NCG080867_MONITORING INFO_20170501

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. Iv C� Ub b �-LQ q
DOC TYPE ❑HISTORICAL FILE
J
I%--MMONITORING REPORTS
DOC DATE ❑ ciiOl q bc� 0
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number iNCS NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 080867
FACILITY NAME Snipes Brothers Oil Company
PERSON COLLECTING SAMPLE(S) _Steve Barnwell
CERTIFIED LABORATORY(S) _Pace Analytical Lab #_12
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING: CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY _Person_
PHONE NO. ( 336_) 227-8881
SIGNATURE OF PERi<1ITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Oulfall
(late
50050
No.
Sample
Collected
Total
Flow (if app.)
Total
Rainfall
TPH, EPA
Method 1664
Total
Suspended
Solids
PH
nto/dd/vr
MG
incites
Mall
Ma/I
Standard units
Benchmark
15
100
6.0 — 9.0
001 (SBOC)
4/6/2017
NA
<5.0
14.8
�'
(field
measurement
6.3
Lab
measurement
Does this facility perform Vehicle Maintenance Activities using more than » gallons of new motor oil per month? _yes _XX no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Re uiretnents
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil'& Grease
(if appl.)
Non -polar
-O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
PH
New Motor
Oil Usage
nto/dd/N,r
MG
inches
mall
mall
unit
aallmo
Form SWU-247, last reviser12/2/2012
Pare 1 of 2

STORM EVENT CHARACTERISTICS:
Date 4/1/2017
Total Event Precipitation (inches): _LOI_
Event Duration (hours): (only if applicable -- see permit.)
(if Snore than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only ifapplicable— see pennit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleiti-h, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel proper!}' gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
-17-,// /J:�
(Da(e)
Form SWU-247, last revised 21212012
Pace 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For,guidance onI-Ming out this form, please visit: htt ): [por-tal.ncdenr.oi- lweh/wq/ws/su/n»dessw#tali-4
Permit No.; N/C/ 0 / 8 /0_/0_/0_/0_/0_/ or Certificate of Coverage No.: N/C/G/0_/8_/0_/8_/6_/7_/
Facility Name: Snipes Brothers Oil Company
County: Roxboro Phone No.
Inspector: fy-e-Ve Wit Lje)
Date of Inspection: 4/6/201.7
Time of Inspection: �_d� "
Total Event Precipitation (inches): _1.01 inches
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
X Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during o "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0A inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-h0ur storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify t! at this report is accurate and complete to the best of my knmvledge:
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No.
too J Structure (l)ipe, dit h, etc.
Receiving Stream: �-
Describe the industrial activities that occur within the outfall draiiiaue area:
2. Color: Describe the color- of the disc] at-ge Using basic colors (i'ed, brown, blue, etc.) and tint
(light, niedlkirli, dark) as descriptot's:. G e,.--c%-n
3. Odor: Describe any di s inct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 04 _e_
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of Floatirig solids in
the storinwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely mktddy:
1 6) 3 4 5
7. Is there any foain in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes ONO
9. is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution: A/C)"l
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-2,12, last modified 10/25/2012

aceAnalytrcal
wvnvpacalabs.cnm
i
April 14, 2017
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
RE: Project: WATER
Pace Project No.: 92336431
Pace Analytical Services, LLC
9800 Kincey Ave- Suite 100
HuntersOje, NO 28078
[phone]
Dear Mr. Watterson:
Enclosed are the analytical results for sample(s) received by the laboratory on April 07, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
[phone]
Project Manager
ElICIGSUre5
cc: Mr. Lyndal 8utler, SWE, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except in lull,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnaVical
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Project: WATER
Pace Project No.: 92336431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave, Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 9900(3001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 46022)
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

aceAnapical
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
{704}875-9092
Project
Pace Project No.:
WATER
92336431
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92336431001
SBOC
EPA 1664E
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA9040
MJS1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalyfical
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1
Project: WATER
Pace Project No.. 92336431
Lab Sample ID Client Sample ID
Vlethod Parameters
92336431001 SBOC
SM 2540D Total Suspended Solids
EPA 9040 pH
SUMMARY OF DETECTION
Result Units
14.8 mglL
6.3 Ste. Units
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except !n full,
without the written consent or Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28075
[phone]
Report Limit Analyzed Qualifiers
5,0 04113/1712:22
0,10 04111 /17 00:20 H6
Page 4 of 16

aceAnaWical
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PROJECT NARRATIVE
Project: WATER
Pace Project No. 92336431
Method: EPA 1664E
Description: HEM, Oil and Grease
Client; S&ME - Greensboro
Date; April 14, 2017
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andlor the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Surrogates:
All surrogales were within OC limits with any exceptions noted below.
Method Blank;
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 16

, 7 ace Analytical
wu�v.pacernbs.ram
PROJECT NARRATIVE
Project: WATER
Pace Project No.: 92336431
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: S&ME - Greensboro
Date: April 14, 2017
Pace Analytical Services, LLC
9500 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
i sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within CC Il mits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
CC Batch: 356529
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
DUP (Let) ID: 1977698)
• Total Suspended Solids
DUP (Lab ID: 1977699)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except iri full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 16

aceAnalXical
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PROJECT NARRATIVE
Project: WATER
Pace Project No.: 9233C431
Method: EPA 9040
Description: 9040 pl-I
Client: S&ME - Greensboro
Date: April 14.2017
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
I sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA required holding time.
• SBOC (Lab ID: 92336431001)
Method Blank:
All analytes were below the report limit in the melhod blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: 356066
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1975207)
• phi
Additional Comments:
phis data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
TNs report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 7 of 16

aceAnal ical
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i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvi1e, NC 28078
[phone]
Project: WATER
Pace Project No.: 92336431
Sample: SBOC
Lab ID: 92336431001 Collected: 04/06/17 13 05
Received: 04/07/17 09:01 Matrix: Water
Parameters
Re$ lts Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
<5.0 mglL
5 0 1
04/12/17 07 07
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
14.6 mglL
5.0 1
04/13/17 12:22
9040 pH
Analytical Method: EPA 9040
pH
6.3 Sid. Units
0,10 1
0411111700:20 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
1 04/14/2017 01:13 AM without the written consent of Pace Analytical Services, LLC. Page a of 16

7aceAnaVical
- ww,veacnla0s.com
QUALITY CONTROL DATA
Project WATER
Pace project No.: 92336431
QC Batch: 356272 Analysis Method: EPA 1664B
QC Batch Method EPA 1664B Analysis Descriptlon: 1664 HEM, Oil and Grease
Associaled Lab Samples: 92336431001
METHOD BLANK, 1976390
Associated Lab Samples 92336431001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 1976391
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix Water
Blank Reporting
Result Limit Analyzed Qualifiers
<5.0 5.0 04112/17 07:05
Spike LCS LCS % Rec
Conc. Result % Rec Llntits Qualifiers
40 37.7 94 78-114
MATRIX SPIKE SAMPLE: 1976392
92336431001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L <5.0 40 40.2 98 78-114
Results presented on thus page are in the units indicated by the "units" column eKcePt where an alternate unit is presented to the rlyht of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu11,
Date: 04/14/2017 01:13 AM without the written consent of Pace Analytical Services, -LC. Page 9 of 16

aceAnaVical
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r
Project: WATER
Pace Project No.: 92336431
QC Batch: 353529
OC Batch Method: SM 2540D
Associated Lab Samples: 92335431001
METHOD BLANK: 1977696
Associated Lab Samples: 92336431001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 1977f397
Parameter
Units
Tolai Suspended Solids
mg/L
SAMPLE DUPLICATE: 1977698
Parameter
Units
Total Suspended Solids
rnglL
SAMPLE DUPLICATE: 1977699
Parameter
Units
Total Suspended Solids
mglL
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Descriplion: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
<2.5 2.5 04/1311712:21
Spike LCS
Conc. Result
250 246
92336360001 Dup
Result Result
14.4 11.8
92336649002 pup
Result Result
9.4 10.6
Pace Analytical Services, LLC
9800 Klncey Ave, Suite 1p0
Huntersville, INC 28078
(704) 87 5- 9092
LCS % Rec
e% Rec Limits Qualifiers
96 90-110
RPD Qualifiers
20 D6
RPD Qualifiers
12 D6
Results presented on this page are in the units indicawd by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/1412017 01:13 AM without the written consent of Pace Analytical Services, LLC, Page 10 of 16

