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HomeMy WebLinkAboutNCG080786_MONITORING INFO_20181128STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V Ci& Ui D � DOC TYPE ❑HISTORICAL FILE Cyt MONITORING REPORTS DOC DATE ❑ a 0A 1 I a YYYYMMDD Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted November 20,2019 CERTIFICATE OF COVERAGE No. NCG08 0 7 8 6 FACILITY NAME Republic Services of NZ L—LC-- &SAWa—shi—naton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: t SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthlvi. (month) RECE1115RCHARGING TO CLASS 0ORW [:]HQW [:]Trout [:JPNA �- Elzero-flow DwaterSupply [:jSA NOV 2 8 zoI8 ❑ ®Other C; Sw, NSW CENT-RAL Fl 0'N,R,SECTj0jNjLeS - PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x—no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) 0 No discharge this periods No Date ,4A: sp Sample ColleRei, F K a — DR M Tbta _Suspended --PH *Stiiidaid:unit� 86�VW761and jdr— TP A -aierak*gavmo--: lkpmiw,0:0 9 63 0- Outfall 2 10/26/18 2.7 7.9 3.15.1 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) N' Sample Collected,i—%A46440Z fc-6 I p�n4 k- N� Ina -HEM j N*wWN I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 10-26-18 (first event sampled) Total Event Precipitation (inches): Trace Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR includina all "No _Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case o "No Discha e" reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there ad$igificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Si nature of Permittee) (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wci/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 (Q-o Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 7, 2018 Republic Services of NC (RE014) Attn: Nicky Hopkins 450 Flanders Filter Rd Washington, NC 27889 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Washington Stormwater ENCO Workorder(s): CB09843 Dear Nicky Hopkins, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, October 29, 2018. Unless otherwise noted In an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as reoeked by the laboratory, and may only be reproduced In full. Page 1 of 7 i Ca No, I Goi I P-j www.encalabs.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client ID: Outfal1002 Lab ID: C009643-01 Sampled: 10/26/18 11:13 itecelved: 10/29/18 08:50 - --- Parameter Preparation EPA 1664A EPA 1664A jigjd Date/17mefs) 11/23/18 EMU DateMme(s) 11/01/18 12:25 Analysis 11/05/18 11:39 Fleld NO PREP 10/26/18 11:29 10/26/18 11:15 10/26/18 11:15 SM 254OD-2011 NO PREP 11/02/18 10/30/18 10:02 10/30/18 10:02 FINAL, This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 2 Of 0 Fn = Nk" I� www.encolabs.com SAMPLE DETECTION SUMMARY plant ID: Outfall 002 Lab ID: C509843-01 Anal 6esulte flu MQL WL Mill" Method Notes Oil & Grease (HEM-SGT) Non -Polar Material 3.15 1 2.70 5.00 mg/L EPA 1664A pH 7.9 0.0 0.0 pH Units Field Total Suspended Solids 2.7 2.5 2.5 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 3 Of 7 www.encolabs.com ANALYTICAL RESULTS Description: 0utfall 002 Lab Sample ID: CB09843-01 Received: 10/29/18 08:50 (Matrix: Surface Water Sampled:10/26/18 11:15 Work Order: CB09843 Project: Washington Stormwater Sampled By: CLIENT Classical Chemistry Parameters ^ - EXV a,rmrMeadanaryra[NC S911 Analvte rCAS NumtNE] $egu Eing Unita RE M" M Bntsh Method Annla d am N4te8 Total Suspended SolldsA 2.7 mg/L 1 2.5 2.5 8330003 SM 25401)-2011 10/30/18 10:02 OMR Field Parameters Rardllta Elm !lops 211 MM PI L Bntdt Method Analyzed By ids PH 7.9 pH Units 1 0.0 0.0 8KO7007 Reld 10/26/18 11:15 CLI Classical Chemistry Parameters Oil & Grease (HEM-SGT) Non -Polar Material 8eslllta an unify 2E MU EM AAIGh Method 3.15 l mg/L 1 2.70 5.00 8K01008 EPA 1664A AnahQsd Bit n9ka t1/0511811:39 SMA FINAL This repot relates only to the sample as reoelved by the laboratory, and may only be reproduced In MI. I Page 4 Of 7 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch B730003 - NO PREP Blank (8330003-BLKI) prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD AnalyU Result Elm PQL Unb Level Result %REC UM[b RPD LIMB Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9330003-13si) Prepared & Analyzed; 10/30/2018 10;02 Spike Source %REC RPD Anal Result El" PQL URRa Level Result %REC Limits RPD Lbt Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 Duplicate (B330003-DUPI) Prepared & Analyzed: 10/30/2018 10:02 Source: C815181.01 Spike Source %REC RPD Anal fdB RCsuR Elao POL Unka Level Result %REC LbJU RPD 11011t tlOWi Total Suspended Solids 2700 500 mg/L 2200 19 20 Duplicate (8330003-DUP2) Prepared & Analyzed: 10/30/2018 10:02 Source: CB16046-01 Spike Source %REC RPD Alulhr�o RCEWI 15189 PQL LIU& Levu! Resin %REC UMLW RPD =ft I1tM Total Suspended Solids 220 50 mg/L 230 4 20 Classical Chemistry Parameters - Quality Control Batch BK01008 - EPA 16648 Blank (8K01008-BLKi) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD AnalVft ROM Elan PQL UnRs Level Result %REC Lj" RPD (,[pit Jute Oil & Grease (HEM-SGT) Nan -Polar Material 2.70 U 5.00 mg/L LCS (SK01008-BSI) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Amllete RC1iuR Elan PQL Unite Level Result %REC LkAl U RPD L!lglt Notes Oil & Grease (HEM-SGT) Non -Polar Material 78.6 5.00 mg/L 82.3 96 64-132 LCS Dup (BK01008-BSDi) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Spike Source %REC RPD Anal YIC P=l Elan ML Unib level Result %REC UM ti RPD Limit Nato Oil & Grease (HEM-SGT) Non -Polar Material 86.8 5.00 mg/L 80.0 108 64-132 10 34 Matrix Spike (SK03008-Mil) Prepared: 11/01/2018 12:25 Analyzed: 11/05/2018 11:39 Source: B8043a7-03 Spike Source %REC RPD Anal Result an PQL Un11s Level Result %REC LWI" RPD IfinR Nolan Oif & Grease (HEM-SGT) Nan -polar Material 86.1 5.00 mg/L 84.4 6.12 95 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 Of 7 www.encolubs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value Is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quandtation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. F[NAL This report relates only to the sample as reCeNCd by the laboratory, and may only be reproduced in fun. I Page 6 0f % Court, �. Irt�,� a k f_xo lle.F Park 6-606 Setle tfi , Cary, Or,antla. FL 3262a Jacksas rnige. F7., 3?2f 6fi069 Cary, NC 27511 L �co� t0775 LFL-9l 4Dr Jacksonville. (4e7) BZ&5314 Fax (407) 850-6945 (904)296-9(V7 Fax (904)296-6210 4919) 467-3p90 Fax (919) 467.3515 Page of C: wn Nama Republic Services of NC (RE014) "00 Number [none] Requested Anatirwas Requested Turnaro Q rules ti Nob : Rush requests sutW m acceptance by the tadtit ti Standard Expedited Due l I 0 r 00 ° m v CL O v) F Address 1220 Commerce St- SW Box 1 PrOfM NameMese Washington Storm inter CaylsTlT� Congver, NC 28613 PO a / awing Into Tel (828) 464-2414 Fax Repooft contuA Ray Hoffman Sampiens) Name. AtManon (Print] IN Contact cas Norris Samplar(s) SiwMWre I Sde tAcatxtn T Tarte Zone Lab Warkvrder CB09843 Preservation (See Codes) (Combine as necessary) Item r Salnpte ID (Field Iaerr..tiraSr Cosecuon Date C Maction Time Comp! Grab Matrix (see woos) Total s of Canainers Sample Comments outfall002 a I/� .� tl �' sw 4 x x x /A_7 _ � t <--Total # of Containers Sample Kit Prepared By DaielTirtte Rang ' - Datrrrme - R - DaterTime GommentsrSpepal Peportmg Reqummenls - jr RW:nWi Byf DatWrrnV ecei By DatePrime Flalmquisbed BY Daternme R ived By Dat&TMM Cooler #'s & Temps on Receipt A2 Combbon Upon Rent ✓Acceptable Unacceptable Uzbft : GW-Groundwater SO-Sed DW-Drinldrg Water aft--'AOMOM SW- Winer Water W W-WYasrerater a-Ae piJmM (perax In wmmenrs) Pig*FVnHo l: FIce r1-M f u-rs 4UJ snzwa mw-Naun u-vurer IMMO m wmmernsl Note: AN samples submttlad to ENCO labs are in accordance with the terms and wnddions fisted on the reverse Of efts form. wtles, Prior *=on agreemartts exist � I Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted May 7, 2018, CERTIFICATE OF COVERAGE No. NCG08 0 7 8 6 FACILITY NAME Republic Services of NC, L-LC-- G-D-S-W-a-shi-ngton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY—ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD 0 Jan -June [:) July -Dec or D MonthlyL knonth) DISCHARGING TO CLASS []ORW [-]HQW [-]Trout F]PNA OZero-flow OWater Supply EISA E I V E D MOther—C; Sw, NSW MAY 15 2018 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 0, Did this facility per -form Vehicle Maintenance Activities using more than 55 gal log![-:6fT"tnTdt&,%iI per month? (if yes, report your analytical results in the table immediately below) DWR SECTION Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) yes -x-no D No discharge this period' o. ��:z aie r .14mpleC61lettedi oosio W-' T6th I Sd rn I&Z" �Solids,- -- �';"7 it S - A 7 -PW�' 5 S ii 'I tali a 6 Its �f �Ihb-961iFibir C1%AF4iW1TP H PA t5� M ciffilA 1 Niii.m6thr,01 -us -Ann aj.