NCG080762_COMPLETE FILE - HISTORICAL_20161114

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V C&b8 t)
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ (�cI
YYYYMMDD

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah RECEIVED rfr
5102 LaRoche Avenue NOV 14 2016 i
Savannah, GA 31404 L931
Tel: [phone] CENTRAL FILES
DWR SECTION N
TestAmerica Job ID: 680-131537-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. William Ross
C! l
Authorized for release by.
111712016 10:46:04 AM
Lisa Harvey, Project Manager II
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NEt AG and 2009 TN! requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Case Narrative
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-131537-1
Project/Site: NCVA RR
Job ID: 680-131537-1 C� {
Laboratory: TestAmerica Savannah
r
Narrative
Client: Genesee & Wyoming, Inc.
Project: NCVA RR
Report Number: 680-131537-1
With the exceptions noted as Flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no t .'
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the O
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 11/01/2016: the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 5.2 C.
HEM AND SGT-HEM
Sample Waste Water (holding lank) (680-131537-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared and analyzed on 11/04/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water (holding tank) (680-131537-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 11/01/2016.
No additional analytical or quality issues were noted, other than those described above or in the DefinitionslGlossary page
CORROSIVITY (PHI
Sample Waste Water (holding tank) (680-131537-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 11103Y2016.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample was analzed in the
laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 2 of 12 11/7/2016

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Lab Sample ID Client Sample ID
680-131537-1 Waste Water (holding tank)
Sample Summary
Matrix
Water
TestAmerica Job ID: 680-131537-1
Collected Received
10131/16 08:00 11101 /16 10:05
TestAmerica Savannah
Page 3 of 12 11/7/2016

Method Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-131537-1
N
Method Method Description
Protocol Laboratory
1664B HEM and SGT-HEM
16648 TAL SAV
©,
SM 254DD Solids, Total Suspended (TSS)
SM TAL SAV
SM 4500 H+ B pH
SM TAL SAV
Protocol References:
3
16648 = 1664B
I
SM = "Standard Methods For The Examination OF Water And Wastewater',
I
U
Laboratory References:
j
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Ri
7i
TestAmerica Savannah
Page 4 of 12 11/7/2016

Definitions/Glossary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Qualifiers
TestAmerica Job ID: 680-131537-1 --
I
General Chemistry
Qualifier
Qualifier Description
HF
Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation
These commonly used abbreviations may or may not be present In this report.—
u
Listed under the " Y column to designate that the result is reported on a dry weight basis
%R
Percent Recovery
;
CFL
CNF
Contains Free Liquid
Contains no Free Liquid
o
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
to Do Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 5 of 12 11/7/2016

Client Sample Results
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-131537-1
Project/Site: NCVA RR
—� —__- --- ----------------------- r
Client Sample ID: Waste Water (holding tank) Lab Sample ID: 680-131537-1 ;
Date Collected: 10131116 09:00 Matrix: Water
Date Received: 11/01/16 10:05 ..I
I �'J
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac
HEM (Oil & Grease) 2.1 J 5.7 1.6 mg1L 11/04116 08:44 11104116 11:27 1
Total Suspended Solids 8.5 2.1 2.1 mglL 11101/16 14:17 1
pH 8.0 HF SU 11/0311616:35 1
5�711
TestAmerica Savannah
Page 6 of 12 11/7/2016

QC Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NOVA RR
Method: 1664E - HEM and SGT-HEM
Lab Sample ID: MB 68046630711-A
Matrix: Water
Analysis Batch: 456361
MB MB
Analyte Result Qualltrer
HEM (Oil & Grease) <5.0
Lab Sample ID: LCS 68045630712-A
Matrix: Water
Analysis Batch: 456361
Spike
Analyte
Added
HEM (Oil & Grease)
40.0
Lab Sample ID: LCSD 68045630713-A
Matrix: Water
Analysis Batch: 456361
Spike
Analyte
Added
HEM (Oil & Grease)
40.0
RL MDL Unit
5.0 1.4 mglL
LCS LCS
Result Qualifier Unit
36.20 mglL
LCSD LCSD
Result Qualifier Unit
37.40 mglL
TestAmerica Job ID: 680-131537-1
-
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 456307
D Prepared Analyzed Dil Fac
i
11/04/16 08:44 11/04/16 11:27 1
��
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 456307
j
%Rec.
D %Rec Limits
I
91 78 _ 114
-
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 456307
%Rec. RPD
-
D %Rec Limits RPD Limit
4
n 93 78-114 3 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-45666611
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 455666
MB M8
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed DII Fee
Total Suspended Solids
<1.0
1.0 1.0 mg/L
11/01/1608:22 1
Lab Sample ID: LCS 68045566612
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 455666
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
Total Suspended Solids
20.0
16.0
mglL
80 80 - 120
Lab Sample ID: LCSD 68045566613
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 455666
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec Limits RPD Limit
Total Suspended Solids
20.0
18's
mg1L
93 80- 120 14 25
------ ---------------------- -.-.-.--..------ .­...... .-... __..............................
Method: SM 4500 H+ B - pH
.... ............. _..................................................................
--.... ,- -------- - ---------- _....-_........
- -._...
---.,._.-.------- ------------------------------------
Lab Sample ID: LCS 680-46628215
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type-Total/NA
Analysis Batch: 456282
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
pH
7.00
7.1
Su
101 63- 158
TestAmerica Savannah
Page 7 of 12 11/7/2016

