI) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17;51 Spike Source %REC RPD _An?ilvte Result Flag PQL Units Level Result °/oREC hi!nits RPD Likl]lt Notes - Oil & Grease (HEM-SGT) Non -Polar Material 68.5 5.00 mg/L 78.7 87 64-132 LCS Dup (611-07004-13SD11.) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Spike Source %REC RPD Anal vte Result Flay P_4.L YOU Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 81.2 5.00 mg/L 80.0 102 64-132 17 34 Matrix Spike (6L07004-MSS) Prepared: 12/07/2016 11:31 Analyzed: 12/08/2016 17:51 Source: SZO5272-01 Spike Source %REC RPD .Analvte Result Flag P-4L Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 105 5.00 mg/L 83.3 97.9 9 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 9 (J�Go www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Central Pon Dr. 4810 Exacutivo Park Court, Suiio 111 102-A Woo0eAnds Intlusirial CI. Orlando. FL 32824 JacksonvLle, FL 32216-6069 Cary, NG 27511 (407)826-5314 Fax(407)850.6945 (W.)296-3007 Fax(904)296-6210 (919)467-3U90 Fax(919)467.3515 Page of Client Name Project Number Requested Analyses Requested Turnaround Ti-tirk Pads4kllAaH.) [none) Times pddr@35 Project NameiiAe '. Note :flush rr:rfirests sua(C41 to Q_Rox 427 Marsh Truck Parts acceptance by flte facility Cay)ST2iµ PO P ! Billing Inra Siler C;it' , NC 273,14 U) U, _ Standard Tel Fax 1loportmg Conlrm, (9'1 9) 6 3- 1 903 Sieve Mari;h 0 U ��x} �! W"I Chi � i Expedited Due SamplorW Name. Ati fration (Print) Billing Coruact Chuck Hoffman 0 to Ct L �; Cfl [ fl Samplm(s} Signalurc Site Location f Time Zone Uibf workarder - �...', l� r �, oD C1 t._ �.. t - �•�_�+{§ Preservation (See Codes) (Combine as necessary) Item >r Sampso ID (Fie:d Idontil?cation) Co[Wtion Date WICGian Time Cornµ ! Grab Maim (sae codes) Total 4 of Coniainors Sample Comments _ Nd •i j f Y. �.L4�L �, ��:1 •I rI 'I f' d. I E -'! T•i f..� .s .t .:. t < Totalif o6 Containers e Kit Pteµated 8y D . firm peG lgrisheo Dy DateJrirno Roccivod Sy Date, rune _ Comments pedx al Reputing Requirennt5 Rel" ,ed By Datelrime Roce, By D ter i e t i'�rc= f /� R .nquishetl By Datorrimo R By Daie;Time et Ws & Temps on Raceipl Condition UponReceipt rC_'1.. Acceptable Uni•' Uatrlx ; GWGroundwatar SO -Soil DW-Drinking Water SE -Sediment SWSudace Water WW-Wastewater A -Air O.Oihor(dolaol in comments) Preservation: Wce H-I+CI N4IN03 S412SO4 NO-Na011 0-01trei (delaB in t:ornmenls) Note: All samples submittee to ENCO Labs are in accordance with the terms and conditions listed on the reverse o' this form, lrnle"ss pnor wriunn agreements exist Sample Preservation Verification ENCO Cary Work Order: CZ12424 Project: Marsh Truck Parts Client: Marsh Truck Parts (MA035) Project [none] Logged In: 30-Nov-16 13:22 Logged By: Andrew S Coons CZ1 2424-01 - P � --I i.-,res,(pH)k PH . CheckedI 'Ad" 6te&-'-� �Xaterrimeg.,.� Zea� 'U Co edts6d/i� Requirement 14 o tm'�.: q il Ad B 250mLA+H2SO4 <2 Y N~i NA Y n�) NA 11 C 250ml-A+H2SO4 <2 Y (N-� NA Y 1 NA D 250mLP+HNO3 I <2 ry) N NA Y N NA CZ1 2424-02 Pont, P '(pH).'.- pH Checked 1. ";XDaterrime". -pHlAdj" Adlust&d--'-�,� B 250mLA+H2SO4 <2 Y C) NA Y 1 N NA C 250rnLA+H2SO4 <2 Y &)I NA Y Q4)/ NA FDT25OmLP+HNO3 <2 - Pv N / NA YrNJ NA CZI 2424-03 Cont ,Ty0ea Presjpff�— Y -C —hk q d3te Requirement, ton r6 lus B 250mLA+H2SO4 <2 Y (N-"I NA Y FN)/ NA i I C. 250mLA+H2SO4 <2 Y I(N') NA Y rN � NA 1250mLP+HNO3 <2 Y N I NA Y I IJ NA Reagent Name ID 2 Rea ent Name ID 3 . .... . 41 Reaqent Name ID 5 6 Page 1 of 1 C_."; M*od Atlantic Engineering & Environmental Solutions December 26, 2016 EIV Ee�� NCDEQIDWR Attention: Central Files .BAN 2017 1617 Mail Service Center CFN7'Rk F� Raleigh, North Carolina 27699-1617 DWR SEC7_10N Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — TRUCK YARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919,250.9918 facsimile 919.250.9950 MAAONUNE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfails A and B on November 29, 2016 and analyzed for total suspended solids (TSS), pH, oil and grease and ethylene glycol (please note that the samples were not analyzed in the laboratory for total recoverable lead for the current sampling event). As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values, with the exception of TSS at Outfall A and Oil and Grease at Outfall B. Based on these results, a Tier One Response has been implemented at the facility. Samples will be collected from each outfall during the January -June 2017 monitoring period and analyzed for TSS, pH, oil and grease, ethylene glycol and total recoverable lead. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron J. Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE + 4 -w CMlod Atlantic Engineering & Environmental Solutions June 23, 2016 RECEIVED NCDEQIDWR JUL 08 2U16 Attention: Central Files CNTFtAk. FILES 1617 Mail Service Center OWR SEC110N Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — CAR YARD 211 EAST 11T" STREET SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100015 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 001 on May 5, 2016 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. With the exception of TSS, all parameters were reported below or within their respective benchmark values, as indicated on the attached DMR. Based an the results of the May 2016 sampling event, a Tier One Response has been implemented at the facility. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100015 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 REC-� / V FACILITY NAME Marsh Auto Parts Inc. - Ca and PERSON COLLECTING SAMPLE(S) Stephen Marsh ,Z'fb CERTIFIED LABORATORY(S) ENCO, Inc.�:ab Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Chatham PRONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 �- 9.01 300/50Z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 S/5/2016 1.75 7.2 150 4.551 <4.0 0.03 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122, Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is im plementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ,1"65S 0. ��9iZS�I Name (Print name) Title (Print title) Sign ure Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ure of Permittee or Designee) 6-.367, Date) Form SWU-251, lost revised October 25, 2012 Page 2 of 2 plod Atlantic Engineering & Environmental Solutions June 23, 2016 NCDEQIDWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. — TRUCK YARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919,250.9918 facsimile 919.250.9950 MAAONLINE.COM RECEIVED JUL 0,8 zuia CENTRAL FILES DWR SECTION Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on May 5, 2016 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 FACILITY NAME Marsh Auto Parts, Inc.