NCG080759_MONITORING INFO_20190131

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v uc,
DOC TYPE
El HISTORICAL FILE
�1 MONITORING REPORTS
DOC DATE
❑ aul 5 DI 3 �
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG080000
Date submitted 1/9/2019
CERTIFICATE OF COVERAGE NO. NCG08 0 7 5 9
FACILITY NAME Chesapeake & Albermarle Railroad
COUNTY Pasquotank
PERSON COLLECTING SAMPLES Shannon Lonergan (Adamson)
LABORATORY Eurofins Lancaster Labs Lab Cert. # 521
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR 2018
SAMPLE PERIOD ❑ Jan -June 0 July -Dec
or ❑ Monthly) (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
RC DOther sW
JAN 31 2o19 PLEASE REMEMBER TO SIGN ON THE REVERSE 4
CEN-1"RAL FILES
Did this facility perform Vehicle Maintenance Activities using more than 55,g,�ljp¢��ie"bil per month? ❑ yes ❑■ no (if yes, complete Part A)
Part A: Vehicle & Equipment Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period
Outfall No. Date Sample Collected) 24-hourrainfall amount, Non -Polar Oil &Grease Total Suspended Solids, New Motor. or Hydraulic Oil Usage,
(mo/dd/yr) Inches mg/L mg/L; : gal/mon
Benchmarks 15 100or 50°
Parameter'Code - 46529 00 552.. ,: C0530 - _ ..... NCOIL -
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Permit Date: 11/1/2018-5/31/2021 SWU-248, last revised 11/1/2018
Page 1 of 2

r.." Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) ❑ No discharge this period
Outfall
=Date Sample '
24-hour rainfall" ,
Sample Collected)7
TotaLSuspended
pH
Non Polar
No
Collected)
-amount,
mo'/,dd/yr
Solids,
_.
Standard units
: =-Grease,
(mo/dd/yr) .
lriche s3
mg/L . .
mg/``
Permit Limit
_
100 or S. 4
'6:0 9:0
15
s
Pgramefer
C0530
00400 _
00552; ,
001
1 12/10/2018
1.2 inches
12/10/2018
3.58 mg/L
7.9
<1.4 mg/L
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO E]
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ® NO
REGIONAL OFFICE CONTACT NAME:
Mail an original copv of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitorina period in the
case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Permit Date: 11/1/2018-5/31/2021
Date
SWU-248, last revised 11/1/2018
Page 2 of 2

a Genesee & Wyoming Company
January 26, 2018
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080759
Dear Sir :
C & VD
FEB 01 2018
CENTRAL FILES
DVVR ,ECTION
Please find enclosed our DMR for the second half of 2017. We are sampled from the holding tank that
we utilize to pump storm waters that are collected in the locomotive inspection/parking area of the
yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
�wh
Jason Woods
General Manager
Chesapeake & Albemarle Railroad • 214 Railroad Street North • Ahoskie, NC 27910 • 252-332-2778 Fax [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted 01/26/2018
CERTIFICATE OF COVERAGE NO. NCG080759
FACILITY NAME: Chesapeake & Albemarle Railroad
COUNTY: Pasquotank
PERSON COLLECTING SAMPLES: Jeff Moore
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis: Sample collected from SW
Holding tank
SAMPLE COLLECTION YEAR: 2017
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
❑Zero -flow [_]Watersupply []SA
®Other: SC
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfal l
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
t -
001
12/14/2017
17.5
7.9
4.6
67
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal l
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0,
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date: *NA (first event sampled) *Sampled from holding tank
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
I—Z6—Z,o19,
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-250
last revised April 11. 2013
Page 2 of 2

........... LiNks .........:..
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results,through
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-146889-1
Client Project/Site: CA RR - Waste Water Holding Tank
For:
Genesee & Wyoming, Inc.
1 Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. William Ross
Authorized for release by:
1212912017 4:24:17 PM
Keaton Conner, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