QC Association Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
General Chemistry
Analysis Batch: 455666
Lab Sample ID
Cllent Sample ID
Prep Type
680-131537-1
Waste Water (holding tank)
Total/NA
MB 68045566611
Method Blank
Total/NA
LCS 680455666/2
Lab Control Sample
Total/NA
LCSD 68045566613
Lab Control Sample Dup
Total/NA
Analysis Batch: 456282
Lab Sample ID
Client Sample ID
Prep Type
680-131537-1
Waste Water (holding tank)
TotallNA
LCS 680456282/5
Lab Control Sample
Total/NA
Prep Batch-456307
Lab Sample ID
Client Sample ID
Prep Type
680-131537-1
Waste Water (holding tank)
TotallNA
MB 680456307/1-A
Method Blank
TotallNA
LCS 680456307/2-A
Lab Control Sample
Total/NA
LCSD 68045630713-A
Lab Control Sample Dup
Total/NA
Analysis Batch: 456361
Lab Sample ID
Cllent Sample ID
Prep Type
680-131537-1
Waste Water (holding tank)
Total/NA
MB 6BO-45630711-A
Method Blank
Total/NA
LCS 680-456307/2-A
Leh Control Sample
TotallNA
LCSD 68045630713-A
Lab Control Sample Dup
TotaUNA
Page 8 of 12
TestAmerica Job ID: 680-131537-1go
i
Matrix
Water
Method
SM 25400
Prep Batch
Water
SM 2540D
Water
SM 2540D
FT
Water
SM 2540D
Matrix
Method
Prep Batch
Water
SM 4500 H+ B
Water
SM 4500 H+ B
�j
Matrix
Method
Prop Batch
Water
1664B
Water
1664B
Water
1664E
Water
1664E
i' r
Matrix
Method
Prep Batch
Water
1664E
456307
Water
16648
456307
Water
1664B
456307
Water
1664B
456307
TestAmerica Savannah
11/7/2016

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Client Sample ID: Waste Water (holding tank)
Date Collected: 10131116 09:00
Date Received: 11101N6 10:05
Lab Chronicle go
TestAmerica Jab ID: 680-131537-1
Lab Sample ID: 680-131537-1
Matrix: Water
Batch Batch
Dil
Initial
Prop Type Type Method Run
Factor
Amount
TotalINA Prep 1664E
436 mL
TotaUNA Analysis 16646
1
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D
1
480 mL
Instrument ID: NoEquip
Total/NA Analysis SM 4500 H+ B
1
Instrument ID: MANTECH
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Final Batch
Amount Number
500 mL 456307
456361
1000 mL 455666
456282
Prepared
or Analyzed
Analyst
Lab
11104116 08:44
JNN
TALSAV
j
11/04/1611:27
JNN
TALSAV
11/01/1614:17
JCM
TALSAV
--
�I
11/03/16 16:35
JCM
TAL SAV
TestAmerica Savannah
Page 9 of 12
11/7/2016

Serial Number 107584
z
CD
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
rat, TestAmerica Savannah Website: www.testamericainc.com
r� 5102 LaRoche Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
Alternale Laboratory NameiLocation
Phone:
Fax:
PROJECT REFER CE
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PROJECT NO-
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aROJECT LOCATION
(STATE) NC.,
MATRIX
TYPE
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ANALYSIS
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CONTRACT NO.
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OF COOLED SUBMITTED
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PER SHIPMENT.
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SAMPLE IDENTIFICATION
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NUMBER
OF
CONTAINERS
SUBMITTED
REMARKS
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DATE
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LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY: DATE TWE CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS
ISIGN ATUREt YES O SEAL NO. LOG NO.
:damp o
TALB241FBe0 (IDOAI

Client: Genesee & Wyoming, Inc.
Login Number: 131537
List Number: 1
Creator: Jackson, Victor L
Question
Login Sample Receipt Checklist
Answer Comment
i
Job Number: 680-131537-1
�
List Source: TestAmerica Savannah P13 fI
Radioactivity wasn't checked or is <f= background as measured by a survey
NIA
L_1
_
meter.^�
The coolers custody seal, if present, is intact.
Sample custody seals, if present, are intact.
True
True
l!
a J!
The cooler or samples do not appear to have been compromised or
True
r
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
m
COG is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
L I�..
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection dateltimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol, for all requested analyses, Incl. any requested
True
MS1MSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (114").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
TestAmerica Savannah
Page 11
of 12
11/7/2016

Certification Summary
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-131537-1
Project/Site: NCVA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority
Program
EPA Region
Certification ID
Expiration Data
A21-A
Dod FLAP
399.01
02-28-17
A21-A
ISOIIEC 17025
399.01
02-28-17
Alabama
State Program
4
41450
06-30-17
Arkansas DEQ
State Program
6
BB-0692
01-31-17
California
State Program
9
2939
07-31-16"
Colorado
State Program
8
NIA
12-31-16
Connecticut
State Program
1
PH-0161
03-31-17
Florida
NELAP
4
E07052
06-30-17
GA Dept. of Agriculture
State Program
4
NIA
06-12-17
Georgia
State Program
4
NIA
06-30-17
Georgia
State Program
4
803
06-30-17
Guam
State Program
9
15-005r
04-16-17
Hawaii
State Program
9
NIA
06-30-17
Illinois
NELAP
5
200022
11-30-16 '
Indiana
State Program
5
NIA
06-30-17
Iowa
State Program
7
353
06-30-17
Kentucky (DW)
State Program
4
90084
12-31-16
Kentucky (LIST)
State Program
4
18
06-30-17
Kentucky (INW)
State Program
4
90084
12-31-16
Louisiana
NELAP
6
30690
06-30-17
Louisiana (DW)
NELAP
6
LA160019
12-31-16
Maine
State Program
1
GA00006
09-24-18
Maryland
State Program
3
250
12-31-16
Massachusetts
State Program
1
M-GA006
06-30-17
Michigan
State Program
5
9925
06-30-17
Mississippi
State Program
4
NIA
06-30-16 '
Nebraska
State Program
7
TestAmerica-Savannah
06-30-17
New Jersey
NELAP
2
GA769
06-30-17
New Mexico
State Program
6
N/A
06-30-17
New York
NELAP
2
10842
03-31.17
North Carolina (DW)
State Program
4
13701
07-31-17
North Carolina (WWISW)
State Program
4
269
12-31-16
Oklahoma
State Program
6
9984
08-31-17
Pennsylvania
NELAP
3
68-00474
06-30.17
Puerto Rico
State Program
2
GA00006
12-31-16
South Carolina
State Program
4
98001
06-30-17
Tennessee
State Program
4
TN02961
06-30-17
Texas
NELAP
6
T104704185-15-8
11-30-16'
USDA
Federal
SAV 3-04
06-11-17
Virginia
NELAP
3
460161
06-14-17
Washington
State Program
10
C805
06-10-17
West Virginia (DW)
State Program
3
9950C
12-31-16
West Virginia DEP
State Program
3
094
08-31-16 `
Wisconsin
State Program
5
999819810
08-31-17
Wyoming
State Program
8
STMS-L
06-30-16'
' Certification renewal pending - certification considered valid.
TestAmerica Savannah
Page 12 of 12 11/7/2016