1�zAnaWical"
www pacefnbs.com
QUALITY CONTROL DATA
Project: WATER
Pace Project No.: 92336431
QC Batch: 356066 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 923364310D1
SAMPLE DUPLICATE: 1975207
92336097001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7,0 7.2 2 D6,HB
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the ut lts indicated by the "Units" column except where an alternate unit is presented W the right or the result.
REPORT OF LABORATORY ANALYSIS
This repon Shall not be reproduced, except in full,
Hate: 04/14/2017 01:13 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 16

aceAnalytical
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QUALIFIERS
Project WATER
Pace Project No.. 92336431
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersvOle, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL- Ad)usted Method Detection Limit.
Pa - Practical Quantitalion Limit
RL - Reporting Limit.
S - Surrogate
1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl elhec
A separate vial preserved to a i of 4-5 is recommended in SVV846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
Fib Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reprOdueed, except in full.
Date: 04/14/2017 01:13 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

aceAncilytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WATER
Pace Project No.: 92336431
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NC 26078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92336431001
SBOC
1=PA 1664H
356272
92336431001
SBOC
SM 2540D
356529
92336431001
SBOC
EPA 9040
356066
Date 04/14/2017 01:13 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Analytical
Batch
Page 13 of 16

Document Name:
Document Revised; Sept. 21, 2016
/- �acaAnalyficW
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.;
Issuing Authority:
1
F•CAR-CS-033-Rev.01
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[]
CIi Name:. ':
� 1 �C ��' Project
Courier: []Fed Ex I ❑UPS ❑usPS ❑Client
[I Commercial ]Pace 00ther:
Custody Seal Present? ❑Yes No Seals Intact? I/ IYes :No �) )l 1� I t
TTTT��� P pate/initials Person Examining Contents: I� �( JI
Packing Material: ❑Dabble U.'ran 6ubble Bags ❑None ❑Other;
Thermomete : Wet El ❑.None arnples on ice, cooling process has begun
IR Gun ID; Typc. f Ice,: (((((( !
Correction actor: Cooler Temp Corrected ('C}; � � Biological Tissue Frozen? []Yes PN/A
Temp should be abave freezing to 6°C
--.._--
Did sampl s originate in a quarantine zone viitift the United States: CA, NY, or SC (check maps)?
nYe 'PiNc
WU#:92.336431
11811911II' 111 V I I III
92335431
Did samples originate from a foreign source (inter ationally,
including Ha .,ad and Puerto Rico]? nyes VINo
r —r
Comments/Discrepancy: —
Chain Of Custody Present?
myes
❑No
ON/A.
1.
Samples Arrived within Hold Time?
{ Yes
[]No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
j Yes
ONO
❑N/A
3.
Rush Turn Around Time Requested?
❑yes
NO
❑N/A
d.
Sufficient Volume?
[]Yes
[]NO
❑N/A
S. —
Correct Containers Used?
-Pace Containers USed?
yes
eyes
❑No
[]NO
❑N/A
❑N/A
6.
�Onlaincl's Intact?
Des
❑No
Dim
i.
Samples Field Filtered?
❑Yes
ONO
N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Klatch COO
__Includes Date/Time/iD/Analysis fViatrix: �f
]Yes
/
❑No
❑N/A
9.
lleadspace if) VOA dials (>5.6mm)?
❑Yes
[-]No
da/A
`
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
L ❑Ycs
❑No
❑No
N/A
., N/A
11,
CLIENT NOTIFICATION/RESOLUTION
Person Cc mtacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: --(�L.
Project Manager SRF Review: (C
Field Data Required? ❑Yes ❑Ido
Date/Time;
Date, lid
r_.
Date:
Mote: Whenever [here is it discrepancy affecting North Carolina compliance samples, a copy cf this form %,Jli be sent to the North Carolina DCHNR Certification Office (i.e.
Out of hold, incorrect prese(vative, out of temp, incorrect containers)
Page 14 of 16

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SAPAPLER:
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Q0

STORMWATER DISCHARGE 0UTFALL (SDO)
MONITORING REPORT
Permit Number NCS NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 080867
FACILITY NAME Snipes Brothers Oil Company
PERSON COLLECTING SAMPLE(S) _Steve Barnwell
CERTI FI ED LABORATORY(S) _Pace Analytical Lab 4_12
Lab ti
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall he received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY _Person_
PHONE NO. (_336_) 227-8881
SIGNA"FURL OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
,r-f,r_%\/Pn
Outfall
No.
Date
Sample
Collected
50050
Total
FloNV (if app.)
Total
Rainfall
TPH, EPA
Method 1664.
Total
Suspended
Solids
pH
CRNTRAL
EB 2 Q Z017
FILES
No/dd/yr
MG
inches
Mg/l
MQ/l
Standard units
QWR
SECTION
Bench m:lrk
!
100
6.0 — 9.0
001 (S130C)
12/7/2016
NA
, s 3
<5.0
16,2
(field
measurement
[does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _XX_no
(if yes, complete Part B)
Part i3: Vehicle Maintenance Activity Monitoring Re uirements
Ontfall
No.
Date
Sample
Collected
50050
Total Flow
(if applicable)
005i6
00530
00400
Total
Rainfall
Oil S Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
molddhvr
me
inches
nla,/I
nlg/I
unit
<yal/mo
norm S W U-247_ last revised 2/2/2012
Pate 1 of 2

STORM EVFNT CHARACTERISTICS:
Date _12/7/2016
Total Event Precipitation (inches): —
only ifapplicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (honrs): (only if applicable —see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, [north Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance wills a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information.
including the possibility of fines and imprisonment for knowing violations."
1.3 IgIl 7t t It U U1 f t"[ 111 It l CCU
f
(Date)
Form SWU-247_ last revised 21212012
1'a,e 2 of 2

NCDEN
Stormwater Discharge 4utfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: h t orral n 1 nr. r web we w s r n d ,s wtrrb
Permit No.: N/C/ 0 / 8 /0-/0_/0_/0_/0_/ or Certificate of Coverage No.: N/C/G/0_/8_/0-/8_/6_/7-/
Facility Name: Snipes Brothers Oil Company
County: Roxboro Phone No. JA - d-
Inspector: S 4-?,U�e fe
Date of Inspection: 12/7/2016
Time of Inspection: 1- 3 -S- AM
Total Event Precipitation (inches): f 13
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
X Yes ❑ No
Please verify whether Qualitative Monitoring n7ust be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that meastn'es greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inclies has occurred. A single storm event May contain up to 10 consecutive hoUr'S of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I C�gtify that this report is accurate and complete to the best of my knowledge:
ignature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description: n
Outfall No. 00-1- Structure (pipe, ditch, etc.)
Receiving Stream:
NO
Describe the industrial activities that dCC111- within the otgfall �lrainagq/,gea:
2. Color: Describe the color of the di charge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: C leer
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): A 6. 1 -e--
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy: % V 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4, 5
G. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely nudely:
1 0 3 4- 5
7. Is there any foam in the stormwater discharge? Yes �No
8. is there an oil sheen in the stormwater discharge? Yes N
9. Is there evidence of erosion or deposition at the outtalk'? Yes / to
10. other Obvious Indicators of Stormwater Pollution: /
/V
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5WU-242, Last modified 10/25/2012

1�2ce Analytical
� wx•,epacelaDs.com
j
December 14, 2016
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
RE: Project: SNIPES BROS OIL
Pace Project No.: 92322623
Paco Analytical Services, LLC
98DO Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Watterson:
Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2016,
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
cc: Mr. Lyl Butler, SWE, Inc.
Q 11 C �D
{ REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
98 RA10
Page 1 of 14

r aceAnal tical
wrnvpacelaos.cwn
Project: SNIPES BROS OIL
Pace Project No.: 92322623
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification fps
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Caroiina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification los
2225 Riverside drive, Asheville, NC 28804
PloridalNELAP Certification #: E87648
Massachusetts Certification k M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

Pace Analytical Services, LLC
/a'ceAnalyfical" 9800 Kincey Ave. Suite100
Huntersville, NC 28078078
wmvpacelabs.com [phone]
i
SAMPLE ANALYTE COUNT
Project: SNIPES BROS OIL
Pace Project No.: 92322623
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92322623001 SBOC EPA 1664B JMS 1 PASI-C
SM 2540D MJS1 1 PASI•A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 14

aceAnaV cal
f wmv.pacelabs.corn
i
Project: SNIPES BROS OIL
Pace Project No 92322623
Lab Sample ID Client Sample ID
Method Parameters
92322623001 SBOC
SM 2540D Total Suspended Solids
SUMMARY OF DETECTION
Result
16.2 mglL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, Li
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(7 04) 875-9 092
Report Limit Analyzed Qualifiers
6.2 12/13/16 22:39
Page 4 of 14

_ aceAnalytical
ww paceleDs.com
PROJECT NARRATIVE
Project: SNiPES BROS OIL
Pace Project No.: 92322623
Method: EPA 1664B
Description: HEM, Oil and Grease
Client: S&ME - Greensboro
Date: December 14, 2016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sampie was analyzed for EPA 166413. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC {mils with any exceptions noted below.
Method Blank:
All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
A!l percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shakl not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 14

