NCG080762_MONITORING INFO_20180201

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT N0.
IV C& M D -7(Q a
DOC TYPE
❑HISTORICAL FILE
5?, MONITORING REPORTS
DOC DATE
❑ ani-i 0 a fl I
YYYYMMDD

e
a Genesee & Wyoming Company
January 26, 2018
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080762
Dear Sir :
FFB 01 2018
CENTRAL FILES
DVVR SECTION
Please find enclosed our DMR for the second half of 2017. We are sampled from the holding tank that
we utilize to pump storm waters that are collected in the locomotive inspection/parking area of the
yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
Jason Woods
General Manager
North Carolina & Virginia Railroad • 214 Railroad Street North • Ahoskie, NC 27910. 252-332-2778 Fax [phone]

Semi-annual Stormwater Discharge Monitori E Report
for North Carolina Division of Water Quality General Permit No. NCG080000
CERTIFICATE OF COVERAGE No. NCGO80762
FACILITY NAME: NCVA Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: Aaron Blake
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis:
Date submitted: January 26, 2018
SAMPLE COLLECTION YEAR: 2017
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthiyl (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
[]Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —x_ yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
12/13/17
6.4
8.2
3.2
338
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS: All collected waters are held in storage tank until sampled and discharged
Date (first event sampled)
Total Event Precipitation (inches): NA —(water is contained in holding tank)
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement rer 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an on inal and one copy of this DMA including all "No Discharge" reports, within 30 days of receipt of the lob results or at end of monitoring period in
the case of Discharge„ reports) -to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
l-2Z6-7.,a1%-
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/wlsu/npdessw#tab-4
SWU-250
last revised April 11, 2013
Paize 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME: NCVA Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: Aaron Blake
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis:
Date submitted: January 26, 2018
SAMPLE COLLECTION YEAR: 2017
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly month
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
- Outfa l l
- No.
Date
Sample Collected,
mo/dd/yr
005 30
00400
00556
TotalSuspendedpH,
Solids, mg/L
Standard units
Non --Polar Oil and Grease/TPH EPA_
Met hod- 1664-(SGT-HEM),=mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 200 see permit
Within 6.0 — 9.0
15
-
12/13/17
6.4
8.2
3.2
338
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal I ,
No..
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended -Solids,
mg/L
pH,
Standard units
Permit Limit
-
IS
50 or 100 see permit
6.0 — 9.0
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWLJ-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS: All collected waters are held in storage tank until sampled and discharged
Date (first event sampled)
Total Event Precipitation (inches): NA —(water is contained in holding tank)
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must implement rer 1, rer 2, or 1 ier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one cony of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(—Z_�.-2"ot �-
(Date)
Additional copies of this form may be downloaded at: http:/Zportal.ncdenr.oEg/web/wcl/wsZsu/npdessw#tab-4
SWU-250
last revised April 11, 2013
Page 2 of 2

I ............. ;INKS ......... i.
Revieilwyour project
results,througk
TO
Have,&Questlon?'
Ask
PThe
Expert
Vlsitius°at:
www.testamericainc.com
TestAmerica rr
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT 4,
TestAmerica Laboratories, Inc.
TestAmerica Savannah r
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica ,lob ID: 680-146907-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre RECEIVED
Suite 300 FEB Q 1 2018
Rochester, New York 14618
CENTRAL FILES
Attn: Mr. William Ross DWR SECTION
-� C.—
Authorized for release by:
1212912017 4:25:50 PM
Keaton Conner, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Case Narrative
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Job ID: 680-146907-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc.
Project: NCVA RR
Report Number: 680-146907-1
TestAmerica Job ID: 680-146907-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required. "p
s
RECEIPT
The samples were received on 12115/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.4 C. The following sample was received at the laboratory without a sample collection date or time documented on
the chain of custody: NCVA Waste Water Holding Tank (680-146907-1). The client was contacted, and the laboratory was instructed to
use a sample collection date and time of 12/13/17 @ 7:30AM. No sample ID was listed on the COC or sample containers. The default ID
of "NCVA Waste Water Holding Tank" has been used.
HEM AND SGT-HEM
Sample NCVA Waste Water Holding Tank (680-146907-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B.
The samples were prepared and analyzed on 12/29/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample NCVA Waste Water Holding Tank (680-146907-1) was analyzed for total suspended solids in accordance with SM 2540D. The
samples were analyzed on 12/1912017.
Total Suspended Solids exceeded the RPD limit for the duplicate of sample 680-146975-1. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample NCVA Waste Water Holding Tank (680-146907-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The
samples were analyzed on 12127/2017.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 2 of 13 12/29/2017

Sample Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-146907-1
Lab Sample ID Client Sample ID Matrix Collected Received
680-146907-1 NCVA Waste Water Holding Tank Water 12113/17 07:30 12/15/17 11:18
TestAmerica Savannah
Page 3 of 13 12/29/2017

Method Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-146907-1
Method
Method Description
Protocol
Laboratory
1664B
HEM and SGT-HEM
1664B
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B
pH
SM
TAL SAV
Protocol References:
1664B = 1664B
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestArnerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 4 of 13 12/29/2017

Definitions/Glossary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Qualifiers
TestAmerica Job ID: 680-146907-1
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glos
Abbreviation These commonly used abbreviations may or may not be present In this report.
KC Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDlDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DOD/DOE)
LOO Limit of Quantitation (DDDIDOE)
MIDA Minimum Delectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
POL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
��I! �i
-- -
Page 5 of 13 12/29/2017

Client Sample Results
Client: Genesee & Wyoming, Inc.
ProjectlSite: NCVA RR
TestAmerica Job ID: 680-146907-1
Client Sample ID: NCVA Waste Water Holding Tank
Lab Sample ID: 680-146907-1
Date Collected: 12/13/17 07:30
Matrix: Water
Date Received: 12/15/17 11:18
General Chemistry
Analyte
Result Qualifier RL
MDL Unit
D Prepared Analyzed DII Fac
HEM (Oil & Grease)
3.2 2.6
0.73 mg1L
12/29/17 OB:20 12/29/17 10:33 1
Total Suspended Solids
6A 2.0
2.0 mg/L
12/19/17 11:54 1
pH
8.2 HF
SU
12127/1711:47 1
TestAmerica Savannah
Page 6 of 13 12/29/2017