-. U average;gal/mo �50.qr�100 rrnhitt sM.pe -0 fw�: 7; 7 Outfall 2 04/24/18 5.4 7.8 <2.70 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) -"o 11- ate' N R WE Im R P S� --N Nbn;Polar.01 -'and Me -NN61tu-sp6ffidiid'Ulld .�qoje#� -:I 2- IN _StandaygmmuQ - nt�N -OW�WU�WFMwdm !re I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 5W-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 04-24-18 (first event sampled) Total Event Precipitation (inches): 1.91 _ Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of_the lab results for at end of monitoring period in the case of "No Disc_harae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.ore/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 ENCO Laborato Accurate. Timely. Responsive, Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 929.467.3515 Friday, May 4, 2018 Republic Services of NC (RE014) Attn: Nicky Hopkins 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Washington Stormwater ENCO Workorder(s): CB00133 Dear Nicky Hopkins, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, April 25, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted In the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduoed in full. Page = www.encolobs.com SAMPLE SUMMARYILABORATORY CHRONICLE Client ID: Outfall002 Lab ID: CG00133-01 Sampled: 04/24/18 13:10 Received: 04/25/1010:15 Parameter Preparation EPA 1664A EPA 1664A (gl 05/22/18 Pren DatelTlmefs] 05/02/18 13:54 Analysis DatelTime[s] 05/03/18 14:49 Field NO PREP 04/24/18 13:24 04/24/18 13:10 04/24/18 13:10 SM 254OD-1997 NO PREP 05/01/18 05/01/18 15:35 05/01/18 15:35 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 Of 7 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 003 Lab ID: C600133-01 AnalYte Raul 9 Elan m" 2" unb NWh4d ado PH 7.8 0.0 0.0 pH Units Feld Temperature 17.3 0 0 °C Feld Total Suspended Solids 5.4 2.5 2.5 mg/L SM 254OD-1997 FINAL Th{s repot relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 3 of 7 CS NSL' 0 0) www.encolabs.com ANALYTICAL RESULTS Description: Outfall 002 Lab Sample ID: C800133.01 Received: 04/25/18 10:15 Matrix: Surface Water Sampled:04/24/18 13:10 Work Order: C800133 Project: Washington Stormwater Sampled By. Mcky Hopkins Chemistry Parameters ^ - EMCO QVy-rW d malyte (AC 5911 Analyte MAS Numberl Results f ng Mob 2E Nip}, pRL flffth Method Aged am fidal Total Suspended Solids^ 5.4 mg/L 1 2.5 2.5 8E01002 SM 254OD-1997 05/01/18 15:35 OMR Field Parameters Analvte MAS Numberl Results Flia uglta QE MU EQL Batch Method Analyzed flu h= PH 7.8 pH Units 1 0.0 0.0 81)26005 Field 04/24/18 13:10 CLI Temperature 17.3 "C 1 0 0 8D26005 Reid 04124/1813:10 CLI Classical Chemistry Parameters Anande_fCAS Numberl Oil & Grease (HEM-SGT) Non -Polar Material ftesul Elias Vab 9f M EQL latch Method Analyzed AN MQw 2.70 U mg/L 1 2.70 5.00 SE02009 EPA 1664A 05/03/18 14:49 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 4 Of % www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch BEOIO02 - 11110 PREP Blank (BE01002-SLK1) Prepared & Analyzed: 05/01/2018 15:35 Spike Source %REC RPD Anal ldc Result Elea P9L Va to Level Result %REC )dmlta RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SE01002-851) Prepared & Analyzed: 05/01/2018 15:35 Spike Source %REC RPD Anal ld0 Result 1-78a ML Units Level Resin %REC limits RPD LIMB Notes Total Suspended Solids 88 2.5 mg/L 100 88 80•I20 Duplicate (BE01002-DUPI) Prepared & Analyzed: 05/01/2018 15:35 Source: C001514-01 Spike Source %REC RPD AnalResult flag PAL Units Leval Result %REC Limb RPD Unlit Notes Total Suspended Solids 53 10 mg/L 57 7 20 Duplicate (SE01002-DUP2) Prepared & Analyzed: 05/01/2018 15:35 Source: CB01690-01 Spike Source %REC RPD AOellse Rand an WL UWN Level Result %REC JLmb RPD Um t Notn Total Suspended Solids 100 12 mg/L 120 0.5 20 Classical Chemistry Parameters - Quality Control Batch SE02OOO - EPA 1864E Blank (BE02009-BLK3) Prepared: 05/02/2018 13:54 Analyzed: 05/0312018 14:49 Spike Source %REC RPD Ana hdO Raw 17a0 ROL UAlta Level Result %REC Lm[U RPD 1113211; tYates Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (SE02009-BSI) Prepared: 05/02/2018 13:54 Analyzed: 05/03/2018 14:49 Spike Source %REC RPD Ana Result Elm Ml. Wall Level Result %REC LJmON RPD LJB1Jt Notes Oil & Grease (HEM-SGT) Non -Polar Material 87.6 5.00 mg/L 77.2 114 64-132 LCS Dup (8E02009-BSD1) Prepared: 05/02/2018 13:54 Anayzed: 05103/2018 14:49 Spike Source %REC RPD Ana hRC Resldt HN E21. Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 67.9 5.00 mg/L 75.5 90 64-132 25 34 Matrix Spike (SE02009-MS1) Prepared: 05/02/2016 13:54 Analyzed: 05/03/2018 14:49 Source: 8801911-01 Spike Source %REC RPD Anal 1 Result Ran Pal. WIN Level Besult %REC Limits RPD "mM J�otes Oil & Grease (HEM-SGT) Non -Polar Material 92.4 5.00 mg/L 80.3 2.70 U 115 64-132 FFNAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 5 Of T Who rrr r www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected In the associated method blank. D The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quandtation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, In the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as maNed by the laboratory, and may only be reproduced to fuu• I Page 6 of 7 19775 Centre! Fbrt Dr. 4810 ErreuoLre Peek Court, Svire t1 t 102-A Waodwfrds lrx7ustrial Gt. Or wWo, FL 32824 Jacksonville. FL 32216.6069 Cary, NC 27511 Lem; Nhk '14-0-94 1407) 825-5314 Fax (407) 850.6.445 (904) 296.3007 Fax (9041296-6210 1919) 46T-3090 Fax (919) A67-3515 cyan Name l PM"— Nranbar I Reaunbd Analyzes .. ��Lucas Norris rR we ".we iLViRiiJ�.LVife Page of n Requested Turners o Times � m N= : Rush regorsts acmmWIM by me twili ca Standard Expedited Due _r Lair Workarder C B00133 Sample Comments g9fl %�l.3°c- Sa"Ae Kit Prepared BY Oatafrene 7L RBlvlgr@SheO Dateffane Recervvd DetelTime C-nenWSpecalRepanmg Do Tune Irved Lww.me Relinqudshed By DaWrme R DaWnroe on Aaceipr Cooler s'p & T&Ygn on 11erolpt 177A 't t' cceptable _ Unacceptable daWx : OW-Croundweter 50$ae DW-Dnn" water SE,9*d aeon SW -Surface Water WW-Wastewater A -Air G4JMw (decal In catatrwts) PreiarvaWn., Er[e "U n-KNW s-M2S44 1404ftUH 04)rhar (detail on aom erns) Nola : Al samples SLR ftad to ENCO Labs are in acmrdanoe with Ore terms and candiho ss knW an the reverse of tw bnn, urlese prior written agreements exist . Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted November 30, 2017 CERTIFICATE OF COVERAGE No. NCGO8 0 7 8 6 FACILITY NAME Republic rvicesofNE.L—LC--G—D-5-W—a—shi—nkrton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY ENCO Lab Cert. # 592 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June 0 July -Dec or ❑ Monthly' (month) RECARMFE&G TO CLASSE]ORW [:]HQW [:]Trout OPNA E]Zero-flow OWater Supply E]SA DEC 0 5 2017 ®Other Ci Sw. NSW CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes -x-no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) El No discharge this period' N o'. &F'." - �t - 7 �Dite--Tji� -.F� 5�--" E- Collected, plb Collie Vd/yif -- - . 3071 -]� -004WU *K 21R111.6659el&i 'F- -T&A Suspended a[ d d---' units. OlWa —Non-Polar-� �if&G&igj/TPKTPk WLI��-- Mitti6dA664:r HEM)17rn 0torEOi '.Usage ge 1111101 5 v A mit 0 i lk� per 0 1F A Outfall 2 11/09/17 2.8 7.51 3.94 J <55 Part 8: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) = No ;� D' Sample Collected, J Non=Pofar�Otl and.Grease/TPH'EPA Method V =�-Natal Suspended Solids, _ � �pH, - - un fii3 Pirmit!tj - ­Mskor 460- 35- I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 .0, STORM EVENT CHARACTERISTICS: Date 11-09-17 (first event sampled) Total Event Precipitation (inches): 0.17 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Ter 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an onainal and one aoav of this DMR including all "No Discharge" reports; within 30 days of receipt of the lab results (or at end of monitaringaeriad in the case of `No Discharge" renortsl to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �J/ !