1_�;aceAnaVical'
wvnvpacelahs.ccm
i
I
PROJECT NARRATIVE
Project: SNIPES BROS OIL
Pace Project No.: 92322623
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: S&ME - Greensboro
Dato: December 14, 2016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: 340435
D6. The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1888203)
• Total Suspended Solids
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 14

1�ace A nalyticaI
f ww,vpacalabs.corn
ANALYTICAL RESULTS
Project: SNIPES BROS OIL
Pace Project No.: 92322623
Paco Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sal SBOC Lab 1D: 92322623001 Collected: 12/07116 09:40 Received: 12/08/16 11:26 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16646
Oil and Grease <5.0 mg/L 5.0 1 12/14/16 06:40
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 16.2 1 1 1 12/13/16 22:39
Date: 12/1412016 03:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 14

aceAnalytrcal
1 wwwpacafvbs.com
f
t
r
Project: SNIPES BROS OiL
Pace Project No.: 92322623
OC Balch: 340739
QC Batch Method: EPA 1664E
Associated Lab Samples: 92322623001
METHOD BLANK: 1890052
Associated Lab Samples: 92322623001
Parameter Units
Oil and Grease mg1L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
<5,0 5.0 12/14/16 06:35
Pace Analytical Services, LLC
9500 Kincey Ave. Suite 100
Huntarsville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1890053
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 38.0
95
78-114
MATRIX SPIKE SAMPLE-
1890054
92322595001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
ND 40
371
93
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Theis report shall not be reproduced, except in full.
Date: 12/14/2016 03:47 PM without the written consent of Pace Analytical Services, LLC,
Page 8 of 14
r

_ aceAnalytical
mnvpacolada.rcm
I
QUALITY CONTROL DATA
Project: SNIPES BROS OIL
Pace Project No.: 92322623
Pace Analytical Services, LLC
9800 Kincey Ave. Suile 100
Huntersville, NC 28078
[phone]
QC Batch: 340435
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92322623001
METHOD BLANK: 1888201
Matrix: Water
Associated Lab Samples: 92322623001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
<2.5 2.5 12/13/16 22:34
'
LABORATORY CONTROL SAMPLE: I B88202
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
%s Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 224
90 90-110
SAMPLE DUPLICATE: 1888203
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1888204
Parameter
Total Suspended Solids
92322559003 Dup
Units Result Result RPD Qualifiers
mg1L 11.8 12.4 6 D6
92322606003 Dup
Units Result Result RPD Qualifiers
mg1L ND <5.0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/1412016 03:47 PM without the written consent of Pace Analytical Services, t_LC. Page 9 of 14

,� aceAnaVical®
ww,vpncelaBs.com
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QUALIFIERS
Project: SNIPES BROS OIL
Pace Project No.: 92322623
DEFINITIONS
Pace Analytical Services, LLC
9B00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The resull for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NO - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes
TNI - The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuii,
Date', 12/14/2016 03:47 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnaWicaf
wm�:pacelabs.eom
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project SNIPES BROS Olt_
Pace Project No,: 92322623
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92322623001 SBOC EPA 16645 340739
92322623001 SBOC SM 2540D 340435
Date: 12/14/2016 03:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in U1.
without the written consent of Pace Analytical Services, LLC
Page 11 of 14

Document Name:
Document Revised: Sept. 21, 2016
�,- ac -eAnapicai
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
Client Name:
i , Project H:
Courier; ed Ex UPS ❑U5P5 ❑Client
❑ Commercial Pace ❑Other:
Custody Seal Present? ❑Yes No sea s Intact? ❑Yes v No
iaoa . erszasza
92322623
Sr �-
Date/Initials Person Examining Contents: Z�Z q
Packing Material; ❑Bubble Wrap Rubble Bags []None ❑Other;
Thermometer;
❑ IR Gun ID: 1 0 Type of Ice: © et []Blue❑Tione Samples on lee, coolie( 7roce55 Itas begun
Correction Factor; Cooler Temp Corrected (°[); Z r� Biological Tissue Frozen? ❑Yes �`No ❑N/A
Temp should be above fr ezing to VC
USDA Regulated Soil { 2N/A, water sample) /
Did sample originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? did samples originate from a foreign source linteroaiionaiiy,
Ayes No indudine Hawaii and Puerto Rico)? F]Yes Vic,
Comments/Discrepancy;
Chain of Custody Present?
dyes
[:]No
❑N/A
1.
Samples Arrived vrithin Hold Time?
Yes
❑ o
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
(:]Yes
No
❑N/A
3,
i
Rush Turn Around Time Requested?
❑Yhs
No
❑N/A
4.
Sufficient Volume?
es
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Y s
Y s
[:]No❑N/A
❑No
❑N/A
6.
Contafnersintact?
Yes
❑ o
❑N/A
7.
Sam lei field Filtered?
❑y s
. No
❑N/A
&, Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
ONO
❑N/A
9.
Headspace In VOA Vals (>5-6nzm)?
❑Yes
FINP
UdNIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Dyes
Dyes
❑ Jo
[)Noi
❑ A11.
NN(A
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: [ (-
Project Manager SRF Review:
Field Data Required? []Yes ❑No
Date/Time:
Date: I Z Jttc ^
Date. 12 -7 I L
Note: Whenever there is a discrepancy affecting Norl#t Carolina compliance samples, a copy of this form ME be sent to the North Carolina DEHPJR Certification Office (i.e.
Chit of hold, incorrect preservative, out of temp, incorrect containers)
Page 12 of 14

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SP5T-12S mL Steri€e Plastic (N/A — lab)
SM-250 mL Sterile Piastic (N/A —lab)
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CHAIN -OF -CUSTODY f Analytical Request document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
0
Page- j of m
1 cu
Rrqulred CVenl Irformation_ Required Project Information: Invoice In`ormaUOn:
Company: 'j P,-r, ro: Attention: 3 1
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Parchise Order No.:
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Site Location
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STATE: Yj "
Requested Due DateriAT: -
Project iJumi:er: `
Pace Prot;c tr:
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Analysis
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Section D ihalrix Code:
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Permit Number NCS NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 080867
STORMWATER DISCHARGE OUTFALL (SDO)
,11VE` ;REPORT R1fd
SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
FEB. 1 201�This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
CENTRAL FILES
FACILITY NAME Snipes Brothers Oil Company DWR �ITFKW _Person_
PERSON COLLECTING SAMPLE(S) _Steve Barnwell PHONE NO. (_336J 227-8881
CERTIFIED LABORATORY(S) _Pace Analytical Lab #_12
Lab #
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall
Dale
50050
No.
Sample
Collected
Total
Flow (if app.).
Total
Rainfall
TPH, EPA
Method 1664
Total
Suspended
Solids
PH
nioldd/ yr
MG
inches
Mall
Ma/I
Standard units
Benchmark
15
100
6.0 — 9.0
001 (SBOC)
12/4/2015
NA
"']
<5.0
48.4
(field
measurement
6.6
(laboratory)
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes _XX no
(if yes, complete fart B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfali
No.
Date
Sample ,
Collected
50050
00556
Oil & Grease
(if appl.)
Non -polar
O&C/TPH
(Method 1664
SGT-HEM), if
apI.
W30
Total
Suspended
Solids
00400
pH -
New Motor
Oil Usage
Total Floe'
(if applicable)
_
Total
Rainfall
mo/dd/vr
MG
inches
ma/l
m /I
unit
al/mo
Form SWU-247, lust revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
r
Date 12/1/2015
Total Event Precipitation (inches): —
only if applicable -- see permit.)
(if more than one storm event was sampled)
Date 12/2/2015
Total Event Precipitation (inches): _0.27
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel proper[y gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Form SWU-247, last remised 21212012
Pa<ae 2 oft

STORMWATER DISCHARGE OUTFALL (SDO)
r(r
ryl NITORING REPORT
Permit Number NCS NCG080000 �� SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
CERTIFICATE OF COVERAGE NO. NCC08 080867 (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Snipes Brothers Oil Company
PERSON COLLECTING SAMPLE(S) _Steve Barnwell
CERTIFIED LA BORATORY(S)_Pace Analytical
Part A: Specific Monitoring Requirements
COUNTY _Person_
PHONE NO. (_336_) 227-8881
Lab ##_ 12
Lab
��I `ED
JUL 11 2016
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
Date
50050
No.
Sample
Collected
Total
Flow (if app.)
Total.
Rainfall
T 1 , PA
Method 1664
Total
Suspended
Solids
pH
-'
mo/dd/yr
MG
inches
M01II
M(Yll
Standard units
Benchmark
15
100
6.0 — 9.0
001 (SI1OC)
5/18/2016
NA
r� n
r V j
1.61
15.6
(field
measurement
7.0
(laboratory)
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _XX_no
(if yes, complete ]'art B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/vr
MG
inches
mg/I
m«/I
unit
al/mo
Form SWIJ-247, last revised 21212012
Pale l of 2