QC Sample Results M
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-146907-1
Project/Site: NCVA RR
r
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 680-508097/1-A
Matrix: Water
Analysis Batch: 508133
MB MB
Analyte Result Qualifier
HEM (Oil & Grease) <5.0
Lab Sample ID: LCS 680-50809712-A
Matrix: Water
Analysis Batch: 508133
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 680-508097/3-A
Matrix: Water
Analysis Batch: 508133
Analyte
HEM (Oil & Grease)
Client Sample ID: Method Blank
Prep Type: Total,. —
Prep Batch: 508097
RL MDL Unit D Prepared Analyzed Oil Fac
5.0 1.4 mglL 12/29/17 08:20 12/29/17 10:33 1 o
Client Sample ID: Lab Control Sample
Prep Type: TotalINA
Prep Batch: 508097
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Roe Limits
40.0 37.40 mg/ 93 78 -114
Spike LCSD LCSD
Added Result Qualifier
40.0 37.80
Method: SM 2540D - Solids, Total Suspended
Lab Sample ID: MB 680-507008/1
Matrix: Water
Analysis Batch: 507008
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 508097
%Rec. RPD
Unit D %Rec Limits RPD Limit
mgll- 94 78 - 114 1 18
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fee
Total Suspended Solids <1.0 1.0 1.0 mglL 12/19/17 11:54 1
Lab Sample ID: LCS 680-507008/2
Matrix: Water
Analysis Batch: 507008
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-507008/3
Matrix: Water
Analysis Batch: 507008
Analyte
Total Suspended Solids
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-507833133
Matrix: Water
Analysis Batch: 507833
Analyte
pH
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier Unit
D %Rec
Limits
20.0
17.5
mglL
88
80-120
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
20,0
19.5
mglL
98
80-120 11 25
Spike
Added
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
7.0 5U 100 63 -158
TestAmerica Savannah
Page 7 of 13
12/29/2017

Client: Genesee & Wyoming, Inc. QC Sample Results TestAmerica Job ID: 680-146907-1
Project/Site: NCVA RR L%
Method: SM 4500 H+ B - pH (Continued
Lab Sample ID: 680.146907-1 DU
Matrix: Water
Analysis Batch: 507833
Sample Sample
Analyte Result Qualifier
pH 8.2 HF
Client Sample ID: NCVA Waste Water Holding Tank
�l
Prep Type: Total/NA
DU DU RPD 13
Result Qualifier Unit D RPD Limit Ffl
8.2 SU 0.4 40
TestAmerica Savannah
Page 8of13
12/29/2017

QC Association Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-146907-1
General Chemistry
'� }
Analysis Batch: 507008
{ j
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
j
660-146907-1
NCVA Waste Water Holding Tank
Total/NA
Water
SM 2540D
MB 680-507008/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-507008/2
Lab Control Sample
Total/NA
Water
SM 25401)
G
LCSD 680-507008/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 507833
[%
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-146907-1
NCVA Waste Water Holding Tank
Total/NA
Water
SM 4500 H+ B
LCS 680-507833/33
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
680-146907-1 DU
NCVA Waste Water Holding Tank
Total/NA
Water
SM 4500 H+ B��
Prep Batch: 508097
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-146907-1
NCVA Waste Water Holding Tank
Total/NA
Water
1664E
MB 680-508097/1-A
Method Blank
Total/NA
Water
1664B
LCS 680-508097I2-A
Lab Control Sample
Total/NA
Water
16648
LCSD 680-508097/3-A
Lab Control Sample Dup
Total1NA
Water
1664B
L -
Analysis Batch: 508133
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-146907-1
NCVA Waste Water Holding Tank
Total/NA
Water
1664B
508097
MB 680-50809711-A
Method Blank
Total/NA
Water
1664E
508097
LCS 680-508097/2-A
Lab Control Sample
Total/NA
Water
1664B
508097
LCSD 680-50809713-A
Lab Control Sample Dup
Total/NA
Water
1664E
508097
TestAmerica Savannah
Page 9 of 13 12/29/2017

Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Lab Chronicle
TestAmerica Job ID: 680-146907-1
r -
Client Sample ID: NCVA Waste Water Holding Tank
Date Collected: 12113/17 07:30
Date Received: 12/15/17 11:18
Lab Sample ID: 680-146907-1 L_s3
Matrix Water
A
Batch Batch
III
Initial
Final
Batch
Prepared
Prep Type
Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst
Lab
TotaI1NA
Prep 1664E
961 mL
500 mL
5 80097
12/29/17 08:20 JAS
TAL SAV
IC
TotallNA
Analysis 1664B
1
508133
12/29/17 10:33 JAS
TAIL SAV
Instrument ID: NOEQUIP/
Total/NA
Analysis SM 2540D
1
500 mL
1000 mL
507008
12/19/17 11:54 KLD
TAL SAV
Instrument ID: NOEQUIP
Total/NA
Analysis SM 4500 H+ B
1
507833
12/27/17 11:47 JER
TAL SAV
InstrumentID: MANTECH
Laboratory References:
TAL SAV = TestAmerica
Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 10 of 13
12/29/2017

M:
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Phone [phone] Fax [phone]
681-Atlanta
Chain of Custody Record
TestAmerica
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sampler
Lab PM
Ce'rtr TraCkM9 Nuts)
COC No.
Client Information
Harvey, Lisa M
680-81495-30842.1
Green Co:raa
phone
E.M.i_
P-ye.
Jay Welch
[e-mail]
Page 1 of 1
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Login Sample Receipt Checklist r
Client: Genesee & Wyoming, Inc.
Job Number: 680-146907-1
Login Number: 146907
List Source: TestAmerlca Savannah
List Number: 1
Creator: Anderson, Jordan K
Question
Answer
Comment
Radioactivity wasn't checked or is <1= background as measured by a survey
NIA
meter.
The coolers custody seal, if present, is intact.
True
�
Sample custody seals, if present, are intact.
True
o
The cooler or samples do not appear to have been compromised or
True
t
tampered with.
J
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
False
Refer to Job Narrative for details.
Is the Field Sampler's name present on COC?
NIA
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
False
No date or time on COC or sample containers
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, Incl. any requested
True
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (1/4").
Mulliphasic samples are not present.
True
Samples do not require splitting orcompositing.
True
Residual Chlorine Checked,
NIA
TestAmerica Savannah
Page 12 of 13 12/29/2017

Accreditation/Certification Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Laboratory: TestAmerica Savannah
The accreditationslcertifications listed below are applicable to this report.
TestAmerica Job ID: 680-146907-1
CAuthority Program EPA Region Identification Number Expiration Date
North Carolina (VAWSM State Program 4 269 12-31-18
12
TestAmerica Savannah
Page 13 of 13 12/29/2017

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted: July 17, 2017
CERTIFICATE OF COVERAGE NO. NCG080762
FACILITY NAME: NCVA Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: William Ross
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR: 2017
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly" (month)
CE1vebHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
JUL 2 4 2011 ❑other
DVVR SEC-r/ON PLEASE REMEMBER TO SIGN ON THE REVERSE 4
4ly
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —x— yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100:see permit
Within 6.0 — 9.0
15
-
06/29/17
<5 mg/L
8.1
2.0
382
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0-9.0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Pagel of 2

