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Home My WebLink AboutNCG080828_MONITORING INFO_20190104STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT N0. iC�� DOC TYPE. ❑HISTORICAL FILE � MONITORING REPORTS DOC DATE ❑ I I 0 I D y YYYYMMDD r Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted January 4, 2019 CERTIFICATE OF COVERAGE NO. NCG08_0_ _8_ _2_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2018 RECSAMPLE PERIOD ❑ Jan -June ® July -Dec EIVED or ❑ Monthly( _(month JAN I ODIU CHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA jj ❑Zero -flow ❑Water Supply ❑SA CENTF AL FILES ®Other C, SW DVVR S=C71ON -- PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfa l l No: Date- Sample Collected, n,o/ad/yr 00530; - .. = s 00400 Total Suspended Solids, mg/L _- pH; _ = ,Standard units Non�P,olar Oil"and'G er ase/TPfiEPA Method�1664�(SGT HEM)mg%L New MotorOil"Usage, : Anrsual average:gal/mo Benthmark - h 50 or l0p.see permit:' = Within 6 0 9"0 i -15 _ 001 12/16/18 3.6 7.0 <2.70 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample.Collected, Trio/dd/yr 00556 . 1 _:41 rrR ~ „"£':' 0053D .,r. 00400 Non -Polar 0il,and Grease/TPH EPP�Method 1664 (SGT-HEM); mg/L � 1 Total Suspended 5ol�ds T; g. mg/L pH, Standar&units Permit Limit5fl,o�$100`see�pei=rnit s, 6.0 - 9 0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page I of 2 STORM EVENT CHARACTERISTICS: Date _12/16/18 (first event sampled) Total Event Precipitation (inches): _1.0_ Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of recei t of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wca/ws/su/npdessw#tab-4 SWU-250 last revised April 1 1.2013 Page 2 of 2 e"=kk ft FW�CO Labordton"es- 20 Acci:raie. Timely. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, December 31, 2018 Republic Services of NC (RE014) Attn: David Lawson 2477 Hwy 301 North Dunn, NC 28334 RE: Laboratory Results for Project Number: [none], Project Name/Desc: RWS-Dunn ENCO Workorder(s): CB19973 Dear David Lawson, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, December 18, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL. This report relates only to me sample as received by the laboratory, and may only be reproduced in full. J Page 1 of 7 ElC vrAwencolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: oatfall 1 Lab ID: C019973-01 Sampled: 12/16/18 14:30 Received: 12118/18 13:45 PaWmete PregAratlon Hold DatelTlmefsl Prep DatelTimeW Analysis D m EPA 1664A EPA 1664A 01/13/19 12/26/18 14:14 12/26/18 15:50 Feld NO PREP 12/16/18 14:44 12/16/18 14:30 12/16/18 14:30 SM 2540a2011 NO PREP 12/23/18 12/19/18 10:13 12/19/18 10:13 FINAL This report relates only to the Sample as received by the laboratory, and may only be reproduced In toll. Page 2 of 7 (��C-o www.eneciabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 1 Lab ID: C819973-01 Analxts Results Eta MP1 PQL unith Method tlst� pH Total Suspended Solids 7.0 0.0 0.0 pH Units Feld 3.6 3.6 3.6 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 Of 7 CE Nkkkk,co www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CB19973-01 Received: 12/18/18 13:45 Matrix: Surface Water Sampled:12/16/18 14:30 Work Order: CB19973 Project: RWS-Dunn Sampled By: CLIENT JClassical Chemistry Parameters ^ - ENR7 Cary -rtfied anelyte INC 5911 Analyte ICAS Numberl Results fiq Units pE Mph E46 Batch Method Analyzed Ng;es Total Suspended solids^ 3.6 mg/L 1.43 3.6 3.6 BL19002 SM 2540D-2011 12/19/18 10:13 OMR Field Parameters Analyte 1CAS Numberl Resin fin Units 2E M2L E" @8.t.ffi Method Analyzed lilt Notes pH 7.0 pH Units 1 0.0 0.0 81.19005 Feld 12/16/18 14:30 CL1 Classical Chemistry Parameters Anande ICAS Numbed Oil N Grease (HEM-SGT) Non -Polar Material Results Flee VA:& PIE MU E L Allch Method Analyzed Bit Notes 2.70 U rrg/t 1 2.70 5.00 BL26014 EPA 1664A 12/26/18 15:50 5MA FINAL This repot relates only to the sample as received by the laboratory, and may only he reproduEed In full. Page 4 Of 7 CIE.NCO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 8119002 - NO PREP Blank (BL19002-BLK3) Prepared & Analyzed: 12/19/2018 10:13 Spike Source %REC RPD Anaiyte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended SoWs 2.5 U 2.5 mg/L LCS (BL39002-BS3) Prepared & Analyzed: 12/19/2018 10:13 Spike Source %REC RPD .Anaiyte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 94 2.5 mg/L 100 94 80-120 Duplicate (BL19002-DUPl) Prepared & Analyzed: 12/19/2018 10:13 Source: CB13613-01 Spike Source %REC RPD AMIVte Result Flau POL Units Level Resutt %REC urnt RPD LIM11 Notes Total Suspended Solids 140 42 mg/L 140 1 20 Duplicate (BL19002-DUP2) Prepared & Analyzed: 12/19/2018 10:13 Source: C816866-01 Spike Source %REC RPD Analyte Result Flaw PQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 100 33 mg/L 100 0 20 Classical Chemistry Parameters - Quality Control Batch SL25014 - EPA 1664E Blank (BL26014-BLKS) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source %REC RPD .Analyte Result Flag POL Units Level Resul %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (8L26014-BSI) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 80.0 5.00 mg/L 81.6 98 64-132 LCS Dup (BL26014-BSDi) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:50 Spike Source °/uREC RPD Analyte Result Flau PQL Units Level Result %REC Limits RPD 1j11111; Notes Oil & Grease (HEM-SGT) Non -Polar Material 73.6 5.00 mg/L 80.0 92 64-132 8 34 Matrix Spike (BL26014-MSI) Prepared: 12/26/2018 14:14 Analyzed: 12/26/2018 15:S0 Source: C819973-01 Spike Source %REC RPD Analvte Result Flag PM units Level Result %REC Limits RPD Lima Notes Oil & Grease (HEM-SGT) Non -Polar Material 77.9 5.00 mg/L B5.1 2.70 U 92 64-132 FINAL Thks report relates only to the Sample as received by the laboratory, and may only be reproduced in full. I Page 5 of ! CC-== www.encolabs.com FLAGS/NOTES AND DEFINITIONS 8 The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit, The MRL is roughly equivalent to the practical quandtation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. 7-1 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7 10775 Central Paft or. 4810 ExeanWe Park Court, suite s 11 102-A Woodwinds Indusiria3 G. - Odando, FL 32824 JackSormile, FL 32216-6069 Cary, NO 27511 _ .. (407) 628-5314 Fax (407) 8W-69•t5 (904) 29G3007 Fax (904) 296•6210 (919) 467-3090 Fax (919) 4674515 Page of 0 Diem Name' Project Numder - - Railuesie6 Metlraea Requested iilmar0 Repubi Ic Servimsoft =0i4; Times ' Address- . r - - Project Nama/Dasc Nate :Rush requests subje CM 2.47?.H -• 301 Nnrth ..RWS-DLriri accep:ante by to tanl'u - CO CityfSTiLp' _ PO I ! swing Into - -- -. •. _ .