oClient: Genesee & Wyoming, Inc. Definitions/Glossary TestAmerica Job ID: 680-146889-1
Project/Site: CA RR - Waste Water Holding Tank
Qualifiers LIE
General Chemistry
Qualifier Qualifier Description "s '
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request. 551
Glossary
I ;
Abbreviation
These commonly used abbreviations may or may not be present in this report.
- I
o
Listed under the "D" column to designate that the result is reported on a dry weight basis
%R
Percent Recovery
CFL
Contains Free Liquid
CNF
Contains No Free Liquid
DER
Duplicate Error Ratio (normalized absolute difference)°
❑
Dil Fac
Dilution Factor
DL
Detection Limit (DoD/DOE)
DL, RA, RE, IN
Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC
Decision Level Concentration (Radiochemistry)
EDL
Estimated Detection Limit (Dioxin)
LOD
Limit of Detection (DoD/DOE)
LOQ
Limit of Quantitation (DoD/DOE)
--:
MDA
Minimum Detectable Activity (Radiochemistry)
MDC
Minimum Detectable Concentration (Radiochemistry)
MDL
Method Detection Limit
ML
Minimum Level (Dioxin)
NC
Not Calculated
ND
Not Detected at the reporting limit (or MDL or EDL if shown)
PQL
Practical Quantitation Limit
QC
Quality Control
RER
Relative Error Ratio (Radiochemistry)
RL
Reporting Limit or Requested Limit (Radiochemistry)
RPD
Relative Percent Difference, a measure of the relative difference between two points
TEF
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 2 of 13 12/29/2017

Sample Summary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR - Waste Water Holding Tank
Lab Sample ID Client Sample ID Matrix
680-146889-1 Waste Water Holding Tank Water
TestAmerica Job ID: 680-146889-1
Collected Received
12/14/17 08:15 12/15/17 11:18
TestAmerica Savannah
Page 3 of 13 12/29/2017

Client: Genesee & Wyoming, Inc.
Project/Site: CA RR - Waste Water Holding Tank
Job ID: 680-146889-1
Laboratory: TestAmerica Savannah
Narrative
Case Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc.
Project: CA RR - Waste Water Holding Tank
Report Number: 680-146889-1
TestAmerica Job ID: 680-146889-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12/15/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.0 C. No sample ID was listed on the COC or sample containers. The default ID of "CA RR" has been used.
HEM AND SGT-HEM
Sample Waste Water Holding Tank (680-146889-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared and analyzed on 12/29/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water Holding Tank (680-146889-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 12/19/2017.
Total Suspended Solids exceeded the RPD limit for the duplicate of sample 680-146975-1. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Waste Water Holding Tank (680-146889-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 12/27/2017.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
M
n
TestAmerica Savannah
Page 4 of 13 12/29/2017

Client Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR - Waste Water Holding Tank
Client Sample ID: Waste Water Holding Tank
Date Collected: 12/14/17 08:15
Date Received: 12/15/17 11:18
General Chemistry
Analyte Result Qualifier
HEM (Oil & Grease) 4.6
Total Suspended Solids 7.5
pH 7.9 HF
TestAmerica Job ID: 680-146889-1
Lab Sample ID: 680-146889-1
Matrix: Water
n
RL MDL Unit
D Prepared Analyzed
t "t
Dil Fac
2.4 0.67 mg/L
12/29/17 08:20 12/29/17 10:33
1
1.0 1.0 mg/L
12/19/1711:54
1
SU
12/27/1711:39
1 171
�l
HOP].
TestAmerica Savannah
Page 5 of 13
12/29/2017

QC Sample Results M
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-146889-1 7
Project/Site: CA RR - Waste Water Holding Tank
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 680-508097/1-A
Matrix: Water
Analysis Batch: 508133
MB MB
Analyte Result Qualifier
HEM (Oil & Grease) <5.0
Lab Sample ID: LCS 680-508097/2-A
Matrix: Water
Analysis Batch: 508133
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 680-508097/3-A
Matrix: Water
Analysis Batch: 508133
Analyte
HEM (Oil & Grease)
Client Sample ID: Method Blank (�
Prep Type: Total/NA
Prep Batch: 508097
RL MDL Unit D Prepared Analyzed Dil Fac
5.0 1.4 mg/L 12/29/17 08:20 12/29/17 10:33 1 °
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 508097�
Spike
LCS LCS
%Rec.
--
Added
Result Qualifier
Unit
D %Rec
Limits
IC
40.0
37.40
mg/L
93
78 -114
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 508097
Spike
LCSD LCSD
%Rec. RPD
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit���
40.0
37.80
mg/L
94
78 -114 1 18
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C)
Lab Sample ID: MB 680-507008/1
Matrix: Water
Analysis Batch: 507008
Analyte
Total Suspended Solids
Lab Sample ID: LCS 680-507008/2
Matrix: Water
Analysis Batch: 507008
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-507008/3
Matrix: Water
Analysis Batch: 507008
Analyte
Total Suspended Solids
Method: 4500 H+ B-2011 - pH
Lab Sample ID: LCS 680-507833/33
Matrix: Water
Analysis Batch: 507833
Analyte
pH
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
<1.0 1.0 1.0 mg/L 12/19/1711:54 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 17.5 mg/L 88 80 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 19.5 mg/L 98 80 -120 11 25
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
7.00 7.0 SU 100 63 -158
TestAmerica Savannah
Page 6 of 13 12/29/2017