STORM EVENT CHARACTERISTICS: All collected waters are held in storage tank until sampled and discharged
Date (first event sampled)
Total Event Precipitation (inches): NA —(water is contained in holding tank)
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must implement Ter 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
?^I13—Zoc'7
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-250
last revised April 11. 2013
Page 2 of 2

0
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING j
ANALYTICAL REPOR
T
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-140535-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. William Ross
Authorized for release by.
711212017 1:47.02 PM
Kathryn Smith, Manager of Project Management
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TN! requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Case Narrative
Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Job ID: 680-140535-1
Laboratory: TestAmerica Savannah
TestAmerica Job ID: 680-140535-1
Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc. s-
Project: NCVA RR
Report Number: 680-140535-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 0613012017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 3.4° C.
HEM AND SGT-HEM
Sample Wastewater Holding Tank (680-140535-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared and analyzed on 07111/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Wastewater Holding Tank (680-140535-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 07105/2017.
Due to the nature of the sample matrix, a sample volume less than 1 L was utilized for this procedure and produced less than the 2,5mg
dried residue specified by the SM 25400 reference method. The following samples was impacted: Wastewater Holding Tank
(680-140535-1) and (680-140535-C-1 DU).
Total Suspended Solids exceeded the RPD limit for the duplicate of sample Wastewater Holding TankDU (680-140535-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Wastewater Holding Tank (680-140535-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were
analyzed on 07104/2017.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This analysis was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the DefnitionslGlossary page.
TestAmerica Savannah
Page 2 of 13 7/12/2017

Sample Summary 151
Client: Genesee & Wyoming, Inc. TestAmerica Job 10: 680-140535-1
Project/Site: NOVA RR
Lab Sample ID Client Sample ID Matrix Collected Received
680-140535-1 Wastewater Holding Tank Water 06/29117 0T.30 06/30/17 10:58
TestAmerica Savannah
Page 3 of 13 7/12/2017

1
Method Summary 19
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-140535-1
Project/Site: NCVA RR
Method
Method Description
Protocol
Laboratory
1664B
HEM and SGT-HEM
1664B
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B
pH
SM
TAL SAV
Protocol References:
1664E = 1664B
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
4
i
Page 4 of 13 7/12/2017

Definitions/Glossary
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-140535-1
Project/Site: NCVA RR
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F5 Duplicate RFD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the
absolute difference is less than the RL.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report.
a Listed underthe "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Oil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoDIDOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
NO Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
E
5
Page 5 of 13 7/12/2017

Client Sample Results
Client: Genesee & Wyoming, Inc.
ProjecVSite: NCVA RR
Client Sample ID: Wastewater Holding Tank
Date Collected: 06/29117 07:30
Date Received: 06130117 10.58
General Chemistry
Analyte Result Qualifier
HEM (Oil & Grease) 2.0 J
Total Suspended Solids 4.8
pH 8.1 HF
RL MDL Unit
2.6 0.73 mg1L
2.0 2.0 mglL
SU
TestAmerica Job ID: 680-140535-1
Lab Sample ID: 680-140535-1
Matrix: Water
D Prepared Analyzed DII Fac
07/11/17 07:55 0711 V17 10:24 1
0710511716:47 1
07/04/17 14:13 1 ,
ll
TestAmerica Savannah
Page 6 of 13
7/1212017

Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Method: 1664B - HEM and SGT-HEM
QC Sample Results F�
TestAmerica Job ID: 680-140535-1
Lab Sample ID: MB 680-487257/1-A
Matrix: Water
Analysis Batch: 487290
MB MB
Analyte Result Qualifier
HEM (Oil & Grease) <5.0
Lab Sample ID: LCS 680-487257/2-A
Matrix: Water
Analysis Batch: 487290
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 680-48725713-A
Matrix: Water
Analysis Batch: 487290
Analyte
HEM (Oil & Grease)
Spike LCS LCS
Added Result Qualifier
40.0 35.80
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 467257
RL MDL Unit D Prepared Analyzed Dil Fac j a,
5.0 1.4 mg/L 07111/17 07:55 07111117 10:24 1 ,
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 487257 [
%Rec.
Unit D %Rec Limits}
mglL 90 78 -114
Client Sample ID: Lab Control Sample Dup
Prep Type: Total1NA
Prep Batch: 487257
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D °/.Rec Limits RPD Limit
40.0 36.60 mg1L 92 78 -114 2 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-48674211 Client Sample ID: Method Blank
Matrix: Water Prep Type: TotalINA
Analysis Batch: 486742
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac
Total Suspended Solids <1.0 1.0 1.0 mglL 07105/17 16:47 1
Lab Sample 10: LCS 680-48674212
Matrix: Water
Analysis Batch: 486742
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-486742/3
Matrix: Water
Analysis Batch: 486742
Analyte
LTotal Suspended Solids
Lab Sample ID: 680-140535-1 DU
Matrix: Water
Analysis Batch: 486742
Sample Sample
Analyte Result Qualifier
Total Suspended Solids 4.8
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 16.0 mg1L 80 80 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 16.5 mg1L 83 80 -120 3 25
Client Sample ID: Wastewater bolding Tank
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
4.40 F5 mglL 9 5
TestAmerica Savannah
Page 7of13
7/12/2017

QC Sample Results}:
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-140535-1
Project/Site: NCVA RR
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-48667415 Client Sample ID: Lab Control Sample !1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 486674
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7.00 7.1 Sl1 101 63 -158
TestAmerica Savannah
Page 8 of 13 7/12/2017

QC Association Summary
Client: Genesee & Wyoming, Inc,
Project/Site: NCVA RR
TestAmerica Job ID: 680-140535-1
General Chemistry
Analysis Batch: 486674
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-140535-1
Wastewater Holding Tank
Total/NA
Water
SM 4500 H+ B
LCS 680-486674/5
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Analysis Batch: 486742
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch I l�
680 140535-1
Wastewater Holding Tank
Total/NA
Water
SM 2540D
L
MB 680-486742/1
Method Blank
TotallNA
Water
SM 2540D
LCS 680-486742/2
Lab Control Sample
Total/NA
Water
SM 2540D
'
LCSD 680-486742/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
680-140535-1 DU
Wastewater Holding Tank
Total/NA
Water
SM 2540D
a
Prep Batch: 487257
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-140535-1
Wastewater Holding Tank
Total/NA
Water
1664E
MB 680-4 8725711 -A
Method Blank
Total/NA
Water
1664B
LCS 680-487257/2-A
Lab Control Sample
Total/NA
Water
1664B
LCSD 680-487257/3-A
Lab Control Sample Dup
Total/NA
Water
1664E
Analysis Batch: 487290
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-140535-1
Wastewater Holding Tank
Total/NA
Water
16648
487257
MB 680-487257/1-A
Method Blank
TotallNA
Water
1664B
487257
LCS 680-487257/2-A
Lab Control Sample
Total/NA
Water
16648
487257
LCSD 680-48725713-A
Lab Control Sample Dup
Total/NA
Water
16646
487257
TestAmerica Savannah
Page 9 of 13 7/12/2017