+ -:,. - ... (Dunn .NC 28334 2015: BP04813i83 Standard Tel (910) 891-4461 David L-awson Q p i _ Expedited Samplers) Name, Affiliation (Print) BidContact Canta IN David Lawson �. Due Samplers) Signature Site Location/Time Zone. V) 0 (` CA - - -- Preservation (See Codes) (Combine as necessary) - coeec7lon Maotx Totals or Item x $ample ID (Field Identifilation) Collection Da.a^ Time Comp! Grab (sea codes) � Cdnitiiners Sample Comments av!- 1l 1z: t6-lid Z3o ��qb t 701 1 / I I <-- Total it of nnntainnm Sampie 4 Prepared By Data!t-xne Relinquished Daterilme Rec By Datamme Comments/Sp;&W Reporting Requirements Relinqu' B Datefilme R6ceived By - Oatamme - t Re"u6RedBy. -- -. - DateMms ii -\ BY DweRme ' - r" - Cooler ss 8 Temps on Receipt !i�/t pan Receipt f, lGandman Acceptable Unacceptable Matrix: GW-Grounctwater SV-Soil ow-Unnking Water 6E-Sediment SW-SurtaCe Water WW-Waste'YY81er A -Air O-Utner (datall In Comments) PrtferYatlen: HCe M•ML:I N•HNU3 5•hr2SU4 NU-I'taUM V-kMvr taerau in Wmmant.9) Note : Art samples submitted to £NCO Labs are .n accordance with the terms and conditions listed on the reverse of this form. uniess prior written agreements exist • a Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted July 6, 2018 CERTIFICATE OF COVERAGE NO. NCG08_0_ _$_ _2_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett RECEIVED PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 JUL 13 2018 Comments on sample collection or analysis: , �S CENTI��:I_ i-1�.�� n�nJrR- SECT10^:' SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ®Other C SW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) no ® No discharge this period' Outfall : No. Date Sample Collected, : mo/drl/yr= - 00530 _ . 00400 TotalSuspended- -. :Solids :m , g/ Stan l rd units _ ;: - d. _:. Non Palar?Oili.arid�Grease/TPH=EPA; =M L .. ethod 1064 (SGTsHEM),Amg/_ ._:_ OiIFUsage, . _.Annualrayera u ge gal/mo Benchmark -. z3 t Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) Outfall. No. Date Sample Collected, _' mo/dd/yr 00556 300530��.:°- 00400. Non. -Polar Oil and+Grease%TPH, EP*,Method ^ s r T664-(SGT-HEM) iiig/L "'*Fj' �TotalaSus ended,Solids p A j�A p H; Standard units Permit Limit ' _. - 5 f . ..� _ ,:50lort100'see�permrt>._ �6.0 — 9:0 , ... I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date (first event sampled) Total Event Precipitation (inches): Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, i_ncludina all "No Discharge" reports, within 30 days of receipt of the lab results at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sign ifica �alties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted January 2, 2018 CERTIFICATE OF COVERAGE NO. NCG08_0_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' month ®�r pj\, RC&RGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ii !! �r'' ❑Zero -flow ❑Water Supply ❑SA JAN 1 9-2018 ®Other C, SW _. DWR SECTION INFORMATION PROCESSING UNIT PLEASE REMEMBER TO SIGN ON THE REVERSE --> Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) no No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400' - 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Wand Grease/TPH,EPA =, Method-1664 (SGT-HEM), mg/L New Motor Oil Usage, . Annuahaverage gal/mo Benchmark - 50 or 100 see permit _ Within 6.0 - 9.0 =- _ • .. _ 151 001 12/11/2017 <2.5 6.2 9.73 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH.EPA Method 1664 (SGT=HEM), mg/L Total Suspended Solids, pH, Standard units Permit Limit - 15 50 or 100'see•permit 6.0 — 9.0 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Pagel of 2 STORM EVENT CHARACTERISTICS: Date _12/11/17 (first event sampled) Total Event Precipitation (inches): 2.0 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitorin-q period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant.penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw##tab-4 SWU-250 last revised April 11, 2013 Page 2.of 2 NCO Laborato s Accurate. Timely. Responsive. Innovative. 202-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, December 22, 2017 Republic Services of NC (RE014) Attn. David Lawson 2477 Hwy 301 North Dunn, NC 28334 RE: Laboratory Results for Project Number: [none], Project Name/Desc: RWS-Dunn ENCO Workorder(s): CA08174 Dear David Lawson, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, December 13, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Ila q-1-00 Stephanie Franz Project Manager Enclosure(s) FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In Full. Page 1 of 8 r�uL= o www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall 1 Lab ID: CA08174-01 Sampled: 12/11/17 15:00 Received: 12/13/17 09:30 71 Parameter Preparation Hold Date/Time(s) PreR Date/Tjmefsl Analysis Date/Timefsl EPA 1564A EPA 1664A 01/06/18 12/19/17 11:55 12/20/17 15:52 SM 25400-1997 NO PREP 12/18/17 12/18/17 17:55 12/18/17 17:55 SM 4500H+®-2000 NO PREP 12/11/17 15:14 12/21/17 10:49 12/21/17 10:49 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 2 Of �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfali 1 Lab ID: CA08174-01 Analvte Results Flag MQ6 E" Units Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 9.73 2.70 5.00 mg/L EPA 1664A pH 6.2 1.0 1.0 pH SM 4500H+B-2000 Q-01 Temperature for pH (deg. C) 23 pH SM 4500H+B-2000 Q-01 PINAL rhfS report relates only to the sample as received by the laboratory, and may only be reproduced in fullI Page 3 Of ENCO www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CA08174-01 Received: 12/13/17 09:30 Matrix: Surface Water Sampled:12/11/17 15:00 Work Order: CA08174 Project: RWS-Dunn Sampled By: David Lawson Classical Chemistry Parameters J - svC17 01y --V&d arslyre (AC sir] Ag1yte_ICAS Number l Results f1m Units RE 11P1 M ftub Method Analyzed (1y Notes pHA 6.2 pH 1 1.0 1.0 71-210113 ;M4500H+B-200[ 12121/1710:49 MKS Q-Ol Temperature for pH (deg. C) 23 pH 1 71-21018 3M 4500H+B-200[ 12/21/17 10:49 MKS Q-Ol Total Suspended SolidsA 2.5 U mg/L 1 2.5 2.5 7L18016 SM 254OD-1997 12/18/17 17:55 OMR LP-02 Classical Chemistry Parameters Analyte rCAS Numberl Results fin Units RE IJ�DL M Mch Method Analyzed ft Notes Oil & Grease (HEM-SGT) Non -Polar 9.73 rl 1 2.70 5.00 7L19006 EPA 1664A 12/20/17 15:52 SMA Material FINAL This report relates only to the sample as recelved by the laboratory, and may only be reproduced In full. Page 4 Of S 0EmmNkq www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Balm 7LI8016 - NO PREP Blank (71-18016-BLKI) Prepared & Analyzed: 12/18/2017 17:55 Spike Source %REC RPD Analyte Result Flaa POL Units Level Resu1S %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7LI6016-BS1) Prepared & Analyzed: 12/18/2017 17:55 Spike Source %REC RPD jvmh to Result Flag POL units Level Result %REC Limits RPD Limft Notes Total Suspended Solids 86 2.5 mg/L 100 86 80-170 Duplicate (71-18016-DU131) Prepared & Analyzed: 12/18/2D17 17:55 Source: CA16550-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 740 100 mg/L 700 5 20 Duplicate (7L18016-DUP2) Prepared & Analyzed: 12/18/2017 17:55 Source: CA16621-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Resin %REC Limits RPD Limit Notes Total Suspended Solids 70 50 mg/L 82 16 20 Balch 7L21O18 - NO PREP LCS (7L21018-BSI) Prepared & Analyzed: 12/21/2017 10:49 Spike Source %REC RPD -AnalNto Result Ela9 QOL Units Level Result %REC Limits RPD Limit Notes PH 7.0 1.0 pH 6.98 10D 99-101 Duplicate (7L21018-DUP1) Prepared & Analyzed: 12/21/2017 10:49 Source: CA08174-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes - pH 6.2 1.0 pH 6.2 0 25 Classical Chemistry Parameters - Quality Control Blank (7LI9006-BLKI) Prepared: 12/19/2017 11:55 Analyzed: 12/20/2017 15:52 Spike Source %REC RPD Analvte Result Rao POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (7L19006-BSI) Prepared: 12/19/2017 11:55 Analyzed: 12/20/2017 15:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result °/ REC Limits RPD Limit Notes Oil & Grease (HEM-SG1) Non -Polar Material 81.9 5.00 mg/L 92.6 88 64-132 LCS Dup (7L19006-BSDl) Prepared: 12/19/2017 11:55 Analyzed: 12/20/2017 15:52 Spike Source %REC RPD Analide Result Ela9 P91 Units Level gesul %REC LimiRPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 85.6 5.00 mg/L 92.6 92 64-132 4 34 FINAL This report relates only to the sample as receNed by the laboratory, and may Only be reproduced in full. Page 5 Of S �Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Oaft* 7L19006 - EPA 16"D - Continued Matrix Spike (71-14006-1VIS1) Prepared: 12/19/2017 11:55 Analyzed: 12/20/2017 15:52 Source: BA05307-01 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Umits RPD Limit Motes Oil & Grease (HEM-SGT) Non -Polar Material 23.3 5.00 mg/L 75.2 2,70 U 31 64-132 QM-07 FINAL This repot relates onty to the sample as receNed by the laboratory, and may ony be reproduced in fulf. Page 6 of $ �uco www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank, D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. LP-02 Less than 1000 ml of sample filtered and residue range of 2.5-200 mg was not met. Due to insufficient sample, analysis cannot be repeated. Q-01 Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 8 ",iV11'1V111YlLI�rI'\L yy1VJV111f1liVIV'f.!\VVrlf'Ir VfIILY Yllr-111 V-y1'-YVMIYVI fFLV V11✓ 10775 Central Port Dr. 4810 Executive Park Court, Suite 1 i I 102•A Woodwinds ind'1StfW Ct. Ortando, FL 32824 Jacksorrotte. FL 32216-6069 Cary, NC 27511 (407)825,5314 Fax4407)85Q-6945 {90412963087 Fax(904)296-6210 - (919)467.3090 Fax(919)467-3515 Chord Name - r r E Project Number - Requested Analyses � r. 0 0 � �. . Address 77 Hvvy 301 Nil h Pro;ec NamafOesa City/sT2ip - - - -- Dunn NC 28WA PO t-! Billing Into 2015: BP04813783 TEO Fats - _ 91 01391-4461 Reporting Contact David Lawson '^ er(s) Name, Affiliation (Print) 1 �4o56n Z Bi19ng Contact � David Lawson Sampler( s- nature Site LoCation % Time Zi7ne . - - Presmalian (See Codes) (Coinbne as recassa+ item A - Sample 1D (F1eld Identiticalienl Collecwxi Data Covectior. Time - - - Cgrrip r Grab Matrix (see copes) ' - Teal t of - ewmwiriwo - C u rl I 12-�t-17 3_Pn. C�Sw 4 X <-- Total tE of Containers ri ri rnt•GtttVIPU7.Lanl1 Page of 00 Requested Turnarour o Times co to Nate :Rush requests siAect� aCCeptarxo by the te0lity d _ Standard _ Expedited Due -ab Workorder CA08114 Samole Comments Sample Kit Prepared By Datetrime i Relinquished By Data7ime Rece By Daierl'ime - Comments/Special Reporting Requirements Relinquished By - Datefrmse Rocei ed By `` DetwTime " • - - - - Relinquished By - DaleTrime Received By Dat&Trrrle r -,� ITIisB Te Ps on Receipt C.� Camd+-A :[on' Receipt , [/ Acceptable Unacceptable Matrix;GW-Grounewator SO -Sod DWAnnking Water SE-Sertrment SW,Surtace Water WW-Wastmrater A•Air O-CWwIdetiul v comments) Prese"allen_Hce R-HCi N-HNO3 S•H2SD4 NO-NaOH O-Other(detad in corrmwrus) Note : Ail samples submitted to ENCO labs are in a=rclw= with the terms and conditions listed on the reverse of Mrs ;arm, unless prior written agreements exist ' Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted May 9, 2017 CERTIFICATE OF COVERAGE NO. N0008_0_ _8_ _2_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' (month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow ❑Water Supply ❑SA ®other C SW MAY 1 5 Z017 CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended' Solids; mg/L pH - Standard units " . Non -;Polar Oil`and°Grease/:TPH'.EPA Methodlfifi4 (SGL'HEM) rrig/L- New Motor Oil Usage,. - Annual avers ge.gal/mo Benchmark - 50-or"100 see permit Within 6 0 - 970- 001 04/27/2017 <2.5 7.29 <2.70 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample -.Collected; mo/dd/yr 00556 00530 "` 00400 " . Non=Polar'Oil and--Grease/TPH EPA Method- 1fifi4 {SGT.`HEM),"mg/L . Total Suspended 5olids,` ;mg : _ __`, __ pH; Standard units Permit Limit - . 15 SQor 1UO set permit= - 6:0:— 9:0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11.2013 Pagel of 2 STORM EVENT CHARACTERISTICS: Date _04/27/17 (first event sampled) Total Event Precipitation (inches): 4.5 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of lab results (or_ at end of monitoring period in the case of "No Discharge" Eeeeortsl ta: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) '%•el :1l (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/"wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 NCO Laboratories Ir, �Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, May 9, 2017 Republic Services of NC (RE014) Attn: Matt Einsmann 5111 Chin Page Rd Durham, NC 27703 RE: Laboratory Results for Project Number: [none], Project Name/Desc: RWS-Dunn ENCO Workorder(s): CZ17872 Dear Matt Einsmann, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, April 28, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as recelved by the laboratory, and may only be reproduced In full. I page 1 of 8 CS uco www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: OutFallI Lab ID: CZ17872-01 Sampled: 04/27/17 08:00 Received: 04/28/17 D9:30 Parameter Hold Date/Ttme(s) Prep Date/Timefs) Analysis DatelTime(s) EPA 1664A 05/25/17 05/03/17 12:19 05/04/17 16:42 Field 04/27/17 08:14 G4127/17 08:00 04/27/17 08:00 SM 254OD-1997 05/04/17 05/02/17 14:10 05/02/37 14:10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full Page 2 Of 8 CeN0 0) www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 1 Lab ID: CZ17872-01 AnalM Results fkg Mph Em Units Method i�4Sti pH 7.29 0 0 pH Units Field FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 3 o H �V ow wlr www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CZ17872-01 Received: 04/28/17 09:30 Matrix: Surface Water Sampled:04/27/17 08:00 Work Order: CZ17872 Project: RWS-Dunn Sampled By.David Lawson (Classical Chemistry Parameters ' ^ - &VC0 C ry mtnfed analy[e (AfC S911 Analyle [CAS Numbed Bgsults EkQ units DIE MDL Ea A115t MetbQQ Analyzed ft N Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 7E02008 SM 254OD-1997 05/02/17 14:10 OMR LP-02 Field Parameters Analyte fCAS Numberl ResulfC Bg 1lnits pE = E" match Method Analyzed fy Noces pH 7.29 pH Units 1 0 0 7EO1013 Feld 04/27/17 08:00 CLI Classical Chemistry Parameters Analyte ICAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material Resultf Flag units PE MDL M Batch Method Analyzed BY Notes 2.70 U mg/L 1 2.70 5.00 7F03009 EPA 1664A 05/04/17 16:42 SMA FINAL This report relates only to the sample as rmelved try the laboratory, and may only be reproduced In full. I Page. 4 01 U (9 �e 0 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Ba" 7EO200B - NO PREP Blank (7EO2008-BLK1) Prepared & Analyzed: 05/02/2017 14:10 Spike Source %REC RPD Ar lvte Result Flaq POL Units Level Result %REC Li i RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7E02008-BS1) Prepared & Analyzed: 05/02/2017 14:10 Spike Source 0/6REC RPD -ADi1l Result Elan PAX Units Level Resull %REC Limits RPD Limit Notes Total Suspended Solids 99 2.5 mg/L 100 99 80-120 Duplicate (7EO2008-DUPi) Prepared & Analyzed: 05/02/2017 14:10 Source: CA03275-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 110 25 mg/L 100 8 20 Duplicate (7EO2008-DUP2) Prepared & Analyzed: 05/02/2017 14:10 Source: CA03392-01 Spike Source %REC RPD Analyze Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 34 17 mg/L 43 24 20 QM-12 Classical Chemistry Parameters - Quality Control Bahclh 7ffi30LV - EPA 1664H Blank (7E03009-811-11(l) Prepared: 05/03/2017 12:19 Analyzed: 05/04/2017 16:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limi Notes Oil & Grease (HEM-SGT) Nor lar Material 2.70 U 5.00 ml LCS (7EO3009-BS1) Prepared: 05/03/2017 12:19 Analyzed: 05/04/2017 16:42 Spike Source %REC RPD Anal vte Result FIM POL Uni Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 71,0 5.00 mg/L 79.4 90 64-132 LCS Dup (7EO3009-BSDI) Prepared; 05/03/2017 12;19 Analyzed: 05/04/2017 16:42 Spike Source %REC RPD Analyte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 75.1 5,00 mg/L 76.6 98 64-132 6 34 Matrix Spike (7EO3009-MSl) Prepared: 05/03/2017 12:19 Analyzed: 05/04/2017 16:42 Source: CZ17872-01 Spike Source %REC RPD Analyze Result Flaq POL Units Level Result %REC Limits RPD M 111 Notes Oil & Grease (HEM-SGT) Non -Polar Material 63.6 5.00 mg/L 84.7 2.70 U 75 64-132 rINAL This report relates only to the sample as recelved by the laboratory, and may only be reproduced in full. I Page 5 Of eN' www.encolabs.com FLAGS/NOTES AND DEFINITIONS 8 The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. LP-02 Less than 1000 ml of sample filtered and residue range of 2.5-200 mg was not met. Due to insufficient sample, analysis cannot be repeated. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the Sample as received by the laboratory, and may only be reproduced in full. I Page 6 of -� /�.`..•rrrVl♦PIVr\'1!\L�+Vi\JLIlYJ1!l�IE��NUV[1MIVRIG.7 4r'E1"1,1ri�Vr'LrV�IVUi 11C{.V11iJ - i (Ms� 10775 Conical Pod Dr. 4811) ExQO*vQ Park Court- Suits 111 tw-A Woodwumis indusinal Q. \` —Orlando, FL 32824 Jack\orm le, FL s2i'.1&-6%9 Cary. NC 27511 (407) 828.5314 Fax (407) 85f1-fi9t5 {9t74)299.30f)7 F ()28.8210 19181 4&7.3t)9U Fax f91914fi7.3515 CGant Name Project Maribor Requested Analyses P r Rr f 1 Addnxs •. PrOj Nam6'tYCSC City7STrzv PO a ! BnO$uV Into Conover, NQ 28613 2015: EP04813783 Tel Fax Reporting Contact l(828 464-2414 Ray Hoffman er(s) Name. Atliliation IPrint) - Billvtg Contact SVrd WOSCr\ OYjS'M t&.n_ Ray Hoffman SarnoWs) Signatut - Site Location 1 Tune Zone COIlectwn Matra Total of Item a sample ID (Field Idantitication) Collection Date Time Comp ! Grab (see awes) Containers NM f� QCO i U C? t C OL H preservation (See Codes) fCombine as riev <•- Total # of Containers www.encoiaDs.com Page of •,•_ CO Requested Turnarou o Times f` (v Nets : Rlah regLeata IIt 0, t� M acceptance by the tacit& (L Standard Expedited Due La(b�Workordeer Vy� Z1 l V7 Samu)e Comments SRmple Ktl Prepared By � .. Dalamme i a 3 RMirquicned 6y Daliam-e Rec d By UatrJTimv ,-�• j 0.. Cwn rr eni5,rSPO ial Reporting Ramwem8nts _ Relutpt fished By Dma/rime By Date/Time Relinquished By - Dai&TIme ivo DW& Ttme Cooler Va 8 Temps on Receipt ` . 1 �— �' Condition/Upon Receipt tJ Acceptable Unacceptable Matrix : GW.Groundwater So -Soil DW-Drinking Water SE-Sadimant Sue-Surtace Water WWWastowater A -Air Q-Olhor (detail in comments) Proservatton: 14ce tl-HL;l N-HNUJ 5-HZ6U4 NU-NBUH U.Umar tdelad in commentet Note: As samples submitted 10 NCO Lath are in accordance wish the terms and COrKktionS listed on the reVOMe of this tam, urdeSs prior wnulen apte9ments exist Sample Preservation Verification ENCO Cary Work Order: CZ17872 Project: RWS-Dunn Client: Republic Services of NC (RE014) Project M [none] Logged In: 28-Apr-17 10:18 Logged By: John C King CZ17872-01 Cont Type `� . - „ +: Pres (pH),,.. Requ[re;nent pH Checked ! In Control, , . 1 :._ . •' Da!emme pH Adjusted Adlusted . _:, ,.I Reagent used omments - A 250mLA+H2SO4 <2 Y 1 N! NA Y 1TVf NA B 250mLA+H2SO4 <2 / N I NA Y 1ZP/ NA Reaclent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID 5 6 Page 8 of 8 age 1 C .A0 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted January 3 2017 CERTIFICATE OF COVERAGE NO. NCG08_0_ _8_ _2_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month REPNA t-otf �ING ®TO CLASS ❑❑ORW ero-flo❑wHQW ❑Wat❑er SupplyTrout ❑❑ A ,BAN 06 2017 ®other C. SW CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' °Outfall= No. Daat- :': Sara Collected, :. mo%dd%yrr, :;: _ 00530. _ . �-00400 - _ �:00556 - ;: Total)Suspended °- Solids; trig/,L _ ' _ �'pii, _ -Stan dardunrts -, ' Non Polar Oit�and Grease/wTPH EPA = Method1664(SGT HEM_Ann New Motor. Oil 'Usage;` ual_average;gal/mo._. `Bencl r aek :. " •'- 50 oi100�see}permita Witi in640.- 4 0}_ ` ;_. 15� ry �• rt ' i . 001 12/07/16 44 7.2 <2.70 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) ditfall >No. Date Sample_Collected, 00556 ;:. ;: 00530=SW -.'00400 Non;Polar Oil and:Grease/TPH EPA Method' = I 64;(SGT HEM), mg/=L� - 3 .. - Total SuspendedeSolids, _= � :;`. �mg/� M _ - � =_sue pH, Standard u�iits - Permit;Limi#`..:"15< 50.;'or-100tsee permit :;. 60 9.0_' . For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date _12/07/2016 (first event sampled) Total Event Precipitation (inches): 0.15 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoringperiod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) ,3 A >0,7 (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted July 13, 2016 CERTIFICATE OF COVERAGE NO. NCGOS_O_ _8_ _2_ _S_ FACILITY NAME Republic Waste Services - Dunn_ COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ® Jan -Junes ❑ July -Dec or ❑ Monthly1 (month) RECEI`DlEIARGING TO CLASS"❑ORW ❑HQW ❑Trout -®PNA ❑Zero -flow ❑Water Supply=OSA JUL 18 M6 ®Other C. SW �_ CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERS DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) no No discharge this period' Outfall No. _Date - • Sample Collected, • mo/dd/yr ' - .00530 00400 .