QC Sample Results
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-146889-1
Project/Site: CA RR - Waste Water Holding Tank
Method: 4500 H+ B-2011 - pH (Continued)
Lab Sample ID: LCS 680-507833/7 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 507833
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7.00 7.1 SU 101 63 -158
TestAmerica Savannah
Page 7 of 13 12/29/2017

QC Association Summary
Client: Genesee & Wyoming, Inc.
TestAmerica Job ID: 680-146889-1
Project/Site: CA RR - Waste Water Holding Tank
General Chemistry
Analysis Batch: 507008
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-146889-1 Waste Water Holding Tank
Total/NA
Water
2540 D-2011
MB 680-507008/1 Method Blank
Total/NA
Water
2540 D-2011
LCS 680-507008/2 Lab Control Sample
Total/NA
Water
2540 D-2011
LCSD 680-507008/3 Lab Control Sample Dup
Total/NA
Water
2540 D-2011
Analysis Batch: 507833
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-146889-1 Waste Water Holding Tank
Total/NA
Water
4500 H+ B-2011
LCS 680-507833/33 Lab Control Sample
Total/NA
Water
4500 H+ B-2011
LCS 680-507833/7 Lab Control Sample
Total/NA
Water
4500 H+ B-2011
Prep Batch: 508097
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-146889-1
Waste Water Holding Tank
Total/NA
Water
1664E
MB 680-508097/1-A
Method Blank
Total/NA
Water
1664B
LCS 680-508097/2-A
Lab Control Sample
Total/NA
Water
1664B
LCSD 680-508097/3-A
Lab Control Sample Dup
Total/NA
Water
1664B
Analysis Batch: 508133
Lab Sample ID
680-146889-1
MB 680-508097/1-A
LCS 680-508097/2-A
LCSD 680-508097/3-A
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Waste Water Holding Tank
Total/NA
Water
1664E
508097
Method Blank
Total/NA
Water
1664B
508097
Lab Control Sample
Total/NA
Water
1664B
508097
Lab Control Sample Dup
Total/NA
Water
1664E
508097
TestAmerica Savannah
Page 8 of 13 12/29/2017

Client: Genesee & Wyoming, Inc. Lab Chronicle TestAmerica Job ID: 680-146889-1 Fq
Project/Site: CA RR - Waste Water Holding Tank [�?
Client Sample ID: Waste Water Holding Tank Lab Sample ID: 680-146889-1
Date Collected: 12/14/17 08:15 Matrix: Water !
Date Received: 12/15/17 11:18 Q 1
Batch Batch
Prep Type
Type Method Run
Total/NA
Prep 1664E
Total/NA
Analysis 1664E
Instrument ID: NOEQUIP
Total/NA
Analysis 2540 D-2011
Instrument ID: NOEQUIP
Total/NA
Analysis 4500 H+ B-2011
Instrument ID: MANTECH
Dil
Initial
Final
Batch
Prepared
Fo
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
1044 mL
500 mL
508097
12/29/17 08:20
JAS
TAL SAV
1
508133
12/29/17 10:33
JAS
TAL SAV
aIT�
I
1
1000 mL
1000 mL
507008
12/19/17 11:54
KLD
TAL SAV
1
507833
12/27/17 11:39
JER
TAL SAV
❑
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
LA
Page 9 of 13
12/29/2017