-Truckyard _ _ COUNTY Chatham PERSON COLLECTING SAMPLE(5) Stephen Marsh PHONE NO. 919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. -Lab #591 Lab #�� j PLEASE REMEMBER TO SIGN ON THE REVERSE �! Part A: Stormwater Benchmarks and Monitoring Results JUL 08 Z016 For sampling periods with no discharge, you must submit this dis 69�n�t'Whfr form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply wrtfi-Ppnit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 5/5/2016 1.75 6.8 68 <2.70 <4.0 0.00756 J NA Outfall8 5/5/2016 1.75 7.1 29 <2.70 <4.0 0.0111 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, lost revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of PeAittee or Designee] [Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT .410111h, CERTIFICATE OF COVERAGE NO. NCG100014 SAMPLES COLLECTED DURING CALENDAR YEAR:2015 FACILITY NAMEMarsh Auto Parts. Inc. - Truckyard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh _ _ _ PHONE NO. (919) 663-1908 CERTIFIED LABORATORY(S) ENCO, Inc. Lab #591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/50z 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 11/19/2015 1.50 6.7 42 <2.7 <4.0 <0.00310 NA Outfall B 11/19/2015 1.50 6.8 36 <2.7 <4.0 <0.00310 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, lost revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT _4w Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." -�+eD � en3 �- , MA ' Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 1--L�-i Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." IN (Signature of Permittee or Designee) -- L 4 -- (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Marsh Auto Parts, Inc. - Truckyard _ COUNTY Chatham F� PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. 919) 663-3.908 CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE �l Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring farm noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 05/01/2015 1.75 6.7 19 <2.60 <8.7 0.00365 J NA Outfall B 05/01/2015 1.75 7.1 26 <3.04 <8.7 0.00483 J NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." C= Name (Print name) Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C_ -- - �)� (Signature of Permittee or Designee) 5 -ZZ-I s (Date) Form 5W U-251, last revised October 25, 2012 Page 2 of 2 Mod Atlantic Engineering & Environmental Solutions May 15, 2015 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: RECEIVED MAY 2 6 2015 CENTRAL FILES DWR SECTION 409 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on May 1, 2015 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, PG Project Geologist Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE ENCOLaboraton'es- Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 14, 2015 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results For Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C414992 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 1, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page I of 9 (F�Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard lab ID: C414992-01 Sampled: 05/01/15 09:30 Received: 05/01/15 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Aoa]ySmS Date/Time(s) EPA 1664A 05/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28j15 05/08/15 12:08 05/11/15 14:29 EPA 8015C 05/15/15 05/12/15 11:10 05/12/15 18:11 SM 2540D-1997 05/08/15 05/05/15 09:09 05/05/15 09:09 Client ID: Truckyard A Lab ID: C414992-02 Sampled: 05/01/15 09:40 Received: 05/01/15 11:05 Paramete Hold PaWThmefs)Prep Date/Timefs) Analysis_Date/Time(s) EPA 1664A 05/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28/15 05/08/15 12:06 05/11/15 14:31 EPA 8015C 05/15/15 05/12/15 11:10 05/12/15 16:28 SM 254OD-1997 05/08/15 05/05/15 09:09 05/05/15 09:09 Client ID: Truckyard B Lab ID: C414992-03 Sampled: 05/01/15 10:15 Received: 05/01/15 11.05 Parameter Hold DateIj'ime(s) Prep Date/Time(s) analysis Date/Timefs) EPA 1664A 05/29/15 05/12/15 10:02 05/13/15 14:22 EPA 6010C 10/28115 05/DB/15 12:08 05/11/15 14:34 EPA 8015C 05/15/15 05/12/15 11:10 05/12/15 18:45 SM 254OD-1997 05/09j15 05/05/15 09:09 05/05/1S 09:09 FINAL This repots relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 (� �Cmo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Caryand Lab ID: C414992-DI AnalResults E109 MDL FQL Units Notes Lead - Total 0.00380 1 0.00310 0.0100 mg/L EPA 6010C Total Suspended Solids 20 3.3 3.3 mgYL SM 25400-1997 I Client ID: Truckyard A Lab ID: C414992-02 Analvte Results Flag MDL EQLL Units Method Notes Lead - Total 0.00365 3 0.00310 0.0100 mg/L EPA 6010C Total Suspended Sohds 19 3.3 3.3 mg/L SM 2540D-1997 Client ID: Truckyard B Lab ID: C414992-03 Anal vte Results Fig MDL M Yalu Method Notes Lead - Total 0.00483 3 0.00310 0.0100 mg/L EPA 6010C Total Suspended Solids 26 5.0 5.0 mg/L SM 2540D-1997 FINAL This report relates ony to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 ��Go www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C414992-01 Received: 05/01/15 11:05 Matrix: Surface Water Project: Marsh Truck Parts Sampled: 05/01/15 09:30 Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods Work Order: C414992 ^ - ENCO Cary certified analyte (NC 5911 Analyte NAS Numberl Results Flag Units PF MDL p46 A=h Method Analyzed By Notes Lead [7439-92-1]^ 0.00380 J mg/L 1 0.00310 0.0100 5EO8014 EPA 6010C 05/11/15 14:29 JDH Classical Chemistry Parameters ^ - ENCO Cary certified .7-w PVC 591) Analyte KAS Numberl Results Elag MD95 pF MDL E" Batch Method Analyzed RY Notes Total Suspended Solids^ 20 mg/L 1 3.3 3.3 5E05004 SM 2540D-1997 05/05/15 09:09 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENCO Jacksonville cerfi/led analyfe [NC 442] AnalM [CAS Number] Results Egg Units PIE MDL P_Q.L Batch Method Analyzed Ay Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/t 1 8.7 10 5E12008 EPA 8015C 05/12/15 18:11 LTS Surrmates Results PF Spike Ly! % % Rec Limits 6afch Method nA aly By No o 1,3-8utylene Glycol 210 1 200 10496 