° _ _ 00556... Total Suspended Solids, mg/L- pH, Standard units Non -Polar Oil and Grease/TPH EPA ; Method 1664 (SGT-HEM),;mg/Ls New Motor Oil Usage, _ Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0 — 9.0 15 - 001 06/28/16 13 7.6 <2.70 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall -No. ' :: Date Sample Collected, mo/dd/yr. 00556 00530 00400 -Non-Polar Oil and Grease/TPH EPA Method = 1664'(SGT-HEM),.mg/L Total Suspended Solids, - mg/L pH, Standard units ..' Permit Limit . ' - 15: - =50 or 100 see -permit `. 6.0'-9.0 1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Pagel of2 ST011M.-cVENT CHARACTERISTICS: l- Date _06/28/2016 (first event sampled) Total Event Precipitation (inches): 0.5 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMA, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/weblwq/ws/su/npdessw#tab-4 S WU-250 last revised April 1 1. 2013 Page 2 of 2 hcco�o�a � a�i� }� - NCO Laboratories `Aeenrate. Timely. Responsive. innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, July 12, 2016 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: RWS-Dunn ENCO Workorder(s): CZ07892 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory an Thursday, June 30, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sampie as received by the laboratory, and may only be reproduced in full. I Page 1 of 8 MN�G www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outtall 1 Lab ID: CZ07892-01 Sampled: 06/28/16 15:00 Received: 06/30/16 09:45 Parameter Bold Date/Time(s) Prep Date/Time(s) Analysis DatelTime(s) EPA 1664A 07/26/16 07/07116 10:38 07/07/16 14:57 Field 06/28/16 15:14 06/28/16 15:00 06/28/16 15:00 SM 25400-1997 07/05/16 07/01/16 09:00 07/01/16 09:00 FINAL This report relates only to the sample as received by the laWatory, and may only be reproduced in full. I Page 2 Of S �JVC� www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall 1 Lab ID: CZ07892-01 Sampled: 06/28/16 15:00 Received: 06/30/16 09:45 Parameter Hold DatelTime(s) Prep Date(Time(sl Analysis DatelTlme(s) EPA 1664A 07/26/16 07/07/16 10:38 07/07/16 14:57 Field 06/28/16 15:14 SM 25400-1997 07/05/16 06/28/16 15:00 06/28/16 15:00 07/O1/16 WOO 07/01/16 09:00 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in run. I Pegg 2 Of $ www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 1 Lab ID: CZ07892-01 inal]ds Results Flag ma P41 Units l CMgd N pH Total Suspended Solids 7.6 0 0 pH Units Field 13 6.2 6.2 mg/L SM 25QD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 8 OF MN www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CZ07892-01 Received: O6l30l16 09:45 Matrix: Surface Water Sampled:06/28/16 15:00 Work Order: CZ07892 Project: RWS-Dunn Sampled By:Client (Classical Chemistry Parameters ^ - FhCO Cary n9'trW anaAae PW 5911 Analyte [CAS Numberl Results Ew Units Pf MA P41 Alkh Method AnalyZ fly hmin Total Suspended SolidsA 13 mg/L 25 6.2 6.2 6GO1001 SM 254OD-1997 07/01/16 09:00 MMR Field Parameters Analyte [CAS Numbed RcIVI Elial Units U = EQ4 wto Meth Analyzed fix K5210 PH 7.6 pH Units 1 0 0 6GO1013 Field 06/28/16 15:00 CLI Classical Chemistry Parameters Analyte rCAS Numbed Oil & Grease (HEM-SGT) Non -Polar Material $s fts Eln Units I2E MQL 24L Mich Meth 44 Analyzed JU Notes 2.70 U MKg L 1 2.70 5.00 6GO6013 EPA 1664A 07/07/16 14:57 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 CSNk'CO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6GO1004 - NO PREP Blank (6GO1004-BLKl) Prepared & Analyzed: 07/01/2016 09:00 Spike Source %REC RPD Anallts, Re$u)_L Ela4 E41 units Level Result %REC Umi RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (GG01004-BSI) Prepared & Analyzed: 07/Ol/2016 09:00 Spike Source %REC RPD Anal f Result Elan P" Units Level Result %REC Limi RPD Limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (61301004-DUP1) Prepared & Analyzed: 07/01/2016 09:00 Source: CZ05945-01 Spike Source %REC RPD Anal]3. RtesuR EI83 P-QL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 88 50 mg/L 88 0 20 Classical Chemistry Parameters - Quality Control Batch 6GO6013 - EPA 1664A Blank (6GO6013-BLKI) Prepared: 07/07/2016 10:38 Analyzed: 07/07/2016 14:57 Spike Source %REC RPD Anal Yte Result Eka P41 Units Level get %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 0,703 U 1.30 mg/L LCS (6GO6013-B51) Prepared: 07/07/2016 10:38 Analyzed: 07/07/2016 14:57 Spike Source %REC RPD Anal rte Result EIP4 POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Nan -Polar Material 67.4 5.00 mg/L 75.8 89 64-132 LCS pup (6606013-BSD1) Prepared: 07/07/2016 10:38 Analyzed: 07/07/2016 14:57 Spike Source %REC RPD Anal Result Flag EQL Units Level Result °kREC Limits RPD Limit Noires Oil & Grease (HEM-SGL) Non -Polar Material 69.5 5.00 mg/L 76.3 91 64-132 3 34 Matrix Spike (6GO6013-MSl) Prepared: 07/07/2016 10:38 Analyzed•. 07/07/2016 14:57 Source: 8Z02898-01 Spike Source °hREC RPD Anal Result flag P-Q.L i1114 Level Result %REC UMF RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 20.4 1.36 mg/L 21.8 0.735 U 94 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 8 (9019G-) www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (8511/o or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of S ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.corn 1 Wfli ccritnal Pwl Or. 4A 10 Eaccu'loa Pj:6 CLjr:. Swu '.1 102-A WumrmdS Lndjsl,td Ct 001A.,A). `1-v8,4 mcka�anvwn. I'l. ;W?. I 6,6=0 Cary. NC I {41V) A26-5o]4 I-- 14LI-I A'," 11444 1913.1296-3W? Fq 19: 467-StV Fa. ;" I rj -167,35 15 Page of Piqnrl Nhimbw Paqu..Icd Away— Requested Turnaround Times. Q 0 1 Billnij 11110 G_\�e r Cyr o 2.0 CD Standard f828j4f-1-241-1. —Ray timan < Expedited 2 Due Ray Hoffman Sac ccca,.On I 7imU.!Ixw Lab.Workor.d.er - (tj .CZ07892 11 4f7.:I:. [I hnal I G I w I I Sample Comments -S Tolal 4 of Containers RaTzh l(-. I J; I BV Caul, .1. -T-3 F) T Lz-- — — $F H —t.--astw: Ry Fbj.)rWj 41n11,1—wlls Va-VImV CD fL l4cem,W, Camblion Upan Pt-cpl tinacreplatge CO Ub GW-GTVWII L11" 50-5011 DW-0011461q WO*? 