���3, /,, 2,d/ 7 (Signature of Permittee) (Date) Additional copies of this form may be downloaded at:.httl2:1/12ortal.ncdenr.o[gLweb/wci/ws/su/nr)dessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 V� ENCO Labor-atories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone. 919.467.3090 FAX: 919.467.3515 Wednesday, November 22, 2017 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: P06284063, Project Name/Desc: Washington Stormwater ENCO Workorder(s): CA10051 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, November 10, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/ procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL ihls repot relates only to the sample as recelved by the laboratory, and may only be reproduced In full. Page 1 of 7 Ce N' e a www.encolobs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall Opt Lab ID: CA10051-01 Sampled: 11/09117 13:50 Received: 11/10/17 10:00 Parameter Analysis Date/Time(sl Preoeraden EPA 1664A EPA 1664A Hold Date/Time(s) 12/07/17 Prep Date/Time(al 11/18/17 12:15 11/21/17 15:46 Field NO PREP 11/09/17 14:04 11/09/17 13:50 11/09/17 13:53 SM 2540D•1997 NO PREP 11/16/17 11/14/17 18:25 11/14/17 18:25 FINAL Thts report relates only to the sample as recehed by the laboratory, and may only be reproduced to full. I Page 2 Of % �� 9 www.encolabs.com SAMPLE DETECTION SUMMARY alone ID: Outfall 002 Lae M. CA10051-01 Anal Results tin lam. PQL dolts Method lYetas 01 & Grease (HEM-SGT) Nan -Polar Material 3.94 ] 2.70 5.00 mg/L EPA 1664A pH 7,51 0 0 pH llnits Field Temperature 17.4 0 0 °C Field Total Suspended Solids 2.8 2.5 2.5 MO. SM 25400.1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 3 of 7 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 002 Lab Sample I13:CA10051-01 Received: 11/10/17 10:00 Matrix: Surface Water Sampled:11/09/17 13:50 Work Order: CA10051 Project: Washington Stormwater Sampled By: Client Chemistry Parameters ^-5VWmr-tW&w'rtfflP+C 5911 Analyte rCAS Number l gesyl>a an Will Qp H" E" Balch Math yQ Anabse t BY No Total Suspended Solids^ 2.8 mg/L 1 2.5 2.5 71(14008 SM 2540D-1997 11/14/17 18:25 OMR Field Parameters Analda ICAS Nun1W Result Flag Malls RP MIN MI. Batch Method Anahmw B11 No PH 7.51 pH Units 1 0 0 71<13010 Field 11/09/17 13:53 CLI Temperature 17.4 °C 1 0 0 7K13010 Field 11/09/1713:53 CLI Classical Chemistry Parameters Analvte rQAS Numberl Oil 6 Groh (HEM-SGT) Non -Polar Material Resin fin umm QE MIX E" Batch Math gd Anal laed BY 1= 3.94 1 mg/L 1 2.70 5.00 71(18002 EPA 1664A 11/21/17 15:46 SMA FINAL This report relates only to the sample as recelVed by the laboratory, and may only be reproduced In full. I Page 4 of 7 r err www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control B81'rY! 7KI4000 - MO PKEP Blank (7K14008-8LK1) Prepared & Analyzed: 11/14/2017 18:25 Spike Source %REC RPO Analvte Result Flao POL Units Leval Result %REC yinAtg RPD L1Dllt Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7K14008-111lSi) Prepared IN Analyzed: 1I/I4/2017 18:25 Spike Source %REC RPD Anal 1[ta Result Elm R'OL unb Laval Result %REC LIMN RPD Lit Notes Tote} Suspended Solids 93 2.5 mg/L 100 93 80-120 Duplicate (7K14008-DUPi) Prepared & Analyzed: 11/1412017 18:25 Source: CA09948.01 Spike Source %REC RPD Analyte Result Flaq POL Units Level Result %REC Limits RPO Lbt Notes Total Suspended Solids 260 50 mg/L 250 3 20 Duplicate (7K14008-DUP2) Prepared & Analyzed: 11/14/2017 18:25 Source: CA11394-01 Spike Source %REC RPD Analyte Result Flaq POL Unite Level Raoul %REC Llml18 111130 Lll1111111 Notes Total Suspended Solids 260 50 mg/L 270 0.8 20 Classical Chemistry Parameters - Quality Control AWdl11KISM - EPA J"W Blank (71(18002-BLK3) Prepared: 11/18J2017 12:15 Analyzed; 11/21/2017 15:46 Spike Source %REC RPD Analvto Result Flaq POL Units Level gesul %REC Uml RPD LIMB Notes Oil & Grease (HEM -SG) Non -Polar Material 2.70 U 5.00 mg/L LCS (7K18002-851) Prepared: 11/18/2017 12:15 Analyzed: 11/21/2017 15:46 Spike Source %REC RPD Anal BEsult Elm POL Units Level gffiul %REC Limlta RPD UMLI Rotes Oil & Grease (HEM-SGT) Non -Polar Material 79.3 5.00 mg/L 816 96 64.132 LCS pup (711(38002-13SDI) Prepared: 11/18/2017 12AS Analyzed: I1/21/2017 15:46 Spike Source %REC RPD Analvte Remit Flea POL units Level gesul %REC ylm)tg RPD UMB Notes Oil & Grease (HEM -SG 0 Non -Polar Material 88.5 5.00 mg/L 79.4 112 64.132 11 34 Matrix Spike (7K18002-MSI) Prepared: 11/18/2017 12:15 Analyzed: 11/21/2017 15:46 Source: BA04918-01 Spike Source %REC RPD Analyte Result Flaq POL Units Level Result %REC jjtl11� RPD LlNlt Notes Oil & Grease (HEM-SGT) Non -Polar Material 67.9 5.00 mg/L 73.0 2.70 U 93 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 5 Of % www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quandtation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soll samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL. This report relates only to the sample as receNed by the laboratory, and may only be reproduced In full, I Page 6 of 7 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIWOO-bUST61!)Y'RECORD, www encotabsxam � �. �' !�T€°.�reftlii�tiCi• !ra�O�kuxfew�uitiOIIcut;�anis-lri- [o.'FE,WapCut+tio:�dumtuC"!� - - �J�dx=`'i:l7"es �iti�lgp<�'t�9Y3#Ury�"i � �+ty #t4"7€r'.rlt_• t4:pw> 43-,f rlutIM)IM -01 fliogywxvr cwm--A) jo av:a►�R'. oa a �n� .z'; ispage 9R+l�fl@fHll:Fha5uaglSY Ipo'ic'k"=�Flrye�. F�ifrna�tut3.f5�.. r ._ . i]¢tjffitcTo- ��.�• . i��q. } f�+� fir#MraingxrS*! ;f i� �aV1A7St ?i!M f3�aT7arrn � FSu�tw" fr WWI" #L�si�.orFBp �JtCY�n rn m V O ✓r Wat [ti b Lrfam N14* cp" �,• � M .may flcti[t'SCtt'Jw s f��: T�G7��miiva�nr"�.f;�m��VaL'� �YncAm,ruSW-fat�.:t�r�•t7aa+l+r�aba A'.+� bS�ria!':�laLi(trfnrlf!Ynt+t3[s P�r►earatiaft�i-tmi Ft.:f�3tU11N33'S�t-4`+C� F96slo�ii"�-Lk►uK3N13tittFhi��R�nw•`s4t Now :AN.wjqqftb ittmdtbii#baka i:ian molt -I im 5 d'!(ifa 1�41 Pft-tv no MOd rKflenapieeehal Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted May 8, 2017 CERTIFICATE OF COVERAGE NO. NCGO8_0_ 7_ _8_6 FACILITY NAME Republic Services of NC. LLC_- GDS-Wa_shi_ngton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY ENCO Lab Cert. # 592 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow ❑Water Supply ❑SA ®Other C: Sw, NSW MAY 15 2017 CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of iiew" ring%r on per month? _ yes _x_no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall= No Date -_ s -,Sample Collected, mo/dd/yr a_0053fl = {=004{m' _ _ =00556 Y :,- Total=5usperided _ Solids,_ g/L , - -. ,pH, =' _ ,; , - Stan and unEts Non-Polar'O�l and Grea_se/TPH:EPA Mi thod�f (50 HEM), mgJL New Motor, Oil Usage, ,. :Annual average gal/mo Benchitark = -- _ k'$fl or 1Q0 seeermrtf= . _ ` Withrri;6 fl 9.0_ _ _ w Outfall2 04/25/17 4.4 7.84 26.9 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) ry0utfall_ Date .� ---Y�..L - e - 00556' �-yam 004fl0 - _0E}530 No Sample Collected = NorrPalariiancl Grease/TPH EPA Method "` To#al 5uspertded.Scii�ds, �_ �- =pH, - - riio/dd/yr= - � 16fi4 [SGT=HEl1A} `mgll -="� Standard snits- - rng/L-FINE Q 023 t?ar1�=see:perrrirt�� W E � 1 0-90 _ `-� � _= I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 5WU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 04-25-17 (first event sampled) Total Event Precipitation (inches): 1.13 _ Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMX including all "No Discha e" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" rMortsl to: Division of Water Quality Attn: DWQ Central Files . 