50-150 SE12008 EPA 8015C 0511211518:11 LTS Classical Chemistry Parameters Analyte fCA&Numberl Results Elfin Units P-E MDL FRL Batch Method Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.50 U mg1L 1 2.60 5.00 5E12005 EPA 1664A 05/13/15 14:22 SMA Description: Truckyard A Lab Sample ID:C414992-02 Received: 05/01/15 11:05 Matrix: Surface Water Sampled: 05/01/15 09:40 Work Order: C414992 Project: Marsh Truck Parts Sampled By:Client ]Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified ana yte (NC 5911 Analyte FCAS Numberl Results FlaFlao Units dF MDL POLL Batch Method Analyz By Now Lead [7439-92-1]A 0.00365 J mg/L 1 0.00310 0.0100 SE08014 EPA 6010C 05/11/15 14:31 JDH Classical Chemistry Parameters ^ - ENCO Cary mrohed analyte INC 5911 AnalvW FCAS Numberl Results Flay Units DF MDL POLL Batch Method Analyzed By Notes Total Suspended Solids^ 19 mg/t 1 3.3 3.3 SE05004 SM 254OD-1997 05/05/15 09:09 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENCO Jacksonville certified analyte (NC 4421 Analyte [CAS -Number] Results wag Units PF MDL POLL Batch Method Analyzed By Notes Ethylene Glycol [107-21-1]^ 8.7 U mg/L 1 8.7 10 5E12008 EPA 8015C 05/12/15 18:28 LTS Surrewtes Results gF SpikeL v/ a/o Rec % Rec Limits Batch Method Anal By Notes 1,3-Butylene Glyml 210 1 200 10596 50-150 5Ei2008 EPA 8015C 0511211518:26 LTS Classical Chemistry Parameters Analyte fCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results Elan Units AF MDL POL Batch Method Analyzed By Notes 2.60 U mg/L 1 2.60 5.00 5E12005 EPA 1664A 05/13/15 14:22 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Description: Truckyard B Matrix: Surface Water Project: Marsh Truck Parts ANALYTICAL RESULTS Lab Sample ID:C414992-03 Sampled: 05/01/ 15 10:15 Sampled By:Client (Metals (total recoverable) by EPA 6000/7000 Series Methods (��Cmo www.encolabs.com Received: 05/01/15 11:05 Work Order: C414992 ^ - ENCO Cary certified anaryte INC 5911 Analvte_fCAS-Numberl Resul Flaa Units PIE MDL E-QL Batch Method Analyzed Ay Notes Lead (7439-92-1]A 0.00483 J mg/L 1 0.00310 0.0100 5E08014 EPA 6010C 05/11/15 14:34 JDH Classical Chemistry Parameters ^ - ENCO Cary certified an iV-- INC 5911 Results Elm Units i?E MPl P.4.L Batch Method Analyzed fix Notes Total Suspended Solid5A 26 mg/L 1 5.0 5,0 5E05004 SM 2540D-1997 05/05/15 09:09 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENC01acksonv14e rvMried anaW (NC 4421 AnalyW KAS Numberl Results Elate Units PIE M21, EQL BDLh Meth Awly3 Ay Notes Ethylene Glycol [107-21-1]A 8.7 U mg/L 1 8.7 10 5E12006 EPA 8015C OS/12/15 18:45 LTS 5urronates Results Of Spike Lv 0/0 0/a RecIimits Batch Method nA alvzed gy Notes 1,3-Butylene Glycol 210 1 200 10596 50-150 5E12008 EPA 8015C 0511211518.45 LTS Classical Chemistry Parameters LJ Analyt[CAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results EW Units PIE MPI. PRL Batch Method Analyzed ft Notes 3.04 U mg/L 1 3.04 5,85 5E12005 EPA 1664A 05/13/15 14:22 SMA FINAL This report relates only to the ample a5 received by the laboratory, and may Drily be reproduced in full. Page 5 of 9 �Cmo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 5EO8O14 - EPA 3OO5A Blank (SED8014-BLK1) Prepared: 05/O8/2015 12:08 Analyzed: 05/11/2015 13:43 Spike Source 0/nREC RPD -Analyte Result Flag POL Units Level Result %REC LirnitE RPD Limit Notes Lead 0.00310 11 0.0100 mg/L LCS (5E08014-BSI) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:46 Spike Source %REC RPD Anal vte Result Ulm P- 1 Units Level Sesult %REC Limits RPD Limit Notes Lead 0.210 0.0100 mg/L 0.200 10S 80-120 Matrix Spike (SED8014-MS1) Prepared: 05I08/2015 12:08 Analyzed: 05/11/2015 13:52 Source; C504820-01 Spike Source %REC RPD Analvte Resy-t Flag POL Units Level Result %REC Limits RPD knift Notes Lead 0.210 0.0100 mg/L 0.200 0.00310 U 105 75-125 Matrix Spike Dup (5E08014-MSDI) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:55 Source: C504820-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Resu %REC Limits RPD Limit Notes Lead 0.214 0.0100 mg/L 0.200 0.00310 U 107 75-125 2 20 Post Spike (SE08014-PSI) Prepared: 05/08/2015 12:08 Analyzed: 05/11/2015 13:57 Source: C504820-01 Spike Source %REC RPD Analvte Result Flag POL units Level Result %REC Limits RPD Limit Notes Lead 0.197 0.0t00 mg/L 0.200-0.00345 98 80-120 Classical Chemistry Parameters - Quality Control Batch 5EO5OO4 - NO PREP Blank (5E05004-BLK1) Prepared & Analyzed: 05/05/2015 09:09 Spike Source %REC RPD Anal Resul Flan P-01 Wiit4 Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5l 05004-BSI) Prepared & Analyzed: 05/05/2015 09:09 Spike Source %REC RPD Analyte Resat Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (5E05004-DUPI) Prepared & Analyzed: 05/05/2015 09:09 Source: C504669-02 Spike Source %REC RPD Analyte Res -wit Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 390 62 mg/L 380 3 20 Duplicate (5E05004-DUP2) Prepared & Analyzed: OS/0512015 09:09 Source: C505434-02 Spike Source %REC RPD Analyte Result Elag POL Units Level Result %REC Limits RPD Limit Notes - Total Suspended Solids 5100 500 mg/L 4500 13 20 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 (J�09 www.encolabs.com 1. QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 5E12008 - NO PREP Blank (5E12008-BLK1) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 17:54 Spike Source %REC RPD -AnalYte Result Flag EOL Units Level Result %REC Limits RPD LIM A Notes Ethylene Glycol 8.7 U 10 mg7L 113-Butylene Glycol 220 m9/L 200 112 50-150 LCS (5E12008-BSI) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 14:26 Spike Source %REC RPD Anal Result Flaq POL Units Level Result %REC Limits RPD Emit Notes Ethylene Glycol 190 10 mg/L 200 95 70-130 113-Butylene Glycol 220 mg/L 200 108 50-150 Matrix Spike (SE12008-MSl) Prepared: 05/12/2015 11:10 Analyzed: 05/12/2015 19:02 Source: C414992-01 Spike Source %REC RPD Analvte Result Flao P01- Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 8.7 U 94 70-130 1,3-Sutylene Glycol 210 m9/L 200 104 50-150 Matrix Spike Dup (SE12008-MSD1) Prepared: 05/12/2015 11:10 Analyzed: 05/12l2015 19:18 Source: C414992-01 Spike Source %REC RPD Anal vte Result Flan P" Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 8.7 U 95 70-130 1 25 1,3-Butylene Glycol 210 m9/L 200 10/ 50-150 Classical Chemistry Parameters - Quality Control Batch 5EI2005 - Same Blank (5E12005-BLK1) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Spike Source 0/nREC RPD Analyte Result Flau Q units Level Result %REC Limits RPD limit Notes> Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U 5.00 mg/L LCS (SE12005-BSI) Prepared: 05/12/2015 10:02 Analyzed: 05/13l2015 14:22 Spike Source %REC RPD AadlYk Result ELM P-OL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.2 5.00 mg/L 21.7 64 64-132 LCS Dup (SE12005-BSDI) Prepared: 05/12/2015 10:02 Analyzed: 05/13/2015 14:22 Spike Source %REC RPD Analvte Resin Elag PQL Units Level ResUlt %REC Limits RPD iLaift Notes Oil & Grease (HEM-SGT) Non -Polar Material 15.9 5.00 mg/L 21.1 75 64-132 13 34 Matrix Spike (SE12005-MS1) Prepared: OS/12/2015 10:02 Analyzed: 05/13/2015 14:22 Source: B404894-01 Spike Source %REC RPD AnalYte ResulS Flag ROL Units Level Result %REC Limits RPD 2nift Notes Oil & Grease (HEM-SGT) Non -Polar Material 11.0 5.56 mg/L 23.2 2.89 U 47 64-132 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only he reproduced in full. Page 7 of 9 (J�Go www.entolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 250/c concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 9 CQ 10775 Central Part Or. 4810 Executive Bark Court, Suite 111 102•A Woodwinds Industrial Ci. Orlando, FL 32824 Jacksonville. FL 32216.6069 Cary, NC 27511 ' Uawftl (407) 826-5314 Fax (407) 850-6945 (9(4) 2963007 Fax (904)-296.6210 (919) 467-3090 Fax (919) 467.3515 Page Of - Client Name Project Number Requested Analyses Requested Turnaround Marsh Truck P rts M D35 none times Note; Rush requests subject to Address Project NamaVese P.O. BOX 427 Marsh Truck Paris ` exeptance by the facility City/STMp PO M 1 Billing Info Siger City , NC 27344 0 Ln w © Q Standard TO Fax Reporting Contact (919) 663-1908 Steve Marsh 0 < c° IU N _ Expedited Due. Samolarts) Name. Alfilialion (Print) Billing Contact Chuck Hoffman T_ r (!} Sampler(s) Signature Site Local on i Time Zone Lab Workorder o ° a C414992 Preservation (see Codes) (Combine as necessary) Collection rdatrix Total a e1 {{ r ' Item a Sample ID (Field tdentilication) Collection Date Tim (PA —A Camp / Grab (see codes) Containers 1 -Sample Comments -Caryard4�15 r 3� I_C=_r�-tt _sir TrLICk'rd L\ S\Y 7 x x x x { 'i-rUCk and S S1N 7 x x X X P �� t .S Ng-J_ ''/ f R k ARA j 'T aR —7 ! 5 i ( <-- Total # of Containers mp Klt Prepared By fe 7m Relinquished By 3• ❑alarnme Receiyveedd7888 Z1 Datelrii i Comment ecial Reporting Requirements Rollnqul=he'd By/ Oawrin-re Rec Dafelilme Z.C/r� �r 'Jay n ' " t Relinquished By Oalomme R K*d ly natemme C ar 11's 8 T Hecaipl l(. Condition%port Recaiat 'Acceptable Unacceptable Matrix: GWGroundwator SO -Sail OWDAnking Wales SE-Socilment SWSurface Waler WW-Waslenater A -Air O-Other (dutalf in oamments) Preservation: 1-Ice H-HCI N-HNO3 s•H28O4 NO-NaOH O.Other (dotail in comments) Note: Ali serrlples subrrlitted to ENCO Labs are in accordance with the tar= and condilions listed on the remrso at this farm, unless prior written agreements exist r- x' Mid Atlantic Engineering & Environmental Solutions May 5, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS MARSH AUTO PARTS, INC. 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 To Whom It May Concern: RECEIVED MAY 15 2014 CENTRAL FILES DWQIBOG 409 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls A and B on April 7, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, PG Project Geologist Attachment: Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100014 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _Marsh Auto Parts, Inc. - Truckyard PERSON COLLECTING SAMPLE(S) Stephen Marsh CERTIFIED LABORATORY(S) ENCO, Inc. Lab # 591 Lab # Part A: Stormwater Benchmarks and Monitoring Results COUNTY Chatham PHONE NO. 919) 663-1908 PLEASE REMEMBER TO SIGN ON THE REVERSE --> For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 - - - - 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 4/7/2014 1.75 7.1 53 <1.6 <8.7 0.00538 J NA Outfall B 4/7/2014 1.75 6.8 64 4.30 J <8.7 0.01000 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9- 2 See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." L . 5� Name (Print name) iA4,4" c� Title (Print title) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617.Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee.) (Date] Form SWU-251, last revised October 25, 2012 Page 2 of 2 JP E NCO Laboraton'es Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, April 22, 2014 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C401660 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, April 8, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 9 (� �Go www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C401660-01 Sampled: 04/07/14 10:00 Received: 04/08/14 12:00 Peet Hold Date/Timefs) Prep DateLTime(s) Analysis Date/Timefs) EPA 1664A 05/05/14 04/10/14 11:30 04/15/14 09:35 EPA 6010C 10/04/14 04/09/14 13:19 04/10/14 12:47 EPA 8015C 04/21/14 04/21/14 10:10 04/21/14 15:04 SM 2540D-1997 04/14/14 04/09/14 08:56 04/09/14 08:56 ClientlD: TruckyardA Lab ID: C401660-02 Sampled: 04/07/14 11:30 Received: 04/08/14 12:00 Parameter EPA 1664A Hold Date/Timefs) O5105/14 Prep DatelTime(s) 04/10/14 11:30 04/15/14 09:35 EPA 6010C 10/04/14 04/09/14 13:19 04/10/14 12:59 EPA 8015C 04/21/14 04/21/14 10:10 04/21/14 15:21 SM 2540D-t997 04/14/14 04/09/14 08:56 04/09/14 08:56 Client ID: Truckyard B Lab ID: C401660-03 Sampled: 04/07/14 11.45 Received: 04/08/14 12:00 Parameter EPA 1664A Hold Date/Time(s) 05/05/14 Prep Date/Timefs) 04/10/14 Analysis Date/Time(s) 11:30 04/15/14 09:35 EPA 6010C 10/04/14 04/09/14 13:19 04/10/14 13:02 EPA 8015C 04/21/14 04/21/14 10:10 04/21/14 15:38 SM 2540D-1997 04/14/14 04/09/14 08:56 04/09/14 08:56 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 9 (� �Go www.encolabs.com SAMPLE DETECTION SUMMARY Client IM Caryard Lab ID: C401660-01 Ana Results E199 MQL POL Units Method Now Lead - Total 0.00276 3 0.00210 0.0100 mg/L EPA 6010C Total Suspended Solids 8.4 1.0 1.0 mg/L SM 2540D-1997 Client in. Truck -yard A lab ID: C401660-02 Ana Results EWS MDL Em y31b Method Nst� Lead - Total 0.00538 3 0.00210 010100 mg/L EPA 6010C Total Suspended Solids 53 1.0 1.0 mg/L SM 254OD-1997 Client ID: Truckyard B Lab ID: C401660-03 Anal rte Results Flag MU E4.L Units Method Notes Lead - Total 0.0100 0.00210 0.0100 mg/L