5E. tjW.TArt 5%V-Sjrti,P'.VA,-M A AAr O.othr I dw,-sg ftaservaliorc 14m H IiCl N-4W0-1 0.1 PSOA NO-NaOl I O-OLbei (deUA in tomnentu Nola: All Io[NCO L.4)-..trL FI =01WIML' WWI iITW Wflnh UrJ lLte -J.ljLrjj: kSJW ct, Oq (&seI5e c4 065 F-rn. WnI,2SG Prof Ynt:cn 3pfeemeots ez)Q Sample Preservation Verification ENCO Cary Work Order. , C207802 (Aent, Republic Services of NC (REO 14) Logged In. 29-klay-15 13:33 U07892-01 - WRrazjpit " MOP. PH Checked MW A jMAt-H2,SO4 <2 e,,7,;�,IIA 8 11LA4Q,-104 e2 -----L R. e acr:e i -, L Name D Prn;ee! r e C t 41. r vj ne Rv Jahn Kin .pH Aril :' ;.,;I tW' tq i Page 8 of—8 —1 -4� . Semi-annual Stormwater Discharge Monitoring Report y for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted December 21, 2015 CERTIFICATE OF COVERAGE NO. NCG08 0 _8_ 2 8 SAMPLE COLLECTION YEAR 2015 FACILITY NAME Republic Waste Services -Dunn SAMPLE PERIOD ❑ Jan -June ® July -Dec COUNTY Harnett or ❑ Monthly' 7(month PERSON COLLECTING SAMPLES David Lawson DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY ENCO Lab Cert. # 442 RFCEIVED ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: ®Other C, SW _ DEC 2 9 2015 CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more tharQ5 ga`�ilons of new motor oil per month? _x_ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfal l No. Date Sample Collected, '- �mo%dd/yr '- 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH'EPA Method 1664 (SGT-HEM), mg/L -New Motor Oil Usage,- Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0-9.0 15 - 001 12/08/2015 31 7.93 3.19 >55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected,, mo/dd/yr 00556. 00530 00400 Non -Polar Oil and Grease/TPH EPA Method' ` 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L - pH, _ Standard units Permit Limit. - 15 - 50 or 100 see permit 6.079.0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. r r SWU-250 last revised April 11, 2013 Page i of 2 STORM EVENT CHARACTERISTICS: Date _12/08/2015 (first event sampled) Total Event Precipitation (inches): 0.3 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoringPeriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sipificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Signature of Permittee] z, D� Zvis_ (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/sulnpdessw#tab-4 E.`l►. 1D Kf] last revised April 1 1, 2013 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report r Alvo for North Carolina Division of Water Quality General Permit No. NCG080001 Date submitted January 8, 2015 4e4 0 b CERTIFICATE OF COVERAGE NO. N0008_0_ _8_ _2_ _8_ SAMPLE COLLECTION YEAR z014 q040 FACILITY NAME Republic Waste Services_ - Dunn_ SAMPLE PERIOD ❑ Jan -Jun J -Dec COUNTY Harnett or Monthly (month PERSON COLLECTING SAMPLES David Lawson pC�C' IC ISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout '❑PNA � LABORATORY ENCO Lab Cert. # 442 RE G V G ❑Zero -flow [:]waterSupply []SA Comments on sample collection or analysis: JAN 14 2015 ®Other C. SW -- - t; RAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE -� DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' OutfallF. -No:Sam `-_ma%dd/yrini5 le Colle t d, -- _00400 __ - - U55 -�--. - _Toal`Sus endedH,- liiis, mg/L ,: =Sta da unitst1/lethod Non Polar_Qil;anarG_rease/zTPHEPA== 1664rSGT�HEM g/iL :N w Motor Annual avera a I" o- sBenc h arka _ s50x0 1Osee p re mite : :11UEthin 0� .9_0 =r-._�__r_; 1 12/24/14 <2.50 7.8 <2.70 55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) .Outfall Date 00556 00530 0#}400 No l=Samle�Co�Ilected; Non=Polar�Ceil'andlGreasePPA M hodsTotaiSus ended Solids, _ p Po on- so/dd/,yr 1664 HEM)_mg/L units ,_= r T, (SGT _ - mg/L rd ga- P�ermi}�Limit -_, NM -r �'= W - _. .�-4- �-ss_ .. � _.�.' < N/A I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 1 1, 2013 Page l of 2 STORM EVENT CHARACTERISTICS: Date 12-24-14 (first event sampled) Total Event Precipitation (inches): 0.7 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coov of this DMR. includina all "No Discharae" reports. within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 8 J : -'e lc9/ (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.orp/web/wq/ws/su/npdessw4#tab-4 SWU-250 last revised April 11. 2013 Page 2 of 2 vvc-r---o�o82�8 ap Iy tE NICO Laboraton*es raf � Accurate. Timely. Responsive. Innovative. 4810 Executive Park Court, Suite 111 Jacksonville FL, 32216-6069 Phone: 904.296.3007 FAX: 904.296.6210 Monday, January 5, 2015 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Dunn Location ENCO Workorder(s): B402578 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, December 29, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, m Chris Tompkins Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7 (� �Go www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Out(allI Lab ID: B402578-01 Sampled: 12/24/14 16:00 Received: 12/29/14 08:45 Parameter Hold Date/Time(,s PrSH Date/Time(s) Analysis D Tim EPA 1664A 01/21/15 12/31/14 12:32 01/05/15 10:14 SM 254OD-1997 12/31/14 12/30/14 10:35 12/3V14 11:11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. page 2 of 7 (��Cmi www.encolabs.com SAMPLE DETECTION SUMMARY No positive results detected. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Pago 3 of 7 Cf=co www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID: B402578-01 Received: 12/29/14 08:45 Matrix: Surface Water Sampled:12/24/14 16:00 Work Order: B402578 Project: Dunn Location sampled By: David Lawson Classical Chemistry Parameters ^ - ENCO Jacksonville cerrirvd analyte [NC 442] An Results Elm Units 1 l DL POL Batch Method Analyzed f]t Notes Oil & Grease (HEM) [C-0007) 2.70 U mg/L 1 2.70 S.63 401004 EPA 1664A 01/05/15 10:14 M)F Total Suspended SolidSA 2.50 U mg/L 1 2.50 2.50 41-30011 SM 254OD-1997 12/31/14 11:11 mjf/s FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 4 of 7 FJ�Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4L30011 - Same Blank (4L30011-BLK1) Prepared: 12/30/2014 10:35 Analyzed: 12/31/2014 11:11 Spike Source %REC RPD ; Analyte Resu Flan EQL Units Level Result a7oREC Limits RPD Limit Notes Total Suspended Solids 2.50 U 2.50 mg/L LCS (4L30011-BSI) Prepared: 12/30/2014 10:35 Analyzed: 12/31/2014 11:11 Spike Source %REC RPD Analin Result MCI! E" Units Level Result %REC Limits RPD Llmlt NSUS Total Suspended Solids 101 2.50 mg/L 100 101 80-120 Duplicate (4L30011-DUPI) Prepared: 12/30/2014 10:35 Analyzed: 12/31/2014 11:11 Source: 9405318-02 Spike Source a/oREC RPD Analvte Result Flao POL Ynftj Level Rest] %REC Limits RPD Limit Notes Total Suspended Solids 2,50 U 2.50 mg/L 2.50 U 5 Duplicate (41.30011-DUP2) Prepared: 12/30/2014 10:35 Analyzed: 12/31/2014 11: It Source: B405670-02 Spike Source %REC RPD Analyte Result Flag P4.