LINKS ......••••••
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-124978-1
Client Project/Site: NCVA Railroad
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. William Ross
Authorized for release by:
5/23/2016 9:49: 55 AM
RECEIVED
JUN 08 dis
CENTRAL. FILES
DWR SECTION
Lisa Harvey, Project Manager ll
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Case Narrative
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Job ID: 680-124978-1
Laboratory: TestAmerica Savannah
Narrative
Client: Genesee & Wyoming, Inc.
Project: NCVA Railroad
Report Number: 680-124978-1
TestAmerica Job ID: 680-124978-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or anaiytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 0510612016; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.2 C.
HEM AND SGT-HEM
Sample Waste Water (Holding Tank) (680-124978-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared on 05/19/2016 and analyzed on 05120/2016.
Method(s) 1664A, 166413: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MSIMSD/DUP) associated with 434260,
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water (Holding Tank) (680-124978-1) was analyzed for total suspended solids in accordance with SM 2540D. The
samples were analyzed on 0511112016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Waste Water (Holding Tank) (680-124978-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 0511712016.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample was analyzed in the
laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 2 of 13 5/23/2016

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Lab Sample ID
680-124978-1
Client Sample ID
Waste Water (Holding Tank)
Sample Summary
TestAmerica Job ID: 680-124978-1
Matrix Collected Received
Water 0510511610:00 05/0611611:15
TestAmerica Savannah
Page 3 of 13 5/23/2016

Method Summary
Client: Genesee & Wyoming, Inc.
TestAmerica Job ID: 680-124978-1
Project/Site: NCVA Railroad
Method Method Description
Protocol
Laboratory
16646 HEM and SGT-HEM
1fi64B
TAL SAV
SM 2540D Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B pH
SM
TAL SAV
Protocol References:
1664E = 1664B
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 4 of 13 5/23/2016

Definitions/Glossary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Qualifiers
TestAmerica Job ID: 680-124978-1
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossa
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantilation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 5 of 13 5/23/2016

Client Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
TestAmerica Job ID: 680-124978-1
Client Sample ID: Waste Water (Holding Tank) Lab Sample ID: 680-124978-1
Date Collected: 0 510 5/16 10:00 Matrix: Water
Date Received: 05106/16 11:15
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
HEM (Oil & Grease)
1.2 J
2.7 0.76 mg1L
05119116 17:27 05/20116 12:53 1
Total Suspended Solids
5.1
2.9 2.9 mg1L
05/11/16 19:24 1 n
pH
T33 HF
SU
05/1711613:13 1
TestAmerica Savannah
Page 6 of 13 5/23/2016

QC Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 680-434138118-A
Matrix: Water
Analysis Batch: 434260
MB MB
Analyte Result Qualifier RL MDL Unit
HEM (Oil & Grease) <5.0
Lab Sample ID: LCS 680-434138/19-A
Matrix: Water
Analysis Batch: 434260
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 680-434138/20-A
Matrix: Water
Analysis Batch: 434260
Analyte
HEM (Oil & Grease)
5.0 1.4 mg1L
TestAmerica Job ID: 680-124978-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 434138
D Prepared Analyzed Dil Fee
0511911 117.27 0512011612:53 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 434138
Spike LCS LCS %Rec.
Added Result Qualifier Unit D aARec Limits
40.0 37.6 mg/L 94 78 -114
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 434138
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rae Limits RPD Limit
40.0 36.8 mg/L 92 78 -114 2 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-43290511
Matrix: Water
Analysis Batch: 432905
MB MB
Analyte Result Qualifier
Total Suspended Solids <1.0
Lab Sample ID: LCS 680-432905/2
Matrix: Water
Analysis Batch: 432905
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-432905/3
Matrix: Water
Analysis Batch: 432905
Anaiyte
Total Suspended Solids
Method: SM 4500 H+ B -
Lab Sample ID: LCS 680-433735/7
Matrix: Water
Analysis Batch: 433735
Analyte
pH
Client Sample ID: Method Blank
Prep Type: Total1NA
RL MDL Unit D Prepared Analyzed DII fac
1.0 1.0 mg/L 05/11 /16 19:03 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 16.0 mg1L _ 80 80- 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 18.5 mg1L 93 80 -120 14 25
Spike
Added
7.00
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
6.850 SU 98 63 -158
TestAmerica Savannah
Page 7 of 13 5/23/2016

QC Sample Results
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-124978-1
Project/Site: NCVA Railroad
Method: SM 4500 H+ B - pH (Continued)
Lab Sample ID: 680-124978-1 DU Client Sample ID: Waste Water (Holding Tank)
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433735
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
pH 7.33 HF 7.330 SU 0 40
TestAmerica Savannah
Page 8 of 13 5/23/2016