EPA 601DC Oil & Grease (HEM-SGT) Non -Polar Material 4.30 ] 1.60 5.00 mg/L EPA 1664A Total Suspended Solids 64 1.0 1.0 mg/L SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 9 (��Cmo www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C401660-01 Received: 04/08/14 I Matrix: Surface Water Sampled:04/07/14 10:00 Work Order: C401660 Project: Marsh Truck Parts Sampled By: Client [Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary rertrfe+d anatyte INC 541] Results Eta Units PE MQI, PSL Batch Method Analyzed BY Notes Lead[7439-92-1]^ 0.00276 J mg/L 1 0.00210 0.0100 4DO9027 EPA6010C 04/1011412:47 )DH (Classical Chemistry Parameters ^ • ENCO Cary ce tlW anaW [NC 5911 Analyte. rCAS Number] Results E129 t1.DA5 PIE MU 291 02= Method Anahaed By Notes Total Suspended Solids [ECL-0169]^ 8.4 mg/L 1 1.0 1.0 4D09005 SM 2540D-1997 D4/09/14 08:56 MMR INon-Halogenated Semivolatile Organics by GC ^ - ENCO JackSonnJA' certified analyze (NC 442J Anahfie rCAS Numberl Results Flag Units 2E MRL EU [latch Method Analyz $y Notes Ethylene Glycol [107-21-1]1 8.7 u mg/L 1 8.7 10 4D18010 EPA 8015C 04/21/14 15:04 JwJ &LMNAU Resulcs Q)f Suike Lv1 0 % Rec Limirs t Meth Anahzed fir Notes 1,3-Butylene Glycol 210 1 200 10596 50-150 4DIB010 EPA B015C 0412111415:04 JWJ Classical Chemistry Parameters Ana [CAS Numberl Oil & Grease (HEM-SGl') Non -Polar Material Results Elsa Units PE MU R L Batch Method Analyzed By Notes 1,60 u mg/L 1 1.60 5.00 4D10003 EPA 1664A 04/15/14 09:35 MJF Description: Truckyard A Lab Sample ID:C401660-02 Received: 04/08/14 12:00 Matrix: Surface Water Sampled:04/07/14 11:30 Work Order: C401660 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ • ENCO Cary certified analyte INC 5911 Analyte rCAS Number] Resents Elg Units QE MP6 POL Batch Method An Ind PX Notes Lead [7439-92-1]^ 0.00538 J mg/L 1 0.002L0 0.0100 4DO9027 EPA 6010C 04/10/14 12:59 JDH Classical Chemistry Parameters ^ . ENCO Cary cectlfied analyte (NC 5911 Analyte rCAS Number] Results E[0g dulls PE M-L EQL Batch Method Analyzed OX Notes Total Suspended Solids [ECL-0169]^ 53 mg/L 1 1.0 1.0 4D09W5 SM 2540D-1997 04/09/14 08:56 MMR Non -Halogenated Semivolatile Organics by GC ^ • ENCO Jackson w1k-certlfedanalyte[NC 4421 Analyte rCAS Numberl Results E619 Units QE M-L P91 Batch Method Analyzed By Notes Ethylene Glycol[1Q7-21-1]^ 8.7 U mg/L 1 8.7 10 4D18010 EPA 9015C 04/21/14 15:21 Jw) Surmoafes Res rlts 1,3-Butylene Glycol 210 PE 1 Spikev! % Rec Jim 200 104 % 50-150 Batt¢ Method 4018010 EPA 8015C ABY 1141&5 04121114 15.11 JWJ Classical Chemistry Parameters Analyte rCAS Number fug Units PIE MPI EQL Batch Method Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar Material 1.60 u mg/L 1 1.60 5.00 4D10003 EPA 1664A 04/15/14 09:35 MJF [ECL-0104] FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 9 Ica www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C401660-03 Received: 04/08/14 12:00 Matrix: Surface Water Sampled;G4/07/14 11:45 Work Order: C401660 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary ce&rud analyte (NC 591) Analft (CAS Numberl Results Elm Units L)f MDL E91 gash Method Analyzed Ay No Lead [7439-92-1]^ 0.0100 mg/L 1 0.00210 0.0100 4DO9027 EPA 6010C 04/10/14 13:02 JDH Classical Chemistry Parameters ^ - ENCO Cary cerfiw analyte INC 5911 Analyte rCAS Numberl Results E1@S Units PE KU Pm Batch Method Analyzed By Notes Total Suspended Solids [ECL-0169]^ 64 mg/L 1 1.0 1.0 4DO9005 SM 254OD-1997 04/09/14 08:56 MMR Non-HalogenatedSemivolatile Organics by GC ^ - ENCO lacksonvllle CCr111fed analytt (NC 4411 Analyte rCAS blumber Results Eft Units PE 11126 P_1= A h Method Analyzed Jay Notes Ethylene Glycol [107-21-1]^ 8.7 u mg/L 1 8.7 10 4D18010 EPA 8015C 04/21/14 15:38 lw) S Bwotes Results _of ,Fnike L v1 % Rec % Rec [im/ts Ban¢ Afe Analyzed By (Vow 1,3-Butylene Glycol 200 1 200 IDI % 50.150 4018010 EPA 8015C D412111415.38 JWJ Classical Chemistry Parameters Analyte rCAS Numberl Oil & Grease (HEM -SG ) Non -polar Material [ECL-0104] Results EIM Units pE I✓ DL P_U Datrh Method Analyzed By lei 4.30 J mg/L 1 1.60 5.00 4DID003 EPA 1664A 04/15/1409:35 MY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 9 E�Go www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 4DO9027 - EPA 3005A Blank (4D09027-BLK1) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:33 Spike Source %REC RPD .AoaAe Result Flag IQ Units Level Result °/aREC Limits RPD Limit Notes Lead 0.00210 U 0.0100 mg/L LCS (4D09027-BSI) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:42 Spike Source %REC RPD Analyte Rellat Flag P— L Units Level Result %REC Limits RPD Limit Notes Lead 0,207 0.0100 mg/L 0.200 103 80-120 Matrix Spike (4D09027-MS1) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:49 Source: C401660-01 Spike Source %REC RPD .Analvte Result Flao POL Units Level Result %REC Limits RPD Limi Notes Lead 0.217 0.0100 mg/L 0.200 0.00276 107 75-125 Matrix Spike Dug (4D09027-MSDi) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:52 Source: C401660-01 Spike Source %REC RPD Anal RResu Flag PQL Units Level Result "/nREC Limits RPD Limit Notes Lead 0.211 0.0100 mg/L 0.200 0.00276 104 75.125 3 20 Post Spike (4D09027-PS1) Prepared: 04/09/2014 13:19 Analyzed: 04/10/2014 12:54 Source:C401660-01 Spike Source %REC RPD Anal Result Elag PQL Unm Level Result %REC Limits RPD Limit Notes Lead 0.195 0.0100 mg/L 0.200 0.00276 96 80-120 Classical Chemistry Parameters - Quality Control Batch 4DO9005 - NO PREP Blank (4D09005-BLK1) Prepared & Analyzed: 04/09/2014 08:56 Spike Source %REC RPD Anal vte Result Flag P3lL Units Level Result %REC Limi RPD UMA Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (4D09005-BS3) Prepared & Analyzed: 04/09/2014 08:56 Spike Source °/aREC RPD -Anal Result Flao RQL Units Level Resul %REC Lim! RPD UmLt Notes Total Suspended Solids 100 1.0 mg/L 100 103 80-120 Duplicate (4D09005-DUP1) Prepared & Analyzed: 04/09/2014 08:56 Source: C404629-01 Spike Source %REC RPD .Analfe Result Flag PQL Units Level Resin cVoREG Limits RPD Limit Notes Total Suspended Solids 440 1.0 mg/L 400 10 10 Duplicate (4D09005-DUP2) Prepared & Analyzed: 04/09/2014 08:56 Source: C404629-02 Spike Source %REC RPD Anal Yl& Result Elsa PQL VABS Level Result %REC Limits RPD Limit Notes Total Suspended Solids 26 1.0 mg/L 26 3 10 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 9 