Accreditation/Certification Summary
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-146889-1
Project/Site: CA RR - Waste Water Holding Tank
Laboratory: TestAmerica Savannah
The accreditations/certifications listed below are applicable to this report.
Authority
Program
EPA Region
Identification Number
Expiration Date
Alabama
State Program
4
41450
06-30-18
Arkansas DEQ
State Program
6
88-0692
02-01-19
California
State Program
9
2939
06-30-18
Colorado
State Program
8
N/A
12-31-18
Connecticut
State Program
1
PH-0161
03-31-19
Florida
NELAP
4
E87052
06-30-18
GA Dept. of Agriculture
State Program
4
N/A
06-12-18
Georgia
State Program
4
803
06-30-18
Guam
State Program
9
15-005r
04-16-18
Hawaii
State Program
9
N/A
06-30-18
Illinois
NELAP
5
200022
11-30-18
Indiana
State Program
5
N/A
06-30-18
Iowa
State Program
7
353
06-30-19
Kentucky (DW)
State Program
4
90084
12-31-18
Kentucky (UST)
State Program
4
18
06-30-18
Kentucky (WW)
State Program
4
90084
12-31-18
Louisiana
NELAP
6
30690
06-30-18
Louisiana (DW)
NELAP
6
LA160019
12-31-18
Maine
State Program
1
GA00006
09-24-18
Maryland
State Program
3
250
12-31-18
Massachusetts
State Program
1
M-GA006
06-30-18
Michigan
State Program
5
9925
06-30-18
Mississippi
State Program
4
N/A
06-30-18
Nebraska
State Program
7
TestAmerica-Savannah
06-30-18
New Jersey
NELAP
2
GA769
06-30-18
New Mexico
State Program
6
N/A
06-30-18
New York
NELAP
2
10842
03-31-18
North Carolina (DW)
State Program
4
13701
07-31-18
North Carolina (WW/SW)
State Program
4
269
12-31-18
Oklahoma
State Program
6
9984
08-31-18
Pennsylvania
NELAP
3
68-00474
06-30-18
Puerto Rico
State Program
2
GA00006
12-31-18
South Carolina
State Program
4
98001
06-30-18
Tennessee
State Program
4
TN02961
06-30-18
Texas
NELAP
6
T104704185-16-9
11-30-18
USDA
Federal
SAV 3-04
06-14-20
Virginia
NELAP
3
460161
06-14-18
Washington
State Program
10
C805
06-10-18
West Virginia (DW)
State Program
3
9950C
12-31-17
West Virginia DEP
State Program
3
094
06-30-18
Wisconsin
State Program
5
999819810
08-31-18
Wyoming
State Program
8
8TMS-L
06-30-16
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Savannah
Page 10 of 13 12/29/2017

Method Summary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR - Waste Water Holding Tank
TestAmerica Job ID: 680-146889-1
Method
Method Description
Protocol
Laboratory
1664B
HEM and SGT-HEM
1664B
TAL SAV
2540 D-2011
Total Suspended Solids (Dried at 103-105°C)
SM
TAL SAV
4500 H+ B-2011
pH
SM
TAL SAV
Protocol References:
1664B = 1664B
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 11 of 13 12/29/2017

W
N
N
N
0
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Phone [phone] Fax [phone]
Chain of Custody Record mulanw-M
Client Information
Sampler: �I
Haar' e—
Lob PM'
Canner, Keaton
Carrier Trucking No(s):
COG No:
680-88956-29881.1
Client Contact:
Accounts Payable
Phone:
-�7-i: Z [-A
E-Mail:
lkeaton-conner@testamericainC.00M
Page:
Page 1 of 1
Company;
Genesee 8 Wyoming, Inc.
Analysis Requested
Job
Address:
200 Meridian Centre Suite 300
Due Date Requested:
oil
}
1
+.�
y�!
S$
y
j
r 1
m
O
w
=
19
s
o
y
n
g °Other:
yi
c
$
a
=
Q
a
E
�
rs-
Preservation Codes:
A -HCL M- Hexene
B - NaOH N - None
C - Zn Acetate O - AsNaO2
D - Nitric Acid P - Na204S
E - NaHSO4 0 - Na2SO3
F - McOH R - Na2S203
G- Amchlor S-H2SO4
H -Ascorbic Add T -TSP Dodecahydrala
I - Ice tJ - Acetone
J- DIWater V-MCAA
K-EDTA W -pH 4-5
L -EDA Z-other(specify)
City:
Rochester
TAT Requested (days):
State, Zp:
NY, 14618
Phone:
757.272-4082(rel)
PO #:
Purchase Order not required
Email:
Project Name:
CA RR
WO #:
Project N: -,
68014624
2
m
W
Site:
SSOW#:
Sample Identification
Sam to Date
Sample
Time
Sample
Type
_
(C-comp,
&m rab)
Matrix
(w- W.,a-.tea
0- .M e,
er.�—n Ao-
Special Instructions/Note:
Preservation Code.
XXS,
N
N
¢
Water
f
Water
680-146889
Chain
of Custody
-4-
Possible Hazard Identilcation
= Non -Hazard 0 Flammable Skin trritant = Poison B = Unknown =Radiol ical
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
"Retum To Client Disposal By Lab =Archive For Months
Deliverable Requested: I, II, lit, IV, Other (specify)
Special Instructions/QC Requirements:
Empty Kit Relinquished by: Date: Time: Method of Shipment:
Relinquished by:
Date/Time:
Company
Received by:
Date/Time:
Company
Relinquished by:
Oate/rime:
Company
Received by:
Date/Tine:
Company
RelingoShad by:
Datemms:
Company
Receive tl by:
Date/TIm
z i5 / 7 j / : ! 8
Company
74
Custody Seals Intact:
AYes ANo©3
Custody Seal No.:
Cooler TempsraEws(s) °C and er Remarks:
1- de Qot_
r� Ver:08:04'201b