QC Association Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Genera! Chem
Analysis Batch: 432905
TestAmerica Job ID: 680-124978-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-124978-1
Waste Water (Holding Tank)
Total/NA
Water
SM 2540❑
LCS 680-43290512
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-432905/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
MB 680-432905/1
Method Blank
Total/NA
Water
SM 2540D
Analysis Batch: 433735
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-124978-1
Waste Water (Holding Tank)
Total/NA
Water
SM 4500 H+ B
'
680-124978-1 DU
Waste Water (Holding Tank)
Total/NA
Water
SM 4500 H+ B
LCS 680-433735f7
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Prep Batch: 434138
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-124978-1
Waste Water (Holding Tank)
Total/NA
Water
1664E
LCS 680-434138119-A
Lab Control Sample
TotalINA
Water
1664B
LCSD 680434138120-A
Lab Control Sample Dup
Total/NA
Water
1664B
MB 680-434138/18-A
Method Blank
Total/NA
Water
166413
Analysis Batch: 434260
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-124978-1
Waste Water (Holding Tank)
Total/NA
Water
1664B
434138
LCS 680-434138119-A
Lab Control Sample
Total/NA
Water
16648
434138
LCSD 680-43413812D-A
Lab Control Sample Dup
Total/NA
Water
1664B
434138
MB 680-434138118-A
Method Blank
Total/NA
Water
1664E
434138
TestAmerica Savannah
Page 9 of 13 5/23/2016

Lab Chronicle
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-124978-1
Project/Site: NCVA Railroad
Client Sample ID: Waste Water (Holding Tank) Lab Sample ID: 680-124978-1
Date Collected: 05/05/16 10:00 Matrix: Water
Date Received: 05106116 11:15
Batch Batch
Oil
Initial
Final
Batch
Prepared
Prep Type
Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep 1664B
927 mL
500 mL
434138
05/19/16 17:27
BSJ
TAL SAV
Total/NA
Analysis 1664E
1
927 mL
500 mL
434260
05/20/16 12:53
BSJ
TAL SAV
Instrument ID: NOEQUIP
Total/NA
Analysis SM 2540D
1
350 mL
1000 mL
432905
05/11/16 19:24
JER
TAL SAV
Instrument ID: NOEQUIP
Total/NA
Analysis SM 4500 H+ B
1
433735
05/17/16 13:13
LAF
TAL SAV
Instrument ID: MANTECH
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 10 of 13 5/23/2016

Serial Number 107583
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
'4�TestArnerlce Savannah webslte: www.testameocalnc.cam
SLaRoche Avenue Phone_ (912)58
Savannah, GA 31404 Fax: [phone]-D165
<:D Alternate Laboratory Name&Dcation
Phone:
Fax:
PROJECT REFERENCE '
km\r A ita., c � �
PROJECT NO.
G 10B 6
D :CT LOCATION
f E
REQUIRED ANALYSIS
PAGE OF
TAL MB) PROJECT MANAGER
K 4:K, r w1 S
P.O. NUMBER
CONTRACT NO.
d
<
5
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v
JD
w-
D
a
U'
o
a
p
D
Z
p.
h
Ca
STANDARD REPORT
DELIVERY Q
DATE DUE
EXPEDITED REPORT
DELIVERY
(SURCHARGE)
DATE DUE
CLIENT (SITE) P
CLIENT PHONE
CLIENT FAX
CLIENT NAME
CLIENT E41A1L
m
CLIENTADDRESS
[ 0U
i>L
COMPANY CONTRACTING THIS WORK (a applicable)
w
�� I : �'-;
": I
a'y
s�•
NUMBER OF COOLERSSUBMrrTEp
PER SHIPMENT:
SAMPLE
SAMPLE IDENTIFICATION
v
NUMBER OF
CONTAINERS
SUBMITTED
REMARKS
DATE
TIME
REUNQUIS BY: (semquan-) DATE
TIME
RELINQUISHED BY: (sistwuRE)
DATE
TIME
RELINQUISHED BY- (srmTuHt5 DATE
TIME
RECEIVEDBY:(str.W1JRE) DATE TIME REGENEDSY:(siammtq DATE TIME RECEIVEDBY:(SlCuan _-
LABORATORY USE ONLY
DECEIVE A LABO TD Y B , PATE TIME r C TpDO ACT CUSTODY SEAL NO. SAVANNAH LABORATORY REMARKSYES 111
I
CD 680-124978 Chain of Custody
TAM46680 (1008)
1 a t.

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 124978
List Number: 1
Creator: White, Menica R
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is Celled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection dateltimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (1 /4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Job Number: 680-124978-1
List Source: TestAmerica Savannah
NJ
TestAmerica Savannah
Page 12 of 13 5/23/2016

Certification Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA Railroad
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority
Program
A21-A
DoD ELAP
A21-A
ISOIIEC 17025
Alabama
State Program
Arkansas DEG
State Program
California
State Program
Colorado
State Program
Connecticut
State Program
Florida
NELAP
GA Dept. of Agriculture
State Program
Georgia
State Program
Guam
State Program
Hawaii
State Program
Illinois
NELAP
Indiana
State Program
Iowa
State Program
Kentucky (DW)
State Program
Kentucky (UST)
State Program
Kentucky (WW)
State Program
Louisiana
NELAP
Louisiana (DW)
NELAP
Maine
State Program
Maryland
State Program
Massachusetts
State Program
Michigan
State Program
Mississippi
State Program
Nebraska
State Program
New Jersey
NELAP
New Mexico
State Program
New York
NELAP
North Carolina (DW)
State Program
North Carolina (WW/SW)
State Program
Oklahoma
State Program
Pennsylvania
NELAP
Puerto Rico
State Program
South Carolina
State Program
Tennessee
State Program
Texas
NELAP
USDA
federal
Virginia
NELAP
Washington
State Program
West Virginia (DW)
State Program
West Virginia DEP
State Program
Wisconsin
State Program
Wyoming
State Program
" Certification renewal pending - certification considered valid.
TestAmerica Job ID: 680-124978-1
EPA Region
Certification ID
Expiration Date
399.01
02-28-17
399.01
02-28-17
4
41450
06-30-16 "
6
88-0692
01-31-17
9
2939
07-31-16 '
8
NIA
12-31-16
1
PH-0161
03-31-17
4
E87052
06-30-16 `
4
NIA
06-12-17
4
803
06-30-16 "
9
15-005r
04-16-17
9
NIA
06-30-16 '
5
200022
11-30-16
5
NIA
06-30-16 '
7
353
06-30-17
4
90084
12-31-16
4
18
06-30-16 '
4
90084
12-31-16
6
30690
06-30-16
6
LA160019
12-31-16
1
GA00006
09-24-16
3
250
12-31-16
1
M-GA006
06-30-16 *
5
9925
06-30-16 `
4
NIA
06-30-16 *
7
TestAmerica-Savannah
06-30-16'
2
GA769
06-30-16 '
6
NIA
06-30-16 `
2
10842
03-31-17
4
13701
07-31-16 *
4
269
12-31-16
6
9984
08-31-16
3
68-00474
06-30-16 *
2
GA00006
12-31-16
4
98001
06-30-16 *
4
TN02961
06-30-16 *
6
T104704185-14-7
11-30-16
SAV 3-04
06-11-17
3
460161
06-14-16 "
10
C805
06-10-16 "
3
9950C
12-31-16
3
094
06-30-16 "
5
999819810
08-31-16
8
8TMS-L
06-30-16 "
TestAmerica Savannah
7;3
Page 13 of 13 5/23/2016