Lab Chronicle 01
Client: Genesee & Wyoming, Inc, TestAmerica Job ID: 680-140535-1
Project/Site: NCVA RR
--------- _.-.--....-------- ------- _-.-._---.---------.--_-_--- ......... _------------._..._...__--_-....•-
Client Sample ID: Wastewater Holding Tank Lab Sample ID: 680-140535-1
Date Collected: 06/29/17 07:30 Matrix: Water -
Date Received: 06/30/17 10:58 !
Batch Batch
Prep Type
Type Method Run
TotaUNA
Prep 166413
TotallNA
Analysis 1664B
Instrument ID: NOEQUIP
Total/NA
Analysis SM 2540D
Instrument ID: NOEQUIP
Total/NA
Analysis SM 4500 H+ B
Instrument ID: MANTECH
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
954 mL
500 mL
487257
07/11/17 07:55
JAS
TAL SAV
1
487290
07/11/17 10:24
JAS
TAL SAV
L_
r
1
500 mL
1000 mL
486742
07/05117 16:47
JEC
TAL SAV
1
486674
07/04/17 14:13
KLD
TAL SAV
`o)
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 10 of 13
TestAmerica Savannah
7/12/2017

W
N
N
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1
TestArnerica Savannah
5102 LaRoche Avenue S $1 _Atta nta
Savannah. GA 31404
Phone[phone] Fax [phone]
Chain of Custody Record
TestAmerica .
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Comer TrecY,ng Nq%)
coc No
Client Information
Harvey, Lisa M
68"1495.30842.1
Char••'-^•-•-•••.
Phone
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Analysis Requested
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2001ideridian Centre Suite 300
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E - NaHSO4 0 - Na2S03
F . LrfOt1 R . Na25203
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757-272.4082(Tel)
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Possible Hazard ldantrfieation
Samplo Disposal (A fee may be assessed if samples are retained longer than 1 month)
ED I' 0 r-::3Radioiagicar
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M E:j
©Disposal
Non -Hazard Flammable lmlant Poison B Unknown
Reium To Client By Lob Archive Por Months
Deliverable Requested: I. 11, III, IV. Other (speaTy)
Special InstruMonslflC Requirements:
Empty Kit Relinquished by: Pate: Time: Method dl ShLlw,ent
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Custody Seals lrttact Custody Seat No.:
C7T s� and Ocher Remarks
d Yes A No
J E.

Client: Genesee & Wyoming, Inc.
Login Number: 140535
List Number: 1
Creator: Flanagan, Naomi V
Question
Login Sample Receipt Checklist
Job Number: 680-140535-1
List Source: TestAmerica Savannah L `• '
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
o
Samples were received on ice,
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
NIA
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
TestAmerica Savannah
Page 12 of 13 7/12/2017

h: 'a
Accreditation/Certification Summary },
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-140535-1
Project/Site: NCVA RR
Laboratory: TestAmerica Savannah
The accreditationslcertifications listed below are applicable to this report.
Authority Program EPA Region Identification Number
North Carolina (MISM State Program 4 269
Expiration Date
12-31-17
[12]
TestAmerica Savannah
Page 13 of 13 7/12/2017

ft
a Qeneeee & Wyoming Company
July 18, 2017
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080762
Dear Sir :
Please find enclosed our DMR for the first half of 2017. We are sampled from the holding tank that we
utilize to pump storm waters that are collected in the locomotive inspection/parking area of the yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
Jason Woods
General Manager
North Carolina & Virginia Railroad - 214 Railroad Street North - Ahoskie, NC 27910. 252-332-2778 Fax [phone]

Semi-annual Stormwater Dischange Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted 11/08/2016
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME: North Carolina & Virginia Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: William Ross
LABORATORY: Test America Lab Cert. #i 269
' `ECEIVEDSAMPLE COLLECTION YEAR: 2016
NOV 14 2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
CENTRAL FILES DISCHARGING TO CLASS ❑ORW ❑HOW ❑Trout ❑PNA
DWn SECTION ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: Sample collected from SW ®Other: City Storm
Holding tank
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
-Outfall
No.
Date
Sample Collected, -
mo/dd/.yr
-00530
00400_
00556
Total. Suspended_
Solids, mg/L '
pH, _
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage;
Annual average gal/rno
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
002/003
10/31/2016
8.5
8.0
2.1
372
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal I
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 -- 9.0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date: *NA (first event sampled) *Sampled from holding tank
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement rer 1, rer 2, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring Period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
il— lo—kko
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-250
last revised April 11, 2013
Page 2 of 2

r {_ W
Semi-annual Stormwater Discharge Monitoring Report
_ for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted 05/27/2016
CERTIFICATE OF COVERAGE NO. NCG080762 SAMPLE COLLECTION YEAR: 2016
FACILITY NAME: North Carolina & Virginia Railroad RECEIVED SAMPLE PERIOD ® Jan -June ❑ July -Dec
COUNTY: Hertford JUG! 0 8 2016 or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES: William Ross DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA
LABORATORY: Test America Lab Cert. ## 269 CENTRAL FILES ❑Zero -flow []Water Supply ❑SA
Comments on sample collection or analysis: Sample collected fromgWR SECTION ®other: City Storm
Holding tank V�00
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil pe onth? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable) �A*
❑ No discharge this period
i
Outfal I
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
002/003
05/05/2016
6.1
7.33
1.2
285
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal I
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
t For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page I of 2

STORM EVENT CHARACTERISTICS:
Date: *NA (first event sampled) *Sampled from holding tank
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one cop yof this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
S--Z-7—ISo
(Date)
Additional copies of this form may be downloaded at: http.Lportal.ncdenr,org/web/w-q/ws/`su/npdessw#tab-4
svw-2s0
last revised April 11, 2013
Page 2 of 2

E.
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted January 19, 2016
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME North Carolina & Virginia RR
COUNTY Hertford
PERSON COLLECTING SAMPLES
LABORATORY TestAmerica
William Ross
Lab Cert. # 269
Comments on sample collection or analysis:
Sampled Holding Tank from Maintenance Pit
2015
SAMPLE COLLECTION YEAR
SAMPLE PERIOD ❑ Jan -June July -Dec
or ❑ Monthlyl month
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ❑zero -flow ❑Watersupply ❑SA
,IAN 21 2016 ❑Other
CENTRAL FILESPLEASE REMEMBER TO SIGN ON THE REVERSE -i
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of P ;F09TIRMr month? yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period-'
Outfan
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 9.0
15
-
002/003
12/28/2015
7.8
8.27
1.9
295
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 - 9.0
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Pagel of 2