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 146889
List Number: 1
Creator: Johnson, Jessica R
Question
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Answer
N/A
True
True
True
True
True
True
True
True
False
True
True
True
True
True
True
True
True
True
True
N/A
True
True
N/A
Job Number: 680-146889-1
List Source: TestAmerica Savannah
Comment
Refer to Job Narrative for details.
F12
TestAmerica Savannah
Page 13 of 13 12/29/2017

July 24, 2017
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080759
Dear Sir :
a Genesee & Wyoming Company
RAF UV- � t�
JUG 21 Z017
C:`f . . ti1LES
D\rV R 1,EC fION
Please find enclosed our DMR for the first half of 2017. We are sampled from the holding tank that we
utilize to pump storm waters that are collected in the locomotive inspection/parking area of the yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
Jason Woods
General Manager
Chesapeake & Albemarle Railroad • 214 Railroad Street North • Ahoskie, NC 27910 • 252-332-2778 Fax [phone]

Semi-annual Stormwater Discharge Monitoring Report
-for North Carolina Division of Water Quality General Permit No. NCG080000
CERTIFICATE OF COVERAGE NO. NCG080759
FACILITY NAME: C & A Railroad
COUNTY: Pasquotank
PERSON COLLECTING SAMPLES:
LABORATORY:
Comments on sample collection or analysis:
Date submitted: July 24, 2017
SAMPLE COLLECTION YEAR: 2017
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
❑Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _x_ yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
® No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

STbRM EVENT CHARACTERISTICS: All collected waters are held in storage tank until sampled and discharged
Date (first event sampled)
Total Event Precipitation (inches): NA
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copv of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
-7-2-4- l-7
(Date)
Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/`npdessw#tab-4
SWU-250 last revised April 11, 2013
Page 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted 11/08/2016
CERTIFICATE OF COVERAGE NO. NCG080759
FACILITY NAME: Chesapeake & Albemarle Railroad
COUNTY: Pasquotank
PERSON COLLECTING SAMPLES: Jeff Moore
LABORATORY: Test America Lab Cert. # 269
Comments on sample collection or analysis: Sample collected from SW
SAMPLE COLLECTION YEAR: 2016
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ❑ Monthly' (month)
���ppDISSC DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
1 1l ❑Zero -flow ❑Water Supply ❑SA
NOV 14. 2016 ®other: SC
Holding tank CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4
DVVR 5Ei TION
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
50 or 100 see permit
Within 6.0 — 9.0
15
-
001
10/13/2016
18
7.9
2.8
103
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfal I
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
-
15
50 or 100 see permit
6.0 — 9.0
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here,
SWU-250 last revised April 11, 2013
pave 1 of 7.

_ vp
STORM EVENT CHARACTERISTICS:
Date: *NA (first event sampled) *Sampled from holding tank
Total Event Precipitation (inches):
Date: NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
o A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
* TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one coov of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
11-lo -Ib
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-250
last revised April 11, 2013
Paee 2 of 2

4., A
9<3eE M�p�PV�
a Genesee 6 Wyoming Company
July 30, 2015
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: DMR/NCG080759
Dear Sir :
RECEIVE®
AUG 0 3 2015
CENTRAL FILES
DWR SECTION
Please find enclosed our DMR for the first half of 2015. We are sampled from the holding tank that we
utilize to pump storm waters that are collected in the locomotive inspection/parking area of the yard.
Should you require additional information, please feel free to contact me at 252-332-2778.
Sincerely,
. "" �'
Jason Woods
General Manager
Chesapeake & Albemarle Railroad Co., Inc. 21.4 Railroad St. North Ahoskie, NC 27910
252-332-2778 Fax:[phone]

1
TestAmenca
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-114060-1
Client Project/Site: CA RR
For:
Genesee & Wyoming, Inc.
Railroad Company, Inc
200 Meridian Centre
Suite 300
Rochester, New York 14618
Attn: Mr. Aaron Blake
Authorized for release by.
711512015 12:12:41 PM
Lisa Harvey, Project Manager II,
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Qualifiers
1
TestAmerica Job ID: 680-114060 1
IM
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
o Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 2 of 13 7/15/2015