STORM EVENT CHARACTERISTICS:
Date _5/18/2016
Total Event Precipitation (inches):
Event Duration (hours): _ �> (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
includinb the possibility of fines and imprisonment for knowing violations."
(Signature of Per
-7/71//
(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http:///portal.ncdeni .or;J« eb/wq/ws/su/m�dessw#tad 4
Permit No.: N/C/ 0 / 8 /0_/0_/0_/0_/0_/ or Certificate of Coverage No.: N/C/G/0_/8_/0_/8_/6_/7_/
Facility Name: Snipes Brothers Oil Company
County: Roxboro Phone No.
Inspector: c`fe- w e- jA
Date of Inspection: 1 1
Time of Inspection: V
rW
Total Event Precipitation (inches): ' ` !
Was this a "Representative Storm Event" or "Measureable Storm Even s defined by the permit?
(See information below.)
X Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representotry s orm
event"or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
perforined daring a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, l certify that this
report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall D scription: p
OLitfall No. 66! Structure (pipe, di ch, etc.) ! '
Receiving Stream: 1 P: b o f v NCP . r` l) U'
Describe the industrial activities that ocEur within the utfall drainage area:
dM_ 13 V
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: e Iec, r
3. Odor: Describe any distinct n that the discharge may have (i.e„ smells strongly of oil,
weals chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloddy:
2 3 4. 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 [ 2) 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 11 is no solids and 5 is extremely muddy:
1 4Y 3 4 5
7. Is there any foam in the stormwater discharge? Yes Do
8. Is there an oil sheen in the stormwater discharge? Yes 0
9. Is there evidence of erosion or deposition at the outfall? Yes (No
10. Other Obvious indicators of Stormwater Pollution: /V Q (1e-
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5WU-242, Lase modified 10/25/2012

's
aceAnalytical
! w�nupecarabs.pam
f
December 16, 2015
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
RE: Project: REF. SNIPES OIL
Pace Project No.: 92278575
Dear Mr. Watterson:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 04, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Report revised on 12.16.15to correct a discrepancy with the Total Dissolved Solids analysis.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
trey. [e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 1 of 15

aceAnalytrcal
wwwpacelabs.com
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1CO
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia(VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiafVEt.AP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 15

aceAnaVical
.pacolabs.com
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Lab ID Sample ID
92278575001 SBOC 1121314
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
{704}875-9092
SAMPLE ANALYTE COUNT
Analyles
Method
Analysts
Reported
Laboratory
EPA 16648
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA 9040
MLS
1
PASi-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 15

aceAnalyfrcal
wwvpacelabs.com
Project:
REF. SNIPES OIL
Pace Project No.:
92278575
Lab Sample ID
Client Sample ID
Method
Parameters
92278575001
SBOC 1121314
SM 2540D
Total Suspended ScAs
EPA 9040
pH
SUMMARY OF DETECTION
Result Units
48.4 mg1L
6.6 Std Units
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc,.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersviVie, NC 28078
(704)B75-9092
Report Limit Analyzed Qualifiers
10.0 12/08/15 14:36
0.10 12/08/1512:55 HS
Page 4 of 15

aceAnaVical
NM1 'v JlacahlbS.C=
r
E
PROJECT NARRATIVE
Project: REF, SNIPES OIL
Pace Project No.: 92278575
Method: EPA 1664B
Description: HEM, Oil and Grease
Client: S&ME- Greensboro
Date: December 16, 2015
Pace Analytical Services, lnc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 1664B All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 15

u aceAnaVical
! NM vp8calsts.=
PROJECT NARRATIVE
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: SWE - Greensboro
Date: December 16, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below,
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc., Page 6 of 15

aceAnalXical
ff www.pacelabs.com
1
PROJECT NARRATIVE
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Method: EPA 9040
Description: 9040 pH
Client: S&ME - Greensboro
Date: December 16, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersvHle. NC 28075
[phone]
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain-ef custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SBOC 1121314 (Lab ID. 92278575001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
Ad percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sampte:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 15

aceAnalytical
1 wmvpacelabs.com
f
ANALYTICAL RESULTS
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Pace Analytical Services, Inc.
9800 Kincey Ave- Suite 100
Huntersville, NC 25078
[phone]
Sample: SBOC 1/21314
Parameters
Lab ID: 92278575001 Collected: 12/04/1509:50
Results Units Report Limit DF
Received: 12/0411512:50 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
<5.0 mg1L
5.0
1
12/09115 06:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
48.4 mg1L
10.0
1
12/08115 14:36
9040 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units
0.10
1
12108/15 12:55 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1211612015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15

aceAnalylrcal
wmvpaculabs.com
t
Project: REF. SNIPES OIL
Pace Project No.: 92278575
CC Batch: GCSV123473
QC Batch Method: EPA 1664E
Associated Lab Samples: 92278575001
METHOD BLANK: 1623358
Associated Lab Samples: 92278575001
Parameter Units
Oil and Grease mglL
LABORATORY CONTROL SAMPLE: 1623359
Parameter Units
Oil and Grease mgli
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, NC 25078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
45.0 5.0 12/09/15 06:33
Spike 1_CS LCS % ReC
Conc. Result % Rec Limits Qualifiers
40 35,1 88 78-114
MATRIX SPIKE SAMPLE: 1623360
35219622001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mglL 4.2J 40 385 86 78-114
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/16/2015 04:28 PM without the written consent of Pace Analytical Services. Inc.. page 9 of 15

aceAnalyfical
w WYAypeceiab$. com
QUALITY CONTROL DATA
Project: REF. SNIPES OIL
Pace Project No : 92278575
QC Batch: WET141814 Analysis Method: SM 2540D
QC Balch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lap Samples: 92278575001
METHOD BLANK: 1622580 _ Matrix: Water
Associated Lab Samples: 92278575001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L <2.5 2 5 12108/15 14:33
LABORATORY CONTROL SAMPLE:
1622581
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1622582
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, Inc.
9800 Klncey Ave. Sulte 100
Huntersville, NO 28075
(7 04 )875-9 092
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 230 92 90-110
92278446001 Dup
Result Result RPD Qualifiers
ND <5,0
SAMPLE DUPLICATE: 1622583
92278585001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND 0.9
RPD Qualifiers
Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12M612015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

1�?ceAnalyfical"
wenv.pacalabs.com
Project: REF. SNIPES OIL
Pace Project No.: 92278575
OC Batch: WET141811
QC Batch Method: EPA 9040
Associated Lab Samples: 92278575001
SAMPLE DUPLICATE: 1622127
Parameter
Units
pH
Sid. Units
SAMPLE DUPLICATE, 1622128
Parameter
Units
pH
Sid. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description 9040 pH
92278455001 Dup
Result Result RPD Qualifiers
8.1 8.1 0 H6
92278377002 Dup
Result Result RPD Qualifiers
6.8 6.8 0 H6
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28D78
[phone]
Results presented on this page are In the units indicated by the: "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/16/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15

aceAnalyfical
wvnvpecefebs.cnm
f1
1
QUALIFIERS
Project: REF. SNIPES OIL
Pace Project No.: 92278575
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S. - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acroiein and Acrylonitrile by EPA
Method 6260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
Ti - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/16/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 15

aceAnalytical
wwwpaceln0.ccm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: REF. SNIPES OIL
Pace Project No.: 92278575
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huorlersvilie, NC 28075
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92278575001
SSOC 1121314
EPA 1664E
GCSV123473
92278575001
SBOC 1121314
SM 2540D
WET141814
92278575001
SBOC 1121314
EPA9040
WET141811
Date: 12/1612015 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 13 of 15