www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 4D18010 - NO PREP Blank (4D18010-BLK1) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 12:38 Spike Source %REC RPD Anal vte Result Flay POL Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 8.7 U t0 mg,lL 1,3 8utylene Glycol 210 mg/L 200 105 50-150 LCS (4D18010-BSI) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 10:30 Spike Source %REC RPD Anal Result Flay POL Units Level ResuR %REC Limi RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 102' 70-130 1,3-8utylene Glycol 230 mg/L 200 113 50-150 Matrix Spike (4D18010-MS1) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 10:56 Source: B401742-01 Spike Source %REC RPD Anal lde Result Flag Pot units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 200 10 mg/L 200 8.7 U 102 70-130 1,3-8utylene Glycol 210 mg/L 200 106 50-150 Matrix Spike Dup (41318010-MS131) Prepared: 04/21/2014 10:10 Analyzed: 04/21/2014 11:13 Source: B401742-01 Spike Source %REC RPD Anal l Result Flag Poll. Units Level Result %REC Limits RPD L!Mft Notes Ethylene Glycol 200 10 mg/L 200 8.7 U 99 70-130 3 25 1,3-8utylene Glycol 210 mg/L 200 107 50-150 Classical Chemistry Parameters - Quality Control Batch 4D10003 - EPA 1664A Blank (4D30003-BLK3) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source %REC RPD -Analvte Result Flan POL Units Level ResuR %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 1.60 U 5.00 mg/L LCS (4D30003-BS1) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source %REC RPD Anal sde Result Flag POL Units Level Res %REC Limits RPD Limi Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.4 5.00 mg/L 21.1 87 64-132 LCS Dup (4D10003-BSD1) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Spike Source %REC RPD .Analvte Result Flag P-QL units Level Resul %REC Limits RPD M02A Notes Oil & Grease (HEM-SGT) Non -Polar Material 18.4 5.00 mg/L 21.2 87 64-132 0.2 34 Matrix Spike (41310003-MSI) Prepared: 04/10/2014 11:30 Analyzed: 04/11/2014 09:07 Source: 8401565-02 Spike Source %REC RPD Anal Rgjult Flay POL Units Level Result %REC Limits RPD WAlit Notes Oil & Grease (HEM-SGT) Non -Polar Material 94.4 6.35 mg/L 26.0 34.3 231 64-132 QM-07 FINAL This report relates only to the sample as received 6y the laboratory, and may only be reproduced in full. Page 7 of 9 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page a of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD uej�k (a 10775 Central Port Dr, 48t0 Executive Park Court, Suite 1 I is 102-A Woudwirnis lndusbiai CL Oriando, FL 32824 Jacksonville, FL 922t6-6069 Cary, NC 27511 NED 14071026-5314 Fax (407) 850-6945 t9o4) 296r30U7 Faxj904) 296-621U (919)467-3090 Fax(919)467-3515 www.encolabs.somn Page of Cliati Name Pioject Numter Requested Analyses Requesled Turnaround Marsh Truck Parts (MA035) _[pane] Times Note; Rush requests srh, rt in Address Project Name:Desc P,O. Box 427 Marsh Truck Parts acceptance by the facility Glty,5T2p PO rr / Billing Info Siier City , NC 27344 p O Standard Tel Fax Reporting Contact (919) 663-190,0, Steve Marsh 7" U Expedited Due 5arrp!Ml3) Hzme. Affli3tlon (Print) sil'!na Contact Chuck Hoffman r- ;r, E ! Sarrpler(s) Signaiu;e Sitn Location i Time Zonr. Lab WorlOrder_ •- :_s ; c �• "� ' ,�.y�—y � f �/ ^� � 1 � l '-' I ".1. .�1�'.'ay _t `�` 0. Preservatton (Sea Gcoes) l ombine as nacessaryj _ Culleciiun - Mamx rclal 4 of Kern 4 Samp:e ID i,Field Identificaton) Collection Date Time Comp; Crab (see codes) Containers Sample Corrtrtlerlt5 y •+ zi'�_ Truck and A "I � ' L't 1 t ; :7D fit C :r SW 7 X X X X TrLic: Sd 7 X )( )C X I s JLC r;) —Total of of Containers Samae Kit ?capered Ep Date, rime Relinquished Ely i D flruTimu Hrxered y pas T e I / S Comments/epee-.iel Reootvng 3equimmenis Relinquished y ate, R ee:ed y �atteMme ITO Relinquished By Date,'Time Rer}ei,:ed By ` i)ar liima Cooler it's 8 Ternps on Receipt Condition l 1pon Receipt �- V Acr:eptable Unacceptable Watrix GN'-Groundwale 1 54Soif DW-0rinking W. ii1r SESndimont SW-Sudace Waim WW-'Naslavater A -Air O-C)Wat (detail in comments) Preservation: r-Ice H-HCl N-HNO3 5-H2SO4 NO-NaOH 0-0ther {detail in comments) Note : All samples submitted in FNCO tabs are in accordance with the temtc and mndilions hated un the itavume of this total, unless prior written agreements exisi Mid Atlantic Englnoving & Envieaiwantnl Solutions May 5, 2014 Mr. Steve Marsh Marsh Auto Parts, Inc. Post Office Box 427 J Siler City, NC 27344 Subject: MARSH AUTO PARTS, INC. — TRUCKYARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCGl00014 MID -ATLANTIC JOB NO. 00OR2372.01 Dear Mr. Marsh: 409 Rogers View Court RaWgh. NC 27510 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find three copies of the Stormwater Discharge Monitoring Report (DMR) for the above -referenced site. Please follow the instructions below to complete this sampling event. 1. Sign and date each DMR on page 2; 2. Forward the first two copies of the report along with the attached cover letter to the Division of Water Quality (mailing address is on the first page of the DMR); and 3. Insert the third copy (labeled "FILE") into Appendix C of your Stormwater Pollution Prevention Plan (SPPP). Please note that the next stormwater sample can be collected on or after July 1, 2014. We will arrange for delivery of the sample coolers prior to this date. If you have any questions, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, PG Project Geologist Attachments: Cover Letter Stormwater Discharge Monitoring Reports Laboratory Analytical Reports EXPERIENCED CUSTOMER FOCUSED INNOVATIVE Mid Atlantic Erlgiaiaobeiq & Ea)vie6rwa6r%ts1 S61utim)i December 9, 2014 Mr. Steve Marsh Marsh Auto Parts, Inc. Post Office Box 427 Siler City, NC 27344 Subject: MARSH AUTO PARTS, INC. — TRUCKYARD 3700 SILER CITY SNOW CAMP ROAD SILER CITY, NORTH CAROLINA NPDES PERMIT NO. NCG100014 MID -ATLANTIC JOB NO. 000R2372.01 Dear Mr. Marsh: 4C9 Rogers View CourL Raleigh, NC 27610 office 919.250.9718 haimile 919,250,9950 R_CE V E® DEC 18 2014 CENTRAL FILES DWR SECTION MAAONLINE,COM Attached please find three copies of the Stormwater Discharge Monitoring Report (DMR) for the above -referenced site. Please follow the instructions below to complete this sampling event. 