Sample Summary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
1,
TestAmerica Job ID: 680-114060-1
Lab Sample ID Client Sample ID Matrix Collected Received
680-114060-1 Waste Water Holding Tank Water 06/30/15 14:00 07/01/15 09:45
'Y
TestAmerica Savannah
Page 3 of 13 7/15/2015

Case Narrative
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Job ID: 680-114060-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: Genesee & Wyoming, Inc.
Project: CA RR
Report Number: 680-114060-1
TestAmerica Job ID: 680-114060-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 07/01/2015; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.9 C.
OIL AND GREASE AND TPH
Sample Waste Water Holding Tank (680-114060-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The
samples were prepared and analyzed on 07/10/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water Holding Tank (680-114060-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 07/01/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
1
CORROSIVITY (PH)
Sample Waste Water Holding Tank (680-114060-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 07/01/2015.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
TestAmerica Savannah
Page 4 of 13 7/15/2015

Client Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Client Sample ID: Waste Water Holding Tank
Date Collected: 06/30/15 14:00
Date Received: 07/01/15 09:45
General Chemistry
Analyte Result Qualifier
HEM (Oil & Grease) 12
Total Suspended Solids 24
pH 6.85 HF
RL
5.0
5.0
MDL Unit
1.4 mg/L
5.0 mg/L
SU
TestAmerica Job ID: 680-114060-1 `
Lab Sample ID: 680-114060-1
Matrix: Water
D Prepared Analyzed Dil Fac
07/10/15 08:03 07/10/15 12:28 1
07/01 /15 12:26 1
07/01 /15 12:57 1
TestAmerica Savannah
Page 5 of 13
7/15/2015

Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Method: 1664A - HEM and SGT-HEM
Lab Sample ID: MB 680-390989/21-A
Matrix: Water
Analysis Batch: 391049
QC Sample Results
TestAmerica Job ID: 680-114060-1
Client Sample ID: Method Blank
Prep Type: Total/NA -
Prep Batch: 390989
MB MB u
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM (Oil & Grease) <5.0 5.0 1.4 mg/L 07/10/15 08:03 07/10/15 12:28 1 °
Lab Sample ID: LCS 680-390989/22-A
Matrix: Water
Analysis Batch: 391049
Analyte
HEM (Oil & Grease)
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 390989
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
40.0 34.0 mg/L 85 78 -114 -
Lab Sample ID: LCSD 680-390989123-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391049 Prep Batch: 390989
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
HEM (Oil & Grease) 40.0 35.0 mg/L 88 78 -114 3 18
Method: 2540 D-2011 - Total Suspended Solids Dried at 103-105°C
Lab Sample ID: MB 680-389905/1
Matrix: Water
Analysis Batch: 389905
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <1.0 1.0 1.0 mg/L 07/01/15 10:58 1
Lab Sample ID: LCS 680-389905/2
Matrix: Water
Analysis Batch: 389905
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-389905/3
Matrix: Water
Analysis Batch: 389905
Analyte
Total Suspended Solids
Lab Sample ID: 680-114060-1 DU
Matrix: Water
Analysis Batch: 389905
Sample Sample
Analyte Result Qualifier
Total Suspended Solids 24
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 16.5 mg/L 83 80 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 16.5 mg/L 83 80 -120 0 25
Client Sample ID: Waste Water Holding Tank
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
24.5 mg/L 2 5
TestAmerica Savannah
Page 6 of 13 7/15/2015

Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
QC Sample Results ! T
TestAmerica Job ID: 680-114060-1
Method: 4500 H+ B-2011 - pH
Lab Sample ID: LCS 680-389935/7 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 389935
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7.00 7.070 SU 101 63 -158
TestAmerica Savannah
Page 7 of 13 7/15/2015

QC Association Summary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
General Chem
TestAmerica Job ID: 680-114060-1 Jul
Analysis Batch: 389905
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-114060-1
Waste Water Holding Tank
Total/NA
Water
2540 D-2011
680-114060-1 DU
Waste Water Holding Tank
Total/NA
Water
2540 D-2011
LCS 680-389905/2
Lab Control Sample
Total/NA
Water
2540 D-2011
LCSD 680-389905/3
Lab Control Sample Dup
Total/NA
Water
2540 D-2011
MB 680-389905/1
Method Blank
Total/NA
Water
2540 D-2011
Analysis Batch: 389935
Lab Sample ID Client Sample ID Prep Type Matrix Method
680-114060-1 Waste Water Holding Tank Total/NA Water 4500 H+ B-2011
LCS 680-389935/7 Lab Control Sample Total/NA Water 4500 H+ B-2011
Prep Batch: 390989
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-114060-1
Waste Water Holding Tank
Total/NA
Water
1664A
LCS 680-390989/22-A
Lab Control Sample
Total/NA
Water
1664A
LCSD 680-390989/23-A
Lab Control Sample Dup
Total/NA
Water
1664A
MB 680-390989/21-A
Method Blank
Total/NA
Water
1664A
Analysis Batch: 391049
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-114060-1
Waste Water Holding Tank
Total/NA
Water
1664A
390989
LCS 680-390989/22-A
Lab Control Sample
Total/NA
Water
1664A
390989
LCSD 680-390989/23-A
Lab Control Sample Dup
Total/NA
Water
1664A
390989
MB 680-390989/21-A
Method Blank
Total/NA
Water
1664A
390989
TestAmerica Savannah
Page, 8 of 13 7/15/2015