STORM EVENT CHARACTERISTICS:
e_
Date � NA (first event sampled) 'Sampled from holding tank
Total Event Precipitation (inches):
Date NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMA, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in
the case of "No Discharge" "e orts) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
I. -Zo- SOIS
(Date)
Additional copies of this form may be downloaded at:.http://portal.ncdenr.org/web/wg/ws/su/npdessw#7tab-4
SWU-250
last revised April 11, 2013
Page 2 of 2

r
July 30, 2015
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080762
Dear Sir :
a don►►►► 8 Wyoming Company
RECEIVED
AUG 0 3 2015
CENTRAL FILES
DWR SECTION
Please find enclosed our DMR for the first half of 2015. We are sampled from the holding tank that we
utilize to pump storm waters that are collected in the locomotive inspection/parking area of the yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
14-2�1 &),00—
Jason Woods
General Manager
North Carolina & Virginia Railroad Company, LLC 214, Railroad St, North Ahoskie, NC 27910
252-332-2778 Fax:[phone]

IL_
UNks ............
0
esTtAmenca
_ r
r�, E
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT �
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-114061-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. Aaron Blake
U�
Authorized for release by.
711412015 10:24:21 AM
Lisa Harvey, Project Manager II
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions are rioted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Genesee & Wyoming, Inc.
Project/Site., NCVA RR
Job ID: 680-114061-1
Laboratory: TestAmerica Savannah
Narrative
Case Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc.
Project: NCVA RR
Report Number: 680-114061-1
TestAmerica Job ID: 680-114061-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or anaiytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 07/01/2015; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.9 C.
OIL AND GREASE AND TPH
Sample Waste Water Holding Tank (680-114061-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A, The
samples were prepared and analyzed on 0711012015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water Holding Tank (680-114061-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 07/01/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Waste Water Holding Tank (680-114061-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 07/0112015.
This analysis is normally performed in the held and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
0
�z
FW_
TestAmerica Savannah
Page 2 of 13 7/14/2015

Sample Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
F-T]
TestAmerica Job ID: 680-114061-1
Lab Sample ID Client Sample ID Matrix Collected Received
680-114061-1 Waste Water Holding Tank Water 06/30/15 08:00 07/01/15 09:45
TestAmerica Savannah
[3]
V
Page 3 of 13 7/14/2015

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Method Summary L �
TestAmerica Job ID: 680-114061-1
Method
Method Description
Protocol
1664A
HEM and SGT-HEM
1664A
SM 2540D
Solids, Total Suspended (TSS)
SM
SM 4500 H+ B
pH
SM
Protocol References:
1664A = EPA-821-96-002
SM = "Standard Methods For The Examination Of Water And Wastewater',
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Laboratory
TALSAV ,
TAL SAV
TAL SAV FC
TestAmerica Savannah
Page 4 of 13 7/14/2015

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Qualifiers
Definitions/Glossary
TestAmerica Job ID: 680-114061-1
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at
request.
Glossary -
Abbreviation These commonly used abbreviations may or may not be present In this report.
n Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL it shown)
PQL Practical Quantilation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 5 of 13 7/14/2015

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Client Sample Results i 5
TestAmerica Job ID: 680-114061-1
Client Sample ID: Waste Water Holding Tank Lab Sample ID: 680-114061-1
Date Collected: 06/30/15 08:00 Matrix: Water
Date Received: 07/01115 09:45
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed DII Fac
HEM (Oil & Grease)
6.5
5.4 1.5 mglL
07/10/15 08:03 07/10/15 12:28 1
Total Suspended Solids
23
2.0 2.0 mg1L
07/01/15 12:25 1
pH
7.98 HF
SU
07/0111513:01 1
TestAmerica Savannah
Page 6 of 13 7/14/2015

QC Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Method: 1664A - HEM and SGT-HEM
Lab Sample ID: MB 680-390989/21-A
Matrix: Water
Analysis Batch: 391049
TestAmerica Job ID: 680-114061-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 390989
MS Me
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac
HEM (Oil & Grease) <5.0 5.0 1.4 i gg L 07110/15 06:03 07/10/15 12:28 1
Lab Sample ID: LCS 680-390989/22-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391049 Prep Batch: 390989
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
HEM (Oil & Grease) 40,0 34.0 mg1L 85 78-114
Lab Sample ID: LCSD 680-390989/23-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391049 Prep Batch: 390989
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
HEM (Oil & Grease) 40.0 35.0 mglL 88 76-114 3 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-38990511
Matrix: Water
Analysis Batch: 389905
me MI3
Analyte Result Qualifier
Total Suspended Solids <1.0
Lab Sample ID: LCS 680-389905/2
Matrix: Water
Analysis Batch: 389905
Analyte
LTotal Suspended Solids
Lab Sample ID: LCSD 680-38990513
Matrix: Water
Analysis Batch: 389905
Analyte
Total Suspended Solids
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fee
1.0 1.0 mg1L 07/0111510:58 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Roe.
Added Result Qualifier Unit D %Rec Limits
20.0 16.5 mglL 83 80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: TotaI1NA
Spike LCSD LCSD %Roe, RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 16.5 mg1L 83 80 -120 0 25
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-389935/7 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: TotalINA
Analysis Batch: 389935
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
PH 7.00 7.070 SU 101 63- 158
TestAmerica Savannah
r7]
Page 7of13
7/1412015

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
QC Sample Results r
TestAmerica Job ID: 680-114061-1 ��-
Method: SM 4500 H+ B - pH (Continued)
Lab Sample ID: 680-114061-1 DU Client Sample ID: Waste Water Holding Tank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 389935
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
pH 7.98 HF 8.020 SU 0.5 40
TestAmerica Savannah
Page 8 of 13 7/14/2015