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that therelare significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.oriz/web/wq/wsisu/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 OP ENCO Laboraton'es Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 4, 2017 Republic Services of NC (RE014) Attn: Matt Einsmann 5111 Chin Page Rd Durham, NC 27703 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Washington Stormwater ENCO Workorder(s): CA00067 Dear Matt Einsmann, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, April 26, 2017. Unless otherwise noted in an attached project narrative, all samples were received In acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except In full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Ile Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as receKeed by the laboratory, and may only be reproduced in Full. Page 1 of 7 www.encolabs.eom SAMPLE SUMMARY/LABORATORY CHRONICLE Client 1D: Outfall 002 Lob 1D: CA00067.01 Sampled: 04/29/17 08:00 Received: 04/26/17 10:15 Parameter Hold DateMmefol Preo DMIltme(s) Anatals Date/me(n) EPA 1664A 05/23/17 04/28/17 12:07 05/02/17 13:49 Field 04/25/17 08:14 04/25/17 08:00 04/25/17 08:00 5M 254OD-1997 05/02/17 04/27/17 13:50 04/27/17 13:50 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, I Page 2 Of % www.encolabs.com SAMPLE DETECTION SUMMARY Client I0: Outfall 002 Lab ID: CA00067-01 Anillris RUMI so Elite H" EGl mab Method Nltt� Oil & Grease (HEM-SGT) Non -Polar Material 26.9 2.70 5.00 mg/L EPA 1664A pH 7Z4 0 0 pH Units Feld Temperature Total Suspended Solids 20.4 0 0 °C Field 4.4 2.5 2.5 mg/L SM 254OD-1997 FINAL This report relates only to the sample as recewed by the laboratory, and may only be reproduced In full. Page 3 of 7 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 002 Lab Sample ID:CA00067-01 Received: 04/26/17 10:15 Matrix: Surface Water Sampled,04/25/17 08:00 Work Order: CA00067 Project: Washington Stormwater Sampled By: Micky Hopkins MONSOON Classical Chemistry Parameters Anelyte rCAS Number'! $OS1111b Elm maw lE MU EIL 1;IS Method Analyzed HY ii= Total Suspended So11dsA 4.4 mg/L 1 2.5 2.5 7D27005 SIM 254OD-1997 04/27/17 13:50 OMR Field Parameters Ana a rCAS Numberl Bawl" flag M= lE HL EM muh MothAnalyzed Ay now pH 7.84 pH Units 1 0 0 7D27011 Field 04/25/17 08:00 CLI Temperature 20A °C 1 0 0 7D27011 Field 04125/1708:00 CI.1 Classical Chemistry Parameters Oil fi Grease (HEM-SGT) Non -polar Material Rwulm flag lmnits DE ML EM MG11 Math Qd Analyz Bx lNote 26.9 mg/L 1 2.70 5.00 7D26015 EPA 1664A 05/02/17 13:49 SMA FINAL This reW relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 4 Of 7 www.encolobs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quallty Control All & h 7027O05 - NO PREP Blank (7D27005-BLKI) Prepared & Analyzed: 04/27/2017 19:50 Spike Source %REC RPD AnatM Result Flan POL Units Level Result %REC Wall RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7D27005-BS1) Prepared IN Analyzed: 04/27/2017 1150 Spike Source %REC RPD Anal1d4 Rmit Elm EQL Units Leval Resul %REC Ural RPD Limit Notes Total Suspended Solids 90 2.5 m9/1. 100 90 80-120 Duplicate (7D27005-DUPl) Prepared dr Analyzed: 04/27/2017 13: 50 Source: CA04256-02 Spike Source %REC RPD Analvte Result Flaq POL Units Lave! Result %REC Jbio RPD Limit L'!otes. Total Suspended Solids 1900 250 mg/L 2400 20 20 Duplicate (7D27005-DUP2) Prepared & Analyzed: 04/27/2017 13:50 Source: CA04764-01 Spike Source %REC RPD Analvte Result Flaq POL units Level Resulj %REC Ldmi RPD Limit bates Total Suspended Solids 74 25 mg/L 160 71 20 QM-12 Classical Chemistry Parameters - Quality Control BBtcii 7026015 - EPA 16"0 Blank (7D26015-BLK3) Prepared: 04/27/2017 15:00 Analyzed: 04/28/2017 13:17 Spike Source %REC RPD Anaivte Result Flea POL Units Laval Result %REC Limb RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2,70 U 5100 mg/L LCS (7D26015-BSI) Prepared: 04/27/2017 15:00 Analyzed: 0412B/2017 13:17 Spike Source %REC RPD Anal Ytp 9Cilllt Elea FAL Un11111 Level Result %REC LdmlRPD Limit !Limes Oil & Grease (HEM-SGT) Non -Polar Material 69.9 5.00 mg/L 81.3 86 64-132 LCS Dup (7D26015-BSD3) Prepared: 04/27/2017 15:00 Analyzed: 04/28/2017 13:17 Spike Source %REC RPD Analvte Result Flag POL Units Level R45LllL %REC Umi RPD Limit Note0. Oil & Grease (HEM-SGT) Non -Polar Material 57.8 5.00 mg/L 82.0 70 64.132 19 34 Matrix Spike (7D26015-M51) Prepared: 04/27/2017 15:00 Analyzed: 04/28/2017 13:17 Source: BA01823.01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Raoul %REC u rni RPD Limit Boom Oil & Grease (HEM-SGT) Non -Polar Material 48.1 5,00 mg/L 74.1 2.70 U 65 64-132 FINAL This report relates only to the sample as recehred by the laboratory, and may only be reproduoed In full. Page 5 OT % www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quandtation limit (PQQ and Is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative Identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 6 of 7 CMVln%JMMCPl1ALt.vnJcrivA1(viVL.ADUMAIUMICD iinAm-ur-uurtvL)T Mr-UvMt) www.encoiaDS.COM f ir1775 Camara{ Pon Dr. 4a10 ExeCdNa Park COw, Swo 111 t0Y•A WoodwkWs kxkWh al Ct. Ortardo, FL 32824 ,lacks"ft, FL 32216-6M Cary, NC 27511 (407) 82fr5314 Fpi (4M &W-W45 (904) 2D&WI7 Fax (9pi} 296-6210 (919) 467-3090 Fax (919) 4V-3515 Page of T Cberd Name Project Number RogmhFMd Aeatysas Requested Turnarp o 7 Times tD Note: RAU40raKowme 3 m AQdress 7cem accantanee by the teat (L C4.15T1Zip PO 4 f Ird+1 88 0 m _ C2 0 _ _ Standard Tat Fax CMACI 28 464-24 4 Ra Hoffman l g 2 Expedited Sarnprs) Name. A1t7 mwn (Pratt) Bary cwtw Lucas Norris •gi•nn v � (n � Due Sarnptp s} Sxe Loc9mm / rerrc Zms Lab Yl orkorder f�/ /(jam}. Vf I ,rrs a CA00067 � Mas Codas) fCoftim as nncassary) Wooc*m M4 Tatar ■ a Hera s sample tie (Meta 10eaUhmbon) Cdectlon Data Time Cane r Grab (see codas) Co Vainem Sample Comments s 17 I ain.y I QIACa I 17,,K.., ,7A //AG t Ic—Total,4 n1 Cnnininom Serape ICQ PteParap BY Pata/iime Rp6rr Osnad r balvThrm 6y DatalFer7e Cam--SpecW R" Wrp Regtarmnarits D uwnma ivad 13 Dataf w* PmWxg fished By Datefrvne Het D84aJreris , Coder 1t Z. Temps on Receipt r e®ip1 lc7,7AC:,tatYe LJnaccepta6Fe klmu : ow4u wwvrmr 64j-Sdi Ow-um*wg Wafer sE-5 a SAY-Slrrtaoe WatOf ww-NraSl6Netar A-Atr p-0IMr 4WWO n OWMTMMU PMSOMeit4n: I-" H+U N-HMM S•H2504 lip-rUUH 9-00W (do&-d u1 OOt "o7W Note : AN sempas sued lQ ENCO Labs are m accordance with the Imms and Wrratfi m Row m the reverse of ttds lom rudest prior w=m awownvs exits Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted January 3, 2017 CERTIFICATE OF COVERAGE No. NCG08-0— —7— —8— —6— FACILITY NAME - Republic Services of NC, LLC — GDS-Washinpton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY ENCO Lab Cert. # 592 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD 0 Jan -June N July -Dec or El Monthly'. (month j DISCHARGING TO CLASSF]ORW F]HQW [—]Trout E]PNA Elzero-flow Dwatersupply [:]SA ®Other C. Sw, NSW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x—no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) 0 No discharge this period' 7'v 2— 7. X ;�Siimp e' -ol ""AE 0, t t nitiM 't -NNE N7 -gal V- :"ye!o6-s1Perrnit� WftfiifiT6i0-M �..7 - Outfa1]2 12/13/16 <16 7.11 <2.70 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) 66t ate­Z, WNH =S�m0fiFC61Wt . C- =- N6n;P6Iar-djI i4lEPNMitK6d ---— dtal�SUCD—nrdd&taii&w ff12; lAdlyr M��GMSGT-HEM)prC —AW11 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 �i STORM EVENT CHARACTERISTICS: Date 12-13-16 (first event sampled) Total Event Precipitation (inches): 0.25 _ Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copv of this DMR, includina all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) � : (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/nr)dessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted May 16,2016 CERTIFICATE OF COVERAGE No. NCG08 0 7 8 6 FACILITY NAME Reoublic Services of NC. LLC — GDS-Washinp-ton COUNTY Beaufort PERSON COLLECTING SAMPLES N. Hopkins LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD 0 Jan -June Ej July -Dec or [] monthly' month or DISCHARGING TO CLASS DORW [:]HQW [—]Trout E]PNA []Zero -flow OWaterSupply OSA ®Other C; Sw, NSW PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes —x—no (if yes, report your analytical results -in the table immediately below) RECEIVED 3 Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) MAY 2 aii- CENTRAi En j=,-- []-No discharge this period' 0 MW S Rf�& 6i&IiMf— X -�5 SoIidVrngj — 'n ard:dnits4% 4-N AM g5t.Metpoq-jLkb4. -MMI�Mg/ =;R, - New Motor Oil �4i �;9 IR IAnnuat averse of .mo ftd&.ioksee penmig Ad wwd,��"— W Outfall 2 05/03/16 11 7.02 5.16 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) Outfall --DrakiF�,f ;5 56 EP- PAN od—' kth­ 09 pH; ­-=.