Lab Chronicle
Client: Genesee & Wyoming, Inc.
TestAmerica Job ID: 680-114060-1
Project/Site: CA RR
Client Sample ID: Waste Water Holding Tank
Lab Sample ID: 680-114060-1
Date Collected: 06/30/15 14:00
Matrix: Water
Date Received: 07/01/15 09:45
Batch Batch Dil Initial Final
Batch
Prepared
Prep Type Type Method Run Factor Amount Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 1664A 503 mL 500 mL
390989
07/10/15 08:03
MKA TAL SAV
Total/NA Analysis 1664A 1 503 mL 500 mL
391049
07/10/15 12:28
MKA TAL SAV
Instrument ID: NOEQUIP
I I
Total/NA Analysis 2540 D-2011 1 200 mL 1000 mL
389905
07/01/15 12:26
LBH TAL SAV
Instrument ID: NOEQUIP
e
Total/NA Analysis 4500 H+ B-2011 1
389935
07/01/15 12:57
LBH TAL SAV
Instrument ID: MANTECH
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 9 of 13 7/15/2015

Certification Summary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
r--I
TestAmerica Job ID: 680-114060-1
Authority
Program
EPA Region
Certification ID
Expiration Date
A21-A
DoD ELAP
399.01
02-28-17
A2LA
ISO/IEC 17025
399.01
02-28-17
Alabama
State Program
4
41450
06-30-15
Arkansas DEQ
State Program
6
88-0692
01-31-16
California
State Program
9
2939
07-31-16
Colorado
State Program
8
N/A
12-31-15
Connecticut
State Program
1
PH-0161
03-31-17
Florida
NELAP
4
E87052
06-30-16
GA Dept. of Agriculture
State Program
4
N/A
06-12-17
Georgia
State Program
4
N/A
06-30-16
Guam
State Program
9
14-004r
04-16-16
Hawaii
State Program
9
N/A
06-30-16
Illinois
NELAP
5
200022
11-30-15
Indiana
State Program
5
N/A
06-30-15
Iowa
State Program
7
353
06-30-17
Kentucky (DW)
State Program
4
90084
12-31-15
Kentucky (UST)
State Program
4
18
06-30-16
Kentucky (WW)
State Program
4
90084
12-31-15
Louisiana
NELAP
6
30690
06-30-15
Louisiana.(DW)
NELAP
6
LA150014
12-31-15
Maine
State Program
1
GA00006
09-24-16
Maryland
State Program
3
250
12-31-15
Massachusetts
State Program
1
M-GA006
06-30-16
Michigan
State Program
5
9925
06-30-15 *
Mississippi
State Program
4
N/A
06-30-15 *
Montana
State Program
8
CERT0081
12-31-15
Nebraska
State Program
7
TestAmerica-Savannah
06-30-15 *
New Jersey
NELAP
2
GA769
09-30-15
New Mexico
State Program
6
N/A
06-30-15 *
New York
NELAP
2
10842
03-31-16
North Carolina (DW)
State Program
4
13701
07-31-15 *
North Carolina (WW/SW)
State Program
4
269
12-31-15
Oklahoma
State Program
6
9984
08-31-15
Pennsylvania
NELAP
3
68-00474
06-30-16
Puerto Rico
State Program
2
GA00006
12-31-15
South Carolina
State Program
4
98001
06-30-15
Tennessee
State Program
4
TN02961
06-30-16
Texas
NELAP
6
T104704185-14-7
11-30-15
USDA
Federal
SAV 3-04
06-11-17
Virginia
NELAP
3
460161
06-14-16
Washington
State Program
10
C805
06-10-16
West Virginia (DW)
State Program
3
9950C
12-31-15
West Virginia DEP
State Program
3
094
06-30-16
Wisconsin
State Program
5
999819810
08-31-15
Wyoming
State Program
8
8TMS-L
06-30-15
* Certification renewal pending - certification considered valid.
TestAmerica Savannah
Page 10 of 13 7/15/2015