........... LINKS
e
hC�ro Sb76 TestAmenca r
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job 0: 680-120544-1
Client Project/Site: NCVA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. Aaron Blake
Authorized for release by.
1/1212016 11:36:53 AM
Lisa Harvey, Project Manager II
[phone] e.3221
lisa.harvey@testamericainc,com
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
\1
0

Case Narrative
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Job ID: 680-120544-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc.
Project: NCVA RR
Report Number: 68O-120544-1
TestAmerica Job ID: 680-120544-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12131/2015: the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.8 C.
HEM AND SGT-HEM
Sample waste water holding tank (680-120544-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared and analyzed on 01/11/2016.
Method(s) 1664A, 16648: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated
with analytical batch 400-290010.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample waste water holding tank (680-120544-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 01/0312016.
Method(s) 160.2, SM 254OD: Insufficient sample volume was provided to produce results within the specifications of SM 2540D which
requires at least 2.5 mg dried residue with a sample volume not to exceed 1 L. A sample volume less than 1 L. that yielded less than 2.5
mg dried residue, was provided for the following sample: wastewater holding tank (680-120544-1).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVtTY PH
Sample waste water holding tank (680-120544-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were
analyzed on 0110212016.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample was analyzed in the
laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the DefinitionslGlossary page
TestAmerica Savannah
Page 2 of 15 1/12/2016

Sample Summary
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
TestAmerica Job ID: 680-120544-1
Lab Sample ID Client Sample ID Matrix Collected Received
680-120544-1 waste water holding tank Water 12/28115 10:30 12/31/15 08:53
TestAmerica Savannah
131
Page 3 of 15 1/12/2016

Method Summary
Client: Genesee & Wyoming, Inc.
TestAmerica Job
ID: 680-120544-1
--�
Project/Site: NCVA RR
Method Method Description
Protocol
Laboratory
1664E HEM and SGT-HEM
1664E
TAL PEN
SM 2540D Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B pH
SM
TAL SAV
Protocol References:
1664E = 1664B
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 4 of 15 1/12/2016

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Qualifiers
Definitions/Glossary, +
TestAmerica Job ID: 680-120544-1
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossa
Abbreviation Those commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum delectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 5 of 15 1/12/2016

Client Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Client Sample ID: waste water holding tank
Date Collected: 12/28115 10:30
Date Received: 12131116 08:53
General Chemistry
Analyte Result Qualifier
HEM (Oil & Grease)
Total Suspended Solids 7.6
pH 8.27 HF
RL
4.1
4.0
MOIL Unit
1.4 mg/L
4.0 mg/L
SU
y! f
TestAmerica Job ID: 680-120544-1 `
Lab Sample ID: 680-120544-1
Matrix: Water
D Prepared Analyzed DII Fa(; rc
01 /11116 08:15 01/11/16 11:05 1
01/03/16 09:33 1 �+
01/02/16 14:07 1
TestAmerica Savannah
Page 6 of 15
1 /12/2016

QC Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 400-290010/1-A
Matrix: Water
Analysis Batch: 290043
MB MB
Analyte Result Qualifier
HEM (Oil & Grease) <4.0
Lab Sample ID: LCS 400-290010/2-A
Matrix: Water
Analysis Batch: 290043
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 400-29001013-A
Matrix: Water
Analysis Batch: 290043
Analyte
HEM (Oil & Grease)
RL MDL Unit
4.0 1.4 mg1L
,s
TestAmerica Job ID: 680-120544-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 290010
D Prepared Analyzed Dil Fac
01111/16 08:15 01/11/16 11:05 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 290010
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
40.0 43.7 mg/L 109 78 -114
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 290010
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
40.0 39.5 mg1L 99 78 -114 10 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-41689411 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416894
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac
Total Suspended Solids <1.0 1.0 1.0 mg/L 01/03/16 09:33 1
Lab Sample ID: LCS 680-41689412 Client Sample ID; Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416894
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 20.0 18.0 mg1L 90 60 -120
Lab Sample ID: LCSD 680-416894/3 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416894
Analyte
Total Suspended Solids
Method: SM 4500 H+ B - qH
Lab Sample ID: LCS 680-416883/7
Matrix: Water
Analysis Batch: 416883
Analyte
pH
Spike
Added
20.0
LCSD LCSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
20.5 mglL 103 80 -120 13 25
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
7.00 7200.SU 103 83 -158
TestAmerica Savannah
Page 7 of 15
1 / 12/2016