` Units Level Result %REC Limits RPD Limi Notes Total Suspended Solids 7.60 2.50 mg/L 7.60 0 5 Batch 4L31004 - EPA 1664A Blank (4L31004-BLKL) , Prepared: 12/31/2014 12:32 Analyzed: 01/05/2015 10:14 Spike Source a/oREC RPD AnalYte Result Elm E4L Units Level Result %REC Limits RPD king Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (4L31004-BS1) Prepared: 12/31/2014 12:32 Analyzed: 01/05/2015 10:14 Spike Source %REC RPD Anal Result Flag Q Units Level Result %REC Limits RPD Limit notes Oil & Grease (HEM) 33.3 5.00 mg/L 41.4 80 78-114 LCS Dup (4L31004-BSDS) Prepared: 12/31/2014 12:32 Analyzed: 01/05/2015 10:14 Spike Source a/oREC RPD Analye ResuR Flag PAL unb Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 34.7 5.00 mg/L 41.0 85 78-114 4 18 Matrix Spike (4L31004-M51) Prepared: 12/31/2014 12:32 Analyzed: 01/05/2015 10:14 Source: B405679-01 Spike Source 0/aREC RPD Analyt ResuI Flao M units Level Result 0/aREC Limits RPD Limit Notes Oil & Grease (HEM) 33.6 5.00 mg/L 41.4 2.40 U 81 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7 (� �Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 250/a concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD 10775 Cenlyd I'rrrt Dr. nRi0 iixrrutivr 1'nrk r:un11. Sw-n 11 1 1W-A W(YYJwilxis h,dusn'nd Cl, Orlaimk . FL JLN24 .I�x;k�;cnl+lrlkt, FL :L_l li eithi'.r Gary. NC 27511 (407) 8'Ld-5314 Fax i40/i atilb04 : ('914) 29a-3W'I Fw I`.4141 H,:«i-fit ip 10131 467-30M Fax {:11',)1-Sri7.3.,15 www.encolabs.com Page - 01 Clsxnl Nome Republic Services of NC (RE014) Prtlier:l NurnlxY � I �- C� o Fiecluesled Analyses — 1C:u:rk>.nu --- a:: ,ruun_�.`a, — li - — Requested Turnaround Times Nkrtr. ; Flrr;h imitioslt: mdriecl la ,,;1;1ri11:rni a try rlw r:r,}';'y _ Standard _Expedited DUe � C C � i I C1iur�) pridrd�s 1220 Commerce St. SW Box 1 Pr;l;erf NametLTe sc Dunn Location C;nytti I lf.1p Conover, NC 28613 - --�— „ re (8.28) - 8 164-241 -Ilya I _ 110 a ; kS111nx1 Inro ---_-- P04154031 - - 4 F:�r131Ray Hoffman -- Snm %Fart-) None, IIWi[<tirvi IP1inr} --__ _._.. —�;ll _ Hn4n�1 Conlnrt Ray Hoffman Y --- - - - ;ltc Lax:;rt+ltrl: Irmo Ztq1,: Lab Workordor B402578 Presorvntlan Ic.!N) n ut u Sauq la to {F al 4 klernilicar ,n) C:r> IrCann I ) yr IZ Z�-L� . C01!a;1i0,1 lime Ll Pin (:.Nnp t I if )h • (SQ6 Wtlrlx Isr,-- cocks) sw Toial 40 C: xllnrinr5 Sample. COmments -Outfali 1 3 x x - 1 I 1 1 <-- Toiai II rlt containers anjAu Kii Pfopared By nnifi limp.. C.wnmr•.rd:''',{xx:�rlrkarurlirxJ13cquirranciIU, T I lNirxllr!3hed FSy "OnquiSk?d$IV i)a N7rinnr: Itnll:rrmu: — Receives Rurew'jBy— — 0:11021 mc: r lY.rtr..'lanr. Win4uishedny nr,leirmtr IP.-mYY-CIBY D;* rirne. C+]alel d's & Temps on Receipt !� Condition Upu eceim eptable Unacceptable alrix:GW-Urutrs,d'.+rrler $O ;nil l7W nrinklnn W:rtrr SH ,Srxlinlrnl SW -Surface Wate, WW-War;wwaler A-Nr 0-00wr idul;IiF in ronlfngniSj Preservaliun: I-icv tlJICI N-HN()3 5 112gU•I NO-NeUH 0,0thor (c]Mtif in rommunls) ti Nole : NI ::anlples SuLxnillt'd to ENCO Labs ale 6 ac:Cu,dance with are It'r * arvJ CJndilions listed on rho r,rvarsn n1 INs term, rink•;: prier writirn nglrrmenln ex,sl • Semi-annual Stormwater Discharge Monitoring Repo for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted August 7, 2014 CERTIFICATE OF COVERAGE NO. N C G 0809 28 FACILITYNAME Waste Industries -Stedman COUNTY CUMBERLAND PERSON COLLECTING SAMPLES J D FREI/ SwSG LABORATORY —Pace Analytical Lab Cert. # 12/ 67 Comments on sample collection or analysis: pH measured infield by SwSG (Lab Cert No. 5054) SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ❑ Jan -June 0 July -Dec or El Monthly' (month) REG'QcYAM G TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA- JAN 15 2015 - ❑zero -flow ❑Water Supply ❑SX� 0 CENTRAL FILES Other C, Sw DV!/R SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE IV Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ✓ yes _no (if yes, report your analytical results in the table immediately below) }� Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this periodl: Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L ' pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0 — 9.0 15 - 001 12/29/14 23.8 6.72 < 5.0 +/- 95 002 12/29/14 10.6 6.60 < 5.0 Part B: oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit - 15 50 or 100 see permit 6.0-9.0 t For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWLJ-250 last reviscd April 11, 2013 Pagc l of 2 STORM EVENT CHARACTERISTICS: Date 12/29/14 (first event sampled) Total Event Precipitation (inches): 0.51" Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark,'you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMFTER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 0 IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, indudina all No Discharge' reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge_ reports _ ) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant p nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Perriiittee) i /3 { ate Additional copies of this form may be downloaded at: http://portal.ncdenr,orp,/web/wq/ws/su/npdessw#tab-4 S W U-250 Iasi revised April 11, 2013 Page 2 of 2 STORMWATER DISCHARGE OUTFAI L (SDO) r MOl\1 I UK NU REPORI GENERAL PERMIT NO- NC0180000 SAMPLES COLLECTED DURING CALENDAR YEAR: ")o I � CERTIFICATE OF COVERAGE NO- NCG08 O 130 (This monitoring report is clue at the Division no later than M days front _ the date the facility receives the sampling results from the laboratory.) FACILITYNAME oy'fi�z�stern /'re�yrti- Lires_ !�, t Z COUNTY 7)Urko_-^^ PERSON COLLECTING SAMPLES �cr ZGL��+ _ ONE NO. (Y(r CERTIF<`IEDLABORATORY_%S'�G�ner��e. Lab #�9a-$4S&5'_RECE1VWb Lab # PLEASE SIGN ON THE REVERSE. 4 JAN 2 0 2015 Part A: Vehicle Maintenance Areas Monitoring; Requirements Did this facility perftlrm Vehicle Mit tone mcc ActivilicS USmII mr:>rc lhun 55 gt111ons rat ilew Q&N-TR,%-Fj4),EU (d' Ve.s. repon Will- ❑nalyli(:al rr.sultz in the tahle immediately hclow) DWR SECTION No: Date Sample Collected,, . }{,3l h ow . tOSStOutfall Total`Stispended Solids, ... _ • pH; . .Satruit-" la OilY:and Grease ;n�/L ; New Motor Oil --Usage,, average =aViii;nn/dd/vr Benchmark V100:. ' " "_ Within*. ' 1'-:%0.. . , 30 - ND Note: 11'ysxr rep01-1 a samhletl va[Lie in Cxrrss o the henchm:irk valrtc_ Or, (misidc the henchmark rare uc for 111-1. you must implumcnt Ticr 1 mr 'ie.r 2 i-cs1lollses. See Gemm—al fermi( text. Part B: Oiilwater Separators rind Secondary Containment. Areas at Petroleum Bulk Stations and Terminals Outfall No. Date Sample Collected, neoldd 00530 00400 Oil'and'Grease,-' ._•.,Total, Suspended Solids, pH, Standard units Permit Limit - 3W 1.011 ' 6A - 9.0 i STORM EVENT CHARACTERISTICS: Date ('first event sampled) Total Event Precipitation (inches): L-)' S-a Date _ (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): _ iblail Original and one coley to: Division o1 Water duality Attn: DWQ Central Files t617 Mail Service Center Ralc.igie, Nr>rllr Carolirrt 27099-1617 Y.- SWU-250-102107 Page. t of 2 rr "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and Belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fin ° � an 'mprisonment for knowing violations." /Z/?