- 11— iidX o -Rq' em INg �Piirmif Li iit = i7T 6.6 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: 'Date 05-03-16 (first event sampled) Total Event Precipitation (inches): 1.01 _ Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Moil an original and one tope of this DMR including aft "No Discharge" reports within 30 days of receipt of lab results for at end of monitoring period in the case of -No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/nt)dessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 h0&090'1n 0 ENCO Laboraton"es Accurate. Timely. Responsive Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 I � : t Thursday, May 12, 2016 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: (none], Project Name/Desc: Washington Stormwater ENCO Worikorder(s): CZ04981 Dear Ray Hoffman, Enclosed Is a copy of your laboratory report for'test samples received by our laboratory on Wednesday, May 4, 2016. Unless otherwise noted In an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory, This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 1 of 7 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Cllent ID: Outfall 002 Lab ID: CZ04981-01 Sampled: 05/03/16 10:40 Received: 05/04/16 10:00 Para Hold DatelTlme(s) Prep Datemme(sl Analysis DatefflmeW EPA 1664A 05/31/16 05/10/16 14:29 05/11/16 17:19 Field 05/03/16 10:S4 05/03/16 10:40 05/03/16 10:40 SM 25400-1997 05/10/16 f 05/09/16 09:10 05/09/16 09:10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in ruo, Page 2 Of 7 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 001 Lab ID: CZ04981-01 Oil & Grease (HEM-SGT) Non -Polar Material 5.16 2.70 5.00 mg/L EPA 1664A PH 7.02 0 0 pH Units Field Temperature E 21.7 0 l 0 °c Field ) Total Suspended Solids k 11 6.2 ; 6.2 mg/L SM 254OD-1997 FINAL This report relates only to the sample as re<etvW by the laboratory, and may only be reproducm in roil. Page 3 Of 7 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 002 Lab Sample ID:CZ04981-01 Received: 05/04/16 10:00 Matrix: Surface Water Sampled:05/03/16 10:40 Work Order: CZ04981 Project: Washington Stormwater Sampled By. Nicky Hopkins (Classical Chemistry Parameters i - EA► O Carr ck MW anaW[AC 59r1 Analtrte MAS Numberl Results EMU ULM& Qg Ku Ea A= Method Ana110111d By NQlap Total Suspended Sollds^ 11 mg/L 2.5 6,2 6.2 6EO9004 SM 2540o-1997 05/09/16 09:10 MMR Field Parameters Analyte rCAS Num Results Ely Mab QF MU Ill I= Medved A04133 By Ngg1 pH 7.02 pH Units 1 0 0 6EO6014 Field 05/03116 10:40 CLI Temperature 21.7 °C 1 0 0 6EO6014 Field 05/03/1610:40 CLI Classical Chemistry Parameters AnallRe MAS Numberl Resu LS E619 MOLL QF 1111 QQL limb Mcd Anal By I14ta:i Oil & Grease (HEM-SGT) Non -Polar 5.16 mg/L 1 2.70 5,00 6E10015' EPA 1664A 05/11/16 17:19 SMA Material FINIAL This report relates only to the sample as recelved by She laboratory, and may only be reproduced 0 rull, I Page 4 Of 7 www.encolobs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6EO9004 - NO PREP Blank (GE09004-111ILK1) IPrepared & Analyzed: 05/09/2016 09:10 1 Spike Source %REC RPD Analide RtdruEt an E" waits Level Result %REC Limits RPD Limit NaLn Total Suspended Solids 2.5 U 2.5 mg/L LCS (6EO9004-BSI) Prepared & Analyzed: 05/09/2016 09:10 Spike Source eAoREC RPD Anal Resul Eiaa EM unb Level R0S* %REC Umb RPD Limit Notes Total Suspended Solids 92 2.5 mg/L 100 92 W120 Duplicate (GE09004-DUP1) Prepared & Analyzed: 05/09/2016 09:10 Source: CZ04490-01 Spike Source %REC RPD Anal ]de Ecil t Elan M rialto Level Resul %REC LIMitil RPD Limit Notes TotalSuspended Solids 51 25 mg/L 57 11 20 Duplicate (6E09004-OUP2) Prepared & Anatyzed: 05/09/2016 09:10 Source: CZ04501-01 Spike Source %REC RPD Anal tde Result E132 PQL Units Level Result %REC Llmitil RPD Limit Notes Total Smperxled Solids 200 50 mg/L 200 2 20 Classical Chemistry Parameters - Quality Control Batch 6EIO015 - EPA 166" Blank (6E10015-BLK3) Prepared: 05/10/2016 14:29 Analyzed: 05/1112016 17:19 Spike Source %REC RPD Anal lde Result Elaa P91 Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM -SG) Non -Polar Material 2.70 U 5.00 mg/L US (6E10015-051) Prepared: 05/10/2016 14:29 Analyzed: 05/11/2016 17:19 Spike Source %REC RPD Ai>alYt® Result EW EU gob Level Rt autt %REC Llalita RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 62.0 5.00 mg/L 77.5 80 64-132 LCS Dup (6E1001S-8SD1) Prepared: 05/10/2016 14:29 Analyzed: 05/11/2016 17a9 Spike Source %REC RPD Ana heia Molt Elsa EM t181t5 Level Result %REC Lim[ RPD Limit dam Oil & Grease (HEM-SGT) Non -Polar Material 64.5 4.40 mg1L 71.7 90 64-132 4 34 Matrix Spike (6E3001S-MS1) Prepared: 05/10/2016 14:29 Analyzed: 05/11/2016 17:19 Source: BZ01906-02 Spike Source %REC RPD Ana llde Result Elan P.4L knit$ Level Result %REC Llailti RPD Limit Notes Oil & Grease (HEM-SGT) Nat -Polar Material 61.4 5.00 rng/L 75.8 4.47 75 64-132 FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 5 Of www.encolabs.cam FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value Is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation,llmit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 6 of 7 -- -�' 4w 4M 1077SC nbwPCrtDr. O. F! 321124 (407) V65314 FOX MM B504M A CaerA NMW Prayscr Nrnnber 'RepUbljr. LelyipegNCR EO 141 frionge) AAA P+aie4' Naaleraeac 1220 Commerce SL SW Box 1 Washington C tzfp Po a rEMM wb Conover,'NC 28613 TO Fax stem'" Card= 828 464-2414 �� !lay Hoffman S=MWs)14=m. AUUM (Ptifttl BOM Can= I Lucas Norris s.�rwi.) sYte 1�n � Tr1ne zone Aa CCOOCthn 11am a Sarr4is ID (FkW ldenutiutwo) Cobw"O pate TOW Comp tOf 1 -- 4610 E7recuai+i9 Perk Cant ss ' i 11 _ _ - - 102-A. Woodwinft hYriatSri4! Ct. �.• .�. ,fa�, FL 322164M Cary, NC MI I MA) 296=7 Fex "1 Z6&R210 101014$7-3W Pay (919) 4S746IS sa Ma1rEa- ram s ce Tate) N of Containers Page _ of RequestedTumarou o 'rimes Now . Rush gK;Le= aua(ec a=*PU -Cr by foe t5dUty a Standard Expedited Due _i l .ati Wori�rder CZ04981 Sample Comments Ser{p1a Ka Praperau By Da1eltkna Owarrane FrOOMovy Dow 7w Common:ISpaual F1.ppnfrg Remmwnmlffi R - DataTsne By Wealrveya ReWxpLo.wed By DaImMre PA- Dataffw e - COWernaTampsanRpco:p[ >/I C XMMnwpm PIWOO 3 • �L d - 'T # � �% Acceptable Unacceptable MEM CaYFCitaullaMM SO -SW UW4bU*Mg W8W SE-SeMMnt SW,-" ace Water -WW-yKazta� A4W 04MM (GUO In aeenM) Prv2&rVitlOn: t4CM WHO M4V9U3 SHZS' W-rt3OH CHMMIdetadia cgsrxnerrtsl NM: Al samphs sr6rrtitmd so ENCO tabs are in accordx= wM pre terms NO oandmem ftft on No rarersd of nru bM. raOM Pft wrCOn egreements OjO n M. Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted November 16, 2015 CERTIFICATE OF COVERAGE No. NCG08-0— —7— —8— —6— FACILITY NAME Republic Services of NC, LLC - GDS-Washington COUNTY Beaufort PERSON COLLECTING SAMPLES N. HoRkins LABORATORY ENCO Lab Cert. # 591 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD 0 Jan -June M July -Dec or F1 monthly' (month) DISCHARGING TO CLASS F]ORW F]HQW E]Trout [:]PNA Flzero-flow E]Water Supply EISA REC EIVED ®Other C; Sw. NSW NOV 2 3 2015 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTRAL FILES Did this facility perform Vehicle Maintenance Activities using more than 55 gallonfWReMq-ZoNil per month? _yes -x-no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) E] No discharge this period' No Collected,Alotiltlik Sample---, d N&4)a lir0 i I n&6 his$WT�p A. EPAR 4�Newr. ,o FfibTId - Solid �Wffa 'Standard . jMeVkd& 664ISGTMEM); 7iul: ='Annual averagej�ol/�F see perrn Outfall 2 11/03/15 4.9 7.1 7.92 <55 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) - 0. - -- 1 � V- 5 id mo/o dlje- Im - - ---o , ta �6 - - �00530 Rim, - 7 00400( Nonlft -.a Oil and d,- G r 6 i e - T P Me tk6d k!EOA 604SGT7A -j� -z- e E) -1 d �z -,p 4� ai�d:units"- t 5- ti� 106e it 0 rm .0 �-J�6' I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here_ SVIU-250 last revised April 11, 2013 Page I of 2 STORM EVENT CHARACTERISTICS: Date 11-03-15 (first event sampled) Total Event Precipitation (inches): 0.47 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑-NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMIt including all "No Discharge" repartsiwithin 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal,ncdenr.orp/web/wa/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, November 