' aceAnal;�lsal�
Sample Condition Upon Receip4 (SCU
Document NUrnber.
- F-CHR-CS-003-rev.16.1
Pace 1 of 2*
lss0ig Authority,
Pace Huntersviile Quality Office
ent Name: ` . f'�l r-• ' Page 2 of 2 is for Internal Use Only
ler; Fed E>❑ UPC] USP❑ Clier❑ Commefci
❑ �—•—Pace Other .:..;;.; ...
:ody Seat on Cooler/Box Present: ❑ yes [ io Seals intact: ❑ yes �cr
Pra DUe`Da" te ;.
Proi,:,�.�ame
:ing Material: ❑ Bubble Wrap [D—Bubble Bags rJ ❑ None[] Other
mometer Used: IR Gun T1505 Type of [ce t Blue None E] Samptrss on Ice, cooling process has begun
n Correction Factor No Correction
ected Cooler Temp.: �`� r� C
should be above freezing to 8°C
Biological Tissue is Frozen: Yes No NIA Bate and Initials of person examining
contents:l„� • 41-! 5- 6.3
Comments:
n of Custody Present:
ZXoe-0N0
❑NrA
1.
n of Custody Filled Out:
IZ Yer-ONo
❑N'A
2.
In of Custody Relinquished:
[9•Y -sl0No
❑N/A
3.
pler Name & Signature on COG:
ELY6s- DNo
ONIA
4.
pies Arrived within Hold Time:
KlYft-ONo
❑N/A
5.
4 Hold Time Analysis <72hr :
[]Yes ❑No
❑N!A•
6.
h Turn Around Time Requested:
❑Yes []No
15N
7.
cient Volume:
OW—ss ❑No
El NIA
8.
ect Containers Used:
'ace Containers Used:
tl�.Yer"❑No
Ayes- ❑No
❑N/A
❑N1A
9.
:alnors Intact:
B Yrs-12No
❑NIA
10,
red volume received for Dissolved tests
❑Yes ❑No
UWA
11.
pie Labels match CDC:
ncludes dateltime0/Analysis Matrix:
QlYes—t]No
U'�Sy
0NIA
12.�0 O"rcL��tS�
ntalners needing preservation have been checked.
mtainers needing preservatfon are found to be In
rllance with EPA recommendation.
lions: VOA, coliform, TOC, 0$G, WI•DRO (water)
[]Yes ❑No
[]Yes ©No
❑Yes ©No
i3N
MNIA-
13,
iples checked for dechlorination,
❑Yes ❑No
EaWX
14.
dspace in VOA Vials (>8mm):
❑Yes ONO
lowic
15.
Blank Present:
Blank Custody Seals Present
e Trip Blank Lot # (if purchased):
❑Yes ❑No
©Yes ❑No
i
(9,4
B.
nt Notification/ Resolution: Field Data Required? Y 1 N
Person Contacted: DatelTime:
)mmentsl Resolution:
JRF Review: Date: i WO , 92270575
3RF Review:. Date:
te: Whenover there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Offce t i.e out of hold. Incorrect preservative, out of temp, 92278575
incorrect containers)
Page.14 of 15

���Art7f.7ifa1
Section A
Required Client Information.
Section B
Required Project Information:
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information:
to
rn
page : I Of t a
Company: SBME
Report To. WAYN= WATT ERSON
Aiteraan:
Address: 864G WEST MARKET STREET
Copy To 4-_i > �. 7- -i �� rJj i { .� U
c—Pany Name: �: t. J- f.�IF 0
SUITE 105, GREENSBORO, NC 27409
t
Address: r
RegulatorvA nc
Email'
Purchase Ordor k-.
Pane Ouole.
Phone: 1 .j EL( J1�� ?(,; y ax
Project Name: Ref. Snipes Oil
Pace Project Manager. taylor.ezell@0acelatts com.
- State J Location
Requesled Due pate:
Project x:
Pace Profile #:
R
uested
Analysis
Ftltered
IY1Nt
_
a
Z
Nw, Rix coD�
to
COLLECTED
z
Preservatives
r
N
p.uumg vher. LIN
YYa;t+ tYi
Cr
o
V
P.v P
SAMPLE ID � oL
One Character per box. Y+— :w
v
c7
START
END
a
N
o-
.P
^
-O
c
3'
°
/// �7
/
(A-Z. 0.9 r, ) Au AR
o
c.
m
W,
c
oq
V
v
2
Sample Ids must be unique 1-s s
x
TOATETIME
a+
o
�
O
c
G
~
E
a!
a
V
o
N
�
�
L
Q
_
-
r'
-
a
-
'n
¢
H
GATE
TIME
i
z
z
z
O
O
r
IL
1
"s
s
3
C, C,
r
4 s
! :
?�
5
t
s
r
a
s
10.
11
12.
_ AODITIONALCOMMENTS
RELINQUISHED BY I AFFILIATION
DATE-
TIME
- ACCEP7F[78T)AFFIUATIG. _
DATE
IiMr'
SAMPLE CONomons
let
cns
SAMPLER NAME AND 51GNATURE '
c
c
V
PRINT Nang o SAMPLER:
SCJL`L v
s
t`u
m m T
omo
a m o i
0-E y
SIGNATI#RE of 5 1fLER-
GATE Signed: / i f

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
CERTIFICATE OF COVERAGE NO. NCG08 080867 (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Snipes Brothers Oil Company COUNTY —Person—
PERSON COLLECTING SAMPLE(S)_Steve Barnwell �P,HQNR a'N36_) 227-8881
CERTIFIED LABORATORY(S) Pace Analytical Lab #_l t-- A�++
Lab # m 2 6 2015
SIGNATURE OF PERMITTEE OR DESIGNEE
CENTRAL FILES REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements DWR SECTION
OutfaI[
Date
50050
No.
Sample
Collected
Total
Flow (if app.)
Total
Rainfall
TPH, EPA
Method 1664
=
Total
Suspended
Solids
pH
moldd/yr
MG
inches
M /I
M /I
Standard units
Benchmark
15
100
6.0 — 9.0
001 (SBOC)
5/13/2015
NA
1
<5.0
25.1
s
(field
measurement
6.7
(laboratory)
Does this facility perform Vehicle Maintenance Activities using more than 5.5 gallons of new motor oil per month? _ yes _XX_no
(if yes, complete Part 13)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall.
No.
Date
Sample
Collected-
50050
00556
00530
00400
Total Flow'
(if"applicable)
Total
Rainfall -
Oil & Grease
(ifappl.)
Non -polar
O&G1TPH
(Method 1664 -
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
-Oil Usage
mo/dd/yr.
MG
inches
m =/I
nla/I
unit
gal/mo
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date _5/13/2015
Total Event Precipitation (inches): o
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of lave, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

F-1wi
NCD NR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: hUp_//oortaLncdunnorg/web/wct/ws/su/npdessw#tab-4
Permit No.: N/C/ 0 / 8 /0-/0-/0-/0-/0-/ or Certificate of Coverage No.: N/C/G/0-/8_/0-/8_/6-/7-/
Facility Name: Snipes Brothers Oil Company
County: Roxboro
Inspector; S4if t/P
Date of Inspection: S
Time of Inspection: / e?9 /a/-7
Total Event Precipitation (inches): I
Phone No. .s36 - a a -7 - ff)
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
X Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1. inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the perinittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
5WU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. dQ -1- ftru tun
Receiving Stream: 1)
Describe the industrial activities that
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: ('k kA-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): ✓iy 'i -e
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
(1 1 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 V 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 j 3 4 5
7. Is there any foam in the stormwater discharge"? Yes 0
8. is there an oil sheen in the stormwater discharge? Yes (9
9. Is there evidence of erosion or deposition at the Outfall? J No
10. Other Obvious Indicators of Stormwater Pollution: Ah
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5WU-242, Last modiried 10/25/2012

/5a'ceAnalyfical'
mvwpacWabs.com
May 21, 2015
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
RE: Project: Snipes Stormwater
Pace Project No.: 92250022
Dear Mr. Watterson:
Pace Analytical Services, InG.
9800 Kincey Ave. Suite 100
Mnlersville. NC 28078
[phone].
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
arqk
Angela Baioni
angela.bajoni@pacelabs,com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 15

aceAnalytical
—pacelabsxom
fI
i
Project: Snipes Stormwater
Pace Project No.: 92250022
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #; 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87548
Massachusetts Certiflcation #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 367
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 355
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fait,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 15

aceAnalytical
wwHpacelabs.com
SAMPLE ANALYTE COUNT
Project: Snipes Stormwater
Pace Project No.: 92250022
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 1o0
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92250022001 SII 1-4 EPA 1664B
CLW
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
MILS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 15

aceAnalytical
www pacelabs. MM
Project:
Snipes Stormwater
Pace Project No.:
92250022
Lab Sample ID
Client Sample Ifs
Method
Parameters
92250022001
SBOC 1-4
SM 2540D
Total Suspended Solids
EPA 9040
pH
SUMMARY OF DETECTION
Result Units
25.1 mg/L
67 Std. Units
REPORT OF LABORATORY ANALYSES
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. 5ulte 100
Huntersville, NC 28078
[phone]
Report Limit Analyzed Qualifiers
5.6 05/ 19115 21:26
0.10 05/19/1512:05 H3,1-16
Page 4 of 15

aceAnaiyitical
www.pacerabs.cam
1
Pace Analytical Services, Ine.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Snipes Stormwater
Pace Project No.: 92250022
Method: EPA 1664B
Description: 1664 SGT-HEM, TPH
Client: S&ME, Inc.
Date: May 21,2015
General Information:
1 sample was analyzed for EPA 16646, All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within OC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except fn full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 15