QC Association Summary --�-�
Client: Genesee & Wyoming, Inc. TestAmerica ,lob 10: 680-114061-1 � -
Project/Site: NCVA RR
General Chemistry
Analysis Batch: 389905
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-114061-1
Waste Water Holding Tank
Total/NA
Water
SM 25400
a
LCS 680-389905/2
Lab Control Sample
Total1NA
Water
SM 2540D
LCSD 680-38990513
Lab Control Sample Dup
Tota11NA
Water
SM 25400
MB 680-389905/1
Method Blank
Total/NA
Water
SM 2540D
Analysis Batch: 389935
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680.114061-1
Waste Water Holding Tank
Total/NA
Water
SM 4600 H+ B
`
680-114061-1 OU
Waste Water Holding Tank
Total/NA
Water
SM 4500 H+ B
LCS 680-38993517
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Prep Batch: 390989
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-114061-1
Waste Water Holding Tank
TotaUNA
Water
1664A
LCS 680-390989/22-A
Lab Control Sample
Total/NA
Water
1664A
LCSD 680-390989123-A
Lab Control Sample Dup
Total/NA
Water
1664A
MB 680-390989121-A
Method Blank
Total/NA
Water
1664A
Analysis Batch: 391049
Lab Sample ID
Cl lent Sample ID
Prep Type
Matrix
Method
Prep Batch
680-114061-1
Waste Water Holding Tank
Total/NA
Water
1664A
390989
LCS 680-390989/22-A
Lab Control Sample
Total/NA
Water
1664A
390989
LCSO 680-390989/23-A
Lab Control Sample Dup
Total/NA
Water
1664A
390989
MB 680-390989/21-A
Method Blank
Total/NA
Water
1664A
390989
TestAmerica Savannah
Page 9 of 13 7/14/2015

Client: Genesee & Wyoming, Inc. Lab Chronicle TestAmerica Job ID: 680-114061-1
Project/Site: NCVA RR
Client Sample ID: Waste Water Holding Tank
Lab Sample ID: 680-114061-1
Date Collected: 06/30/15 08:00
Matrix: Water
Date Received: 07/01115 09:45
Batch Batch ail
Initial
Final
Batch
Prepared
F9
Prep Type Type Method Run Factor
Amount
Amount
Number
orAnaWed
Analyst Lab
Total/NA Prep 1664A
460 ml-
500 mL
390969
07/10115 08:03
MKA TAL SAV
Total/NA Analysis 1664A 1
460 mL
500 mL
391049
07/10/15 12:28
MKA TAL SAV
Instrument IO: NOEQUIP
Total/NA Analysis SM 2540D 1
495 mL
1000 mL
389905
07/01/15 12:25
LBH TAL SAV
Instrument iD: NOEQUIP
Total/NA Analysis SM 4500 H+ B 1
389935
07/01/15 13:01
LBH TAL SAV
Instrument ID: MANTECH
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmefta Savannah
Page 10 of 13 '711412015

Serial Number 9 3 2 6 7
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
•
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
tgp Tice savannah Webslte: www.testamadealno.com
5i02 LaRoche Avenue Phone: [phone]
Savannah, GA31404 Fax: [phone]
Q Alternate Laborainry NameAzcation
Phone:
Fax.
P RUJECT EF'ERENCF�
PROJECTNO.
0 a $
PROJECT LOCATION
(STATE)
MATRIX
TYPE
RLOUIREDANALYSIS
PAGE
OF
TAL (LAS) PROJECT MANAGER
s'tn:
P.O. NUMBER
CONTRACT NO-
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STANDARD REPORT
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DATE DUE
EXPEDITED REPORT
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CLIENT (SITE) PMA
n.SS
CLIENT PHONE
S2 - 1 -j "7'7
CLIENT FAX
2— 32.-
CUENT NAME
m C-V A L - r o�
CLIENT E-MAIL
o
CLIENTADDRESS f
q : c o, �'� o W e- `- an f
NU ABER OF COOLERS SUBMITTED
PER SHIPMENT:
COMPANY CONTRACTING THIS WORK pt applicable)
SAMPLE
SAMPLE IDENTIFICATION
NUMBER
OF CONTAINERS
SUBMITTED
REMARKS
DATE
TIME
-30
o
k >w
I
Ri TIME
6ao 114061 cnasn >sr c„gcoa�r
RI TIME
RELINQUISHE NATURE!
DATE
TIME
o 00
REL ED BY: {BICi
DATE
TIME
��
RE (sx;NATUIiEj
DATE
TIME
Y.ISI
TE
TIME
LABORATORY USE ONLY
CENED FOR TORY BY:
z 2,
p
TIME
r
CUSTODY INTACT
Q YES
NO CD
CUSTODY SAVANNAH
SEAL NO OG NO_
�0-11 0
LABORATORY REMARKS
C
I✓
TALS240-680 (IWO)

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 114061
List Number: 1
Creator: Kicklighter, Marilyn D
Question Answer
Radioactivity wasn't checked or is </= background as measured by a survey NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COG is present.
True
COC is filled out in ink and legible.
True
COG is filled out with all pertinent information.
True
Is the Field Sampler's name present on COG?
NIA
There are no discrepancies between the containers received and the COG.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (114" ).
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Job Number: 680-114061-1
/ List Source. TestAmerica Savannah
R1
Comment
TestAmerica Savannah
Page 12 of 13 7/14/2015

Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Certification Summary ���
TestAmerica Job ID: 680-1 14061-1
Authority
Program
EPA Region
Certification ID
Expiration Date
North Carolina (WWISW)
Slate Program
4
269
12.31-15
Virginia
NELAP
3
460161
06-14-16
TestAmerica Savannah
❑�3
A
Page 13 of 13 7/14/2015

Semi-annual Stormwater Discharee Monitorine Report
for North Carolina division of Water Quality General Permit No. NCGO80000
Date submitted July 29, 2015
2015
CERTIFICATE OF COVERAGE NO. NCGO80762 SAMPLE COLLECTIn5 YEAR
FACILITY NAME North Carolina 8 Virginia RR SAMPLE PERIOD M Jan -June ❑ July -Dec
COUNTY Hertford or ❑ Monthly' !month)
PERSON COLLECTING SAMPLES William Ross DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
LABORATORY Testamerica Lab Cert. q 269 ❑Zero -flow []Water Supply ❑SA
Comments on sample collection or analysis: ❑Other
Sampled Holding Tank from Maintenance Pit
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?! —yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
0021003
0613012015
23
7.98
6.5
370
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
15
50 or 100 see permit
6.0 — 9.0
t For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here,
SWU-250 last revised April 11, 2013
Page I oft

Il
STORM EVENT CHARACTERISTICS:
Date * NA (first event sampled) 'Sampled from holding tank
Total Event Precipitation (inches):
Date NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier Z, or Tier 3 responses. See General permit text.
FOR PART AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B,
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQREGIONAL OFFICE? YES ❑ NO❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including ail No Discharae" reports, within 30 days of receipt of the lab results.(ar at end of monitoring period in
the case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based an my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
7 - 3 4
(Signature of Permittee) (Date)
Additional copies of this form may be downloaded at: htto://portal.ncdenr.ora/web/wa/ws/su/npdessw#tab-4
S W U-250
Iasi revised April 11, 2013
Page 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted 08/29/2014
CERTIFICATE OF COVERAGE NO. NCG080762 SAMPLE COLLECTION YEAR: 2014
FACILITY NAME: North Carolina & Virginia Railroad 'SAMPLE PERIOD ❑ Jan -June ® July -Dec
COUNTY: Hertford or ❑ Monthly'_ (month)
PERSON COLLECTING SAMPLES: Aaron Blake SEP 0 3 2014 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY: Test America Lab Cert. # 269 TRAi_ C ❑Zero -flow ❑Water Supply ❑SA
(;ENGi ' ®Other: City Storm
Comments on sample collection or analysis: Sample collected #rom WQEg��
Holding tank
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable)
❑ No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil -and Grease/TPH EPA_
Method 1664 (SGT-HEM), mg/L
New. Motor Oil Usage,.
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
002/003
08/06/2014
10
7.49
4.6
411
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal l
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH, .
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
l For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