13, 2015 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Washington Stormwater ENCO Workorder(s): C513042 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, November 4, 2015. Unless otherwise noted in an attached project narrative, all samples were received In acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 1 of 8 Coco www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE LD dlent I0: Outfall 002 Lab ID: C513042-01 Sampled: 11/03/15 12:45 Received: 11/04/15 09:30 Mramete EPA 1664A 12/01/15 Prep Date/Timefgl 11/09/15 Analvals_DatelTlme(s] 16:14 ItA1115 11:51 SM 254OD-1997 11/10/15 11/09/15 09:30 11/09/15 09:30 SM 4500H+B-2000 11/03/15 12:59 11/04115 14:15 11/04/15 14:15 FINAL This report relates only to the sample as reoelved by the laboratory, and may only be reproduoed In lull. I Page 2 0f I www.encDlabs.com SAMPLE DETECTION SUMMARY dlent 1D: Dutfall 002 Lab 1D: C513042-01 aAna It03m(14 fhkg EQL h= Oil & Grease (HEM-SG1) Non -Polar Material 7.92 2.70 5.00 mg/L. EPA 1664A PH 7.1 1.0 1.0 pH SM 4500H+B-2000 Q-01 Total Suspended Solids 4.9 3.3 3.3 mg/L SM 2540D-1997 FINAL This report relates only to the sample as received by the laboratory, and may 0* be reproduced in full. I Page 3 of 8 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 002 Lad Sample ID:C513042-01 Received: 11/04/15 09:30 Matrix: Surface Water Sampled:11/03/15 12:45 Work Order: C513042 Project: Washington Stormwater Sampled By:Nicky Hopkins Classical Chemistry Parameters ^ - EACO Cary C&VI d analyt& (AC• 5911 Anatvta_ICASNumberl Results finp units RE • KU Ml A= mem Anal li Q ft N pHA 7.1 pH 1 1.0 1.0 5K04022 SM 4500H+B-200C 11/04/15 14:15 AE9 Q-01 Total Suspended Solid5A 4.9 mg/L 1.33 3.3 3.3 5K09003 SM 254M-1997 11/09/15 09:30 MMR Classical Chemistry Parameters Analvte_fCASNumberl Resul f1w Mau RE H, EU A=11 Meth Analyzed ley I�f�9 Oil & Grease (HEYI-SGO Nan -Polar 7.92 mg/L I 2.70 5.00 5K09012 EPA 1664A 11/11/15 11:51 SMA Material FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 Of 8 �0Q www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SK04t022 - NO PREP LCS (5K04022-BS1) Prepared & Analyzed: 11/04/2015 14:15 Spike Source %REC RPD -Anahrte Rtsrdt Ba0 POL Units Level gesuf %REC Limilaf RPD Limit Notes pH 7.0 1.0 PH 7.00 100 99.101 Duplicate (SK04D22-DUP1) Prepared & Analyzed; 11/04/2015 14:15 Source: C513042-01 Spike Source %REC RPD Ana hrtC Hssult FIN Ml. Units Level Resul t %REC Limn RPD Limit Notes PH 7.1 1.0 pH 7.1 0.3 25 Batch SKOPOW - NO PREP Blank (SK09003-111.I(1) Prepared & Analyzed: 11/09/2015 09:30 Spike Source %REC RPD -Analyto Result flap POL Units Level Result %REC Llmita RPD Limit Hates Total Suspended Solids 2.5 U 2.5 mg/L LCS (5K09003-BS1) Prepared & Analyzed; 11/09/2015 09:30 Spike Source %REC RPD Anahrte Result F1ae POL Units Level Sesult %REC Limits RPD Limit Notes Total Suspended Solids 94 2.5 mg/L 100 94 80-120 Duplicate (SK09003-DUPl) Prepared & Analyzed: 11/09/2015 09:30 Source: C513263-01 Spike Source %REC RPD Anandaa Result Flag P41 Units Level Result %REC Limits RPD Limit Notes Total Suspend Solids 84 50 mg/L 72 15 20 Duplicate (3K09003-DUP2) Prepared & Analyzed: li/09/2015 09:30 Source: C313674-01 Spike Source %REC RPD -Anil Result fim PUL Units Level Begu(t %REC Limits RPD Limit Ngtes Total Suspended Solids 33 17 mg/L 35 4 20 Classical Chemistry Parameters - Quality Control Bauch SK09012 - EPA 166464 Blank (5K09012-BLKl) Prepared: 11/09/2015 16:14 Analyzed: 11/1112015 11:51 Spike Source %REC RPD -Anah to Restdt fla0 P.12L Units Level Resul %REC Limits RPD Limit Hates Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mgjL LCS (SK09012-851) Prepared: 11/09/2015 16:14 Analyzed: 11/11/2015 11:51 Spike Source %REC RPD .Anatide Randt Flan P41 Units Level Sew %REC Limits RPD Limit Hates Oil & Grease (HEM-SGt) Non -Polar Material 59.9 5.00 mg/L 79.4 76 64-132 LCS Dup (SK09012-BSD1) Prepared: 11109/2015 16:14 Analyzed: 11/11/2015 11:51 Spike Source %REC RPD Ana lYtB Resul Elm P" Units Level get %REC Limits RPD Limit Het Oil & Grease (HEM-SGT) Non -Polar Material 64.5 5.00 mg/L 78.1 83 64-132 7 34 FINAL This report mates only to the sample as receKed by the laboratory, and may only be reproduced In full. Page 5 o 8 www.encolabs.com QUALITY CONTROL DATA ClasslcaI Chemistry Parameters - Quality Control Batch 5900012 - EPA 1664A - Continued Matrix Spike (SK09012-MS1) Prepared: 11/09l2015 16:14 Analyzed: 11/11/2015 11:51 Source; 0504602-02 Spike Source %REC RPD .Analvte Result Flaq POI. Units Level get %REC u nits RPD LLMA Notes Oil & Grease (HEM-SG-0 Non -Polar Material 57.2 5.00 mg/L. 75.8 19.2 50 64-132 QM-07 L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 6 o 8 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. ' MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q-01 Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to me sample as recehted ply the laboratory, and mar only be reproduced in rill. Page 7 of 8 f�as.aaf.....frfof rVe.VIe�VeQYy.LV..■ - ® 70775 Central %n Pr, 4810 Executive Park Coup, Suite 11 i 102-A Woodwinds lndustrW Ct. Orlando, FL 32824 Jackaarr ft. FL 322164M Cary, NC 27511 _ (4u7) 926 5314 Fax (407) 950-G945 (904) 296.3007 Fa: (904) 296-6210 (919) 467-3090 Fax (919) 4673515 page of • 0D Clem Name aroiea Nurn er Reqmexted Anplyeea Requested Tumarou o onr i i� C nr' oifINIC r Al 1 r via` Times CO Name :Rush request sublet OCl 7 Atldrpss F'rOjecl�ldrnNF]i39C - - - accaplarce by am bacday d 1220 Commerce A f City/sTa ID PO e! EMN utmo Ciartover. C 2-8611 14 ? 50179 ('� m _Standard. a Tel Fax Reportnq Cana ff k28 464-2�4 f 4 �oZ ?�d �j� . Ra Hoftarl � � � � Expedited samyer(s} Name. Atfcn (Print) ei9inv Carsact -, I 2 - Due 161�4as Lucas Norris T 2 . (n { (n S—Oar(s) sae Lwat..l T. Zone Gab W orkorder Al " r45 z C 513 0-42 Preservation (See Codesi (Czrtbirm as new} Coflectiors t4la Total + co - F;^ sample lt) WIM raent:.ticatbn) Cdkecl" oam Time Camp/Grab (searndesj Contactors -Sample Comments K'st red ey - OaWraoe A; R By - - - t atan'-une - - Gw.,ftTp.oW Rep .WV Rerssremenu - De1Ml"una ROD" - mime flaiwg ashed 6y Dicarrt ne Received By s's 5 T 3 . Ic_d�__Upon Reaept V Acceptable Unacceptable WaNrx ; GW-G[acmdwater'SO-SW OWOrfnkinp Water SE-90ddWrtl SWSW4lae Wa:ar- VM-Wastewater A -Air O-OLhef (dot" in ramffwas) PreNW8110n: HCa H-HU N•HNU3 S-Fi2SO4-NO-MUK U-UV [ (MM JFI COffawMf Note: As sarrOes gmbuktted to ENCO Labs are at ac=dance with 0* [orris end ox4bons fisted on the reverse d this farm, utdess prior written aprvww to exist Semi-annual Stormwater Discharge Monitoring Report M for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted June 12, 2015 CERTIFICATE OF COVERAGE NO. NCG08_0_ _7_ _8_ _G SAMPLE COLLECTION YEAR 201S FACILITY NAME Republic Services of NC, LLC - GDS-Washington SAMPLE PERIOD ® Jan -June ❑ July -Dec COUNTY Beaufort _ or ❑ Monthly' (month) PERSON COLLECTING SAMPLES _ N. Hopkins RECEIV EUCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ❑PNA � LABORATORY ENCO Lab Cert. # 592 ❑Zero -flow [-]Water Supply []SA Comments on sample collection or analysis: JUN 17 2015 ®Other C: Sw. NSW CENT-RAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 C2 DWR SECriory C= Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x-no �0 (if yes, report your analytical results in the table immediately below) -C Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall w"Samp-je No. - {i053d - Total.Suspehded Solids;img,1 � - _ 0040(]! _ pH, StanaartJlunits_ - - �- 00555 Nor►-Polar-0�) and_G�ease/TPH=EPA Method 2664:(SGTyHEM), mg/L � New Motor Oil UsagN Annual average gal% - - :Bench_ a -SU a_ r flOsee=perm_ its _Withir6 0K�0 . _ _ 15� J - Outf 6/03/15 5.2 7.27 <2.60 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall e 1010ampllected, _. Q0556 _ DD531 OQ4W _ mo/dd yr Non -Polar Oil and Gr a '`JTP9 I PA'M od 16fr4 [SGT HEM};_mgJL -- Total=5usperided Solids, mg%f _ pli, 5tandarct uh - [P mrt;omit i a 0 N ON 15 _9910 3 1 NW- -H.M W50o iW- I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SW-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 6-03-15 (first event sampled) Total Event Precipitation (inches): 4.25 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: ^ Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted- Based