Pace Analytical Services, Inc.
Analytical"9840 Kincey Ave. Suite 144
/5a'ce Huntersville, INC 28478
f www.pacelabs,com [phone]t
i
PROJECT NARRATIVE
Project: Snipes Stormwater
Pace Project 1 92250022
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: SAME, Inc.
Date: May 21, 2015
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: WET137551
D6: The relative percent difference (i between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1463235)
• Total Suspended Solids
• DUP (Lab ID: 1463236)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,. Page 6 of 15

Pace Analytical Services, Inc.
aceAnalytical 9800 Kinsey Ave. Suite100
Huntersville, NC 28078078
www.pacalabs.com (704 )875-90 92
a
PROJECT NARRATIVE
Project: Snipes Stormwater
Pace Project No.: 92250022
Method: EPA 9040
Description: 9040 pH
Client: S&ME, Inc.
Date: May 21,2015
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1-13: Sample was received or analysis requested beyond the recognized method holding time.
• SBOC 1-4 (Lab ID: 92250022001)
1-16: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SBOC 1-4 (Lab ID: 92250022001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below,
QC Batch: WET137511
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1461395)
- pH
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 15

Pace Analytical Services, Ina.
/5a'ceAnalytFical ® 9600 Kincey Ave. Suite100
HuntersvilEe, NC 28075078
wwwpacelab3r vom (704)B75-909 2-
ANALYTICAL RESULTS
Project: Snipes Stormwater
Pace Project No.: 92250022
Sample: SSOC 1-4
Parameters
Lab ID: 92250022001 Collected: 05/13115 13:35
Results Units Report Limit DF
Received: 05/14/15 17:00 Matrix: Water
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, Till
Analytical Method: EPA 1664D
Total Petroteum Hydrocarbons
<5.0 mg/L
5 0 1
05/19/15 09:35
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
25.1 mg/L
5.6 1
05/19/15 21:26
9040 pH
Analytical Method: EPA 9040
pH
6.7 Std. Units
0.10 1
05/19/15 12:05 H3,H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/21/2015 07:50 PM without the written consent of Pace Analytical Services, Inc., Page 8 of 15

aceAnalytical
wwwpacClabB.tom
i
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-90 92-
Project: Snipes Stormwater
Pace Project No.: 92250022
QC Balch: GCSV121360
Analysis Method:
EPA 1664B
QC Balch Method: EPA 1664B
Analysis Description:
1654 SGT-HEM, TPH
Associated Lab Samples' 92250022001
METHOD BLANK: 1462119
Matrix: Water
Associated Lab Samples: 92250022001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mglL
<5.0 5.0 05/19/15 09:24
LABORATORY CONTROL SAMPLE: 1462120
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Totai Petroleum Hydrocarbons
mg1L
20 19.8
99 64-132
MATRIX SPIKE SAMPLE: 1462121
92249815001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 20
18.4 90 64-132
Results presented on this page are in the units indicated by the "Units" c0umn except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date'. 05/21/2015 07:50 PM without the written consent of Pace Analytical Services, 1nc,. Page 9 of 15

aceAnalytical
wu Pecelabs,com
QUALITY CONTROL DATA
Project: Snipes Stormwater
Pace Project No.: 92250022
QC Batch: WET137551 Analysis Method: SM 2540D
QC Batch Method SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92250022001
METHOD BLANK: 1463233 Matrix: Water
Associated Lab Samples: 92250022001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L <2.5 2.5 05/19/15 21:19
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-909--
LABORATORY CONTROL SAMPLE: 1463234
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 242 97 90-110
SAMPLE DUPLICATE: 1463235
92249629001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1t,
146
156 6 D6
SAMPLE DUPLICATE: 1463236
92249671002
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
17.2
21.2 21 D6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2015 07:50 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

aceAnalytical
QUALITY CONTROL DATA
Project: Snipes Stormwater
Pace Project No.: 92250022
QC Batch: WET137511 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92250022001
SAMPLE DUPLICATE: 1461395
92249561001 Dup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 6.8 5.4 23 D6,H3,H6
Pace Analytical Services, Inr..
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone].
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2015 0T50 PM without the written consent of Pace Analytical Services, Inc,.
Page 11 of 15

aceAnalytil 1.
wwwpi3coiabs.com
i
E
QUALIFIERS
Project: Snipes Stormwater
Pace Project No.. 92250022
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Humersville, NC 28078
(704)875-9l
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall nor be reproduced, except in full,
Date', 05/21/2015 07:50 PM without the written consent of Pace Analytical Services, Inc,. Page 12 of 15

aceAnalytical
www.pecelaAs.cnm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Snipes Stormwater
Pace Project 1 92250022
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-909-•
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92250022001
SBOC 1-4
EPA 1564B
GCSV121360
92250022001
SBOC 1-4
SM 2540D
WET137551
92250022001
SBOC 1-4
EPA 9040
WET137511
Date: 05121/2015 07:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 13 of 15

O
-PaceAnalyticaf
NWW.�2CGt2tIS.tpm
Section A
Required Client information:
CHAIN -OF -CUSTODY f Analytical Request Document
The Chaino',Custody is a LEGAL DOCUMENT. All relevant Melds must be completed accurately.
i 3. i /' r
Section 6 Section C ( �(�� Page: of
Required Project Information: n Invoice Information:
!.�' Repar7e: r1 •�P5 ! �� Q .c/� Attention:
5e-;. J
Email To: - lj -
Purchase Order Na.:
vzcc
Refe
Phonc��rlJl��i
)
Project Name:�''�
L
2S i
��� Yam"
gran
Requested Duo- Date lTAT:
Project Number. k
Pac
Section D Matrix Codes
_
RegelredCtwt information MATRW 1 cooE
Rs
COLLECTED
Drinking Water DIN
'^
OU
z
O
Water W7
$
U
Waste Water %W
—
y,�
OT
STARTExp�szca
���'�'
U
Product P
Soiasctid SL
t�7
p
SAMPLE ID °;1 OL
a
(A-Z, 4-91 : 1 Aire AR
w
v
Z
ID
Sample s MUST BE UNIOUE Tissue T S
O
LL
F-
Other OT
U
X
w
r
Z
O
p
1
t
S
a
a
LL
o
~
{
m
DATE
TIME
OATS I
TIME
to
Oc
4
: d REGULATORY AGENCY
NPOES GROUNDWATER - DRINKING WATER
UST - RGRA OTHER
v a�/7 ( site Location
3 le :a% L} STATE:
Requested Analysis Filtered( IN)
Preservatives >
ii
L
2 Z
a
fr Pace Project Nol Lab I.D-
ADORIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS
V
SAMPLER NAME AND S€GNATU RE
C. .;�, GNr.L y
CD PRINT Name of SAMPLER:
DATE Signed
p SIGNATURE of SAfrPLER: � jrrr111D D/YY): �,
Cn 'Impwan: Note: By signory :his form you am accep4r:y Pace's NET 30 day Vayn nt temss arid. 8greo" to Late charges a 1.5% pet m 10 for any knvpi= not paid M:tin. 30 cays_ 1
F-ALL-0-020rev.07, 15-May-2GO7 .

L to S l aBe �f?CQAl1�1)r(!Cc?!Q
Sample Condition Upon Receipt
Document Number:
F-CHR-CS-003-rev.15
Page 1 of 2
Issuing Authority:
Pace Huntersville Quality Office -
Client Name'. H
Courier: ❑ ed Ex ❑ UPS❑ LISPS❑ Client❑ ommerciad-11"Pace Other
Custody Seaton CoolerlBox Present: [Iyes [no Seals intact: ❑ yes ❑ no t �
Packing Material: ❑ Bubble v❑p ❑ BP64 Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ice: rWe't� Blue None ❑ SampEes on Ice, cooling process has begun
Temp Correction Factor TJAQ1 No Correction 1\ Jl
Corrected Cooler Temp.: �C
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No NIA
Comments:
Date and Initials of person ex i Ing
contents:
CWn of Custody Present:
PY05 ❑No
❑NIA
1.
Chain of Custody Filled Out:
es No
❑NIA
2,
Chain of Custody Relinquished:
Y ❑No
❑NIA
3.
Sam ler Name & Signature on COC:
❑ ONO
❑NIA
4.
Samples Arrived within Hold Time:
es ❑No
❑NIA
5.
Short Hold Time Analysis <72hr :
❑Yes 4N
❑NIA
6,
Rush Turn Around Time Requested:
OYe.5, No
❑NIA
7.
Sufficient Volume:
cr ©No
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
❑/eir ONO
OYjt ONO
❑NIA
❑NIA
g,
Containers Intact:
❑Yes ONO
❑NIA
10.
Filtered volume received for Dissolved tests
Dyes DNZ
❑NIA
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
Dyes N
❑NIA
r,Io
12. 1 ►lC
z
All contalners needing preservation have been checked,
All containers needing preservation are found to be in
complfance wilh EPA recommendatlon.
exceptions: VOA, coliform, FOC, o&G, W-DRO (water)
❑Yes ❑No
Dyes ONO
Dyes ONO
NIA
13.
Samples checked for dechlorination:
ClYes ONO
❑NIP:
14.
Headspace in VOA Vials >6mm):
Dyes ©No
❑NIA
15,
Trip Blank Present:
Trip Blank Custody Seals Present
Pace -Trip-Blank.Lct.#..If urchased
Dyes ONO
❑Yes ONO
❑NIPS
El NIA
16,
Cllent Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
-- Comments/ Resolution: ti- (')P ; 1 (y Lu l St.(.tC(A- _ r(--
.� "L�� XIC I_ -----
SC RF Revlew: ��]Date:
Date: rj - -�,5 Place label here
SRF Review: Zn C 1r_ OR
Note: Whenever there Is a discrepancy affecting North Caro{Ina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR Handwrite project number
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
{if no label available)
Incorrect containers)