1. Sign and date each DMR on page 2; 2. Forward the first two copies of the report along with the attached cover letter to the Division of Water Quality (mailing address is on the first page of the DMR); and 3. Insert the third copy (labeled "FILE") into Appendix C of your Stormwater Pollution Prevention Plan (SPPP). Please note that the next stormwater sample can be collected on or after 11/17/14 + 60 days. We will arrange for delivery of the sample coolers prior to this date. If you have any questions, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, PG Project Geologist Attachments: Cover Letter Stormwater Discharge Monitoring Reports Laboratory Analytical Reports EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT .10 CERTIFICATE OF COVERAGE NO. NCG100014 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Marsh Auto Parts Inc. - Truckyard COUNTY Chatham PERSON COLLECTING SAMPLE(S) Stephen Marsh PHONE NO. (919) 663-1908 CERTIFIED LABORATORY(S) ENCO Inc. Lab # 591 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall A 11/17/14 1.50 6.8 47 <2.60 <8.7 0.0102 NA Outfall B 11/17/14 1.50 6.7 51 <2.60 <8.7 0.00617! NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table 11 of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) _ pA % r-. Title (Print title) 4 4 Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) (Date) Form SWU-251, last revised October25, 2012 Page 2 of 2 ENCO Accurate. Timely. Responsive. .innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, December 4, 2014 Marsh Truck Parts (MA035) Attn: Steve Marsh P.O. Box 427 Siler City, NC 27344 RE: Laboratory Results for Project Number: [none), Project Name/Desc: Marsh Truck Parts ENCO Workorder(s): C409618 Dear Steve Marsh, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 16, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fell. Page 1 of 9 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Caryard Lab ID: C409618-01 Sampled: 11/17/14 10.45 Received. 11/18/14 11:45 Parameter EPA 1664A Hold DatelTime(sl 12/15/14 Prep DatelTimefs) 11/25/14 Analysis Date/Time(s) 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 0936 11/24/14 11:09 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:12 SM 254OD-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 Client ID: Truckyard A Lab ID: C409618-02 Sampled: 11/17/14 11:15 Received: 11/18/14 11:45 Parameter EPA 1664A Hold Date/Time(sl 12/15/14 Prep Date/Time(s) 11/25/14 Analysis DatelTlme(s) 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:12 EPA 8015C 12/01/14 11/21/14 15:41 11/21/14 21:29 SM 2540D-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 Client ID: Truckyard 0 Lab ID: C409618-03 Sampled: 11/17/14 11:20 Received: 11/18/14 11:45 Parameter EPA 1664A Hold Date(Time(sl 12/15/14 PMR DatelTimefs) 11/75/14 Analysis DatelTimels) 10:07 11/26/14 16:13 EPA 6010C 05/16/15 11/20/14 09:36 11/24/14 11:22 EPA 8015C W01/14 11/21/14 15:41 11/21/14 21:47 SM 2540D-1997 11/24/14 11/19/14 14:20 11/19/14 14:20 FINAL This report relates Only to the sample as received by die laboratory, and may only be reproduced in full. Page 2 of 9 �nrrrrur Mar www.encolabs.com SAMPLE DETECTION SUMMARY Client JIM Caryard Lab ID: C409618-01 Analvte Lead - Total Total Suspended Solids Results 0.0200 41 f&9 MDL 0.00210 1.0 EQL 0.0100 1.0 Units mg/L mg/L Method Note EPA 6010C SM 2540D-1997 Client ID: Trudcyard A Lab ID: C409618-02 ADalvte Lead - Total Total Suspended Solids krsulrc 0.0102 47 Elam M" 0.00210 1.0 ML 0.0100 1.0 Units mg/L mg/L Method saw EPA 6010C SM 2540D-1997 Client ID: Truckyard B Lab I0: C409618-03 Analldg Lead - Total Total Suspended Solids Results 0.00617 S1L Dag 3 HU 0.00210 1.0 P_4L 0.0100 1.0 units mg/L mg/L Metbgd Notes EPA 6010C SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may mly be reproduced In full. Page 3 of 9 www.encolabs.com ANALYTICAL RESULTS Description: Caryard Lab Sample ID:C409618-01 Received: 11/18/14 11:45 Matrix: Surface Water Sampled: 11/ 17/14 10:45 Work Order: C409618 Project: Marsh Truck Parts Sampled By:Client Metals (total recoverable) by EPA 6000/7000 Series Methods ' ^ - EACD Cary cevUBed analyte [AC 5911 Analyte OCAS Numberl Results flag Units pF HU PQh A=h Me Analyzed Ry Notes Lead [7439-92-1]^ 0.0200 mg/L 1 0.00210 0,0100 41(20013 EPA 6010C 11/24/14 11:09 ]DH Classical Chemistry Parameters ^ - EACD Cary c"fied analyte [AC 5911 Analyte rCAS Numberl Results Hag Units RE M PQk Batch Method Analyz Ry Notes Total Suspended Solids' 41 mg/L 1 1.0 1.0 4K19019 SM 254OD-1997 11/19/14 14:20 MMR (Non -Halogenated Semivolatile Organics by GC t ^ - EACD7ack5mvfAe certified anaryte [AIC 4421 Analyle ICAS Numberl Results E[pg Units RE MDL ML Batch Mg r� Analyzed Ay Notes Ethylene Glycol [107-21-11A 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:12 ]W] Sumoaates Results P,L i5v e I JJs 9/0 Rec I A@L' Notes 113-ButyreneGlycol 220 1 200 110% 50-150 4K21008 EPA6015C 1112111421:12 JWJ Classical Chemistry Parameters Analyte FCAS Numberl Results fim Units pE M Mi. B11111:11 Met aHll Analyzed Ay Notes Oil & Grease (HEM-SGI) Non -Polar Material 2.60 U mg/L 1 2.60 5.00 4K25008 EPA 1664A 11/26/14 16:13 MJF Description: Truckyard A Lab Sample ID: C409618-02 Received: 11/18/14 11:45 Matrix: Surface Water Sampled: 11/17/14 11:15 Work Order: C409618 Project: Marsh Truck Parts Sampled By:Client (Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - EAICO Cary cerYlRed analyte fNC 5911 Analyte [CAS Number Results flag Units pE = P91 Ratch Meamd Analyzed @y Notes Lead [7439-92-1]A 0.0102 mg/L 1 0.00210 0.0100 4K20013 EPA 6010C 11/24/14 11:12 JDH Classical Chemistry Parameters ^ - EACO Cary ceftfied analrte 1AfC 5911 Analyte fCAS Numberl Results )1g Units pf MDL EQL Batch Mgthod iiy Notes Total Suspended Solids^ 47 mg/L 1 1.0 1.0 4K19019 SM 254OD-1997 11/19/14 14:20 MMR (Non -Halogenated Semivolatile Organics by GC ^ - Eati4rO Ax*scnWL, co tilled ana44v [NC 442] Results Eka Units RE Mph EQL Batch Method Analyzed BY Notes Ethylene Glycol [107-21-1]A 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:29 JWJ .Surrogates Results PE Solke L vl % Ret % Rec Lfmits Ajrft MothodAnalned BY Notes 1,3-Butylene GlKd 220 1 200 10B % 50-150 4K21008 EPA 8015C 11/204 21:29 JWJ Classical Chemistry Parameters Anal R fCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Results Plan Units pL MDL P91. Batch Metes Analyzed Am Notes 2.60 U mg/L 1 2.60 5.00 41<25008 EPA 1664A 11/26/14 