on my inquiry of the person or persons who manage the'system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) / a - (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 _ _ Page 2 of 2 ENCO Luaboraton*es Accurate. Timely. Responsive. I»»arative 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 i I i Thursday, June 11, 2015 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 Conover, NC 28613 RE: Laboratory Results for Project Number: PO4154198, Project Nameldesc: Washington Stormwater ENCO Workorder(s): C506625 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, June 4, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further Information, please do not hesitate to contact me. Sincerely, r' K1�Ile Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduoed In full, Pago 1 of 0 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE CllentID: Outfal12 Lab ID: C506625-01 Sampled: 06/03/15 10:40 Receive!: 06/04/15 10:30 Para PMU Dat j/Tlme[sl Analysis Da6elTime(s) EPA 1664A 07/01/15 06/10/15 12:49 06/11/15 12:26 Field 06/03/15 10:54 06/03/15 10:40 06/03/15 10:40 SM 2540D-1997 06/10/15 06/04/15 14:00 1 06/04/15 14:00 FINAL This report relates Dnly to the sample as received by the laboratory, and may only be reproduced In full. Pape 2 of 8 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 2 Lab IM C506625-01 Analrte Resin ON Ma ML Mulls Meths tl210 PH 7.27 0 0 pH Units Field Temperature 24.7 0 0 ^C Field Total Suspended Solids 5.2 k.2 4.2 mg/L. SM 2540D-1997 i t , i FINAL This report relates only to the sample as received by the laboratory, and may only he repraduced In full. Pepe 3 of 8 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 2 Lab Sample ID:C506625-01 Received: 06/04/15 10:30 Matrix: Surface Water Sampled:06/03/15 10:40 Work Order: C506625 Project: Washington 5tormwater Sampled By. Nicky Hopkins CClassical Chemistry Parameters t ^ - EAC17 [.dry arolkd analyte (AC SvfJ Analyte rCAS Numherl Regilits I-l&a Malta U. NU RQL =11 Method Analn Ng�g Total Suspended So11dsA 5.2 mg/L 1.67 4.2 4.2 5FO4025 5M 2540p-1997 06/04/15 14:00 MMR Field Parameters AnalJU [CAS Number] lissulta Elea Malta BE MQL eQL Batch Mctlyod Analyzed am notes pH 7.27 pH Units 1 0 0 5F05005 Field 06/03/15 10A0 CLI Temperature 24.7 °C 1 0 0 5F05005 Field 06/0311510:40 CLI 1. Classical Chemistry Parameters Allaldll rCAS Numberl Resells Elsa Malta DE MQL EQL Batch Mdhud Analatid BY Notes Oil & Crease (HEM-SGT) Non -Polar Material 2.60 U mg/L 1 2.60 5.00 5FO9012 EPA 1664A 06/11/15 12:25 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced 0 rue, Pape 4 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SF04025 - NO PREP i Blank (SF04025-BLK1) Prepared & Analyzed: 06/04/2015 14:00 1 r Spike Source %REC RPD Ana h[ta Resu Elan ML llnlle Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5F04025-BSI) Prepared & Analyzed: 06/04/2015 14:00 Spike Source %REC RPD 9nahtte Result fin eal. Ua tt Level Result %REC Limns RPD Limit boots. Total Suspended Solids 90 2.5 mg/L 100 90 80.120 Duplicate (5F04025-DUPl) Prepared & Analyzed: 06/04/2015 14:00 Source: CSOS436-01 Spike Source %REC RPD Anal Result Elm M1 units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 4700 500 mg/L 5300 12 20 Duplicate (SF04025-DUP2) Prepared & Analyzed: 06/04/2015 14:00 Source: C506235-01 Spike Source %REC RPD Anal lda Result 112 MI. 1lnits Level Rewlt %REC Limits RPD Limit slates Total Suspended Solids 40000 2500 mg/L 43000 7 20 Classical Chemistry Parameters - Quality Control Batch 5FOOO12 - Same Blank (5F09012-BLKI) Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05 Spike Source %REC RPD Anal ]ria Besialt Elan EM units Level Result %REC LltDltt RPD Limit [lout Oil & Grease (HEM-SGT) Non -Polar Material 2.60 U 5.00 mg/L LCS (SF09012-11151) Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05 Spike Source %REC RPD Anal ltte Result Elsa MI. mum Level Result %REC Limlta RPD Limit Now Oil & Grease (HEM-5GT) Non -Polar Material 17.1 5.00 mg/L 21.5 79 6+132 LCS Pup (SF09012-BSD3) Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05 Spike Source %REC RPD Anal Yia Result Elan RM Units Level Resu1C %REC Urnita RPD limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 17.1 5.00 mg/L 21.5 79 64.132 0 34 Matrix Spike (5F09012-MS3) Prepared: 06/09/2015 15:00 Analyzed: 06/10/2015 15:05 Source: B502322-02 Spike Source %REC RPD Anal Yte Resu1L Elan P9L !inns Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 30.3 5.00 mg/L 23.0 341 NR 64-132 QM-07 FINAL This report relates only to the sample as racdvad by the iaboralwy, and may only be reproduced In ruii. Pape 5 of 8 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received try the laboratory, and may only be reproduced In full. Page a of a ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com - 1037r Cawhi Puri Dt. 48 W Exeeue M Park CWL SWQ 111 102,A Woodwinds OKRMVW Cl. Orlar=, F1,328;M . .ladaotwde. rL 9T21&sov Cary, NC 27511 - (467).82fr5314 Fax (407) a504945 ") 29&3007 Fa: (W4) 296.6210 (919) 467-3090 Fm,(919) 467.351s .Page at Clint Nartw Rmtect Number Requufsa ArWdysaa I Requested Turnaround liblic'StantiCes of r + Times AtStltass - Pro)dc7 Namc1€k!sa Note : hush requests wbj wl to 9=ptarm try qte hiclily [}'Commerce St SW Box I Washing n St mwa er- oty)sra p PO to t B&Uv ir:lo- Conover, NC 28613 O 7(,.;' 9� Lt _ Standard Tat Fax RcflwLrtp Can= Cn r p - 8.28) 464-2414 Ray Hoffman < Expedited surfs) Kvpe, OAK/aauon(Prat) awn coraaa Due __Jl C f1 r, Lucas Norris SAMAiar(fi) SRO Location! TEmu 7.mw Lab�fii6ff(DfdBr - %y OL,JC7�J Preservation (sea Codes) MOT—*u necessary) Coaecmn M1a6rrtx Twat a at I tram a sawok to (Rigid ftnt1;coml CaBecaat Dan Tin* r or= r G= (see aaaas) cavasrars f Sample Comments i �L r a r -Total # of Containers s W Kd Propwad By Dew Hdrnqumrt vd ey --pawrr" A By Daterfirm ! P; �'oyI ' Fkporling R-4LIft mtarrts RetstgUtted By E Dw.aiimo - DatISM"W Aakngt nn9d By DaWTinw j llj IioCeivoC 8y Paug nme _ Cooler rs & Tmnps an Aecmw Cj_ 3 #� G Con�bw upon Rao* e�Acceptabde Unacceptable USK*-: GW-Gr0Lwdw ser SD�Sos DW-Drarmrg Water SE-sodrwm sw-sw ace LVarer W W-Y.—dsww ar A-Aa 0-02UN (Waa in conxirer:M). Prosa<ratlon_ "M H-HG N-KNW S-H2SO4 KWI40H G43M r (detail in 0WTWmrds) NDto AN samples serprri,led to Ef4W Lam are to &=wdence w4h ttw farms andmneffipns rrs;ad ae 7re reverse of eis Wm, udass W= w#Wn aReerrwnts mrst Page 7 aF a Sample Preservation Verification ENCQ Cary CCJ Work Order: C506625 Project: Washington Stormwater Client: Republic Services of NC (RE014) Project #: [none] Logged In: 04-Jun-15 11:3a logged By: Jennifer L. Jackson C506625-01 Cant Type f,' p Pros (pH) Requirement p : , aakad, . In Control pHAdlusted a#e fine k " Adjusted Reagent Used/Comments. 1. A 1LA+H28O4 <2 Y! N I Y I N/ B 1 LA+H2504 t2 Y! N I Y/ N I N W r Rea ent Name ID 1 2 Rea ent Name ID 31 4 Rea.gent Name ID 5 6 Pape 8 of 8 f 1 Semi-annual Stormwater Discharfire Monitoring Mort for North,Carolina Division of Water Quality General Permit No. NCG080000 Date submitted December 9, 2014 CERTIFICATE OF COVERAGE No. NCG08 0 7 8 6 FACILITY NAME Republic Services of NZ LLC­- G—D—SAWa—shi—ngton COUNTY Beaufort PERSON COLLECTING SAMPLES M. Homard LABORATORY ENCO Lab Cert. # 442 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2024 SAMPLE PERIOD ❑ Jan -June E July -Dec or ❑ Monthly" (month] DISC I" TO CLASS 0ORW []HQW [jTrout F]PNA ECG Dzero-flow Dwater Supply F]SA ®Other C: Sw. NSW g&I-FILF-S PLEASE REMEMBER TO §16-N ON THE REVERSE --> cWR SECTIONDid this facility perform Vehicle Maintenance Activities using more than 55 gallons of n9wmotor oil per month? _yes -x-no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) E] No discharge this period1 -4 E : 00530'z W soe6di- W N(6 o—i01V zn - ­--kifild/,iii;� �-7 m A�IhK� g-­--Sfiindir&uhiti--`--.Method " ' .96ncWhiark.=0-­-- 8-046r�460 see;permii= F----7tffl—AWftfiiK--6 Ouffall 2 11/25/14 4.00 7.30 <2.40 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (if applicable) y No ­-D CqffibW _Collected, -g- `00556 6 N Polar Oil 9i TP k. EpwMkhbd-15 6 -(5GZ! Y. REM),� 64 u- i 56 Suspended F27 pi rm Limit !M�ISWFM�. 