Table #
Summary of Analytical Results - Water Samples
Snipes Stormwater
05/21 /2015 19:49
Facility ID# or NCDENR's Incident #
Analytical
Method
EPA
EPA9040
SM2540D
Total
Total
Petrole
Suspen
Constituent of Concern
um
pH
ded
Sample ID
Hydroc
Solids
arbons
Date
Sample
Std.
Collected
Depth
mg/L
Units
mg/L
(mm/dd/yyl
(ft. BGS)
SBOC 1-4
OS/13/2015
5.0
6.7
25.1
2L Class GA Standards
N/A
6.5-8.5
N/A
2L Class GSA Standards
NIA
6.5 - s.5
N/A
2L Class GCL Standards
N/A
N/A
N/A
NOTES:
ND = Not Detected
VPH = Volatile Petroleum Hydrocarbon - Massachusetts Department of Environmental Protection
EPH = Extractable Petroleum Hydrocarbon - Massachusetts Department of Environmental Protection
ft. BGS = feet below ground surface
mg/L = milligrams per liter
ug/L = micrograms per liter
Bold data above the MSCC (Soil to Groundwater)

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: http://portal.ncdennorg/web/wq/ws/su/nr2dessw#tab-4
Permit No.: N/C/ 0 / 8 /0_/0_/0_/0_/0_/ or Certificate of Coverage No.: N/C/C/0_/8_/0_/8_/6_/7_/
Facility Name: Snipes Brothers Oil Company
County: Roxboro
Inspector: -4--e U e rA vie I
Date of Inspection: `�151 1 q
Time of Inspection: /0 : 0 S Ai- Al
Total Event Precipitation (inches): L
Phone No
Was this a "Representative Storm Event" or "Measureable Storm Even i 0 by the permit?
(See information below.) ED
X Yes ❑ No
AUG 22 2014
CENTRAL FILES
Please verify whether Qualitative Monitoring must be performed during a "re$yI aI dive storm
event" or "measureable storm. even, 0' (requirements vary; depending.on-the-permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." however,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10'consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
i
By this signature, 1 certify that this report is acctkr�fe and complete to the best of my knowledge:
(Signature of Permittee or Designee)
. .....- . - -IiIf
Pagel of 2
5WU-242, Last modified 10/25/2012

X. Out aI Descrjption.
Outfall No. a Structure (pipe,„ditch, etc.) 2
Receiving Stream: �r : bt�-in r.' o f /L%(j/'�,f-�
Describe the industrial activities tha occur within the outfall dra
r
X^
2. Color: Describe the color of the dis/�barge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor; Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.)-. h e'Al
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 6 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
(9 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes 60
8. Is there an oil sheen in the stormwater discharge? Yes
• L�J
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution: / A" /0,A-(
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
_._
Page 2 of 2
SWU-242, Last modified 10/25/2012

Permit Number NCS NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 080867
FACILITY NAME Snipes Brothers Oil Company
PERSON COLLECTING SAMPLE(S) _Steve Barnwell
CERTIF[ED LABORATORY(S) _Pace Analytical
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
-Lab 412
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY _Person_
PHONE NO. (_336_) 227-8881
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfail
No. :ry
Date
Sample
Collected
50050
Total 7. ..
Flow (if app.)
Total
Rainfall
TPH, EPA
Method 1.664
Total
Suspended
Solids
pH
mo/dO,r
MG
inches
M /l
M /l
Standard units
Benchmark
15
100
6.0 — 9.0
001 (SBOC)
10/17/2014
NA
<5.0
19.2
D
(field
measurement
6.6
(laboratory)
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _XX_no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050'
00556
00530
00400
Total Flow.
(if applicable)
Total
Rainfall
Oil & Grease
(if app1.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
a I.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ -r
MG
inches
mg/1
mg/1
unit
al/mo
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date _10/17/2014
Total Event Precipitation (inches): ; , 11 7
Event Duration (hours): (only if applicable —see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: httu: //aortal.ncdenr.org/weblwg/ws/sii/nndessw#tab-4
Permit No.: N/C/ 0 / 8 /O-/0_/0_/0_/0_/ or Certificate of Coverage No.: N/C/G/0_/8_/0_/8-/6-/7-/
Facility Name: Snipes Brothers Oil Company
County: Roxboro
Inspector: -54
n
IV
Date of Inspection: d f /
Time of Inspection: /1 ; /S--
Total Event Precipitation (inches): • v 7
Phone No. 3.S C - a a -7 - 5 f' K
Was this a "Representative Storm Event" or "Measureable Storm Event' as defined by the permit?
(See information below.)
X Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Pagel of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. 00-- Structure (pipe, ditch, etc.) `M1
Receiving Stream: �. c /Z�4
Describe the industrial activities that/Occur within the outfall ainage area:
P�ld el 4 z!Nd
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: e lea.-^
3. Odor: Describe any distinct odors that the discharge may have (i,e., smells strongly of oil,
weak chlorine odor, etc.): 4y��
4. Clarity. Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy; �q
1 / Z} 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where
�1�is no solids and 5 is the surface covered with floating solids:
j 1j 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 V 3 4 5
7. Is there any foam in the stormwater discharge? Yes �o
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10, Other Obvious Indicators of Stormwater Pollution: Ne I e
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 22, 2014
Mr. Wayne Watterson
S&ME, Inc.
3718 Old Battleground Road
Greensboro, NC 27410
RE: Project: Snipes Oil
Pace Project No.: 92222103
Dear Mr. Watterson:
Enclosed are the analytical results for sample(s) received by the laboratory on October 20, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
�Q-pGCR&
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )87 5-9092
CERTIFICATIONS
Project: Snipes Oil
Pace Project No.: 92222103
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Caroiina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiafVELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
www.pacalabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, 128078
[phone]
Project: Snipes Oil
Pace Project 1 92222103
Lab ID Sample ID
92222103001 S1130C 1-4
SAMPLE ANALYTE COUNT
Method
Analysts
Analyses
Reported Laboratory
EPA 1664E
CLW
1 PASI-C
EPA 1664E
CLW
1 PASI-C
SM 2540D
TEP
1 PASI-A
EPA 9040
MAB
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 17

aoAnalytical
www,pecelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 16p
Huntersville, NC 28076
[phone]
SUMMARY OF DETECTION
Project: Snipes Oil
Pace Project No.: 92222103
Lab Sample ID Client Sample ID
Method Parameters Result Units
92222103001 SBOC 1-4
SM 2540D Total Suspended Solids 19.2 mg1L
EPA 9040 pH 6.6 Std. Units
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Report Limit Analyzed Qualifiers
10.0 10/21/14 06:13
0.10 10/2211413:45 H6
Page 4 of 17

aceAnalytical
..pacelabs.com
i
Pace Analytical Services, Inc.
9500 Kincey Ave Suite 100
Huntersville, NC 26078
[phone]
PROJECT NARRATIVE
Project: Snipes Oil
Pace Project No.: 92222103
Method: EPA 1664E
Description: HEM, Oil and Grease
Client: SWE, Inc.
Date: October 22. 2014
General Information:
1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below,
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,. Page 5 of 17

aceAnalytical
WWW.pecelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hintersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Snipes Oil
Pace Project 1 92222103
Method: EPA 1664B
Description: 1664 SGT-HEM, TPH
Client: SWE, Inc.
Date: October 22, 2014
General Information:
1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank,
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,. Page 6 of 17