Client: Genesee & Wyoming, Inc.
Project/Site: NCVA RR
General Chemi
Prep Batch: 290010
QC Association Summary
TestAmerica Job ID: 680-120544-1 --
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-120544-1
waste water holding tank
Total/NA
Water
1664B
LCS 400-29001012-A
Lab Control Sample
Total/NA
Water
1664B
LCSD 400-290010/3-A
Lab Control Sample Dup
Totall
Water
1664E
MB 400-290010/1-A
Method Blank
Total/NA
Water
1664B
Analysis Batch: 290043
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
fi80 120544-1
waste water holding tank
Total/NA
Water
1664E
LCS 400-290010/2-A
Lab Control Sample
Total/NA
Water
1664B
LCSD 400-290010/3-A
Lab Control Sample Dup
Total/NA
Water
1664B
MB 400-290010/1-A
Method Blank
Total/NA
Water
1664E
Analysis Batch: 416883
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-120544-1
waste water holding tank
Total/NA
Water
SM 4500 H+ B
LCS 680-416883/7
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Analysis Batch: 416894
Lab Sample ID
Cilent Sample ID
Prep Type
Matrix
Method
680-120544-1
waste water holding tank
Total/NA
Water
SM 2540D
LCS 680-416894/2
Lab Control Sample
Total/NA
Water
SM 25400
LCSD 680-416894/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
MB 680-416894/1
Method Blank
Total/NA
Water
SM 2540D
Prep Batch
Prep Batch n
290010 '
290010
290010
290010
Prep Batch
Prep Batch
TestAmerica Savannah
Page 8 of 15 1/12/2016

Lab Chronicle
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-120544-1
Project/Slte: NCVA RR
Client Sample ID: waste water holding tank
Lab Sample ID: 680-120544-1
Date Collected: 12/28/15 10:30
Matrix: Water
Date Received: 12/31115 08:53
Batch Batch Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 16648
980 mL
i0 00 mL
29 0010
01/11/16 08:15
NDB TAL PEN
Total/NA Analysis 1664E 1
980 mL
1000 mL
290043
01/11/16 11:05
NDB TAL PEN
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D 1
250 mL
1000 mL
416894
01103M6 09:33
LAF TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis SM 4500 H+ B 1
416883
01/02/16 14:07
01-8 TAL SAV
Instrument ID: MANTECH
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL
[phone]
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 9 of 15 1/12/2016

Serial Number 93266
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
"TestAnericaSsirannah wehsite:www.testamerictinc.com
5102 LaRoche Avenue Phone: [phone]WEI
Savannah, GA 31404 Fax: [phone]
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Q Alternate Laboratcry Namelocafion
Phone:
Fax:
PROJECT REFgRENG
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TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Phone 19121354-7858 Fax [phone]
Chain of Custody Record JUHRIMMMIRR ; ll TestAvr�cG
CIE LSAMRSK TUTM-C
sampler
Lab PLYL
CarrierTraddrg Wsj
COC No:
Client Information (Sub Contract Lab)
[e-mail]
Harvey, Lisa M
680-417118.1
CRem Contact
Phone:
E-Mat
Page:
ShippinglReceMng
Page 1 of t
Company.
Job i`
TestAmerra Laboratcaes, Inc-
Analysis Requested
680-120544-1
Address:
Due Date Requested:
i
Preservation Codes,
3355 MCLemore Drive,
1I13r2016
_
T
h•
A - FICL M - Hexane
H - NaOH N -None
C hr
TAT Requested {days)-
Pensacnia
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C-ZnAontaln 0-ASNa02
D-NdricAcid P-Na204S
state.7m:
FL,32514
E-N&4SG4 a-Na25os
F - M80H R - Na2S=
Phone:
PO
850.478-2671(Fax)
.:co"�a50-474-1001(Fel)
H - AsAdd T Doderahydrate
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Project Name:
Project:
NGVA RR
68D08EF95
£
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offer.
Site:
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Sample
Matrix
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Type
(
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Sample
(C=comp,
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Sample Identification - Client ID b II)
Sam le Date
Time
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Special InstrucHormMote:
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waste water holding tank (680-120544-i)
08Gf11EM. Fstrad ILior NC REQ
12128/15
10-30
Water
X
2
Possible Hazard ldentifca6wr
Sample Disposal ( A fee maybe assessed if samples are retained longer than i month)
Unconfirmed I
© Return To CCsgt Disposal By lab iD Arrhrva For Mordhs
Deliverable Requested: I, Il, ill, IV, Other (specify)
Special InstruchonsiQ equiremertts:
Empty finquish Data: Time: Mettnd of shipment
Re1rVJj
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CustodySealslntact
Custody SealNo.: '.
CmwlTempersaxe(s)°CAndoewRamarm
e Yes A No
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{i' "9'S . .•

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 120544
List Number: 1
Creator: Banda, Christy S
Question
Radioactivity wasn't checked or is <I= background as measured by a
survey meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time.
Sample containers have legible labels,
Containers are not broken or leaking.
Sample collection dateltimes are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, Incl. any requested
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (114").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Answer
NIA
True
True
True
True
True
True
True
True
True
NIA
True
True
True
True
True
True
True
NIA
True
NIA
True
True
NIA
Comment
Job Number: 680-120544-1
List Source: TestAmerica Savannah
M
TestAmerica Savannah
Page 12 of 15 1/12/2016

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 120544
List Number: 2
Creator: Crawford, Lauren E
Question
Radioactivity wasn't checked or is <1= background as measured by a
survey meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS1MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (114").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Answer
NIA
True
NIA
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
NIA
True
True
NIA
Job Number: 680-120544-1
List Source: TestAmerica Pensacola _
List Creation: 01/06116 01:39 PM rrt
Comment
1.9°C IR-2 10
TestAmerica Savannah
Page 13 of 15 1/12/2016