503 adljzsi�e permi z�q: L I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SVX-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 11-25-14 (first event sampled) Total Event Precipitation (inches): 0.32 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN'THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) y <3 e-, (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 0. ENCO Laboratones Accurate. Timely. Responsive. Innovative. 4810 Executive Park Court, Suite 111 Jacksonville FL, 32216-6069 Phone: 904.296.3007 FAX: 904.296.6210 f Tuesday, December 9, 2014 Republic Services of NC (RE014) Attn: Ray Hoffman 1220 Commerce St. SW Box 1 . Conover, NC 28613 RE: Laboratory Results for Project Number: [none], Project Name/Desc: GD5-Washington ENCO Workorder(s): B402587 Dear Ray Hoffman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, November 26, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chris Tompkins Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Pega 1 of 7 (a Nik I CM w► www.ancolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall 2 Lab ID: 0402557-02 Sampled: 11/25/24 11:35 Received: 11/26/14 10:25 ParaWAIC Hold DatelTimefsl Ew DatalTlmefsl Analysis DamlTimefsl EPA 1664A 12/23/14 12/03/14 14:05 12/04/14 13:06 SM 25400-1997 12/02/14 12/02/14 10:23 12/02/14 AM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 2 of 7 www.encolabs.com SAMPLE DETECTION SUMMARY Cllemt M. Outfall 2 Lab ID: 0402sa7-02 9nallyte PASUIElm NU Em l= Total Suspended Solids 4.00 2.50 2.50 mg/L SM 25400-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. age 3 of 7 e■ r www.encolabs.com ANALYTICAL RESULTS Description: Outfall 2 Lab Sample ID:8402587-02 Received: 11/26/14 10:25 Matrix: Surface Water Sampled:11/25/14 11:35 Work Order: B402587 Project: GD5-Washington Sampled By:Nlcky Hopkins Classical Chemistry Parameters ^ • EAC0 0S M»yk ClYtlW arUWe fAIC 44V - Results flan Urga RE MU E21. @alsh Method Analyzed 1}1! N Oil & Grease (HEM) (C-0007) 2.40 U mg/L 1 2.40 5.00 4LO3005 EPA 1664A 12/04/14 13:06 MIF Total Suspended Solids^ 4.00 mg/L 1 2.50 2.50 4LO100B SM 2WD-1997 12/02/14 14:22 M]F I FINAL This report relates only to the sample as rwelved by the laboratory, and may only be reproduced In hAl, Page 4 of 7 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4L01008 - Same Blank (4L03008-BLK1) Prepared; 12/02/2014 10:73 Analyzed: 12/02/2014 14:22 r Spike Source %REC RPD AnalYtd, Res111L Elm EM glDlts Level Resldt %REC LWft RPD L[mlt Notes Total Suspended Solids 2.50 U 2.50 mg/L LCS (4L01008-BS1) Prepared: 12/02/2014 10:23 Analyzed: 12/02/2014 14:22 Spike Source %REC RPD Anal Result ON ML Un" Level Resu %REC LiMUS RPD MIDI& Notes Total Suspended Solids 111 2.50 mg/L 100 111 80-120 Duplicate (41.01008-DUP3) Prepared: 12/02/2014 10:23 Analyzed: 12/03/2014 14:58 Source: B404849-01 Spike Source %REC RPD Anal !Result flee EM YOU Level Resu R %REC LjDI(tg RPD Uall Ngtas Total Suspended Solids 130 2.50 mg/L 152 16 5 QM-12 Duplicate (4L01008-DUP2) Prepared: 12/02/2014 10:23 Analyzed; 12/03/2014 14:58 Source: B404763-01 Spike Source %REC RPD Anallfte Result F)aa E" UD tl Level Result %REC Lam(! RPD Limit Notag Total Suspended Solids 122 2,50 mg/L 120 2 5 Batch 4L030O5 - EPA 1664A Blank (4L03005-BLK3) Prepared: IV0312014 14:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD Ana Rouii W2 E41 MOM Level Resu %REC LlmllS RPD Limit Rye Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (4L03005-BS1) Prepared: 12/03/2014 14:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD ADalllte Result flan Ea gaits Level Result %REC L1t1111S RPD Lb a Motes Oil & Grease (HEM) 35.3 5.00 mg/L 41.4 85 78-114 LCS Dup (4L03005-BSDI) Prepared: 12/03/2014 14:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD Anal Result Elm EU Uhm Level RJR %REC Unifts RPD !,bft Notes Oil & Grease (HEM) 38.7 5.00 mg/L 41.3 94 70-114 9 18 Matrix Spike (4L0300544S1) Prepared: 12/03/2014 14:05 Analyzed: 12/04/2014 13:06 Source: B405230-01 Spike Source %REC RPD Anal Yt® Result flea E41 )tilts Level Result %REC Lal)a RPD Lb t Notes Oil & Grease (HEM) 69.3 5.D0 mg/L 44.4 21.8 107 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 5 of 7 s � www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85e/a or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. r FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 8 of 7 V I ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.eiicolabs.com 10775 Gaiitm;i funk Or. � 48 W jmmdiwl hark Coins. Suite i i i I[W=A Wongwuntls irxittsiriai CL �i (ndo. FC 32824 .Z:rcksorn�e. FL �2F6£Ori9 f=urY� NC �751 tOrlando. (4t77j82"314 Pax (44)711150-W45 (904)?6-3W7 17i (i1(34):iM-6210 IW!44TI-3twp Fm(919)467,LSI5 Page of Gkent Nano Republic Services of NC (RE014) _ Frey i Number Requested Anak+cis Requested Turnaround Times - NPtO: Rush �etlrr„-:3s atitNCf31t, mrcepLv tr7 the baciUy Standard _ Expedited Due l.�I r p C 6� Atldms5 1220 Commerce St. SW Box 1 - Prcgecl Hafki&D r - ashington 01Y.S rizip Conover, NC 28613 lKl 8 i fliam Info P04154198 TM F:t_x 828 484-2414 ;' �� ? ( ) f^• �i _ 3 Rapti hwj c-rnlnrl Ra Hoffman Y _ S.rmplrr(S} Mims. Aliilitirn (Fnnf) '.J _ HiUnl Ganiecl Ray Hoffman Ssmplegsl 5i/riite:re lr� t Sna l.oca€wn i rune ztna Lab WOrkorder. r v Fresmation 15" Cod esi IGanXB nr. as n"Assary). Items . Svnpk:11)(FvtdIgantleahuni Cu4ar2rtmLiam Ccft- Tin —1mX, comp!Graft Immi tsar::*3rcj 7Ut..t A cW r.rnaina<, I SampteComments Outfal[,1 _ SW- 3 X VX r Outfall 2 /1;' ' �N f;'J '11r• v Sw 3 X x < Total 6 of Containers — - .SwrPlu Kit l`tytared cty bntef7ime Reliext,:i5txd I3y Daiamriu; J {deceived By ( Dale,Tum Ej GrinnnuruslSpeci.-ii iirpamng flpgmefr u,Its P.a6ntplished By rTalp. me lief&,*o ey flat&Mn,e IiciNuislied BY Ti-itisTmc Revtli ^ J By f Data7inm Cnuler 4's & firrnps nn Hn-Qip1 e-� t e-' 2 '� Condnion Upon Receipt ptabie Unacceptable m trix : GW-Groundrtaler 5G-%rXI DWrOnn" SVatee SE-SockvicM SW-Sunace Water WW-Nhriewliter A•Air 0.06cr trbiilnir in cntri munbs} Preearwai6n; i-Tie H-HCI N-H1403 S412SO4 NO-NaOH 0 Cktwr(de d in comrnenls) m Not@: All ii impins m;bnulred to ENCO Utis alo in Vc0,Ltuwe with M mftll4 and t;&v.M ww lisle] on tr., t w mse of this lixrm, Lrde s pnx wditen agawntnts chm pV S � Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted _April 16, 2014 CERTIFICATE OF COVERAGE NO. NCGO8 0 7 i 8 _6_ FACILITY NAME Republic Services of NC LLC - GDS-Washin on COUNTY Beaufort PERSON COLLECTING SAMPLES M. Hoggard LABORATORY ENCO Lab Cen. # 442 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2014 SA RIOD ® Jan -June ❑ July -Dec RECEI or ❑ Monthly" (month) DISC ARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA APR 21 20 ❑Zero -flow ❑Water Supply ❑SA CENTRAL FILES ®Other C• Sw, NSW owatBOG PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform. Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) yes -x-no ❑ No discharge this period' OutfalfI"K00530 - No. al1suspended jS1_4s,Mg/! pH, Standard�units �-��—�-_•ems—�� W-Non-Polar O11 an d�Grease/TPH-E4FAn Methodxlf64 (SGTHEMj,,nng/nuala�erage New Mator Oifl Usa,o gal/mo- .Benehmarlc �- - 1Q0aee,permit 50 ar9:0 Witliin;CO - _ - _ _] 5 - Outfall2 04/08/2014 7.20 7.82 <2.60 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall Date ._ No. Sample Collected, mo/dcl/yr Non -Pots a iliand�Gr a e/TPH EPA Method 1664r(SGTHEM), rng/L TotallSuspended solids, _ _mg/�t 'i pH, Standard unitsN. .Permit Lt 'm -- 15 - 50"r�10U sit 6Q 9 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page l of 2 i1r t i dd' STORM EVENT CHARACTERISTICS: Date 4-08-14 (first event sampled) Total Event Precipitation (inches): 0.35 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: !f you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: a A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. a 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B. a TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one coov of this DMR, includin all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitoring period in the case o "No Dischar e" reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there ale significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) 4 (Date) Additional copies of this form may be downloaded at: htti3://Portal.ncdenr.org/weblwq/`ws/su/npdessw#tab-4 S WU-250 last revised April 11, 2013 Page 2 of 2