/-z i (signature of fern it A (U te} SWU-250-102107 Page 2 cof' 2 Client: Southeastern Freight Lines Project/Site: SEFL Raleigh NC Client Sample ID: SEFL Raleigh NC Date Collected: 42/09114 01:01 Date Received: 12110114 08:30 General Chemistry Analyte HEM (Oil & Grease) Total Suspended Solids pH Temperature Client Sample Results Result qualifier ND 9.28 7.88 HF 21.0 HF RL 3.88 1.03 0 100 0.100 VIOL Unit mg1L mglt SU Degrees C � 1 TestAmerica Jab IDS 490-68298-1 Lab Sample ID: 490-68298-1 Matrix: Water D Prepared Analyzed Oil Fac 12/ 17/14 1 1'27 12/17/14 1 1:27 1 12/11/14 11 40 1 • 12/11/14 11',35 1 12111114 11:35 1 TestAmerica Nashville Page 6 of 15 12/22/2014 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted June 26, 2014 CERTIFICATE OF COVERAGE NO. NCGO8_0_ _8_ _2_ _8_ FACILITY NAME Republic Waste Services - Dunn COUNTY Harnett PERSON COLLECTING SAMPLES David Lawson LABORATORY ENCO Lab Cert. # 442 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ® Jan -June ❑ July -Dec RECQCKDor ❑ Monthly', _ (month) DISC�i G TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA JUN 3 0 2014 ❑Zero -flow ❑Water Supply ❑SA CENTRAL FILES ®Other C. SW DWQIBOG PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) No discharge this period' Outfall No. - Date ` Sample Collected, mo/dd/_yr 00530. 00400 00556..:.:. , Total Suspended Solids .<mg/L-.= ., pH, Standar&units-_, . , ::Nan-Polar.Oil-and'Grease/TPH EPA. :- Method 16644{S_GT HEM); mg/L_ New;Motor.Oil Usage, Annual average. gal/mo Benchmark - 50 &.400 see permit-: Within 6.0 - 9.0 15 - 1 06/13/14 <2.50 7.5 <2.77 55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall Date _. " 00556 ;Q,0530 00400, No. Sample Collected, Non=Polar Oil and Grease/TPH EPA Method:". -Total Sus pended-5olids;. - mo/dd/yc - ° . 1664 (SGT=HEM), mg/L - mg/L Standard units,. = ; Permit Limit = :-. 15. 50 or se it 6 0-:9.0 N/A I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 6-13-14 (first event sampled) Total Event Precipitation (inches): 1.0 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on inal and one copy of this DMR including all "No Discharge"' reports, within 30 days of recei t of the lab results or at end of monitoring eriod in the case o-`No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq[wslsu/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 u. CO .laboratorieso� Accurate. Timely. Responsive. Innovative. 4810 Executive Park Court, Suite III Jacksonville FL, 32216-6069 Phone: 904.296.3007 FAX: 904.296,6210 Monday, June 23, 2014 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Dunn Location ENCD Workorder(s): B400088 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, June 16, 2014, Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCD Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chris Tompkins Project Manager Enclosure(s) FINAL This iepen i eSa.es only W We Sample as iece and pl me lanwalgry, afv may only X7 ie0roaucea m hAl- Pege t of 7 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client10: WWII Lab10: 640008"I Sampled: 06/13/14 09:00 Received: 06/16/14 09:43 Parameter lioW,patelTime(sl Prep DatelTfine(s) Analysis pate/Tfrne(sl EPA 1664A 07/11/14 06/18/14 12:01 06/15/14 09:36 SM 254OD-1997 D6120114 06/17/14 15:00 06/l8/14 14:34 Ff NAL this report ratites only to the sampk at oeCWOG by the ataiat&V, and may dnM be ieproouced rn (Al- Pagn 2 of 7 n � � www.encolabs.com SAMPLE DETECTION SUMMARY No positive results detected. FINAL TNS repot rda;et Or,y tome sample at scarred DV the labmtory, ar-0 mar OftN W reoroau.ad In full, Pape 3 of t C4 S- 1 01-99 www.encolabs.com ANALYTICAL RESULTS Description: Outiall 1 Lab Sample ID:B400088-01 Received: 06/16j14 09:43 Matrix: Surface Water Sample4d:06113/14 09:a0 Work order: B400088 Project: Dunn Location Sampled By: David Lawson Classical Chemistry Parameters .• - IXOJW4 W Wle r&vfga xu,4,teINC 44.l) Ulu PI 11.Dk E" Batch WhQd Al U210 Od & Grease (HEN)IC-0007) 2.77 U mg/L 1 2.77 5.77 4F18002 EPA 1664A 06/19/14 09:36 WF Total Suspended Sapds (ECL-0169)1 2.50 U mg/L I 2.50 2.50 4F17016 SM 2540D1997 06/18/14 14:34 seta FlriAt Ttvs repot rebus pntyto L" sampie as rya by the sa0aratav, a% rney anN be r=OQLKW in tyt PIQO 4 Of 7 E11 r � www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4F17016 - same Blank (4F17016-8LK3) Prepared: 06/17/2014 15:00 Anal(zed: 06/18/2014 14:34 Spike Source %REC RPO .Arlalyte Result Vag POL Umb Level ResuR %REC UMLU RPO ftj Notes Total Suspended Solds 2.50 U 2.50 mg/L LCS (017016-11SI) Prepared: 06/17/2014 15:00 Analysed: 06/18/2014 14:34 Spike Source %REC RPD Ana lYlS Res;j E1a9 PQL YfLits Level Rm %REC Ilmfts RPD limit Rota Total5uspa)ded Solids 117 2.50 mg/L 100 117 80.120 Duplicate (017016-DUPl) Prepared: (16/17/2014 15:DO Analyted: 0611812D14 14:34 Source: B402046-01 Spike Source %REC RPD .Analyts Rssfllt flag PQL Units Level Result %REC LimiSg RPD Limit Notes Total Suspended Solids 132 2.5D mg/L 153 15 25 Duplicate (4F17016-DUP2) Prepared; 06/0/2011 35700 Analyzed: W1812014 14:34 Source: B40M2-01 Spike Source %REC RPD .An?tvte Result Flag Pot Vnits Level Result %REC Limits RPD Wrals Notes total Suspended colds 655 2.50 mg/L 715 9 25 Batch 4FI S002 - EPA 1664A Blank (038002.8LKi) Prepared: 06/18/2011 12:01 Awlyred: 06/19/2014 09:36 Spike Source %REC RPD .Mahn Result Etas PQL Units Level Resyl %REC L)MJU RPD Limit Notes 01 & Grease (HEM) 2.40 U 5.DO rnglk LCS (4F18002-BSI) Prepared: 06111112014 12:01 Analyzed: 1)6/1912014 09:36 Spike Source %REC RPD .Anal]dL Result 156W e" I1.0iU Level Resut %REC 11m11s RPD Limit DJ & Crease (HEM) 38.8 5,00 rr*L 41.3 94 78.114 LCS Dup (018002.9SD1) Prepared: 06/1B/2014 12:01 Analyzed: 06/19/2014 09:36 Spike Source %REC RPD .9Rah tS Result Fias 90.1 Uaiw Level Result %REC Limps RPD Limp Notes Oil & Grease (HEM) 38.5 5.130 mg/L 41.5 93 78-114 1 is matrix spike (41`18002-MS 1) Prepared: 06/18/2014 12:01 Anasytcd: 06/ 19/2014 09:36 Source: 8400088-01 Spike Source %REC RPD jvwytc Result Elao PQL Unlit Level Result %REC LiMLU RPD Limp tl1&M al & Grease (HEM) 47.9 6.43 r*L 51.8 3.0811 93 78.114 FWAL TMs report feta:es orrN to Inc sample as je=ea w the latoratory, AM mar onry to reaaaucw m fJL Papa 5 of 7 www.encolabs.com FLAGS/NOTES AND DEFINITIONS 6 The analyze was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyze is an estimated value above the calibration range of the instrument. This value is considered an estimate. NRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. The anaWs. indicates the presence of an anaiyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". FINAL Trot IeWil reldU* only to Me W%* as received tra the ratmaUxY, and mai 01* to ,eDrocumc in rat P40A 6 or 7 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD ou 17. A7, -1 4 3 4) qt)x 0 Ick U"a L'5-'Ws6 sir 3 x x www.encolabs.com Page __ c ff Lit to .,'it) Wr-rkorclei B400088 Sm I ip P - - t „ I i I- - I I P1' 1-6-0 — Llll:., I ,