Client: Genesee & Wyoming, Inc.
Project/Site. NCVA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Certification Summary
TestAmerica Job ID, 680-120544-1
Authority
Program
QLA
DoD ELAP
A21-A
ISOIIEC 17025
Alabama
State Program
Arkansas DEO
State Program
California
State Program
Colorado
State Program
Connecticut
State Program
Florida
NELAP
GA Dept. of Agriculture
State Program
Georgia
State Program
Guam
State Program
Hawaii
State Program
Illinois
NELAP
Indiana
State Program
Iowa
State Program
Kentucky (DW)
State Program
Kentucky (UST)
State Program
Kentucky (WW)
State Program
Louisiana
NELAP
Louisiana (DW)
NELAP
Maine
State Program
Maryland
State Program
Massachusetts
State Program
Michigan
State Program
Mississippi
State Program
Nebraska
State Program
New Jersey
NELAP
New Mexico
State Program
New York
NELAP
North Carolina (DW)
State Program
North Carolina (WWISW)
State Program
Oklahoma
State Program
Pennsylvania
NELAP
Puerto Rico
State Program
South Carolina
State Program
Tennessee
State Program
Texas
NELAP
USDA
Federal
Virginia
NELAP
Washington
State Program
West Virginia (DW)
State Program
West Virginia DEP
State Program
Wisconsin
State Program
Wyoming
State Program
Laboratory: TestAmerica Pensacola
The certifications listed below are applicable to this report.
EPA Region
Certification ID
Expiration Date
399.01
02-28-17
399,01
02-28-17
4
41450
06-30-16
6
88-0692
01-31-17
9
2939
07-31-16
8
NIA
12-31-16
1
PH-0161
03-31-17
4
E87052
06-30-16
4
NIA
06-12-17
4
803
06-30-16
9
14-004r
04-16-16
9
NIA
06.30-16
5
200022
11-30-16
5
NIA
06-30-16
7
353
06-30-17
4
90084
12-31-16
4
18
06-30-16
4
90084
12-31-15'
6
30690
06-30-16
6
LA160019
12-31-16
1
GA00006
09-24-16
3
250
12-31-16
1
M-GA006
06-30-16
5
9925
03-05-16
4
NIA
06-30-16
7
TestAmerica-Savannah
06-30-16
2
GA769
06-30-16
6
N/A
06.30-16
2
10842
03-31-16
4
13701
07-31-16
4
269
12-31-16
6
9984
08-31-16
3
68-00474
06-30-16
2
GA00006
12-31-16
4
98001
06-30-16
4
TN02961
06-30-16
6
T104704185-14-7
11-30-16
SAV 3-04
06-11-17
3
460161
06.14-16
10
C805
06-10-16
3
9950C
12-31-15
3
094
06-30-16
5
999819810
08-31-16
8
8TMS-L
06-30-16
Authority Program EPA Region Certification ID Expiration Date
Alabama State Program 4 40150 01-31-16
` Certification renewal pending - Certification considered valid.
TestAmerica Savannah
Page 14 of 15 1/12/2016

Certification Summary
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-120544-1
Project/Site: NCVA RR
Laboratory: TestAmerica Pensacola (Continued)
The certifications listed below are applicable to this report.
Authority
Program
EPA Region
Certification ID
Expiration Date
Arizona
State Program
9
A 0710
01-11-16 `
Arkansas DE4
State Program
6
88-0689
09-01-16s
Florida
NELAP
4
E81010
06-30-16
Georgia
State Program
4
NIA
06-30-16
Illinois
NELAP
5
200041
10-09-16
Iowa
State Program
7
367
07-31-16
Kansas
NELAP
7
E-10253
01-31-16'
Kentucky (UST)
State Program
4
53
06-30-16
Kentucky (WW)
State Program
4
98030
12-31-15'
Louisiana
NELAP
6
30976
06-30-16
Maryland
State Program
3
233
09-30-16
Massachusetts
State Program
1
M-FL094
06-30-16
Michigan
State Program
5
9912
06-30-16
New Jersey
NELAP
2
FL006
06-30-16
North Carolina (WW1SW)
State Program
4
314
12-31-15 *
Oklahoma
State Program
6
9810
08-31-16
Pennsylvania
NELAP
3
68-00467
01-31-16
Rhode Island
State Program
1
LA000307
12-30-15 '
South Carolina
State Program
4
96026
06-30-16
Tennessee
State Program
4
TN02907
06-30-16
Texas
NELAP
6
T104704286-15-9
09-30-16
USDA
Federal
P330-13-00193
07.01-16
Virginia
NELAP
3
460166
06-14-16
West Virginia DEP
State Program
3
136
06-30-16
' Certification renewal pending - certification considered valid.
TestAmerica Savannah
Page 15 of 15 1/12/2016

NIX
i�CDEE R
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, PE Dee Freeman
Governor Director Secretary
January 12, 2012
Mr. Jay Welch
NC & VA Railroad
214 N. Railroad Street
Ahoskie, NC 27910
Subject: NPDES Stormwater Permit — Notice of Inspection
NC & VA Railroad Ahoskie
Hertford County
Dear Mr. Welch:
On September 14, 2011, 1 visited your facility per your request to determine future sampling procedures and
locations. I met on site with you and Ms. Joni Willhite of Black and White Technologies, Inc.. According to Ms.
Willhite she informed the Division of Water Quality of this problem in several occasions, however this is the first
site visit that was performed. During the site visit it became apparent that the outfalls designated in NPDES
General Stormwater Permit NCGO80762 are as follows:
• inaccessible, being located in curb inlets covered with heavy grates and being a part of Town's
stormwater drainage system;
• and in the other case being located along the portion of NC & VA Railroad property that currently is not
being used for daily operations.
The site is currently graded in such way that most of the stormwater runoff is going to Railroad Maintenance Pit
and from there, the runoff is being pumped to a large water cistern. Periodically, if not needed the water from
cistern will be released toward designated outfalls.
I agreed with Ms. Willhite that good sampling point would be at the discharge from said cistern. The stormwater
discharged will better show the characteristics of this type of industrial activity rather than if the discharge is mixed
with the Town's stormwater from parking areas.
To conclude, the cistern discharge point can be used for future sampling,
If you have any questions, please feel free to contact me at Samir.DumporOncdenr,.gov- or telephone 252-948-
3959.
Sincerely,
cc: /WaRO
North Carolina Division of Water Quality Internet: www.ncwateLquglily.org
943 Washington Square Mall
Washington, NC 27889
Phone: [phone]
FAX: [phone]
Samir Dumpor, PE
Environmental Engineer
Surface Water Protection Section
NorthCarolina
naturally
An Equal Opportunity/Affirmative Action Employer— 50% RecycledllD% Post Consumer Paper