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
aceAnalytrcal Huntersville, INC 28078
www.pacelabs.com [phone]
PROJECT NARRATIVE
Project: Snipes Oil
Pace Project No.: 92222103
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: S&ME, Inc.
Date: October 22, 2014
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc., Page 7 of 17

m
aoAnalj4ical
www.pacelabs.com
j
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 106
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Snipes Oil
Pace Project No.: 92222103
Method: EPA 9040
Description: 9040 pH
Client: S&ME, Inc.
Date: October 22, 2014
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
H6: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SBOC 1-4 (Lab ID: 92222103001)
Method Blank:
All analytes were below the report limit In the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the w(itlen consent of Pace Analytical Services, Inc.. Page 8 of 17

aceAnalytical
www.pamtabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Snipes Oil
Pace Project No.: 92222103
Sample: SBOC 1-4
Parameters
Lab ID: 92222103001 Collected: 10/17/14 11:14
Results Units Report Limit DF
Received: 10120/14 15:07 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
<5.0 mg/L
5.0 1
10/21/14 08:50
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
<5.0 mg1L
5.0 1
10/21/14 08:58
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
19.2 mg1L
10.0 1
10/21/14 06:13
9040 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units
0,10 1
10/22/14 13A5 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 17

aceAnall
www.pacalBbs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersvNe, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Snipes Oil
Pace Project No.: 92222103
QC Batch: GCSV119242 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92222103C01
METHOD BLANK: 1311267
Associated Lab Samples: 92222103001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 1311268
Parameter Units
Oil and Grease mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
<5.0 5.0 10/21/14 08:50
Spike LCS LCS % Rec
Conc, Result % Rec Limits Qualifiers
40 37.8 94 78-114
MATRIX SPIKE SAMPLE: 1311269
92222103001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L <5.0 40 36.6 92 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc,. Page 10 of 17

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Snipes Oil
Pace Project No.: 92222103
QC Batch: GCSV119243 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92222103001
METHOD BLANK: 1311274
Associated Lab Samples: 92222103001
Parameter Units
Total Petroleum Hydrocarbons mg/L
LABORATORY CONTROL SAMPLE: 1311275
Parameter Units
Total Petroleum Hydrocarbons mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
<5 0 5.0 10/21/14 08:50
Spike LCS LIDS % Rec
Conc. Result % Rec Limits Qualifiers
20 18.1 90 64-132
MATRIX SPIKE SAMPLE: 1311276
92222103001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L <5.0 20 16.9 84 64-132
Results presented on this page are in the units indicated by the "Units" column except whore an alternate unit is presented to the right of the rosu It.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 17

aceAnalytical
www.pacolabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Snipes Oil
Pace Project No.: 92222103
QC Batch: WET133840
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92222103001
METHOD BLANK: 1311233
Matrix: Water
Associated Lab Samples: 92222103C01
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids mg1L
<2.5 2.5 10/21/14 06:08
LABORATORY CONTROL SAMPLE: 1311234
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids mg/L
250 244
98 90-110
SAMPLE DUPLICATE: 1311235
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1311236
Parameter
Total Suspended Solids
92222108001 Dup
Units Result Result
mg1L 5.5 5.7
92222078001 Dup
Units Result Result
mglL 13.7 14.9
RPD Qualifiers
4
RPD Qualifiers
9
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc. Page 12 of 17

aceAnalytical
wwwpocalabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1 GO
Huntersville, NC 28078
[phone]
Project: Snipes Oil
Pace Project No.: 92222103
QC Batch: VVET133868
QC Batch Method: EPA 9040
Associated Lab Samples: 92222103001
SAMPLE DUPLICATE: 1312282
Parameter Units
pH
Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
92222103001 Dup
Result Result RPD
6.6 6.7
Qualifiers
1 H6
Results presented on this page ore in the units indicated by the "Units" column except whore an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 17

lac e A na lytica l m
wwwpacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )87 5-9 092
QUALIFIERS
Project: Snipes Oil
Pace Project No.. 92222103
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantltation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2014 03:57 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 17

_ �aceAnalytical
wwwpacelabs.com
Pace Analytical Services, Inc.
9800 KnceyAve. Suite 100
Nuntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Snipes Oil
Pace Project No.: 92222103
Lab ID
Sample ID
QC Batch Method
QC Batch
92222103001
SBOC 1-4
EPA 1664B
GCSV119242
92222103001
SBOC 1-4
EPA 1664B
GCSV119243
92222103001
SBOC 1-4
SM 2540D
WETI33840
92222103001
SBOC 1-4
EPA 9040
WETI33868
Date: 10/22/2014 03:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical Method
Analytical
Batch
Page 15 of 17

�__U,OoAnapixf*
Sample Condition Upon Receipt Scu
Document Number:
F-CHR-CS-003-rev.15
Issuing Authority:
ce Huntersville Quality Office
Client Name: S y M E
Courier: ❑ Fed Ex ❑ UPS❑ USPU Client❑ Commercial❑ ace they
Custody Seal on Cooler/Box Present: ❑ yes 12 no Seals Intact: ❑ yes ❑ no
Packing Material: [r]Bubble VE)p Bubble Bags ❑ None ❑ Other
Thermometer Used:• IR (3un T1 Type of.lc Wet Blue None sample; on Ice, cooling process has begun
Temp Correction Factor T1401 No Correction
r Data and Initials of person examining
Co
rrected Cooler Temp,: 3. 7 'C Biological Tissue is Frozen: Yes No contents: to 01np r _� _
Temp should be above freezing to,F'C _ Comments:
Chain of Custody Present: C�fes ONO ❑NIA 1.
Chain.of Custody Filled Out: , ti es 4L� ❑NIA 2. J�?ti r-, Q, t 5 ,�5 ,.na, r 1cA,•(.
Chain of CustodZ Relinquished:
ONO
❑N/A
3,
Sampler Name & Signature on COC:
�D�
Ares ONO
❑NtA
4.
= 0
Samples Arrived within Hold Time:
CKe�s ONO
❑NrA
5.
Z r U & CG
Short Hold Time Anaiysls (<72hr):
❑Yes 260
❑NIA
6.
Rush Turn Around Time Requested:
©Yes
No
❑NrA
7, H r )'
Sufficient Volume:
C<11
❑No
❑NIA
$,
Correct Containers Used:
Kees
ONO
❑NIA
9,
-Pace Containers Used:
C!I`Yes
ON,
❑NIA
Containers Intact:
We
ONO
❑NIA
10.
Filtered volurnejereived for Dissolved tests . Dyes ONo �A: 11,
Sample Labels match COC: r Dyes B o ❑NtA. 12. �^11 60 t'k'�� frrt,�A 5q _
3�} tL i Pcrie 54 i
-includes dateltimellDlAnalysis Matrix: 1A10f ky—
�1Ia G)ntbhler3,naCiLsig l„Lw,crva;ion ha.^ �^sn checked. I JYe s ON 12flIA I13.'
All containers needing preservation are IQWLL: 10 be in Dyes ❑No eiN1A
compliance with EPA recommendation..
exceptluns; VOA, colilorm, TOC, 0&G, W-DRO (water) EW,, , El No
I IS'
fi Iq
Samples checked for dechlorination: ❑Yes ONO L�4A 14.
Heads ace in VOA Vials >6mm ; - Dyes, ©No ON/16 15.
Trip Blank Present: Dyes ❑No NIA 16.
Trip Brink Custody Seals Present Dyes ONO OtIlA
Pace Trip Blank Lot # (i(purchased):
Client Notification! Field Data Required? Y I N
Person Contacted: DatelTime:
Comments/ Resolution: l) i) • c 1 C i ALy
�� ') [.� °) j 75�
_..- - -- - --T—�
[ r ,n t , U n .Y s <:a=;-i✓-, i• id"-�}....". l,iv�-rli-/'�=I
SCURF Review: HI- ' Date: l i
SRF Review: �t Date: `Ol�L1 �� �� ' ..9222 ' 1.0'
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina 0EHNR Ili! ill! ililililllllljlililij
Certificakian Office (3.e out of ho d, incorrect preservative, out of temp, 922�2iO3 ;"
Incorrect containers)
Page 16 of 17

I —
CHAIN -OF -CUSTODY / Analytical Request Document o
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must bo completed accurately. r
aceAnalytical'
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Section A _ ! G—�- `� � Section 8 Section G
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Company Report To: Attention:
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Address:
Copy To:
Company Name:
- -
REGULATORY.AGENCY
Address:
i NPDES i GROUNDWATER ! DRINKING WATER
"' UST = RCRA - OTHER
Err a I To:Pwphse
Order No.:
Pxa clwte
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Phone. 4.
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Name: -
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STATE:
Requested Due Date1TAT:
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Paco Pile iJ: L-1 kJ-
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