16:13 MJF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 9 rrq www.encolabs.com ANALYTICAL RESULTS Description: Truckyard B Lab Sample ID:C409618-03 Received: 11/18/14 11:45 Matrix: Surface Water Sampled. It/ 17/14 11:20 Work Order: C409618 Project: Marsh Truck Parts Sampled By: Client Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary Corked andlyre (NC 5911 Results am Units VIE MAD E L Batch Method Analyzed @Y Notes Lead t7439-92-1]A 0.00617 1 mg/L 1 0.00210 0,0100 4K20013 EPA 6010C 11/24/14 11:22 ]DH Llassical Chemistry Parameters I ^ - EACO Cary -&Acd analyre [AC S911 Anal fCAS Numbed g�i 5 nag Units pE Jyp` F" Batch Method Analyzed By Notes Total Suspended Solids^ 51 mg/L 1 1.0 1.0 4K19019 SM 254OD-1997 11/19/14 14:20 MMR Non -Halogenated Semivolatile Organics by GC ^ - ENCO ld[kscvrvrAe C"fied dnalyte [AC 442] Results Elaq UDA2 Qf MDL Eg- Batch Me Analyzed ¢y Notes Ethylene Glycol i107-2t-l]^ 8.7 U mg/L 1 8.7 10 4K21008 EPA 8015C 11/21/14 21:47 ]W] mates Results _Of Spike 1 vl ° % Be L190Oclr Meth AQa(gr Note 1,3-6utyb- G1yro1 210 1 200 107 % 50-150 4K21008 EPA 8015C IV2111421:47 JWJ Classical Chemistry Parameters Analyte fCAS Numbed ail & Grease (HEM-SG-0 Nan -Polar Material Results EIS WU PE L1 L I'_Q6 patch Metw Analyzed ft Notes 2.60 U mg/L 1 2.60 5.00 4K25008 EPA 1664A 11/26/14 16:13 M]F FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 0( 9 ■r r www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 4K20013 - EPA 3003A Blank (4K20013-BLKI) Prepared: 11/20/2014 09:36 Analyzed: 1 V24/2014 10:47 Spike Source %REC RPD Anal Yte Rewlt Flaa FM Units Level Result %REC Limits RPD U111 t Notes Lead 0.00210 U 0.0100 mg/L LCS (4K20013-BS1) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:51 Spike Source °/oREC RPD _Aualut& Result Flaa POL Units Level Result %REC Limns RPD Limit Notes Lead 0.208 0.0100 mg/L 0.200 104 80.120 Matrix Spike (4K20013-14Sl) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:57 Source:C414111-01 Spike Source %REC RPD Anal vte Result F1au M units Level Resul a/aREC Limits RPD Limit Notes Lead 0.221 0.0100 mg/L 0.200 0,00210 U 111 75-125 Matrix Spike Dup (4K20013-MSDl) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 10:59 Source: C414111-01 Spike Source %REC RPD Anal vte Result Elaa POL uIllt4 Level Result a/aREC Liml RPD Limit Notes Lead 0.212 0.0100 mg/L 0.200 0,00210 U 106 75-125 4 20 Post Spike (4K20013-PSI) Prepared: 11/20/2014 09:36 Analyzed: 11/24/2014 11:02 Source: C414111-01 Spike Source a/oREC RPD Analvxe Result IIaa P L units Level Result %REC Limits RPD Limit Notes Lead 0.193 0.0100 mg/L 0.200 0.00104 96 80-120 Classical Chemistry Parameters - Quality Control Batch 4K19019 - NO PREP Blank (41(19019-81-K3) Prepared & Analyzed: 11/19/2014 14:20 Spike Source %REC RPD .Allalvte Result Elan P_QL Units Level $€sim!t %REC Limits RPD Llllllt Notes_ Total Suspended Solids 1.0 U 1.0 mg/L LCS (41(19019-B51) Prepared & Analyzed: 11/19/2014 14:20 Spike Source o/aREC RPD Anal 1dL Rend Hall PQL unm Level Result °/aREC Limits RPD jilt Notts Total Suspended Solids 100 1.0 mg/L 100 101 80-120 Duplicate (4K19o19-DUPl) Prepared & Analyzed: 11/19/2014 14:20 Source: C409616-01 Spike Source a/oREC RPD _Anatvte Result Elao PL Units Level Re u %REC Limits RPD Limit Note Total Suspended Solids 39 1.0 mg/L 41 5 to Duplicate (41(19019-DUP2) Prepared & Analyzed: 11/19/2014 14:20 Source: C409618-02 Spike Source %REC RPD Analye Result flag PAL units Level Result %REC Limits RPD limit Notes - Total Suspended Solids 50 1.0 mg/L 47 7 10 Non -Halogenated Semivolatile Organics by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In NO. Page 6 of 9 �r a I�rtilRArl ® t� www.encolabs.com QUALITY CONTROL DATA Non -Halogenated Semivolatile Organics by GC - Quality Control Batch 4K21008 - NO PREP Blank (4K21008-BLK1) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 17:47 Spike Source %REC RPD Anal Result Flag e4L Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 8.7 U 10 mg/L 1,3-eulylene GlKd 190 _WL 200 95 50-150 LCS (4K21008-BSI) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:02 Spike Source %REC RPD Analy ResVlt ELag PDL Units Level Itesul %REC Limits RPD Limit Notes Ethylene Glycol 190 10 mg/L 200 95 70.130 1,3-804*v a Gtyrd 210 nWL 200 107 -10-15D Matrix Spike (4K21008-MSI) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:19 Source: B405123-01 Spike Source %REC RPD Analy Result Flae FIX Units Level Result %REC Limits RPD Limit Notes Ethylene Glycol 210 10 mg/L 200 8.7 U 107 70-130 1,3-8utykm Glycol 220 mg/L 200 111 50-150 Matrix Spike Dup (4K21008-MSDI) Prepared: 11/21/2014 10:41 Analyzed: 11/21/2014 14:36 Source: 8405123-01 Spike Source %REC RPD .ADaLVIC Result Flag P_QL !!nits Level Result %REC Limits RPD l:[M t Notes Ethylene Gyoal 220 10 mg/L 200 8.7 U 108 70-130 2 25 1,3-Bu44_— G4iW 110 -91L 200 110 50-150 Classical Chemistry Parameters - Quality Control Batch 4K25008 - EPA 1664A Blank (4K25008-BLKl) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Anal 1d& Reisilt flag E" units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-5GT) Non -Polar Material 2.60 U 5.00 mg/L LCS (4K25008-BSI) Prepared: 11/25/2014 10:07 Anayzed: 11/26/2014 16:13 Spike Source %REC RPD Ana111tC Result flag E" shuts Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SG-T) Nan -Polar Material 21.2 5.00 mg/L 20.8 102 64-132 LCS Dup (4K25008-BSD1) Prepared: 11/25/2014 10:07 Analyzed: 11/26/2014 16:13 Spike Source %REC RPD Ana hde fl4.sult Flag P44 llnits Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 20.9 5.00 mg/L 20.6 101 64-132 1 34 FINAL This report relates only to the sample as reoeived by the laboratory, and may any be reproduced In full. Page 7 of 9 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification" P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in cull. Page 8 of 9 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolal)s.com 1.:/ i.rntna Pan r;,. •i9 10 Ew-uliv- N4. Cu: I. SuQ= 11 IP-A vloalm.),5 lltjjyLjrfl C;. I ;2C 5314 (it)-, 96-300, (ql.l I (I "q 57 ;4-nl Narrm ?!I)Lj;:l 5;eVj90gd Ana!ycws Reques: - ec Tm icvcund Px::. cilv,,. T,2 r J Uilhl 14 il T'A j blot M;:, EYpedited i u _U! XW1 L 1),' Lab Wc Pm-6,­eL Wv c,3c Go Imi (:n 4.1.,16 0 MAI) cm.- X 7 j AL-L n. vllirll x Y 1 J-1-H 0 K.] J'(. 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