J
f
STORM EVENT CHARACTERISTICS:
Date: NA (first event sampled)
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, rer 2, or rer 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge" re orts within 30 days of receipt of the Jab results or at end of monitoring period in
the case o "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature
C9 -Z9 - Zak+
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdesswittab-4
SWU-250
last revised April 11, 2013
Page 2 of 2

a Geneses & Wyoming Company
August 29, 2014
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080762
Dear Sir :
Please find enclosed our DMR for the last half of 2014. At the direction of Mr. Samir Dumpor, we
sampled from the holding tank that is utilized to pump storm waters that were collected in the
locomotive inspection/parking area of the yard during the second half of 2014. We are submitting this
report at his direction (letter dated January 12, 2012).
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
Jason Woods
General Manager
North {;arolina & Virginia Railroad Company, LLC 214, Railroad St, North Ahoskie, NC 27910
252-332-2779 l,= 252-332-3325

a Oanssos & Wyoming Company
February 26, 2014
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080762
Dear Sir :
Please find enclosed our DMR for the last half of 2013 and the first half of 2014. At the direction of Mr.
Samir Dumpor, we sampled from the holding tank that is utilized to pump storm waters that were
collected in the locomotive inspection/parking area of the yard during the first six months of 2014. We
are submitting this report at his direction (letter dated January 12, 2012).
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
Jason Woods
General Manager
RECEIVED
FEB 2 7 2414
CENTRAL FILES
DWQIBOG
North Carolina & Virginia Railroad Cnnnpany, LLC 214, Railroad St. North Ahoskic, NC 27910
252-332-2778 Fax:[phone]

Iff
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted: 02/27/2014
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME: North Carolina & Virginia Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: NA
LABORATORY.
Lab Cert. #
Comments on sample collection or analysis: Industrial storm waters are
collected and sampled prior to discharge
SAMPLE COLLECTION YEAR: 2013
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthlyl tmonth)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
® No discharge this period'
Outfa I I
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total'Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New.Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non=Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

ww� ' I
s
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches): _
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement tier 1, Tier 2, or rer 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
+ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mall an original and one copy of this OMR, including all "No Discharge" reports, within 30 days of receipt of the tab results (or at end of monitoring period in
the case o "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant T
s for submitting false information, including the possibility of fines and imprisonment for knowing violations."
—4Z.4-1
v`o N' z
(i
(Signature of Permittee) (Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/suZopdessw#tab-4
SA U-250 last revised April 11, 2013
Page 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted 02/26/2014
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME: North Carolina & Virginia Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: William Ross
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis: Sample collected from SW
SAMPLE COLLECTION YEAR: 2014
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly' _ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: City Storm
Holding tank
PLEASE REMEMBER TO SIGN ON THE REVERSE -�
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfal l
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit .
Within 6.0 — 9.0
15
-
002/003
02/12/2014
14
7.73
3.4
368
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfa l l
No.
Date
Sample Collected,
mo/dd/yr
.00556
00530'
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/I.
Total Suspended Solids,
mg/L
pH,
Standard units
Permit!Limit
-
15
50 or 100 see permit
6.0 — 9.0
l For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date: NA (first event sampled)
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART A AND PART 8 MONITORING RESULTS:
0 A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one cow o f this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring Period in
the _case ojEfNo Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there aye significanAplenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Q z� P
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/wsZsu/nr)dessw#tab-4
SwU-2s0
last revised April 1 t, 2013
Page 2 of 2

i. ----;.
Semi-annual Stormwater Discharge Monitoring. Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted 02/26/2014
CERTIFICATE OF COVERAGE NO. NCGO80762
FACILITY NAME: North Carolina & Virginia Railroad
COUNTY: Hertford
PERSON COLLECTING SAMPLES: William Ross
LABORATORY: Test America Lab Cert. #.269
Comments on sample collection or analysis: Sample collected from SW
Holding tank
SAMPLE COLLECTION YEAR: 2014
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthlyl (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: City Storm
PLEASE REMEMBER TO SIGN ON THE REVERSE -->
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
No discharge this period1
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0-9.0
15
-
002/003
02/12/2014
14
7.73
3.4
369
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date: NA (first event sampled)
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART it SECTION B.
+ 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorinaperiod in
the case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there arre significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
()Z-r+ P
( Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wglws/su/npdessw#tab-4
SWU-250
last revised April 11, 2013
Page 2 of 2

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
f,
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-98706-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. Aaron Blake
Authorized for release by.
212412014 1:48:02 PM
Bernard Kirkland, Manager of Project Management
[phone] e.3238
[e-mail]
Designee for
Lisa Harvey, Project Manager II
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Laboratory: TestAmerica Savannah
Narrative
TestAmerica Job ID: 680-98706-1
With the exceptions noted as Bags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 02118/2014; the samples arrived in good condition, property preserved and on ice. The temperature of the
coolers at receipt was 3.2 G.
OIL ANQ GREASE AND TPH
Sample Wastewater holding Tank (680.98706-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The
samples were analyzed on 0212012014.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Wastewater Holding Tank (680-98706-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 0211912014.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
CORROSIVITY WHi
Sample Wastewater Holding Tank (680-98706-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ 8, The samples were
analyzed on 02119/2014.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Savannah
Page 2 of 13 2/24/2014

Client: Genesee & Wyoming, Inc. TestAmerica Job IQ: 680-98706-1
Project/Site: NCVA RR
Lab Sample ID Client Sample ID Matrix Collected Received
680-98706-1 Wastewater Holding Tank _ Water 02/12/14 14:00 02/10/14 10:10
TestAmerica Savannah
Page 3 of 13 2/24/2014

Client: Genesee & Wyoming, Inc.
TestAmerica Job ID: 680-98706-1
Project/Site: NCVA RR
Method Method Description
Protocol Laboratory
1664A HEM and SGT-HEM
1664A TAL SAV
SM 2540D Solids. Total Suspended (TSS)
SM TAL SAV
SM 4500 H+ B pH
SM TAL SAV
Protocol References:
1664A = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 4 of 13 2/24/2014