Method Summary
Client: Genesee & Wyoming, Inc.
TestAmerica Job
ID: 680-114060-1
Project/Site: CA RR
Method Method Description
Protocol
Laboratory
1664A HEM and SGT-HEM
1664A
TAL SAV
2540 D-2011 Total Suspended Solids Dried at 103-105°C
SM
TAL SAV
4500 H+ B-2011 pH
SM
TAL SAV
Protocol References:
1664A = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 11 of 13 7/15/2015

Serial Number 85544
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
(,'5<—}est4merica savannah Website: www.testamericainc.com
'14102 LaRoche Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
Alternate Laboratory Name/Location
Phone:
Fax:
PROJECT REFERENCE
2
PROJECT NO.
01
PROJECT LOCATION
(STATE)
MATRIX
TYPE
REQUIRED ANALYSIS
PAGE
OF
TAL ( B) PROJECT MANAGER
P
h, C-V4 5 Pry
P.O. NUMBER
CONTRACT NO.
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�(
STANDARD REPORT
DELIVERY
DATE DUE
EXPEDITED REPORT O
DELIVERY
(SURCHARGE)
DATE DUE
CLIENT (SITE) M
�1Ake
CLIENT PHONE
CLIENT FAX
CLIENT NAME
C4A ��
CLIENT E-MAIL
CLIENTADDRESS
t, m r-o c-Z s� .s c a~�9 o
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F
=
NUMBER OF COOLERS SUBMITTED
PER SHIPMENT:
COMPANY CONTRACTING THIS WORK (if applicable)
SAMPLE
SAMPLE IDENTIFICATION
o
0
NUMBER
OF
CONTAINERS
SUBMITTED
REMARKS
DATE
TIME
3 0 -OS
140
� w � �-. � �.►
i
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�
680-114060 Chain of Custody
TIME RELINQUISHED BY: (SIGNATURE) DATE TIME
fie '
RELINQUIS BY: (SIGNATURE)
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DATE
- d T
TIME
A400
REL QUISF ED BY IGN -
E)
DAT
RECZn. SIGNA E)
DATE
TIME
91ECEIVED BY: (SIG RE)
DATE
TIME
RECEIVED BY: (SIGNATURE)
DATE
TIME
LABORATORY USE ONLY
ECEIVED FOR LABORATORY BY:
SIGNATU E)
DAT
/
TIME
�s
CUSTODY INTACT
ES
Y�
NO Q
CUSTODY
SEAL N0.
SAVANNAH
�OGG N0. %
y—, - 1 / c1 � `�
LABORATORY REMARKS
r �'% L �-
1
- TAL8240.660 (1008)
d - --9 - IJ L

Client: Genesee & Wyoming, Inc.
Login Number: 114060
List Number: 1
Creator: Kicklighter, Marilyn D
Question
'T
Login Sample Receipt Checklist
Job Number: 680-114060-1
List Source: TestAmerica Savannah
a
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Savannah
Page 13 of 13 7/15/2015

r nt
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted July 29, 2015
CERTIFICATE OF COVERAGE NO. NCG08 0 7 5 9 SAMPLE/COLLECTIO YEAR 2015
FACILITY NAME Chesapeake & Albermarle RR SAMPLE PERIOD gJan-June ❑ July -Dec
COUNTY Pasquotank or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES Aaron Blake DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY TestAmerica Lab Cert. # 269 ❑Zero -flow ❑Water Supply [:]SA
Comments on sample collection or analysis: ❑Other
Sample collected from Holding Tank
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? !/yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period'
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00530
00400
00556
Total Suspended
Solids, mg/L
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method 1664 (SGT-HEM), mg/L
New Motor Oil Usage,
Annual average gal/mo
Benchmark.
-
50 or 100 see permit
Within 6.0 —9.0
15,
001
1 06/30/2015
24
6.85
12
62
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No.
Date
Sample Collected,
mo/dd/yr
06556
00536
00406
Non -Polar Oil and Grease/TPH EPA Method
1664_(SGT-HEM), mg/L
Total Suspended Solids,
mg/L
pH,
Standard units
Permit Limit
15
50 or 100 see permit
6.0-9.0
t For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of

STORM EVENT CHARACTERISTICS:
Date 'NA (first event sampled) Collected from Holding Tank
Total Event Precipitation (inches):
Date NA (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in
the case of "No Discharge" ieports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-250 last revised April 11, 2013
Page 2 of 2