I I § § A I I I I � I I I I � � � A I I I 111 � �
ro
0
N
I

PTEMBER4.2011- WEDNESDAY
MEET WITH JONI WILLHITE - WITH NC -VA RAILROAD IN AHOSKIE
ADDRESS: 214 N. RAILROAD STREET,10:30 AM. SHE WILL ARRIVE FROM GEORGIA ON SEPTEMBER 113.
1 NEED TO CALL HER DAY AHEAD TO CONFORM TIME OF MEETING
JONI'S TEL NUMBER IN GEORGIA IS. 770-886-2382
CELL: 678-231-2297
NC -VA RAILROAD HAS A NCG PERMIT WITH US. THE STORMWATER OUTFALL FROM SITE DRAINS INTO
THE STORMWATER MANHOLE THAT IS LOCKED. THEY NEED TO FIGURE IT OUT HOW TO SAMPLE THIS
SITE (POSSIBLY CREATE NEW OUTFALL)
jf CGi G 00 7E2

� '� .. � � , � t _
... ��

�0F W A T�RQ
CO
0 �
Mr. Brad Ovitt
North Carolina and Virginia Railroad
214 N. Railroad Street
Ahoskie, NC 27910
Dear Mr. Ovitt:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
February 9, 2007
Alan W. Klimek, P.E. Director
Division of Water Quality
F r H 12 2007
Subject. General Permit No. NCG080000
North Carolina and Virginia Railroad
COC NCG080762
Hertford County
In accordance with your application for a discharge permit received on July 6, 2005, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state —NPDES
general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-
215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection
Agency dated May 9, 1994 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to the
Division of Water Quality. The Division of Water Quality may require modification or revocation and
reissuance of the certificate of coverage. Please also note the requirement to have a Stormwater Pollution
Prevention Plan and to comply with the cut off concentrations listed in the permit.
This permit does not affect the legal requirements to obtain other permits which may be required
by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area.
Management Act or any other federal or local governmental permit that may be required.
If you have any questions concerning this permit, please contact Kelly Johnson at telephone
number [phone] ext. 376.
Sincerely,
Alan W. Klimek, P.E.
cc: Washington Regional Office, Jeffery Manning
Central Files
Stormwater Permitting Unit Files
NQ°`hCaro' a
Yaturm,=
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: www.ncwaterqualitv.org Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycledlt 0% Post Consumer Paper

61
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES .
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG080000
CERTIFICATE OF COVERAGE No. NCGO80762
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
North Carolina and Virginia Railroad
is hereby authorized to discharge stormwater from a facility located at
North Carolina and Virginia Railroad
214 N. Railroad Street
Ahoskie
Hertford County
to receiving waters designated as Whiteoak Swamp, a class C, NSW water in the Chowan River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I, II, III, IV, V, and VI of General Permit No. NCGO8000 as attached.
This certificate of coverage shall become effective February 9, 2007.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 9`h day of February 2007.
for Alan W. Klimek, P.E., Director
Division of Water Quality
By the Authority of the Environmental Management Commission

LOCATION MAP:
Latitude: 36°17'13" N NCG080762 Facility
Longitude: 761159 4
} " W North Carolina and
County: Hertford Location
Stream Class: C; NSW Virginia Railroad
Receiving Stream: WhiteoakSwamp
-Sub-basin: 03-01-01 (Chowan River Basin) CffO'tfh SCALE 1-:24,000

[Fwd: [Fwd: [Fwd: NCG080762]]]
Subject: [Fwd: [Fwd: [Fwd: NCG08076211]
From: Jeff Manning <[e-mail]>
Date: Wed, 07 Feb 2007 09:23:26 -0500
To: Kelly Johnson <kelly.p [e-mail]>
Kelly,
At this time I have no problems with issuing the permit.
Jeffery
Subject: [Fwd: [Fwd: NCG80762]]
From: Jeff Manning <[e-mail]>
Date: Thu, 01 Feb 2007 14:15:54 -0500
To: Jeff Manning <[e-mail]>
Subject: [Fwd: NCG080762]
From: Kelly Johnson <kelly.p [e-mail]>
Date: Thu, 11 Jan 2007 07:29:00 -0500
To: [e-mail]
CC: [e-mail]
Jeff,
I had sent this to Pat last month, but I know that you guys have had a change in staff
so I thought that I would resend it to you. (Actually, my predecessor received this
back in 2005.)
Thanks,
Kelly
Subject: NCG080762
From: Kelly Johnson <[e-mail]>
Date: Mon, 11 Dec 2006 15:41:19 -0500
To: [e-mail]
CC: [e-mail]
Hi Pat
We've received an NOI from the North Carolina and Virginia Railroad for their facility
in Ahoskie (Hertford County) for coverage under NCG08 (Transit and Transportation
SW/WW permit). The site discharges stormwater into White Oak Swamp (C, NSW water).
The NOI is attached. This request was received by a previous employee in June 2005,
and it is unclear from the files whether or not you have already discussed this with
him. BIMS does not have a note about it, so I assume that this is the first contact
you have had? I am slowly making my way through these old files.
Does the Washington Regional Office have any concerns about issuing this facility a
COC "for this general permit? If we don't receive any objections, we'll issue the COC
1 of 2 2/7/2007 9:55 AM

[Fwd: [Fwd: tFwd: NCGO80762111
in 30 days.
Thanks,
Kelly Johnson
Content -Type: message/rfc822
[Fwd: 1Fwd: NCG08076211I
Content -Encoding: 7bit
1Fwd: Ncco807621Content-Type: messagelrfc822
Content -Encoding: 7bit
Content -Type: application/pdf
NCC 080762_Application.pdf
Content -Encoding: base64
Content -Type: messagelrfc822
NCC080762
Content -Encoding: 7bit
i Content -Type: application/pdf
NCG 080762_Application.pdf
Content -Encoding: base64
2 of 2 2/7/2007 9:55 AM