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CNF Contains no Free liquid
DER Duplicate error ratio (normalized absolute difference)
Oil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
NO Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 680-98706-1
TestAmerica Savannah
u
Page 5 of 13 2/24/2014

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-98706-1
Data Collected: 02/12/14 14:00
Matrix: Water
Date Received: 02/18/14 10:10
General Chemistry
Analyte
Result Qualifier
NONE
NONE
Unit
0 Prepared Analyzed
DII Fac ��-
pH
7.73 HF
SU
02119/1412:04
1
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
DII Fac
HEM (Oil & Grease)
3.4 J
4,8
1.3
mglL
02/20/14 19.38
1
Analyte
Result Qualifier
RL
RL
Unit
0 Prepared Analyzed
Dil Fac
Total Suspended Solids
14
5.0
5.0
mglL
02/19114 14:11
1
TestAmerica Savannah
Page 6 of 13
2/24/2014

QC Sample Results
Client: Genesee & Wyoming, Inc.
TestAmerica Job ID: 680-98706-1
Project/Site: NCVA RR
Method: 1664A - HEM and SGT-HEM
Lab Sample ID: MB 680-316586122
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316586
MB MB
a
Analyte Result Qualifier
RL MOL Unit D Prepared Analyzed Oil Fac
HEM (Oil & Grease) <5.0
5.0 1.4 mg7L 02/20/14 19:38 1
Lab Sample ID: LCS 680-316586123
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316586
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Roe Limits
HEM (Oil & Grease)
40.0
36.2 mglL 90 78 _ 114
Lab Sample ID: LCSD 680-316586/24
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316586
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limlts RPD Limit
HEM (Oil & Grease)
40.0
36.6 mglL 92 78 - 114 1 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID, MB 680-31630311
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316303
MB MB
Analyte
Result Qualifier
RL RL Unit
D Prepared Analyzed Oil Fac
Total Suspended Solids
<5,0
5.0 5.0 mglL
02/19/14 14:07 1
Lab Sample ID: LCS 680-316303/2
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316303
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit 0 %Roe Limits
Total Suspended Solids
100
94.0
mg1L 94 80 - 120
Lab Sample ID: LCSD 680-31630313
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: TotallNA
Analysis Batch: 316303
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rat Limits RPD Limit
Total Suspended Solids
100
1GI
mg/t. 101 80 - 120 7 25
Lab Sample ID: 680-98706-1 DU
Client Sample ID: Wastewater Holding Tank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 316303
Sample Sample
DU DU
RPD
Analyte
Result Qualifier
Result Qualifier
Unit D RPD Limit
Total Suspended Solids
14 12.0 mg/L 15 25
TestAmerica Savannah
Page 7 of 13 2/24/2014

QC Sample Results
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-98706-1
Project/Site: NCVA RR
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-316312/7
Matrix: Water
Analysis Batch: 316312
Spike
Analyte Added
pH 7.00
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Lin It D %Rec Limits
6,970 SU 100 63 - 158
AT
TestAmerica Savannah
Page 8 of 13 2/24/2014

QC Association Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
General Chemistry
TestAmerica Job ID: 680-98706-1
Analysis Batch: 316303
Lab Sample ID
Client Sample ID
Prop Typo
Matrix
Method
660-98706-1
Wastewater Holding Tank
Total/NA
Water
SM 2540D
680-98706-1 DU
Wastewater Holding Tank
Total/NA
Water
SM 2540D
LCS 600-31630312
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-31630313
Lab Control Sample Dup
Total/NA
Water
SM 2540D
MB 680.31630311
Method Blank
Total/NA
Water
SM 25400
Analysis Batch: 316312
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-98706-1
Wastewater Holding Tank
TotaYNA
Water
SM 4500 H+ B
LCS 680.316312f7
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Analysis Batch: 316586
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
fi80-98706-1
Wastewater Holding Tank
Total/NA
Water
1664A
LCS 680-316586/23
Lab Control Sample
Total/NA
Water
1664A
LCSD 680-316586/24
Lab Control Sample Dup
TotaUNA
Water
1664A
MB 680-316586122
Method Blank
Total/NA
Water
1664A
Prep Batch -
Prep Batch a
Prop Batch
TestAmerica Savannah
Page 9 of 13 2/24/2014

Lab Chronicle
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-98706-1
Project/Site: NCVA RR
Client Sample ID: Wastewater Holding Tank Lab Sample ID: 680.98706.1
Date Collected: 02/12/14 14.00 Matrix: Water
Date Received: 02118114 11010
Batch
Batch
Dilution
Batch
Prepared
Prop Type Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
Total/NA Analysis
SM 2540D
1
318303
02/19114 14:11
LBH
TAL SAV
Total/NA Analysis
SM 4500 H+ S
1
316312
02/19/14 12:04
LBH
TAL SAV
Total/NA Analysis
1664A
1
316586
02/20/14 19:38
ALC
TAL SAV
Laboratory References;
TAL SAV = TestAmerica Savannah,
5102 LaRoche Avenue, Savannah, GA 31404. TEL [phone]
TestAmerica Savannah
Page 10 of 13 2/24/2014
0

Serial Number 84772
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
-<S�<TestAmmica savannah website: www_testamericainc.com
5102 LaRoche Avenue Phone: [phone]
Savannah, GA31404 Fax: [phone]
Q Alternate Laboratory Name/Location
Phone:
Fax:
PROJECT REFERENCE
G ✓
PROJECT NO.
PROJECT LOCATION
(STAB
MATRIX
TYPE
REQUIREDANALYSIS
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TAL (LA8) PROJECT MANAGER
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DATE DUE
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NUMBER OF COOLERS SUBMITTED
PER SHIPMENT:
THIS WORK (d applicable) r
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NUMBER OF
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REMARKS
DATE
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680-98706 Chain of Custody
RELINQUIS1i�J.BY: (SlcruTmE)
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DATE
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DATE
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RELINQUISHED BY. (S*MTURE)
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DATE
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DATE
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DATE
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LABORATORY REMARKS
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04
TAM404M (1008)

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 98706
List Number: 1
Creator: Klcklighter, Marilyn D
Question
Answer
Radioactivity wasn't checked or is <1= background as measured by a
N/A
survey meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
NIA
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking,
True
Sample collection dateltimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, Incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Comment
Job Number: 680-98706-1
List Source: TestAmerica Savannah
TestAmerica Savannah
Page 12 of 13 2/24/2014

Certification Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
CAuthorlty Program EPA Region
North Carolina DENR State Program 4
TestAmerica Job ID: 680-98706-1
Certification 1D Expiration Date
269 12-31-14
TestAmerica Savannah
Page 13 of 13 2/24/2014